#------------------------------------------------------------------------------ #$Date: 2024-08-05 21:07:04 +0300 (Mon, 05 Aug 2024) $ #$Revision: 293764 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/20/1572008.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572008 loop_ _publ_author_name 'Lee, Yunjeong' 'Jhun, Byung Hak' 'Woo, Sihyun' 'Kim, Seoyeon' 'Bae, Jaehan' 'You, Youngmin' 'Cho, Eun Jin' _publ_section_title ; Charge-recombinative triplet sensitization of alkenes for DeMayo-type [2 + 2] cycloaddition. ; _journal_issue 30 _journal_name_full 'Chemical science' _journal_page_first 12058 _journal_page_last 12066 _journal_paper_doi 10.1039/d4sc02601b _journal_volume 15 _journal_year 2024 _chemical_formula_sum 'C27 H17 N O' _chemical_formula_weight 371.42 _chemical_melting_point 477 _chemical_name_systematic A _chemical_properties_physical Light-sensitive,Photo-sensitive _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2017/1 _audit_update_record ; 2022-12-08 deposited with the CCDC. 2024-06-27 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 115.935(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.908(4) _cell_length_b 5.7056(12) _cell_length_c 19.221(4) _cell_measurement_temperature 296(2) _cell_volume 1864.8(7) _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.3484 _diffrn_reflns_av_unetI/netI 0.1215 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 5 _diffrn_reflns_limit_k_min -5 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 27647 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 21.911 _diffrn_reflns_theta_max 21.911 _diffrn_reflns_theta_min 1.260 _exptl_absorpt_coefficient_mu 0.080 _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.323 _exptl_crystal_F_000 776 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: methanol' _exptl_crystal_size_max 0.900 _exptl_crystal_size_mid 0.300 _exptl_crystal_size_min 0.200 _refine_diff_density_max 0.254 _refine_diff_density_min -0.265 _refine_diff_density_rms 0.063 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.699 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 262 _refine_ls_number_reflns 2228 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.699 _refine_ls_R_factor_all 0.2695 _refine_ls_R_factor_gt 0.2381 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.5855P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2681 _refine_ls_wR_factor_ref 0.2947 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1696 _reflns_number_total 2228 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc02601b2.cif _cod_data_source_block LYJ1044_0m _cod_depositor_comments 'Adding full bibliography for 1572008.cif.' _cod_original_cell_volume 1864.7(7) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1572008 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.931 _shelx_estimated_absorpt_t_max 0.984 _shelx_res_file ; TITL LYJ1044_0m_a.res in P2(1)/n LYJ1044_0m.res created by SHELXL-2017/1 at 20:52:10 on 24-Jun-2022 CELL 0.71073 18.9082 5.7056 19.2206 90.000 115.935 90.000 ZERR 4.00 0.0040 0.0012 0.0042 0.000 0.003 0.000 LATT 1 SYMM -x+1/2, y+1/2, -z+1/2 SFAC C H N O UNIT 108 68 4 4 L.S. 4 ACTA BOND $H FMAP 2 PLAN 5 SIZE 0.200 0.300 0.900 HTAB CONF TEMP 23.000 WGHT 0.100000 0.585504 FVAR 0.54979 O1 4 0.585529 0.635738 0.950237 11.00000 0.07385 0.11851 = 0.03588 -0.02534 0.02071 -0.00649 N1 3 0.570413 0.594137 0.825017 11.00000 0.04412 0.07037 = 0.02678 -0.00966 0.01216 0.00476 C1 1 0.335581 -0.298091 0.864477 11.00000 0.07994 0.07406 = 0.09678 0.02268 0.06201 0.01092 AFIX 43 H1 2 0.313605 -0.387651 0.890467 11.00000 -1.20000 AFIX 0 C2 1 0.321384 -0.358002 0.788967 11.00000 0.08178 0.06610 = 0.08906 0.00586 0.06119 0.00894 AFIX 43 H4 2 0.290392 -0.487309 0.764861 11.00000 -1.20000 AFIX 0 C3 1 0.353388 -0.225136 0.750929 11.00000 0.07437 0.05470 = 0.05994 -0.00347 0.04511 0.00504 AFIX 43 H5 2 0.342655 -0.263629 0.700262 11.00000 -1.20000 AFIX 0 C4 1 0.402089 -0.031847 0.786029 11.00000 0.04602 0.05479 = 0.03850 0.00676 0.02366 0.01836 C5 1 0.437317 0.101367 0.747051 11.00000 0.05430 0.06438 = 0.03086 0.00421 0.02648 0.01056 AFIX 43 H3 2 0.427646 0.063138 0.696639 11.00000 -1.20000 AFIX 0 C6 1 0.485195 0.284843 0.783476 11.00000 0.03775 0.05685 = 0.03362 0.00524 0.01665 0.00680 C7 1 0.529159 0.450254 0.760671 11.00000 0.03938 0.06165 = 0.02909 -0.00249 0.01601 0.00641 C8 1 0.546448 0.518981 0.701540 11.00000 0.03512 0.04801 = 0.03578 -0.00080 0.01370 0.00311 C9 1 0.520329 0.413601 0.624947 11.00000 0.04211 0.05341 = 0.03097 0.00556 0.01840 0.01013 C10 1 0.438712 0.322784 0.585177 11.00000 0.04570 0.05094 = 0.02012 0.00428 0.01975 0.00721 C11 1 0.421041 0.112757 0.544958 11.00000 0.06066 0.05501 = 0.04309 -0.00433 0.02595 0.00516 AFIX 43 H15 2 0.461459 0.025961 0.542379 11.00000 -1.20000 AFIX 0 C12 1 0.345509 0.029555 0.508861 11.00000 0.07327 0.07727 = 0.05196 -0.00647 0.02671 -0.01124 AFIX 43 H12 2 0.334998 -0.111279 0.481823 11.00000 -1.20000 AFIX 0 C13 1 0.285517 0.155176 0.512840 11.00000 0.05241 0.09754 = 0.04740 0.00293 0.01645 -0.01765 AFIX 43 H2 2 0.234287 0.098364 0.489156 11.00000 -1.20000 AFIX 0 C14 1 0.380882 -0.111494 0.900017 11.00000 0.06626 0.09525 = 0.05022 0.02405 0.03718 0.01684 AFIX 43 H17 2 0.388806 -0.073116 0.949926 11.00000 -1.20000 AFIX 0 C15 1 0.416610 0.027148 0.863149 11.00000 0.05236 0.06582 = 0.03806 0.01714 0.02556 0.01968 C16 1 0.466511 0.217752 0.899109 11.00000 0.05349 0.08924 = 0.02964 0.00455 0.02243 0.01781 AFIX 43 H16 2 0.476219 0.261055 0.949136 11.00000 -1.20000 AFIX 0 C17 1 0.500531 0.338601 0.860739 11.00000 0.04462 0.07349 = 0.02495 0.00452 0.01552 0.00821 C18 1 0.599786 0.715362 0.730856 11.00000 0.04305 0.05441 = 0.03723 0.00320 0.01620 0.01160 C19 1 0.635600 0.867454 0.698745 11.00000 0.04465 0.05762 = 0.04696 0.00570 0.01641 0.00505 AFIX 43 H6 2 0.626871 0.849203 0.647532 11.00000 -1.20000 AFIX 0 C20 1 0.683613 1.043524 0.742997 11.00000 0.05089 0.06511 = 0.07373 0.00659 0.02254 -0.00258 AFIX 43 H7 2 0.707325 1.143494 0.721254 11.00000 -1.20000 AFIX 0 C21 1 0.697515 1.075610 0.819084 11.00000 0.05207 0.06484 = 0.08021 -0.00884 0.01812 -0.00829 AFIX 43 H9 2 0.730989 1.195159 0.847797 11.00000 -1.20000 AFIX 0 C22 1 0.662935 0.934698 0.853056 11.00000 0.04942 0.06679 = 0.04759 -0.01943 0.00727 -0.00603 AFIX 43 H8 2 0.671476 0.956654 0.904076 11.00000 -1.20000 AFIX 0 C23 1 0.614857 0.758763 0.807900 11.00000 0.03549 0.05669 = 0.04702 -0.00313 0.01481 0.00839 C24 1 0.556240 0.537373 0.888486 11.00000 0.05142 0.07734 = 0.03375 -0.00624 0.02015 0.01086 C25 1 0.567814 0.399986 0.590444 11.00000 0.06153 0.07408 = 0.04583 -0.00307 0.03209 0.00365 AFIX 93 H10 2 0.618803 0.458237 0.615097 11.00000 -1.20000 H11 2 0.549992 0.332226 0.541691 11.00000 -1.20000 AFIX 0 C26 1 0.301196 0.365525 0.551935 11.00000 0.05080 0.08846 = 0.04764 0.00706 0.02511 0.00507 AFIX 43 H13 2 0.260584 0.451490 0.554441 11.00000 -1.20000 AFIX 0 C27 1 0.377031 0.447712 0.587183 11.00000 0.05259 0.05986 = 0.04160 0.00070 0.02517 0.00518 AFIX 43 H27 2 0.387105 0.590669 0.612985 11.00000 -1.20000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM LYJ1044_0m_a.res in P2(1)/n REM R1 = 0.2381 for 1696 Fo > 4sig(Fo) and 0.2695 for all 2228 data REM 262 parameters refined using 0 restraints END WGHT 0.0000 16.3923 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 0.254, deepest hole -0.265, 1-sigma level 0.063 Q1 1 0.7009 1.1788 0.8953 11.00000 0.05 0.22 Q2 1 0.6466 1.0686 0.8885 11.00000 0.05 0.22 Q3 1 0.3980 0.6826 0.6158 11.00000 0.05 0.22 Q4 1 0.4664 0.1700 0.8224 11.00000 0.05 0.21 Q5 1 0.2427 -0.0854 0.4848 11.00000 0.05 0.20 ; _shelx_res_checksum 56457 _shelx_hkl_file ; 0 0 -1 0.09 0.14 0 0 -1 0.07 0.23 0 0 -1 1.14 0.41 0 0 -1 0.31 0.26 0 0 -1 0.09 0.14 0 0 -1 0.07 0.23 0 0 -1 1.14 0.41 0 0 -1 0.31 0.26 0 0 1 0.08 0.24 0 0 1 0.08 0.24 0 0 1 1.02 0.32 0 0 1 0.13 0.24 0 0 1 0.03 0.30 0 0 1 0.11 0.22 0 0 1 1.02 0.32 0 0 1 0.13 0.24 0 0 1 0.03 0.30 0 0 1 0.11 0.22 0 0 -2 2139.74 13.26 0 0 -2 3157.15 16.14 0 0 -2 3179.16 16.35 0 0 -2 2139.64 13.26 0 0 -2 3157.01 16.14 0 0 -2 3179.16 16.35 0 0 2 3554.96 29.41 0 0 2 3554.96 29.41 0 0 2 3219.03 16.29 0 0 2 3933.43 21.95 0 0 2 3133.34 16.21 0 0 2 3218.93 16.29 0 0 2 3933.43 21.95 0 0 2 3133.34 16.21 0 0 -3 0.19 0.63 0 0 -3 0.19 0.63 0 0 3 0.12 0.78 0 0 3 -0.62 0.65 0 0 3 0.96 0.82 0 0 3 0.12 0.78 0 0 3 -0.62 0.65 0 0 3 0.96 0.82 0 0 -4 76.48 3.72 0 0 -4 76.48 3.72 0 0 4 117.37 8.26 0 0 4 117.37 8.26 0 0 4 88.86 4.13 0 0 4 109.66 5.52 0 0 4 86.68 4.17 0 0 4 88.85 4.13 0 0 4 109.66 5.52 0 0 4 86.68 4.17 0 0 -5 -0.67 0.74 0 0 -5 -0.56 0.74 0 0 5 0.93 1.59 0 0 5 0.93 1.59 0 0 5 1.13 1.24 0 0 5 0.52 1.27 0 0 5 -2.54 1.41 0 0 5 1.13 1.24 0 0 5 0.52 1.27 0 0 5 -2.54 1.41 0 0 -6 935.41 15.32 0 0 -6 935.34 15.32 0 0 6 1324.61 31.51 0 0 6 1324.61 31.51 0 0 6 1119.61 16.87 0 0 6 1282.87 22.11 0 0 6 1099.53 16.88 0 0 6 1119.54 16.87 0 0 6 1282.87 22.11 0 0 6 1099.53 16.88 0 0 -7 1.12 1.20 0 0 -7 1.12 1.20 0 0 7 2.44 2.60 0 0 7 2.44 2.60 0 0 7 -0.08 1.63 0 0 7 1.22 2.51 0 0 7 1.60 1.75 0 0 7 -0.08 1.63 0 0 7 1.22 2.51 0 0 7 1.60 1.75 0 0 -8 174.75 7.94 0 0 -8 174.90 7.95 0 0 8 222.74 15.41 0 0 8 222.74 15.41 0 0 8 196.38 8.52 0 0 8 215.32 10.50 0 0 8 186.95 8.50 0 0 8 196.37 8.52 0 0 8 215.32 10.50 0 0 8 186.95 8.50 0 0 -9 0.48 1.43 0 0 -9 0.48 1.43 0 0 9 -1.37 3.00 0 0 9 -1.37 3.00 0 0 9 -0.97 2.21 0 0 9 0.04 2.15 0 0 9 -0.97 2.21 0 0 9 0.04 2.15 0 0 -10 14.67 3.27 0 0 -10 14.67 3.27 0 0 10 11.08 4.80 0 0 10 11.08 4.80 0 0 10 11.13 4.12 0 0 10 13.10 3.55 0 0 10 11.13 4.12 0 0 10 13.10 3.55 0 0 -11 1.25 1.80 0 0 -11 1.25 1.80 0 0 11 -2.86 2.80 0 0 11 -2.86 2.80 0 0 11 -2.74 3.74 0 0 11 1.86 3.31 0 0 11 -2.74 3.74 0 0 11 1.86 3.31 0 0 -12 20.38 4.07 0 0 -12 20.38 4.07 0 0 12 17.58 7.74 0 0 12 17.58 7.74 0 0 12 25.53 6.86 0 0 12 9.12 5.71 0 0 12 25.53 6.86 0 0 12 9.12 5.71 0 0 -13 1.37 2.43 0 0 -13 1.38 2.43 0 0 13 0.44 5.15 0 0 13 0.44 5.15 0 0 13 1.34 5.67 0 0 13 1.57 4.73 0 0 13 1.34 5.67 0 0 13 1.57 4.73 0 0 -14 7.52 3.66 0 0 -14 7.49 3.65 0 0 14 8.24 9.32 0 0 14 8.24 9.32 0 0 14 20.61 7.58 0 0 14 7.47 6.14 0 0 14 20.61 7.58 0 0 14 7.47 6.14 0 0 15 -1.27 8.06 0 0 15 -1.27 8.06 0 0 16 3.33 12.34 0 0 16 3.33 12.34 0 0 16 9.10 10.35 0 0 16 9.10 10.35 0 0 17 -10.55 16.36 0 0 17 -10.55 16.36 0 0 17 -6.37 10.07 0 0 17 -6.37 10.07 0 0 18 16.49 15.76 0 0 18 16.49 15.76 0 0 18 8.93 9.36 0 0 18 8.93 9.36 0 1 0 0.00 0.61 0 1 0 0.00 0.61 0 1 0 0.41 0.71 0 1 0 0.27 0.68 0 1 0 0.11 0.51 0 1 0 0.41 0.71 0 1 0 0.27 0.68 0 1 0 0.11 0.51 0 -1 1 52.68 4.66 0 -1 1 52.68 4.66 0 -1 1 61.75 2.80 0 -1 1 55.58 3.30 0 -1 1 51.94 2.52 0 -1 1 65.67 2.92 0 -1 1 61.76 2.80 0 -1 1 55.58 3.30 0 -1 1 51.94 2.52 0 -1 1 65.67 2.92 0 1 -1 59.29 2.63 0 1 -1 61.33 2.71 0 1 -1 59.28 2.63 0 1 -1 61.33 2.71 0 1 1 36.89 3.76 0 1 1 36.89 3.76 0 1 1 66.43 3.81 0 1 1 54.17 3.30 0 1 1 59.84 3.60 0 1 1 66.47 3.81 0 1 1 54.17 3.30 0 1 1 59.84 3.60 0 -1 2 1563.30 24.97 0 -1 2 1563.30 24.97 0 -1 2 1800.99 10.85 0 -1 2 1550.60 17.26 0 -1 2 1644.19 10.67 0 -1 2 1718.45 10.93 0 -1 2 1800.90 10.85 0 -1 2 1550.60 17.26 0 -1 2 1644.19 10.67 0 -1 2 1718.45 10.93 0 1 -2 1671.69 10.42 0 1 -2 1549.02 10.38 0 1 -2 1671.67 10.41 0 1 -2 1549.02 10.38 0 1 2 1678.51 25.43 0 1 2 1678.51 25.43 0 1 2 1593.52 18.87 0 1 2 1716.38 18.50 0 1 2 1522.73 18.39 0 1 2 1593.39 18.87 0 1 2 1716.38 18.50 0 1 2 1522.73 18.39 0 -1 3 1298.77 25.37 0 -1 3 1298.77 25.37 0 -1 3 1684.33 7.86 0 -1 3 1320.66 17.69 0 -1 3 1590.62 8.84 0 -1 3 1684.04 7.86 0 -1 3 1320.66 17.69 0 -1 3 1590.62 8.84 0 1 -3 1419.19 7.15 0 1 -3 1301.08 8.02 0 1 -3 1419.35 7.15 0 1 -3 1301.08 8.02 0 1 3 1405.98 25.93 0 1 3 1405.98 25.93 0 1 3 1335.83 18.87 0 1 3 1377.69 18.37 0 1 3 1309.99 18.68 0 1 3 1335.80 18.87 0 1 3 1377.69 18.37 0 1 3 1309.99 18.68 0 -1 -4 1167.78 18.91 0 -1 -4 1167.75 18.91 0 -1 4 1487.00 29.99 0 -1 4 1487.00 29.99 0 -1 4 1307.78 7.36 0 -1 4 1486.32 20.71 0 -1 4 1590.83 9.68 0 -1 4 1307.65 7.35 0 -1 4 1486.32 20.71 0 -1 4 1590.83 9.68 0 1 -4 1831.16 8.66 0 1 -4 1601.85 9.76 0 1 -4 1830.88 8.66 0 1 -4 1601.85 9.76 0 1 4 1657.02 31.01 0 1 4 1657.02 31.01 0 1 4 1340.17 20.30 0 1 4 1454.62 20.79 0 1 4 1329.36 20.24 0 1 4 1340.11 20.30 0 1 4 1454.62 20.79 0 1 4 1329.36 20.24 0 -1 -5 1422.23 22.27 0 -1 -5 1422.18 22.27 0 -1 5 1884.56 36.50 0 -1 5 1884.56 36.50 0 -1 5 1827.00 25.04 0 -1 5 1838.59 12.82 0 -1 5 1827.00 25.04 0 -1 5 1838.59 12.82 0 1 -5 2043.67 12.18 0 1 -5 1748.01 11.26 0 1 -5 2162.49 13.96 0 1 -5 2043.57 12.18 0 1 -5 1747.99 11.26 0 1 -5 2162.49 13.96 0 1 5 2032.68 37.42 0 1 5 2032.68 37.42 0 1 5 1701.80 24.40 0 1 5 1925.80 26.08 0 1 5 1638.75 23.99 0 1 5 1701.71 24.40 0 1 5 1925.80 26.08 0 1 5 1638.75 23.99 0 -1 -6 80.45 5.76 0 -1 -6 80.45 5.76 0 -1 6 106.02 9.82 0 -1 6 106.02 9.82 0 -1 6 109.17 6.88 0 -1 6 105.66 3.93 0 -1 6 109.17 6.88 0 -1 6 105.66 3.93 0 1 -6 101.10 3.41 0 1 -6 106.37 4.67 0 1 -6 101.09 3.41 0 1 -6 106.34 4.67 0 1 6 129.86 10.66 0 1 6 129.86 10.66 0 1 6 103.38 6.81 0 1 6 109.43 7.02 0 1 6 90.41 6.51 0 1 6 103.37 6.81 0 1 6 109.43 7.02 0 1 6 90.41 6.51 0 -1 -7 98.18 6.71 0 -1 -7 98.18 6.71 0 -1 7 120.64 11.23 0 -1 7 120.64 11.23 0 -1 7 112.76 7.70 0 -1 7 109.13 4.89 0 -1 7 112.76 7.70 0 -1 7 109.13 4.89 0 1 -7 110.24 4.18 0 1 -7 110.24 4.18 0 1 7 135.19 11.67 0 1 7 135.19 11.67 0 1 7 114.36 7.54 0 1 7 109.81 7.49 0 1 7 107.07 7.15 0 1 7 114.36 7.54 0 1 7 109.81 7.49 0 1 7 107.07 7.15 0 -1 -8 85.48 6.70 0 -1 -8 85.55 6.70 0 -1 8 124.96 12.26 0 -1 8 124.96 12.26 0 -1 8 104.47 8.36 0 -1 8 103.69 5.27 0 -1 8 104.47 8.36 0 -1 8 103.69 5.27 0 1 -8 90.75 4.34 0 1 -8 90.75 4.34 0 1 8 129.36 12.33 0 1 8 129.36 12.33 0 1 8 102.69 7.56 0 1 8 100.25 8.03 0 1 8 100.99 7.85 0 1 8 102.69 7.56 0 1 8 100.25 8.03 0 1 8 100.99 7.85 0 -1 -9 7.41 2.64 0 -1 -9 7.41 2.64 0 -1 9 -1.00 1.03 0 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2.66 1.93 -1 2 3 2.72 2.34 -1 2 3 1.70 2.43 1 -2 -3 3.06 1.48 1 -2 -3 3.06 1.48 1 2 -3 4.02 1.63 1 2 -3 3.75 1.50 1 2 -3 4.02 1.63 1 2 -3 3.75 1.50 -1 -2 2 611.18 19.15 -1 -2 2 611.18 19.15 -1 -2 2 611.46 13.33 -1 -2 2 611.46 13.33 -1 2 2 622.25 21.05 -1 2 2 622.25 21.05 -1 2 2 642.93 15.26 -1 2 2 559.69 14.37 -1 2 2 628.17 15.26 -1 2 2 642.93 15.26 -1 2 2 559.69 14.37 -1 2 2 628.17 15.26 1 -2 -2 565.53 14.15 1 -2 -2 560.82 14.20 1 -2 -2 565.50 14.15 1 -2 -2 560.82 14.20 1 2 -2 617.03 12.34 1 2 -2 630.40 11.71 1 2 -2 617.00 12.34 1 2 -2 630.40 11.71 -1 -2 1 444.75 16.06 -1 -2 1 444.75 16.06 -1 -2 1 429.12 11.06 -1 -2 1 429.12 11.06 -1 2 1 424.57 17.19 -1 2 1 424.57 17.19 -1 2 1 378.75 11.01 -1 2 1 416.09 12.07 -1 2 1 472.66 12.49 -1 2 1 378.75 11.01 -1 2 1 416.09 12.07 -1 2 1 472.66 12.49 1 -2 -1 426.09 11.53 1 -2 -1 428.40 12.19 1 -2 -1 426.07 11.53 1 -2 -1 428.40 12.19 1 2 -1 288.12 13.01 1 2 -1 288.12 13.01 1 2 -1 444.33 11.22 1 2 -1 429.40 11.12 1 2 -1 471.66 11.15 1 2 -1 444.30 11.22 1 2 -1 429.40 11.12 1 2 -1 471.66 11.15 -1 2 0 4.47 2.36 -1 2 0 4.47 2.36 -1 2 0 2.81 1.72 -1 2 0 3.58 2.08 -1 2 0 0.57 1.52 -1 2 0 2.82 1.72 -1 2 0 3.58 2.08 -1 2 0 0.57 1.52 1 -2 0 6.43 2.84 1 -2 0 6.43 2.84 1 -2 0 0.22 1.04 1 -2 0 2.25 1.70 1 -2 0 -3.20 1.40 1 -2 0 0.22 1.04 1 -2 0 2.25 1.70 1 -2 0 -3.20 1.40 1 2 0 1.04 1.22 1 2 0 1.04 1.22 1 2 0 1.69 1.58 1 2 0 2.16 1.66 1 2 0 0.81 1.48 1 2 0 1.69 1.58 1 2 0 2.16 1.66 1 2 0 0.81 1.48 -1 2 -1 8.72 3.13 -1 2 -1 8.72 3.13 -1 2 -1 3.22 1.58 -1 2 -1 3.22 1.58 1 -2 1 3.86 2.37 1 -2 1 3.86 2.37 1 -2 1 1.10 1.04 1 -2 1 0.41 1.11 1 -2 1 1.10 1.04 1 -2 1 0.41 1.11 1 2 1 2.34 1.53 1 2 1 2.34 1.53 1 2 1 -0.50 1.02 1 2 1 0.11 1.53 1 2 1 1.92 1.96 1 2 1 -0.50 1.02 1 2 1 0.11 1.53 1 2 1 1.92 1.96 -1 2 -2 521.67 9.77 -1 2 -2 521.63 9.77 1 -2 2 443.77 18.51 1 -2 2 443.77 18.51 1 -2 2 465.02 9.13 1 -2 2 445.21 12.93 1 -2 2 478.04 10.29 1 -2 2 465.02 9.13 1 -2 2 445.21 12.93 1 -2 2 478.04 10.29 1 2 2 9.02 2.17 1 2 2 9.02 2.17 1 2 2 489.63 14.08 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79.94 3.87 1 2 6 75.97 9.37 1 2 6 75.97 9.37 1 2 6 70.84 7.56 1 2 6 69.42 7.32 1 2 6 57.78 6.44 1 2 6 70.85 7.55 1 2 6 69.42 7.32 1 2 6 57.78 6.44 -1 -2 -7 -2.49 2.13 -1 -2 -7 -2.49 2.13 1 -2 7 -0.07 3.03 1 -2 7 -0.07 3.03 1 -2 7 -0.87 2.60 1 -2 7 1.26 1.52 1 -2 7 -0.87 2.60 1 -2 7 1.26 1.52 1 2 7 -1.40 3.02 1 2 7 -1.40 3.02 1 2 7 -2.31 2.91 1 2 7 -5.35 2.91 1 2 7 -2.31 2.92 1 2 7 -5.35 2.91 -1 -2 -8 65.40 7.58 -1 -2 -8 65.39 7.58 1 -2 8 65.60 10.72 1 -2 8 65.60 10.72 1 -2 8 66.91 7.63 1 -2 8 90.94 4.35 1 -2 8 66.91 7.63 1 -2 8 90.94 4.35 1 2 8 68.30 9.99 1 2 8 68.30 9.99 1 2 8 78.72 8.65 1 2 8 75.12 9.15 1 2 8 73.18 9.04 1 2 8 78.72 8.65 1 2 8 75.12 9.15 1 2 8 73.18 9.04 -1 -2 -9 1.81 2.91 -1 -2 -9 1.81 2.91 1 -2 9 12.83 5.56 1 -2 9 12.83 5.56 1 -2 9 4.30 3.43 1 -2 9 4.30 3.43 1 2 9 3.82 4.51 1 2 9 3.82 4.51 1 2 9 6.23 4.50 1 2 9 97.12 8.93 1 2 9 10.04 5.73 1 2 9 6.23 4.50 1 2 9 97.12 8.93 1 2 9 10.04 5.73 -1 -2 -10 36.45 6.72 -1 -2 -10 36.44 6.71 1 -2 10 34.66 9.06 1 -2 10 34.66 9.06 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8.05 -1 5 7 2.08 4.50 -1 5 7 0.13 8.54 -1 5 7 0.13 7.67 -1 5 7 2.08 4.50 -1 5 7 0.13 8.54 -1 5 7 0.13 7.67 1 -5 -7 -3.23 5.86 1 -5 -7 -16.39 13.39 1 -5 -7 -3.20 5.85 1 -5 -7 -16.39 13.39 -1 -5 6 26.40 14.10 -1 -5 6 26.40 14.10 -1 -5 6 3.26 6.87 -1 -5 6 3.26 6.87 -1 5 6 5.08 6.96 -1 5 6 5.08 6.96 -1 5 6 2.47 6.21 -1 5 6 8.11 9.88 -1 5 6 4.66 6.14 -1 5 6 2.47 6.21 -1 5 6 8.11 9.88 -1 5 6 4.66 6.14 1 -5 -6 3.19 6.16 1 -5 -6 -6.38 9.99 1 -5 -6 3.18 6.15 1 -5 -6 -6.38 9.99 -1 -5 5 907.06 24.27 -1 -5 5 907.06 24.27 -1 -5 5 1.20 6.93 -1 -5 5 1.20 6.93 -1 5 5 0.48 8.15 -1 5 5 0.48 8.15 -1 5 5 2.60 5.43 -1 5 5 -3.10 7.48 -1 5 5 0.55 6.20 -1 5 5 2.60 5.43 -1 5 5 -3.10 7.48 -1 5 5 0.55 6.20 1 -5 -5 -0.24 3.71 1 -5 -5 118.21 9.98 1 -5 -5 -0.25 3.70 1 -5 -5 118.21 9.98 -1 -5 4 910.93 24.24 -1 -5 4 910.93 24.24 -1 -5 4 10.92 6.77 -1 -5 4 10.92 6.77 -1 5 4 19.82 10.31 -1 5 4 19.82 10.31 -1 5 4 14.17 5.63 -1 5 4 10.84 7.33 -1 5 4 9.31 8.34 -1 5 4 14.16 5.62 -1 5 4 10.84 7.33 -1 5 4 9.31 8.34 1 -5 -4 7.46 5.76 1 -5 -4 6.67 6.40 1 -5 -4 60.47 12.91 1 -5 -4 7.46 5.75 1 -5 -4 6.67 6.40 1 -5 -4 60.47 12.91 -1 -5 3 279.34 20.03 -1 -5 3 279.34 20.03 -1 -5 3 0.98 6.13 -1 -5 3 0.98 6.13 -1 5 3 7.76 7.40 -1 5 3 7.76 7.40 -1 5 3 1.13 3.75 -1 5 3 4.13 7.53 -1 5 3 4.12 5.69 -1 5 3 1.13 3.75 -1 5 3 4.13 7.53 -1 5 3 4.12 5.69 1 -5 -3 5.46 5.31 1 -5 -3 5.03 5.16 1 -5 -3 120.25 14.83 1 -5 -3 5.47 5.31 1 -5 -3 5.03 5.16 1 -5 -3 120.25 14.83 -1 -5 2 -12.82 8.71 -1 -5 2 -12.82 8.71 -1 -5 2 6.26 6.04 -1 -5 2 6.26 6.04 -1 5 2 5.97 7.59 -1 5 2 5.97 7.59 -1 5 2 6.94 5.24 -1 5 2 6.69 8.25 -1 5 2 8.09 6.68 -1 5 2 6.94 5.24 -1 5 2 6.69 8.25 -1 5 2 8.09 6.68 1 -5 -2 -2.53 14.68 1 -5 -2 -2.53 14.68 1 -5 -2 4.05 4.61 1 -5 -2 12.28 7.39 1 -5 -2 52.35 10.72 1 -5 -2 4.09 4.61 1 -5 -2 12.28 7.39 1 -5 -2 52.35 10.72 -1 -5 1 -0.18 3.98 -1 -5 1 4.77 6.57 -1 -5 1 57.66 10.68 -1 -5 1 -0.18 3.99 -1 -5 1 4.77 6.57 -1 -5 1 57.66 10.68 -1 5 1 1.50 6.27 -1 5 1 1.50 6.27 -1 5 1 1.41 3.66 -1 5 1 6.28 7.30 -1 5 1 0.89 5.16 -1 5 1 1.43 3.66 -1 5 1 6.28 7.30 -1 5 1 0.89 5.16 1 -5 -1 61.58 15.35 1 -5 -1 61.58 15.35 1 -5 -1 -0.86 3.84 1 -5 -1 12.66 7.29 1 -5 -1 34.79 9.24 1 -5 -1 -0.85 3.82 1 -5 -1 12.66 7.29 1 -5 -1 34.79 9.24 1 5 -1 -0.16 5.17 1 5 -1 -0.16 5.17 -1 -5 0 -29.87 10.83 -1 -5 0 -29.87 10.83 -1 -5 0 4.69 4.81 -1 -5 0 4.53 5.64 -1 -5 0 42.00 8.78 -1 -5 0 4.69 4.81 -1 -5 0 4.53 5.64 -1 -5 0 42.00 8.78 -1 5 0 3.04 5.49 -1 5 0 3.04 5.49 -1 5 0 7.42 5.54 -1 5 0 7.43 5.54 1 -5 0 -3.77 11.00 1 -5 0 -3.77 11.00 1 -5 0 3.15 4.17 1 -5 0 4.52 5.88 1 -5 0 51.14 9.42 1 -5 0 3.15 4.17 1 -5 0 4.52 5.88 1 -5 0 51.14 9.42 1 5 0 -4.44 4.40 1 5 0 -4.44 4.40 1 5 0 0.22 4.97 1 5 0 0.40 4.98 1 5 0 0.54 5.46 1 5 0 0.22 4.97 1 5 0 0.40 4.98 1 5 0 0.54 5.46 -1 -5 -1 -13.67 8.63 -1 -5 -1 -13.67 8.63 -1 -5 -1 -4.63 4.14 -1 -5 -1 1.93 5.98 -1 -5 -1 12.63 10.97 -1 -5 -1 -4.63 4.14 -1 -5 -1 1.93 5.98 -1 -5 -1 12.63 10.97 1 -5 1 -22.59 12.70 1 -5 1 -22.59 12.70 1 -5 1 2.96 6.05 1 -5 1 2.96 6.05 1 5 1 -1.85 2.74 1 5 1 -1.85 2.74 1 5 1 -0.74 5.44 1 5 1 -0.28 5.90 1 5 1 3.99 5.89 1 5 1 -0.74 5.43 1 5 1 -0.28 5.90 1 5 1 3.99 5.89 -1 -5 -2 -24.06 11.74 -1 -5 -2 -24.06 11.74 -1 -5 -2 8.24 5.64 -1 -5 -2 3.22 5.76 -1 -5 -2 190.36 11.85 -1 -5 -2 8.23 5.64 -1 -5 -2 3.22 5.76 -1 -5 -2 190.36 11.85 1 -5 2 2086.22 58.81 1 -5 2 2086.22 58.81 1 -5 2 10.98 6.23 1 -5 2 10.98 6.23 1 5 2 2.61 4.19 1 5 2 2.61 4.19 1 5 2 12.53 7.17 1 5 2 1.72 6.54 1 5 2 5.72 6.48 1 5 2 12.54 7.17 1 5 2 1.72 6.54 1 5 2 5.72 6.48 -1 -5 -3 6.95 5.20 -1 -5 -3 10.67 6.40 -1 -5 -3 6.95 5.19 -1 -5 -3 10.67 6.40 1 -5 3 325.52 23.43 1 -5 3 325.52 23.43 1 -5 3 4.90 6.66 1 -5 3 4.90 6.66 1 5 3 4.11 4.81 1 5 3 4.11 4.81 1 5 3 0.34 6.04 1 5 3 8.84 7.88 1 5 3 7.64 7.09 1 5 3 0.34 6.03 1 5 3 8.84 7.88 1 5 3 7.64 7.09 -1 -5 -4 21.76 8.21 -1 -5 -4 137.04 13.46 -1 -5 -4 21.70 8.19 -1 -5 -4 137.04 13.46 1 -5 4 990.82 27.61 1 -5 4 990.82 27.61 1 -5 4 25.27 8.22 1 -5 4 25.27 8.22 1 5 4 17.31 8.00 1 5 4 17.31 8.00 1 5 4 31.72 9.36 1 5 4 23.11 8.50 1 5 4 32.28 10.27 1 5 4 31.72 9.36 1 5 4 23.11 8.50 1 5 4 32.28 10.27 -1 -5 -5 1.24 5.97 -1 -5 -5 118.73 13.74 -1 -5 -5 1.27 5.97 -1 -5 -5 118.73 13.74 1 -5 5 974.66 27.54 1 -5 5 974.66 27.54 1 -5 5 6.55 7.31 1 -5 5 6.55 7.31 1 5 5 8.08 7.26 1 5 5 8.08 7.26 1 5 5 6.84 7.36 1 5 5 4.08 8.70 1 5 5 -0.62 8.10 1 5 5 6.84 7.36 1 5 5 4.08 8.70 1 5 5 -0.62 8.10 -1 -5 -6 11.33 6.69 -1 -5 -6 12.91 9.92 -1 -5 -6 11.31 6.67 -1 -5 -6 12.91 9.92 1 -5 6 61.89 18.95 1 -5 6 61.89 18.95 1 -5 6 13.43 8.14 1 -5 6 13.43 8.14 1 5 6 14.99 9.43 1 5 6 14.99 9.43 1 5 6 11.03 6.56 1 5 6 23.88 10.35 1 5 6 16.16 8.72 1 5 6 11.02 6.56 1 5 6 23.88 10.35 1 5 6 16.16 8.72 -1 -5 -7 -4.81 6.14 -1 -5 -7 -17.98 12.38 -1 -5 -7 -4.74 6.13 -1 -5 -7 -17.98 12.38 1 -5 7 496.83 25.13 1 -5 7 496.83 25.13 1 -5 7 0.97 6.85 1 -5 7 0.97 6.85 1 5 7 -2.33 7.04 1 5 7 -2.33 7.04 1 5 7 4.22 5.73 1 5 7 4.36 9.31 1 5 7 -6.65 8.85 1 5 7 4.22 5.72 1 5 7 4.36 9.31 1 5 7 -6.65 8.85 -1 -5 -8 -5.77 6.85 -1 -5 -8 -13.12 13.85 -1 -5 -8 -5.76 6.84 -1 -5 -8 -13.12 13.85 1 -5 8 -9.68 11.25 1 -5 8 -9.68 11.25 1 -5 8 -0.13 8.44 1 -5 8 -0.13 8.44 1 5 8 -3.01 7.90 1 5 8 -3.01 7.90 1 5 8 2.71 7.46 1 5 8 -5.67 10.56 1 5 8 -6.27 10.24 1 5 8 2.71 7.47 1 5 8 -5.67 10.56 1 5 8 -6.27 10.24 -1 -5 -9 -14.05 6.41 -1 -5 -9 -21.60 14.78 -1 -5 -9 -14.02 6.40 -1 -5 -9 -21.60 14.78 1 -5 9 -37.52 16.23 1 -5 9 -37.52 16.23 1 -5 9 11.25 8.63 1 -5 9 11.25 8.63 1 5 9 1.46 6.31 1 5 9 1.46 6.31 1 5 9 3.88 8.03 1 5 9 1.02 10.49 1 5 9 -8.92 10.90 1 5 9 3.88 8.03 1 5 9 1.02 10.49 1 5 9 -8.92 10.90 -2 0 18 17.84 19.82 -2 0 18 17.84 19.82 -2 0 18 195.56 15.88 -2 0 18 195.56 15.88 -2 0 17 6.04 11.18 -2 0 17 6.04 11.18 -2 0 17 157.87 11.64 -2 0 17 157.87 11.64 -2 0 16 6.47 13.44 -2 0 16 6.47 13.44 -2 0 16 21.80 9.26 -2 0 16 21.80 9.26 -2 0 15 -10.14 4.57 -2 0 15 -10.14 4.57 -2 0 15 0.92 4.99 -2 0 15 -1.86 6.02 -2 0 15 0.92 4.99 -2 0 15 -1.86 6.02 -2 0 14 17.65 9.13 -2 0 14 17.65 9.13 -2 0 14 19.12 6.53 -2 0 14 17.05 5.45 -2 0 14 19.12 6.53 -2 0 14 17.05 5.45 2 0 -14 22.82 3.97 2 0 -14 -5.10 4.29 2 0 -14 22.82 3.97 2 0 -14 -5.10 4.29 -2 0 13 -3.14 2.80 -2 0 13 -3.14 2.80 -2 0 13 -3.26 4.53 -2 0 13 -1.61 3.92 -2 0 13 -3.26 4.53 -2 0 13 -1.61 3.92 2 0 -13 0.38 1.86 2 0 -13 -7.15 3.42 2 0 -13 0.38 1.86 2 0 -13 -7.15 3.42 -2 0 12 321.75 23.83 -2 0 12 321.75 23.83 -2 0 12 259.38 15.37 -2 0 12 235.07 11.96 -2 0 12 259.38 15.37 -2 0 12 235.07 11.96 2 0 -12 230.35 11.13 2 0 -12 185.91 10.20 2 0 -12 230.33 11.13 2 0 -12 185.91 10.20 -2 0 11 1.33 3.15 -2 0 11 1.33 3.15 -2 0 11 -0.93 3.87 -2 0 11 -1.46 2.86 -2 0 11 -0.93 3.87 -2 0 11 -1.46 2.86 2 0 -11 1.14 1.85 2 0 -11 3.85 3.14 2 0 -11 1.14 1.84 2 0 -11 3.85 3.14 -2 0 10 954.42 33.94 -2 0 10 954.42 33.94 -2 0 10 908.18 23.66 -2 0 10 761.55 17.56 -2 0 10 908.18 23.66 -2 0 10 761.55 17.56 2 0 -10 710.75 17.42 2 0 -10 720.37 17.07 2 0 -10 710.73 17.41 2 0 -10 720.37 17.07 -2 0 9 0.86 2.40 -2 0 9 0.86 2.40 -2 0 9 -0.05 2.27 -2 0 9 0.11 2.19 -2 0 9 -0.05 2.27 -2 0 9 0.11 2.19 2 0 -9 -0.19 1.04 2 0 -9 1.84 2.19 2 0 -9 -0.19 1.04 2 0 -9 1.84 2.19 -2 0 8 1402.33 35.89 -2 0 8 1402.33 35.89 -2 0 8 1374.51 24.98 -2 0 8 1101.04 18.40 -2 0 8 1374.51 24.98 -2 0 8 1101.04 18.40 2 0 -8 805.03 16.53 2 0 -8 1004.34 17.32 2 0 -8 805.00 16.53 2 0 -8 1004.34 17.32 -2 0 7 2.52 1.96 -2 0 7 2.52 1.96 -2 0 7 1.35 2.25 -2 0 7 -0.51 1.34 -2 0 7 1.35 2.25 -2 0 7 -0.51 1.34 2 0 -7 -0.01 0.76 2 0 -7 -2.72 1.05 2 0 -7 -0.01 0.76 2 0 -7 -2.72 1.05 -2 0 6 3662.53 48.99 -2 0 6 3662.53 48.99 -2 0 6 3506.29 33.55 -2 0 6 2948.76 25.64 -2 0 6 3506.29 33.55 -2 0 6 2948.76 25.64 2 0 -6 2579.18 23.97 2 0 -6 2579.18 23.97 -2 0 5 0.53 1.72 -2 0 5 0.53 1.72 -2 0 5 0.18 1.24 -2 0 5 -0.41 1.31 -2 0 5 0.18 1.24 -2 0 5 -0.41 1.31 2 0 -5 -0.75 0.37 2 0 -5 -0.75 0.37 -2 0 4 6607.21 52.24 -2 0 4 6607.21 52.24 -2 0 4 6788.27 36.68 -2 0 4 6788.27 36.68 2 0 -4 4459.58 26.03 2 0 -4 4459.58 26.03 -2 0 3 -0.01 0.76 -2 0 3 -0.01 0.76 -2 0 3 1.12 0.81 -2 0 3 1.12 0.81 2 0 -3 -0.50 0.28 2 0 -3 -0.50 0.28 -2 0 2 839.74 12.85 -2 0 2 839.74 12.85 -2 0 2 782.27 8.51 -2 0 2 858.80 11.97 -2 0 2 782.27 8.51 -2 0 2 858.80 11.97 2 0 -2 844.25 10.36 2 0 -2 844.17 10.36 -2 0 1 0.05 0.52 -2 0 1 0.05 0.52 -2 0 1 0.13 0.48 -2 0 1 0.18 0.79 -2 0 1 0.13 0.48 -2 0 1 0.18 0.79 2 0 -1 0.78 0.41 2 0 -1 0.52 0.46 2 0 -1 1.03 0.56 2 0 -1 0.78 0.41 2 0 -1 0.52 0.46 2 0 -1 1.03 0.56 -2 0 0 4662.96 20.37 -2 0 0 4662.96 20.37 2 0 0 3363.29 23.39 2 0 0 3363.29 23.39 2 0 0 5842.43 25.47 2 0 0 2230.01 14.08 2 0 0 5985.04 27.16 2 0 0 5841.11 25.47 2 0 0 2230.01 14.08 2 0 0 5985.04 27.16 2 0 1 -0.15 0.27 2 0 1 -0.15 0.27 2 0 1 -0.17 0.63 2 0 1 -0.08 0.39 2 0 1 0.13 0.57 2 0 1 -0.17 0.63 2 0 1 -0.08 0.39 2 0 1 0.13 0.57 2 0 2 223.26 9.22 2 0 2 223.26 9.22 2 0 2 203.07 5.68 2 0 2 232.96 6.89 2 0 2 228.17 6.51 2 0 2 203.06 5.68 2 0 2 232.96 6.89 2 0 2 228.17 6.51 2 0 3 1.73 1.42 2 0 3 1.73 1.42 2 0 3 -0.02 1.06 2 0 3 0.25 1.55 2 0 3 -0.82 1.25 2 0 3 -0.02 1.06 2 0 3 0.25 1.55 2 0 3 -0.82 1.25 2 0 4 11.67 3.12 2 0 4 11.67 3.12 2 0 4 19.78 2.87 2 0 4 22.24 3.51 2 0 4 20.47 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16.62 6.48 -2 2 10 15.32 6.03 2 -2 -10 26.21 5.40 2 -2 -10 26.21 5.40 -2 -2 9 25.74 6.86 -2 -2 9 25.74 6.86 -2 -2 9 29.66 5.51 -2 -2 9 29.66 5.51 -2 2 9 13.85 5.12 -2 2 9 13.85 5.12 -2 2 9 25.82 5.76 -2 2 9 23.66 6.18 -2 2 9 27.59 5.86 -2 2 9 25.82 5.76 -2 2 9 23.66 6.18 -2 2 9 27.59 5.86 2 -2 -9 17.17 4.61 2 -2 -9 18.29 5.65 2 -2 -9 17.17 4.60 2 -2 -9 18.29 5.65 2 2 -9 32.76 3.01 2 2 -9 32.76 3.01 -2 -2 8 -1.50 3.29 -2 -2 8 -1.50 3.29 -2 -2 8 -0.93 2.37 -2 -2 8 -0.93 2.37 -2 2 8 2.59 3.70 -2 2 8 2.59 3.70 -2 2 8 0.64 2.52 -2 2 8 3.50 4.32 -2 2 8 1.81 3.01 -2 2 8 0.65 2.52 -2 2 8 3.50 4.32 -2 2 8 1.81 3.01 2 -2 -8 -0.80 1.60 2 -2 -8 -2.69 3.03 2 -2 -8 -0.80 1.60 2 -2 -8 -2.69 3.03 2 2 -8 2.76 1.25 2 2 -8 2.76 1.25 -2 -2 7 123.38 12.75 -2 -2 7 123.38 12.75 -2 -2 7 95.99 7.44 -2 -2 7 95.99 7.44 -2 2 7 99.39 11.21 -2 2 7 99.39 11.21 -2 2 7 98.97 8.03 -2 2 7 94.20 8.57 -2 2 7 83.02 7.63 -2 2 7 99.03 8.03 -2 2 7 94.20 8.57 -2 2 7 83.02 7.63 2 -2 -7 82.90 7.13 2 -2 -7 72.32 7.26 2 -2 -7 82.90 7.13 2 -2 -7 72.32 7.26 2 2 -7 103.92 4.72 2 2 -7 103.92 4.72 -2 -2 6 140.28 11.34 -2 -2 6 140.28 11.34 -2 -2 6 141.08 7.86 -2 -2 6 141.08 7.86 -2 2 6 136.82 12.71 -2 2 6 136.82 12.71 -2 2 6 127.61 8.89 -2 2 6 135.64 8.68 -2 2 6 123.64 8.57 -2 2 6 127.58 8.88 -2 2 6 135.64 8.68 -2 2 6 123.64 8.57 2 -2 -6 110.87 7.99 2 -2 -6 107.39 7.08 2 -2 -6 111.08 8.00 2 -2 -6 107.39 7.08 2 2 -6 145.71 5.56 2 2 -6 145.71 5.56 -2 -2 5 362.28 16.49 -2 -2 5 362.28 16.49 -2 -2 5 376.33 11.69 -2 -2 5 312.57 5.49 -2 -2 5 376.33 11.69 -2 -2 5 312.57 5.49 -2 2 5 375.04 18.70 -2 2 5 375.04 18.70 -2 2 5 357.84 13.39 -2 2 5 324.67 12.76 -2 2 5 369.85 13.75 -2 2 5 357.82 13.39 -2 2 5 324.67 12.76 -2 2 5 369.85 13.75 2 -2 -5 319.44 12.37 2 -2 -5 311.85 12.21 2 -2 -5 319.40 12.37 2 -2 -5 311.85 12.21 2 2 -5 393.85 9.08 2 2 -5 374.52 5.87 2 2 -5 393.85 9.08 2 2 -5 374.52 5.87 -2 -2 4 31.76 5.03 -2 -2 4 31.76 5.03 -2 -2 4 74.72 5.24 -2 -2 4 74.72 5.24 -2 2 4 69.43 8.48 -2 2 4 69.43 8.48 -2 2 4 69.88 6.14 -2 2 4 77.80 6.86 -2 2 4 79.75 6.63 -2 2 4 69.88 6.14 -2 2 4 77.80 6.86 -2 2 4 79.75 6.63 2 -2 -4 72.83 5.75 2 -2 -4 63.32 6.62 2 -2 -4 72.82 5.75 2 -2 -4 63.32 6.62 2 2 -4 78.45 4.66 2 2 -4 74.29 3.68 2 2 -4 78.41 4.66 2 2 -4 74.29 3.68 -2 -2 3 6.73 2.59 -2 -2 3 6.73 2.59 -2 -2 3 30.02 3.46 -2 -2 3 30.02 3.46 -2 2 3 13.70 3.48 -2 2 3 13.70 3.48 -2 2 3 32.05 4.35 -2 2 3 24.12 3.96 -2 2 3 42.47 5.17 -2 2 3 32.05 4.35 -2 2 3 24.12 3.96 -2 2 3 42.47 5.17 2 -2 -3 26.72 3.84 2 -2 -3 27.37 4.07 2 -2 -3 26.71 3.84 2 -2 -3 27.37 4.07 2 2 -3 33.23 3.36 2 2 -3 38.30 3.14 2 2 -3 33.23 3.36 2 2 -3 38.30 3.14 -2 -2 2 140.03 8.88 -2 -2 2 140.03 8.88 -2 -2 2 117.80 5.68 -2 -2 2 117.80 5.68 -2 2 2 131.34 10.61 -2 2 2 131.34 10.61 -2 2 2 138.77 7.23 -2 2 2 126.27 7.66 -2 2 2 131.14 7.50 -2 2 2 138.77 7.23 -2 2 2 126.27 7.66 -2 2 2 131.14 7.50 2 -2 -2 124.79 6.72 2 -2 -2 117.77 6.94 2 -2 -2 124.78 6.72 2 -2 -2 117.77 6.94 2 2 -2 143.87 6.63 2 2 -2 145.59 6.15 2 2 -2 143.86 6.62 2 2 -2 145.59 6.15 -2 -2 1 23.59 3.58 -2 -2 1 23.59 3.58 -2 -2 1 39.21 3.38 -2 -2 1 39.21 3.38 -2 2 1 30.32 4.87 -2 2 1 30.32 4.87 -2 2 1 27.60 3.99 -2 2 1 41.21 4.34 -2 2 1 27.60 3.99 -2 2 1 41.21 4.34 2 -2 -1 41.72 3.82 2 -2 -1 37.26 4.11 2 -2 -1 26.80 3.90 2 -2 -1 41.72 3.82 2 -2 -1 37.26 4.11 2 -2 -1 26.80 3.90 2 2 -1 24.00 3.65 2 2 -1 24.00 3.65 2 2 -1 37.33 4.16 2 2 -1 38.32 3.67 2 2 -1 41.67 4.06 2 2 -1 37.33 4.16 2 2 -1 38.32 3.67 2 2 -1 41.67 4.06 -2 2 0 16.08 3.77 -2 2 0 16.08 3.77 -2 2 0 18.88 3.68 -2 2 0 18.88 3.68 2 -2 0 16.03 3.82 2 -2 0 16.03 3.82 2 -2 0 23.74 2.86 2 -2 0 16.64 3.45 2 -2 0 15.87 2.99 2 -2 0 23.73 2.86 2 -2 0 16.64 3.45 2 -2 0 15.87 2.99 2 2 0 16.62 3.07 2 2 0 16.62 3.07 2 2 0 20.67 3.57 2 2 0 20.39 3.02 2 2 0 21.31 3.32 2 2 0 20.67 3.57 2 2 0 20.39 3.02 2 2 0 21.31 3.32 2 -2 1 819.06 25.86 2 -2 1 819.06 25.86 2 -2 1 852.47 13.48 2 -2 1 786.90 17.65 2 -2 1 859.81 15.34 2 -2 1 852.43 13.48 2 -2 1 786.90 17.65 2 -2 1 859.81 15.34 2 2 1 842.52 21.07 2 2 1 842.52 21.07 2 2 1 896.57 18.74 2 2 1 840.74 15.25 2 2 1 879.52 18.43 2 2 1 896.52 18.74 2 2 1 840.74 15.25 2 2 1 879.52 18.43 2 -2 2 -0.18 0.68 2 -2 2 -0.18 0.68 2 -2 2 -0.41 0.56 2 -2 2 1.60 1.77 2 -2 2 2.58 1.79 2 -2 2 -0.41 0.56 2 -2 2 1.60 1.77 2 -2 2 2.58 1.79 2 2 2 -1.72 1.12 2 2 2 -1.72 1.12 2 2 2 0.03 1.35 2 2 2 -0.40 1.64 2 2 2 -6.28 2.23 2 2 2 0.03 1.35 2 2 2 -0.40 1.64 2 2 2 -6.28 2.23 2 -2 3 1.70 0.71 2 -2 3 -0.03 2.07 2 -2 3 0.79 1.53 2 -2 3 1.70 0.71 2 -2 3 -0.03 2.07 2 -2 3 0.79 1.53 2 2 3 -0.23 1.05 2 2 3 -0.23 1.05 2 2 3 -1.20 1.89 2 2 3 0.72 1.76 2 2 3 -3.84 2.53 2 2 3 -1.20 1.89 2 2 3 0.72 1.76 2 2 3 -3.84 2.53 2 -2 4 11.64 4.04 2 -2 4 11.64 4.04 2 -2 4 22.68 1.17 2 -2 4 20.44 1.38 2 -2 4 14.78 3.98 2 -2 4 17.87 2.70 2 -2 4 23.01 1.17 2 -2 4 20.44 1.38 2 -2 4 14.78 3.98 2 -2 4 17.87 2.70 2 2 4 -1.12 1.11 2 2 4 -1.12 1.11 2 2 4 19.27 4.00 2 2 4 17.64 3.59 2 2 4 16.12 4.34 2 2 4 19.27 4.00 2 2 4 17.64 3.59 2 2 4 16.12 4.34 2 -2 5 3.52 2.99 2 -2 5 3.52 2.99 2 -2 5 -0.12 1.71 2 -2 5 -4.28 1.79 2 -2 5 -0.12 1.71 2 -2 5 -4.28 1.79 2 2 5 1.46 1.72 2 2 5 1.46 1.72 2 2 5 -0.13 2.38 2 2 5 2.32 2.79 2 2 5 0.56 2.27 2 2 5 -0.13 2.38 2 2 5 2.32 2.79 2 2 5 0.56 2.27 2 -2 6 20.91 6.77 2 -2 6 20.91 6.77 2 -2 6 7.46 3.76 2 -2 6 21.97 3.03 2 -2 6 7.46 3.76 2 -2 6 21.97 3.03 2 2 6 21.90 5.09 2 2 6 21.90 5.09 2 2 6 13.56 4.13 2 2 6 19.92 4.43 2 2 6 17.21 4.58 2 2 6 13.55 4.13 2 2 6 19.92 4.43 2 2 6 17.21 4.58 2 -2 7 192.79 17.65 2 -2 7 192.79 17.65 2 -2 7 166.20 10.83 2 -2 7 206.09 7.10 2 -2 7 166.20 10.83 2 -2 7 206.09 7.10 2 2 7 242.57 16.87 2 2 7 242.57 16.87 2 2 7 183.42 12.01 2 2 7 142.28 9.76 2 2 7 184.17 11.79 2 2 7 183.42 12.01 2 2 7 142.28 9.76 2 2 7 184.17 11.79 2 -2 8 27.96 7.83 2 -2 8 27.96 7.83 2 -2 8 37.50 6.97 2 -2 8 44.47 4.35 2 -2 8 37.50 6.97 2 -2 8 44.47 4.35 2 2 8 42.40 7.93 2 2 8 42.40 7.93 2 2 8 39.94 6.38 2 2 8 127.35 9.66 2 2 8 39.67 6.92 2 2 8 39.93 6.38 2 2 8 127.35 9.66 2 2 8 39.67 6.92 -2 -2 -9 3.36 2.80 -2 -2 -9 3.36 2.80 2 -2 9 7.65 6.37 2 -2 9 7.65 6.37 2 -2 9 6.54 4.85 2 -2 9 6.54 4.85 2 2 9 23.03 6.67 2 2 9 23.03 6.67 2 2 9 6.93 4.35 2 2 9 83.64 9.00 2 2 9 9.49 5.23 2 2 9 6.93 4.35 2 2 9 83.64 9.00 2 2 9 9.49 5.23 -2 -2 -10 -1.14 3.11 -2 -2 -10 -1.14 3.11 2 -2 10 -11.71 5.30 2 -2 10 -11.71 5.30 2 -2 10 -0.62 4.21 2 -2 10 -0.62 4.21 2 2 10 13.11 7.17 2 2 10 13.11 7.17 2 2 10 7.05 4.76 2 2 10 187.57 10.80 2 2 10 3.67 5.23 2 2 10 7.04 4.76 2 2 10 187.57 10.80 2 2 10 3.67 5.23 -2 -2 -11 40.14 7.41 -2 -2 -11 40.12 7.41 2 -2 11 41.61 12.15 2 -2 11 41.61 12.15 2 -2 11 55.57 9.37 2 -2 11 55.57 9.37 2 2 11 83.01 14.54 2 2 11 83.01 14.54 2 2 11 54.78 9.81 2 2 11 204.49 12.69 2 2 11 56.88 9.38 2 2 11 54.78 9.81 2 2 11 204.49 12.69 2 2 11 56.88 9.38 -2 -2 -12 4.24 4.70 -2 -2 -12 4.21 4.70 2 -2 12 -6.02 10.49 2 -2 12 -6.02 10.49 2 -2 12 3.71 6.01 2 -2 12 3.71 6.01 2 2 12 18.34 9.15 2 2 12 18.34 9.15 2 2 12 8.49 6.61 2 2 12 157.14 12.17 2 2 12 6.44 7.55 2 2 12 8.48 6.61 2 2 12 157.14 12.17 2 2 12 6.44 7.55 -2 -2 -13 41.59 8.02 -2 -2 -13 41.56 8.02 2 -2 13 405.90 22.55 2 -2 13 405.90 22.55 2 -2 13 36.02 9.60 2 -2 13 36.02 9.60 2 2 13 57.69 16.18 2 2 13 57.69 16.18 2 2 13 50.71 9.36 2 2 13 234.77 15.38 2 2 13 45.02 11.69 2 2 13 50.72 9.36 2 2 13 234.77 15.38 2 2 13 45.02 11.69 -2 -2 -14 5.45 5.16 -2 -2 -14 5.46 5.16 2 -2 14 14.04 13.25 2 -2 14 14.04 13.25 2 -2 14 9.56 6.94 2 -2 14 9.56 6.94 2 2 14 -6.37 11.06 2 2 14 -6.37 11.06 2 2 14 13.28 7.75 2 2 14 195.82 14.86 2 2 14 46.52 13.08 2 2 14 13.26 7.75 2 2 14 195.82 14.86 2 2 14 46.52 13.08 -2 -2 -15 20.24 7.50 -2 -2 -15 20.24 7.49 2 -2 15 205.88 19.60 2 -2 15 205.88 19.60 2 -2 15 29.46 10.98 2 -2 15 29.46 10.98 2 2 15 110.00 25.49 2 2 15 110.00 25.49 2 2 15 20.33 9.01 2 2 15 252.88 16.77 2 2 15 24.99 12.07 2 2 15 20.31 9.01 2 2 15 252.88 16.77 2 2 15 24.99 12.07 -2 -2 -16 -8.10 4.99 -2 -2 -16 -8.08 4.99 2 -2 16 303.28 25.32 2 -2 16 303.28 25.32 2 -2 16 -7.70 8.34 2 -2 16 -7.70 8.34 2 2 16 67.52 23.31 2 2 16 67.52 23.31 2 2 16 -5.07 7.75 2 2 16 467.26 22.69 2 2 16 -2.61 10.45 2 2 16 -5.04 7.75 2 2 16 467.26 22.69 2 2 16 -2.61 10.45 -2 -3 16 124.19 18.35 -2 -3 16 124.19 18.35 -2 -3 16 -0.38 8.91 -2 -3 16 -0.38 8.91 -2 3 16 35.91 16.56 -2 3 16 35.91 16.56 -2 3 16 -7.30 12.26 -2 3 16 -5.83 10.42 -2 3 16 -7.30 12.26 -2 3 16 -5.83 10.42 2 -3 -16 2.83 5.94 2 -3 -16 292.19 16.14 2 -3 -16 2.77 5.94 2 -3 -16 292.19 16.14 -2 -3 15 160.24 25.09 -2 -3 15 160.24 25.09 -2 -3 15 88.95 14.28 -2 -3 15 88.95 14.28 -2 3 15 284.09 37.80 -2 3 15 284.09 37.80 -2 3 15 100.18 19.02 -2 3 15 101.13 16.71 -2 3 15 100.18 19.02 -2 3 15 101.13 16.71 2 -3 -15 81.70 12.18 2 -3 -15 252.38 18.37 2 -3 -15 81.66 12.18 2 -3 -15 252.38 18.37 -2 -3 14 314.71 17.04 -2 -3 14 314.71 17.04 -2 -3 14 5.16 6.89 -2 -3 14 5.16 6.89 -2 3 14 64.63 15.93 -2 3 14 64.63 15.93 -2 3 14 -8.04 10.88 -2 3 14 3.18 7.11 -2 3 14 -8.04 10.88 -2 3 14 3.18 7.11 2 -3 -14 3.51 5.11 2 -3 -14 1.46 8.76 2 -3 -14 3.52 5.11 2 -3 -14 1.46 8.76 -2 -3 13 53.28 19.54 -2 -3 13 53.28 19.54 -2 -3 13 66.68 10.99 -2 -3 13 66.68 10.99 -2 3 13 163.15 24.65 -2 3 13 163.15 24.65 -2 3 13 73.96 14.60 -2 3 13 70.18 13.38 -2 3 13 73.96 14.60 -2 3 13 70.18 13.38 2 -3 -13 48.50 9.21 2 -3 -13 186.61 14.97 2 -3 -13 48.49 9.21 2 -3 -13 186.61 14.97 -2 -3 12 6.92 9.97 -2 -3 12 6.92 9.97 -2 -3 12 14.19 7.10 -2 -3 12 14.19 7.10 -2 3 12 45.09 13.39 -2 3 12 45.09 13.39 -2 3 12 13.12 9.52 -2 3 12 17.37 9.08 -2 3 12 13.12 9.52 -2 3 12 17.37 9.08 2 -3 -12 13.57 5.73 2 -3 -12 124.32 11.82 2 -3 -12 13.56 5.72 2 -3 -12 124.32 11.82 -2 -3 11 -17.04 7.42 -2 -3 11 -17.04 7.42 -2 -3 11 -3.10 4.56 -2 -3 11 -3.10 4.56 -2 3 11 9.21 6.35 -2 3 11 9.21 6.35 -2 3 11 -4.22 6.30 -2 3 11 -3.10 4.77 -2 3 11 -4.22 6.30 -2 3 11 -3.10 4.77 2 -3 -11 -0.20 3.22 2 -3 -11 94.67 6.91 2 -3 -11 -0.19 3.22 2 -3 -11 94.67 6.91 -2 -3 10 148.84 18.39 -2 -3 10 148.84 18.39 -2 -3 10 86.48 10.27 -2 -3 10 86.48 10.27 -2 3 10 81.19 14.47 -2 3 10 81.19 14.47 -2 3 10 101.17 11.64 -2 3 10 69.46 10.88 -2 3 10 73.42 10.64 -2 3 10 101.17 11.64 -2 3 10 69.46 10.88 -2 3 10 73.42 10.64 2 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-4 4.39 2.29 2 -3 -4 -0.59 4.41 2 3 -4 2.04 2.15 2 3 -4 1.11 2.17 2 3 -4 2.04 2.15 2 3 -4 1.11 2.17 -2 -3 3 31.21 4.54 -2 -3 3 31.21 4.54 -2 3 3 29.81 6.16 -2 3 3 29.81 6.16 -2 3 3 34.98 5.67 -2 3 3 32.43 6.08 -2 3 3 33.99 5.83 -2 3 3 34.97 5.67 -2 3 3 32.43 6.08 -2 3 3 33.99 5.83 2 -3 -3 27.81 4.81 2 -3 -3 31.02 5.22 2 -3 -3 27.81 4.81 2 -3 -3 31.02 5.22 2 3 -3 39.90 4.86 2 3 -3 38.51 4.69 2 3 -3 39.90 4.86 2 3 -3 38.51 4.69 -2 -3 2 561.91 22.41 -2 -3 2 561.91 22.41 -2 -3 2 485.74 14.33 -2 -3 2 485.74 14.33 -2 3 2 519.84 24.57 -2 3 2 519.84 24.57 -2 3 2 556.36 16.85 -2 3 2 503.81 17.22 -2 3 2 538.03 17.23 -2 3 2 556.36 16.85 -2 3 2 503.81 17.22 -2 3 2 538.03 17.23 2 -3 -2 481.61 15.51 2 -3 -2 468.94 16.60 2 -3 -2 463.72 16.05 2 -3 -2 481.82 15.51 2 -3 -2 468.94 16.60 2 -3 -2 463.72 16.05 2 3 -2 525.14 15.36 2 3 -2 513.79 14.31 2 3 -2 525.11 15.36 2 3 -2 513.79 14.31 -2 -3 1 37.03 6.37 -2 -3 1 37.03 6.37 -2 -3 1 50.47 5.55 -2 -3 1 50.47 5.55 -2 3 1 35.99 6.63 -2 3 1 35.99 6.63 -2 3 1 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6.21 2 3 1 96.60 9.98 2 3 1 96.60 9.98 2 3 1 87.81 8.06 2 3 1 83.83 7.12 2 3 1 85.68 8.15 2 3 1 87.80 8.06 2 3 1 83.83 7.12 2 3 1 85.68 8.15 2 -3 2 23.00 6.27 2 -3 2 23.00 6.27 2 -3 2 23.22 3.31 2 -3 2 27.43 5.31 2 -3 2 17.38 3.63 2 -3 2 23.21 3.31 2 -3 2 27.43 5.31 2 -3 2 17.38 3.63 2 3 2 19.06 4.55 2 3 2 19.06 4.55 2 3 2 23.26 5.31 2 3 2 23.57 4.91 2 3 2 28.85 5.62 2 3 2 23.25 5.30 2 3 2 23.57 4.91 2 3 2 28.85 5.62 2 -3 3 -6.67 3.13 2 -3 3 -6.67 3.13 2 -3 3 -0.18 1.06 2 -3 3 0.93 2.49 2 -3 3 1.86 2.71 2 -3 3 -0.18 1.06 2 -3 3 0.93 2.49 2 -3 3 1.86 2.71 2 3 3 0.03 2.54 2 3 3 0.03 2.54 2 3 3 -0.03 2.64 2 3 3 -0.08 2.66 2 3 3 0.92 2.69 2 3 3 -0.03 2.64 2 3 3 -0.08 2.66 2 3 3 0.92 2.69 2 -3 4 -0.87 0.94 2 -3 4 -2.04 2.01 2 -3 4 2.99 2.80 2 -3 4 -0.87 0.94 2 -3 4 -2.04 2.01 2 -3 4 2.99 2.80 2 3 4 1.71 1.88 2 3 4 1.71 1.88 2 3 4 0.98 2.78 2 3 4 0.79 2.54 2 3 4 0.65 3.73 2 3 4 0.98 2.78 2 3 4 0.79 2.54 2 3 4 0.65 3.73 2 -3 5 247.05 20.26 2 -3 5 247.05 20.26 2 -3 5 216.69 13.15 2 -3 5 256.32 9.27 2 -3 5 216.69 13.15 2 -3 5 256.32 9.27 2 3 5 -0.12 1.85 2 3 5 -0.12 1.85 2 3 5 224.25 13.89 2 3 5 222.79 12.57 2 3 5 226.78 13.95 2 3 5 224.24 13.89 2 3 5 222.79 12.57 2 3 5 226.78 13.95 2 -3 6 356.39 16.99 2 -3 6 356.39 16.99 2 -3 6 53.38 7.93 2 -3 6 53.38 7.93 2 3 6 40.69 7.81 2 3 6 40.69 7.81 2 3 6 42.70 7.46 2 3 6 56.62 7.83 2 3 6 47.55 7.81 2 3 6 42.71 7.45 2 3 6 56.62 7.83 2 3 6 47.55 7.81 2 -3 7 19.30 10.00 2 -3 7 19.30 10.00 2 -3 7 22.74 6.04 2 -3 7 22.74 6.04 2 3 7 12.11 5.57 2 3 7 12.11 5.57 2 3 7 14.66 4.77 2 3 7 20.13 6.33 2 3 7 12.76 6.29 2 3 7 14.64 4.77 2 3 7 20.13 6.33 2 3 7 12.76 6.29 -2 -3 -8 9.36 4.25 -2 -3 -8 9.36 4.25 2 -3 8 11.94 10.38 2 -3 8 11.94 10.38 2 -3 8 12.36 5.91 2 -3 8 12.36 5.91 2 3 8 18.49 6.32 2 3 8 18.49 6.32 2 3 8 17.13 5.46 2 3 8 18.48 7.23 2 3 8 14.16 6.18 2 3 8 17.13 5.46 2 3 8 18.48 7.23 2 3 8 14.16 6.18 -2 -3 -9 -6.11 2.74 -2 -3 -9 -6.13 2.74 2 -3 9 -5.34 9.63 2 -3 9 -5.34 9.63 2 -3 9 9.22 4.69 2 -3 9 9.22 4.69 2 3 9 0.30 4.51 2 3 9 -1.57 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409.13 14.42 3 -2 3 503.58 12.08 3 2 3 484.98 18.08 3 2 3 484.98 18.08 3 2 3 427.66 15.09 3 2 3 477.16 13.29 3 2 3 451.60 15.16 3 2 3 427.64 15.09 3 2 3 477.16 13.29 3 2 3 451.60 15.16 3 -2 4 203.94 15.81 3 -2 4 203.94 15.81 3 -2 4 238.82 4.25 3 -2 4 196.93 4.13 3 -2 4 186.71 10.80 3 -2 4 239.11 8.50 3 -2 4 238.79 4.24 3 -2 4 197.15 4.13 3 -2 4 186.71 10.80 3 -2 4 239.11 8.50 3 2 4 231.27 13.75 3 2 4 231.27 13.75 3 2 4 194.19 10.96 3 2 4 -1.11 1.50 3 2 4 195.63 10.65 3 2 4 194.19 10.96 3 2 4 -1.11 1.50 3 2 4 195.63 10.65 3 -2 5 44.43 8.12 3 -2 5 44.43 8.12 3 -2 5 59.30 7.11 3 -2 5 79.85 5.39 3 -2 5 59.30 7.11 3 -2 5 79.85 5.39 3 2 5 -1.41 1.34 3 2 5 -1.41 1.34 3 2 5 45.79 6.47 3 2 5 75.35 6.89 3 2 5 57.94 6.66 3 2 5 45.78 6.47 3 2 5 75.35 6.89 3 2 5 57.94 6.66 3 -2 6 296.30 20.83 3 -2 6 296.30 20.83 3 -2 6 288.36 14.20 3 -2 6 367.20 10.50 3 -2 6 288.36 14.20 3 -2 6 367.20 10.50 3 2 6 324.64 18.59 3 2 6 324.64 18.59 3 2 6 275.90 14.44 3 2 6 233.92 11.86 3 2 6 295.15 15.01 3 2 6 275.88 14.44 3 2 6 233.92 11.86 3 2 6 295.15 15.01 3 -2 7 13.08 6.84 3 -2 7 13.08 6.84 3 -2 7 5.92 3.54 3 -2 7 12.67 3.10 3 -2 7 5.92 3.54 3 -2 7 12.67 3.10 3 2 7 6.14 4.02 3 2 7 6.14 4.02 3 2 7 8.90 4.01 3 2 7 91.84 7.27 3 2 7 26.54 6.34 3 2 7 8.90 4.00 3 2 7 91.84 7.27 3 2 7 26.54 6.34 3 -2 8 19.35 8.20 3 -2 8 19.35 8.20 3 -2 8 24.69 5.84 3 -2 8 33.41 4.53 3 -2 8 24.69 5.84 3 -2 8 33.41 4.53 3 2 8 33.69 7.66 3 2 8 33.69 7.66 3 2 8 23.99 6.24 3 2 8 112.29 8.59 3 2 8 21.70 6.69 3 2 8 23.98 6.24 3 2 8 112.29 8.59 3 2 8 21.70 6.69 3 -2 9 5.64 6.76 3 -2 9 5.64 6.76 3 -2 9 4.95 5.09 3 -2 9 4.95 5.09 3 2 9 -2.74 2.57 3 2 9 -2.74 2.57 3 2 9 6.93 3.79 3 2 9 5.44 5.70 3 2 9 2.50 5.51 3 2 9 6.93 3.79 3 2 9 5.44 5.70 3 2 9 2.50 5.51 -3 -2 -10 7.95 4.29 -3 -2 -10 7.95 4.29 3 -2 10 12.73 7.68 3 -2 10 12.73 7.68 3 -2 10 14.02 5.30 3 -2 10 14.02 5.30 3 2 10 15.12 8.97 3 2 10 15.12 8.97 3 2 10 17.15 6.07 3 2 10 23.50 7.11 3 2 10 16.00 7.30 3 2 10 17.15 6.07 3 2 10 23.50 7.11 3 2 10 16.00 7.30 -3 -2 -11 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38.23 11.23 4 -5 -2 26.41 18.06 4 -5 -2 26.41 18.06 4 -5 -2 22.92 6.38 4 -5 -2 34.86 9.27 4 -5 -2 57.20 10.89 4 -5 -2 22.91 6.38 4 -5 -2 34.86 9.27 4 -5 -2 57.20 10.89 4 5 -2 32.18 8.10 4 5 -2 32.18 8.10 -4 5 1 47.47 15.70 -4 5 1 47.47 15.70 4 -5 -1 -22.07 16.59 4 -5 -1 -22.07 16.59 4 -5 -1 21.34 8.29 4 -5 -1 40.92 10.82 4 -5 -1 21.34 8.29 4 -5 -1 40.92 10.82 4 5 -1 18.28 7.21 4 5 -1 18.53 6.93 4 5 -1 18.28 7.21 4 5 -1 18.53 6.93 4 -5 0 5.06 7.12 4 -5 0 -4.44 9.05 4 -5 0 5.06 7.12 4 -5 0 -4.44 9.05 4 5 0 6.89 5.96 4 5 0 9.94 6.22 4 5 0 6.89 5.96 4 5 0 9.94 6.22 4 -5 1 -38.37 14.88 4 -5 1 -38.37 14.88 4 -5 1 1.53 6.27 4 -5 1 1.53 6.27 4 5 1 2.97 4.67 4 5 1 6.06 6.48 4 5 1 2.98 4.67 4 5 1 6.06 6.48 4 -5 2 2715.52 68.40 4 -5 2 2715.52 68.40 4 -5 2 0.07 7.04 4 -5 2 0.07 7.04 4 5 2 -4.73 5.54 4 5 2 -4.36 6.48 4 5 2 -4.73 5.54 4 5 2 -4.36 6.48 4 -5 3 524.68 28.94 4 -5 3 524.68 28.94 4 -5 3 27.29 9.30 4 -5 3 27.29 9.30 4 5 3 29.04 7.66 4 5 3 34.49 10.41 4 5 3 29.04 7.66 4 5 3 34.49 10.41 4 -5 4 1101.29 32.59 4 -5 4 1101.29 32.59 4 -5 4 6.60 7.48 4 -5 4 6.60 7.48 4 5 4 9.29 5.67 4 5 4 0.81 5.71 4 5 4 9.29 5.67 4 5 4 0.81 5.71 4 -5 5 501.31 16.37 4 -5 5 501.31 16.37 4 -5 5 -1.21 8.14 4 -5 5 -1.21 8.14 4 5 5 -0.15 4.36 4 5 5 -11.24 8.01 4 5 5 -0.16 4.36 4 5 5 -11.24 8.01 -4 -5 -6 20.32 9.98 -4 -5 -6 20.31 9.97 4 -5 6 45.83 15.72 4 -5 6 45.83 15.72 4 -5 6 27.67 10.15 4 -5 6 27.67 10.15 4 5 6 35.55 10.23 4 5 6 15.26 10.79 4 5 6 35.55 10.22 4 5 6 15.26 10.79 -4 -5 -7 -5.07 7.59 -4 -5 -7 -5.05 7.58 4 -5 7 553.33 28.29 4 -5 7 553.33 28.29 4 -5 7 1.70 6.70 4 -5 7 1.70 6.70 4 5 7 2.23 7.53 4 5 7 15.32 9.48 4 5 7 2.23 7.53 4 5 7 15.32 9.48 -5 0 19 143.01 30.88 -5 0 19 143.01 30.88 -5 0 19 100.44 18.49 -5 0 19 100.44 18.49 -5 0 18 -5.91 10.21 -5 0 18 -5.91 10.21 -5 0 18 -11.46 10.08 -5 0 18 -11.46 10.08 -5 0 17 81.25 19.69 -5 0 17 81.25 19.69 -5 0 17 64.25 13.22 -5 0 17 64.25 13.22 5 0 -17 54.14 8.37 5 0 -17 54.13 8.37 -5 0 16 -3.80 9.02 -5 0 16 -3.80 9.02 -5 0 16 -1.34 7.63 -5 0 16 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19.27 5 -2 -8 548.68 18.27 5 -2 -8 548.40 19.27 5 2 -8 677.44 15.93 5 2 -8 642.10 10.06 5 2 -8 677.43 15.93 5 2 -8 642.10 10.06 -5 -2 7 5.44 2.60 -5 -2 7 5.44 2.60 -5 -2 7 2.00 2.17 -5 -2 7 2.00 2.17 -5 2 7 1.79 3.28 -5 2 7 1.79 3.28 -5 2 7 2.75 3.65 -5 2 7 2.75 3.65 5 -2 -7 1.33 1.72 5 -2 -7 -8.45 2.82 5 -2 -7 1.33 1.72 5 -2 -7 -8.45 2.82 5 2 -7 0.46 1.57 5 2 -7 1.89 1.69 5 2 -7 0.46 1.57 5 2 -7 1.89 1.69 -5 -2 6 781.81 21.56 -5 -2 6 781.81 21.56 -5 -2 6 730.05 13.61 -5 -2 6 730.05 13.61 -5 2 6 605.76 25.84 -5 2 6 605.76 25.84 -5 2 6 593.56 18.17 -5 2 6 593.56 18.17 5 -2 -6 618.91 18.26 5 -2 -6 577.14 18.13 5 -2 -6 618.89 18.25 5 -2 -6 577.14 18.13 5 2 -6 735.61 16.71 5 2 -6 731.54 12.89 5 2 -6 735.60 16.71 5 2 -6 731.54 12.89 -5 -2 5 19.27 3.36 -5 -2 5 19.27 3.36 -5 -2 5 15.82 2.35 -5 -2 5 15.82 2.35 -5 2 5 11.01 3.74 -5 2 5 11.01 3.74 -5 2 5 12.86 4.26 -5 2 5 12.86 4.26 5 -2 -5 2.57 1.45 5 -2 -5 5.05 2.93 5 -2 -5 2.57 1.45 5 -2 -5 5.05 2.93 5 2 -5 3.93 1.96 5 2 -5 4.15 1.71 5 2 -5 3.93 1.96 5 2 -5 4.15 1.71 -5 -2 4 139.36 7.56 -5 -2 4 139.36 7.56 -5 -2 4 129.10 4.64 -5 -2 4 129.10 4.64 -5 2 4 117.70 11.20 -5 2 4 117.70 11.20 -5 2 4 100.65 8.28 -5 2 4 100.65 8.28 5 -2 -4 125.61 7.80 5 -2 -4 103.30 6.84 5 -2 -4 125.61 7.80 5 -2 -4 103.30 6.84 5 2 -4 129.67 7.60 5 2 -4 140.40 6.72 5 2 -4 129.67 7.60 5 2 -4 140.40 6.72 -5 -2 3 -1.69 1.02 -5 -2 3 -1.69 1.02 -5 -2 3 1.03 1.15 -5 -2 3 1.03 1.15 -5 2 3 0.13 1.63 -5 2 3 0.13 1.63 -5 2 3 0.42 2.50 -5 2 3 0.42 2.50 5 -2 -3 -1.70 0.91 5 -2 -3 1.83 2.63 5 -2 -3 -1.70 0.91 5 -2 -3 1.83 2.63 5 2 -3 0.47 1.68 5 2 -3 0.47 1.68 -5 -2 2 59.75 4.15 -5 -2 2 59.75 4.15 -5 -2 2 66.70 3.35 -5 -2 2 66.70 3.35 -5 2 2 83.74 10.10 -5 2 2 83.74 10.10 -5 2 2 69.95 6.35 -5 2 2 69.95 6.35 5 -2 -2 92.73 6.05 5 -2 -2 69.65 6.09 5 -2 -2 91.92 7.00 5 -2 -2 92.73 6.05 5 -2 -2 69.65 6.09 5 -2 -2 91.92 7.00 5 2 -2 82.34 6.46 5 2 -2 74.70 3.51 5 2 -2 22.43 3.93 5 2 -2 82.34 6.46 5 2 -2 74.70 3.51 5 2 -2 22.43 3.93 -5 2 1 152.24 12.70 -5 2 1 152.24 12.70 -5 2 1 150.07 9.32 -5 2 1 150.07 9.32 5 -2 -1 174.89 14.29 5 -2 -1 174.89 14.29 5 -2 -1 182.91 7.90 5 -2 -1 161.68 9.50 5 -2 -1 181.93 9.28 5 -2 -1 182.91 7.90 5 -2 -1 161.68 9.50 5 -2 -1 181.93 9.28 5 2 -1 163.92 7.02 5 2 -1 163.92 7.02 5 2 -1 189.22 9.72 5 2 -1 156.81 5.35 5 2 -1 192.82 9.51 5 2 -1 189.22 9.72 5 2 -1 156.81 5.35 5 2 -1 192.82 9.51 -5 2 0 1.50 2.16 -5 2 0 1.50 2.16 5 -2 0 4.44 2.72 5 -2 0 4.44 2.72 5 -2 0 2.09 1.39 5 -2 0 3.91 2.43 5 -2 0 5.08 2.90 5 -2 0 2.09 1.39 5 -2 0 3.91 2.43 5 -2 0 5.08 2.90 5 2 0 2.60 1.50 5 2 0 2.60 1.50 5 2 0 5.61 2.58 5 2 0 4.27 1.85 5 2 0 2.77 2.74 5 2 0 5.61 2.58 5 2 0 4.27 1.85 5 2 0 2.77 2.74 5 -2 1 2.36 2.82 5 -2 1 2.36 2.82 5 -2 1 2.64 1.35 5 -2 1 1.02 2.17 5 -2 1 2.61 2.32 5 -2 1 2.64 1.35 5 -2 1 1.02 2.17 5 -2 1 2.61 2.32 5 2 1 2.17 1.74 5 2 1 2.17 1.74 5 2 1 -1.32 2.45 5 2 1 3.63 2.05 5 2 1 4.05 2.78 5 2 1 -1.32 2.44 5 2 1 3.63 2.05 5 2 1 4.05 2.78 5 -2 2 13.33 4.51 5 -2 2 13.33 4.51 5 -2 2 16.79 2.48 5 -2 2 5.37 3.40 5 -2 2 13.88 3.60 5 -2 2 16.79 2.48 5 -2 2 5.37 3.40 5 -2 2 13.88 3.60 5 2 2 7.83 2.59 5 2 2 7.83 2.59 5 2 2 12.36 3.48 5 2 2 7.02 2.53 5 2 2 10.00 3.72 5 2 2 12.36 3.48 5 2 2 7.02 2.53 5 2 2 10.00 3.72 5 -2 3 208.93 18.09 5 -2 3 208.93 18.09 5 -2 3 450.02 9.80 5 -2 3 349.39 15.27 5 -2 3 421.77 13.21 5 -2 3 450.00 9.80 5 -2 3 349.39 15.27 5 -2 3 421.77 13.21 5 2 3 398.71 16.64 5 2 3 398.71 16.64 5 2 3 355.97 15.48 5 2 3 342.05 11.71 5 2 3 376.03 15.27 5 2 3 355.95 15.48 5 2 3 342.05 11.71 5 2 3 376.03 15.27 5 -2 4 35.66 8.20 5 -2 4 35.66 8.20 5 -2 4 44.21 3.32 5 -2 4 29.90 5.85 5 -2 4 34.28 5.16 5 -2 4 44.17 3.32 5 -2 4 29.90 5.85 5 -2 4 34.28 5.16 5 2 4 33.15 5.75 5 2 4 33.15 5.75 5 2 4 31.03 5.63 5 2 4 18.22 3.93 5 2 4 26.19 5.57 5 2 4 31.02 5.63 5 2 4 18.22 3.93 5 2 4 26.19 5.57 5 -2 5 -2.35 3.60 5 -2 5 -2.35 3.60 5 -2 5 4.40 1.39 5 -2 5 6.86 4.28 5 -2 5 4.77 3.09 5 -2 5 4.39 1.39 5 -2 5 6.86 4.28 5 -2 5 4.77 3.09 5 2 5 7.31 3.54 5 2 5 7.31 3.54 5 2 5 1.05 2.67 5 2 5 3.02 2.43 5 2 5 2.55 4.35 5 2 5 1.05 2.67 5 2 5 3.02 2.43 5 2 5 2.55 4.35 5 -2 6 161.83 20.11 5 -2 6 161.83 20.11 5 -2 6 139.56 10.49 5 -2 6 178.04 9.58 5 -2 6 139.56 10.49 5 -2 6 178.04 9.58 5 2 6 179.75 15.02 5 2 6 179.75 15.02 5 2 6 130.49 10.38 5 2 6 168.81 10.78 5 2 6 137.26 12.04 5 2 6 130.49 10.38 5 2 6 168.81 10.78 5 2 6 137.26 12.04 5 -2 7 -5.99 5.26 5 -2 7 -5.99 5.26 5 -2 7 -1.68 2.73 5 -2 7 3.58 3.62 5 -2 7 -1.68 2.73 5 -2 7 3.58 3.62 5 2 7 -0.24 1.66 5 2 7 -0.24 1.66 5 2 7 -0.50 2.47 5 2 7 2.84 4.26 5 2 7 -6.58 4.44 5 2 7 -0.50 2.47 5 2 7 2.84 4.26 5 2 7 -6.58 4.44 5 -2 8 55.56 13.58 5 -2 8 55.56 13.58 5 -2 8 41.63 7.82 5 -2 8 61.27 7.32 5 -2 8 41.63 7.82 5 -2 8 61.27 7.32 5 2 8 47.93 9.91 5 2 8 47.93 9.91 5 2 8 51.64 8.25 5 2 8 64.72 9.70 5 2 8 45.32 8.25 5 2 8 51.63 8.24 5 2 8 64.72 9.70 5 2 8 45.32 8.25 5 -2 9 410.54 29.94 5 -2 9 410.54 29.94 5 -2 9 362.64 20.00 5 -2 9 362.64 20.00 5 2 9 515.30 31.38 5 2 9 515.30 31.38 5 2 9 391.62 20.22 5 2 9 415.31 20.23 5 2 9 367.08 19.11 5 2 9 391.62 20.22 5 2 9 415.31 20.23 5 2 9 367.08 19.11 5 -2 10 0.38 7.59 5 -2 10 0.38 7.59 5 -2 10 4.51 6.07 5 -2 10 4.51 6.07 5 2 10 3.50 6.43 5 2 10 3.50 6.43 5 2 10 4.71 5.96 5 2 10 6.12 7.65 5 2 10 5.87 6.30 5 2 10 4.71 5.96 5 2 10 6.12 7.65 5 2 10 5.87 6.30 5 -2 11 273.22 32.97 5 -2 11 273.22 32.97 5 -2 11 298.24 20.07 5 -2 11 298.24 20.07 5 2 11 374.27 30.47 5 2 11 374.27 30.47 5 2 11 273.23 18.48 5 2 11 309.76 20.52 5 2 11 359.72 24.30 5 2 11 273.21 18.48 5 2 11 309.76 20.52 5 2 11 359.72 24.30 -5 -2 -12 6.05 5.63 -5 -2 -12 5.99 5.63 5 -2 12 4.97 13.61 5 -2 12 4.97 13.61 5 -2 12 14.74 8.69 5 -2 12 14.74 8.69 5 2 12 -2.49 12.54 5 2 12 -2.49 12.54 5 2 12 14.69 7.81 5 2 12 19.79 8.92 5 2 12 7.31 10.50 5 2 12 14.69 7.81 5 2 12 19.79 8.92 5 2 12 7.31 10.50 -5 -2 -13 1.37 5.34 -5 -2 -13 1.39 5.35 5 -2 13 -9.77 12.13 5 -2 13 -9.77 12.13 5 -2 13 -4.67 7.12 5 -2 13 -4.67 7.12 5 2 13 -19.84 12.72 5 2 13 -19.84 12.72 5 2 13 -1.24 7.15 5 2 13 -1.90 10.47 5 2 13 -6.88 9.81 5 2 13 -1.24 7.14 5 2 13 -1.90 10.47 5 2 13 -6.88 9.81 -5 -2 -14 29.77 8.90 -5 -2 -14 29.75 8.90 5 -2 14 458.91 31.21 5 -2 14 458.91 31.21 5 -2 14 52.85 11.60 5 -2 14 52.85 11.60 5 2 14 41.85 23.21 5 2 14 41.85 23.21 5 2 14 31.31 11.80 5 2 14 53.30 13.31 5 2 14 21.14 12.85 5 2 14 31.34 11.81 5 2 14 53.30 13.31 5 2 14 21.14 12.85 -5 -3 17 -46.59 16.67 -5 -3 17 -46.59 16.67 -5 -3 17 0.09 10.42 -5 -3 17 0.09 10.42 -5 3 17 42.28 20.39 -5 3 17 42.28 20.39 -5 3 17 0.44 8.98 -5 3 17 -4.75 7.53 -5 3 17 0.44 8.98 -5 3 17 -4.75 7.53 5 -3 -17 98.43 17.44 5 -3 -17 98.43 17.44 -5 -3 16 372.81 26.07 -5 -3 16 372.81 26.07 -5 -3 16 1.33 9.61 -5 -3 16 1.33 9.61 -5 3 16 57.39 17.63 -5 3 16 57.39 17.63 -5 3 16 8.92 11.94 -5 3 16 4.06 10.86 -5 3 16 8.92 11.94 -5 3 16 4.06 10.86 5 -3 -16 120.00 12.75 5 -3 -16 120.00 12.75 -5 -3 15 377.81 24.72 -5 -3 15 377.81 24.72 -5 -3 15 184.48 14.11 -5 -3 15 184.48 14.11 -5 3 15 114.04 23.52 -5 3 15 114.04 23.52 -5 3 15 49.09 11.98 -5 3 15 27.73 11.48 -5 3 15 49.09 11.98 -5 3 15 27.73 11.48 5 -3 -15 13.87 6.68 5 -3 -15 168.58 19.58 5 -3 -15 13.87 6.68 5 -3 -15 168.58 19.58 -5 -3 14 48.19 11.05 -5 -3 14 48.19 11.05 -5 -3 14 -1.20 6.92 -5 -3 14 -1.20 6.92 -5 3 14 8.65 8.90 -5 3 14 8.65 8.90 -5 3 14 0.74 9.06 -5 3 14 -3.84 8.50 -5 3 14 0.74 9.06 -5 3 14 -3.84 8.50 5 -3 -14 -2.78 3.78 5 -3 -14 70.82 13.16 5 -3 -14 -2.77 3.78 5 -3 -14 70.82 13.16 -5 -3 13 70.31 12.41 -5 -3 13 70.31 12.41 -5 -3 13 10.35 6.60 -5 -3 13 10.35 6.60 -5 3 13 20.58 10.61 -5 3 13 20.58 10.61 -5 3 13 21.91 9.94 -5 3 13 10.41 9.01 -5 3 13 21.91 9.94 -5 3 13 10.41 9.01 5 -3 -13 14.11 5.26 5 -3 -13 131.51 16.07 5 -3 -13 14.11 5.26 5 -3 -13 131.51 16.07 -5 -3 12 202.94 16.52 -5 -3 12 202.94 16.52 -5 -3 12 0.87 5.37 -5 -3 12 0.87 5.37 -5 3 12 -9.22 5.18 -5 3 12 -9.22 5.18 -5 3 12 0.45 7.29 -5 3 12 0.02 5.03 -5 3 12 0.45 7.29 -5 3 12 0.02 5.03 5 -3 -12 -0.83 3.54 5 -3 -12 97.53 9.87 5 -3 -12 -0.83 3.54 5 -3 -12 97.53 9.87 -5 -3 11 143.17 17.24 -5 -3 11 143.17 17.24 -5 -3 11 132.50 11.44 -5 -3 11 132.50 11.44 -5 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4 18.69 5.68 -5 3 4 16.32 4.81 -5 3 4 16.32 4.81 5 -3 -4 14.96 3.50 5 -3 -4 40.44 7.06 5 -3 -4 14.95 3.49 5 -3 -4 40.44 7.06 5 3 -4 -0.89 1.50 5 3 -4 27.92 4.48 5 3 -4 -0.89 1.50 5 3 -4 27.92 4.48 -5 -3 3 15.00 4.39 -5 -3 3 15.00 4.39 -5 -3 3 47.72 4.57 -5 -3 3 47.72 4.57 -5 3 3 24.66 6.72 -5 3 3 24.66 6.72 -5 3 3 35.45 6.95 -5 3 3 35.45 6.95 5 -3 -3 49.34 5.82 5 -3 -3 35.07 6.47 5 -3 -3 38.31 5.44 5 -3 -3 49.33 5.82 5 -3 -3 35.07 6.47 5 -3 -3 38.31 5.44 5 3 -3 37.24 5.46 5 3 -3 51.36 6.25 5 3 -3 37.20 5.46 5 3 -3 51.36 6.25 -5 -3 2 18.98 3.90 -5 -3 2 18.98 3.90 -5 -3 2 18.76 3.30 -5 -3 2 18.76 3.30 -5 3 2 14.38 5.08 -5 3 2 14.38 5.08 -5 3 2 15.70 5.65 -5 3 2 15.70 5.65 5 -3 -2 15.08 6.09 5 -3 -2 15.08 6.09 5 -3 -2 17.89 3.74 5 -3 -2 18.07 5.50 5 -3 -2 12.63 4.29 5 -3 -2 17.89 3.74 5 -3 -2 18.07 5.50 5 -3 -2 12.63 4.29 5 3 -2 22.61 4.67 5 3 -2 15.73 3.13 5 3 -2 6.51 2.86 5 3 -2 22.60 4.67 5 3 -2 15.73 3.13 5 3 -2 6.51 2.86 -5 -3 1 21.23 3.97 -5 -3 1 21.23 3.97 -5 -3 1 27.90 3.85 -5 -3 1 27.90 3.85 -5 3 1 17.03 5.69 -5 3 1 17.03 5.69 -5 3 1 27.77 5.72 -5 3 1 27.77 5.72 5 -3 -1 20.20 6.70 5 -3 -1 20.20 6.70 5 -3 -1 27.48 4.20 5 -3 -1 29.62 5.61 5 -3 -1 40.76 5.98 5 -3 -1 27.48 4.20 5 -3 -1 29.62 5.61 5 -3 -1 40.76 5.98 5 3 -1 18.55 3.80 5 3 -1 18.55 3.80 5 3 -1 31.94 5.35 5 3 -1 26.29 4.04 5 3 -1 33.90 5.64 5 3 -1 31.93 5.34 5 3 -1 26.29 4.04 5 3 -1 33.90 5.64 -5 3 0 4.66 3.97 -5 3 0 4.66 3.97 5 -3 0 2.18 4.08 5 -3 0 2.18 4.08 5 -3 0 8.34 2.32 5 -3 0 8.83 3.91 5 -3 0 14.02 4.21 5 -3 0 8.34 2.32 5 -3 0 8.83 3.91 5 -3 0 14.02 4.21 5 3 0 6.61 2.68 5 3 0 6.61 2.68 5 3 0 6.50 4.26 5 3 0 7.53 2.94 5 3 0 7.68 3.82 5 3 0 6.48 4.26 5 3 0 7.53 2.94 5 3 0 7.68 3.82 5 -3 1 48.49 9.30 5 -3 1 48.49 9.30 5 -3 1 44.35 4.02 5 -3 1 41.02 6.71 5 -3 1 60.47 7.01 5 -3 1 44.38 4.02 5 -3 1 41.02 6.71 5 -3 1 60.47 7.01 5 3 1 31.82 4.97 5 3 1 31.82 4.97 5 3 1 44.14 6.82 5 3 1 54.41 5.85 5 3 1 47.83 7.30 5 3 1 44.08 6.82 5 3 1 54.41 5.85 5 3 1 47.83 7.30 5 -3 2 -0.13 1.18 5 -3 2 2.42 3.22 5 -3 2 2.66 3.11 5 -3 2 -0.13 1.18 5 -3 2 2.42 3.22 5 -3 2 2.66 3.11 5 3 2 -2.45 1.76 5 3 2 -2.45 1.76 5 3 2 -0.58 3.48 5 3 2 -0.16 2.45 5 3 2 -2.61 2.19 5 3 2 -0.58 3.48 5 3 2 -0.16 2.45 5 3 2 -2.61 2.19 5 -3 3 7.15 2.23 5 -3 3 1.48 3.08 5 -3 3 3.22 3.61 5 -3 3 7.13 2.23 5 -3 3 1.48 3.08 5 -3 3 3.22 3.61 5 3 3 0.84 2.37 5 3 3 0.84 2.37 5 3 3 -3.39 3.13 5 3 3 1.96 3.76 5 3 3 -2.35 3.88 5 3 3 -3.39 3.13 5 3 3 1.96 3.76 5 3 3 -2.35 3.88 5 -3 4 514.27 17.86 5 -3 4 514.27 17.86 5 -3 4 13.79 5.37 5 -3 4 14.31 4.72 5 -3 4 13.79 5.37 5 -3 4 14.31 4.72 5 3 4 11.32 4.27 5 3 4 11.32 4.27 5 3 4 9.54 4.05 5 3 4 20.97 5.19 5 3 4 17.04 6.12 5 3 4 9.54 4.05 5 3 4 20.97 5.19 5 3 4 17.04 6.12 5 -3 5 21.51 9.64 5 -3 5 21.51 9.64 5 -3 5 17.28 6.06 5 -3 5 23.51 4.47 5 -3 5 17.28 6.06 5 -3 5 23.51 4.47 5 3 5 7.26 4.17 5 3 5 7.26 4.17 5 3 5 11.58 5.43 5 3 5 17.05 5.31 5 3 5 12.93 6.73 5 3 5 11.58 5.43 5 3 5 17.05 5.31 5 3 5 12.93 6.73 5 -3 6 -1.14 5.73 5 -3 6 -1.14 5.73 5 -3 6 0.85 3.15 5 -3 6 0.85 3.15 5 3 6 6.32 4.05 5 3 6 6.32 4.05 5 3 6 4.22 4.68 5 3 6 2.96 4.24 5 3 6 26.51 8.23 5 3 6 4.22 4.68 5 3 6 2.96 4.24 5 3 6 26.51 8.23 5 -3 7 -7.25 6.13 5 -3 7 -7.25 6.13 5 -3 7 15.36 6.02 5 -3 7 15.36 6.02 5 3 7 9.56 5.23 5 3 7 9.56 5.23 5 3 7 5.22 4.87 5 3 7 -0.08 5.16 5 3 7 1.68 5.40 5 3 7 5.22 4.87 5 3 7 -0.08 5.16 5 3 7 1.68 5.40 5 -3 8 15.89 14.47 5 -3 8 15.89 14.47 5 -3 8 12.60 5.69 5 -3 8 12.60 5.69 5 3 8 20.47 6.93 5 3 8 20.47 6.93 5 3 8 11.96 7.06 5 3 8 19.77 7.87 5 3 8 8.83 6.81 5 3 8 11.96 7.06 5 3 8 19.77 7.87 5 3 8 8.83 6.81 5 -3 9 -2.73 13.30 5 -3 9 -2.73 13.30 5 -3 9 13.68 5.94 5 -3 9 13.68 5.94 5 3 9 -3.57 4.25 5 3 9 -3.57 4.25 5 3 9 -0.81 6.47 5 3 9 0.80 8.71 5 3 9 -0.81 6.47 5 3 9 0.80 8.71 5 -3 10 35.08 14.29 5 -3 10 35.08 14.29 5 -3 10 25.88 8.18 5 -3 10 25.88 8.18 5 3 10 33.11 11.35 5 3 10 33.11 11.35 5 3 10 37.46 9.64 5 3 10 61.97 11.47 5 3 10 25.54 11.59 5 3 10 37.48 9.65 5 3 10 61.97 11.47 5 3 10 25.54 11.59 -5 -3 -11 26.69 7.71 -5 -3 -11 26.68 7.70 5 -3 11 54.26 20.53 5 -3 11 54.26 20.53 5 -3 11 48.53 11.62 5 -3 11 48.53 11.62 5 3 11 45.64 13.00 5 3 11 45.64 13.00 5 3 11 36.48 9.19 5 3 11 72.34 13.02 5 3 11 30.00 10.25 5 3 11 36.48 9.19 5 3 11 72.34 13.02 5 3 11 30.00 10.25 -5 -3 -12 -1.59 4.36 -5 -3 -12 -1.59 4.36 5 -3 12 -1.91 13.56 5 -3 12 -1.91 13.56 5 -3 12 -1.32 7.84 5 -3 12 -1.32 7.84 5 3 12 6.04 11.47 5 3 12 6.04 11.47 5 3 12 1.97 6.02 5 3 12 -13.28 10.20 5 3 12 -7.21 10.78 5 3 12 1.97 6.01 5 3 12 -13.28 10.20 5 3 12 -7.21 10.78 -5 -4 14 430.26 20.83 -5 -4 14 430.26 20.83 -5 4 14 20.90 14.11 -5 4 14 20.90 14.11 -5 4 14 19.43 10.31 -5 4 14 12.95 9.58 -5 4 14 19.43 10.31 -5 4 14 12.95 9.58 5 -4 -14 22.99 8.43 5 -4 -14 45.07 16.82 5 -4 -14 22.96 8.43 5 -4 -14 45.07 16.82 -5 -4 13 -11.17 14.55 -5 -4 13 -11.17 14.55 -5 4 13 -14.08 13.64 -5 4 13 -14.08 13.64 -5 4 13 4.01 12.07 -5 4 13 2.08 7.82 -5 4 13 4.01 12.07 -5 4 13 2.08 7.82 5 -4 -13 -1.33 3.79 5 -4 -13 23.25 14.40 5 -4 -13 -1.34 3.79 5 -4 -13 23.25 14.40 -5 -4 12 -22.23 11.75 -5 -4 12 -22.23 11.75 -5 4 12 -13.16 11.20 -5 4 12 -13.16 11.20 -5 4 12 -1.02 10.21 -5 4 12 3.54 9.57 -5 4 12 -1.02 10.21 -5 4 12 3.54 9.57 5 -4 -12 -1.80 5.10 5 -4 -12 77.56 15.54 5 -4 -12 -1.78 5.09 5 -4 -12 77.56 15.54 -5 4 11 0.52 7.29 -5 4 11 0.52 7.29 -5 4 11 -2.49 8.50 -5 4 11 -1.75 6.02 -5 4 11 -2.49 8.50 -5 4 11 -1.75 6.02 5 -4 -11 -1.20 4.86 5 -4 -11 51.00 8.79 5 -4 -11 -1.20 4.85 5 -4 -11 51.00 8.79 -5 -4 10 1.26 10.03 -5 -4 10 1.26 10.03 -5 4 10 62.59 14.96 -5 4 10 62.59 14.96 -5 4 10 3.58 8.21 -5 4 10 -3.51 7.80 -5 4 10 3.58 8.21 -5 4 10 -3.51 7.80 5 -4 -10 0.79 3.55 5 -4 -10 55.16 13.25 5 -4 -10 0.80 3.55 5 -4 -10 55.16 13.25 -5 -4 9 0.31 8.70 -5 -4 9 0.31 8.70 -5 4 9 8.25 10.29 -5 4 9 8.25 10.29 -5 4 9 11.71 7.15 -5 4 9 11.69 7.86 -5 4 9 11.71 7.15 -5 4 9 11.69 7.86 5 -4 -9 12.77 5.31 5 -4 -9 54.45 12.21 5 -4 -9 12.76 5.31 5 -4 -9 54.45 12.21 -5 -4 8 -1.21 6.27 -5 -4 8 -1.21 6.27 -5 4 8 -1.11 4.71 -5 4 8 -1.11 4.71 -5 4 8 -2.04 6.64 -5 4 8 -2.04 6.64 5 -4 -8 -1.61 3.69 5 -4 -8 40.81 10.20 5 -4 -8 -1.61 3.69 5 -4 -8 40.81 10.20 -5 -4 7 6.23 5.74 -5 -4 7 6.23 5.74 -5 4 7 -0.38 5.32 -5 4 7 -0.38 5.32 -5 4 7 5.90 7.00 -5 4 7 5.90 7.00 5 -4 -7 7.93 4.69 5 -4 -7 68.29 7.32 5 -4 -7 7.93 4.69 5 -4 -7 68.29 7.32 -5 -4 6 178.11 18.39 -5 -4 6 178.11 18.39 -5 4 6 104.63 16.17 -5 4 6 104.63 16.17 -5 4 6 105.12 13.50 -5 4 6 105.12 13.50 5 -4 -6 133.31 11.95 5 -4 -6 188.40 12.42 5 -4 -6 133.32 11.95 5 -4 -6 188.40 12.42 5 4 -6 123.65 10.46 5 4 -6 123.64 10.46 -5 -4 5 74.35 14.73 -5 -4 5 74.35 14.73 -5 4 5 73.97 13.98 -5 4 5 73.97 13.98 -5 4 5 84.05 11.79 -5 4 5 84.05 11.79 5 -4 -5 89.45 9.09 5 -4 -5 72.95 10.36 5 -4 -5 136.56 11.46 5 -4 -5 89.46 9.09 5 -4 -5 72.95 10.36 5 -4 -5 136.56 11.46 5 4 -5 94.47 9.36 5 4 -5 94.45 9.36 -5 4 4 0.91 4.13 -5 4 4 0.91 4.13 -5 4 4 2.08 6.38 -5 4 4 2.08 6.38 5 -4 -4 0.33 2.95 5 -4 -4 1.63 4.31 5 -4 -4 22.09 7.44 5 -4 -4 0.33 2.95 5 -4 -4 1.63 4.31 5 -4 -4 22.09 7.44 5 4 -4 -1.51 3.16 5 4 -4 3.88 4.40 5 4 -4 -1.50 3.16 5 4 -4 3.88 4.40 -5 4 3 148.28 18.06 -5 4 3 148.28 18.06 -5 4 3 125.67 11.76 -5 4 3 125.67 11.76 5 -4 -3 144.01 20.83 5 -4 -3 144.01 20.83 5 -4 -3 169.67 10.63 5 -4 -3 133.39 11.49 5 -4 -3 159.46 13.57 5 -4 -3 169.68 10.63 5 -4 -3 133.39 11.49 5 -4 -3 159.46 13.57 5 4 -3 125.90 10.68 5 4 -3 140.62 11.06 5 4 -3 125.89 10.68 5 4 -3 140.62 11.06 -5 4 2 8.71 5.92 -5 4 2 8.71 5.92 -5 4 2 8.76 6.69 -5 4 2 8.76 6.69 5 -4 -2 2.47 7.70 5 -4 -2 2.47 7.70 5 -4 -2 8.60 4.11 5 -4 -2 2.84 5.18 5 -4 -2 24.85 7.59 5 -4 -2 8.60 4.11 5 -4 -2 2.84 5.18 5 -4 -2 24.85 7.59 5 4 -2 11.94 4.75 5 4 -2 4.17 4.51 5 4 -2 11.93 4.75 5 4 -2 4.17 4.51 -5 4 1 -3.82 6.65 -5 4 1 -3.82 6.65 5 -4 -1 14.96 11.36 5 -4 -1 14.96 11.36 5 -4 -1 0.17 2.02 5 -4 -1 -2.73 3.76 5 -4 -1 -13.89 5.30 5 -4 -1 0.16 2.02 5 -4 -1 -2.73 3.76 5 -4 -1 -13.89 5.30 5 4 -1 -0.46 3.50 5 4 -1 -4.49 3.69 5 4 -1 -0.45 3.50 5 4 -1 -4.49 3.69 -5 -4 0 22.85 7.64 -5 -4 0 22.85 7.64 5 -4 0 22.70 10.33 5 -4 0 22.70 10.33 5 -4 0 25.40 4.88 5 -4 0 28.18 6.74 5 -4 0 21.30 7.17 5 -4 0 25.39 4.88 5 -4 0 28.18 6.74 5 -4 0 21.30 7.17 5 4 0 31.62 6.85 5 4 0 24.96 6.07 5 4 0 31.61 6.84 5 4 0 24.96 6.07 5 -4 1 7.17 8.58 5 -4 1 7.17 8.58 5 -4 1 8.30 5.31 5 -4 1 6.56 5.75 5 -4 1 8.30 5.31 5 -4 1 6.56 5.75 5 4 1 17.37 5.19 5 4 1 19.46 6.82 5 4 1 17.37 5.19 5 4 1 19.46 6.82 5 -4 2 1637.34 48.88 5 -4 2 1637.34 48.88 5 -4 2 3.10 4.49 5 -4 2 -0.39 4.96 5 -4 2 3.10 4.49 5 -4 2 -0.39 4.96 5 4 2 -0.62 4.18 5 4 2 -2.57 4.73 5 4 2 -0.62 4.18 5 4 2 -2.57 4.73 5 -4 3 382.80 22.19 5 -4 3 382.80 22.19 5 -4 3 3.67 5.31 5 -4 3 3.67 5.31 5 4 3 5.96 5.06 5 4 3 -2.90 3.70 5 4 3 5.96 5.06 5 4 3 -2.90 3.70 5 -4 4 744.58 22.33 5 -4 4 744.58 22.33 5 -4 4 6.11 4.48 5 -4 4 6.11 4.48 5 4 4 -0.90 4.11 5 4 4 1.14 4.74 5 4 4 -0.90 4.11 5 4 4 1.14 4.74 5 -4 5 366.20 19.27 5 -4 5 366.20 19.27 5 -4 5 1.45 4.76 5 -4 5 1.45 4.76 5 4 5 -3.33 6.24 5 4 5 -2.16 6.16 5 4 5 -4.39 6.38 5 4 5 -3.33 6.24 5 4 5 -2.16 6.16 5 4 5 -4.39 6.38 5 -4 6 521.69 27.09 5 -4 6 521.69 27.09 5 -4 6 36.68 8.41 5 -4 6 36.68 8.41 5 4 6 34.93 9.69 5 4 6 31.47 9.18 5 4 6 34.02 10.69 5 4 6 34.92 9.69 5 4 6 31.47 9.18 5 4 6 34.02 10.69 5 -4 7 -22.26 14.00 5 -4 7 -22.26 14.00 5 -4 7 -1.24 4.79 5 -4 7 -1.24 4.79 5 4 7 -5.28 6.32 5 4 7 -0.33 6.82 5 4 7 -4.65 5.44 5 4 7 -5.28 6.32 5 4 7 -0.33 6.82 5 4 7 -4.65 5.44 5 -4 8 -11.56 11.65 5 -4 8 -11.56 11.65 5 -4 8 11.64 7.86 5 -4 8 11.64 7.86 5 4 8 3.52 5.49 5 4 8 -1.61 7.43 5 4 8 -2.10 8.67 5 4 8 3.52 5.49 5 4 8 -1.61 7.43 5 4 8 -2.10 8.67 5 -4 9 13.62 13.80 5 -4 9 13.62 13.80 5 -4 9 2.03 6.13 5 -4 9 2.03 6.13 5 4 9 4.60 5.54 5 4 9 1.85 10.61 5 4 9 2.47 10.54 5 4 9 4.60 5.54 5 4 9 1.85 10.61 5 4 9 2.47 10.54 -5 -4 -10 -7.38 5.46 -5 -4 -10 -7.36 5.45 5 -4 10 -20.79 17.95 5 -4 10 -20.79 17.95 5 -4 10 11.74 7.67 5 -4 10 11.74 7.67 5 4 10 -0.14 7.67 5 4 10 9.07 13.98 5 4 10 -11.90 11.93 5 4 10 -0.26 7.67 5 4 10 9.07 13.98 5 4 10 -11.90 11.93 -5 5 11 -4.48 10.80 -5 5 11 -4.48 10.80 -5 5 11 8.00 12.77 -5 5 11 8.00 12.77 5 -5 -11 1.03 5.39 5 -5 -11 1.03 5.39 -5 5 10 5.82 14.47 -5 5 10 5.82 14.47 -5 5 10 -4.33 10.51 -5 5 10 -4.33 10.51 5 -5 -10 5.53 7.24 5 -5 -10 12.53 14.64 5 -5 -10 5.50 7.24 5 -5 -10 12.53 14.64 -5 5 9 -4.41 14.43 -5 5 9 -4.41 14.43 -5 5 9 6.66 12.37 -5 5 9 6.66 12.37 5 -5 -9 24.92 9.19 5 -5 -9 95.22 16.41 5 -5 -9 24.88 9.18 5 -5 -9 95.22 16.41 -5 5 8 -0.54 10.79 -5 5 8 -0.54 10.79 5 -5 -8 -1.95 4.01 5 -5 -8 7.94 12.46 5 -5 -8 -1.95 4.00 5 -5 -8 7.94 12.46 -5 5 7 4.55 13.78 -5 5 7 4.55 13.78 -5 5 7 12.02 10.86 -5 5 7 12.02 10.86 5 -5 -7 20.82 8.15 5 -5 -7 92.11 15.68 5 -5 -7 20.83 8.15 5 -5 -7 92.11 15.68 -5 5 6 75.84 18.19 -5 5 6 75.84 18.19 -5 5 6 68.33 15.00 -5 5 6 68.33 15.00 5 -5 -6 61.86 10.58 5 -5 -6 62.26 11.24 5 -5 -6 124.13 17.50 5 -5 -6 61.87 10.58 5 -5 -6 62.26 11.24 5 -5 -6 124.13 17.50 -5 5 5 115.71 21.05 -5 5 5 115.71 21.05 -5 5 5 109.27 16.67 -5 5 5 109.27 16.67 5 -5 -5 82.05 20.47 5 -5 -5 82.05 20.47 5 -5 -5 73.25 10.81 5 -5 -5 69.73 11.56 5 -5 -5 127.71 17.58 5 -5 -5 73.14 10.80 5 -5 -5 69.73 11.56 5 -5 -5 127.71 17.58 -5 5 4 80.83 18.79 -5 5 4 80.83 18.79 -5 5 4 47.82 12.70 -5 5 4 47.82 12.70 5 -5 -4 6.64 19.86 5 -5 -4 6.64 19.86 5 -5 -4 49.21 8.77 5 -5 -4 48.70 10.80 5 -5 -4 75.97 13.52 5 -5 -4 49.19 8.77 5 -5 -4 48.70 10.80 5 -5 -4 75.97 13.52 -5 5 3 135.84 23.62 -5 5 3 135.84 23.62 -5 5 3 128.37 17.13 -5 5 3 128.37 17.13 5 -5 -3 122.69 27.57 5 -5 -3 122.69 27.57 5 -5 -3 175.49 12.87 5 -5 -3 105.21 13.92 5 -5 -3 199.62 19.02 5 -5 -3 175.73 12.89 5 -5 -3 105.21 13.92 5 -5 -3 199.62 19.02 5 5 -3 21.20 6.76 5 5 -3 21.20 6.76 -5 5 2 44.52 17.19 -5 5 2 44.52 17.19 -5 5 2 154.84 12.28 -5 5 2 154.84 12.28 5 -5 -2 104.62 25.67 5 -5 -2 104.62 25.67 5 -5 -2 28.92 8.84 5 -5 -2 63.67 12.22 5 -5 -2 28.92 8.84 5 -5 -2 63.67 12.22 5 5 -2 29.70 8.43 5 5 -2 29.66 8.42 -5 5 1 11.10 9.98 -5 5 1 11.10 9.98 5 -5 -1 -14.87 12.74 5 -5 -1 -14.87 12.74 5 -5 -1 5.02 7.70 5 -5 -1 -14.62 9.00 5 -5 -1 5.02 7.70 5 -5 -1 -14.62 9.00 5 5 -1 4.87 6.86 5 5 -1 -1.88 4.93 5 5 -1 4.90 6.86 5 5 -1 -1.88 4.93 5 -5 0 -28.23 10.65 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1.69 6.79 7 -5 0 1.96 6.62 7 -5 0 1.96 6.62 7 5 0 -0.07 5.43 7 5 0 -1.27 7.08 7 5 0 -0.11 5.43 7 5 0 -1.27 7.08 7 -5 1 2802.66 75.22 7 -5 1 2802.66 75.22 7 -5 1 8.76 7.36 7 -5 1 8.76 7.36 7 5 1 6.67 6.79 7 5 1 -1.36 7.65 7 5 1 6.67 6.77 7 5 1 -1.36 7.65 7 -5 2 -5.57 12.06 7 -5 2 -5.57 12.06 7 -5 2 -3.86 7.26 7 -5 2 -3.86 7.26 7 5 2 -0.30 5.05 7 5 2 -6.03 7.87 7 5 2 -0.30 5.05 7 5 2 -6.03 7.87 7 -5 3 551.85 18.64 7 -5 3 551.85 18.64 7 -5 3 0.62 7.63 7 -5 3 0.62 7.63 7 5 3 -1.05 8.36 7 5 3 -2.02 8.19 7 5 3 -1.05 8.36 7 5 3 -2.02 8.19 7 -5 4 1153.10 32.18 7 -5 4 1153.10 32.18 7 -5 4 5.52 7.84 7 -5 4 5.52 7.84 7 5 4 1.98 8.78 7 5 4 1.75 7.09 7 5 4 1.98 8.78 7 5 4 1.75 7.09 -8 0 20 51.36 20.81 -8 0 20 51.36 20.81 -8 0 20 265.56 21.45 -8 0 20 265.56 21.45 -8 0 19 52.70 19.13 -8 0 19 52.70 19.13 -8 0 19 234.10 19.30 -8 0 19 234.10 19.30 -8 0 18 108.30 22.08 -8 0 18 108.30 22.08 -8 0 18 243.32 18.29 -8 0 18 243.32 18.29 8 0 -18 31.39 6.47 8 0 -18 31.23 6.44 -8 0 17 57.01 15.71 -8 0 17 57.01 15.71 -8 0 17 150.47 14.20 -8 0 17 150.47 14.20 8 0 -17 10.87 3.94 8 0 -17 10.78 3.92 -8 0 16 97.66 17.07 -8 0 16 97.66 17.07 -8 0 16 57.73 10.38 -8 0 16 57.73 10.38 8 0 -16 39.12 6.68 8 0 -16 7.44 14.13 8 0 -16 38.84 6.64 8 0 -16 7.44 14.13 -8 0 15 32.71 9.97 -8 0 15 32.71 9.97 -8 0 15 -7.14 5.07 -8 0 15 -7.14 5.07 8 0 -15 -2.47 2.02 8 0 -15 -13.49 4.61 8 0 -15 -2.47 2.01 8 0 -15 -13.49 4.61 -8 0 14 89.27 14.11 -8 0 14 89.27 14.11 -8 0 14 36.46 8.05 -8 0 14 36.46 8.05 8 0 -14 41.09 7.13 8 0 -14 32.90 7.16 8 0 -14 40.77 7.09 8 0 -14 32.90 7.16 -8 0 13 1.76 3.71 -8 0 13 1.76 3.71 8 0 -13 -4.59 2.48 8 0 -13 9.10 5.10 8 0 -13 -4.58 2.48 8 0 -13 9.10 5.10 -8 0 12 12.96 4.69 -8 0 12 12.96 4.69 -8 0 12 35.70 7.41 -8 0 12 35.70 7.41 8 0 -12 33.40 5.88 8 0 -12 31.78 5.67 8 0 -12 33.34 5.87 8 0 -12 31.78 5.67 -8 0 11 -3.30 1.74 -8 0 11 -3.30 1.74 -8 0 11 2.19 3.40 -8 0 11 2.19 3.40 8 0 -11 7.47 2.64 8 0 -11 1.91 2.76 8 0 -11 7.43 2.64 8 0 -11 1.91 2.76 -8 0 10 24.12 5.76 -8 0 10 24.12 5.76 -8 0 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32.49 6.90 8 -2 -2 36.88 8.17 8 -2 -2 36.88 8.17 8 -2 -2 63.62 6.18 8 -2 -2 36.19 6.17 8 -2 -2 46.94 6.72 8 -2 -2 63.61 6.18 8 -2 -2 36.19 6.17 8 -2 -2 46.94 6.72 8 2 -2 54.19 6.69 8 2 -2 40.86 2.09 8 2 -2 44.63 6.34 8 2 -2 54.10 6.69 8 2 -2 40.86 2.09 8 2 -2 44.63 6.34 8 -2 -1 1719.96 46.64 8 -2 -1 1719.96 46.64 8 -2 -1 2202.53 31.43 8 -2 -1 1522.56 31.19 8 -2 -1 1937.27 33.64 8 -2 -1 2202.37 31.43 8 -2 -1 1522.56 31.19 8 -2 -1 1937.27 33.64 8 2 -1 1661.83 13.82 8 2 -1 1661.83 13.82 8 2 -1 1871.75 34.80 8 2 -1 1801.35 17.09 8 2 -1 1968.44 34.62 8 2 -1 1871.67 34.79 8 2 -1 1801.35 17.09 8 2 -1 1968.44 34.62 8 -2 0 339.05 21.83 8 -2 0 339.05 21.83 8 -2 0 436.54 13.80 8 -2 0 297.86 14.94 8 -2 0 382.17 15.48 8 -2 0 436.50 13.80 8 -2 0 297.86 14.94 8 -2 0 382.17 15.48 8 2 0 359.81 11.00 8 2 0 359.81 11.00 8 2 0 332.71 15.42 8 2 0 351.48 9.45 8 2 0 463.63 17.48 8 2 0 332.46 15.41 8 2 0 351.48 9.45 8 2 0 463.63 17.48 8 -2 1 366.71 22.49 8 -2 1 366.71 22.49 8 -2 1 359.01 12.17 8 -2 1 238.13 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2.70 8.48 11 -3 -5 28.53 5.93 11 -3 -5 9.98 5.06 11 -3 -5 0.62 7.46 11 -3 -5 28.59 5.93 11 -3 -5 9.98 5.06 11 -3 -5 0.62 7.46 11 3 -5 11.22 5.36 11 3 -5 102.58 9.18 11 3 -5 11.21 5.36 11 3 -5 102.58 9.18 -11 3 4 -0.35 4.20 -11 3 4 -0.35 4.20 11 -3 -4 -5.73 6.87 11 -3 -4 -5.73 6.87 11 -3 -4 -1.13 3.52 11 -3 -4 -0.16 4.24 11 -3 -4 -3.22 5.70 11 -3 -4 -1.12 3.51 11 -3 -4 -0.16 4.24 11 -3 -4 -3.22 5.70 11 3 -4 4.64 4.26 11 3 -4 -9.95 4.20 11 3 -4 4.63 4.26 11 3 -4 -9.95 4.20 -11 3 3 79.28 14.73 -11 3 3 79.28 14.73 11 -3 -3 53.49 17.26 11 -3 -3 53.49 17.26 11 -3 -3 76.73 9.40 11 -3 -3 65.87 10.40 11 -3 -3 83.93 12.44 11 -3 -3 76.73 9.40 11 -3 -3 65.87 10.40 11 -3 -3 83.93 12.44 11 3 -3 84.55 11.23 11 3 -3 85.97 11.37 11 3 -3 84.53 11.23 11 3 -3 85.97 11.37 11 -3 -2 164.74 24.41 11 -3 -2 164.74 24.41 11 -3 -2 174.77 12.19 11 -3 -2 128.31 12.04 11 -3 -2 134.11 12.85 11 -3 -2 174.76 12.19 11 -3 -2 128.31 12.04 11 -3 -2 134.11 12.85 11 3 -2 146.57 14.80 11 3 -2 422.83 23.15 11 3 -2 146.57 14.80 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-4.75 12.02 18 -2 -12 -21.71 8.67 18 -2 -12 -4.84 8.01 18 -2 -12 -15.79 12.28 18 -2 -12 -21.70 8.67 18 -2 -12 -4.84 8.01 18 -2 -12 -15.79 12.28 18 2 -12 0.79 5.10 18 2 -12 0.34 7.25 18 2 -12 0.79 5.10 18 2 -12 0.34 7.25 -18 2 11 2.55 9.36 -18 2 11 2.55 9.36 -18 2 11 3.74 10.57 -18 2 11 3.74 10.57 18 -2 -11 3.12 10.61 18 -2 -11 -5.74 7.10 18 -2 -11 -13.94 11.47 18 -2 -11 3.11 10.61 18 -2 -11 -5.74 7.10 18 -2 -11 -13.94 11.47 18 2 -11 0.44 6.75 18 2 -11 -7.58 6.94 18 2 -11 0.44 6.75 18 2 -11 -7.58 6.94 -18 2 10 7.93 9.96 -18 2 10 7.93 9.96 18 -2 -10 29.77 11.90 18 -2 -10 2.94 6.86 18 -2 -10 -1.04 13.83 18 -2 -10 29.76 11.90 18 -2 -10 2.94 6.86 18 -2 -10 -1.04 13.83 18 2 -10 5.32 7.58 18 2 -10 3.15 9.25 18 2 -10 5.33 7.58 18 2 -10 3.15 9.25 -18 2 9 -6.07 8.88 -18 2 9 -6.07 8.88 18 -2 -9 56.29 20.13 18 -2 -9 56.29 20.13 18 -2 -9 12.18 10.40 18 -2 -9 -2.71 7.89 18 -2 -9 -6.50 13.18 18 -2 -9 12.17 10.39 18 -2 -9 -2.71 7.89 18 -2 -9 -6.50 13.18 18 2 -9 2.15 7.03 18 2 -9 -9.69 8.57 18 2 -9 2.15 7.03 18 2 -9 -9.69 8.57 -18 2 8 -2.58 8.92 -18 2 8 -2.58 8.92 18 -2 -8 -42.26 15.05 18 -2 -8 -42.26 15.05 18 -2 -8 -11.71 4.68 18 -2 -8 0.00 7.33 18 -2 -8 -5.39 12.25 18 -2 -8 -11.72 4.68 18 -2 -8 0.00 7.33 18 -2 -8 -5.39 12.25 18 2 -8 -6.11 7.14 18 2 -8 1.43 6.53 18 2 -8 -6.11 7.14 18 2 -8 1.43 6.53 18 -2 -7 -8.77 7.45 18 -2 -7 5.22 7.11 18 -2 -7 6.77 9.03 18 -2 -7 -8.79 7.45 18 -2 -7 5.22 7.11 18 -2 -7 6.77 9.03 18 2 -7 0.92 8.93 18 2 -7 3.11 9.03 18 2 -7 0.92 8.95 18 2 -7 3.11 9.03 18 -2 -6 11.72 16.67 18 -2 -6 11.72 16.67 18 -2 -6 54.60 12.96 18 -2 -6 32.84 10.59 18 -2 -6 36.59 13.48 18 -2 -6 54.58 12.96 18 -2 -6 32.84 10.59 18 -2 -6 36.59 13.48 18 2 -6 34.43 10.05 18 2 -6 48.34 12.53 18 2 -6 34.43 10.04 18 2 -6 48.34 12.53 18 -2 -5 3213.36 76.44 18 -2 -5 3213.36 76.44 18 -2 -5 4.29 9.63 18 -2 -5 2.25 7.55 18 -2 -5 -8.17 9.01 18 -2 -5 4.30 9.64 18 -2 -5 2.25 7.55 18 -2 -5 -8.17 9.01 18 2 -5 4.64 8.71 18 2 -5 1.60 6.02 18 2 -5 4.63 8.71 18 2 -5 1.60 6.02 18 -2 -4 618.29 32.59 18 -2 -4 618.29 32.59 18 -2 -4 9.88 9.67 18 -2 -4 8.81 7.47 18 -2 -4 52.03 16.63 18 -2 -4 9.91 9.67 18 -2 -4 8.81 7.47 18 -2 -4 52.03 16.63 18 2 -4 3.95 8.48 18 2 -4 3.38 6.74 18 2 -4 3.95 8.47 18 2 -4 3.38 6.74 19 0 -13 39.35 13.28 19 0 -13 6.33 11.60 19 0 -13 39.33 13.28 19 0 -13 6.33 11.60 19 0 -12 -8.21 8.05 19 0 -12 -4.97 7.78 19 0 -12 -8.21 8.05 19 0 -12 -4.97 7.78 19 0 -11 -9.75 7.66 19 0 -11 24.82 13.06 19 0 -11 -9.75 7.66 19 0 -11 24.82 13.06 19 0 -10 -8.95 6.38 19 0 -10 24.00 12.91 19 0 -10 -8.95 6.38 19 0 -10 24.00 12.91 19 0 -9 19.30 10.90 19 0 -9 9.75 10.98 19 0 -9 19.31 10.90 19 0 -9 9.75 10.98 19 0 -8 -6.54 7.76 19 0 -8 -9.07 8.32 19 0 -8 -6.53 7.76 19 0 -8 -9.07 8.32 19 0 -7 0.43 6.28 19 0 -7 2.13 10.60 19 0 -7 0.43 6.28 19 0 -7 2.13 10.60 19 0 -6 -4.04 7.16 19 0 -6 -1.40 7.69 19 0 -6 -4.05 7.16 19 0 -6 -1.40 7.69 19 0 -5 -3.22 7.23 19 0 -5 -3.90 7.49 19 0 -5 -3.25 7.22 19 0 -5 -3.90 7.49 19 0 -4 -3.41 6.68 19 0 -4 -1.72 9.47 19 0 -4 -3.41 6.68 19 0 -4 -1.72 9.47 19 -1 -12 105.65 17.77 19 -1 -12 123.01 19.37 19 -1 -12 105.64 17.77 19 -1 -12 123.01 19.37 19 1 -12 108.41 16.67 19 1 -12 95.31 16.14 19 1 -12 108.45 16.68 19 1 -12 95.31 16.14 19 -1 -11 -7.67 6.87 19 -1 -11 -0.11 8.02 19 -1 -11 -7.66 6.87 19 -1 -11 -0.11 8.02 19 1 -11 0.93 8.62 19 1 -11 -6.37 7.15 19 1 -11 0.92 8.63 19 1 -11 -6.37 7.15 19 -1 -10 37.80 11.15 19 -1 -10 25.08 10.41 19 -1 -10 37.81 11.15 19 -1 -10 25.08 10.41 19 1 -10 34.12 11.12 19 1 -10 28.99 12.44 19 1 -10 34.12 11.12 19 1 -10 28.99 12.44 19 -1 -9 14.05 12.46 19 -1 -9 -6.44 7.41 19 -1 -9 14.05 12.46 19 -1 -9 -6.44 7.41 19 1 -9 -12.69 5.95 19 1 -9 2.55 10.21 19 1 -9 -12.71 5.95 19 1 -9 2.55 10.21 19 -1 -8 8.09 11.42 19 -1 -8 35.76 15.05 19 -1 -8 8.08 11.41 19 -1 -8 35.76 15.05 19 1 -8 0.61 5.40 19 1 -8 -3.89 8.71 19 1 -8 0.61 5.40 19 1 -8 -3.89 8.71 19 -1 -7 46.86 13.29 19 -1 -7 115.85 19.37 19 -1 -7 46.86 13.29 19 -1 -7 115.85 19.37 19 1 -7 38.79 11.47 19 1 -7 54.18 11.96 19 1 -7 38.80 11.47 19 1 -7 54.18 11.96 19 -1 -6 -0.86 8.11 19 -1 -6 -2.52 8.38 19 -1 -6 -0.86 8.11 19 -1 -6 -2.52 8.38 19 1 -6 -4.67 7.17 19 1 -6 -5.32 6.23 19 1 -6 -4.67 7.17 19 1 -6 -5.32 6.23 19 -1 -5 34.94 9.64 19 -1 -5 56.73 12.89 19 -1 -5 34.95 9.64 19 -1 -5 56.73 12.89 19 1 -5 32.53 12.36 19 1 -5 48.53 13.05 19 1 -5 32.56 12.36 19 1 -5 48.53 13.05 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 20478 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.5855(3) 0.6357(9) 0.9502(3) 0.0773(16) Uani 1 1 d . . . . . N1 N 0.5704(3) 0.5941(9) 0.8250(3) 0.0483(15) Uani 1 1 d . . . . . C1 C 0.3356(5) -0.2981(15) 0.8645(5) 0.075(2) Uani 1 1 d . . . . . H1 H 0.313605 -0.387651 0.890467 0.090 Uiso 1 1 calc R U . . . C2 C 0.3214(4) -0.3580(13) 0.7890(5) 0.070(2) Uani 1 1 d . . . . . H4 H 0.290392 -0.487309 0.764861 0.084 Uiso 1 1 calc R U . . . C3 C 0.3534(4) -0.2251(12) 0.7509(4) 0.0573(19) Uani 1 1 d . . . . . H5 H 0.342655 -0.263629 0.700262 0.069 Uiso 1 1 calc R U . . . C4 C 0.4021(3) -0.0318(11) 0.7860(3) 0.0446(17) Uani 1 1 d . . . . . C5 C 0.4373(3) 0.1014(11) 0.7471(3) 0.0470(17) Uani 1 1 d . . . . . H3 H 0.427646 0.063138 0.696639 0.056 Uiso 1 1 calc R U . . . C6 C 0.4852(3) 0.2848(11) 0.7835(3) 0.0424(16) Uani 1 1 d . . . . . C7 C 0.5292(3) 0.4503(11) 0.7607(3) 0.0430(16) Uani 1 1 d . . . . . C8 C 0.5464(3) 0.5190(10) 0.7015(3) 0.0403(16) Uani 1 1 d . . . . . C9 C 0.5203(3) 0.4136(10) 0.6249(3) 0.0413(16) Uani 1 1 d . . . . . C10 C 0.4387(3) 0.3228(11) 0.5852(3) 0.0370(16) Uani 1 1 d . . . . . C11 C 0.4210(4) 0.1128(11) 0.5450(4) 0.0517(17) Uani 1 1 d . . . . . H15 H 0.461459 0.025961 0.542379 0.062 Uiso 1 1 calc R U . . . C12 C 0.3455(5) 0.0296(13) 0.5089(4) 0.068(2) Uani 1 1 d . . . . . H12 H 0.334998 -0.111279 0.481823 0.081 Uiso 1 1 calc R U . . . C13 C 0.2855(4) 0.1552(15) 0.5128(4) 0.068(2) Uani 1 1 d . . . . . H2 H 0.234287 0.098364 0.489156 0.081 Uiso 1 1 calc R U . . . C14 C 0.3809(4) -0.1115(15) 0.9000(4) 0.066(2) Uani 1 1 d . . . . . H17 H 0.388806 -0.073116 0.949926 0.080 Uiso 1 1 calc R U . . . C15 C 0.4166(4) 0.0271(12) 0.8631(4) 0.0500(17) Uani 1 1 d . . . . . C16 C 0.4665(4) 0.2178(13) 0.8991(3) 0.0559(19) Uani 1 1 d . . . . . H16 H 0.476219 0.261055 0.949136 0.067 Uiso 1 1 calc R U . . . C17 C 0.5005(3) 0.3386(12) 0.8607(3) 0.0476(17) Uani 1 1 d . . . . . C18 C 0.5998(3) 0.7154(11) 0.7309(3) 0.0454(17) Uani 1 1 d . . . . . C19 C 0.6356(3) 0.8675(12) 0.6987(4) 0.0511(17) Uani 1 1 d . . . . . H6 H 0.626871 0.849203 0.647532 0.061 Uiso 1 1 calc R U . . . C20 C 0.6836(4) 1.0435(13) 0.7430(5) 0.065(2) Uani 1 1 d . . . . . H7 H 0.707325 1.143494 0.721254 0.078 Uiso 1 1 calc R U . . . C21 C 0.6975(4) 1.0756(13) 0.8191(5) 0.070(2) Uani 1 1 d . . . . . H9 H 0.730989 1.195159 0.847797 0.084 Uiso 1 1 calc R U . . . C22 C 0.6629(4) 0.9347(12) 0.8531(4) 0.0596(19) Uani 1 1 d . . . . . H8 H 0.671476 0.956654 0.904076 0.072 Uiso 1 1 calc R U . . . C23 C 0.6149(3) 0.7588(12) 0.8079(4) 0.0476(17) Uani 1 1 d . . . . . C24 C 0.5562(4) 0.5374(13) 0.8885(4) 0.0536(19) Uani 1 1 d . . . . . C25 C 0.5678(4) 0.4000(11) 0.5904(4) 0.0574(19) Uani 1 1 d . . . . . H10 H 0.618803 0.458237 0.615097 0.069 Uiso 1 1 calc R U . . . H11 H 0.549992 0.332226 0.541691 0.069 Uiso 1 1 calc R U . . . C26 C 0.3012(4) 0.3655(14) 0.5519(4) 0.061(2) Uani 1 1 d . . . . . H13 H 0.260584 0.451490 0.554441 0.073 Uiso 1 1 calc R U . . . C27 C 0.3770(3) 0.4477(11) 0.5872(3) 0.0497(17) Uani 1 1 d . . . . . H27 H 0.387105 0.590669 0.612985 0.060 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.074(3) 0.119(4) 0.036(3) -0.025(3) 0.021(2) -0.006(3) N1 0.044(3) 0.070(4) 0.027(3) -0.010(3) 0.012(3) 0.005(3) C1 0.080(6) 0.074(6) 0.097(7) 0.023(5) 0.062(5) 0.011(5) C2 0.082(5) 0.066(5) 0.089(6) 0.006(5) 0.061(5) 0.009(4) C3 0.074(5) 0.055(4) 0.060(5) -0.003(4) 0.045(4) 0.005(4) C4 0.046(4) 0.055(4) 0.038(4) 0.007(4) 0.024(3) 0.018(3) C5 0.054(4) 0.064(5) 0.031(4) 0.004(4) 0.026(3) 0.011(4) C6 0.038(4) 0.057(4) 0.034(4) 0.005(4) 0.017(3) 0.007(3) C7 0.039(4) 0.062(4) 0.029(4) -0.002(4) 0.016(3) 0.006(3) C8 0.035(4) 0.048(4) 0.036(4) -0.001(3) 0.014(3) 0.003(3) C9 0.042(4) 0.053(4) 0.031(4) 0.006(3) 0.018(3) 0.010(3) C10 0.046(4) 0.051(4) 0.020(3) 0.004(3) 0.020(3) 0.007(3) C11 0.061(5) 0.055(5) 0.043(4) -0.004(4) 0.026(3) 0.005(4) C12 0.073(5) 0.077(5) 0.052(5) -0.006(4) 0.027(4) -0.011(5) C13 0.052(5) 0.098(6) 0.047(5) 0.003(5) 0.016(4) -0.018(5) C14 0.066(5) 0.095(6) 0.050(5) 0.024(5) 0.037(4) 0.017(5) C15 0.052(4) 0.066(5) 0.038(4) 0.017(4) 0.026(3) 0.020(4) C16 0.053(4) 0.089(6) 0.030(4) 0.005(4) 0.022(3) 0.018(4) C17 0.045(4) 0.073(5) 0.025(4) 0.005(4) 0.016(3) 0.008(4) C18 0.043(4) 0.054(4) 0.037(4) 0.003(4) 0.016(3) 0.012(3) C19 0.045(4) 0.058(4) 0.047(4) 0.006(4) 0.016(3) 0.005(4) C20 0.051(4) 0.065(5) 0.074(6) 0.007(5) 0.023(4) -0.003(4) C21 0.052(5) 0.065(5) 0.080(6) -0.009(5) 0.018(4) -0.008(4) C22 0.049(4) 0.067(5) 0.048(4) -0.019(4) 0.007(3) -0.006(4) C23 0.035(4) 0.057(4) 0.047(5) -0.003(4) 0.015(3) 0.008(3) C24 0.051(4) 0.077(5) 0.034(4) -0.006(4) 0.020(3) 0.011(4) C25 0.062(4) 0.074(5) 0.046(4) -0.003(4) 0.032(3) 0.004(4) C26 0.051(5) 0.088(6) 0.048(4) 0.007(5) 0.025(4) 0.005(4) C27 0.053(4) 0.060(4) 0.042(4) 0.001(3) 0.025(3) 0.005(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C23 N1 C24 136.8(5) . . ? C23 N1 C7 110.3(5) . . ? C24 N1 C7 112.9(5) . . ? C14 C1 C2 120.6(7) . . ? C14 C1 H1 119.7 . . ? C2 C1 H1 119.7 . . ? C3 C2 C1 119.4(7) . . ? C3 C2 H4 120.3 . . ? C1 C2 H4 120.3 . . ? C2 C3 C4 122.0(7) . . ? C2 C3 H5 119.0 . . ? C4 C3 H5 119.0 . . ? C3 C4 C5 121.8(6) . . ? C3 C4 C15 118.2(6) . . ? C5 C4 C15 120.0(6) . . ? C6 C5 C4 120.0(5) . . ? C6 C5 H3 120.0 . . ? C4 C5 H3 120.0 . . ? C5 C6 C17 119.4(6) . . ? C5 C6 C7 133.4(5) . . ? C17 C6 C7 107.2(6) . . ? C8 C7 N1 108.7(5) . . ? C8 C7 C6 144.6(6) . . ? N1 C7 C6 106.6(5) . . ? C7 C8 C18 106.1(5) . . ? C7 C8 C9 128.3(6) . . ? C18 C8 C9 125.6(5) . . ? C25 C9 C8 121.4(5) . . ? C25 C9 C10 119.9(5) . . ? C8 C9 C10 118.7(4) . . ? C27 C10 C11 117.5(6) . . ? C27 C10 C9 120.4(6) . . ? C11 C10 C9 122.1(5) . . ? C12 C11 C10 121.7(6) . . ? C12 C11 H15 119.1 . . ? C10 C11 H15 119.1 . . ? C11 C12 C13 119.6(7) . . ? C11 C12 H12 120.2 . . ? C13 C12 H12 120.2 . . ? C12 C13 C26 120.0(7) . . ? C12 C13 H2 120.0 . . ? C26 C13 H2 120.0 . . ? C1 C14 C15 121.6(7) . . ? C1 C14 H17 119.2 . . ? C15 C14 H17 119.2 . . ? C16 C15 C14 123.4(6) . . ? C16 C15 C4 118.4(6) . . ? C14 C15 C4 118.2(7) . . ? C17 C16 C15 120.0(6) . . ? C17 C16 H16 120.0 . . ? C15 C16 H16 120.0 . . ? C16 C17 C6 122.0(7) . . ? C16 C17 C24 128.6(6) . . ? C6 C17 C24 109.3(5) . . ? C19 C18 C23 116.2(6) . . ? C19 C18 C8 134.3(6) . . ? C23 C18 C8 109.5(6) . . ? C20 C19 C18 119.8(6) . . ? C20 C19 H6 120.1 . . ? C18 C19 H6 120.1 . . ? C19 C20 C21 121.5(7) . . ? C19 C20 H7 119.3 . . ? C21 C20 H7 119.3 . . ? C22 C21 C20 121.2(7) . . ? C22 C21 H9 119.4 . . ? C20 C21 H9 119.4 . . ? C21 C22 C23 116.7(7) . . ? C21 C22 H8 121.7 . . ? C23 C22 H8 121.7 . . ? C22 C23 N1 130.0(6) . . ? C22 C23 C18 124.6(7) . . ? N1 C23 C18 105.4(6) . . ? O1 C24 N1 124.8(7) . . ? O1 C24 C17 131.3(6) . . ? N1 C24 C17 104.0(5) . . ? C9 C25 H10 120.0 . . ? C9 C25 H11 120.0 . . ? H10 C25 H11 120.0 . . ? C27 C26 C13 119.7(6) . . ? C27 C26 H13 120.1 . . ? C13 C26 H13 120.1 . . ? C26 C27 C10 121.5(6) . . ? C26 C27 H27 119.3 . . ? C10 C27 H27 119.3 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C24 1.206(7) . ? N1 C23 1.392(7) . ? N1 C24 1.397(7) . ? N1 C7 1.403(7) . ? C1 C14 1.350(9) . ? C1 C2 1.398(9) . ? C1 H1 0.9300 . ? C2 C3 1.365(8) . ? C2 H4 0.9300 . ? C3 C4 1.406(8) . ? C3 H5 0.9300 . ? C4 C5 1.421(7) . ? C4 C15 1.425(8) . ? C5 C6 1.361(8) . ? C5 H3 0.9300 . ? C6 C17 1.417(8) . ? C6 C7 1.447(8) . ? C7 C8 1.370(7) . ? C8 C18 1.447(8) . ? C8 C9 1.462(7) . ? C9 C25 1.331(7) . ? C9 C10 1.484(7) . ? C10 C27 1.382(7) . ? C10 C11 1.385(8) . ? C11 C12 1.371(8) . ? C11 H15 0.9300 . ? C12 C13 1.372(9) . ? C12 H12 0.9300 . ? C13 C26 1.378(9) . ? C13 H2 0.9300 . ? C14 C15 1.415(8) . ? C14 H17 0.9300 . ? C15 C16 1.407(9) . ? C16 C17 1.359(8) . ? C16 H16 0.9300 . ? C17 C24 1.479(9) . ? C18 C19 1.399(8) . ? C18 C23 1.402(8) . ? C19 C20 1.372(8) . ? C19 H6 0.9300 . ? C20 C21 1.380(9) . ? C20 H7 0.9300 . ? C21 C22 1.369(9) . ? C21 H9 0.9300 . ? C22 C23 1.377(8) . ? C22 H8 0.9300 . ? C25 H10 0.9300 . ? C25 H11 0.9300 . ? C26 C27 1.373(8) . ? C26 H13 0.9300 . ? C27 H27 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C14 C1 C2 C3 -0.4(10) . . . . ? C1 C2 C3 C4 1.6(10) . . . . ? C2 C3 C4 C5 177.9(6) . . . . ? C2 C3 C4 C15 -1.2(9) . . . . ? C3 C4 C5 C6 -178.9(5) . . . . ? C15 C4 C5 C6 0.3(8) . . . . ? C4 C5 C6 C17 1.1(8) . . . . ? C4 C5 C6 C7 179.7(5) . . . . ? C23 N1 C7 C8 0.2(6) . . . . ? C24 N1 C7 C8 179.8(5) . . . . ? C23 N1 C7 C6 179.7(4) . . . . ? C24 N1 C7 C6 -0.6(6) . . . . ? C5 C6 C7 C8 1.6(12) . . . . ? C17 C6 C7 C8 -179.6(8) . . . . ? C5 C6 C7 N1 -177.6(6) . . . . ? C17 C6 C7 N1 1.1(6) . . . . ? N1 C7 C8 C18 -0.8(6) . . . . ? C6 C7 C8 C18 -180.0(7) . . . . ? N1 C7 C8 C9 176.8(5) . . . . ? C6 C7 C8 C9 -2.5(12) . . . . ? C7 C8 C9 C25 -142.4(6) . . . . ? C18 C8 C9 C25 34.6(8) . . . . ? C7 C8 C9 C10 38.2(8) . . . . ? C18 C8 C9 C10 -144.7(5) . . . . ? C25 C9 C10 C27 -137.7(6) . . . . ? C8 C9 C10 C27 41.7(7) . . . . ? C25 C9 C10 C11 42.2(8) . . . . ? C8 C9 C10 C11 -138.4(5) . . . . ? C27 C10 C11 C12 -0.5(8) . . . . ? C9 C10 C11 C12 179.5(5) . . . . ? C10 C11 C12 C13 -0.5(9) . . . . ? C11 C12 C13 C26 1.0(10) . . . . ? C2 C1 C14 C15 -1.1(10) . . . . ? C1 C14 C15 C16 -177.6(6) . . . . ? C1 C14 C15 C4 1.5(9) . . . . ? C3 C4 C15 C16 178.8(5) . . . . ? C5 C4 C15 C16 -0.3(8) . . . . ? C3 C4 C15 C14 -0.3(8) . . . . ? C5 C4 C15 C14 -179.5(5) . . . . ? C14 C15 C16 C17 178.1(6) . . . . ? C4 C15 C16 C17 -1.0(8) . . . . ? C15 C16 C17 C6 2.4(9) . . . . ? C15 C16 C17 C24 -177.9(5) . . . . ? C5 C6 C17 C16 -2.5(8) . . . . ? C7 C6 C17 C16 178.6(5) . . . . ? C5 C6 C17 C24 177.7(5) . . . . ? C7 C6 C17 C24 -1.2(6) . . . . ? C7 C8 C18 C19 -176.6(6) . . . . ? C9 C8 C18 C19 5.7(10) . . . . ? C7 C8 C18 C23 1.1(6) . . . . ? C9 C8 C18 C23 -176.5(5) . . . . ? C23 C18 C19 C20 1.3(8) . . . . ? C8 C18 C19 C20 178.9(6) . . . . ? C18 C19 C20 C21 -0.2(9) . . . . ? C19 C20 C21 C22 -1.0(10) . . . . ? C20 C21 C22 C23 0.9(9) . . . . ? C21 C22 C23 N1 -178.0(6) . . . . ? C21 C22 C23 C18 0.3(9) . . . . ? C24 N1 C23 C22 -0.5(10) . . . . ? C7 N1 C23 C22 179.0(6) . . . . ? C24 N1 C23 C18 -179.0(6) . . . . ? C7 N1 C23 C18 0.5(6) . . . . ? C19 C18 C23 C22 -1.4(8) . . . . ? C8 C18 C23 C22 -179.6(5) . . . . ? C19 C18 C23 N1 177.2(5) . . . . ? C8 C18 C23 N1 -1.0(6) . . . . ? C23 N1 C24 O1 -1.0(11) . . . . ? C7 N1 C24 O1 179.5(6) . . . . ? C23 N1 C24 C17 179.4(6) . . . . ? C7 N1 C24 C17 -0.1(6) . . . . ? C16 C17 C24 O1 1.5(11) . . . . ? C6 C17 C24 O1 -178.7(6) . . . . ? C16 C17 C24 N1 -178.9(6) . . . . ? C6 C17 C24 N1 0.8(6) . . . . ? C12 C13 C26 C27 -0.4(9) . . . . ? C13 C26 C27 C10 -0.7(9) . . . . ? C11 C10 C27 C26 1.2(8) . . . . ? C9 C10 C27 C26 -178.9(5) . . . . ?