Crystallography Open Database

Information card for entry 1572010

1572009 << 1572010 >> 1572011

Preview

Coordinates	1572010.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H42 N4 O11
Calculated formula	C36 H42 N4 O11
Title of publication	Enantioconvergent and diastereoselective synthesis of atropisomeric hydrazides bearing a cyclic quaternary stereocenter through ternary catalysis.
Authors of publication	Wang, Xia; Wang, Shao-Jie; Xin, Xiaolan; An, Hao; Tu, Zhifeng; Yang, Hui; Wong, Ming Wah; Lu, Shenci
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	33
Pages of publication	13240 - 13249
a	15.78147 ± 0.00011 Å
b	14.09396 ± 0.00013 Å
c	16.78114 ± 0.00012 Å
α	90°
β	98.9652 ± 0.0007°
γ	90°
Cell volume	3686.92 ± 0.05 Å³
Cell temperature	301 ± 2 K
Ambient diffraction temperature	301 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0522
Residual factor for significantly intense reflections	0.0489
Weighted residual factors for significantly intense reflections	0.135
Weighted residual factors for all reflections included in the refinement	0.1379
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
294475 (current)	2024-09-06	cif/ Updating files of 1572009, 1572010 Original log message: Adding full bibliography for 1572009--1572010.cif.	1572010.cif
292645	2024-06-29	cif/ Adding structures of 1572009, 1572010 via cif-deposit CGI script.	1572010.cif