Crystallography Open Database

Information card for entry 1572057

1572056 << 1572057 >> 1572058

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Coordinates	1572057.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H29 N O2
Calculated formula	C30 H29 N O2
Title of publication	1,5-Hydrogen atom transfer of α-iminyl radical cations: a new platform for relay annulation for pyridine derivatives and axially chiral heterobiaryls.
Authors of publication	Zhou, Yu-Qiang; He, Kui-Cheng; Zheng, Wei-Hao; Lv, Jing-Fang; He, Shi-Mei; Yu, Ning; Yang, Yun-Bo; Liu, Lv-Yan; Jiang, Kun; Wei, Ye
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	20
Pages of publication	7502 - 7514
a	8.15719 ± 0.00019 Å
b	11.2106 ± 0.0002 Å
c	27.1349 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	2481.41 ± 0.09 Å³
Cell temperature	291.19 ± 0.1 K
Ambient diffraction temperature	291.19 ± 0.1 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0533
Residual factor for significantly intense reflections	0.0502
Weighted residual factors for significantly intense reflections	0.1411
Weighted residual factors for all reflections included in the refinement	0.146
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
292730 (current)	2024-07-04	cif/ Adding structures of 1572056, 1572057 via cif-deposit CGI script.	1572057.cif