Crystallography Open Database

Information card for entry 1572017

1572016 << 1572017 >> 1572018

Preview

Coordinates	1572017.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H20 F10 P S2 Sb
Calculated formula	C14 H20 F10 P S2 Sb
Title of publication	A geminal antimony(iii)/phosphorus(iii) frustrated Lewis pair.
Authors of publication	Krieft, Jonas; Trapp, Pia C.; Vishnevskiy, Yury V.; Neumann, Beate; Stammler, Hans-Georg; Lamm, Jan-Hendrik; Mitzel, Norbert W.
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	30
Pages of publication	12118 - 12125
a	8.6271 ± 0.0006 Å
b	11.2928 ± 0.0009 Å
c	12.0061 ± 0.001 Å
α	74.243 ± 0.007°
β	74.812 ± 0.007°
γ	70.602 ± 0.007°
Cell volume	1042.64 ± 0.15 Å³
Cell temperature	100.01 ± 0.1 K
Ambient diffraction temperature	100.01 ± 0.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0315
Residual factor for significantly intense reflections	0.0292
Weighted residual factors for significantly intense reflections	0.0696
Weighted residual factors for all reflections included in the refinement	0.0723
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
293769 (current)	2024-08-05	cif/ Updating files of 1572016, 1572017, 1572018, 1572019, 1572020, 1572021, 1572022 Original log message: Adding full bibliography for 1572016--1572022.cif.	1572017.cif
292666	2024-07-02	cif/ Adding structures of 1572016, 1572017, 1572018, 1572019, 1572020, 1572021, 1572022 via cif-deposit CGI script.	1572017.cif