Crystallography Open Database

Information card for entry 1572015

1572014 << 1572015 >> 1572016

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Coordinates	1572015.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H41 N3 O4 Si
Calculated formula	C35 H41 N3 O4 Si
Title of publication	Photoinduced [4 + 2]-cycloaddition reactions of vinyldiazo compounds for the construction of heterocyclic and bicyclic rings.
Authors of publication	Bao, Ming; Bohórquez, Arnold R Romero; Arman, Hadi; Doyle, Michael P.
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	30
Pages of publication	12042 - 12046
a	14.0714 ± 0.0002 Å
b	14.8588 ± 0.0002 Å
c	16.3784 ± 0.0002 Å
α	90.572 ± 0.001°
β	92.785 ± 0.001°
γ	107.376 ± 0.001°
Cell volume	3263.25 ± 0.08 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0737
Residual factor for significantly intense reflections	0.0669
Weighted residual factors for significantly intense reflections	0.1395
Weighted residual factors for all reflections included in the refinement	0.1432
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
293767 (current)	2024-08-05	cif/ Updating files of 1572014, 1572015 Original log message: Adding full bibliography for 1572014--1572015.cif.	1572015.cif
292647	2024-06-29	cif/ Adding structures of 1572014, 1572015 via cif-deposit CGI script.	1572015.cif