#------------------------------------------------------------------------------ #$Date: 2024-09-06 01:48:15 +0300 (Fri, 06 Sep 2024) $ #$Revision: 294398 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/20/1572062.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572062 loop_ _publ_author_name 'K\"orner, Lukas' 'Bockfeld, Dirk' 'Bannenberg, Thomas' 'Tamm, Matthias' _publ_section_title ; 2,3-Diamino-4,5-diarylcyclopentadienone iron carbonyl complexes as catalysts for reductive amination reactions ; _journal_issue 16 _journal_name_full 'Catalysis Science & Technology' _journal_page_first 4522 _journal_page_last 4532 _journal_paper_doi 10.1039/D4CY00372A _journal_volume 14 _journal_year 2024 _chemical_formula_moiety 'C35 H41 Fe N3 O3, 0.705(C7 H8), 0.295(C6 H14)' _chemical_formula_sum 'C41.71 H50.77 Fe N3 O3' _chemical_formula_weight 697.93 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-03-06 deposited with the CCDC. 2024-07-05 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 113.551(6) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.1925(5) _cell_length_b 28.2554(8) _cell_length_c 12.9763(6) _cell_measurement_reflns_used 36595 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 35.9520 _cell_measurement_theta_min 2.1060 _cell_volume 3761.9(3) _computing_cell_refinement 'CrysAlisPro 1.171.42.64a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.64a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.64a (Rigaku OD, 2022)' _computing_publication_material 'OLEX2 v1.3 (O. V. Dolomanov et al., J. Appl. Cryst., 2009, 42, 339-341)' _computing_structure_refinement 'SHELXL-2018/3 (G. M. Sheldrick, Acta Cryst., 2015, C71, 3-8)' _computing_structure_solution 'SHELXT 2018/2 (G. M. Sheldrick, Acta Cryst., 2015, A71, 3-8)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at offset/far, HyPix' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0712 _diffrn_reflns_av_unetI/netI 0.0408 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 42 _diffrn_reflns_limit_k_min -42 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 133590 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 32.577 _diffrn_reflns_theta_min 2.112 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.442 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.516 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.64a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.232 _exptl_crystal_description irregular _exptl_crystal_F_000 1488 _exptl_crystal_size_max 0.230 _exptl_crystal_size_mid 0.190 _exptl_crystal_size_min 0.050 _refine_diff_density_max 0.833 _refine_diff_density_min -0.784 _refine_diff_density_rms 0.072 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.125 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 547 _refine_ls_number_reflns 13691 _refine_ls_number_restraints 247 _refine_ls_restrained_S_all 1.131 _refine_ls_R_factor_all 0.0916 _refine_ls_R_factor_gt 0.0675 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0466P)^2^+4.2590P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1425 _refine_ls_wR_factor_ref 0.1516 _reflns_Friedel_coverage 0.000 _reflns_number_gt 10581 _reflns_number_total 13691 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4cy00372a3.cif _cod_data_source_block lk43db _cod_depositor_comments 'Adding full bibliography for 1572060--1572070.cif.' _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1572062 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.905 _shelx_estimated_absorpt_t_max 0.978 _oxdiff_exptl_absorpt_empirical_full_min 0.839 _oxdiff_exptl_absorpt_empirical_full_max 1.325 _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _shelx_res_file ; TITL lk43db_a.res in P2(1)/n lk43db.res created by SHELXL-2018/3 at 14:32:01 on 22-Jun-2023 REM Old TITL lk43db in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.124, Rweak 0.012, 0.054 REM 0.438 for 177 systematic absences, Orientation as input REM Formula found by SHELXT: C41A N3 O3 Fe CELL 0.71073 11.1925 28.2554 12.9763 90 113.551 90 ZERR 4 0.0005 0.0008 0.0006 0 0.006 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Fe N O UNIT 166.82 203.09 4 12 12 RIGU C36A C37A C38A C39A C40A C41A C42A RIGU C36B C37B C38B C39B C40B C41B C42B RIGU C36C C37C C38C C39C C40C C41C ISOR 0.01 0.02 C36C C37C C38C C39C C40C C41C DFIX 1.52 C36C C37C C37C C38C C38C C39C C39C C40C C40C C41C DANG 2.54 C36C C38C C37C C39C C38C C40C C39C C41C ISOR 0.01 0.02 C36A C41A H42b H40c C42A H42a C38A C37A H38c H41d C39A H37c = H39C H42C C40A ISOR 0.01 0.02 C42B C39B C37B H40d C38B H38d H42f H42d C36B H39d C41B H42e = H41E H37D C40B SUMP 1 0 1 2 1 3 1 4 L.S. 20 0 0 PLAN 10 SIZE 0.05 0.19 0.23 TEMP -173 CONF list 4 more -1 fmap 2 53 acta REM REM REM WGHT 0.046600 4.259000 FVAR 0.39977 0.40371 0.30090 0.29539 FE1 3 0.361736 0.365415 0.311994 11.00000 0.02067 0.01389 = 0.02259 -0.00008 0.00765 0.00007 O1 5 0.617976 0.407621 0.531324 11.00000 0.03048 0.02004 = 0.02842 -0.00621 0.01177 -0.00781 O2 5 0.310536 0.338200 0.080438 11.00000 0.03631 0.03368 = 0.02542 -0.00268 0.00801 0.00081 O3 5 0.080469 0.379638 0.240912 11.00000 0.02400 0.03445 = 0.04415 0.00494 0.00790 0.00604 N1 4 0.672695 0.350961 0.356692 11.00000 0.02189 0.01976 = 0.02682 -0.00167 0.01103 -0.00533 N2 4 0.491229 0.266034 0.301171 11.00000 0.01634 0.01513 = 0.02477 -0.00331 0.00707 -0.00234 N3 4 0.401782 0.432411 0.311786 11.00000 0.02979 0.01836 = 0.03125 0.00038 0.01429 0.00184 C1 1 0.554164 0.372715 0.481095 11.00000 0.02263 0.01689 = 0.02200 -0.00074 0.00834 -0.00234 C2 1 0.571983 0.344570 0.391622 11.00000 0.02034 0.01581 = 0.02233 -0.00003 0.00821 -0.00251 C3 1 0.486517 0.303793 0.367693 11.00000 0.01562 0.01466 = 0.01953 0.00004 0.00453 -0.00129 C4 1 0.400193 0.310273 0.424574 11.00000 0.01715 0.01507 = 0.02045 0.00022 0.00499 -0.00096 C5 1 0.434493 0.354322 0.486294 11.00000 0.02166 0.01501 = 0.02350 -0.00126 0.00864 -0.00099 C6 1 0.647302 0.346792 0.237617 11.00000 0.03052 0.02214 = 0.02937 -0.00091 0.01682 -0.00348 AFIX 23 H6A 2 0.571297 0.325814 0.200349 11.00000 -1.20000 H6B 2 0.723644 0.332186 0.229789 11.00000 -1.20000 AFIX 0 C7 1 0.620065 0.395344 0.179342 11.00000 0.03834 0.02640 = 0.03072 0.00330 0.01666 -0.00332 AFIX 23 H7A 2 0.607872 0.391626 0.099893 11.00000 -1.20000 H7B 2 0.538836 0.408693 0.180513 11.00000 -1.20000 AFIX 0 C8 1 0.733632 0.429219 0.239173 11.00000 0.04317 0.02727 = 0.04801 0.00750 0.02276 -0.00842 AFIX 23 H8A 2 0.812371 0.417883 0.229767 11.00000 -1.20000 H8B 2 0.711825 0.461066 0.204930 11.00000 -1.20000 AFIX 0 C9 1 0.761505 0.432260 0.363852 11.00000 0.03275 0.01996 = 0.04578 0.00051 0.01480 -0.00883 AFIX 23 H9A 2 0.687617 0.447967 0.373568 11.00000 -1.20000 H9B 2 0.840590 0.451619 0.402666 11.00000 -1.20000 AFIX 0 C10 1 0.781692 0.383021 0.416442 11.00000 0.02247 0.02044 = 0.03592 -0.00131 0.01135 -0.00636 AFIX 23 H10A 2 0.862931 0.369305 0.416112 11.00000 -1.20000 H10B 2 0.792304 0.385799 0.495688 11.00000 -1.20000 AFIX 0 C11 1 0.378034 0.234811 0.251675 11.00000 0.01799 0.01895 = 0.02607 -0.00403 0.00732 -0.00332 AFIX 23 H11A 2 0.296935 0.253243 0.233623 11.00000 -1.20000 H11B 2 0.381284 0.209836 0.306242 11.00000 -1.20000 AFIX 0 C12 1 0.377922 0.212194 0.144883 11.00000 0.02347 0.02314 = 0.02845 -0.00773 0.00872 -0.00290 AFIX 23 H12A 2 0.367143 0.237077 0.088137 11.00000 -1.20000 H12B 2 0.303493 0.190054 0.113478 11.00000 -1.20000 AFIX 0 C13 1 0.504932 0.185474 0.169549 11.00000 0.02649 0.01992 = 0.03636 -0.00835 0.01123 0.00024 AFIX 23 H13A 2 0.505809 0.173084 0.098491 11.00000 -1.20000 H13B 2 0.510809 0.158248 0.219372 11.00000 -1.20000 AFIX 0 C14 1 0.622079 0.218116 0.226120 11.00000 0.02224 0.02195 = 0.03455 -0.00508 0.01174 0.00092 AFIX 23 H14A 2 0.703525 0.199542 0.248050 11.00000 -1.20000 H14B 2 0.622806 0.242770 0.172162 11.00000 -1.20000 AFIX 0 C15 1 0.616962 0.241582 0.329778 11.00000 0.01922 0.01746 = 0.03087 -0.00085 0.00854 0.00082 AFIX 23 H15A 2 0.628290 0.217326 0.388003 11.00000 -1.20000 H15B 2 0.689107 0.264673 0.360841 11.00000 -1.20000 AFIX 0 C16 1 0.319118 0.273221 0.448180 11.00000 0.01853 0.01713 = 0.02136 -0.00175 0.00834 -0.00270 C17 1 0.379473 0.233980 0.515662 11.00000 0.02125 0.02061 = 0.02241 0.00055 0.00806 -0.00173 C18 1 0.301271 0.201679 0.541857 11.00000 0.02823 0.02321 = 0.02273 0.00262 0.00967 -0.00250 AFIX 43 H18 2 0.340831 0.175179 0.587919 11.00000 -1.20000 AFIX 0 C19 1 0.167079 0.207395 0.502153 11.00000 0.02578 0.02780 = 0.02631 -0.00121 0.01343 -0.00742 AFIX 43 H19 2 0.116457 0.184724 0.521049 11.00000 -1.20000 AFIX 0 C20 1 0.105907 0.245909 0.435062 11.00000 0.01963 0.02671 = 0.02516 -0.00453 0.01058 -0.00376 C21 1 0.184090 0.278517 0.410494 11.00000 0.02001 0.02046 = 0.02293 -0.00235 0.00878 -0.00073 AFIX 43 H21 2 0.144074 0.305444 0.366355 11.00000 -1.20000 AFIX 0 C22 1 0.524077 0.224538 0.560989 11.00000 0.02092 0.02564 = 0.03285 0.00894 0.00679 0.00197 AFIX 137 H22A 2 0.540574 0.196875 0.523025 11.00000 -1.50000 H22B 2 0.556901 0.218431 0.641966 11.00000 -1.50000 H22C 2 0.568692 0.252175 0.547420 11.00000 -1.50000 AFIX 0 C23 1 -0.039697 0.251689 0.388206 11.00000 0.02207 0.03845 = 0.04130 -0.00181 0.01484 -0.00389 AFIX 137 H23A 2 -0.075898 0.246222 0.306863 11.00000 -1.50000 H23B 2 -0.061231 0.283849 0.403365 11.00000 -1.50000 H23C 2 -0.076870 0.228763 0.423847 11.00000 -1.50000 AFIX 0 C24 1 0.388687 0.370051 0.574186 11.00000 0.02627 0.01758 = 0.02842 -0.00318 0.01420 -0.00378 C25 1 0.466862 0.360991 0.687627 11.00000 0.03278 0.02276 = 0.02922 0.00076 0.01599 -0.00020 C26 1 0.422490 0.376198 0.768539 11.00000 0.04322 0.03064 = 0.02938 -0.00068 0.01974 -0.00041 AFIX 43 H26 2 0.473865 0.369751 0.845512 11.00000 -1.20000 AFIX 0 C27 1 0.306163 0.400341 0.740240 11.00000 0.04249 0.02692 = 0.04077 -0.00778 0.02844 -0.00568 AFIX 43 H27 2 0.278862 0.410131 0.797459 11.00000 -1.20000 AFIX 0 C28 1 0.229465 0.410270 0.628813 11.00000 0.02948 0.02287 = 0.04602 -0.01070 0.02136 -0.00763 C29 1 0.272321 0.394802 0.547016 11.00000 0.02331 0.02275 = 0.03335 -0.00740 0.01213 -0.00477 AFIX 43 H29 2 0.220320 0.401391 0.470244 11.00000 -1.20000 AFIX 0 C30 1 0.595332 0.335711 0.723388 11.00000 0.04278 0.04314 = 0.02738 0.00483 0.01481 0.01283 AFIX 137 H30A 2 0.580186 0.302558 0.699490 11.00000 -1.50000 H30B 2 0.640870 0.337183 0.805391 11.00000 -1.50000 H30C 2 0.648689 0.350911 0.688596 11.00000 -1.50000 AFIX 0 C31 1 0.104048 0.437436 0.596358 11.00000 0.03338 0.03304 = 0.05897 -0.01108 0.02668 -0.00214 AFIX 137 H31A 2 0.034124 0.415804 0.592955 11.00000 -1.50000 H31B 2 0.081820 0.452101 0.522553 11.00000 -1.50000 H31C 2 0.114524 0.462094 0.652431 11.00000 -1.50000 AFIX 0 C32 1 0.331615 0.350300 0.170292 11.00000 0.02557 0.01834 = 0.02669 0.00238 0.00848 0.00220 C33 1 0.191333 0.373699 0.272948 11.00000 0.02815 0.01915 = 0.02969 0.00185 0.01055 0.00159 C34 1 0.431743 0.471064 0.318448 11.00000 0.04239 0.02063 = 0.05630 -0.00657 0.03239 -0.00274 C35 1 0.470163 0.520675 0.324551 11.00000 0.09471 0.02109 = 0.16825 -0.02598 0.09969 -0.01891 AFIX 137 H35A 2 0.432975 0.534607 0.249135 11.00000 -1.50000 H35B 2 0.565421 0.522900 0.354721 11.00000 -1.50000 H35C 2 0.437898 0.537838 0.373897 11.00000 -1.50000 AFIX 66 PART 1 C36A 1 0.090115 0.475031 0.922324 21.00000 0.04314 0.05412 = 0.03540 -0.00026 0.01839 0.00717 C37A 1 0.052752 0.428722 0.930264 21.00000 0.05923 0.05809 = 0.05870 0.02225 0.02761 0.01613 AFIX 43 H37C 2 0.103115 0.409832 0.993252 21.00000 -1.20000 AFIX 65 C38A 1 -0.058300 0.410051 0.846043 21.00000 0.08412 0.05881 = 0.11208 -0.03050 0.04462 -0.00210 AFIX 43 H38C 2 -0.083836 0.378400 0.851470 21.00000 -1.20000 AFIX 65 C39A 1 -0.131990 0.437689 0.753882 21.00000 0.04536 0.10349 = 0.06729 -0.04894 0.02326 -0.01079 AFIX 43 H39C 2 -0.207890 0.424928 0.696321 21.00000 -1.20000 AFIX 65 C40A 1 -0.094629 0.483998 0.745940 21.00000 0.05336 0.10406 = 0.05730 0.00849 0.03120 0.03765 AFIX 43 H40C 2 -0.144993 0.502888 0.682952 21.00000 -1.20000 AFIX 65 C41A 1 0.016424 0.502670 0.830160 21.00000 0.05590 0.04769 = 0.06070 0.01172 0.04396 0.01747 AFIX 43 H41D 2 0.041959 0.534321 0.824733 21.00000 -1.20000 AFIX 0 C42A 1 0.206822 0.493413 1.013944 21.00000 0.04680 0.14575 = 0.05350 -0.03963 0.02349 -0.02849 AFIX 137 H42A 2 0.206259 0.483740 1.086274 21.00000 -1.50000 H42B 2 0.207475 0.528039 1.009853 21.00000 -1.50000 H42C 2 0.284762 0.480749 1.006961 21.00000 -1.50000 AFIX 0 PART 2 C42B 1 -0.140428 0.495288 0.659360 31.00000 0.08371 0.05499 = 0.08542 0.01988 0.05874 0.02677 AFIX 137 H42D 2 -0.210961 0.478057 0.600619 31.00000 -1.50000 H42E 2 -0.072525 0.503111 0.632456 31.00000 -1.50000 H42F 2 -0.174994 0.524502 0.677612 31.00000 -1.50000 AFIX 66 C36B 1 -0.086486 0.466562 0.757100 31.00000 0.06003 0.03169 = 0.06590 0.00219 0.04732 0.01478 C41B 1 -0.142442 0.426439 0.781218 31.00000 0.06082 0.03274 = 0.04424 0.00487 0.00682 0.00214 AFIX 43 H41E 2 -0.222733 0.414673 0.727603 31.00000 -1.20000 AFIX 65 C40B 1 -0.080921 0.403530 0.883781 31.00000 0.05352 0.03552 = 0.04905 0.00100 0.01468 0.01627 AFIX 43 H40D 2 -0.119165 0.376107 0.900264 31.00000 -1.20000 AFIX 65 C39B 1 0.036557 0.420744 0.962229 31.00000 0.05527 0.07922 = 0.03791 -0.00120 0.00925 0.00747 AFIX 43 H39D 2 0.078604 0.405087 1.032326 31.00000 -1.20000 AFIX 65 C38B 1 0.092515 0.460867 0.938113 31.00000 0.06874 0.09525 = 0.08228 -0.01561 0.03323 -0.01386 AFIX 43 H38D 2 0.172806 0.472632 0.991729 31.00000 -1.20000 AFIX 65 C37B 1 0.030995 0.483777 0.835549 31.00000 0.07802 0.07252 = 0.07946 -0.00523 0.04932 -0.01006 AFIX 43 H37D 2 0.069240 0.511199 0.819067 31.00000 -1.20000 AFIX 0 PART -3 C41C 1 0.445076 0.503085 1.035514 41.00000 0.15156 0.09112 = 0.11510 0.01958 -0.00659 0.02709 AFIX 137 H41A 2 0.506516 0.501747 1.114439 41.00000 -1.50000 H41B 2 0.472487 0.527763 0.996520 41.00000 -1.50000 H41C 2 0.443609 0.472431 0.999695 41.00000 -1.50000 AFIX 0 C40C 1 0.307935 0.514565 1.029059 41.00000 0.17560 0.18872 = 0.14875 0.01216 0.06637 -0.01161 AFIX 23 H40A 2 0.310420 0.528394 1.099988 41.00000 -1.20000 H40B 2 0.259491 0.535876 0.965458 41.00000 -1.20000 AFIX 0 C39C 1 0.253083 0.465215 1.010118 41.00000 0.19582 0.17162 = 0.17702 -0.00803 0.06732 0.00473 AFIX 23 H39A 2 0.281577 0.450202 0.954790 41.00000 -1.20000 H39B 2 0.297108 0.447906 1.081757 41.00000 -1.20000 AFIX 0 C36C 1 -0.114694 0.426145 0.918299 41.00000 0.21342 0.22142 = 0.20722 -0.01393 0.08200 -0.04051 AFIX 137 H36A 2 -0.181700 0.405489 0.865649 41.00000 -1.50000 H36B 2 -0.150250 0.458074 0.914967 41.00000 -1.50000 H36C 2 -0.087394 0.413643 0.994765 41.00000 -1.50000 AFIX 0 C38C 1 0.113458 0.455582 0.972283 41.00000 0.21747 0.23326 = 0.24089 -0.00154 0.09477 -0.01369 AFIX 23 H38A 2 0.077022 0.488024 0.960254 41.00000 -1.20000 H38B 2 0.108025 0.445003 1.043017 41.00000 -1.20000 AFIX 0 C37C 1 0.003548 0.428075 0.886119 41.00000 0.22001 0.20840 = 0.21318 -0.01102 0.09176 -0.00643 AFIX 23 H37A 2 0.033205 0.395502 0.880845 41.00000 -1.20000 H37B 2 -0.022203 0.443269 0.811583 41.00000 -1.20000 AFIX 0 HKLF 4 REM lk43db_a.res in P2(1)/n REM wR2 = 0.1516, GooF = S = 1.125, Restrained GooF = 1.131 for all data REM R1 = 0.0675 for 10581 Fo > 4sig(Fo) and 0.0916 for all 13691 data REM 547 parameters refined using 247 restraints END WGHT 0.0466 4.2589 REM Highest difference peak 0.833, deepest hole -0.784, 1-sigma level 0.072 Q1 1 0.3859 0.3614 0.2573 11.00000 0.05 0.67 Q2 1 0.3344 0.3631 0.3645 11.00000 0.05 0.63 Q3 1 0.5226 0.5197 0.3916 11.00000 0.05 0.61 Q4 1 0.1910 0.4601 1.0371 11.00000 0.05 0.50 Q5 1 -0.1411 0.4635 0.7047 11.00000 0.05 0.50 Q6 1 0.4188 0.3600 0.5366 11.00000 0.05 0.46 Q7 1 -0.2166 0.4601 0.8967 11.00000 0.05 0.46 Q8 1 0.2615 0.4020 0.5940 11.00000 0.05 0.46 Q9 1 0.2610 0.5435 1.0537 11.00000 0.05 0.44 Q10 1 0.4443 0.2997 0.4007 11.00000 0.05 0.39 ; _shelx_res_checksum 85455 _shelx_hkl_file ; 0 0 -2 2840.92 101.18 0 0 2 2669.83 101.24 0 0 -2 2707.18 101.25 0 0 2 2728.71 101.39 0 0 -2 2726.79 101.44 0 0 2 2713.33 101.29 0 0 -2 2882.71 101.38 0 0 -2 2806.43 100.96 0 0 -3 -0.27 2.08 0 0 -3 -2.43 3.33 0 0 3 0.81 3.49 0 0 -3 3.68 3.55 0 0 3 -0.13 3.43 0 0 -3 -0.29 3.68 0 0 -4 580.69 22.67 0 0 4 556.30 22.48 0 0 -4 555.55 22.05 0 0 -4 605.56 22.66 0 0 4 572.14 21.48 0 0 -4 554.55 21.53 0 0 -4 547.90 21.50 0 0 -5 -1.16 2.78 0 0 5 -0.63 4.57 0 0 -5 5.43 4.80 0 0 5 -2.92 4.02 0 0 -5 1.36 4.38 0 0 -5 -2.29 4.84 0 0 5 0.32 2.75 0 0 -5 3.07 3.17 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0 -1 -5 185.56 9.71 0 -1 5 177.76 9.44 0 1 5 170.99 9.44 0 1 -5 176.89 9.74 0 -1 -5 188.59 9.78 0 -1 5 169.22 9.08 0 1 -6 64.21 4.55 0 1 -6 56.65 6.70 0 -1 6 52.89 6.21 0 -1 -6 66.49 6.86 0 1 6 50.29 6.13 0 -1 6 62.63 6.12 0 -1 -6 59.18 5.71 0 1 6 59.32 5.74 0 1 -6 58.90 5.98 0 1 -6 54.95 6.67 0 -1 -6 70.51 6.97 0 1 -6 54.35 4.63 0 -1 -6 58.95 4.56 0 1 6 54.62 4.43 0 -1 -6 61.29 5.00 0 -1 6 56.88 4.35 0 -1 -7 1.74 3.77 0 -1 7 1.61 2.98 0 1 7 3.55 3.19 0 1 -7 1.06 3.44 0 -1 -7 7.03 3.15 0 1 -7 4.48 3.26 0 1 -7 5.37 5.51 0 -1 -7 7.00 5.54 0 1 -7 10.95 5.08 0 -1 -7 1.37 4.71 0 -1 7 2.60 4.94 0 1 7 -0.21 4.61 0 1 -7 7.07 5.86 0 -1 -7 2.70 6.10 0 -1 -7 4.26 5.08 0 1 7 3.72 5.04 0 -1 7 -1.74 4.92 0 1 -7 7.16 5.58 0 1 -8 43.10 4.73 0 -1 -8 48.62 4.40 0 -1 8 44.64 4.22 0 1 8 45.27 4.31 0 1 -8 40.43 4.33 0 1 8 37.15 4.14 0 -1 -8 52.81 5.21 0 -1 -8 46.15 7.08 0 1 -8 42.18 6.83 0 1 -8 50.69 6.37 0 -1 8 42.92 6.03 0 1 8 40.45 5.93 0 -1 -8 43.16 5.85 0 -1 -8 54.01 7.57 0 1 -8 44.90 7.29 0 -1 -8 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19.49 5.59 0 -2 -8 22.25 6.29 0 2 8 20.28 5.72 0 2 -8 22.37 3.95 0 -2 8 19.50 3.54 0 -2 -8 20.21 4.49 0 2 8 20.27 3.73 0 2 -8 18.24 3.77 0 -2 -8 15.13 3.68 0 2 8 16.54 3.59 0 -2 -8 27.39 6.25 0 2 -8 21.43 6.20 0 2 -8 19.64 5.53 0 2 8 17.07 5.01 0 -2 -8 20.65 5.08 0 -2 8 19.60 5.63 0 -2 -8 14.99 6.22 0 2 -8 18.95 6.86 0 2 8 21.26 5.80 0 -2 -9 284.98 15.34 0 -2 -9 301.94 16.15 0 -2 9 283.81 15.10 0 2 9 257.80 14.67 0 -2 -9 290.56 13.65 0 2 -9 313.73 15.80 0 2 9 287.21 12.97 0 -2 -9 309.07 13.20 0 -2 9 298.14 12.92 0 2 -9 275.66 12.96 0 2 9 285.93 12.71 0 2 -9 277.84 13.06 0 -2 -9 306.82 14.28 0 2 9 305.66 13.98 0 -2 9 308.93 14.87 0 2 -9 302.86 14.88 0 2 -9 329.08 15.80 0 2 9 292.27 14.68 0 -2 -9 278.37 15.98 0 2 -9 314.24 16.26 0 2 -10 1.36 7.27 0 -2 -10 8.32 7.22 0 2 10 8.08 4.06 0 -2 10 -0.20 3.77 0 2 -10 -1.26 4.50 0 -2 -10 3.11 5.10 0 2 10 0.56 3.84 0 2 -10 -0.24 4.12 0 -2 -10 5.17 4.13 0 -2 10 0.47 7.26 0 2 10 1.42 7.17 0 2 -10 -5.79 6.86 0 -2 -10 0.32 5.80 0 -2 10 -5.06 6.36 0 2 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0 -11 11 298.89 17.08 0 11 11 292.47 12.41 0 11 -11 314.94 18.33 0 -11 -11 266.18 17.28 0 11 -11 262.93 17.17 0 -11 -12 3.98 8.63 0 -11 -12 4.86 8.96 0 -11 12 -9.08 5.00 0 11 -12 -4.64 4.47 0 -11 -12 1.34 5.27 0 11 12 7.86 8.22 0 -11 12 -1.09 8.04 0 11 -12 4.62 9.88 0 -11 12 13.39 8.95 0 11 12 2.73 4.46 0 11 -12 0.68 9.59 0 -11 -12 -5.51 8.67 0 11 -12 11.67 8.69 0 -11 -13 79.92 12.14 0 -11 -13 96.52 11.95 0 11 -13 99.74 12.73 0 -11 -13 104.08 8.35 0 -11 13 90.59 11.46 0 11 13 99.53 11.69 0 11 13 108.06 6.75 0 -11 13 101.36 11.78 0 -11 -13 108.36 13.09 0 11 -13 80.06 12.38 0 11 -13 116.65 13.46 0 11 -14 54.40 12.25 0 -11 -14 58.92 11.43 0 -11 -14 28.09 11.13 0 11 -14 46.10 11.25 0 -11 -14 43.51 6.88 0 11 14 55.16 10.81 0 -11 14 62.92 10.90 0 -11 14 48.03 10.68 0 11 14 58.75 5.74 0 11 -14 61.19 12.53 0 -11 -14 45.49 11.53 0 11 -15 70.42 13.46 0 -11 -15 42.50 11.50 0 11 -15 28.49 11.45 0 -11 -15 29.48 11.60 0 -11 -15 18.41 6.55 0 11 15 34.84 5.34 0 -11 15 28.73 10.64 0 -11 -15 45.39 12.33 0 11 -15 52.18 13.47 0 -11 15 29.99 10.64 0 11 15 63.39 11.65 0 11 -16 1.74 12.32 0 -11 -16 -21.85 11.93 0 11 -16 5.73 11.79 0 -11 -16 -3.83 11.97 0 11 16 18.80 11.21 0 -11 16 -2.10 10.60 0 -11 16 13.87 10.45 0 11 -16 13.26 12.75 0 -11 -16 18.00 12.13 0 -11 -17 -9.52 12.15 0 -11 -17 7.11 11.76 0 11 -17 -5.06 11.95 0 -11 17 14.86 7.46 0 11 17 -10.55 11.42 0 -11 17 -9.50 11.14 0 -11 17 28.92 11.19 0 11 -17 8.04 13.49 0 -11 -17 20.01 12.76 0 -12 0 322.19 14.79 0 -12 0 296.66 12.96 0 12 0 316.45 13.11 0 12 0 307.56 13.24 0 -12 0 313.44 13.75 0 -12 1 1957.90 72.67 0 -12 1 2053.36 73.71 0 -12 -1 1995.57 73.86 0 12 1 1984.88 73.92 0 -12 -1 1837.76 71.83 0 12 -1 1972.85 72.65 0 -12 1 1891.09 72.56 0 12 1 1869.97 71.98 0 -12 1 1993.29 72.75 0 12 1 2006.51 72.76 0 -12 -1 1994.00 72.51 0 12 -1 2043.16 72.36 0 -12 -2 115.35 7.90 0 -12 -2 111.90 7.47 0 12 2 101.65 7.66 0 -12 2 138.30 7.40 0 -12 2 127.57 5.54 0 12 2 119.11 5.78 0 12 2 111.61 8.78 0 -12 -2 110.22 8.77 0 12 2 98.37 5.67 0 -12 2 123.64 7.79 0 -12 2 112.42 7.35 0 12 -2 133.87 7.61 0 12 2 109.08 5.56 0 12 -2 119.84 5.91 0 -12 2 137.80 5.42 0 -12 -2 110.70 5.91 0 -12 -3 5.74 5.30 0 12 -3 13.36 5.81 0 -12 3 16.44 6.16 0 12 3 10.15 6.00 0 12 3 8.99 5.58 0 -12 -3 15.30 5.41 0 12 3 10.56 3.87 0 -12 3 12.96 3.50 0 -12 3 13.82 4.65 0 12 3 9.34 2.36 0 -12 3 6.39 5.31 0 -12 3 10.66 3.09 0 12 3 13.60 3.59 0 12 -3 13.52 5.03 0 -12 3 9.03 5.13 0 -12 4 233.93 12.03 0 12 -4 223.70 11.88 0 12 4 204.98 11.94 0 -12 -4 222.43 11.60 0 12 4 204.94 11.55 0 -12 4 242.90 10.50 0 -12 4 227.14 10.88 0 12 -4 200.80 11.09 0 -12 4 222.52 10.20 0 -12 4 220.94 11.55 0 -12 4 199.90 11.23 0 12 -4 212.52 10.93 0 -12 -4 212.96 11.66 0 12 5 6.01 5.08 0 -12 -5 10.71 5.16 0 12 -5 4.01 5.99 0 -12 5 16.02 5.76 0 -12 -5 17.57 6.17 0 12 5 5.26 5.49 0 -12 5 8.23 4.10 0 -12 -5 11.87 3.24 0 12 5 5.16 5.86 0 -12 5 11.14 4.67 0 12 -5 11.85 5.52 0 -12 5 8.93 5.41 0 -12 -5 6.68 5.39 0 12 -5 7.27 4.85 0 -12 -6 71.78 7.59 0 12 6 90.68 7.52 0 -12 6 86.36 7.75 0 -12 -6 82.67 7.96 0 -12 -6 65.37 6.15 0 12 6 83.49 7.67 0 -12 -6 78.17 4.81 0 -12 6 84.42 6.07 0 -12 6 81.53 6.80 0 -12 6 70.47 6.51 0 -12 6 76.03 7.67 0 12 -6 108.35 8.07 0 -12 -6 73.36 7.76 0 12 6 75.23 7.12 0 12 -6 78.87 7.12 0 -12 7 382.11 16.10 0 -12 -7 345.49 17.60 0 12 7 373.18 17.10 0 -12 7 417.38 17.37 0 -12 -7 344.65 17.35 0 12 7 332.46 16.84 0 -12 -7 356.09 16.08 0 -12 -7 356.40 14.42 0 -12 7 370.07 15.60 0 -12 7 374.90 16.57 0 -12 7 354.21 16.65 0 12 7 354.43 16.79 0 -12 7 372.19 17.65 0 12 -7 425.14 17.61 0 12 7 329.05 13.52 0 -12 -7 350.39 17.42 0 12 -7 378.24 16.86 0 12 7 352.36 16.75 0 12 8 113.90 8.29 0 -12 8 116.41 8.12 0 -12 8 112.56 9.26 0 -12 -8 97.65 9.44 0 -12 -8 106.15 9.41 0 -12 -8 114.14 7.77 0 12 8 94.16 8.56 0 -12 8 125.02 7.30 0 -12 8 102.81 8.96 0 12 8 109.44 9.07 0 12 8 94.16 5.20 0 -12 -8 104.11 9.75 0 12 8 98.36 8.76 0 12 -8 118.10 9.04 0 12 9 10.85 6.11 0 -12 9 -1.59 5.73 0 -12 -9 2.61 7.32 0 -12 -9 4.12 6.77 0 12 -9 6.32 8.06 0 -12 -9 5.10 5.04 0 12 9 1.09 6.01 0 -12 9 0.24 4.25 0 12 9 -5.44 6.88 0 -12 9 2.41 6.62 0 12 9 4.76 3.19 0 12 -9 4.96 7.93 0 12 -9 3.78 6.78 0 12 9 11.76 6.68 0 -12 -10 27.78 8.53 0 12 -10 40.12 9.20 0 -12 -10 21.09 7.76 0 12 10 32.34 6.75 0 -12 -10 28.09 5.77 0 -12 10 26.79 5.12 0 12 10 38.48 4.09 0 -12 10 25.78 8.85 0 12 -10 39.47 9.40 0 12 10 33.99 8.04 0 -12 10 39.01 8.07 0 12 -10 45.32 8.64 0 -12 -10 24.42 8.33 0 -12 -11 62.50 9.96 0 -12 -11 43.28 9.72 0 -12 -11 41.28 6.50 0 -12 11 41.37 5.65 0 12 11 34.63 7.27 0 12 11 31.32 8.88 0 -12 11 28.67 8.84 0 12 -11 59.77 10.88 0 -12 11 43.43 9.99 0 12 11 45.61 4.62 0 12 -11 59.51 10.67 0 12 -11 33.43 9.75 0 -12 -11 44.75 9.28 0 -12 -12 13.30 8.96 0 -12 -12 4.21 9.21 0 -12 -12 10.35 5.64 0 12 -12 6.06 4.53 0 -12 12 9.71 8.35 0 12 12 -2.23 8.78 0 12 -12 24.26 10.16 0 12 12 2.58 4.02 0 -12 12 18.49 9.55 0 12 -12 16.47 10.17 0 12 -12 2.06 8.72 0 -12 -12 4.83 9.07 0 -12 -13 20.71 10.25 0 -12 -13 14.92 10.09 0 12 -13 24.66 10.91 0 -12 -13 24.36 6.35 0 12 -13 1.85 5.15 0 12 13 9.05 9.28 0 -12 13 12.82 9.29 0 12 13 18.59 4.48 0 -12 13 3.89 9.75 0 -12 -13 1.51 9.51 0 12 -13 21.14 10.56 0 12 -13 36.91 11.38 0 -12 -14 6.00 9.65 0 12 -14 10.90 11.21 0 12 -14 1.70 6.53 0 12 -14 2.47 10.41 0 -12 -14 2.48 10.00 0 -12 -14 2.59 5.76 0 12 14 1.94 9.03 0 -12 14 8.09 8.95 0 -12 14 7.53 9.84 0 12 14 0.45 4.16 0 12 -14 2.46 11.18 0 -12 -14 3.33 10.68 0 12 -15 32.37 12.80 0 -12 -15 31.35 11.29 0 -12 -15 27.66 11.85 0 12 -15 16.00 10.99 0 -12 -15 20.73 6.45 0 -12 15 31.83 10.97 0 -12 -15 10.77 12.18 0 12 -15 18.66 12.19 0 -12 15 35.69 10.49 0 12 15 24.63 10.78 0 -12 -16 3.78 11.34 0 12 -16 20.95 12.24 0 -12 -16 10.52 12.29 0 12 16 40.25 11.93 0 -12 16 23.62 11.05 0 -12 16 17.91 11.08 0 12 -16 24.77 13.76 0 -12 -16 16.24 12.30 0 -12 -17 -1.59 11.98 0 -12 -17 11.13 12.25 0 12 -17 17.14 12.50 0 -12 17 -4.99 8.00 0 12 17 -7.50 11.33 0 -12 17 2.89 10.84 0 -12 17 25.19 10.92 0 12 -17 9.08 13.40 0 -12 -17 -5.03 12.60 0 -13 0 -1.72 5.96 0 13 0 -4.27 4.16 0 -13 0 -3.35 4.20 0 13 0 -0.97 4.28 0 -13 0 -1.20 4.99 0 -13 1 41.55 5.17 0 13 1 44.40 6.95 0 -13 1 42.20 7.23 0 -13 -1 40.63 6.81 0 13 1 46.78 4.32 0 -13 1 46.49 5.48 0 13 -1 40.99 5.49 0 -13 -1 46.17 4.20 0 -13 1 49.32 5.59 0 13 1 51.71 5.47 0 -13 -1 44.91 5.01 0 13 -1 52.13 4.96 0 -13 -2 752.80 29.67 0 13 2 720.08 29.04 0 -13 -2 708.87 28.77 0 -13 2 736.71 27.27 0 -13 2 763.64 28.86 0 13 2 730.61 27.47 0 13 2 702.60 30.10 0 -13 -2 678.41 29.91 0 -13 2 738.76 28.99 0 13 2 676.53 27.56 0 13 -2 726.86 28.97 0 -13 2 766.79 28.88 0 13 -2 777.13 28.92 0 13 2 729.52 27.37 0 -13 2 758.80 27.21 0 13 -2 772.95 27.66 0 -13 -2 677.36 27.58 0 -13 -3 33.89 5.66 0 13 3 30.99 5.79 0 -13 -3 31.76 5.60 0 -13 3 31.56 3.65 0 13 3 29.33 3.91 0 -13 3 36.99 5.07 0 -13 3 36.96 6.55 0 13 -3 35.57 6.51 0 13 3 34.39 6.68 0 -13 3 33.46 5.94 0 13 3 28.60 2.80 0 -13 3 29.45 5.43 0 13 -3 41.45 5.44 0 13 3 27.87 3.58 0 -13 3 32.64 3.37 0 13 -3 37.36 4.13 0 -13 -4 612.03 26.80 0 13 4 617.85 27.09 0 13 -4 692.53 27.07 0 -13 4 675.91 26.95 0 13 4 639.25 26.69 0 -13 -4 608.18 26.34 0 -13 4 675.59 26.14 0 13 4 613.20 25.37 0 -13 4 662.79 25.30 0 -13 4 617.87 26.40 0 -13 4 687.45 26.71 0 -13 4 666.06 25.09 0 13 4 619.36 25.11 0 13 -4 657.11 25.99 0 13 5 22.19 4.24 0 -13 5 30.83 4.17 0 -13 -5 27.41 5.94 0 13 5 27.71 5.73 0 13 -5 31.96 6.27 0 -13 -5 28.69 6.46 0 -13 5 24.01 6.33 0 13 5 27.09 6.28 0 -13 5 31.07 4.31 0 -13 -5 26.09 3.59 0 -13 5 30.53 5.11 0 13 5 26.54 6.09 0 -13 5 26.32 4.69 0 13 5 28.86 4.69 0 -13 5 37.07 6.20 0 -13 -5 27.63 5.90 0 13 -5 34.23 5.36 0 13 6 429.05 18.49 0 -13 6 447.83 18.46 0 13 6 421.65 19.47 0 -13 -6 394.18 19.95 0 13 -6 487.51 19.93 0 -13 6 477.53 20.03 0 -13 -6 402.81 20.00 0 13 6 412.14 19.81 0 -13 -6 435.28 18.98 0 -13 -6 426.79 17.41 0 -13 6 453.94 18.50 0 -13 6 437.34 18.88 0 13 6 419.51 19.02 0 -13 6 441.11 19.11 0 -13 6 457.05 20.20 0 13 -6 465.73 19.98 0 -13 -6 421.42 19.92 0 13 6 430.11 19.40 0 13 -6 463.35 19.25 0 -13 7 28.46 5.31 0 13 7 19.92 5.20 0 13 7 25.99 6.41 0 -13 -7 17.57 6.47 0 -13 7 27.37 6.62 0 13 -7 26.43 6.93 0 -13 -7 25.55 7.02 0 13 7 27.21 6.60 0 -13 -7 21.72 5.25 0 -13 7 22.85 4.69 0 -13 -7 25.49 3.49 0 13 7 14.07 5.67 0 -13 7 29.08 5.84 0 -13 7 26.63 5.95 0 -13 7 12.47 6.86 0 13 -7 35.22 6.67 0 -13 -7 17.16 6.82 0 13 -7 27.42 6.13 0 13 7 22.17 6.33 0 13 8 10.62 5.44 0 -13 8 13.00 5.49 0 -13 -8 4.78 6.56 0 -13 8 14.29 6.73 0 -13 -8 14.82 6.98 0 -13 -8 14.60 5.18 0 13 8 12.41 6.46 0 -13 8 13.84 4.63 0 13 8 10.27 1.92 0 13 8 12.24 6.43 0 13 -8 8.82 6.37 0 13 8 2.94 6.35 0 -13 8 19.25 6.37 0 -13 -8 8.59 7.10 0 -13 -9 81.52 9.61 0 -13 -9 88.66 9.60 0 -13 9 92.80 6.79 0 13 9 75.73 8.16 0 -13 -9 95.27 7.52 0 -13 9 81.39 8.79 0 13 9 78.38 8.88 0 13 9 83.10 4.53 0 13 9 78.51 7.73 0 -13 9 96.97 8.19 0 -13 -9 93.80 9.72 0 13 -9 92.31 9.63 0 13 9 101.32 9.18 0 -13 -10 3.60 7.79 0 -13 -10 7.24 5.50 0 13 10 4.28 6.42 0 -13 10 2.05 4.72 0 13 10 0.16 2.96 0 13 -10 9.41 7.57 0 -13 -10 -3.33 7.83 0 -13 10 -3.10 7.20 0 13 10 4.16 7.64 0 -13 -10 10.60 8.22 0 -13 11 10.85 5.03 0 13 11 2.75 6.34 0 -13 -11 -1.03 5.66 0 13 11 12.21 8.47 0 -13 11 17.14 8.26 0 -13 -11 11.19 8.48 0 13 -11 4.96 8.50 0 -13 11 12.80 9.14 0 13 11 11.87 3.37 0 13 -11 10.01 9.11 0 -13 -11 18.79 8.87 0 13 -12 127.77 8.60 0 13 12 155.30 10.79 0 -13 -12 169.26 10.35 0 13 12 169.76 13.18 0 -13 12 160.85 12.82 0 -13 -12 170.74 14.15 0 -13 -12 182.18 13.69 0 -13 12 148.01 13.38 0 13 12 159.04 7.57 0 13 -12 204.19 15.29 0 13 -12 149.80 13.75 0 -13 -12 166.94 14.03 0 -13 -13 68.26 12.00 0 -13 -13 90.09 11.50 0 -13 -13 85.22 7.63 0 -13 13 85.93 11.13 0 13 13 60.55 10.91 0 13 -13 40.25 7.90 0 -13 13 93.28 11.42 0 13 13 66.37 4.92 0 13 -13 80.33 12.54 0 -13 -13 58.32 11.76 0 13 -13 48.30 10.96 0 -13 -14 5.04 10.46 0 13 -14 1.43 5.90 0 -13 -14 -4.04 9.85 0 -13 -14 6.07 6.00 0 13 14 14.73 9.67 0 -13 14 14.19 9.46 0 -13 14 19.57 9.99 0 13 -14 -1.64 9.84 0 -13 -14 5.78 10.57 0 13 -14 -1.65 11.18 0 -13 -15 -7.89 10.53 0 13 -15 11.54 11.50 0 -13 -15 7.12 10.90 0 -13 -15 -15.02 6.75 0 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211.55 10.70 0 -14 2 211.95 10.69 0 14 2 190.33 9.01 0 14 -2 219.82 10.76 0 -14 2 220.12 10.56 0 14 2 207.60 8.51 0 -14 -2 188.75 8.79 0 14 -2 202.88 8.83 0 -14 2 222.14 8.32 0 14 3 249.04 13.72 0 14 -3 278.17 13.88 0 -14 -3 255.48 12.56 0 14 3 265.86 13.07 0 -14 3 286.82 12.49 0 -14 3 272.74 10.97 0 14 3 260.31 11.19 0 -14 -3 247.27 13.16 0 14 -3 266.04 12.82 0 -14 3 276.60 12.98 0 14 3 232.79 10.45 0 14 -3 275.06 12.50 0 -14 3 252.06 12.54 0 14 3 261.55 10.99 0 14 -3 280.09 11.46 0 -14 3 285.92 10.85 0 -14 -3 252.39 11.36 0 -14 4 1.48 3.18 0 14 -4 2.37 3.91 0 14 4 0.90 3.40 0 -14 -4 -1.01 5.16 0 -14 4 6.56 6.01 0 14 -4 -3.58 5.72 0 14 4 -2.18 5.86 0 -14 4 1.85 3.48 0 -14 4 0.25 4.30 0 14 4 3.01 5.58 0 14 4 -1.88 3.78 0 -14 4 -5.98 5.62 0 -14 -4 -0.84 5.16 0 14 -4 1.13 4.69 0 -14 4 -3.34 5.39 0 14 5 6.40 3.86 0 -14 5 5.38 3.60 0 -14 -5 2.58 5.12 0 -14 5 11.75 5.97 0 14 -5 0.99 5.36 0 -14 -5 0.76 6.27 0 14 5 9.01 6.02 0 -14 5 1.56 3.73 0 -14 -5 4.65 3.26 0 -14 5 3.03 4.06 0 -14 5 8.53 4.68 0 14 5 3.52 4.35 0 14 5 0.34 5.36 0 -14 5 9.28 5.67 0 -14 -5 10.78 5.39 0 14 -5 9.40 4.90 0 14 6 315.07 14.70 0 -14 6 340.10 14.71 0 -14 -6 323.60 16.53 0 14 6 335.66 16.01 0 -14 6 366.55 16.59 0 14 -6 351.85 16.21 0 -14 -6 307.95 16.51 0 14 6 336.16 16.62 0 -14 -6 319.83 15.27 0 -14 6 340.25 14.86 0 -14 -6 340.09 13.84 0 -14 6 368.56 15.68 0 -14 6 321.95 15.04 0 14 6 293.90 15.09 0 -14 6 348.51 16.56 0 14 -6 345.56 16.38 0 -14 -6 318.27 16.24 0 14 -6 349.16 15.61 0 14 6 313.48 15.76 0 -14 7 64.06 6.13 0 14 7 54.92 6.05 0 -14 -7 51.88 7.73 0 14 7 66.20 7.44 0 14 -7 60.33 7.48 0 -14 -7 70.31 8.30 0 -14 7 57.85 7.60 0 -14 -7 41.43 6.02 0 14 7 51.98 7.39 0 -14 -7 50.70 4.34 0 -14 7 58.14 5.71 0 -14 7 55.16 6.59 0 14 7 42.04 6.54 0 -14 7 67.85 6.84 0 -14 7 68.56 8.33 0 14 -7 62.27 7.56 0 -14 -7 59.88 8.19 0 14 7 59.38 7.54 0 14 -7 64.71 7.10 0 -14 -8 21.62 7.46 0 14 -8 13.32 6.84 0 -14 -8 7.34 6.99 0 14 8 12.35 6.45 0 -14 -8 14.34 5.61 0 -14 8 14.22 4.71 0 -14 -8 16.76 3.54 0 -14 8 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521.13 22.72 0 -21 -6 478.16 20.01 0 -21 6 484.42 19.79 0 21 6 464.66 20.07 0 -21 6 485.00 22.75 0 21 -6 491.42 20.91 0 -21 6 481.63 19.38 0 21 6 470.97 19.63 0 -21 -6 430.36 20.69 0 21 -6 522.89 21.90 0 21 -7 15.05 6.00 0 21 7 11.04 4.93 0 -21 7 5.05 4.50 0 -21 -7 16.73 6.30 0 -21 -7 3.37 8.04 0 21 -7 15.50 7.78 0 21 7 -0.55 8.00 0 -21 -7 10.77 6.52 0 -21 -7 15.07 4.56 0 -21 7 19.50 5.37 0 21 7 4.92 5.56 0 -21 7 4.19 8.20 0 21 -7 11.23 7.45 0 21 7 8.59 6.93 0 -21 -8 5.39 8.23 0 21 -8 0.96 8.15 0 21 8 7.79 8.18 0 -21 -8 10.32 6.71 0 -21 -8 6.28 4.21 0 21 8 3.53 6.17 0 -21 8 9.47 5.95 0 -21 8 5.02 8.75 0 21 -8 9.35 8.50 0 -21 -8 5.00 6.90 0 21 -8 0.41 6.80 0 21 8 1.55 5.33 0 -21 8 4.71 5.03 0 -21 -9 -8.35 8.69 0 21 -9 3.77 7.49 0 -21 -9 7.62 6.54 0 21 9 12.88 8.04 0 -21 -9 -1.01 3.93 0 -21 9 4.30 8.90 0 21 -9 5.22 6.88 0 -21 9 5.89 5.28 0 -21 -9 5.75 7.13 0 -21 9 0.33 6.17 0 21 9 2.94 6.49 0 21 -9 6.89 8.71 0 21 -10 35.01 8.79 0 -21 -10 42.70 7.56 0 21 10 41.12 9.11 0 21 10 49.01 8.08 0 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182.37 13.45 0 25 4 150.18 10.69 0 25 -4 175.30 9.60 0 -25 -4 170.33 10.07 0 25 4 139.60 7.06 0 -25 4 178.66 11.25 0 -25 4 185.61 11.27 0 25 4 175.16 11.33 0 25 -4 162.40 11.04 0 25 4 159.03 6.23 0 -25 -5 270.40 16.21 0 25 -5 302.79 17.13 0 25 5 285.03 17.05 0 25 5 271.14 14.88 0 25 -5 284.40 13.25 0 -25 -5 252.64 14.01 0 25 -5 275.02 14.49 0 25 5 267.73 11.08 0 25 5 258.24 14.69 0 -25 5 270.45 15.13 0 -25 5 299.50 15.42 0 -25 5 247.69 10.34 0 25 -5 243.00 11.39 0 25 5 248.87 10.79 0 -25 5 228.48 10.17 0 -25 -5 227.36 11.39 0 -25 -6 83.32 7.18 0 25 6 88.53 5.95 0 25 -6 88.52 7.11 0 -25 6 79.27 5.25 0 -25 -6 81.64 10.43 0 25 -6 110.14 11.27 0 25 6 90.04 11.06 0 -25 -6 93.21 7.53 0 25 6 82.60 6.36 0 -25 6 88.97 5.73 0 -25 6 103.08 10.97 0 25 -6 95.99 9.81 0 -25 6 74.49 9.95 0 -25 -7 31.86 9.29 0 25 -7 51.60 9.91 0 25 7 45.87 9.86 0 -25 -7 49.57 5.93 0 -25 7 40.09 9.63 0 25 7 39.39 6.06 0 -25 7 43.90 5.32 0 25 -7 57.32 6.84 0 25 7 54.00 5.46 0 -25 7 46.42 4.84 0 -25 -7 47.88 6.81 0 25 -7 52.10 9.07 0 25 -8 0.56 8.51 0 -25 -8 1.91 7.23 0 25 8 -0.65 8.48 0 25 8 -4.15 4.88 0 25 -8 7.20 6.44 0 -25 -8 4.98 6.49 0 -25 -8 1.34 8.72 0 -25 8 -1.09 9.04 0 25 8 -0.56 5.49 0 -25 8 0.24 4.95 0 25 -8 0.56 8.23 0 25 -9 25.84 8.99 0 25 9 7.79 9.20 0 -25 -9 28.56 7.84 0 -25 -9 12.48 7.42 0 25 -9 18.53 7.36 0 -25 -9 12.76 9.10 0 -25 9 23.19 10.52 0 -25 9 25.63 6.04 0 25 9 22.49 6.60 0 25 -9 41.00 10.03 0 25 -10 28.21 8.99 0 -25 -10 25.64 7.81 0 25 10 35.12 9.73 0 25 -10 31.16 8.09 0 -25 -10 30.41 8.28 0 -25 -10 45.90 11.03 0 -25 10 53.47 11.26 0 25 10 27.04 7.23 0 -25 10 30.66 6.57 0 25 -10 47.39 10.17 0 25 -11 8.66 8.45 0 25 11 37.05 9.70 0 -25 -11 27.56 7.99 0 25 -11 16.37 8.58 0 -25 -11 17.60 8.63 0 -25 -11 20.06 10.83 0 -25 11 25.24 11.41 0 25 -11 51.33 11.37 0 25 11 23.49 7.44 0 -25 11 25.73 7.10 0 -25 -12 65.78 12.28 0 -25 -12 46.63 8.74 0 25 12 50.35 10.38 0 -25 -12 46.53 10.22 0 25 -12 57.56 10.15 0 25 -12 33.45 9.18 0 -25 12 46.78 11.64 0 25 -12 76.48 12.84 0 -25 12 44.34 8.23 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8.23 0 -26 7 7.82 4.16 0 26 7 13.17 4.92 0 26 -8 136.75 12.65 0 26 8 162.86 13.40 0 -26 -8 138.36 11.30 0 -26 8 129.17 8.33 0 26 8 143.48 9.06 0 -26 8 167.96 13.41 0 -26 -8 128.96 13.17 0 -26 -8 142.24 10.10 0 26 -8 135.46 10.12 0 26 8 125.76 8.35 0 26 -8 147.06 12.59 0 26 -9 17.09 8.71 0 26 9 -0.67 8.85 0 -26 -9 -3.00 7.08 0 26 -9 1.29 6.93 0 -26 -9 7.80 6.75 0 -26 -9 11.62 9.56 0 -26 9 5.90 9.67 0 26 9 1.57 5.96 0 -26 9 -3.22 5.28 0 26 -9 -3.73 8.91 0 26 -10 71.65 10.67 0 -26 -10 67.16 9.21 0 26 10 63.82 10.85 0 26 -10 69.19 9.27 0 -26 -10 61.83 9.31 0 -26 -10 85.38 12.07 0 -26 10 82.46 12.42 0 26 10 72.23 8.47 0 -26 10 76.94 7.81 0 26 -10 92.01 11.97 0 26 -11 15.78 8.67 0 -26 -11 33.44 8.03 0 26 11 32.84 10.20 0 26 -11 5.53 7.90 0 -26 -11 20.01 8.58 0 -26 -11 26.20 11.05 0 -26 11 14.47 10.93 0 26 -11 30.74 10.80 0 26 11 17.97 7.39 0 -26 11 7.03 6.64 0 -26 -12 17.31 11.25 0 -26 -12 6.24 7.81 0 26 12 5.98 9.42 0 -26 -12 13.52 9.47 0 26 -12 12.88 8.85 0 26 -12 -6.87 8.77 0 -26 12 26.16 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17.63 4.48 0 27 -7 35.20 8.91 0 27 -8 6.66 8.70 0 27 8 15.95 9.52 0 -27 -8 12.77 7.66 0 27 -8 4.54 6.19 0 -27 -8 1.41 6.48 0 27 8 4.28 4.75 0 -27 -8 25.51 10.03 0 -27 8 20.87 10.02 0 27 8 6.69 5.38 0 -27 8 21.46 4.85 0 27 -8 23.24 8.91 0 27 -9 -4.72 8.90 0 27 9 5.55 8.91 0 -27 -9 4.65 7.55 0 -27 -9 5.43 7.04 0 27 -9 -2.89 6.86 0 -27 -9 -2.23 9.48 0 -27 9 -1.80 9.71 0 27 9 4.51 5.92 0 -27 9 3.54 5.10 0 27 -9 -13.91 9.07 0 27 -10 31.26 9.64 0 27 10 29.10 10.04 0 -27 -10 55.48 8.83 0 -27 -10 27.38 8.18 0 27 -10 33.77 8.26 0 -27 -10 44.64 10.99 0 -27 10 45.67 11.14 0 27 10 30.34 7.03 0 -27 10 27.17 6.45 0 27 -10 23.32 10.06 0 27 -11 4.87 8.98 0 -27 -11 15.36 7.98 0 27 11 -6.21 10.07 0 27 -11 1.07 8.01 0 -27 -11 -4.33 8.26 0 -27 -11 22.45 11.14 0 -27 11 13.34 11.28 0 27 -11 11.84 10.80 0 27 11 -2.70 6.88 0 -27 11 5.71 6.41 0 -27 -12 36.08 12.00 0 -27 -12 51.10 9.17 0 27 12 44.59 10.78 0 27 -12 24.50 9.37 0 -27 -12 51.02 10.02 0 27 -12 18.65 9.26 0 -27 12 34.18 11.81 0 27 -12 23.82 12.27 0 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27.21 8.52 0 28 4 20.66 4.27 0 -28 4 35.52 8.63 0 -28 -4 23.97 7.04 0 28 -4 16.31 6.58 0 -28 -5 161.63 12.75 0 28 -5 175.77 13.88 0 28 5 139.60 13.17 0 28 -5 176.78 11.94 0 28 5 169.78 11.31 0 -28 5 169.96 11.59 0 -28 5 151.65 11.62 0 28 5 157.39 11.28 0 28 -5 145.55 9.10 0 28 -5 175.42 11.19 0 28 5 134.59 5.26 0 28 -6 76.02 5.73 0 28 6 74.60 5.34 0 -28 6 71.47 4.35 0 -28 -6 77.73 10.79 0 28 -6 105.77 12.14 0 28 6 93.93 12.29 0 28 6 62.48 9.05 0 28 -6 102.36 10.53 0 28 6 67.66 5.01 0 -28 -6 66.91 5.74 0 -28 6 80.50 10.70 0 28 -6 93.39 9.82 0 28 -6 87.08 8.00 0 -28 6 84.42 10.24 0 -28 -7 226.66 15.75 0 28 -7 243.14 15.94 0 28 7 210.93 16.05 0 28 7 242.05 14.46 0 28 7 195.85 10.08 0 -28 7 225.62 15.25 0 -28 7 186.19 9.30 0 28 -7 196.80 10.81 0 28 7 188.23 9.75 0 -28 -7 196.26 10.87 0 28 -7 236.00 14.72 0 28 -7 204.31 12.08 0 28 -8 30.65 9.84 0 -28 -8 29.56 8.18 0 28 8 34.37 10.42 0 -28 -8 37.25 6.72 0 28 -8 21.39 6.21 0 -28 -8 31.95 9.90 0 -28 8 36.15 10.24 0 -28 8 21.00 4.63 0 28 8 15.07 5.19 0 28 -8 27.23 9.52 0 28 -9 58.34 11.07 0 28 9 67.29 11.24 0 -28 -9 92.70 9.84 0 28 -9 61.21 8.37 0 -28 -9 54.33 8.00 0 -28 -9 44.13 11.16 0 -28 9 87.15 11.99 0 28 9 60.25 7.13 0 -28 9 57.88 6.32 0 28 -9 79.64 11.04 0 28 -10 -0.59 8.68 0 -28 -10 14.02 7.94 0 28 10 17.13 9.31 0 28 -10 4.13 7.30 0 -28 -10 -8.80 7.39 0 -28 -10 12.00 10.37 0 -28 10 17.38 10.72 0 -28 10 1.67 5.50 0 28 10 -3.97 6.17 0 28 -10 9.73 10.07 0 28 -11 94.54 11.70 0 -28 -11 114.07 11.19 0 28 11 125.74 13.18 0 -28 -11 95.83 11.02 0 28 -11 90.36 10.72 0 -28 -11 118.57 14.16 0 -28 11 125.84 14.25 0 28 11 94.92 9.28 0 28 -11 107.74 14.03 0 28 -12 -4.12 8.71 0 -28 -12 5.46 8.00 0 28 12 4.93 10.04 0 28 -12 -0.58 8.55 0 28 -12 -3.21 11.22 0 -28 12 -1.41 11.56 0 -28 -12 11.63 11.78 0 28 12 0.41 7.42 0 28 13 11.58 7.91 0 28 13 9.66 10.18 0 -28 -13 6.58 8.18 0 -28 -13 23.43 12.69 0 -28 13 23.47 12.35 0 28 -13 5.98 12.58 0 28 -13 8.89 8.98 0 29 0 -2.84 7.21 0 29 0 1.69 6.41 0 29 0 2.00 6.52 0 -29 0 -0.85 5.63 0 29 0 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187.43 14.60 0 29 5 189.76 15.13 0 29 -6 23.45 3.85 0 -29 -6 17.27 3.93 0 29 6 20.22 3.60 0 -29 -6 24.65 9.50 0 29 -6 37.07 10.37 0 29 6 15.53 10.31 0 29 -6 21.28 8.18 0 29 6 16.47 7.85 0 -29 6 21.90 9.12 0 29 -6 29.12 6.58 0 29 -6 29.32 8.37 0 -29 6 33.67 8.84 0 -29 -7 20.72 9.60 0 29 -7 18.54 9.97 0 29 7 26.58 10.84 0 29 7 18.65 7.98 0 29 7 19.13 4.14 0 29 -7 23.86 5.09 0 -29 -7 11.55 5.12 0 -29 7 24.59 9.88 0 29 -7 16.47 6.74 0 29 -7 33.96 9.16 0 29 7 18.79 4.55 0 -29 -8 10.43 9.79 0 29 -8 5.17 9.18 0 -29 -8 13.63 7.65 0 29 8 2.22 9.40 0 29 8 4.55 8.37 0 -29 8 13.99 10.18 0 29 8 -0.91 4.80 0 29 -8 2.10 5.72 0 -29 -8 2.75 5.64 0 29 -8 -2.86 6.79 0 29 -8 11.46 9.02 0 29 -9 12.54 9.74 0 29 9 22.13 10.14 0 -29 -9 25.26 8.28 0 29 -9 20.86 6.73 0 -29 -9 10.89 10.32 0 -29 9 3.09 10.44 0 29 9 12.32 5.77 0 29 -9 21.54 10.00 0 29 -10 14.44 9.31 0 -29 -10 -6.10 8.19 0 29 -10 -4.80 7.31 0 -29 -10 25.26 10.67 0 -29 10 6.53 10.52 0 29 10 7.28 6.12 0 29 -10 8.45 10.32 0 29 -11 13.67 9.67 0 29 11 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6 -6.67 11.24 0 33 -6 -1.32 8.76 0 33 6 0.59 8.35 0 -33 -6 22.95 10.50 0 -33 6 5.46 9.27 0 -33 6 5.15 8.95 0 33 -6 10.17 8.78 0 33 -6 2.00 6.51 0 33 7 43.12 11.88 0 33 7 52.01 9.83 0 -33 -7 46.65 11.52 0 -33 7 36.62 10.59 0 33 -7 36.32 11.35 0 33 -7 33.60 7.49 0 33 -7 39.92 10.14 0 -33 -8 4.32 8.82 0 33 8 -0.83 10.60 0 33 8 11.16 8.84 0 -33 -8 0.82 10.29 0 -33 8 16.67 10.67 0 33 -8 0.72 10.52 0 33 -8 6.48 9.89 0 33 -8 -5.78 7.03 0 33 9 -4.92 11.26 0 -33 -9 46.28 9.76 0 33 9 16.54 9.34 0 -33 -9 41.41 11.87 0 -33 9 35.87 11.39 0 33 -9 17.99 10.65 0 33 -9 13.52 7.22 0 33 -9 9.00 10.38 0 -33 -10 6.77 8.87 0 33 10 5.69 10.62 0 33 10 -2.61 9.11 0 -33 -10 -5.25 11.33 0 -33 10 21.23 11.58 0 33 -10 -1.98 9.57 0 33 -10 3.70 10.46 0 -33 -11 31.32 9.42 0 33 11 20.88 11.39 0 33 11 23.33 9.80 0 -33 -11 24.62 11.81 0 -33 11 27.17 11.82 0 33 -11 26.73 11.86 0 33 -11 20.42 10.39 0 34 0 90.97 10.35 0 -34 0 103.39 10.61 0 34 0 75.84 8.76 0 34 0 86.50 13.13 0 34 -1 15.49 6.82 0 34 1 17.56 7.14 0 34 1 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362.48 13.95 -1 9 0 377.87 13.99 -1 -9 -1 229.76 11.10 1 -9 1 237.28 10.58 1 -9 1 251.43 11.34 1 9 1 225.08 11.73 1 9 1 240.35 9.89 1 -9 1 235.58 10.89 1 -9 1 246.05 10.33 -1 9 -1 258.49 10.43 -1 -9 -1 232.46 10.09 -1 9 -1 275.38 10.16 -1 -9 -2 195.05 10.03 1 -9 2 193.56 9.12 1 9 2 184.91 10.38 -1 9 -2 210.67 9.70 1 -9 2 194.72 9.15 1 -9 2 201.05 9.98 -1 9 -2 197.49 8.96 -1 -9 -2 171.10 8.98 -1 9 -2 220.96 9.17 1 9 3 594.61 24.63 -1 -9 -3 571.46 24.96 -1 9 -3 645.48 24.36 1 -9 3 629.26 24.87 1 9 3 583.95 24.95 -1 -9 -3 595.70 25.02 1 -9 3 621.08 24.36 1 -9 3 623.26 24.99 -1 9 -3 634.67 24.98 -1 9 -3 687.78 24.56 -1 -9 -3 573.63 24.29 -1 9 -3 580.96 24.03 -1 -9 -4 -4.81 4.70 -1 9 -4 0.96 4.67 1 9 4 3.78 4.73 1 -9 4 3.26 5.41 -1 -9 -4 2.61 5.48 -1 9 -4 2.09 4.36 1 9 4 0.26 5.15 -1 -9 -4 3.97 4.13 -1 -9 -4 2.22 2.24 1 -9 4 1.45 3.99 1 -9 4 6.93 4.48 -1 9 -4 4.39 5.57 1 -9 4 4.56 5.65 -1 -9 -4 1.38 5.72 -1 9 -4 0.19 4.54 -1 9 -5 326.45 14.72 -1 -9 -5 295.82 14.41 1 9 5 282.21 14.20 -1 9 -5 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-4 -1 63.77 4.35 -2 4 -1 70.15 4.27 -2 -4 -1 67.96 2.98 2 -4 1 59.37 5.41 2 -4 1 66.06 4.26 2 4 1 64.22 4.34 2 -4 1 61.77 4.30 -2 -4 -1 49.02 5.23 2 -4 1 60.40 3.89 2 4 1 56.89 5.31 -2 4 -1 60.20 4.03 2 4 2 28.97 4.21 2 -4 2 37.85 3.95 -2 -4 -2 14.03 4.17 -2 -4 -2 26.84 3.59 -2 4 -2 25.46 3.44 2 4 2 31.71 3.81 2 -4 2 28.04 4.79 -2 4 -2 39.31 4.94 2 -4 2 34.98 3.96 2 4 2 29.05 5.11 -2 -4 -2 27.78 5.06 -2 4 -2 32.38 4.06 -2 -4 -2 28.29 4.47 2 -4 2 36.33 4.34 -2 -4 -3 355.57 15.81 2 4 3 334.44 14.54 -2 -4 -3 317.29 14.58 2 -4 3 370.00 14.65 -2 4 -3 346.44 14.88 -2 -4 -3 356.69 14.80 -2 4 -3 374.65 14.92 -2 4 -3 407.05 15.90 2 4 3 342.63 14.94 2 -4 3 347.82 15.11 2 -4 3 344.07 15.84 2 4 3 339.36 15.54 2 -4 3 360.39 15.05 -2 4 -3 362.88 15.00 2 4 3 361.86 15.99 -2 -4 -3 368.21 15.90 -2 -4 -4 1908.00 72.47 2 4 4 1899.06 71.64 2 -4 4 1950.58 71.90 2 -4 4 1934.96 71.21 2 4 4 1831.36 70.90 -2 -4 -4 1781.37 70.98 -2 4 -4 1967.74 71.58 -2 -4 -4 1887.67 71.45 -2 4 -4 1963.05 71.56 2 4 4 1939.59 71.63 -2 4 -4 2010.13 72.26 2 4 4 1947.24 72.54 -2 4 -4 2010.24 71.80 -2 -4 -4 1951.59 72.43 2 4 4 1844.76 72.03 2 -4 4 1874.98 71.65 2 4 5 1.48 4.65 -2 -4 -5 3.69 4.60 2 -4 5 9.23 4.97 2 -4 5 3.44 4.31 -2 4 -5 6.31 5.20 -2 -4 -5 2.70 4.04 -2 -4 -5 -0.43 3.98 2 4 5 1.89 3.89 2 4 5 2.72 3.55 2 -4 5 4.87 3.73 -2 4 -5 5.24 4.02 -2 4 -5 3.52 5.41 2 4 5 0.99 6.02 -2 4 -5 0.57 5.49 2 4 5 6.20 4.88 2 -4 5 4.48 4.87 -2 -4 -5 2.38 5.70 -2 -4 -6 279.10 14.72 -2 -4 -6 265.41 13.31 2 -4 6 281.69 13.89 2 -4 6 282.41 13.07 2 4 6 280.12 13.63 -2 -4 -6 264.23 12.50 -2 4 -6 291.57 13.81 2 4 6 287.67 12.86 2 4 6 261.05 12.02 -2 -4 -6 285.50 13.04 2 -4 6 296.79 12.77 -2 4 -6 312.61 14.37 -2 4 -6 288.82 13.06 2 4 6 284.60 10.84 2 4 6 290.23 13.41 -2 4 -6 298.60 14.00 2 -4 6 275.89 13.49 -2 -4 -7 4.07 5.99 2 4 7 9.64 5.21 2 -4 7 8.36 5.05 2 -4 7 8.70 5.42 -2 -4 -7 7.24 5.40 -2 4 -7 8.51 2.21 -2 4 -7 8.31 5.95 -2 -4 -7 8.42 4.31 -2 -4 -7 2.90 4.20 2 -4 7 6.90 3.97 2 4 7 13.11 3.42 2 4 7 7.72 4.17 -2 4 -7 8.83 4.34 2 4 7 7.10 2.05 -2 4 -7 17.23 6.26 2 -4 7 9.14 6.17 2 4 7 5.86 5.09 -2 4 -7 7.29 5.83 2 -4 7 13.69 5.60 -2 4 -7 13.70 6.90 -2 -4 -8 46.12 8.94 2 -4 8 51.48 7.71 2 4 8 60.17 7.77 -2 -4 -8 67.04 8.03 -2 4 -8 75.79 8.59 -2 -4 -8 52.86 6.20 -2 4 -8 62.23 4.08 2 -4 8 70.81 6.23 2 4 8 65.17 6.38 -2 -4 -8 62.81 6.55 -2 4 -8 55.70 6.68 2 4 8 61.05 3.84 -2 4 -8 57.51 8.61 2 -4 8 39.27 8.03 2 4 8 36.54 7.10 -2 4 -8 37.39 8.30 -2 4 -8 63.48 10.01 2 -4 8 62.52 7.99 -2 4 -9 13.70 7.43 -2 4 -9 10.10 3.14 -2 -4 -9 19.23 5.19 -2 -4 -9 27.96 7.10 2 4 9 13.84 2.84 -2 4 -9 11.05 5.09 -2 -4 -9 14.39 5.23 2 4 9 14.52 5.12 2 -4 9 20.49 5.03 2 4 9 15.95 6.28 2 -4 9 12.77 7.46 -2 4 -9 8.17 7.28 -2 -4 -9 10.91 7.89 -2 4 -9 14.35 8.78 -2 -4 -10 67.45 6.81 -2 -4 -10 80.89 9.44 -2 4 -10 68.47 4.29 -2 4 -10 87.09 10.17 -2 4 -10 79.85 7.26 2 4 10 52.73 4.32 -2 -4 -10 65.04 7.12 2 -4 10 61.93 6.70 2 4 10 64.13 6.98 2 4 10 68.00 8.23 2 -4 10 75.41 9.73 -2 4 -10 65.29 11.28 -2 -4 -10 51.82 10.40 -2 -4 -11 22.56 9.67 2 -4 11 12.98 8.11 2 4 11 21.64 6.94 2 4 11 11.72 3.13 -2 4 -11 11.09 5.73 -2 -4 -11 11.16 5.52 -2 4 -11 23.84 10.09 -2 -4 -11 24.14 8.23 -2 4 -11 16.04 8.52 -2 -4 -11 21.95 5.56 -2 4 -11 6.90 2.27 -2 -4 -12 65.67 11.56 2 -4 12 71.90 10.20 2 4 12 95.98 9.17 2 4 12 68.80 4.76 -2 4 -12 86.10 8.04 -2 -4 -12 78.08 7.80 -2 4 -12 82.84 12.47 -2 -4 -12 101.45 10.84 -2 -4 -12 70.02 6.83 -2 4 -12 103.30 11.58 -2 -4 -13 13.43 10.02 -2 4 -13 21.24 6.21 -2 -4 -13 23.78 6.40 2 -4 13 33.17 9.28 2 4 13 20.01 7.59 -2 4 -13 8.14 11.54 -2 4 -13 8.12 9.99 -2 -4 -13 31.05 9.57 -2 -4 -14 5.44 10.95 2 -4 14 -2.30 4.97 -2 -4 -14 0.84 6.27 -2 4 -14 -5.65 6.17 2 -4 14 10.48 9.99 2 -4 14 -3.80 9.29 2 4 14 -9.85 8.17 -2 4 -14 -1.76 11.11 -2 -4 -14 -15.26 9.95 -2 4 -14 -5.41 10.50 -2 -4 -15 3.89 11.41 -2 4 -15 24.98 7.04 -2 -4 -15 18.11 7.19 2 -4 15 11.95 5.42 2 -4 15 7.75 10.20 2 4 15 33.17 8.59 2 -4 15 25.88 11.57 -2 4 -15 49.98 13.62 -2 -4 -15 -2.05 10.65 -2 4 -15 16.70 11.46 2 -4 16 -4.08 11.88 2 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-14 37.29 10.27 2 5 -13 23.81 10.26 2 -5 -13 20.37 9.47 -2 -5 13 8.87 3.95 2 5 -13 12.62 6.20 -2 -5 13 20.73 6.53 2 -5 -13 11.29 4.23 -2 5 13 17.71 5.57 -2 -5 13 28.76 8.50 2 -5 -13 13.75 6.52 -2 5 13 11.21 5.61 -2 -5 13 12.67 7.75 2 -5 -13 20.85 9.35 2 5 -13 27.18 10.26 2 -5 -13 24.07 9.18 2 -5 -12 87.34 10.64 2 5 -12 68.04 10.62 -2 -5 12 69.88 5.20 2 -5 -12 56.97 8.10 2 -5 -12 69.68 5.54 2 5 -12 63.05 7.11 -2 5 12 71.86 6.72 -2 -5 12 68.43 9.34 -2 5 12 77.25 6.75 -2 -5 12 64.27 8.63 2 -5 -12 77.95 7.54 2 5 -12 82.31 10.79 2 -5 -12 74.47 9.95 2 -5 -12 69.14 10.30 2 -5 -11 164.41 12.46 2 -5 -11 161.80 10.63 -2 -5 11 160.47 7.63 2 -5 -11 138.16 7.87 2 5 -11 157.63 9.36 -2 5 11 163.07 9.19 -2 -5 11 179.40 11.81 -2 5 11 147.23 8.80 2 5 -11 149.86 11.09 2 -5 -11 137.65 9.38 -2 -5 11 148.70 10.75 -2 5 11 133.97 10.21 2 5 -11 175.21 12.72 2 -5 -11 146.86 11.96 -2 -5 10 149.61 9.31 2 -5 -10 123.50 10.60 2 -5 -10 128.17 9.37 2 5 -10 144.17 8.37 -2 -5 10 137.01 6.79 2 -5 -10 128.18 6.99 -2 5 10 136.38 8.20 -2 -5 10 129.90 10.07 -2 -5 10 135.63 9.12 2 -5 -10 143.61 8.44 -2 5 10 141.40 7.89 2 5 -10 138.51 9.76 -2 -5 10 129.54 9.54 2 -5 -10 138.47 10.62 2 5 -10 152.35 11.02 -2 5 10 131.88 9.08 2 -5 -9 61.39 7.79 -2 -5 9 60.61 7.43 -2 5 9 53.87 6.49 -2 -5 9 63.07 4.20 2 -5 -9 64.97 4.59 2 -5 -9 65.08 6.90 -2 5 9 65.24 5.73 -2 -5 9 63.01 7.40 -2 -5 9 62.95 6.53 -2 5 9 70.15 5.27 2 -5 -9 58.73 5.68 2 5 -9 75.66 7.12 -2 -5 9 55.89 7.06 2 5 -9 80.22 8.22 2 -5 -9 70.38 7.75 -2 -5 9 71.78 6.64 -2 -5 8 1949.72 74.08 2 -5 -8 1974.28 74.40 2 -5 -8 1961.08 72.89 -2 -5 8 1966.53 72.64 -2 5 8 1905.09 73.65 -2 -5 8 1927.01 74.64 -2 -5 8 1951.04 74.22 -2 -5 8 2002.48 74.36 2 5 -8 2054.21 74.49 2 -5 -8 1892.60 73.23 -2 5 8 2071.31 73.04 -2 5 8 1942.74 73.98 2 -5 -8 2009.78 74.84 2 5 -8 2002.90 75.15 -2 -5 8 1969.63 74.75 2 -5 -8 1916.34 75.29 2 -5 -7 101.79 7.88 -2 -5 7 100.91 7.73 2 5 -7 106.81 8.58 2 -5 -7 97.31 5.24 -2 -5 7 90.16 4.86 2 -5 -7 106.34 7.38 -2 5 7 83.68 6.27 -2 -5 7 96.91 7.43 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262.16 12.84 6 -3 -7 235.89 9.36 6 -3 -7 246.35 12.09 6 -3 -7 243.28 11.64 -6 -3 7 241.20 12.14 -6 -3 7 197.05 9.10 -6 -3 7 241.86 10.49 6 -3 -7 243.74 11.67 -6 3 7 246.04 9.60 6 3 -7 250.17 11.49 6 -3 -7 249.09 11.74 6 -3 -7 241.38 10.42 6 3 -7 239.49 12.15 6 -3 -6 48.23 5.37 -6 -3 6 46.43 4.41 -6 3 6 55.80 4.36 6 -3 -6 55.86 4.59 6 -3 -6 55.18 6.09 6 3 -6 42.14 6.28 6 -3 -6 48.73 5.82 -6 -3 6 59.14 3.51 6 -3 -6 54.88 3.51 -6 -3 6 49.92 5.84 6 -3 -6 60.85 5.79 -6 3 6 53.75 6.07 -6 3 6 43.66 2.88 6 3 -6 47.20 4.27 -6 -3 6 50.18 4.25 -6 -3 6 52.21 5.63 6 -3 -6 49.61 5.31 6 -3 -6 52.84 5.52 -6 -3 6 55.13 6.87 6 3 -6 57.11 6.37 6 -3 -5 528.27 22.18 -6 -3 5 522.61 20.94 -6 3 5 549.10 20.88 6 -3 -5 529.28 20.93 6 -3 -5 548.86 22.34 6 3 -5 548.94 22.33 6 3 -5 531.01 20.99 -6 -3 5 549.84 21.10 6 -3 -5 546.34 22.41 6 -3 -5 573.09 21.13 -6 3 5 530.84 22.73 6 -3 -5 555.33 22.28 -6 -3 5 552.98 22.62 -6 3 5 544.35 21.19 6 3 -5 514.95 21.12 -6 -3 5 545.89 22.82 6 -3 -5 549.35 21.83 6 3 -5 565.63 22.56 6 -3 -5 549.03 22.04 6 -3 -5 555.63 22.50 -6 -3 5 541.96 22.59 -6 -3 4 0.79 2.18 6 -3 -4 0.56 1.90 6 3 -4 4.45 4.33 6 -3 -4 -4.18 4.19 6 3 -4 -0.55 2.91 6 -3 -4 0.43 2.85 -6 -3 4 -0.45 3.06 -6 3 4 -2.95 4.71 -6 3 4 -1.29 3.27 -6 -3 4 0.71 4.23 6 3 -4 1.54 2.96 6 -3 -4 -3.00 4.50 -6 -3 4 -5.08 4.71 6 -3 -4 3.77 3.81 6 -3 -4 2.92 3.70 6 3 -4 0.44 4.78 -6 -3 4 -0.47 4.85 6 -3 -3 162.88 9.22 6 -3 -3 161.93 8.36 -6 -3 3 140.90 6.19 6 3 -3 153.91 7.74 6 -3 -3 172.63 7.88 -6 -3 3 170.17 8.03 6 3 -3 168.92 7.85 6 -3 -3 153.85 8.27 -6 3 3 170.40 9.27 -6 -3 3 160.91 8.66 -6 3 3 152.69 8.13 6 3 -3 162.69 7.68 -6 3 3 152.45 7.79 6 -3 -3 156.81 7.64 -6 -3 3 155.38 8.88 6 -3 -3 144.14 8.50 6 3 -3 146.42 9.54 6 -3 -2 344.75 15.00 6 3 -2 350.27 16.15 -6 3 2 337.01 14.76 6 -3 -2 329.83 14.66 -6 -3 2 332.81 14.74 6 3 -2 341.41 14.45 6 -3 -2 350.78 14.52 6 -3 -2 339.40 14.43 -6 -3 2 326.87 14.56 -6 -3 2 338.07 12.85 -6 3 2 337.69 13.78 -6 -3 2 330.43 15.08 6 -3 -2 324.03 14.79 6 -3 -2 346.82 15.66 -6 -3 2 341.20 15.48 6 3 -1 809.48 33.02 6 -3 -1 816.48 32.21 6 3 -1 801.73 31.62 6 -3 -1 819.31 31.74 6 -3 -1 835.52 31.30 -6 -3 1 782.49 31.52 6 3 -1 745.20 31.14 6 -3 -1 804.11 31.65 -6 -3 1 793.93 30.41 6 -3 -1 821.61 30.20 -6 -3 1 811.22 32.10 6 -3 -1 827.12 31.67 -6 3 1 856.73 30.89 -6 -3 1 810.88 32.74 6 -3 -1 817.29 32.08 6 -3 -1 836.04 32.95 -6 -3 0 92.21 7.66 6 -3 0 69.11 3.87 6 3 0 99.67 6.58 6 -3 0 97.41 6.45 6 -3 0 89.02 5.32 6 -3 0 93.43 6.15 6 3 0 97.65 5.44 -6 -3 0 92.10 5.83 6 -3 0 85.98 4.86 6 3 0 83.34 4.97 -6 -3 0 89.14 5.22 6 -3 0 79.44 7.77 6 -3 0 76.09 6.46 -6 3 0 84.01 6.43 6 3 0 79.20 7.99 6 -3 0 79.16 7.18 -6 -3 0 95.23 7.51 6 3 1 198.52 11.87 -6 3 -1 217.10 10.48 -6 -3 -1 221.23 11.25 6 -3 1 204.89 11.09 6 -3 1 203.80 10.18 6 3 1 193.75 10.19 6 -3 1 193.18 8.75 6 3 1 195.78 8.86 6 -3 1 205.05 9.67 6 -3 1 200.48 9.19 6 3 1 198.30 9.17 -6 -3 -1 186.39 9.45 6 -3 1 199.61 11.59 6 -3 1 189.01 10.44 -6 -3 -1 213.16 11.65 -6 -3 -2 185.15 11.47 6 3 2 158.05 9.45 6 -3 2 149.52 7.60 -6 -3 -2 199.08 10.29 6 -3 2 206.33 9.87 6 3 2 207.40 10.02 6 3 2 171.92 7.94 -6 3 -2 192.12 10.20 6 -3 2 199.99 9.03 6 -3 2 172.94 8.91 6 3 2 160.71 8.80 -6 -3 -2 178.56 9.49 6 -3 2 183.11 11.18 6 -3 2 183.96 10.22 6 3 2 174.81 10.72 6 -3 2 186.23 10.63 -6 -3 -2 184.70 10.71 -6 3 -2 189.01 10.25 6 3 2 171.20 11.44 -6 -3 -3 1080.97 37.69 6 -3 3 1119.44 37.24 6 -3 3 1060.79 34.73 6 3 3 1049.70 34.66 -6 -3 -3 1035.34 35.37 6 3 3 953.34 34.07 6 -3 3 1101.55 35.35 -6 -3 -3 1036.17 35.84 6 3 3 1064.56 35.34 6 3 3 1026.39 32.96 -6 3 -3 1043.85 36.13 6 -3 3 1111.71 34.25 -6 -3 -3 1063.58 36.42 -6 3 -3 1097.35 35.77 6 -3 3 1132.31 36.48 6 3 3 1053.29 37.34 6 -3 3 1086.94 35.74 6 3 3 1085.78 36.52 6 -3 4 23.45 5.43 -6 -3 -4 24.75 6.05 6 3 4 18.64 5.34 -6 -3 -4 13.33 3.59 6 3 4 11.52 4.04 6 3 4 14.64 7.60 -6 -3 -4 27.91 7.12 -6 3 -4 20.45 6.53 6 -3 4 18.01 4.27 6 3 4 18.05 2.68 -6 -3 -4 22.94 6.06 -6 3 -4 12.39 5.96 6 -3 4 6.40 6.62 6 3 4 13.34 7.38 6 -3 4 24.82 6.95 -6 -3 -4 17.39 7.28 6 -3 4 22.30 6.35 6 3 4 27.47 7.19 6 -3 5 23.58 5.95 -6 -3 -5 34.85 7.06 6 3 5 27.04 6.06 -6 -3 -5 31.12 4.51 6 3 5 19.83 3.54 -6 -3 -5 22.77 6.17 -6 3 -5 29.09 6.78 6 -3 5 33.42 4.60 6 3 5 23.26 8.19 6 3 5 45.30 8.82 6 -3 5 32.14 8.82 -6 3 -5 25.99 7.40 -6 -3 -5 19.15 8.13 6 -3 6 12.33 6.47 -6 -3 -6 10.00 7.19 6 3 6 12.95 6.65 -6 -3 -6 18.88 5.13 6 3 6 13.94 2.05 -6 -3 -6 13.35 6.76 -6 3 -6 12.12 6.98 6 3 6 7.58 8.74 6 3 6 29.14 9.03 6 -3 6 7.93 8.70 -6 -3 -6 16.07 8.83 -6 3 -6 20.05 7.96 -6 -3 -7 130.79 10.36 -6 3 -7 114.73 10.27 -6 -3 -7 142.41 8.82 6 -3 7 141.72 12.86 6 3 7 136.94 12.15 -6 -3 -7 130.68 13.25 -6 -3 -7 138.99 11.41 6 3 8 58.67 10.06 6 -3 8 71.44 10.91 -6 -3 -8 42.70 10.72 -6 -3 -8 76.85 8.98 -6 3 -8 63.16 8.45 -6 -3 -8 71.83 7.32 6 3 9 115.24 11.91 6 -3 9 113.05 11.89 -6 -3 -9 91.42 12.55 -6 -3 -9 115.88 10.29 -6 3 -9 93.34 9.72 6 -3 9 91.25 6.28 -6 -3 -9 91.91 8.62 6 3 10 39.12 9.91 6 -3 10 40.36 10.77 -6 -3 -10 36.74 10.98 -6 -3 -10 43.21 8.43 -6 3 -10 41.60 8.51 -6 -3 -10 31.27 7.75 6 -3 11 13.58 10.46 6 3 11 17.45 9.73 -6 -3 -11 -6.39 11.12 -6 -3 -11 38.55 8.84 -6 3 -11 24.68 8.17 -6 -3 -11 43.76 8.44 6 3 12 2.43 9.51 6 -3 12 11.06 10.69 -6 -3 -12 -4.84 11.88 -6 -3 -12 -7.11 8.06 -6 3 -12 5.21 8.29 -6 -3 -12 -3.03 8.69 6 3 13 3.04 10.04 6 -3 13 9.06 10.75 -6 -3 -13 -13.27 12.50 -6 -3 -13 24.32 8.56 -6 3 -13 8.91 8.24 -6 -3 -13 6.02 8.45 6 3 14 -6.60 10.54 6 -3 14 5.57 11.32 -6 -3 -14 1.07 12.56 -6 -3 -14 -9.25 9.60 -6 3 -14 -6.60 8.80 6 4 -19 19.41 12.80 -6 -4 19 9.50 9.69 -6 -4 19 28.21 9.38 -6 4 19 2.66 8.72 6 4 -18 98.64 13.78 6 -4 -18 92.42 13.45 -6 -4 18 103.72 12.11 -6 4 18 104.37 10.99 -6 -4 18 100.87 11.29 -6 -4 17 6.08 8.36 6 -4 -17 7.04 9.71 6 4 -17 -7.73 10.55 6 4 -17 -5.16 11.92 -6 4 17 -2.03 7.75 -6 -4 17 -12.30 8.22 -6 -4 16 34.19 8.89 6 -4 -16 48.89 10.55 6 4 -16 29.72 10.46 6 -4 -16 56.02 12.19 6 4 -16 48.16 12.65 -6 -4 16 47.87 8.93 -6 4 16 42.65 8.45 -6 -4 15 25.51 8.10 6 -4 -15 10.19 8.71 6 4 -15 12.39 9.24 6 4 -15 50.02 11.90 6 -4 -15 53.45 11.20 -6 -4 15 24.65 7.87 -6 4 15 45.26 8.12 -6 -4 14 19.70 7.67 -6 4 14 19.41 7.56 -6 -4 14 29.59 7.94 6 4 -14 39.92 8.98 6 -4 -14 18.31 8.12 6 -4 -14 40.11 10.70 6 4 -14 41.39 10.87 6 -4 -13 25.94 9.22 6 4 -13 17.12 9.76 6 4 -13 2.87 7.75 -6 -4 13 -0.45 6.77 -6 4 13 15.51 6.89 -6 4 13 1.70 5.47 6 -4 -13 10.56 6.05 -6 -4 13 7.71 7.17 6 -4 -13 8.96 7.38 6 4 -12 131.02 12.20 -6 -4 12 123.85 9.81 -6 -4 12 131.12 10.16 -6 4 12 124.64 9.84 -6 4 12 116.57 8.01 -6 -4 12 110.35 8.56 6 -4 -12 101.73 8.50 6 4 -12 121.07 10.30 6 -4 -12 132.39 9.94 6 -4 -12 133.16 10.69 6 -4 -12 132.17 11.92 6 -4 -11 1.89 6.99 -6 -4 11 3.43 5.78 6 -4 -11 13.46 6.87 -6 4 11 0.99 5.61 6 -4 -11 7.50 7.64 6 4 -11 11.06 7.96 6 4 -11 7.52 6.51 -6 -4 11 -3.57 6.48 -6 4 11 3.12 6.15 -6 4 11 2.63 4.29 -6 -4 11 -1.84 4.82 6 4 -11 2.81 6.40 6 -4 -11 14.80 5.47 -6 -4 11 -1.14 6.05 6 -4 -11 -4.48 6.03 6 -4 -10 48.46 7.82 6 -4 -10 57.31 8.52 6 -4 -10 53.69 7.50 -6 -4 10 68.78 6.73 -6 4 10 59.14 6.70 6 4 -10 58.36 8.92 6 4 -10 49.08 7.07 -6 4 10 45.14 7.09 6 4 -10 58.14 7.19 6 -4 -10 51.26 5.97 6 -4 -10 63.31 8.01 6 -4 -10 58.17 6.63 -6 -4 10 57.37 5.78 -6 4 10 64.16 5.18 -6 -4 10 55.53 6.82 -6 -4 9 14.71 4.49 6 -4 -9 11.87 5.85 6 -4 -9 22.92 5.72 -6 -4 9 24.69 5.26 -6 4 9 16.59 4.97 6 -4 -9 17.38 6.70 6 4 -9 15.70 6.91 6 4 -9 14.62 5.29 6 -4 -9 17.95 5.92 -6 -4 9 13.88 4.39 -6 4 9 12.58 3.53 6 4 -9 18.09 5.75 6 -4 -9 12.81 4.54 -6 -4 9 14.07 5.28 6 -4 -9 12.47 6.17 6 4 -9 21.43 6.58 6 -4 -9 17.70 4.94 6 -4 -8 473.77 20.79 6 -4 -8 518.66 21.74 6 -4 -8 471.18 20.28 -6 -4 8 486.85 20.00 -6 4 8 487.52 19.88 6 4 -8 495.10 21.76 6 -4 -8 463.31 17.87 6 -4 -8 476.02 20.36 -6 -4 8 466.84 20.78 -6 -4 8 495.70 19.50 6 -4 -8 470.01 20.53 -6 4 8 466.72 18.57 6 4 -8 471.67 20.18 6 -4 -8 455.21 20.56 6 -4 -8 485.24 19.47 -6 -4 8 466.31 20.46 6 -4 -8 490.31 19.42 6 4 -8 479.05 20.87 6 -4 -7 11.56 4.68 -6 -4 7 12.46 4.62 6 -4 -7 4.71 4.64 -6 -4 7 8.12 3.95 6 -4 -7 8.83 4.11 6 -4 -7 6.63 5.62 -6 4 7 8.00 3.87 6 4 -7 6.91 5.87 6 -4 -7 12.51 2.28 6 -4 -7 5.53 5.06 6 -4 -7 12.16 4.74 -6 -4 7 9.13 1.95 -6 -4 7 7.76 5.02 -6 4 7 8.04 2.38 -6 -4 7 10.66 3.71 6 4 -7 8.06 4.94 6 -4 -7 7.42 3.47 6 -4 -7 5.15 5.20 6 4 -7 4.27 5.59 6 -4 -6 334.09 14.37 -6 -4 6 311.39 14.59 6 -4 -6 327.91 14.47 -6 4 6 330.30 13.46 6 -4 -6 317.25 13.57 -6 -4 6 302.38 13.50 -6 -4 6 313.66 14.44 6 4 -6 307.50 14.97 -6 -4 6 329.72 12.80 6 -4 -6 321.20 12.87 6 -4 -6 314.21 14.78 -6 4 6 324.25 15.13 6 -4 -6 336.69 14.55 -6 -4 6 325.54 14.90 6 4 -6 298.02 13.48 -6 -4 6 316.51 13.44 6 4 -6 319.87 14.30 -6 -4 6 304.31 15.44 6 -4 -6 321.95 12.91 6 -4 -6 331.91 14.27 6 4 -6 320.93 15.01 6 -4 -5 76.14 5.81 -6 -4 5 84.61 6.14 6 -4 -5 75.94 4.74 -6 -4 5 69.59 4.78 6 4 -5 78.18 6.71 6 -4 -5 73.54 4.72 6 -4 -5 76.14 6.47 -6 -4 5 80.70 4.71 -6 -4 5 82.57 6.44 -6 4 5 84.16 6.75 6 -4 -5 64.64 6.13 6 4 -5 70.97 5.00 -6 -4 5 92.55 7.46 6 4 -5 75.43 6.78 6 -4 -5 75.15 5.73 -6 -4 5 81.32 6.24 6 -4 -5 76.58 6.16 6 -4 -5 71.41 5.81 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53.96 5.00 7 6 -5 58.95 6.85 -7 -6 5 69.73 7.19 7 -6 -5 65.58 4.92 7 -6 -5 57.06 5.39 7 6 -5 61.72 5.51 -7 -6 5 59.45 6.39 7 -6 -5 73.03 6.18 7 6 -5 76.54 6.56 7 -6 -4 207.06 11.16 7 -6 -4 205.95 10.43 7 6 -4 228.98 10.70 7 6 -4 227.10 11.67 7 6 -4 193.99 10.47 7 -6 -4 218.33 10.08 -7 -6 4 218.80 10.22 7 -6 -4 232.88 11.04 -7 -6 4 211.75 10.97 -7 6 4 220.21 10.40 -7 -6 4 215.65 10.07 7 -6 -4 203.55 8.66 7 6 -4 201.58 10.06 -7 -6 4 217.27 11.61 7 -6 -4 213.03 8.97 7 -6 -4 218.80 9.41 7 6 -4 218.53 12.37 7 -6 -3 3.94 4.25 7 6 -3 3.85 6.08 7 6 -3 5.35 3.94 -7 -6 3 -0.93 3.87 7 -6 -3 2.17 3.88 7 -6 -3 1.48 3.50 7 -6 -3 4.01 4.29 -7 -6 3 1.97 4.06 -7 6 3 4.43 3.99 -7 -6 3 1.10 3.33 -7 -6 3 0.29 2.56 7 -6 -3 -0.97 1.87 7 6 -3 5.45 3.73 7 -6 -3 2.14 1.51 7 -6 -3 5.06 2.93 -7 -6 3 -2.34 5.32 7 -6 -3 1.26 4.82 7 -6 -3 -1.39 3.92 7 6 -3 1.20 4.07 7 6 -3 -1.63 5.27 -7 -6 2 96.96 5.44 -7 -6 2 94.89 5.38 7 6 -2 110.54 7.07 -7 -6 2 107.05 7.15 7 -6 -2 104.05 6.73 7 -6 -2 108.71 6.96 -7 -6 2 97.71 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15.80 7 -12 -6 365.08 16.95 7 12 -6 367.12 16.99 7 12 -6 385.79 18.54 7 -12 -5 293.67 14.39 7 12 -5 306.09 14.57 -7 12 5 327.08 14.97 -7 -12 5 299.72 14.74 7 -12 -5 294.90 13.66 7 12 -5 299.47 13.69 7 -12 -5 292.08 13.43 -7 -12 5 279.08 14.19 7 -12 -5 311.03 15.09 -7 -12 5 300.01 13.72 7 -12 -5 283.14 13.43 7 -12 -5 308.95 14.74 7 -12 -5 284.21 13.78 7 12 -5 290.01 13.90 7 12 -5 294.73 14.18 7 12 -5 329.58 15.85 7 -12 -5 296.43 12.24 7 12 -5 310.29 16.40 -7 -12 4 336.68 15.82 7 -12 -4 376.19 16.80 -7 -12 4 370.03 16.00 -7 -12 4 338.35 16.10 7 -12 -4 374.61 15.71 7 -12 -4 346.85 15.17 7 12 -4 325.77 16.11 7 -12 -4 339.13 14.62 7 12 -4 372.02 18.52 7 -12 -4 354.17 15.46 7 -12 -4 366.44 16.47 7 12 -4 351.60 15.60 7 12 -4 373.01 16.71 7 -12 -3 98.98 7.92 7 12 -3 97.37 8.14 7 -12 -3 105.00 7.00 7 12 -3 112.95 7.14 7 -12 -3 98.52 6.49 7 -12 -3 117.56 7.91 -7 -12 3 107.93 7.37 -7 -12 3 105.28 7.68 -7 -12 3 103.58 7.36 7 -12 -3 116.67 7.30 7 12 -3 105.62 7.84 7 12 -3 122.68 10.23 7 -12 -3 95.16 5.89 -7 -12 3 89.13 9.22 7 -12 -2 0.71 4.12 7 12 -2 9.21 4.58 7 12 -2 8.40 5.65 7 -12 -2 7.79 5.42 -7 -12 2 6.05 4.42 -7 -12 2 7.88 4.68 -7 -12 2 6.95 4.97 7 -12 -2 8.24 5.25 -7 -12 2 4.30 4.40 7 -12 -2 8.77 5.29 7 -12 -2 6.02 4.64 7 12 -2 2.58 5.30 7 -12 -2 2.94 2.81 7 -12 -2 5.01 6.29 7 -12 -2 8.44 3.18 7 12 -2 2.47 7.26 -7 -12 2 12.10 7.29 -7 -12 1 3.03 5.32 -7 12 1 6.86 5.38 7 -12 -1 6.17 4.57 7 12 -1 3.25 4.70 7 -12 -1 -3.62 5.50 7 12 -1 7.82 6.08 -7 -12 1 3.72 4.64 -7 -12 1 4.57 4.52 7 -12 -1 4.68 4.92 -7 -12 1 2.06 5.46 7 -12 -1 3.45 4.75 7 -12 -1 7.29 5.18 -7 -12 1 4.44 4.33 7 -12 -1 5.72 3.35 7 -12 -1 2.71 6.68 7 -12 -1 2.18 3.11 7 12 -1 1.53 7.61 -7 -12 1 8.80 7.09 7 -12 0 53.93 7.36 7 12 0 57.35 7.74 -7 -12 0 54.78 6.28 -7 -12 0 55.04 5.50 7 12 0 51.57 9.49 7 -12 0 66.80 6.36 7 -12 0 63.06 5.31 7 -12 0 59.57 4.56 7 12 0 75.02 9.54 7 -12 0 68.38 7.16 -7 -12 0 56.86 5.17 7 -12 0 59.15 5.07 7 -12 0 47.52 8.44 7 -12 0 69.52 6.44 7 12 0 66.33 6.51 -7 12 0 59.09 7.30 -7 -12 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7.42 6.83 7 13 -10 2.10 6.78 7 -13 -9 119.37 8.89 7 13 -9 125.77 11.73 -7 -13 9 113.96 6.46 7 -13 -9 114.22 6.73 7 13 -9 111.26 8.68 -7 -13 9 123.12 8.66 -7 13 9 95.56 5.44 7 -13 -9 125.89 6.70 7 13 -9 101.87 9.21 7 -13 -9 108.47 9.28 -7 13 9 98.42 8.44 -7 -13 9 126.13 9.01 -7 13 8 86.43 7.54 -7 -13 8 94.86 7.57 -7 -13 8 95.51 5.83 7 -13 -8 83.60 5.73 7 13 -8 104.85 7.69 -7 -13 8 110.64 7.51 7 13 -8 81.54 7.37 7 -13 -8 96.97 7.52 7 -13 -8 97.62 7.92 7 13 -8 88.29 7.69 7 -13 -8 92.66 7.53 7 -13 -7 0.85 5.38 -7 -13 7 6.09 6.79 -7 -13 7 11.93 4.56 7 -13 -7 5.52 4.33 7 13 -7 0.32 5.72 7 -13 -7 10.09 5.10 7 -13 -7 3.99 5.45 7 13 -7 5.67 5.69 7 -13 -7 6.82 5.39 7 13 -7 3.12 5.65 -7 13 7 15.00 6.00 7 -13 -7 5.92 5.48 -7 -13 7 5.32 5.60 7 13 -7 6.33 5.54 7 -13 -6 59.26 5.94 -7 -13 6 55.41 7.32 7 -13 -6 64.18 7.84 -7 -13 6 50.58 5.49 7 -13 -6 51.75 5.40 7 13 -6 51.84 6.16 7 -13 -6 44.97 5.92 7 13 -6 52.97 6.38 7 -13 -6 44.14 5.71 7 -13 -6 46.17 6.26 7 13 -6 65.65 6.82 -7 13 6 54.77 6.63 7 13 -6 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31.37 5.09 8 8 -4 39.67 5.50 8 -8 -3 19.24 5.80 8 8 -3 13.03 6.11 8 8 -3 12.83 7.23 8 -8 -3 15.34 4.64 -8 -8 3 22.48 4.93 8 -8 -3 14.96 5.00 -8 -8 3 16.34 5.38 -8 8 3 20.40 5.23 8 -8 -3 27.58 4.51 8 -8 -3 24.66 5.21 8 -8 -3 17.76 2.57 -8 -8 3 15.95 3.49 -8 -8 3 16.80 3.79 8 8 -3 16.90 5.10 8 -8 -3 12.41 1.87 8 -8 -3 16.52 3.23 -8 -8 3 13.49 6.37 8 -8 -3 21.22 4.67 8 8 -3 22.08 4.98 8 8 -2 125.52 10.97 8 -8 -2 112.15 7.97 8 8 -2 143.39 8.53 -8 -8 2 132.10 8.85 8 -8 -2 141.64 8.43 8 -8 -2 145.36 8.53 -8 -8 2 144.63 8.46 -8 8 2 140.59 9.02 8 -8 -2 137.26 8.76 -8 -8 2 133.03 6.56 -8 -8 2 117.92 6.79 8 -8 -2 123.04 6.31 8 -8 -2 126.28 7.10 -8 -8 2 126.73 9.89 8 8 -2 138.59 8.76 8 -8 -2 140.24 9.83 8 8 -2 129.18 9.94 -8 8 2 125.60 9.37 -8 -8 2 135.36 9.37 8 -8 -2 128.87 8.22 8 -8 -1 64.54 4.77 -8 -8 1 59.01 5.18 -8 -8 1 76.34 3.89 8 -8 -1 67.90 6.60 8 8 -1 41.39 8.66 8 8 -1 65.17 6.81 8 -8 -1 74.18 6.18 -8 -8 1 59.53 6.98 8 -8 -1 69.17 6.78 8 -8 -1 71.19 6.50 -8 -8 1 63.87 5.99 -8 8 1 71.41 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5.76 8 -9 -1 73.32 5.25 8 9 -1 81.86 9.70 8 -9 -1 66.50 6.36 8 9 -1 71.94 6.78 8 -9 -1 84.17 6.53 -8 -9 1 55.94 6.99 8 -9 -1 79.83 6.84 -8 9 1 70.42 7.44 8 -9 -1 65.40 6.83 -8 -9 1 72.29 6.12 8 -9 -1 64.44 7.90 8 9 -1 84.58 8.48 8 -9 -1 67.81 5.07 8 -9 -1 75.91 6.81 8 9 -1 79.60 7.04 -8 9 1 70.51 7.79 -8 -9 1 85.44 8.09 -8 -9 1 71.47 8.59 8 -9 -1 74.07 5.68 -8 9 0 272.60 14.44 -8 -9 0 275.54 14.53 -8 -9 0 229.17 9.78 8 -9 0 267.28 11.62 -8 -9 0 245.62 11.97 8 -9 0 251.04 12.01 -8 -9 0 246.60 13.55 -8 -9 0 254.05 11.69 8 -9 0 282.93 13.14 8 -9 0 274.45 15.76 -8 -9 0 252.99 14.58 8 -9 0 253.73 11.98 8 -9 0 258.49 11.56 8 9 0 275.51 14.77 8 -9 0 252.28 12.50 8 9 0 247.01 15.47 -8 -9 -1 149.84 8.92 8 -9 1 138.37 8.25 8 -9 1 148.86 8.14 8 9 1 138.06 11.06 8 -9 1 141.14 7.60 8 -9 1 152.59 9.07 8 9 1 161.28 12.71 8 -9 1 143.02 12.38 8 -9 1 161.48 9.52 -8 9 -1 142.29 11.45 -8 -9 -1 143.04 11.12 -8 9 -1 123.47 6.21 8 -9 1 149.91 8.94 8 -9 2 9.89 4.25 8 -9 2 10.38 3.97 8 9 2 2.46 7.02 8 -9 2 3.10 5.61 8 9 2 12.74 9.05 -8 9 -2 9.93 5.51 8 -9 2 11.99 5.97 8 -9 2 11.16 5.97 8 -9 2 16.28 8.93 -8 9 -2 8.49 7.84 -8 -9 -2 14.74 7.71 -8 -9 -2 10.77 5.71 8 -9 2 8.84 5.06 8 9 3 19.74 6.74 8 -9 3 10.97 3.96 -8 -9 -3 18.00 7.00 8 -9 3 12.02 5.76 -8 9 -3 5.66 6.76 8 -9 3 21.40 5.68 -8 -9 -3 0.37 6.15 8 -9 3 5.08 8.82 -8 9 -3 13.22 8.08 -8 -9 -3 12.00 7.82 -8 9 -3 8.51 5.75 8 -9 3 6.24 6.11 8 9 3 20.39 9.33 8 9 4 201.56 12.04 -8 -9 -4 183.35 13.23 -8 9 -4 218.37 13.57 8 -9 4 208.15 11.66 8 -9 4 211.71 9.81 8 -9 4 197.08 11.56 8 9 4 216.31 11.99 -8 -9 -4 185.84 12.56 8 -9 4 255.48 16.31 -8 9 -4 200.36 15.00 -8 -9 -4 200.59 14.73 8 9 4 203.36 15.54 -8 9 -4 215.95 11.96 8 9 5 14.75 9.81 -8 9 -5 4.59 6.44 -8 -9 -5 5.38 7.02 8 -9 5 6.87 5.67 -8 9 -5 4.22 6.95 -8 -9 -5 7.62 7.17 8 9 5 4.70 8.34 8 9 5 8.88 5.77 -8 -9 -5 3.56 2.76 -8 9 -5 -6.06 8.90 -8 -9 -5 12.74 8.68 -8 -9 -6 133.70 11.34 8 9 6 101.57 7.87 -8 -9 -6 128.20 11.10 -8 9 -6 121.38 10.89 8 9 6 153.71 12.66 8 9 6 142.63 13.45 -8 -9 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4.75 10.77 9 -12 -14 14.75 9.87 9 -12 -14 10.83 8.16 -9 -12 14 14.79 7.54 -9 12 14 24.75 7.88 9 -12 -13 12.18 7.58 9 -12 -13 0.66 9.37 9 12 -13 -3.02 7.82 -9 -12 13 -0.57 8.17 9 12 -13 -6.63 10.83 -9 12 13 7.29 2.66 9 -12 -13 -9.59 8.33 9 12 -13 3.51 8.61 -9 12 13 8.72 7.28 -9 -12 13 6.55 6.87 9 -12 -12 56.88 8.20 9 -12 -12 64.02 10.92 9 12 -12 59.94 8.68 -9 -12 12 27.21 8.96 -9 12 12 43.44 8.10 -9 -12 12 56.50 8.35 9 -12 -12 39.58 8.96 9 12 -12 61.01 9.54 9 12 -12 73.62 11.91 9 12 -11 13.18 9.65 -9 12 11 11.73 6.76 -9 -12 11 2.80 6.77 -9 -12 11 0.26 2.49 -9 -12 11 5.68 7.45 9 -12 -11 -2.80 4.67 9 -12 -11 10.26 7.42 9 12 -11 7.70 7.62 9 -12 -11 -6.51 6.30 -9 -12 11 -7.06 6.55 9 -12 -11 5.64 8.57 9 -12 -10 145.35 11.27 9 12 -10 153.82 11.23 9 -12 -10 155.47 10.08 -9 -12 10 151.35 9.89 9 12 -10 152.74 13.10 9 -12 -10 147.26 8.05 -9 -12 10 139.18 7.42 -9 -12 10 159.38 11.71 9 12 -10 154.57 10.22 9 -12 -10 150.77 9.91 -9 12 10 170.60 11.30 -9 -12 10 186.06 11.58 -9 -12 10 128.70 13.31 -9 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37.81 13.95 -10 -4 18 36.40 10.20 -10 -4 17 12.07 10.00 -10 4 17 16.22 9.77 10 4 -17 6.18 9.12 10 -4 -17 3.33 11.98 10 4 -17 6.95 12.87 -10 -4 17 8.90 8.71 -10 -4 16 53.71 10.51 -10 4 16 60.37 10.88 -10 -4 16 48.77 9.57 10 4 -16 44.57 9.81 10 -4 -16 37.82 8.68 10 4 -16 60.25 13.24 10 -4 -15 15.22 10.93 10 4 -15 6.82 11.23 -10 -4 15 12.44 8.96 -10 4 15 9.54 8.95 10 4 -15 7.15 7.96 10 -4 -15 1.40 9.54 10 -4 -15 -6.28 7.15 -10 -4 15 4.66 8.07 10 -4 -14 22.16 10.43 10 4 -14 8.42 10.35 10 4 -14 13.48 7.62 -10 4 14 10.46 8.91 10 -4 -14 -4.26 6.37 10 -4 -14 5.77 9.00 -10 -4 14 -3.35 7.83 -10 -4 13 2.45 5.43 -10 4 13 12.37 5.99 10 -4 -13 17.30 9.99 10 4 -13 9.69 10.38 10 4 -13 10.27 6.94 10 -4 -13 0.58 8.45 -10 4 13 -2.90 3.27 -10 -4 13 5.17 4.84 -10 -4 13 9.14 7.34 10 -4 -13 8.90 5.98 -10 -4 12 75.61 7.12 -10 4 12 76.28 7.23 10 -4 -12 93.14 10.84 10 4 -12 81.43 11.36 10 4 -12 94.99 8.52 -10 -4 12 83.85 9.82 10 -4 -12 88.91 10.23 -10 -4 12 84.84 6.54 10 -4 -12 85.33 7.24 -10 -4 12 94.45 9.70 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6.63 10 -4 -7 30.56 4.46 -10 4 7 28.30 8.10 -10 -4 7 27.59 7.29 -10 -4 7 21.85 4.65 10 4 -7 21.78 4.16 10 4 -7 43.89 8.40 -10 -4 7 15.74 7.41 10 -4 -6 95.72 7.82 10 4 -6 104.74 8.12 10 4 -6 99.19 7.08 10 -4 -6 116.21 7.29 -10 -4 6 103.63 7.48 -10 4 6 109.84 7.60 -10 -4 6 124.39 9.76 -10 4 6 111.93 10.11 10 4 -6 105.53 6.61 -10 -4 6 106.62 9.75 10 4 -6 125.23 10.93 10 -4 -6 91.78 9.01 10 -4 -6 114.40 9.10 10 -4 -5 96.93 9.12 10 4 -5 110.50 10.95 -10 -4 5 109.30 9.29 -10 4 5 117.71 8.28 10 -4 -5 121.14 7.50 10 4 -5 114.77 7.58 -10 -4 5 112.38 7.89 10 4 -5 93.76 6.64 -10 -4 5 114.05 9.38 10 -4 -5 95.83 7.17 10 4 -4 218.80 13.82 10 -4 -4 201.61 11.98 10 -4 -4 182.37 10.22 10 4 -4 189.77 10.35 -10 -4 4 188.00 10.74 10 -4 -4 198.08 10.86 -10 -4 4 190.34 11.59 -10 4 4 191.25 10.98 10 -4 -4 153.63 7.67 10 4 -4 184.07 9.52 -10 -4 4 206.82 11.68 10 -4 -4 208.23 10.33 10 -4 -4 190.16 8.89 -10 -4 3 399.41 18.10 10 -4 -3 404.20 17.55 -10 -4 3 410.09 18.45 -10 4 3 439.15 18.48 10 -4 -3 328.38 14.96 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12.80 8.12 -10 -5 12 17.23 4.91 10 -5 -12 15.88 5.41 -10 -5 12 23.82 7.54 10 -5 -11 21.64 9.19 10 5 -11 16.32 9.74 10 5 -11 14.21 6.58 -10 -5 11 17.07 8.03 -10 -5 11 30.84 5.39 -10 5 11 14.17 5.22 10 -5 -11 35.39 8.63 10 -5 -11 25.26 5.07 -10 -5 11 17.73 7.63 10 -5 -10 87.83 10.03 10 5 -10 75.92 10.07 10 -5 -10 90.49 4.93 -10 -5 10 96.94 9.90 -10 -5 10 55.58 4.44 -10 5 10 86.03 10.32 -10 -5 10 76.32 6.16 10 -5 -10 87.34 9.46 10 -5 -10 88.71 6.02 10 -5 -10 86.40 8.37 -10 -5 10 94.96 9.71 -10 -5 9 11.48 7.02 10 -5 -9 8.94 6.79 -10 -5 9 12.63 3.81 10 -5 -9 4.15 7.25 10 5 -9 6.98 7.77 10 -5 -9 12.06 3.62 -10 5 9 7.47 7.84 -10 -5 9 6.63 6.87 -10 -5 9 8.91 3.55 10 -5 -9 8.10 3.83 10 -5 -9 12.71 6.23 -10 -5 8 158.77 12.12 10 -5 -8 152.89 11.23 10 -5 -8 183.37 11.72 -10 -5 8 175.22 7.91 10 5 -8 179.33 12.09 10 -5 -8 198.41 9.12 -10 -5 8 160.31 8.97 -10 -5 8 188.85 12.43 -10 5 8 208.51 13.23 10 5 -8 164.72 9.13 -10 -5 8 189.20 13.15 10 -5 -8 193.32 10.68 10 -5 -8 172.34 8.31 10 -5 -7 8.50 5.83 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6.37 10 7 -4 2.84 8.20 10 -7 -4 11.25 6.06 10 7 -4 13.92 5.06 10 -7 -4 10.18 3.96 -10 -7 4 13.12 7.29 10 -7 -4 9.57 4.44 10 -7 -3 10.26 5.72 -10 -7 3 8.64 5.87 -10 -7 3 6.68 5.53 -10 7 3 4.21 5.63 10 7 -3 1.15 8.45 10 -7 -3 14.39 6.43 10 7 -3 0.29 5.07 10 -7 -3 5.86 2.55 10 -7 -3 10.44 4.64 -10 -7 3 6.30 6.82 10 -7 -3 5.60 3.79 10 -7 -2 26.16 6.89 10 7 -2 19.96 8.85 -10 -7 2 21.72 5.95 -10 -7 2 15.70 6.13 -10 7 2 11.99 6.24 10 -7 -2 13.02 5.66 10 -7 -2 16.29 3.32 -10 -7 2 7.17 7.27 10 -7 -2 20.87 5.17 -10 7 2 12.18 6.75 -10 -7 2 11.57 6.75 10 -7 -1 19.01 7.09 10 7 -1 6.69 9.13 10 -7 -1 19.61 5.61 -10 -7 1 11.74 6.62 -10 -7 1 21.19 6.09 -10 7 1 14.17 6.88 10 -7 -1 13.72 2.48 -10 -7 1 14.45 8.11 -10 7 1 10.73 3.16 10 -7 -1 12.78 6.07 -10 7 1 1.57 7.50 -10 -7 1 22.79 7.77 10 7 0 16.45 9.21 10 -7 0 24.64 7.25 10 -7 0 19.89 5.27 -10 -7 0 29.49 7.39 -10 7 0 18.91 6.69 -10 -7 0 20.88 4.54 10 -7 0 21.19 3.62 10 -7 0 31.73 10.12 -10 -7 0 25.95 8.22 10 -7 0 16.32 5.91 -10 7 0 19.30 3.63 -10 7 0 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40.93 8.30 -10 -9 1 37.99 8.06 10 -9 -1 30.96 3.59 -10 -9 1 31.59 4.55 10 -9 -1 30.45 4.06 -10 -9 1 41.50 7.30 10 -9 -1 24.66 5.95 -10 9 1 34.44 7.19 -10 -9 1 30.54 5.97 10 -9 -1 37.60 4.62 10 -9 -1 20.91 9.59 -10 -9 1 46.64 8.37 10 -9 -1 35.29 6.65 10 -9 -1 35.73 5.52 10 9 -1 32.84 9.44 -10 9 0 173.45 12.62 -10 -9 0 147.30 12.15 -10 -9 0 147.19 8.59 10 -9 0 120.81 6.14 10 -9 0 154.51 7.72 10 -9 0 146.55 9.16 -10 -9 0 152.43 11.31 10 -9 0 174.27 14.32 -10 9 0 189.96 11.86 10 -9 0 139.83 8.50 10 -9 0 179.48 10.55 10 9 0 185.09 14.32 -10 -9 0 153.62 12.12 10 -9 0 160.25 9.53 -10 -9 -1 63.22 6.57 10 -9 1 49.09 5.31 10 -9 1 34.05 5.63 10 9 1 52.53 9.09 10 -9 1 44.47 6.86 10 9 1 67.30 11.43 -10 -9 -1 47.31 8.38 10 -9 1 65.81 11.36 -10 -9 -1 37.49 9.32 10 -9 1 50.73 7.53 -10 9 -1 57.60 9.38 -10 -9 -1 44.21 8.89 -10 -9 -2 113.58 8.74 10 9 2 99.25 10.11 10 -9 2 137.07 13.79 10 9 2 117.14 13.03 10 -9 2 119.38 9.39 -10 9 -2 119.47 11.84 -10 -9 -2 117.97 11.81 -10 -9 -2 113.22 11.64 -10 9 -2 106.02 6.07 -10 -9 -3 69.69 8.03 -10 9 -3 48.96 7.36 10 9 3 74.61 12.04 10 9 3 60.01 8.72 10 -9 3 77.27 12.48 -10 9 -3 60.04 5.85 -10 9 -3 77.88 10.98 -10 -9 -3 101.21 11.74 10 9 4 6.06 6.58 10 9 4 28.71 11.27 -10 -9 -4 12.80 8.16 -10 9 -4 29.90 8.26 -10 9 -4 16.03 9.58 -10 -9 -4 23.20 9.73 -10 -9 -4 15.37 7.19 -10 -9 -5 52.92 9.86 -10 9 -5 55.11 9.66 10 9 5 43.11 11.97 10 9 5 43.42 11.21 -10 9 -5 39.46 11.23 -10 -9 -5 50.87 10.79 -10 -9 -5 23.53 8.42 10 9 6 0.74 10.39 10 9 6 14.76 11.28 -10 -9 -6 14.88 9.03 -10 9 -6 11.11 8.63 -10 9 -6 13.09 10.70 -10 -9 -6 1.63 10.08 10 9 7 7.47 10.72 10 -9 7 -3.53 11.72 10 9 7 16.85 11.36 -10 -9 -7 -13.78 11.01 -10 9 -7 25.02 11.48 -10 9 -7 4.07 8.88 -10 -9 -7 4.24 9.12 10 9 8 5.97 11.27 10 -9 8 0.90 12.54 -10 9 -8 -1.81 11.13 -10 -9 -8 2.72 11.47 -10 9 -8 18.21 9.82 -10 -9 -8 18.33 9.60 10 9 9 19.97 11.19 10 -9 9 0.90 12.52 -10 9 -9 1.43 9.82 -10 -9 -9 -7.55 10.68 -10 -9 -9 -11.38 11.71 -10 9 -9 23.72 11.84 10 10 -18 20.49 13.89 10 -10 -18 -2.66 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123.65 8.80 -10 -11 -2 24.50 6.55 10 11 2 22.78 8.33 10 -11 2 21.05 10.45 10 11 2 20.37 10.41 -10 11 -2 17.07 8.63 -10 -11 -2 26.98 8.72 -10 -11 -2 34.99 9.81 -10 -11 -3 139.32 10.09 10 11 3 135.86 14.40 10 11 3 127.83 10.69 10 -11 3 159.98 14.97 -10 11 -3 155.07 13.12 -10 -11 -3 123.90 12.43 10 11 4 4.72 6.93 10 11 4 -2.43 10.86 -10 11 -4 34.44 8.97 -10 -11 -4 5.60 8.22 10 -11 4 20.24 11.52 -10 -11 -4 23.10 7.52 -10 11 -4 23.81 9.56 -10 -11 -4 14.36 9.12 -10 11 -5 12.62 8.50 -10 -11 -5 17.03 8.96 10 11 5 14.99 11.77 10 11 5 12.77 10.37 -10 -11 -5 11.10 8.42 -10 11 -5 39.13 10.75 -10 -11 -5 11.47 10.49 -10 11 -6 10.51 8.75 -10 -11 -6 19.21 9.55 10 11 6 25.62 12.19 10 11 6 10.13 10.42 -10 -11 -6 22.77 9.12 -10 11 -6 17.01 10.73 -10 -11 -6 5.66 10.31 10 11 7 13.11 11.52 10 11 7 7.88 11.77 -10 11 -7 7.48 9.56 -10 -11 -7 13.61 10.07 -10 11 -7 19.64 11.08 -10 -11 -7 23.04 11.14 10 11 8 36.20 11.91 10 -11 8 18.09 12.99 -10 11 -8 37.09 10.47 -10 -11 -8 28.17 10.37 -10 -11 -8 54.67 12.62 -10 11 -8 24.21 11.47 10 11 9 58.48 12.80 10 -11 9 68.69 14.92 -10 11 -9 46.41 11.30 -10 -11 -9 64.00 11.58 -10 -11 -9 45.90 13.11 -10 11 -9 61.79 13.79 10 12 -18 2.99 13.77 10 -12 -18 16.07 12.73 -10 -12 18 12.31 10.46 10 12 -18 -7.60 11.02 -10 -12 18 10.48 9.11 -10 12 18 6.67 9.01 10 12 -17 23.72 14.18 10 -12 -17 16.07 12.26 -10 -12 17 21.82 10.15 10 12 -17 27.38 10.42 -10 12 17 9.00 9.23 -10 -12 17 7.60 8.75 10 12 -16 16.50 9.91 -10 12 16 11.71 8.88 -10 -12 16 18.21 9.08 10 12 -16 6.28 12.98 10 -12 -16 19.94 11.89 10 12 -15 -5.13 8.89 10 12 -15 0.84 11.84 10 -12 -15 14.24 11.01 10 -12 -15 9.25 8.24 -10 12 15 -2.37 7.87 -10 -12 15 0.58 7.61 10 -12 -14 9.82 10.32 10 -12 -14 2.96 7.70 -10 -12 14 0.62 8.65 10 12 -14 -1.06 8.26 10 12 -14 1.58 11.34 10 -12 -14 24.97 9.50 10 12 -14 -1.94 8.95 -10 12 14 5.70 7.92 -10 -12 14 6.74 7.35 10 -12 -13 7.54 7.22 10 -12 -13 16.36 10.04 -10 -12 13 10.68 8.67 10 12 -13 3.96 7.81 -10 12 13 1.09 7.59 -10 -12 13 -2.18 7.75 10 -12 -13 6.00 8.67 10 12 -13 14.22 8.96 10 12 -13 18.31 11.27 10 12 -12 21.66 10.89 -10 12 12 21.29 8.05 -10 -12 12 14.85 7.45 10 -12 -12 20.10 9.74 10 -12 -12 20.01 7.01 10 -12 -12 -1.64 8.12 10 12 -12 15.70 8.55 -10 -12 12 14.73 8.26 10 12 -11 43.49 10.38 10 -12 -11 58.52 9.04 10 12 -11 40.89 8.47 -10 -12 11 33.13 3.64 -10 -12 11 50.13 8.80 -10 -12 11 37.67 6.55 10 -12 -11 48.52 7.03 10 -12 -11 63.07 9.93 -10 12 11 71.39 8.77 -10 -12 11 39.60 8.24 10 -12 -10 260.66 13.06 -10 -12 10 253.11 13.09 10 -12 -10 240.30 15.55 -10 12 10 260.65 15.48 -10 -12 10 296.50 15.77 -10 -12 10 233.20 11.38 -10 -12 10 292.49 15.91 10 12 -10 252.38 13.59 -10 -12 10 237.46 17.07 10 -12 -10 267.10 15.05 10 12 -10 276.91 15.23 10 -12 -10 248.77 13.03 -10 12 9 26.16 7.36 -10 -12 9 38.71 8.02 -10 -12 9 27.31 4.65 10 -12 -9 36.81 5.00 -10 -12 9 33.46 8.09 10 -12 -9 35.13 7.25 10 12 -9 34.29 7.57 10 12 -9 27.01 6.24 -10 -12 9 43.92 10.23 10 -12 -9 35.97 5.68 -10 -12 9 33.35 5.78 10 -12 -9 32.76 5.41 10 -12 -8 124.44 7.11 -10 -12 8 97.43 7.25 10 12 -8 112.69 12.22 -10 -12 8 102.64 7.15 10 -12 -8 101.40 7.08 -10 -12 8 90.04 9.48 10 -12 -8 94.55 8.90 10 12 -8 99.20 9.17 10 12 -8 92.52 7.95 -10 12 8 109.27 10.30 -10 -12 8 122.19 10.38 -10 -12 8 109.79 11.47 10 -12 -8 103.04 6.91 10 12 -7 3.23 8.81 -10 -12 7 3.10 4.75 10 -12 -7 1.31 4.35 -10 -12 7 2.17 6.40 -10 -12 7 -1.20 6.10 10 -12 -7 7.90 3.75 10 12 -7 1.93 5.34 10 -12 -7 1.61 3.67 -10 -12 7 3.78 8.62 10 -12 -7 1.54 5.60 10 12 -7 2.78 5.68 10 12 -6 28.51 10.30 10 -12 -6 33.25 5.83 -10 -12 6 36.61 5.97 -10 -12 6 26.11 7.12 -10 -12 6 36.54 6.41 -10 -12 6 26.43 4.68 10 -12 -6 28.85 3.73 10 12 -6 23.28 6.18 -10 -12 6 24.59 8.84 10 -12 -6 21.34 6.10 10 12 -6 31.49 6.52 -10 -12 5 11.00 5.61 -10 -12 5 -6.12 6.45 10 12 -5 27.38 9.77 10 -12 -5 9.71 5.34 10 12 -5 10.49 5.99 -10 -12 5 10.40 8.28 10 -12 -5 6.58 2.87 -10 -12 5 14.37 5.29 -10 -12 5 7.38 4.12 -10 -12 4 90.64 8.02 -10 -12 4 70.13 7.88 -10 -12 4 78.19 6.32 -10 -12 4 79.78 5.75 10 -12 -4 71.20 4.60 10 12 -4 86.31 7.85 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5.30 10 -12 0 34.26 6.60 -10 -12 0 36.58 7.94 -10 12 0 60.18 8.31 -10 -12 0 40.01 5.93 10 -12 0 46.54 11.24 -10 -12 0 43.09 9.88 10 -12 0 44.94 6.10 10 -12 0 33.74 5.41 10 12 0 27.49 11.63 10 -12 0 31.63 5.92 -10 12 -1 11.67 8.49 -10 -12 -1 16.77 8.09 10 12 1 11.11 8.46 -10 -12 -1 4.81 7.29 10 -12 1 8.36 5.06 10 -12 1 3.63 9.85 10 -12 1 8.58 5.59 10 12 1 -0.75 10.00 -10 -12 -1 19.00 9.13 -10 -12 -1 2.86 5.63 -10 -12 -2 2.18 6.20 10 12 2 11.95 8.32 10 -12 2 11.32 10.21 10 12 2 7.72 10.20 -10 12 -2 8.78 8.30 -10 -12 -2 11.21 8.38 -10 -12 -2 -1.19 9.15 10 12 3 187.57 16.48 10 12 3 160.39 12.97 10 -12 3 203.21 16.72 -10 -12 -3 160.90 11.98 -10 12 -3 194.31 14.44 -10 -12 -3 187.70 14.54 -10 -12 -4 -7.90 7.55 10 12 4 -1.26 7.23 10 12 4 19.86 11.64 -10 12 -4 3.04 7.65 -10 -12 -4 3.77 7.91 10 -12 4 -1.63 10.87 -10 12 -4 0.72 9.13 -10 -12 -4 5.71 9.14 -10 12 -4 5.23 3.62 -10 12 -5 17.75 9.01 -10 -12 -5 -1.32 8.56 10 12 5 7.65 11.52 10 12 5 9.13 10.24 10 -12 5 8.42 11.80 -10 -12 -5 9.30 8.34 -10 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32.87 4.51 10 -14 -1 31.48 4.67 10 -14 -1 34.73 10.19 -10 -14 1 41.93 9.55 10 14 -1 22.09 10.74 -10 14 0 138.64 11.20 -10 -14 0 128.46 10.80 10 14 0 118.61 12.58 -10 -14 0 137.50 10.80 -10 -14 0 128.38 7.83 -10 -14 0 150.65 9.09 -10 -14 0 100.35 4.94 10 -14 0 147.66 13.69 -10 -14 0 117.19 12.46 10 14 0 126.80 13.43 -10 14 -1 7.46 7.52 -10 -14 -1 17.02 8.08 -10 -14 -1 -2.20 7.26 -10 -14 -1 4.90 6.02 10 -14 1 31.37 10.37 10 14 1 -3.01 8.87 -10 -14 -1 10.78 9.50 10 14 1 1.57 10.72 10 14 2 1.62 10.39 -10 -14 -2 6.28 6.68 10 -14 2 19.02 11.14 10 14 2 -2.84 8.41 -10 -14 -2 15.16 9.76 -10 14 -2 12.33 8.09 -10 -14 -2 12.83 8.21 10 14 3 6.67 11.17 -10 -14 -3 4.39 7.15 10 -14 3 15.02 11.09 10 14 3 10.52 8.47 -10 -14 -3 2.67 10.15 -10 14 -3 0.66 8.68 -10 -14 -3 20.38 9.39 -10 -14 -4 5.38 7.63 10 14 4 4.76 7.90 -10 -14 -4 21.76 9.10 10 -14 4 5.75 10.87 10 14 4 21.55 12.34 -10 14 -4 6.37 9.40 -10 -14 -4 14.07 9.49 -10 -14 -5 78.59 11.30 10 14 5 108.72 15.16 10 14 5 50.32 11.95 10 -14 5 81.46 14.28 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8.76 10 -15 -13 44.95 9.75 10 15 -13 41.10 9.68 -10 -15 13 47.33 9.78 10 -15 -13 54.14 8.53 10 -15 -13 52.60 11.15 10 15 -13 51.07 9.37 -10 -15 12 2.83 2.80 -10 -15 12 10.55 8.72 10 -15 -12 6.65 8.12 10 15 -12 3.28 8.67 -10 15 12 10.25 7.67 -10 -15 12 1.07 7.38 10 -15 -12 -2.96 6.96 10 -15 -12 7.66 10.00 -10 -15 11 7.59 3.68 -10 -15 11 14.48 8.03 10 -15 -11 22.74 8.10 10 15 -11 22.49 7.99 10 15 -11 18.78 6.60 10 -15 -11 -1.50 6.22 -10 15 11 22.83 7.54 -10 -15 11 13.16 7.52 -10 15 10 11.54 7.29 -10 -15 10 15.70 7.38 -10 -15 10 8.65 4.16 -10 -15 10 11.64 7.85 10 -15 -10 -2.33 6.95 10 15 -10 11.14 7.37 10 15 -10 -0.41 5.98 -10 -15 10 5.64 9.92 -10 -15 10 2.37 5.97 10 -15 -10 6.96 5.72 10 -15 -9 25.93 5.82 -10 -15 9 24.39 6.16 10 15 -9 25.20 10.06 -10 -15 9 30.34 5.09 -10 -15 9 25.05 8.25 10 -15 -9 26.69 7.10 10 15 -9 24.71 7.44 10 15 -9 27.41 6.55 -10 15 9 25.11 7.59 -10 -15 9 27.66 7.94 -10 -15 9 22.36 10.32 10 -15 -8 6.38 4.77 10 15 -8 6.98 9.26 -10 -15 8 -1.69 4.89 -10 -15 8 17.50 7.21 10 -15 -8 3.64 5.80 10 15 -8 -5.34 6.29 10 15 -8 11.41 6.04 -10 15 8 6.82 7.09 -10 -15 8 10.54 9.50 10 15 -7 53.74 10.84 10 -15 -7 45.26 5.87 -10 -15 7 40.07 5.98 -10 -15 7 34.73 7.64 10 -15 -7 34.49 5.21 10 15 -7 36.31 6.74 -10 -15 7 41.03 9.61 10 -15 -7 35.83 6.48 10 15 -7 40.70 7.29 10 15 -6 90.31 8.14 10 -15 -6 70.98 7.21 -10 -15 6 71.27 7.55 -10 -15 6 72.02 7.23 -10 -15 6 70.61 8.24 10 15 -6 84.79 11.52 10 -15 -6 65.42 6.39 10 15 -6 66.79 7.66 -10 -15 6 77.41 10.67 10 -15 -6 70.35 5.80 -10 -15 5 185.04 10.28 -10 -15 5 177.66 10.80 10 -15 -5 183.91 9.40 10 -15 -5 197.30 9.95 10 15 -5 225.27 16.01 -10 -15 5 201.65 11.71 -10 -15 5 190.07 12.03 10 -15 -5 212.92 13.89 10 15 -5 182.24 11.82 10 -15 -5 206.21 11.47 -10 -15 5 190.65 14.01 10 -15 -4 14.75 3.96 -10 -15 4 28.31 5.27 -10 -15 4 13.11 5.44 -10 -15 4 26.58 6.68 -10 -15 4 4.33 6.11 10 15 -4 20.33 6.71 10 -15 -4 12.62 7.67 10 -15 -4 20.17 4.13 10 15 -4 19.85 10.15 -10 -15 4 28.23 9.11 10 -15 -3 1.75 3.83 -10 -15 3 -0.77 4.95 -10 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80.19 12.58 10 15 2 8.26 10.42 -10 -15 -2 6.52 6.63 10 -15 2 -1.53 10.16 10 15 2 5.33 8.96 -10 -15 -2 18.21 10.18 -10 15 -2 15.25 8.12 -10 -15 -2 1.81 7.85 10 15 3 60.40 13.06 -10 -15 -3 27.55 8.02 10 -15 3 40.49 11.67 10 15 3 39.22 9.59 -10 -15 -3 53.57 11.66 -10 15 -3 59.02 10.35 -10 -15 -3 65.73 10.43 -10 -15 -4 53.50 9.10 -10 -15 -4 75.07 10.55 10 15 4 45.77 9.44 10 -15 4 72.56 13.27 -10 15 -4 76.44 11.38 -10 -15 -4 84.34 11.39 10 15 4 65.91 13.08 -10 -15 -5 84.04 11.33 10 15 5 93.65 14.64 10 -15 5 84.37 14.32 -10 15 -5 99.76 12.60 -10 -15 -5 76.40 12.48 -10 -15 -5 86.17 11.17 -10 -15 -6 4.24 9.06 10 15 6 26.66 12.30 10 15 6 -3.45 10.28 10 -15 6 2.62 11.52 -10 15 -6 9.46 10.08 -10 -15 -6 14.95 10.38 -10 -15 -6 -8.37 8.92 -10 -15 -7 2.20 9.56 10 15 7 -10.33 12.98 10 15 7 -1.38 10.08 -10 15 -7 5.80 10.74 -10 -15 -7 4.98 10.90 -10 -15 -7 0.65 9.45 -10 -15 -8 18.90 9.90 10 15 8 -5.73 12.71 10 15 8 -4.05 10.40 -10 15 -8 6.07 10.76 -10 -15 -8 -11.29 11.75 -10 -15 -8 3.45 10.16 10 16 -17 19.60 10.62 10 -16 -17 28.62 13.14 -10 -16 17 9.48 10.53 10 -16 -17 12.01 10.08 -10 16 17 3.83 9.06 -10 -16 17 41.20 9.46 10 -16 -16 -8.24 11.89 10 -16 -16 18.11 9.37 10 16 -16 -6.62 10.31 -10 16 16 4.32 8.54 -10 -16 16 9.04 8.70 10 -16 -15 10.41 8.88 10 -16 -15 28.08 11.71 -10 16 15 12.50 8.40 -10 -16 15 16.82 8.75 10 16 -15 3.74 9.70 10 -16 -14 1.48 10.36 10 -16 -14 -7.40 8.27 -10 16 14 17.19 7.88 -10 -16 14 5.07 7.76 10 16 -14 6.45 8.93 -10 -16 14 -6.49 8.99 -10 -16 13 4.97 8.64 -10 16 13 7.24 7.55 -10 -16 13 -0.55 7.64 10 -16 -13 1.92 7.51 10 -16 -13 2.08 10.09 10 -16 -13 -1.22 8.57 10 16 -13 -23.28 9.57 10 16 -13 -1.10 8.58 -10 -16 12 53.30 4.59 -10 -16 12 69.33 10.38 10 -16 -12 74.43 9.01 10 -16 -12 98.50 10.77 10 16 -12 83.65 10.47 -10 16 12 105.88 10.38 -10 -16 12 82.78 9.52 -10 16 11 13.90 7.40 -10 -16 11 9.00 7.68 -10 -16 11 0.18 3.77 -10 -16 11 13.53 8.04 10 -16 -11 5.80 6.37 10 16 -11 -0.89 6.51 -10 -16 11 3.04 10.38 10 -16 -11 -0.51 7.37 10 16 -11 15.03 7.89 10 -16 -10 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32.50 9.63 10 16 -1 51.81 11.15 -10 16 0 6.80 7.43 -10 -16 0 15.45 7.58 -10 -16 0 10.64 4.02 10 16 0 16.96 9.98 -10 -16 0 13.38 7.50 -10 -16 0 12.46 5.05 -10 -16 0 5.55 6.25 10 -16 0 5.61 10.13 -10 -16 0 26.85 9.83 10 16 0 14.33 10.89 -10 16 -1 28.70 8.16 -10 -16 -1 23.87 8.36 -10 -16 -1 32.85 8.24 -10 -16 -1 19.54 6.71 10 -16 1 36.69 10.51 -10 -16 -1 26.93 3.40 10 16 1 30.56 10.25 -10 -16 -1 35.09 10.68 10 16 1 28.71 11.32 10 16 2 2.53 10.62 -10 -16 -2 9.29 7.13 10 -16 2 0.76 10.31 10 16 2 7.40 8.95 -10 -16 -2 2.68 10.20 -10 16 -2 15.70 8.31 -10 -16 -2 7.15 8.07 10 16 3 21.71 11.88 -10 -16 -3 13.96 7.62 10 -16 3 28.71 11.09 10 16 3 17.91 9.18 -10 -16 -3 15.52 10.86 -10 -16 -3 26.36 9.24 -10 16 -3 18.15 9.07 -10 -16 -4 14.32 8.16 10 16 4 4.23 8.36 10 -16 4 10.75 11.30 -10 -16 -4 -1.31 8.31 -10 16 -4 9.01 9.15 -10 -16 -4 8.26 8.80 10 16 4 15.23 11.73 10 16 5 19.24 12.65 -10 -16 -5 52.57 10.16 10 -16 5 16.22 11.77 -10 16 -5 24.33 9.85 -10 -16 -5 6.61 9.83 -10 -16 -5 28.52 9.38 -10 -16 -6 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7.34 10 -17 -13 -0.70 10.13 10 -17 -13 6.74 8.60 10 17 -13 -2.39 8.75 10 17 -13 3.39 8.59 -10 -17 12 30.27 4.23 -10 -17 12 58.22 10.02 10 -17 -12 51.93 8.13 10 -17 -12 47.52 9.24 10 17 -12 36.17 9.29 -10 17 12 51.31 8.74 -10 -17 12 61.49 9.02 -10 17 11 27.33 7.83 -10 -17 11 27.64 8.04 -10 -17 11 20.86 4.48 -10 -17 11 34.26 8.73 10 -17 -11 37.94 7.28 10 17 -11 31.88 7.41 -10 -17 11 18.61 11.02 10 -17 -11 22.46 8.18 10 17 -11 24.55 8.30 -10 17 10 5.32 7.22 -10 -17 10 -4.75 7.54 -10 -17 10 5.95 4.30 -10 -17 10 4.88 7.79 10 -17 -10 0.72 5.90 10 17 -10 -3.99 6.41 -10 -17 10 13.97 10.31 10 -17 -10 7.96 6.98 10 17 -10 2.78 7.14 10 -17 -9 54.13 7.92 10 17 -9 47.91 8.09 10 -17 -9 51.62 6.85 10 17 -9 49.90 11.22 -10 -17 9 66.13 6.29 -10 -17 9 67.72 9.29 10 17 -9 65.58 7.97 -10 17 9 44.42 8.33 -10 -17 9 45.16 8.46 -10 -17 9 36.45 10.78 10 -17 -8 13.32 5.56 10 17 -8 22.70 10.59 -10 -17 8 19.84 5.45 -10 -17 8 10.18 7.40 10 17 -8 12.14 6.65 10 -17 -8 26.38 7.91 10 -17 -8 8.09 6.05 10 17 -8 13.88 6.93 -10 -17 8 24.13 9.75 10 -17 -7 14.18 5.37 10 17 -7 22.00 10.38 10 -17 -7 12.90 4.93 -10 -17 7 0.34 5.50 -10 -17 7 0.91 7.05 10 17 -7 13.33 6.61 10 -17 -7 10.99 7.56 10 -17 -7 16.15 5.83 10 17 -7 18.01 6.44 -10 -17 7 20.42 9.59 10 -17 -6 41.88 6.43 10 17 -6 27.75 6.59 10 -17 -6 46.84 5.69 -10 -17 6 37.32 6.96 -10 -17 6 44.96 6.71 -10 -17 6 34.14 7.59 10 17 -6 30.82 7.01 10 -17 -6 49.99 8.57 10 17 -6 40.49 10.88 10 -17 -6 41.70 5.02 -10 -17 6 62.24 9.99 10 -17 -5 1.82 5.56 10 17 -5 1.89 5.76 -10 -17 5 3.51 5.17 10 -17 -5 -0.47 4.59 -10 -17 5 14.54 6.01 -10 -17 5 1.18 5.90 -10 -17 5 6.76 6.29 10 17 -5 5.17 6.47 10 -17 -5 5.42 7.48 10 17 -5 8.12 9.75 10 -17 -5 3.17 3.67 -10 -17 5 -9.36 9.06 10 -17 -4 13.73 4.62 -10 -17 4 16.56 5.48 -10 -17 4 9.15 5.68 -10 -17 4 21.15 6.62 -10 -17 4 13.57 6.34 10 17 -4 14.16 6.87 10 -17 -4 5.74 7.78 10 17 -4 8.19 10.07 -10 -17 4 1.74 8.98 10 -17 -3 55.59 5.75 -10 -17 3 63.81 6.99 -10 -17 3 61.23 6.64 -10 -17 3 68.29 8.30 -10 -17 3 64.38 7.32 10 17 -3 55.09 8.47 10 -17 -3 57.01 9.80 10 17 -3 59.00 12.21 -10 -17 3 59.98 10.19 -10 -17 2 -5.95 5.79 10 17 -2 24.84 11.28 -10 -17 2 5.32 4.97 -10 -17 2 8.20 6.76 -10 -17 2 -0.61 5.31 10 17 -2 0.48 7.06 10 -17 -2 -13.41 8.61 10 17 -2 -3.85 10.01 -10 -17 2 2.97 8.79 -10 -17 1 17.72 6.85 -10 -17 1 18.69 5.96 10 17 -1 11.66 9.38 -10 -17 1 7.18 4.72 -10 -17 1 17.93 7.57 -10 -17 1 6.42 5.01 10 17 -1 8.97 7.06 10 -17 -1 17.42 9.64 -10 -17 1 15.86 9.38 10 17 -1 29.32 10.81 -10 -17 0 98.25 9.97 -10 17 0 114.93 10.25 10 17 0 87.74 12.35 -10 -17 0 115.30 10.61 -10 -17 0 78.70 6.75 -10 -17 0 89.59 6.29 -10 -17 0 105.26 8.79 10 -17 0 97.70 12.42 -10 -17 0 103.69 12.20 10 17 0 96.95 13.57 -10 17 -1 8.89 7.63 -10 -17 -1 4.38 7.46 -10 -17 -1 9.77 8.02 -10 -17 -1 6.78 6.44 10 -17 1 3.68 10.03 -10 -17 -1 6.98 3.83 10 17 1 -4.05 9.55 -10 -17 -1 -5.91 10.19 10 17 1 5.03 10.76 10 17 2 80.11 13.41 -10 -17 -2 69.45 8.88 10 -17 2 74.46 12.27 10 17 2 87.15 11.55 -10 -17 -2 83.25 12.33 -10 17 -2 81.62 10.24 -10 -17 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6.53 8.78 -10 22 13 1.14 8.08 -10 -22 13 -9.85 8.07 -10 -22 13 -0.66 9.66 10 -22 -12 33.41 8.55 -10 -22 12 22.99 5.16 -10 -22 12 38.18 10.12 10 22 -12 37.56 12.41 10 -22 -12 24.94 9.18 10 22 -12 23.58 9.26 -10 22 12 28.98 8.65 -10 -22 12 20.43 8.59 10 -22 -11 21.60 7.87 -10 -22 11 35.85 5.74 -10 -22 11 21.23 8.85 10 22 -11 18.29 11.80 10 22 -11 28.86 8.55 10 -22 -11 21.28 8.33 10 22 -11 35.16 8.98 -10 22 11 17.03 8.39 -10 -22 11 35.49 8.56 10 -22 -10 59.81 8.34 10 22 -10 36.43 11.78 -10 -22 10 55.33 6.61 -10 -22 10 47.85 9.35 10 22 -10 40.35 8.80 10 -22 -10 55.53 8.66 10 22 -10 66.63 9.06 -10 22 10 41.22 8.83 -10 -22 9 5.12 5.53 -10 -22 9 0.55 7.88 10 22 -9 -0.52 7.51 10 -22 -9 -9.73 7.04 10 -22 -9 -2.18 6.55 10 22 -9 15.34 7.31 10 -22 -9 -9.26 6.69 -10 -22 8 103.13 8.94 -10 -22 8 96.56 10.49 10 22 -8 123.38 10.90 10 -22 -8 119.68 10.16 10 -22 -8 122.14 9.69 10 22 -8 121.54 9.85 10 -22 -8 93.55 9.21 -10 -22 7 3.20 6.18 -10 -22 7 19.44 7.96 10 22 -7 20.55 7.62 10 -22 -7 20.14 7.81 10 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6.04 5.23 10 -22 -1 4.69 9.17 -10 -22 1 -1.72 6.70 -10 -22 1 -7.08 10.43 10 22 -1 -10.46 7.87 -10 -22 0 15.35 8.12 10 22 0 31.87 8.73 -10 -22 0 29.22 7.59 10 -22 0 23.31 10.23 -10 -22 0 16.03 10.93 10 22 0 25.52 10.90 -10 22 -1 -3.51 7.24 -10 -22 -1 6.35 7.15 10 22 1 -3.18 10.86 -10 -22 -1 -8.04 8.18 10 22 1 -1.87 8.26 10 -22 1 8.88 10.15 10 22 1 -2.78 12.16 -10 -22 -1 3.76 10.68 -10 -22 -1 8.56 7.43 10 22 2 19.90 11.31 -10 -22 -2 34.08 8.47 10 -22 2 20.05 11.05 10 22 2 24.57 12.92 -10 22 -2 12.50 8.44 -10 -22 -2 2.12 7.80 -10 -22 -2 20.27 11.99 10 22 3 21.07 10.92 -10 -22 -3 11.48 8.24 10 -22 3 28.86 11.97 10 22 3 20.31 13.24 -10 22 -3 22.18 9.05 -10 -22 -3 16.02 8.47 -10 -22 -3 16.20 12.04 10 22 4 42.66 11.66 -10 22 -4 37.41 9.78 -10 -22 -4 34.37 9.84 10 22 4 67.37 14.45 10 -22 4 44.10 13.22 -10 -22 -4 36.27 13.66 -10 -22 -4 29.79 9.71 -10 22 -5 -11.29 9.71 -10 -22 -5 -9.19 9.42 10 22 5 -6.03 13.45 -10 -22 -5 7.19 9.69 10 -22 5 -7.74 11.90 -10 -22 -5 7.89 12.86 -10 -22 -5 -1.87 9.19 -10 22 -6 73.31 11.37 -10 -22 -6 63.64 11.46 -10 -22 -6 66.08 11.29 10 22 6 69.22 15.39 10 -22 6 66.46 14.52 10 22 6 51.92 11.22 -10 -22 -6 61.84 14.74 -10 -22 -6 46.37 11.08 -10 -23 15 45.62 11.25 -10 23 15 35.00 9.70 -10 -23 15 22.67 9.05 10 -23 -15 38.17 10.53 10 -23 -15 19.45 12.72 10 23 -15 41.10 11.54 -10 -23 14 13.29 10.10 -10 23 14 18.01 8.85 -10 -23 14 18.84 8.52 10 -23 -14 0.60 8.96 10 23 -14 5.52 10.07 -10 -23 13 103.51 12.75 10 23 -13 102.80 14.92 -10 23 13 92.52 11.05 -10 -23 13 83.17 10.80 10 -23 -13 105.13 11.37 -10 -23 12 8.13 5.01 -10 -23 12 9.65 9.28 10 23 -12 16.17 11.91 10 23 -12 4.13 8.25 -10 23 12 4.46 8.01 -10 -23 12 11.22 8.25 10 -23 -12 -6.22 8.30 10 -23 -11 5.79 7.96 -10 -23 11 10.07 5.59 -10 -23 11 47.97 10.16 10 23 -11 5.93 11.60 10 23 -11 22.96 8.73 -10 23 11 18.13 8.51 -10 -23 11 8.97 8.36 10 -23 -11 8.83 8.39 10 23 -11 13.52 8.48 10 -23 -10 6.73 7.15 10 23 -10 3.38 10.94 -10 -23 10 -0.65 5.46 -10 -23 10 2.34 8.56 10 23 -10 4.46 7.76 10 -23 -10 14.25 7.48 10 23 -10 -5.08 7.52 -10 23 10 5.98 7.68 10 23 -9 28.61 11.72 -10 -23 9 17.37 6.27 -10 -23 9 13.87 8.21 10 23 -9 -11.44 8.34 10 -23 -9 14.13 6.62 10 -23 -9 3.93 6.95 10 23 -9 7.62 7.18 10 -23 -9 10.91 6.92 10 23 -8 15.16 11.68 -10 -23 8 32.29 6.85 -10 -23 8 22.55 8.57 10 23 -8 30.55 8.53 10 -23 -8 32.69 7.68 10 -23 -8 13.12 6.84 10 -23 -8 24.30 7.07 10 23 -8 24.20 7.35 -10 -23 7 27.60 6.89 -10 -23 7 39.93 8.36 10 23 -7 41.58 8.42 10 -23 -7 39.91 8.33 10 -23 -7 35.38 7.08 10 -23 -7 50.40 7.37 10 23 -7 33.60 7.11 10 23 -6 8.77 13.38 -10 -23 6 25.95 7.09 -10 -23 6 13.85 7.44 10 23 -6 26.86 8.12 10 -23 -6 19.22 8.02 10 23 -6 15.87 6.41 10 -23 -6 27.41 6.50 10 -23 -6 29.82 6.64 -10 -23 5 3.85 7.03 10 -23 -5 17.32 6.41 10 23 -5 8.57 12.94 -10 -23 5 22.42 7.12 -10 -23 5 6.01 6.91 10 23 -5 -1.64 7.64 10 -23 -5 1.04 7.46 10 23 -5 8.11 6.07 10 -23 -5 4.54 5.95 -10 -23 5 11.87 9.99 10 -23 -4 32.50 6.86 -10 -23 4 19.44 7.25 10 23 -4 22.42 12.17 -10 -23 4 40.52 7.92 -10 -23 4 37.65 7.44 10 23 -4 48.76 9.21 10 -23 -4 30.76 8.39 10 23 -4 36.90 6.54 10 -23 -4 29.85 6.25 -10 -23 4 55.62 11.40 10 -23 -3 0.37 6.19 -10 -23 3 0.42 6.73 10 23 -3 6.39 10.89 -10 -23 3 7.30 7.28 -10 -23 3 8.28 6.24 10 23 -3 -2.26 7.78 10 -23 -3 -5.37 8.30 10 -23 -3 -0.35 5.44 -10 -23 3 16.13 10.33 10 23 -2 40.09 12.33 -10 -23 2 27.98 7.98 -10 -23 2 33.89 6.41 10 23 -2 37.11 8.69 10 -23 -2 18.38 9.23 -10 -23 2 27.01 10.97 -10 -23 2 32.52 7.47 10 23 -1 13.93 11.54 -10 -23 1 15.50 8.07 -10 -23 1 23.00 5.60 10 -23 -1 21.43 9.78 -10 -23 1 24.21 7.48 -10 -23 1 16.73 10.52 10 23 -1 27.47 8.98 -10 -23 0 10.22 8.00 10 23 0 0.62 8.38 -10 -23 0 -1.40 6.93 10 -23 0 7.05 9.69 -10 -23 0 -2.99 11.06 10 23 0 6.78 10.90 10 23 1 30.32 11.31 -10 -23 -1 38.29 9.16 10 23 1 27.45 9.40 -10 -23 -1 42.81 8.53 10 -23 1 30.24 10.97 -10 -23 -1 28.55 11.74 -10 23 -1 28.70 7.76 -10 -23 -1 27.89 7.48 -10 23 -2 43.88 8.49 -10 -23 -2 35.51 8.45 10 23 2 34.52 10.08 10 -23 2 40.79 11.93 10 23 2 37.91 11.60 -10 -23 -2 34.30 12.46 -10 -23 -2 35.05 8.73 10 23 3 161.13 15.16 -10 -23 -3 145.58 12.77 10 -23 3 135.56 15.48 10 23 3 178.75 18.13 -10 -23 -3 118.99 12.03 -10 23 -3 151.28 12.49 -10 -23 -3 134.76 16.07 10 23 4 12.63 10.67 -10 23 -4 31.05 9.03 -10 -23 -4 17.89 9.10 10 23 4 34.17 13.67 10 -23 4 19.98 12.42 -10 -23 -4 17.17 13.13 -10 -23 -4 23.26 9.23 -10 23 -5 67.30 11.06 -10 -23 -5 65.74 10.76 10 23 5 49.90 14.90 -10 -23 -5 47.85 10.72 10 -23 5 75.78 14.46 -10 -23 -5 51.68 14.88 -10 -23 -5 39.22 10.81 -10 23 -6 2.06 9.28 -10 -23 -6 1.36 9.35 -10 -23 -6 26.16 10.17 10 23 6 4.12 13.05 10 -23 6 0.89 12.85 10 23 6 -13.32 9.95 -10 -23 -6 6.45 13.26 -10 -23 -6 -1.34 9.89 -10 -24 15 2.19 10.15 -10 24 15 1.78 8.41 -10 -24 15 8.97 8.42 10 -24 -15 2.56 12.59 10 -24 -15 11.61 9.61 10 24 -15 -3.68 10.41 -10 -24 14 -11.29 10.38 -10 24 14 13.35 8.37 -10 -24 14 0.55 8.11 10 -24 -14 4.85 8.84 10 24 -14 -12.66 10.23 10 24 -14 -3.52 12.32 -10 -24 13 6.79 10.12 10 24 -13 -7.84 11.87 -10 24 13 -6.24 8.64 -10 -24 13 1.62 8.03 10 -24 -13 14.77 8.80 -10 -24 12 2.88 5.26 -10 -24 12 32.60 9.95 10 24 -12 25.12 11.92 10 24 -12 6.08 8.74 -10 24 12 1.67 8.34 -10 -24 12 9.02 8.06 10 -24 -12 5.32 8.67 10 -24 -11 187.22 13.10 -10 -24 11 173.23 10.54 -10 -24 11 161.24 14.15 10 24 -11 172.61 16.98 10 24 -11 187.89 13.95 -10 24 11 172.11 13.55 10 -24 -11 160.99 13.03 10 24 -11 173.55 13.19 10 24 -10 -0.86 11.30 -10 -24 10 2.37 8.55 -10 -24 10 8.09 5.74 10 24 -10 -1.73 8.07 10 -24 -10 3.81 7.35 10 24 -10 -5.95 7.47 10 -24 -10 0.46 6.98 10 24 -9 95.97 14.02 -10 -24 9 100.42 8.70 -10 -24 9 109.17 11.19 10 24 -9 69.43 10.25 10 24 -9 106.56 9.75 10 -24 -9 91.88 9.42 10 -24 -9 89.06 9.53 10 24 -8 3.43 11.61 -10 -24 8 -6.75 6.49 -10 -24 8 11.69 8.31 10 24 -8 1.67 7.90 10 -24 -8 -9.54 7.35 10 -24 -8 0.40 6.73 10 24 -8 3.92 6.68 10 -24 -8 -4.16 6.97 10 -24 -7 12.39 6.85 10 24 -7 52.80 15.35 -10 -24 7 30.61 7.29 -10 -24 7 16.02 8.21 10 24 -7 19.34 8.31 10 -24 -7 23.20 7.81 10 24 -7 33.49 11.90 10 -24 -7 26.05 7.07 10 24 -7 26.64 6.78 -10 -24 6 5.05 7.33 10 -24 -6 7.37 6.59 10 24 -6 16.92 13.59 -10 -24 6 2.72 6.95 -10 -24 6 -0.94 7.46 10 24 -6 0.56 7.87 10 -24 -6 5.69 7.65 10 24 -6 -15.49 12.23 10 24 -6 5.32 5.90 10 -24 -6 -2.50 6.11 10 24 -5 44.89 14.17 -10 -24 5 35.00 7.82 -10 -24 5 46.22 8.09 10 24 -5 54.75 9.17 10 -24 -5 55.14 8.75 -10 -24 5 41.40 8.13 10 -24 -5 47.68 7.51 10 -24 -5 41.10 6.67 10 24 -5 42.03 6.81 10 24 -4 29.61 12.51 -10 -24 4 42.03 8.33 -10 -24 4 41.42 7.58 10 24 -4 50.40 9.07 10 -24 -4 44.98 8.98 10 -24 -4 40.67 6.41 10 24 -4 51.96 6.75 10 -24 -4 39.34 7.23 -10 -24 4 52.04 8.11 10 -24 -3 5.44 6.42 -10 -24 3 15.16 7.17 10 24 -3 4.67 11.32 -10 -24 3 5.34 7.15 -10 -24 3 14.97 6.42 10 24 -3 12.80 8.29 10 -24 -3 27.31 8.96 10 -24 -3 13.30 5.54 10 24 -3 9.83 5.78 -10 -24 3 17.28 10.22 10 24 -2 0.91 11.62 -10 -24 2 14.53 7.74 -10 -24 2 17.51 6.00 10 24 -2 18.52 8.92 10 -24 -2 6.31 8.52 -10 -24 2 16.08 10.89 -10 -24 2 7.72 7.29 10 24 -1 31.35 12.14 -10 -24 1 42.18 8.85 -10 -24 1 39.24 6.11 10 24 -1 42.36 9.37 10 -24 -1 24.02 10.05 -10 -24 1 59.65 11.93 -10 -24 1 22.92 7.63 -10 -24 0 13.43 8.03 10 24 0 5.06 8.48 10 24 0 -2.62 11.35 10 -24 0 2.81 9.60 -10 -24 0 13.80 11.10 -10 -24 0 9.71 7.44 -10 -24 -1 37.63 9.53 10 24 1 47.73 9.93 10 24 1 51.42 12.81 10 -24 1 55.89 11.83 -10 -24 -1 55.23 12.77 -10 -24 -1 40.15 8.78 -10 24 -2 18.42 7.96 -10 -24 -2 2.98 7.38 10 24 2 -2.03 9.33 10 24 2 0.81 10.96 10 -24 2 12.31 11.35 -10 -24 -2 8.97 11.89 -10 -24 -2 9.14 8.17 -10 24 -3 13.28 8.62 -10 -24 -3 -0.54 7.97 10 24 3 9.15 9.89 10 -24 3 -0.80 11.43 10 24 3 10.83 11.48 -10 -24 -3 8.44 12.91 -10 -24 -3 10.89 8.84 -10 24 -4 6.51 8.42 -10 -24 -4 14.49 8.87 10 24 4 9.41 10.53 10 -24 4 4.17 11.81 -10 -24 -4 21.82 13.00 -10 -24 -4 7.91 9.04 -10 24 -5 22.01 9.37 -10 -24 -5 48.86 9.84 -10 -24 -5 32.92 10.52 10 24 5 14.42 14.44 10 -24 5 22.39 12.74 -10 -24 -5 46.11 14.48 -10 -24 -5 43.82 10.83 -10 -25 14 17.82 10.48 -10 25 14 17.89 8.91 -10 -25 14 19.60 8.62 10 -25 -14 21.59 9.62 10 25 -14 43.83 11.33 10 25 -14 23.20 12.54 -10 -25 13 24.75 10.31 10 25 -13 7.09 11.89 -10 25 13 15.29 8.51 -10 -25 13 4.28 8.10 10 -25 -13 30.15 9.19 -10 -25 12 48.60 6.59 -10 -25 12 61.95 11.24 10 25 -12 62.56 13.47 10 25 -12 53.29 10.27 -10 25 12 60.18 9.94 -10 -25 12 78.91 9.86 10 -25 -12 68.63 10.24 10 -25 -11 3.57 7.94 -10 -25 11 4.73 5.80 -10 -25 11 -5.67 9.44 10 25 -11 9.66 11.88 10 25 -11 3.67 8.68 -10 25 11 2.20 7.98 10 -25 -11 9.32 8.23 10 25 -11 -9.43 8.24 10 25 -10 8.74 11.70 -10 -25 10 -0.60 8.70 -10 -25 10 0.35 5.98 10 25 -10 -5.96 8.22 10 -25 -10 -4.27 7.66 10 25 -10 2.28 7.45 10 -25 -10 3.35 7.37 10 25 -9 37.53 12.43 -10 -25 9 20.60 6.86 -10 -25 9 35.93 9.50 10 25 -9 23.37 8.97 10 -25 -9 26.98 7.43 10 25 -9 6.68 7.48 10 -25 -9 29.03 7.61 10 -25 -8 96.79 9.88 10 25 -8 108.78 17.92 -10 -25 8 137.92 9.94 -10 -25 8 130.55 11.56 10 25 -8 100.06 11.30 10 -25 -8 114.63 9.87 10 25 -8 110.07 14.77 10 -25 -8 115.39 10.06 10 25 -8 111.04 9.78 10 -25 -7 -1.26 6.90 10 25 -7 10.36 13.96 -10 -25 7 8.33 6.86 -10 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6.02 10 25 -2 3.68 8.28 10 -25 -2 10.05 9.49 -10 -25 2 1.50 10.89 -10 -25 2 18.97 7.60 10 25 -1 -0.92 11.26 -10 -25 1 5.38 7.69 -10 -25 1 -3.40 5.26 10 25 -1 -0.63 8.50 10 -25 -1 0.66 9.21 -10 -25 1 -0.76 10.66 -10 -25 1 2.44 7.53 -10 -25 0 18.04 8.59 10 25 0 6.48 8.69 10 25 0 14.32 12.38 10 -25 0 12.58 10.24 -10 -25 0 32.97 12.01 -10 -25 0 8.56 7.63 -10 -25 -1 13.58 8.85 10 25 1 4.68 9.19 10 25 1 3.47 11.69 10 -25 1 7.34 10.47 -10 -25 -1 4.84 11.41 -10 -25 -1 1.05 7.81 -10 -25 -2 58.11 9.75 -10 -25 -2 39.69 10.27 10 25 2 77.35 11.64 10 25 2 62.69 13.34 10 -25 2 76.84 13.10 -10 -25 -2 78.14 13.80 -10 25 -2 68.05 9.14 -10 -25 -2 66.40 9.02 -10 25 -3 69.97 9.58 -10 -25 -3 66.50 9.61 10 25 3 39.37 10.99 10 -25 3 58.49 13.27 10 25 3 65.99 12.83 -10 -25 -3 57.53 14.24 -10 -25 -3 57.46 10.07 -10 -25 -4 15.51 9.27 10 -25 4 19.13 11.89 -10 25 -4 21.76 8.81 -10 -25 -4 8.39 8.17 10 25 4 15.65 11.05 -10 -25 -4 18.62 13.43 -10 -25 -5 19.17 9.73 -10 25 -5 4.88 8.41 -10 -25 -5 7.78 8.65 10 -25 5 2.58 11.96 -10 -25 -5 -0.92 13.55 -10 -25 -5 2.62 9.77 -10 26 14 27.54 8.97 10 26 -14 -3.67 10.40 10 26 -14 2.72 11.88 10 -26 -14 -13.78 9.44 -10 -26 14 10.79 10.63 -10 26 13 10.15 8.54 -10 -26 13 9.03 10.08 10 26 -13 -2.11 10.28 10 26 -13 9.00 12.33 10 -26 -13 3.55 8.67 -10 26 12 45.48 9.71 -10 -26 12 64.73 11.27 10 26 -12 44.51 10.15 -10 -26 12 74.74 14.39 10 -26 -12 54.79 9.98 10 26 -12 79.65 14.21 -10 -26 11 -7.24 6.03 -10 -26 11 8.94 9.40 10 -26 -11 12.10 7.82 10 26 -11 5.68 8.55 -10 -26 11 -6.32 12.52 10 26 -11 6.25 12.12 -10 -26 10 43.66 7.31 -10 -26 10 60.84 10.38 10 26 -10 56.64 10.08 10 26 -10 43.58 12.84 10 -26 -10 52.48 8.55 10 26 -10 49.59 8.70 10 -26 -10 55.79 8.99 10 -26 -9 3.76 7.40 -10 -26 9 0.79 6.44 10 26 -9 -4.38 15.11 10 26 -9 11.47 8.68 10 -26 -9 4.77 7.00 10 26 -9 -1.25 7.12 10 26 -9 6.22 11.74 10 -26 -8 52.41 8.89 10 26 -8 63.42 16.48 -10 -26 8 79.78 8.81 -10 -26 8 58.49 9.95 10 26 -8 76.89 10.53 10 26 -8 54.16 13.97 10 -26 -8 63.04 8.49 10 26 -8 64.00 8.59 10 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18.41 8.95 10 -27 -6 32.05 8.00 10 27 -6 32.56 12.60 10 -27 -6 18.70 6.85 10 27 -6 14.12 6.27 -10 -27 5 7.24 8.20 10 -27 -5 5.74 7.15 10 27 -5 1.04 12.59 -10 -27 5 10.35 7.88 -10 -27 5 26.85 7.93 10 27 -5 3.72 8.59 10 -27 -5 6.90 7.56 10 27 -5 12.78 11.77 10 -27 -5 13.22 6.11 10 27 -5 5.53 5.89 10 -27 -4 69.10 8.93 -10 -27 4 74.09 9.75 10 27 -4 66.43 14.45 -10 -27 4 76.02 9.82 -10 -27 4 71.37 8.84 10 27 -4 96.77 11.25 10 -27 -4 82.69 9.95 10 27 -4 81.95 14.23 10 -27 -4 77.07 7.71 10 27 -4 75.87 7.66 10 -27 -3 1.80 7.18 -10 -27 3 7.65 7.41 10 27 -3 4.02 11.96 -10 -27 3 3.98 8.06 -10 -27 3 0.38 6.42 10 27 -3 1.91 8.54 10 -27 -3 11.00 8.74 10 27 -3 -15.01 12.33 10 -27 -3 5.43 5.81 10 27 -3 9.02 5.54 10 -27 -2 38.59 8.45 -10 -27 2 45.37 8.92 10 27 -2 50.36 13.34 -10 -27 2 50.55 9.19 -10 -27 2 53.87 7.29 10 -27 -2 45.20 10.25 10 -27 -2 71.09 7.22 10 27 -2 64.45 6.95 10 27 -2 63.41 10.41 10 27 -2 88.01 14.41 -10 -27 1 9.94 8.60 10 27 -1 -5.30 9.30 -10 -27 1 -3.16 7.89 10 -27 -1 -1.31 9.33 10 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13.38 9.55 10 28 -11 2.34 15.71 10 28 -11 6.44 12.06 -10 -28 11 22.37 12.77 10 -28 -10 -1.58 7.80 10 28 -10 -4.58 8.92 10 28 -10 5.50 12.00 -10 -28 10 -14.30 12.27 -10 -28 10 8.62 6.54 -10 -28 9 103.96 9.50 10 -28 -9 89.29 10.22 10 28 -9 92.04 11.71 10 -28 -9 79.80 9.42 10 28 -9 78.24 9.45 -10 -28 9 128.66 15.56 10 28 -9 116.31 15.36 10 -28 -8 6.34 7.57 10 28 -8 13.37 14.18 10 28 -8 14.59 9.35 -10 -28 8 10.83 7.27 10 28 -8 10.05 12.50 10 -28 -8 3.54 6.96 10 28 -8 0.37 7.04 10 -28 -7 -0.48 7.96 10 28 -7 -12.09 13.63 -10 -28 7 2.40 7.72 10 28 -7 1.26 9.17 10 28 -7 16.48 12.18 10 28 -7 6.24 6.56 10 -28 -7 -0.36 6.79 -10 -28 6 -6.04 8.25 10 -28 -6 6.51 7.41 10 28 -6 4.32 13.58 -10 -28 6 6.05 7.50 -10 -28 6 8.45 7.97 10 28 -6 15.81 9.02 10 -28 -6 -3.04 7.22 10 28 -6 1.84 11.92 10 -28 -6 9.55 6.47 10 28 -6 10.16 6.20 -10 -28 5 69.02 10.02 10 -28 -5 71.99 8.97 10 28 -5 104.02 15.76 -10 -28 5 67.32 9.80 -10 -28 5 71.68 9.13 10 28 -5 104.62 11.29 10 -28 -5 70.70 9.43 10 28 -5 70.44 14.13 10 -28 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29 -7 145.15 18.05 -10 -29 7 124.53 15.13 10 29 -7 93.73 15.38 -10 -29 6 53.71 10.12 10 -29 -6 41.65 8.70 10 29 -6 65.88 15.01 -10 -29 6 49.80 8.69 10 29 -6 63.16 10.70 10 29 -6 35.43 13.05 10 29 -6 42.15 7.04 -10 -29 5 38.69 9.36 10 -29 -5 10.58 7.85 10 29 -5 3.24 13.47 -10 -29 5 19.57 8.32 -10 -29 5 26.25 8.00 10 29 -5 28.19 9.54 10 -29 -5 20.01 7.96 10 29 -5 17.84 12.73 10 29 -5 31.20 6.35 10 -29 -4 42.99 8.94 -10 -29 4 53.75 9.72 10 29 -4 39.50 14.60 -10 -29 4 50.61 9.14 -10 -29 4 64.31 8.51 10 29 -4 65.05 10.62 10 -29 -4 61.31 9.57 10 29 -4 77.01 14.46 10 29 -4 45.76 6.64 10 -29 -3 35.70 8.39 -10 -29 3 17.68 8.80 10 29 -3 27.36 13.57 -10 -29 3 33.85 9.03 -10 -29 3 21.95 7.07 10 -29 -3 31.28 9.29 10 29 -3 30.69 6.16 10 29 -3 34.92 10.16 10 29 -3 22.26 13.18 10 29 -2 -6.20 12.50 -10 -29 2 -3.09 8.38 10 29 -2 -6.80 9.51 10 -29 -2 -9.99 8.33 -10 -29 2 2.78 8.31 10 -29 -2 -6.11 9.30 10 29 -2 4.90 5.53 10 29 -2 9.85 12.85 -10 -29 1 62.42 10.75 10 29 -1 72.76 11.65 -10 -29 1 42.97 9.59 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38.16 8.95 10 30 -8 44.45 10.33 10 30 -8 23.01 14.85 -10 -30 8 28.56 13.16 10 30 -8 44.97 13.60 10 30 -7 -8.18 6.48 -10 -30 7 -2.02 7.72 10 -30 -7 7.67 8.38 10 30 -7 0.67 9.91 10 30 -7 9.09 14.00 -10 -30 7 -18.49 12.91 10 30 -7 10.33 12.87 10 30 -6 -3.70 6.19 -10 -30 6 0.59 9.00 10 -30 -6 8.55 8.28 10 30 -6 -1.12 13.92 -10 -30 6 3.72 7.89 10 30 -6 12.03 9.61 10 30 -6 -3.78 12.80 -10 -30 6 -16.56 13.02 -10 -30 5 5.24 8.82 10 -30 -5 6.00 7.93 10 30 -5 4.42 13.73 -10 -30 5 13.90 8.44 -10 -30 5 -0.48 7.56 10 30 -5 0.67 9.31 10 -30 -5 7.94 7.61 10 30 -5 10.46 12.43 10 30 -5 8.55 5.87 10 -30 -4 16.57 8.29 -10 -30 4 17.84 8.72 10 30 -4 27.26 13.68 -10 -30 4 11.03 8.30 -10 -30 4 20.56 7.79 10 30 -4 10.21 9.69 10 -30 -4 21.70 8.61 10 30 -4 13.49 13.38 10 30 -4 9.22 5.59 10 -30 -3 11.70 8.05 -10 -30 3 5.16 8.62 -10 -30 3 16.95 8.31 -10 -30 3 -3.97 7.05 10 -30 -3 5.06 8.73 10 30 -3 10.36 5.52 10 30 -3 4.13 9.28 10 30 -3 8.83 12.67 10 30 -2 9.50 13.35 -10 -30 2 -3.15 8.62 10 30 -2 -0.70 9.30 10 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79.64 10.62 11 -7 -13 65.36 11.38 11 7 -13 82.87 12.55 11 -7 -13 76.96 11.04 11 7 -13 72.20 10.89 -11 7 13 73.56 10.15 -11 -7 13 88.19 10.38 11 7 -13 81.47 9.13 11 7 -12 2.34 6.50 -11 -7 12 1.74 8.11 -11 7 12 5.77 8.04 -11 -7 12 4.04 7.60 11 -7 -12 -4.42 8.34 11 7 -12 6.14 8.22 -11 -7 12 3.47 4.95 11 -7 -12 -5.14 8.81 11 7 -12 15.89 9.76 11 -7 -11 27.58 8.59 11 7 -11 -1.11 9.11 -11 -7 11 16.08 8.24 -11 7 11 15.88 8.75 -11 7 11 33.71 8.29 -11 -7 11 29.68 8.26 11 -7 -11 9.74 7.61 11 7 -11 15.65 8.05 11 -7 -11 9.65 3.33 -11 -7 11 15.98 4.57 11 -7 -10 53.56 9.03 11 7 -10 35.52 9.26 -11 7 10 34.67 8.33 -11 -7 10 25.11 8.35 -11 -7 10 44.68 8.78 -11 -7 10 26.64 4.02 -11 7 10 35.50 9.53 11 -7 -10 30.24 8.08 11 7 -10 21.56 7.81 11 -7 -10 25.36 6.78 11 -7 -10 21.49 2.60 -11 -7 10 27.01 4.33 -11 7 9 -5.13 7.47 -11 -7 9 1.15 7.63 -11 -7 9 -2.81 3.26 11 7 -9 -9.81 7.87 11 -7 -9 8.83 7.36 11 -7 -9 -3.37 3.97 -11 -7 9 6.12 7.16 -11 7 9 -2.44 8.12 -11 -7 9 1.26 3.98 11 -7 -9 -3.19 6.46 11 7 -9 -3.27 6.79 11 7 -9 -5.64 4.68 11 7 -9 6.33 8.80 11 -7 -9 4.85 5.78 -11 -7 9 0.56 8.91 11 -7 -9 2.64 1.63 -11 7 8 5.77 7.37 11 -7 -8 22.69 6.84 11 7 -8 14.06 7.14 11 -7 -8 14.33 4.47 -11 -7 8 11.25 7.29 -11 -7 8 14.81 4.72 11 -7 -8 27.49 6.74 11 7 -8 13.47 6.46 11 7 -8 16.74 4.62 11 -7 -8 11.37 2.25 -11 -7 8 8.43 8.45 11 -7 -8 18.63 5.50 11 -7 -8 10.95 2.08 11 7 -8 22.01 9.27 11 -7 -7 31.35 7.23 11 7 -7 25.00 9.26 11 -7 -7 11.64 4.67 -11 -7 7 14.93 5.14 -11 -7 7 21.54 7.58 11 -7 -7 17.78 6.27 11 7 -7 29.25 6.91 11 7 -7 22.97 4.92 11 -7 -7 17.18 3.17 -11 -7 7 18.55 8.24 11 -7 -7 25.53 6.59 11 -7 -6 236.80 13.12 11 7 -6 208.81 15.43 -11 -7 6 227.43 11.85 -11 -7 6 245.14 13.65 11 -7 -6 236.83 13.12 11 7 -6 220.05 11.02 -11 -7 6 216.58 13.85 11 -7 -6 194.22 9.50 11 -7 -6 221.10 11.69 -11 7 5 18.15 6.24 -11 -7 5 15.20 5.90 -11 -7 5 11.92 6.73 11 -7 -5 17.68 4.84 11 7 -5 14.12 5.07 11 -7 -5 19.90 4.02 -11 -7 5 17.91 7.69 11 7 -5 11.84 8.80 11 -7 -5 17.89 6.68 -11 7 4 40.04 7.14 -11 -7 4 39.68 7.37 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11 -6 85.09 8.42 11 11 -5 36.86 10.64 11 -11 -5 33.20 6.48 -11 -11 5 21.95 7.31 -11 -11 5 25.92 6.28 11 11 -5 32.37 6.35 -11 -11 5 29.73 8.85 -11 -11 5 20.21 3.14 11 11 -4 15.38 9.76 11 -11 -4 9.75 2.78 11 -11 -4 20.31 6.15 -11 -11 4 2.72 6.44 -11 -11 4 16.73 6.43 11 11 -4 9.89 5.84 -11 -11 4 9.42 8.05 -11 -11 4 6.42 3.00 11 -11 -3 3.94 5.65 11 -11 -3 1.54 3.64 11 11 -3 -2.83 9.25 -11 -11 3 1.32 6.35 -11 -11 3 14.47 6.11 11 -11 -3 3.07 1.85 11 11 -3 -6.78 6.28 -11 -11 3 21.36 8.16 -11 -11 3 5.03 3.25 11 -11 -2 20.51 6.31 11 11 -2 10.82 10.10 11 -11 -2 12.03 6.48 -11 -11 2 12.79 6.96 -11 11 2 14.26 7.23 -11 -11 2 8.68 6.00 11 11 -2 9.23 6.71 11 -11 -2 23.36 10.12 -11 -11 2 22.60 8.67 11 -11 -2 4.66 1.64 -11 -11 2 14.65 3.95 11 -11 -2 5.74 1.62 -11 -11 1 11.07 4.50 11 11 -1 29.72 10.67 11 -11 -1 6.40 6.07 -11 -11 1 13.70 7.12 -11 11 1 10.16 7.10 -11 -11 1 8.18 5.66 11 -11 -1 5.91 9.90 -11 11 1 10.70 7.96 -11 -11 1 -7.80 7.49 -11 -11 1 17.58 8.62 -11 -11 0 55.07 6.25 11 11 0 54.66 10.51 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32.38 10.40 -11 -13 4 15.68 6.58 -11 -13 4 18.11 6.72 11 13 -4 19.80 6.56 -11 -13 4 25.71 8.98 11 -13 -4 14.37 2.08 -11 -13 4 14.07 4.15 11 13 -3 52.11 11.02 11 -13 -3 48.23 5.89 -11 -13 3 45.62 7.58 -11 -13 3 47.43 7.21 11 13 -3 50.39 7.51 11 -13 -3 50.34 10.25 -11 -13 3 41.67 9.28 -11 -13 3 47.30 5.00 11 -13 -3 28.94 3.33 11 -13 -2 6.12 5.09 11 13 -2 4.56 10.18 -11 -13 2 -2.45 6.78 -11 -13 2 4.88 5.75 11 13 -2 3.89 6.44 11 -13 -2 5.70 9.38 -11 -13 2 7.05 8.56 11 -13 -2 3.97 3.19 -11 -13 2 5.12 4.46 -11 13 1 219.58 13.61 -11 -13 1 183.11 13.09 11 13 -1 155.72 15.27 -11 -13 1 188.15 12.71 11 -13 -1 177.41 15.46 -11 -13 1 155.50 10.30 -11 -13 1 178.24 9.93 -11 -13 1 214.08 14.26 11 -13 -1 179.42 9.92 11 13 -1 162.44 15.78 -11 13 0 100.09 10.87 -11 -13 0 111.91 10.91 11 13 0 89.73 11.74 -11 -13 0 100.03 10.46 -11 -13 0 86.55 7.73 11 -13 0 104.16 13.18 -11 -13 0 107.88 11.87 11 13 0 96.81 13.69 -11 13 -1 71.24 10.33 -11 -13 -1 70.58 10.14 11 13 1 61.90 10.74 -11 -13 -1 60.72 9.38 -11 13 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12 -7 -9 279.85 15.10 12 -7 -8 12.81 2.02 12 -7 -8 15.33 7.62 12 7 -8 16.57 9.81 -12 -7 8 19.08 5.43 -12 -7 8 31.70 8.32 -12 -7 8 22.37 9.18 12 7 -8 20.60 4.84 12 -7 -8 30.01 7.11 12 -7 -8 28.23 7.25 12 7 -8 30.60 7.78 12 -7 -7 32.05 7.96 12 7 -7 28.13 10.43 -12 -7 7 42.29 6.31 -12 -7 7 54.23 8.71 -12 -7 7 38.66 9.02 12 7 -7 30.95 5.24 12 -7 -7 30.77 6.48 12 -7 -7 29.56 7.20 12 7 -7 32.42 7.45 -12 -7 6 5.84 7.59 -12 -7 6 6.58 5.66 12 -7 -6 6.74 5.53 12 7 -6 7.09 4.99 12 7 -6 1.37 9.53 12 -7 -6 10.12 7.31 -12 -7 6 1.45 8.03 -12 7 5 27.63 7.01 -12 -7 5 40.52 8.07 -12 -7 5 36.27 6.83 12 -7 -5 25.32 4.80 12 7 -5 33.33 5.83 12 7 -5 21.12 9.99 12 -7 -5 40.19 8.07 -12 -7 5 32.23 8.55 -12 7 4 12.79 6.67 -12 -7 4 14.73 6.57 -12 -7 4 18.15 7.13 12 -7 -4 5.95 3.44 12 7 -4 14.96 5.58 -12 -7 4 10.73 7.94 12 7 -4 19.84 10.13 12 -7 -4 11.18 7.17 12 7 -3 96.01 8.24 12 -7 -3 115.15 10.18 12 7 -3 116.73 12.84 -12 -7 3 97.89 9.49 -12 7 3 100.04 9.78 -12 -7 3 107.13 9.46 -12 -7 3 114.78 10.44 12 7 -2 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110.57 11.87 12 -8 -8 116.97 9.62 12 -8 -7 3.05 7.10 12 8 -7 1.41 9.40 -12 -8 7 10.66 5.49 -12 -8 7 11.57 7.55 12 -8 -7 -1.38 6.43 12 8 -7 -0.95 7.13 12 8 -7 1.29 4.83 -12 -8 7 -5.77 8.92 12 -8 -7 -2.83 6.07 -12 -8 6 172.79 10.84 -12 -8 6 158.22 11.95 12 -8 -6 165.00 9.75 12 8 -6 157.77 9.57 12 8 -6 174.52 14.67 12 -8 -6 180.75 11.91 -12 -8 6 193.54 13.14 -12 8 5 4.49 6.15 -12 -8 5 9.19 7.22 -12 -8 5 -1.61 5.91 -12 -8 5 -1.43 8.08 12 8 -5 9.90 5.12 12 8 -5 18.91 9.89 12 -8 -5 14.48 6.97 12 -8 -5 3.90 4.36 -12 -8 4 107.46 9.17 -12 -8 4 103.83 9.50 -12 8 4 118.07 9.61 12 -8 -4 111.81 9.69 12 8 -4 100.60 12.68 12 8 -4 97.75 7.93 -12 -8 4 99.20 10.31 12 -8 -4 85.59 5.84 12 8 -3 17.92 6.10 12 -8 -3 16.99 7.64 12 8 -3 11.35 9.80 -12 8 3 4.77 6.81 -12 -8 3 40.60 7.36 -12 -8 3 22.10 7.14 -12 -8 3 15.72 8.36 -12 -8 2 119.07 10.67 -12 8 2 138.59 10.72 -12 -8 2 132.83 11.21 -12 8 2 92.62 10.89 -12 -8 2 97.58 11.11 12 8 -2 126.44 13.80 12 -8 -2 103.43 10.16 -12 -8 1 -7.57 7.82 -12 8 1 11.91 7.64 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10.90 8.71 12 9 -12 8.77 9.03 -12 -9 11 15.99 8.97 -12 -9 11 23.84 3.80 12 -9 -11 25.26 8.27 12 9 -11 18.70 8.69 -12 9 11 37.86 9.19 -12 -9 11 39.35 9.01 12 9 -11 15.76 9.61 12 -9 -11 33.53 9.12 12 -9 -10 16.59 8.01 12 9 -10 13.17 9.88 -12 -9 10 15.34 7.93 -12 -9 10 8.88 4.18 12 -9 -10 13.22 7.43 12 9 -10 19.37 8.22 12 9 -10 5.71 5.06 -12 9 10 6.43 8.24 -12 -9 10 11.03 8.53 -12 -9 10 4.17 3.25 12 -9 -9 15.75 7.50 12 9 -9 16.03 10.14 -12 -9 9 15.28 8.18 -12 -9 9 8.32 4.74 -12 -9 9 7.37 9.20 12 9 -9 13.01 5.15 12 -9 -9 4.39 6.87 12 9 -9 20.11 7.60 12 -9 -9 18.67 7.53 12 9 -8 121.09 12.95 12 -9 -8 101.48 9.74 -12 -9 8 87.52 7.67 -12 -9 8 115.02 11.05 12 -9 -8 111.38 9.51 12 9 -8 108.88 7.90 -12 -9 8 93.93 11.65 12 9 -8 97.59 9.78 12 -9 -8 113.92 9.92 12 -9 -7 79.11 8.92 12 9 -7 80.22 11.98 -12 -9 7 87.66 7.73 -12 -9 7 91.57 9.75 12 -9 -7 76.11 7.93 12 9 -7 78.17 6.95 -12 -9 7 87.11 10.66 12 -9 -7 83.24 8.68 12 9 -7 87.70 9.12 12 9 -6 18.71 10.37 12 -9 -6 36.74 7.53 -12 -9 6 45.90 6.85 -12 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120.52 10.82 -12 -24 5 95.92 10.27 12 24 -5 137.50 12.13 12 -24 -5 95.67 11.88 12 -24 -5 118.77 9.82 12 24 -5 107.90 9.77 -12 -24 5 124.07 14.55 -12 -24 4 41.09 7.42 12 24 -4 20.36 13.22 -12 -24 4 16.30 8.67 -12 -24 4 16.88 7.26 12 -24 -4 20.43 9.86 -12 -24 4 14.73 11.36 12 24 -4 20.32 9.18 12 24 -4 19.94 7.11 12 -24 -4 26.68 7.08 12 -24 -3 12.29 6.74 -12 -24 3 -4.62 6.83 -12 -24 3 20.13 8.61 12 24 -3 -0.61 8.94 12 24 -3 19.75 12.81 12 -24 -3 17.21 10.36 -12 -24 3 0.77 11.92 12 24 -3 9.12 13.27 -12 -24 2 60.47 8.57 -12 -24 2 59.74 10.30 12 24 -2 55.37 10.86 12 24 -2 63.39 14.72 12 -24 -2 64.71 13.02 -12 -24 2 43.79 13.35 12 24 -2 35.96 15.18 -12 -24 1 37.53 8.51 -12 -24 1 50.84 11.13 12 24 -1 39.58 10.95 12 24 -1 38.09 14.16 12 -24 -1 36.19 13.03 -12 -24 1 38.22 13.78 12 24 -1 31.17 15.32 -12 -24 0 2.66 7.84 -12 -24 0 -0.68 9.39 12 24 0 23.47 10.44 12 24 0 22.29 12.55 12 -24 0 21.26 12.33 -12 -24 0 21.07 12.77 12 24 0 27.38 14.39 -12 -24 -1 31.02 8.82 12 24 1 31.47 13.05 12 24 1 49.92 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42.40 13.21 -12 -27 1 45.24 8.97 -12 -27 0 64.56 11.47 12 27 0 73.24 12.32 12 -27 0 71.63 13.32 -12 -27 0 54.17 14.34 12 27 0 64.70 15.40 12 28 -10 1.23 15.60 -12 -28 10 -0.40 6.23 -12 -28 10 3.14 8.85 -12 -28 10 -5.71 13.48 12 28 -10 7.05 8.81 12 28 -10 1.04 13.87 12 28 -10 -11.29 8.33 12 28 -9 -0.44 7.78 12 28 -9 7.28 14.78 -12 -28 9 -1.32 6.87 -12 -28 9 -4.76 9.00 -12 -28 9 0.50 8.09 12 28 -9 -8.28 9.39 -12 -28 9 20.20 12.85 12 28 -9 32.16 14.09 12 28 -8 -0.42 7.39 12 28 -8 -3.58 14.70 -12 -28 8 0.48 7.11 -12 -28 8 9.55 9.00 -12 -28 8 -4.34 7.93 12 28 -8 2.54 9.03 -12 -28 8 17.01 12.92 12 28 -8 -20.77 13.62 12 28 -7 12.88 7.40 12 28 -7 12.87 14.07 -12 -28 7 21.41 7.81 -12 -28 7 5.79 8.16 -12 -28 7 15.93 8.20 12 28 -7 21.00 9.70 -12 -28 7 22.62 12.75 12 28 -7 22.94 13.61 12 28 -6 13.71 7.08 -12 -28 6 0.92 7.42 12 28 -6 -5.72 13.52 -12 -28 6 1.62 7.72 -12 -28 6 3.92 7.82 12 28 -6 0.64 9.36 12 28 -6 1.05 13.68 -12 -28 6 5.14 12.18 12 28 -5 10.05 6.58 -12 -28 5 -0.45 7.58 12 28 -5 4.48 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13 -6 -7 21.48 5.92 -13 -6 7 52.79 9.10 -13 -6 7 33.17 6.60 13 6 -7 45.09 11.09 13 -6 -7 33.25 8.86 13 6 -7 28.39 4.93 13 -6 -7 32.73 7.30 13 6 -7 13.95 7.57 -13 -6 7 18.02 9.01 13 6 -6 83.55 12.13 13 -6 -6 68.95 9.60 13 6 -6 68.83 6.34 -13 -6 6 78.02 8.13 -13 -6 6 91.52 10.10 -13 6 6 97.29 8.48 -13 -6 6 100.84 10.37 13 -6 -6 70.71 6.35 -13 6 5 12.05 6.64 -13 -6 5 -1.02 7.56 -13 -6 5 5.77 6.43 -13 -6 5 -2.77 7.82 13 6 -5 -4.32 9.96 13 -6 -5 7.89 7.81 13 6 -5 8.68 4.93 -13 6 4 30.36 7.53 -13 -6 4 34.69 8.46 -13 -6 4 27.74 7.40 -13 -6 4 27.37 8.39 13 6 -4 27.37 10.76 13 -6 -4 7.93 8.26 13 6 -4 23.13 5.86 -13 -6 3 1.02 6.92 -13 6 3 4.13 7.34 -13 -6 3 -9.26 7.99 13 -6 -3 20.47 8.79 13 6 -3 -8.04 10.53 13 6 -3 -3.26 5.79 13 6 -2 24.59 11.09 13 -6 -2 15.65 8.38 -13 -6 2 2.22 7.84 -13 -6 2 1.09 7.27 -13 6 2 1.10 7.68 -13 -6 1 7.58 7.48 -13 6 1 7.57 7.53 13 6 -1 9.85 10.63 13 -6 -1 12.27 8.79 13 -6 -1 21.37 11.94 -13 -6 1 15.66 7.96 -13 6 1 4.72 8.81 -13 -6 1 3.34 8.57 13 6 0 84.29 11.40 13 -6 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13.82 12.28 -13 7 16 24.57 11.34 -13 -7 16 -3.74 10.51 13 -7 -16 -0.77 11.05 13 7 -16 -10.17 11.32 -13 7 16 7.37 10.07 -13 -7 16 -24.26 10.78 13 7 -15 31.92 8.56 13 -7 -15 36.27 11.72 13 7 -15 21.19 11.77 -13 -7 15 32.62 10.59 13 -7 -15 40.32 11.43 13 7 -15 24.16 10.89 -13 7 15 28.40 10.36 -13 -7 15 8.69 9.62 13 7 -14 7.83 7.46 13 7 -14 -2.80 10.47 13 -7 -14 6.59 10.03 -13 -7 14 14.04 10.11 13 -7 -14 5.38 9.53 13 7 -14 21.25 10.28 -13 7 14 -7.89 8.84 -13 -7 14 -1.44 8.95 13 7 -13 31.55 7.78 13 7 -13 12.19 10.22 13 -7 -13 35.78 10.35 -13 7 13 33.91 11.36 -13 -7 13 29.18 10.12 13 -7 -13 47.93 10.09 13 7 -13 40.65 10.11 -13 7 13 32.72 9.86 -13 -7 13 43.51 10.09 13 7 -12 79.94 11.99 13 -7 -12 101.14 11.36 -13 -7 12 93.15 11.78 13 -7 -12 87.96 11.20 13 7 -12 93.90 11.31 -13 7 12 96.37 11.91 -13 -7 12 113.83 12.14 13 7 -11 47.31 11.40 13 7 -11 54.50 9.97 13 -7 -11 45.36 9.35 -13 -7 11 60.79 10.28 -13 -7 11 19.52 4.23 13 -7 -11 46.77 9.24 13 7 -11 45.84 9.59 -13 7 11 34.15 10.11 -13 -7 11 42.88 10.34 -13 -7 10 53.77 10.04 -13 -7 10 30.34 5.36 13 -7 -10 39.15 9.21 13 7 -10 41.80 11.49 13 -7 -10 48.66 8.82 13 7 -10 62.90 9.48 13 -7 -10 32.44 8.46 13 -7 -9 16.36 7.47 -13 -7 9 -1.16 5.22 -13 -7 9 -0.59 8.35 13 7 -9 16.64 10.61 13 -7 -9 -1.57 8.36 13 7 -9 -1.82 4.94 13 -7 -9 2.09 7.31 13 7 -9 3.23 7.52 -13 -7 9 6.56 9.03 13 -7 -8 6.33 6.72 -13 -7 8 3.98 8.44 -13 -7 8 -2.01 5.68 13 -7 -8 7.11 8.07 13 7 -8 9.02 10.52 13 7 -8 1.84 4.88 13 -7 -8 13.19 7.78 13 7 -8 -4.19 7.39 -13 -7 8 -6.21 9.36 13 -7 -7 -4.94 5.75 -13 -7 7 7.68 8.40 -13 -7 7 9.74 6.22 13 7 -7 14.92 10.17 13 -7 -7 3.45 7.79 13 7 -7 5.74 4.72 13 7 -7 1.03 7.26 13 -7 -7 -6.53 6.99 -13 -7 7 3.70 8.56 13 7 -6 24.40 10.94 13 -7 -6 20.19 7.90 13 7 -6 13.17 5.10 -13 -7 6 14.76 6.53 -13 -7 6 10.03 8.05 -13 -7 6 14.09 8.41 13 -7 -6 10.68 5.05 -13 -7 5 16.64 7.58 -13 7 5 9.43 6.60 -13 -7 5 5.35 6.42 -13 -7 5 3.36 7.94 13 7 -5 -9.60 10.37 13 -7 -5 6.63 7.85 13 7 -5 9.02 5.13 -13 -7 4 129.85 10.83 -13 -7 4 112.84 10.07 -13 7 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8.96 6.88 13 11 -7 5.67 7.41 -13 -11 7 10.13 9.35 13 -11 -6 3.73 5.25 13 11 -6 5.16 7.33 13 -11 -6 7.49 7.05 -13 -11 6 25.11 8.26 -13 -11 6 -0.43 6.34 13 11 -6 8.15 11.11 13 -11 -6 0.79 7.03 -13 -11 6 2.86 9.06 13 11 -6 14.10 6.09 -13 -11 5 18.12 7.93 -13 -11 5 8.78 6.96 13 -11 -5 14.26 7.18 13 11 -5 0.82 10.79 -13 -11 5 4.44 9.00 13 11 -5 10.66 6.11 -13 -11 4 105.63 10.02 -13 -11 4 105.02 10.04 13 11 -4 89.17 8.92 13 -11 -4 102.91 9.62 13 11 -4 123.48 14.18 -13 -11 4 102.47 11.61 -13 -11 3 -6.90 7.16 -13 -11 3 -12.10 7.26 13 11 -3 0.41 6.52 13 -11 -3 9.29 11.06 13 -11 -3 11.37 7.00 13 11 -3 7.47 10.78 -13 -11 3 -5.43 8.99 -13 -11 2 183.99 13.22 13 -11 -2 202.39 17.21 13 11 -2 143.09 11.40 -13 -11 2 155.57 13.38 13 11 -2 175.38 16.48 13 11 -1 22.90 10.54 13 11 -1 29.07 12.60 -13 11 1 46.76 9.19 -13 -11 1 30.75 8.70 13 11 -1 4.68 7.50 13 -11 -1 30.55 12.38 -13 -11 1 38.75 9.64 -13 11 1 11.15 8.48 -13 -11 1 12.99 8.55 13 11 0 93.58 12.39 13 11 0 104.53 15.33 13 -11 0 115.21 15.50 -13 11 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7.16 13 14 -10 20.51 6.56 -13 -14 10 22.48 11.10 13 -14 -10 19.67 8.46 13 -14 -9 26.89 7.92 13 14 -9 28.88 8.34 -13 -14 9 16.04 8.82 -13 -14 9 25.71 6.22 13 -14 -9 27.85 7.13 13 14 -9 27.33 12.47 13 14 -9 17.28 6.59 -13 -14 9 22.01 11.29 13 -14 -9 13.77 8.26 13 -14 -8 53.87 8.21 13 14 -8 58.90 9.10 -13 -14 8 41.06 6.95 -13 -14 8 65.60 9.66 13 14 -8 65.92 13.56 13 -14 -8 39.44 7.29 13 14 -8 44.93 7.17 -13 -14 8 53.99 11.67 13 -14 -8 47.42 8.48 13 -14 -7 7.41 6.67 13 14 -7 -4.08 7.11 -13 -14 7 6.12 6.18 -13 -14 7 13.51 7.98 13 14 -7 -13.99 11.98 13 14 -7 7.54 6.08 -13 -14 7 6.47 9.90 13 -14 -7 4.02 6.33 13 14 -6 75.32 9.11 13 -14 -6 49.29 7.98 13 14 -6 52.32 12.82 -13 -14 6 47.56 7.89 -13 -14 6 62.37 9.10 13 14 -6 37.29 7.41 -13 -14 6 48.04 10.72 13 -14 -6 56.72 7.09 -13 -14 5 8.16 6.99 -13 -14 5 23.99 7.59 13 14 -5 25.43 6.88 13 -14 -5 14.03 10.40 -13 -14 5 14.00 9.66 13 14 -5 1.75 11.48 -13 -14 4 11.84 7.43 -13 -14 4 -1.73 6.96 13 14 -4 -3.88 6.84 13 -14 -4 6.48 10.67 -13 -14 4 8.42 9.51 13 14 -4 7.01 11.16 -13 -14 3 18.69 7.90 -13 -14 3 25.04 7.04 13 14 -3 12.32 7.24 13 -14 -3 5.88 11.04 -13 -14 3 22.91 9.83 13 14 -3 -3.56 11.75 13 14 -2 23.47 12.60 -13 -14 2 22.79 8.50 13 14 -2 28.04 8.12 13 -14 -2 25.18 12.08 -13 -14 2 15.75 9.81 13 14 -2 30.30 11.98 13 14 -1 27.43 12.53 -13 -14 1 56.97 10.08 13 14 -1 46.05 8.88 13 -14 -1 52.78 13.68 -13 -14 1 36.33 10.81 13 14 -1 23.46 11.50 13 14 0 17.00 10.22 13 14 0 8.36 12.59 -13 -14 0 0.65 8.42 13 14 0 8.69 8.06 13 -14 0 2.75 11.99 -13 14 0 -6.07 9.40 -13 -14 0 4.67 8.56 -13 -14 0 -0.63 10.02 -13 -14 -1 10.31 9.14 -13 -14 -1 16.85 10.52 13 -14 1 25.38 12.98 13 14 1 29.17 13.09 -13 14 -1 12.09 9.31 -13 -14 -1 9.87 8.97 -13 -14 -2 -7.93 9.61 -13 -14 -2 12.01 10.29 13 -14 2 -6.73 12.67 13 14 2 11.47 12.72 -13 14 -2 20.89 9.77 -13 -14 -2 -9.62 9.86 -13 -14 -3 -13.57 10.86 -13 -14 -3 1.37 10.64 13 -14 3 15.67 13.05 -13 14 -3 21.05 10.33 -13 -14 -3 13.95 10.17 13 14 3 8.74 13.27 -13 -15 15 8.75 10.22 13 15 -15 -2.89 9.23 13 -15 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11.30 -15 -19 9 27.11 12.55 15 19 -9 3.50 9.29 15 -19 -9 40.07 9.12 -15 -19 8 14.32 7.73 -15 -19 8 14.95 9.12 15 19 -8 -8.61 15.15 15 -19 -8 20.19 10.88 -15 -19 8 19.07 12.55 15 -19 -8 25.32 8.40 15 19 -8 15.48 8.80 -15 -19 7 3.25 8.67 -15 -19 7 15.56 7.50 15 19 -7 -15.02 14.62 15 -19 -7 4.89 10.63 -15 -19 7 11.58 11.76 15 19 -7 20.93 8.73 15 -19 -7 2.78 7.71 15 19 -6 68.18 18.43 -15 -19 6 67.08 10.05 15 19 -6 71.87 16.46 15 -19 -6 64.63 13.45 -15 -19 6 90.33 13.75 15 -19 -6 77.48 10.07 15 19 -6 80.68 10.92 15 19 -5 -3.07 14.02 15 19 -5 14.03 14.13 15 -19 -5 1.77 12.29 15 19 -5 2.25 8.61 15 -19 -5 5.01 7.93 -15 -19 5 -5.17 11.85 -15 -19 5 -5.20 8.85 -16 0 13 21.23 11.60 16 0 -13 6.48 11.50 16 0 -13 -0.70 10.14 -16 0 12 12.53 10.70 16 0 -12 7.22 11.76 16 0 -12 3.40 9.62 16 0 -11 -3.98 11.32 16 0 -11 0.66 9.11 16 0 -10 57.16 12.81 16 0 -10 59.93 10.33 16 0 -9 7.70 11.01 16 0 -9 16.48 8.87 -16 0 8 9.07 7.15 16 0 -8 19.99 8.56 -16 0 7 -7.19 7.71 16 0 -7 6.72 11.26 16 0 -7 -3.75 8.71 16 0 -6 101.24 14.04 -16 0 6 96.19 11.10 16 0 -5 5.20 10.92 -16 0 5 -0.56 8.31 16 0 -4 10.36 11.05 -16 0 4 26.34 8.91 16 0 -3 -8.14 10.81 -16 0 3 3.80 8.60 16 0 -2 32.51 11.74 -16 0 2 31.41 10.02 -16 1 13 6.01 11.36 -16 -1 13 -0.84 11.50 16 -1 -13 -9.52 11.95 16 1 -13 13.24 11.90 16 -1 -13 -19.70 10.65 -16 -1 12 -9.07 10.56 16 -1 -12 -0.78 11.51 16 1 -12 17.23 11.81 16 -1 -12 8.15 9.49 -16 -1 11 1.62 10.91 16 1 -11 -8.14 11.70 16 -1 -11 3.88 11.01 16 -1 -11 9.23 9.40 16 1 -10 -1.60 11.48 16 -1 -10 16.03 11.26 16 -1 -10 -3.87 9.34 16 1 -10 30.32 9.93 -16 -1 9 20.10 7.15 16 1 -9 6.32 11.00 16 -1 -9 3.75 10.84 16 -1 -9 -1.90 8.65 16 1 -9 17.75 8.91 -16 -1 8 14.30 7.22 -16 1 8 9.03 6.91 16 1 -8 14.02 11.15 16 -1 -8 19.18 10.67 16 -1 -8 8.12 8.52 16 1 -8 10.00 8.42 -16 1 7 58.37 9.29 -16 -1 7 58.11 9.03 16 1 -7 41.48 12.44 16 -1 -7 47.19 12.36 16 -1 -7 85.03 10.70 16 1 -7 77.58 10.72 16 1 -6 26.75 11.73 16 -1 -6 32.53 11.55 -16 1 6 8.33 8.16 -16 -1 6 52.24 9.41 16 1 -5 -4.58 11.93 16 -1 -5 -9.38 10.87 -16 -1 5 -5.06 8.65 -16 1 5 3.37 8.21 16 1 -4 12.18 11.31 16 -1 -4 7.18 10.82 -16 -1 4 34.11 9.26 -16 1 4 5.97 8.42 16 1 -3 6.86 11.19 16 -1 -3 8.61 11.15 -16 -1 3 -7.63 9.35 -16 1 3 -3.81 9.21 16 1 -2 6.85 11.40 16 -1 -2 25.78 11.47 -16 -1 2 17.41 9.63 -16 1 2 33.42 9.92 -16 -2 13 16.60 11.66 16 -2 -13 10.08 11.08 16 2 -13 7.61 12.17 16 -2 -13 41.51 10.94 -16 -2 12 14.65 11.09 16 -2 -12 16.86 11.07 16 2 -12 -15.09 12.09 16 -2 -12 4.07 9.60 -16 -2 11 15.17 11.08 16 -2 -11 -8.33 11.03 16 2 -11 -18.31 11.99 16 -2 -11 7.24 9.29 -16 -2 10 -13.29 11.12 16 2 -10 13.15 11.24 16 -2 -10 5.95 10.71 16 -2 -10 -2.57 8.98 -16 -2 9 4.20 6.45 16 2 -9 -9.73 11.31 16 -2 -9 -5.84 10.90 16 -2 -9 3.79 8.62 -16 -2 8 -5.65 7.10 16 2 -8 12.79 11.21 16 -2 -8 0.72 10.16 16 -2 -8 -12.49 8.68 -16 2 7 -10.50 8.14 -16 -2 7 -0.48 8.03 16 2 -7 9.46 11.68 16 -2 -7 -7.05 10.87 16 -2 -7 28.10 9.21 16 2 -6 10.99 11.62 16 -2 -6 -4.91 10.34 -16 2 6 -8.34 8.12 -16 -2 6 -4.18 7.87 16 2 -5 25.91 12.15 16 -2 -5 57.95 11.88 -16 -2 5 35.44 9.34 -16 2 5 47.62 9.33 16 2 -4 5.48 11.22 16 -2 -4 0.70 10.61 -16 -2 4 11.39 8.59 -16 2 4 -2.39 8.56 16 -2 -3 42.99 11.44 16 2 -3 39.21 12.56 -16 -2 3 22.25 9.93 -16 2 3 36.76 9.70 -16 -2 2 -9.40 9.50 -16 2 2 -18.01 10.10 -16 -3 13 13.97 11.16 16 3 -13 6.04 12.15 16 -3 -13 -7.58 10.90 16 -3 -13 11.94 10.22 -16 -3 12 2.41 10.93 16 -3 -12 -8.97 10.92 16 3 -12 -6.85 12.31 16 -3 -12 10.82 9.61 -16 -3 11 0.79 11.25 16 -3 -11 5.16 10.87 16 3 -11 17.03 12.41 16 -3 -11 17.07 9.40 -16 -3 10 -0.77 10.64 16 3 -10 29.44 12.28 16 -3 -10 3.62 10.46 16 -3 -10 11.57 9.06 -16 -3 9 -1.15 6.54 16 3 -9 7.48 11.81 16 -3 -9 -6.37 10.39 16 -3 -9 8.21 8.62 -16 -3 8 -6.97 7.02 16 3 -8 10.66 11.34 16 -3 -8 -0.70 10.73 16 -3 -8 1.25 8.36 -16 3 7 45.27 8.97 -16 -3 7 56.44 9.00 16 3 -7 64.83 13.37 16 -3 -7 46.50 11.83 16 -3 -7 81.14 10.74 -16 3 6 -10.41 8.36 -16 -3 6 -0.52 8.01 16 -3 -6 -7.48 10.56 16 3 -6 1.61 11.61 -16 3 5 7.85 8.28 -16 -3 5 -2.81 8.18 16 3 -5 0.81 11.22 16 -3 -5 22.30 10.44 -16 3 4 11.96 8.51 -16 -3 4 -5.41 8.49 16 3 -4 5.63 11.34 16 -3 -4 -22.87 11.32 -16 -3 3 3.83 8.87 -16 3 3 9.50 8.94 16 3 -3 4.03 11.62 16 -3 -2 -23.09 14.82 16 3 -2 -7.25 11.37 -16 -3 2 -6.06 9.26 -16 3 2 6.01 9.20 16 -4 -13 -6.31 9.96 16 4 -13 29.00 12.26 16 -4 -13 -8.88 11.09 -16 -4 13 24.40 11.60 16 -4 -12 24.97 10.02 16 -4 -12 24.06 11.53 16 4 -12 5.25 12.15 -16 -4 12 11.95 10.87 16 -4 -11 23.65 9.92 16 -4 -11 46.68 11.58 16 4 -11 34.81 12.50 -16 -4 11 24.10 11.49 16 -4 -10 0.64 8.94 16 4 -10 1.72 11.60 16 -4 -10 16.86 10.94 -16 -4 10 -15.94 10.95 16 -4 -9 1.26 8.35 16 4 -9 -3.40 11.68 16 -4 -9 4.12 9.77 -16 -4 9 -5.18 10.30 -16 -4 9 2.70 6.25 16 -4 -8 10.58 8.28 16 4 -8 0.84 11.24 16 -4 -8 4.72 10.18 -16 -4 8 -7.88 7.51 16 -4 -7 -3.74 8.59 16 4 -7 7.48 11.55 16 -4 -7 -3.31 10.39 -16 -4 7 7.73 7.61 -16 4 6 15.06 8.57 -16 -4 6 43.04 8.80 16 -4 -6 29.58 10.80 16 4 -6 -0.83 11.64 -16 -4 6 20.05 8.55 -16 4 5 -2.24 8.33 -16 -4 5 -3.96 8.39 16 4 -5 19.84 11.90 -16 4 4 22.70 9.14 -16 -4 4 21.74 9.22 16 4 -4 16.50 11.97 -16 4 3 15.81 9.19 -16 -4 3 19.19 9.10 16 4 -3 21.52 12.09 16 -4 -2 38.51 14.81 16 4 -2 31.43 13.04 -16 4 2 35.97 10.13 -16 -4 2 43.27 10.38 -16 -5 13 8.06 10.86 16 5 -13 0.90 11.80 16 -5 -13 -5.78 10.84 16 -5 -13 9.79 10.33 16 5 -13 12.91 10.66 -16 -5 12 33.07 11.95 16 -5 -12 34.10 11.36 16 5 -12 13.38 12.81 16 -5 -12 28.28 10.13 16 5 -12 17.93 10.25 -16 -5 11 -5.38 11.32 16 5 -11 11.55 11.73 16 -5 -11 16.76 10.31 16 -5 -11 19.67 9.97 16 5 -11 24.17 10.11 -16 -5 10 35.19 11.18 16 5 -10 -6.16 12.54 16 -5 -10 17.74 10.68 16 -5 -10 18.57 9.55 16 5 -10 8.51 9.61 -16 -5 9 29.13 10.95 -16 -5 9 9.31 6.76 16 5 -9 4.35 12.03 16 -5 -9 4.66 10.11 16 -5 -9 16.39 9.13 16 5 -9 4.50 9.27 -16 -5 8 1.32 6.98 16 -5 -8 16.80 8.31 16 5 -8 9.49 8.76 16 5 -8 2.58 12.22 16 -5 -8 30.64 10.45 -16 -5 7 12.85 8.85 16 5 -7 47.99 9.67 16 -5 -7 14.33 8.90 16 5 -7 34.89 12.51 16 -5 -7 42.20 10.90 -16 -5 7 16.95 7.66 16 5 -6 15.23 12.06 16 -5 -6 10.71 8.83 -16 5 6 12.44 7.83 -16 -5 6 12.68 8.29 -16 -5 6 20.64 8.77 -16 5 5 10.64 8.35 -16 -5 5 2.27 8.07 16 5 -5 25.42 12.25 -16 -5 5 6.58 8.54 -16 5 4 -3.58 9.28 -16 -5 4 5.44 8.68 16 5 -4 -1.69 12.12 -16 5 3 -8.22 9.00 -16 -5 3 4.50 8.92 16 5 -3 16.12 12.06 16 -5 -2 5.51 14.22 -16 5 2 -0.67 9.24 -16 -5 2 25.13 9.88 16 -6 -12 1.35 9.78 16 6 -12 3.45 9.92 16 -6 -12 4.84 10.49 16 6 -12 -0.91 12.42 -16 -6 12 0.78 10.74 16 -6 -11 17.01 9.81 16 6 -11 26.17 10.33 16 6 -11 3.63 12.67 16 -6 -11 31.18 10.87 -16 -6 11 20.52 11.08 16 -6 -10 17.26 9.33 16 6 -10 36.67 10.11 16 6 -10 34.17 12.92 16 -6 -10 25.10 11.07 -16 -6 10 56.90 11.74 16 -6 -9 18.25 8.82 16 6 -9 28.91 9.58 16 6 -9 35.58 12.76 -16 -6 9 37.31 11.04 -16 -6 9 17.96 7.09 16 -6 -8 -0.62 8.21 16 6 -8 3.80 8.54 16 6 -8 3.52 12.24 -16 -6 8 -1.39 9.91 -16 -6 8 -4.41 7.03 16 6 -7 13.95 12.23 16 -6 -7 -3.73 8.70 16 6 -7 0.63 8.73 -16 -6 7 -3.78 9.10 -16 -6 7 8.79 7.65 16 6 -6 -8.67 12.17 16 -6 -6 -10.06 8.07 -16 -6 6 5.83 8.05 -16 -6 6 8.27 9.03 -16 6 5 82.60 10.35 -16 -6 5 64.40 10.14 16 6 -5 64.23 13.77 -16 -6 5 42.28 10.13 -16 6 4 56.13 10.23 -16 -6 4 60.70 10.31 -16 -6 4 59.04 9.98 16 6 -4 73.80 13.89 16 -6 -3 31.59 14.43 -16 6 3 8.21 8.90 -16 -6 3 -14.14 9.61 16 6 -3 11.29 12.71 16 -6 -2 35.29 15.09 16 6 -2 3.47 12.48 -16 6 2 15.29 10.07 -16 -6 2 17.65 9.91 -16 -7 12 28.57 11.36 16 7 -12 15.77 12.24 16 -7 -12 3.36 9.67 16 7 -12 -6.92 10.43 -16 -7 11 34.59 11.07 16 7 -11 -3.70 12.81 16 -7 -11 10.44 9.42 16 7 -11 14.09 9.79 -16 -7 10 35.04 11.28 16 7 -10 5.51 12.72 16 -7 -10 13.42 9.38 16 7 -10 22.24 9.25 -16 -7 9 36.77 11.20 -16 -7 9 21.20 7.35 16 7 -9 18.62 9.57 16 -7 -9 27.01 9.47 16 7 -9 25.46 13.12 -16 -7 8 24.03 10.21 16 -7 -8 11.80 8.73 16 7 -8 48.66 10.08 16 7 -8 25.24 12.68 -16 -7 8 7.52 9.99 -16 -7 8 20.42 7.56 16 7 -7 101.71 15.27 16 -7 -7 68.23 10.59 16 7 -7 104.65 11.38 -16 -7 7 81.64 11.43 -16 -7 7 57.81 9.48 16 7 -6 2.66 12.65 16 7 -6 7.62 8.61 16 -7 -6 -3.14 8.49 -16 -7 6 -13.80 8.73 -16 -7 6 2.68 9.36 -16 -7 5 -17.12 9.20 16 7 -5 11.55 12.76 -16 -7 5 -6.18 9.37 -16 7 4 1.19 8.68 -16 -7 4 7.32 8.84 -16 -7 4 -2.98 8.75 16 7 -4 -8.89 12.25 16 -7 -3 -7.62 13.80 16 7 -3 -2.67 12.49 -16 7 3 12.62 9.16 -16 -7 3 -3.87 9.02 16 -8 -12 1.34 9.66 16 8 -12 23.50 10.61 16 8 -12 18.91 12.98 -16 -8 12 0.76 10.74 16 8 -11 3.35 9.64 16 -8 -11 -0.65 9.08 16 8 -11 7.55 12.67 -16 -8 11 0.74 10.28 16 -8 -10 7.01 9.24 16 8 -10 21.61 9.88 -16 -8 10 2.16 10.17 16 -8 -9 13.81 8.92 16 8 -9 16.69 9.48 16 8 -9 16.71 13.18 -16 -8 9 20.93 10.58 -16 -8 9 5.94 7.16 16 8 -8 4.61 12.89 16 -8 -8 -8.05 9.54 16 8 -8 -7.59 9.10 -16 -8 8 9.75 10.17 -16 -8 8 -4.92 7.58 -16 -8 8 -6.06 10.08 16 8 -7 7.30 12.66 16 -8 -7 6.19 8.61 16 8 -7 6.92 8.94 -16 -8 7 4.08 9.84 -16 -8 7 -9.87 8.23 16 8 -6 65.38 14.87 16 8 -6 91.89 11.18 -16 -8 6 63.04 10.20 -16 -8 6 79.19 11.63 -16 -8 5 23.52 8.73 -16 -8 5 15.50 9.23 16 8 -5 0.91 12.98 16 -8 -4 18.16 13.69 -16 -8 4 2.45 8.94 -16 -8 4 15.05 8.86 16 8 -4 11.82 13.31 16 -8 -3 -8.69 14.34 -16 -8 3 4.56 8.50 16 8 -3 9.10 12.17 -16 8 3 -7.56 8.99 -16 -8 3 -1.95 9.04 16 -9 -12 11.39 10.01 16 9 -12 1.38 10.07 16 9 -12 14.45 13.15 -16 -9 12 3.79 10.34 16 -9 -11 7.81 9.18 16 9 -11 -4.02 9.89 16 9 -11 -6.72 12.65 -16 -9 11 2.94 9.69 16 -9 -10 30.52 9.60 16 9 -10 47.08 10.41 16 9 -10 52.54 14.47 -16 -9 10 44.22 10.96 16 -9 -9 22.52 8.99 16 9 -9 9.60 9.03 16 9 -9 2.84 12.90 -16 -9 9 11.02 10.42 -16 -9 9 12.41 7.05 16 9 -8 150.62 17.44 16 9 -8 135.63 12.89 16 -9 -8 157.50 12.93 -16 -9 8 120.05 13.69 -16 -9 8 120.64 13.56 16 9 -7 3.73 12.64 16 -9 -7 4.94 8.56 16 9 -7 -3.14 9.17 -16 -9 7 9.04 10.12 -16 -9 7 -1.27 9.63 -16 -9 7 -10.39 8.58 16 9 -6 -12.07 12.90 16 -9 -6 -0.62 8.62 16 9 -6 -6.31 8.63 -16 -9 6 7.50 8.24 -16 -9 6 6.36 9.72 -16 -9 5 12.09 8.43 -16 -9 5 -18.89 9.78 16 9 -5 -12.09 13.04 -16 -9 4 4.30 8.89 -16 -9 4 22.13 9.41 16 9 -4 13.95 12.43 16 -9 -3 4.34 14.17 -16 -9 3 14.25 9.08 16 9 -3 -3.72 12.42 -16 -9 3 -0.65 9.43 -16 -10 11 10.20 10.02 16 10 -11 6.85 12.77 16 -10 -11 5.84 8.81 16 10 -11 12.03 9.76 -16 -10 10 8.47 10.29 16 -10 -10 10.16 9.09 16 10 -10 2.61 9.50 16 10 -10 -3.90 12.86 -16 -10 9 -14.20 10.58 16 -10 -9 22.48 9.10 16 10 -9 20.49 9.42 16 10 -9 2.90 13.52 -16 -10 9 14.53 6.89 -16 -10 9 11.56 9.99 16 10 -8 17.28 13.44 16 -10 -8 18.51 8.85 16 10 -8 8.81 9.20 -16 -10 8 -8.47 10.92 -16 -10 8 9.80 10.45 -16 -10 8 14.03 7.90 16 10 -7 61.94 14.74 16 -10 -7 62.27 10.44 16 10 -7 68.27 10.59 -16 -10 7 52.22 11.20 -16 -10 7 27.36 9.18 -16 -10 7 66.94 10.98 16 10 -6 33.20 13.51 -16 -10 6 45.89 9.05 16 -10 -6 45.33 9.88 16 10 -6 67.94 10.66 -16 -10 6 54.43 11.02 16 -10 -5 24.85 13.93 -16 -10 5 11.60 8.74 -16 -10 5 27.62 10.31 16 10 -5 36.14 13.38 16 -10 -4 -14.84 14.81 -16 -10 4 0.56 9.17 16 10 -4 -10.45 12.66 -16 -10 4 1.86 8.84 16 -11 -11 7.77 9.37 16 11 -11 14.01 10.09 16 11 -11 9.97 13.34 -16 -11 11 0.72 10.49 16 -11 -10 13.30 9.24 16 11 -10 26.72 9.61 16 11 -10 19.84 13.76 -16 -11 10 21.62 10.28 16 11 -9 -2.95 13.01 16 -11 -9 27.42 9.34 16 11 -9 28.11 9.68 -16 -11 9 -2.79 10.60 -16 -11 9 6.91 6.98 -16 -11 9 26.22 10.54 16 11 -8 1.96 13.09 16 -11 -8 14.77 8.81 16 11 -8 8.80 8.78 -16 -11 8 18.11 10.19 -16 -11 8 12.90 9.91 -16 -11 8 6.40 7.27 16 11 -7 -12.64 13.42 -16 -11 7 1.00 7.92 -16 -11 7 -12.92 9.82 16 -11 -7 17.79 9.13 16 11 -7 3.74 8.75 -16 -11 7 3.84 10.31 16 11 -6 -24.21 13.60 16 -11 -6 20.03 13.37 -16 -11 6 -4.90 7.97 16 11 -6 -6.27 9.24 16 -11 -6 11.14 8.45 -16 -11 6 7.40 10.03 16 -11 -5 9.26 13.42 -16 -11 5 -13.38 9.35 -16 -11 5 8.33 9.56 16 11 -5 10.68 13.06 16 -11 -4 23.19 14.13 -16 -11 4 20.27 9.60 16 11 -4 -12.62 13.71 -16 -11 4 8.03 8.81 16 -12 -10 -6.95 9.28 16 12 -10 7.15 9.81 16 12 -10 -4.04 13.52 -16 -12 10 1.38 9.65 16 12 -9 17.07 13.43 16 -12 -9 2.48 8.71 16 12 -9 7.01 9.18 -16 -12 9 11.46 10.73 -16 -12 9 -0.41 6.79 -16 -12 9 -3.99 9.86 16 12 -8 -5.99 13.03 -16 -12 8 3.22 7.17 -16 -12 8 15.90 9.83 16 -12 -8 4.92 8.33 16 12 -8 5.01 8.72 -16 -12 8 -5.51 10.30 16 12 -7 7.93 13.21 16 -12 -7 20.21 12.33 -16 -12 7 -12.72 9.98 -16 -12 7 -1.51 7.71 16 12 -7 30.51 9.28 16 -12 -7 17.71 8.74 -16 -12 7 16.43 10.45 16 12 -6 -9.89 13.50 16 -12 -6 -8.94 13.03 -16 -12 6 3.81 7.81 16 -12 -6 2.46 8.12 16 12 -6 1.87 8.54 -16 -12 6 12.70 10.10 16 -12 -5 5.11 13.75 -16 -12 5 37.63 10.41 16 12 -5 29.74 14.10 -16 -12 5 33.16 8.88 16 13 -9 15.34 13.26 16 -13 -9 17.97 9.12 16 13 -9 -3.81 9.17 -16 -13 9 22.75 10.96 -16 -13 9 1.97 9.69 16 13 -8 -4.07 13.77 -16 -13 8 8.38 7.48 -16 -13 8 24.50 9.81 16 -13 -8 4.90 8.33 16 13 -8 6.88 8.85 -16 -13 8 -11.28 10.81 16 13 -7 53.55 14.74 16 -13 -7 -6.66 13.00 -16 -13 7 14.32 9.66 -16 -13 7 11.14 8.44 16 -13 -7 41.40 9.32 16 13 -7 38.96 9.54 -16 -13 7 36.62 11.40 16 13 -6 -1.01 13.51 16 -13 -6 11.81 12.47 -16 -13 6 3.83 7.90 16 13 -6 -3.10 8.49 16 -13 -6 -3.06 8.35 -16 -13 6 7.83 10.29 16 14 -8 8.29 13.88 16 -14 -8 -3.62 11.71 -16 -14 8 -10.72 7.89 -16 -14 8 3.72 9.15 16 14 -8 -4.36 9.21 16 -14 -8 23.81 9.05 -16 -14 8 -15.13 11.49 16 14 -7 -7.20 14.00 -16 -14 7 12.36 9.95 -16 -14 7 14.27 8.38 16 -14 -7 -0.94 12.18 16 -14 -7 14.57 8.74 16 14 -7 -4.92 9.04 -16 -14 7 16.67 11.35 0 0 0 0.00 0.00 TITL lk43db in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 0.71073 11.192460 28.255398 12.976269 90.0000 113.5512 90.0000 ZERR 1.00 0.000252 0.000395 0.000318 0.0000 0.0028 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Fe UNIT 168.00 192.00 12.00 12.00 4.00 REM CrysAlisPro recorded range (K): Min=99.7; max=100.2; aver:100.0 TEMP -173 SIZE 0.05 0.19 0.23 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 47055 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.36174(3) 0.36542(2) 0.31199(2) 0.01937(7) Uani 1 1 d . . . . . O1 O 0.61798(15) 0.40762(5) 0.53132(13) 0.0263(3) Uani 1 1 d . . . . . O2 O 0.31054(17) 0.33820(6) 0.08044(13) 0.0332(3) Uani 1 1 d . . . . . O3 O 0.08047(16) 0.37964(6) 0.24091(16) 0.0360(4) Uani 1 1 d . . . . . N1 N 0.67269(16) 0.35096(6) 0.35669(15) 0.0224(3) Uani 1 1 d . . . . . N2 N 0.49123(15) 0.26603(5) 0.30117(14) 0.0191(3) Uani 1 1 d . . . . . N3 N 0.40178(18) 0.43241(6) 0.31179(16) 0.0258(3) Uani 1 1 d . . . . . C1 C 0.55416(19) 0.37271(6) 0.48110(16) 0.0207(3) Uani 1 1 d . . . . . C2 C 0.57198(18) 0.34457(6) 0.39162(16) 0.0196(3) Uani 1 1 d . . . . . C3 C 0.48652(17) 0.30379(6) 0.36769(15) 0.0174(3) Uani 1 1 d . . . . . C4 C 0.40019(18) 0.31027(6) 0.42457(16) 0.0184(3) Uani 1 1 d . . . . . C5 C 0.43449(19) 0.35432(6) 0.48629(17) 0.0202(3) Uani 1 1 d . . . . . C6 C 0.6473(2) 0.34679(7) 0.23762(18) 0.0258(4) Uani 1 1 d . . . . . H6A H 0.571297 0.325814 0.200349 0.031 Uiso 1 1 calc R U . . . H6B H 0.723644 0.332186 0.229789 0.031 Uiso 1 1 calc R U . . . C7 C 0.6201(2) 0.39534(8) 0.1793(2) 0.0309(5) Uani 1 1 d . . . . . H7A H 0.607872 0.391626 0.099893 0.037 Uiso 1 1 calc R U . . . H7B H 0.538836 0.408693 0.180513 0.037 Uiso 1 1 calc R U . . . C8 C 0.7336(3) 0.42922(9) 0.2392(2) 0.0380(5) Uani 1 1 d . . . . . H8A H 0.812371 0.417883 0.229767 0.046 Uiso 1 1 calc R U . . . H8B H 0.711825 0.461066 0.204930 0.046 Uiso 1 1 calc R U . . . C9 C 0.7615(2) 0.43226(8) 0.3639(2) 0.0331(5) Uani 1 1 d . . . . . H9A H 0.687617 0.447967 0.373568 0.040 Uiso 1 1 calc R U . . . H9B H 0.840590 0.451619 0.402666 0.040 Uiso 1 1 calc R U . . . C10 C 0.7817(2) 0.38302(7) 0.4164(2) 0.0264(4) Uani 1 1 d . . . . . H10A H 0.862931 0.369305 0.416112 0.032 Uiso 1 1 calc R U . . . H10B H 0.792304 0.385799 0.495688 0.032 Uiso 1 1 calc R U . . . C11 C 0.37803(18) 0.23481(7) 0.25168(17) 0.0215(4) Uani 1 1 d . . . . . H11A H 0.296935 0.253243 0.233623 0.026 Uiso 1 1 calc R U . . . H11B H 0.381284 0.209836 0.306242 0.026 Uiso 1 1 calc R U . . . C12 C 0.3779(2) 0.21219(7) 0.14488(18) 0.0255(4) Uani 1 1 d . . . . . H12A H 0.367143 0.237077 0.088137 0.031 Uiso 1 1 calc R U . . . H12B H 0.303493 0.190054 0.113478 0.031 Uiso 1 1 calc R U . . . C13 C 0.5049(2) 0.18547(7) 0.1695(2) 0.0280(4) Uani 1 1 d . . . . . H13A H 0.505809 0.173084 0.098491 0.034 Uiso 1 1 calc R U . . . H13B H 0.510809 0.158248 0.219372 0.034 Uiso 1 1 calc R U . . . C14 C 0.6221(2) 0.21812(7) 0.22612(19) 0.0261(4) Uani 1 1 d . . . . . H14A H 0.703525 0.199542 0.248050 0.031 Uiso 1 1 calc R U . . . H14B H 0.622806 0.242770 0.172162 0.031 Uiso 1 1 calc R U . . . C15 C 0.61696(19) 0.24158(7) 0.32978(18) 0.0230(4) Uani 1 1 d . . . . . H15A H 0.628290 0.217326 0.388003 0.028 Uiso 1 1 calc R U . . . H15B H 0.689107 0.264673 0.360841 0.028 Uiso 1 1 calc R U . . . C16 C 0.31912(18) 0.27322(6) 0.44818(16) 0.0189(3) Uani 1 1 d . . . . . C17 C 0.37947(19) 0.23398(7) 0.51566(17) 0.0216(4) Uani 1 1 d . . . . . C18 C 0.3013(2) 0.20168(7) 0.54186(17) 0.0249(4) Uani 1 1 d . . . . . H18 H 0.340831 0.175179 0.587919 0.030 Uiso 1 1 calc R U . . . C19 C 0.1671(2) 0.20739(8) 0.50215(18) 0.0257(4) Uani 1 1 d . . . . . H19 H 0.116457 0.184724 0.521049 0.031 Uiso 1 1 calc R U . . . C20 C 0.10591(19) 0.24591(7) 0.43506(17) 0.0233(4) Uani 1 1 d . . . . . C21 C 0.18409(19) 0.27852(7) 0.41049(17) 0.0211(3) Uani 1 1 d . . . . . H21 H 0.144074 0.305444 0.366355 0.025 Uiso 1 1 calc R U . . . C22 C 0.5241(2) 0.22454(8) 0.56099(19) 0.0277(4) Uani 1 1 d . . . . . H22A H 0.540574 0.196875 0.523025 0.042 Uiso 1 1 calc R U . . . H22B H 0.556901 0.218431 0.641966 0.042 Uiso 1 1 calc R U . . . H22C H 0.568692 0.252175 0.547420 0.042 Uiso 1 1 calc R U . . . C23 C -0.0397(2) 0.25169(9) 0.3882(2) 0.0333(5) Uani 1 1 d . . . . . H23A H -0.075898 0.246222 0.306863 0.050 Uiso 1 1 calc R U . . . H23B H -0.061231 0.283849 0.403365 0.050 Uiso 1 1 calc R U . . . H23C H -0.076870 0.228763 0.423847 0.050 Uiso 1 1 calc R U . . . C24 C 0.3887(2) 0.37005(7) 0.57419(18) 0.0231(4) Uani 1 1 d . . . . . C25 C 0.4669(2) 0.36099(7) 0.68763(19) 0.0271(4) Uani 1 1 d . . . . . C26 C 0.4225(3) 0.37620(8) 0.7685(2) 0.0328(5) Uani 1 1 d . . . . . H26 H 0.473865 0.369751 0.845512 0.039 Uiso 1 1 calc R U . . . C27 C 0.3062(2) 0.40034(8) 0.7402(2) 0.0330(5) Uani 1 1 d . . . . . H27 H 0.278862 0.410131 0.797459 0.040 Uiso 1 1 calc R U . . . C28 C 0.2295(2) 0.41027(8) 0.6288(2) 0.0308(5) Uani 1 1 d . . . . . C29 C 0.2723(2) 0.39480(7) 0.5470(2) 0.0262(4) Uani 1 1 d . . . . . H29 H 0.220320 0.401391 0.470244 0.031 Uiso 1 1 calc R U . . . C30 C 0.5953(3) 0.33571(10) 0.7234(2) 0.0375(5) Uani 1 1 d . . . . . H30A H 0.580186 0.302558 0.699490 0.056 Uiso 1 1 calc R U . . . H30B H 0.640870 0.337183 0.805391 0.056 Uiso 1 1 calc R U . . . H30C H 0.648689 0.350911 0.688596 0.056 Uiso 1 1 calc R U . . . C31 C 0.1040(2) 0.43744(9) 0.5964(3) 0.0392(6) Uani 1 1 d . . . . . H31A H 0.034124 0.415804 0.592955 0.059 Uiso 1 1 calc R U . . . H31B H 0.081820 0.452101 0.522553 0.059 Uiso 1 1 calc R U . . . H31C H 0.114524 0.462094 0.652431 0.059 Uiso 1 1 calc R U . . . C32 C 0.3316(2) 0.35030(7) 0.17029(18) 0.0242(4) Uani 1 1 d . . . . . C33 C 0.1913(2) 0.37370(7) 0.27295(19) 0.0260(4) Uani 1 1 d . . . . . C34 C 0.4317(3) 0.47106(8) 0.3184(2) 0.0358(5) Uani 1 1 d . . . . . C35 C 0.4702(4) 0.52067(10) 0.3246(4) 0.0797(14) Uani 1 1 d . . . . . H35A H 0.432975 0.534607 0.249135 0.120 Uiso 1 1 calc R U . . . H35B H 0.565421 0.522900 0.354721 0.120 Uiso 1 1 calc R U . . . H35C H 0.437898 0.537838 0.373897 0.120 Uiso 1 1 calc R U . . . C36A C 0.0901(6) 0.4750(2) 0.9223(5) 0.0434(17) Uani 0.404(3) 1 d G U P A 1 C37A C 0.0528(8) 0.4287(2) 0.9303(6) 0.057(2) Uani 0.404(3) 1 d G U P A 1 H37C H 0.103115 0.409832 0.993252 0.069 Uiso 0.404(3) 1 calc R U P A 1 C38A C -0.0583(8) 0.4101(2) 0.8460(8) 0.083(3) Uani 0.404(3) 1 d G U P A 1 H38C H -0.083836 0.378400 0.851470 0.100 Uiso 0.404(3) 1 calc R U P A 1 C39A C -0.1320(6) 0.4377(3) 0.7539(7) 0.072(3) Uani 0.404(3) 1 d G U P A 1 H39C H -0.207890 0.424928 0.696321 0.086 Uiso 0.404(3) 1 calc R U P A 1 C40A C -0.0946(7) 0.4840(3) 0.7459(5) 0.069(3) Uani 0.404(3) 1 d G U P A 1 H40C H -0.144993 0.502888 0.682952 0.082 Uiso 0.404(3) 1 calc R U P A 1 C41A C 0.0164(7) 0.5027(2) 0.8302(6) 0.0482(18) Uani 0.404(3) 1 d G U P A 1 H41D H 0.041959 0.534321 0.824733 0.058 Uiso 0.404(3) 1 calc R U P A 1 C42A C 0.2068(9) 0.4934(5) 1.0139(8) 0.081(3) Uani 0.404(3) 1 d . U P A 1 H42A H 0.206259 0.483740 1.086274 0.121 Uiso 0.404(3) 1 calc R U P A 1 H42B H 0.207475 0.528039 1.009853 0.121 Uiso 0.404(3) 1 calc R U P A 1 H42C H 0.284762 0.480749 1.006961 0.121 Uiso 0.404(3) 1 calc R U P A 1 C42B C -0.1404(14) 0.4953(4) 0.6594(12) 0.067(3) Uani 0.301(3) 1 d . U P B 2 H42D H -0.210961 0.478057 0.600619 0.100 Uiso 0.301(3) 1 calc R U P B 2 H42E H -0.072525 0.503111 0.632456 0.100 Uiso 0.301(3) 1 calc R U P B 2 H42F H -0.174994 0.524502 0.677612 0.100 Uiso 0.301(3) 1 calc R U P B 2 C36B C -0.0865(10) 0.4666(3) 0.7571(7) 0.046(2) Uani 0.301(3) 1 d G U P B 2 C41B C -0.1424(8) 0.4264(3) 0.7812(7) 0.050(3) Uani 0.301(3) 1 d G U P B 2 H41E H -0.222733 0.414673 0.727603 0.061 Uiso 0.301(3) 1 calc R U P B 2 C40B C -0.0809(9) 0.4035(3) 0.8838(7) 0.048(2) Uani 0.301(3) 1 d G U P B 2 H40D H -0.119165 0.376107 0.900264 0.057 Uiso 0.301(3) 1 calc R U P B 2 C39B C 0.0366(9) 0.4207(4) 0.9622(6) 0.060(3) Uani 0.301(3) 1 d G U P B 2 H39D H 0.078604 0.405087 1.032326 0.073 Uiso 0.301(3) 1 calc R U P B 2 C38B C 0.0925(9) 0.4609(4) 0.9381(9) 0.081(5) Uani 0.301(3) 1 d G U P B 2 H38D H 0.172806 0.472632 0.991729 0.097 Uiso 0.301(3) 1 calc R U P B 2 C37B C 0.0310(11) 0.4838(3) 0.8355(10) 0.071(4) Uani 0.301(3) 1 d G U P B 2 H37D H 0.069240 0.511199 0.819067 0.085 Uiso 0.301(3) 1 calc R U P B 2 C41C C 0.445(2) 0.5031(7) 1.0355(19) 0.138(7) Uani 0.295(3) 1 d D U P C -3 H41A H 0.506516 0.501747 1.114439 0.207 Uiso 0.295(3) 1 calc R U P C -3 H41B H 0.472487 0.527763 0.996520 0.207 Uiso 0.295(3) 1 calc R U P C -3 H41C H 0.443609 0.472431 0.999695 0.207 Uiso 0.295(3) 1 calc R U P C -3 C40C C 0.308(2) 0.5146(9) 1.029(3) 0.171(9) Uani 0.295(3) 1 d D U P C -3 H40A H 0.310420 0.528394 1.099988 0.205 Uiso 0.295(3) 1 calc R U P C -3 H40B H 0.259491 0.535876 0.965458 0.205 Uiso 0.295(3) 1 calc R U P C -3 C39C C 0.253(3) 0.4652(10) 1.010(3) 0.184(10) Uani 0.295(3) 1 d D U P C -3 H39A H 0.281577 0.450202 0.954790 0.221 Uiso 0.295(3) 1 calc R U P C -3 H39B H 0.297108 0.447906 1.081757 0.221 Uiso 0.295(3) 1 calc R U P C -3 C36C C -0.115(3) 0.4261(14) 0.918(3) 0.215(14) Uani 0.295(3) 1 d D U P C -3 H36A H -0.181700 0.405489 0.865649 0.322 Uiso 0.295(3) 1 calc R U P C -3 H36B H -0.150250 0.458074 0.914967 0.322 Uiso 0.295(3) 1 calc R U P C -3 H36C H -0.087394 0.413643 0.994765 0.322 Uiso 0.295(3) 1 calc R U P C -3 C38C C 0.113(3) 0.4556(15) 0.972(4) 0.230(12) Uani 0.295(3) 1 d D U P C -3 H38A H 0.077022 0.488024 0.960254 0.275 Uiso 0.295(3) 1 calc R U P C -3 H38B H 0.108025 0.445003 1.043017 0.275 Uiso 0.295(3) 1 calc R U P C -3 C37C C 0.004(3) 0.4281(15) 0.886(3) 0.212(12) Uani 0.295(3) 1 d D U P C -3 H37A H 0.033205 0.395502 0.880845 0.255 Uiso 0.295(3) 1 calc R U P C -3 H37B H -0.022203 0.443269 0.811583 0.255 Uiso 0.295(3) 1 calc R U P C -3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.02067(13) 0.01389(11) 0.02259(13) -0.00008(10) 0.00765(10) 0.00007(10) O1 0.0305(8) 0.0200(6) 0.0284(7) -0.0062(5) 0.0118(6) -0.0078(5) O2 0.0363(9) 0.0337(8) 0.0254(8) -0.0027(6) 0.0080(7) 0.0008(7) O3 0.0240(8) 0.0345(8) 0.0442(10) 0.0049(7) 0.0079(7) 0.0060(6) N1 0.0219(8) 0.0198(7) 0.0268(8) -0.0017(6) 0.0110(7) -0.0053(6) N2 0.0163(7) 0.0151(6) 0.0248(8) -0.0033(6) 0.0071(6) -0.0023(5) N3 0.0298(9) 0.0184(7) 0.0312(9) 0.0004(6) 0.0143(8) 0.0018(6) C1 0.0226(9) 0.0169(8) 0.0220(9) -0.0007(6) 0.0083(7) -0.0023(6) C2 0.0203(8) 0.0158(8) 0.0223(9) 0.0000(6) 0.0082(7) -0.0025(6) C3 0.0156(8) 0.0147(7) 0.0195(8) 0.0000(6) 0.0045(6) -0.0013(6) C4 0.0172(8) 0.0151(7) 0.0204(8) 0.0002(6) 0.0050(7) -0.0010(6) C5 0.0217(9) 0.0150(7) 0.0235(9) -0.0013(6) 0.0086(7) -0.0010(6) C6 0.0305(10) 0.0221(9) 0.0294(10) -0.0009(8) 0.0168(9) -0.0035(7) C7 0.0383(12) 0.0264(10) 0.0307(11) 0.0033(8) 0.0167(10) -0.0033(8) C8 0.0432(14) 0.0273(11) 0.0480(15) 0.0075(10) 0.0228(12) -0.0084(10) C9 0.0327(11) 0.0200(9) 0.0458(14) 0.0005(9) 0.0148(10) -0.0088(8) C10 0.0225(9) 0.0204(9) 0.0359(11) -0.0013(8) 0.0113(8) -0.0064(7) C11 0.0180(8) 0.0190(8) 0.0261(9) -0.0040(7) 0.0073(7) -0.0033(6) C12 0.0235(9) 0.0231(9) 0.0285(10) -0.0077(7) 0.0087(8) -0.0029(7) C13 0.0265(10) 0.0199(9) 0.0364(11) -0.0083(8) 0.0112(9) 0.0002(7) C14 0.0222(9) 0.0220(9) 0.0345(11) -0.0051(8) 0.0117(8) 0.0009(7) C15 0.0192(9) 0.0175(8) 0.0309(10) -0.0008(7) 0.0085(8) 0.0008(6) C16 0.0185(8) 0.0171(8) 0.0214(8) -0.0018(6) 0.0083(7) -0.0027(6) C17 0.0212(9) 0.0206(8) 0.0224(9) 0.0005(7) 0.0081(7) -0.0017(7) C18 0.0282(10) 0.0232(9) 0.0227(9) 0.0026(7) 0.0097(8) -0.0025(7) C19 0.0258(10) 0.0278(10) 0.0263(10) -0.0012(8) 0.0134(8) -0.0074(8) C20 0.0196(9) 0.0267(9) 0.0252(9) -0.0045(7) 0.0106(8) -0.0038(7) C21 0.0200(8) 0.0205(8) 0.0229(9) -0.0023(7) 0.0088(7) -0.0007(6) C22 0.0209(9) 0.0256(9) 0.0328(11) 0.0089(8) 0.0068(8) 0.0020(7) C23 0.0221(10) 0.0385(12) 0.0413(13) -0.0018(10) 0.0148(9) -0.0039(9) C24 0.0263(9) 0.0176(8) 0.0284(10) -0.0032(7) 0.0142(8) -0.0038(7) C25 0.0328(11) 0.0228(9) 0.0292(10) 0.0008(8) 0.0160(9) -0.0002(8) C26 0.0432(13) 0.0306(11) 0.0294(11) -0.0007(9) 0.0197(10) -0.0004(9) C27 0.0425(13) 0.0269(10) 0.0408(13) -0.0078(9) 0.0284(11) -0.0057(9) C28 0.0295(11) 0.0229(9) 0.0460(13) -0.0107(9) 0.0214(10) -0.0076(8) C29 0.0233(9) 0.0228(9) 0.0334(11) -0.0074(8) 0.0121(8) -0.0048(7) C30 0.0428(14) 0.0431(13) 0.0274(11) 0.0048(10) 0.0148(10) 0.0128(11) C31 0.0334(12) 0.0330(12) 0.0590(17) -0.0111(11) 0.0267(12) -0.0021(9) C32 0.0256(9) 0.0183(8) 0.0267(10) 0.0024(7) 0.0085(8) 0.0022(7) C33 0.0281(10) 0.0192(9) 0.0297(10) 0.0018(7) 0.0105(8) 0.0016(7) C34 0.0424(13) 0.0206(9) 0.0563(16) -0.0066(9) 0.0324(12) -0.0027(9) C35 0.095(3) 0.0211(12) 0.168(4) -0.0260(18) 0.100(3) -0.0189(14) C36A 0.043(4) 0.054(4) 0.035(3) 0.000(3) 0.018(3) 0.007(3) C37A 0.059(5) 0.058(4) 0.059(5) 0.022(4) 0.028(4) 0.016(3) C38A 0.084(6) 0.059(5) 0.112(7) -0.030(5) 0.045(5) -0.002(4) C39A 0.045(4) 0.103(6) 0.067(5) -0.049(5) 0.023(4) -0.011(4) C40A 0.053(4) 0.104(6) 0.057(5) 0.008(5) 0.031(3) 0.038(4) C41A 0.056(4) 0.048(4) 0.061(4) 0.012(3) 0.044(3) 0.017(3) C42A 0.047(4) 0.146(10) 0.054(5) -0.040(6) 0.023(4) -0.028(5) C42B 0.084(8) 0.055(6) 0.085(7) 0.020(5) 0.059(6) 0.027(6) C36B 0.060(5) 0.032(4) 0.066(5) 0.002(3) 0.047(4) 0.015(4) C41B 0.061(6) 0.033(4) 0.044(5) 0.005(4) 0.007(4) 0.002(4) C40B 0.054(5) 0.036(4) 0.049(5) 0.001(3) 0.015(4) 0.016(4) C39B 0.055(6) 0.079(7) 0.038(5) -0.001(5) 0.009(4) 0.007(5) C38B 0.069(7) 0.095(8) 0.082(7) -0.016(6) 0.033(5) -0.014(6) C37B 0.078(6) 0.073(7) 0.079(6) -0.005(5) 0.049(5) -0.010(6) C41C 0.152(11) 0.091(11) 0.115(13) 0.020(10) -0.007(10) 0.027(10) C40C 0.176(11) 0.189(11) 0.149(12) 0.012(9) 0.066(9) -0.012(8) C39C 0.196(11) 0.172(12) 0.177(14) -0.008(9) 0.067(9) 0.005(8) C36C 0.213(16) 0.22(2) 0.21(2) -0.014(17) 0.082(15) -0.041(15) C38C 0.217(12) 0.233(15) 0.241(15) -0.002(10) 0.095(9) -0.014(9) C37C 0.220(13) 0.208(15) 0.213(15) -0.011(10) 0.092(9) -0.006(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -15 6 5 0.0800 -8 34 8 0.0627 15 -6 -5 0.0889 13 -23 -7 0.0992 13 0 -16 0.0309 -12 -4 16 0.0190 11 7 -17 0.0358 -14 11 12 0.0460 -12 -2 16 0.0202 8 -11 -17 0.0519 -3 5 -15 0.1108 12 -17 -14 0.0593 7 -11 11 0.1087 -2 2 18 0.0912 -7 9 18 0.0655 -11 16 15 0.0369 5 34 5 0.1206 3 -37 -7 0.0834 -7 -31 -4 0.0608 -10 -31 6 0.0451 -15 -11 8 0.0443 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C33 Fe1 C32 89.91(10) . . ? C33 Fe1 N3 95.32(8) . . ? C32 Fe1 N3 100.39(9) . . ? C33 Fe1 C4 101.39(8) . . ? C32 Fe1 C4 116.73(8) . . ? N3 Fe1 C4 138.92(8) . . ? C33 Fe1 C5 103.67(9) . . ? C32 Fe1 C5 155.13(8) . . ? N3 Fe1 C5 99.00(7) . . ? C4 Fe1 C5 40.69(7) . . ? C33 Fe1 C3 132.38(8) . . ? C32 Fe1 C3 89.00(8) . . ? N3 Fe1 C3 131.60(7) . . ? C4 Fe1 C3 39.81(7) . . ? C5 Fe1 C3 66.41(7) . . ? C33 Fe1 C2 166.93(8) . . ? C32 Fe1 C2 98.26(8) . . ? N3 Fe1 C2 93.23(7) . . ? C4 Fe1 C2 65.82(7) . . ? C5 Fe1 C2 65.14(7) . . ? C3 Fe1 C2 38.38(6) . . ? C33 Fe1 C1 135.94(9) . . ? C32 Fe1 C1 134.14(8) . . ? N3 Fe1 C1 78.10(7) . . ? C4 Fe1 C1 63.78(7) . . ? C5 Fe1 C1 37.32(7) . . ? C3 Fe1 C1 62.56(7) . . ? C2 Fe1 C1 37.23(7) . . ? C2 N1 C6 119.76(17) . . ? C2 N1 C10 121.41(17) . . ? C6 N1 C10 112.22(16) . . ? C3 N2 C11 119.67(15) . . ? C3 N2 C15 118.25(15) . . ? C11 N2 C15 113.52(15) . . ? C34 N3 Fe1 175.4(2) . . ? O1 C1 C5 127.18(18) . . ? O1 C1 C2 127.46(18) . . ? C5 C1 C2 104.91(15) . . ? O1 C1 Fe1 132.04(14) . . ? C5 C1 Fe1 60.41(10) . . ? C2 C1 Fe1 65.76(10) . . ? N1 C2 C3 125.97(17) . . ? N1 C2 C1 124.57(16) . . ? C3 C2 C1 108.05(16) . . ? N1 C2 Fe1 131.14(14) . . ? C3 C2 Fe1 68.17(10) . . ? C1 C2 Fe1 77.01(11) . . ? N2 C3 C4 128.02(16) . . ? N2 C3 C2 123.98(16) . . ? C4 C3 C2 108.00(15) . . ? N2 C3 Fe1 126.17(13) . . ? C4 C3 Fe1 66.09(10) . . ? C2 C3 Fe1 73.45(10) . . ? C3 C4 C5 107.98(15) . . ? C3 C4 C16 126.96(16) . . ? C5 C4 C16 122.52(17) . . ? C3 C4 Fe1 74.10(10) . . ? C5 C4 Fe1 71.09(11) . . ? C16 C4 Fe1 134.66(13) . . ? C4 C5 C1 108.99(16) . . ? C4 C5 C24 125.66(17) . . ? C1 C5 C24 121.98(17) . . ? C4 C5 Fe1 68.22(11) . . ? C1 C5 Fe1 82.27(12) . . ? C24 C5 Fe1 132.46(14) . . ? N1 C6 C7 111.42(17) . . ? C8 C7 C6 110.3(2) . . ? C9 C8 C7 110.49(19) . . ? C8 C9 C10 110.76(19) . . ? N1 C10 C9 112.53(18) . . ? N2 C11 C12 109.71(16) . . ? C11 C12 C13 110.74(18) . . ? C12 C13 C14 110.51(16) . . ? C15 C14 C13 111.06(17) . . ? N2 C15 C14 110.53(17) . . ? C21 C16 C17 119.02(17) . . ? C21 C16 C4 120.87(17) . . ? C17 C16 C4 119.97(16) . . ? C18 C17 C16 118.33(18) . . ? C18 C17 C22 117.93(18) . . ? C16 C17 C22 123.74(17) . . ? C19 C18 C17 121.57(19) . . ? C18 C19 C20 120.80(18) . . ? C19 C20 C21 117.63(18) . . ? C19 C20 C23 121.40(19) . . ? C21 C20 C23 120.95(19) . . ? C20 C21 C16 122.64(18) . . ? C29 C24 C25 119.00(19) . . ? C29 C24 C5 121.84(19) . . ? C25 C24 C5 119.12(18) . . ? C26 C25 C24 118.2(2) . . ? C26 C25 C30 119.9(2) . . ? C24 C25 C30 121.95(19) . . ? C27 C26 C25 122.1(2) . . ? C26 C27 C28 120.2(2) . . ? C27 C28 C29 118.2(2) . . ? C27 C28 C31 121.0(2) . . ? C29 C28 C31 120.8(2) . . ? C24 C29 C28 122.3(2) . . ? O2 C32 Fe1 176.32(19) . . ? O3 C33 Fe1 175.7(2) . . ? N3 C34 C35 178.8(3) . . ? C37A C36A C41A 120.0 . . ? C37A C36A C42A 118.1(7) . . ? C41A C36A C42A 121.9(7) . . ? C36A C37A C38A 120.0 . . ? C37A C38A C39A 120.0 . . ? C40A C39A C38A 120.0 . . ? C39A C40A C41A 120.0 . . ? C40A C41A C36A 120.0 . . ? C41B C36B C37B 120.0 . . ? C41B C36B C42B 126.7(9) . . ? C37B C36B C42B 113.2(9) . . ? C36B C41B C40B 120.0 . . ? C41B C40B C39B 120.0 . . ? C38B C39B C40B 120.0 . . ? C39B C38B C37B 120.0 . . ? C38B C37B C36B 120.0 . . ? C39C C40C C41C 98.4(18) . . ? C38C C39C C40C 123(3) . . ? C39C C38C C37C 142(3) . . ? C38C C37C C36C 111(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 C33 1.782(2) . ? Fe1 C32 1.784(2) . ? Fe1 N3 1.9456(17) . ? Fe1 C4 2.0602(18) . ? Fe1 C5 2.099(2) . ? Fe1 C3 2.1675(18) . ? Fe1 C2 2.2381(19) . ? Fe1 C1 2.392(2) . ? O1 C1 1.239(2) . ? O2 C32 1.146(3) . ? O3 C33 1.153(3) . ? N1 C2 1.385(2) . ? N1 C6 1.460(3) . ? N1 C10 1.468(3) . ? N2 C3 1.387(2) . ? N2 C11 1.465(2) . ? N2 C15 1.476(2) . ? N3 C34 1.136(3) . ? C1 C5 1.463(3) . ? C1 C2 1.485(3) . ? C2 C3 1.450(2) . ? C3 C4 1.443(3) . ? C4 C5 1.446(3) . ? C4 C16 1.495(3) . ? C5 C24 1.493(3) . ? C6 C7 1.537(3) . ? C7 C8 1.532(3) . ? C8 C9 1.523(4) . ? C9 C10 1.526(3) . ? C11 C12 1.526(3) . ? C12 C13 1.526(3) . ? C13 C14 1.530(3) . ? C14 C15 1.521(3) . ? C16 C21 1.398(3) . ? C16 C17 1.407(3) . ? C17 C18 1.397(3) . ? C17 C22 1.509(3) . ? C18 C19 1.389(3) . ? C19 C20 1.391(3) . ? C20 C21 1.393(3) . ? C20 C23 1.503(3) . ? C24 C29 1.394(3) . ? C24 C25 1.403(3) . ? C25 C26 1.397(3) . ? C25 C30 1.503(3) . ? C26 C27 1.383(4) . ? C27 C28 1.384(4) . ? C28 C29 1.398(3) . ? C28 C31 1.505(3) . ? C34 C35 1.459(3) . ? C36A C37A 1.3900 . ? C36A C41A 1.3900 . ? C36A C42A 1.466(10) . ? C37A C38A 1.3900 . ? C38A C39A 1.3900 . ? C39A C40A 1.3900 . ? C40A C41A 1.3900 . ? C42B C36B 1.421(14) . ? C36B C41B 1.3900 . ? C36B C37B 1.3900 . ? C41B C40B 1.3900 . ? C40B C39B 1.3900 . ? C39B C38B 1.3900 . ? C38B C37B 1.3900 . ? C41C C40C 1.538(18) . ? C40C C39C 1.504(18) . ? C39C C38C 1.464(18) . ? C36C C37C 1.540(19) . ? C38C C37C 1.506(18) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C6 N1 C2 C3 53.8(3) . . . . ? C10 N1 C2 C3 -156.96(19) . . . . ? C6 N1 C2 C1 -141.43(19) . . . . ? C10 N1 C2 C1 7.8(3) . . . . ? C6 N1 C2 Fe1 -37.6(3) . . . . ? C10 N1 C2 Fe1 111.7(2) . . . . ? O1 C1 C2 N1 5.9(3) . . . . ? C5 C1 C2 N1 178.52(18) . . . . ? Fe1 C1 C2 N1 131.37(19) . . . . ? O1 C1 C2 C3 172.99(19) . . . . ? C5 C1 C2 C3 -14.4(2) . . . . ? Fe1 C1 C2 C3 -61.54(12) . . . . ? O1 C1 C2 Fe1 -125.5(2) . . . . ? C5 C1 C2 Fe1 47.15(13) . . . . ? C11 N2 C3 C4 20.1(3) . . . . ? C15 N2 C3 C4 -125.7(2) . . . . ? C11 N2 C3 C2 -159.99(18) . . . . ? C15 N2 C3 C2 54.2(3) . . . . ? C11 N2 C3 Fe1 -66.1(2) . . . . ? C15 N2 C3 Fe1 148.02(14) . . . . ? N1 C2 C3 N2 -3.0(3) . . . . ? C1 C2 C3 N2 -169.83(17) . . . . ? Fe1 C2 C3 N2 122.83(18) . . . . ? N1 C2 C3 C4 176.96(18) . . . . ? C1 C2 C3 C4 10.1(2) . . . . ? Fe1 C2 C3 C4 -57.24(12) . . . . ? N1 C2 C3 Fe1 -125.8(2) . . . . ? C1 C2 C3 Fe1 67.34(13) . . . . ? N2 C3 C4 C5 178.31(18) . . . . ? C2 C3 C4 C5 -1.6(2) . . . . ? Fe1 C3 C4 C5 -63.47(13) . . . . ? N2 C3 C4 C16 16.2(3) . . . . ? C2 C3 C4 C16 -163.70(18) . . . . ? Fe1 C3 C4 C16 134.45(19) . . . . ? N2 C3 C4 Fe1 -118.22(19) . . . . ? C2 C3 C4 Fe1 61.85(13) . . . . ? C3 C4 C5 C1 -7.6(2) . . . . ? C16 C4 C5 C1 155.40(17) . . . . ? Fe1 C4 C5 C1 -73.10(14) . . . . ? C3 C4 C5 C24 -167.11(18) . . . . ? C16 C4 C5 C24 -4.1(3) . . . . ? Fe1 C4 C5 C24 127.4(2) . . . . ? C3 C4 C5 Fe1 65.45(13) . . . . ? C16 C4 C5 Fe1 -131.51(18) . . . . ? O1 C1 C5 C4 -173.87(19) . . . . ? C2 C1 C5 C4 13.5(2) . . . . ? Fe1 C1 C5 C4 63.72(13) . . . . ? O1 C1 C5 C24 -13.5(3) . . . . ? C2 C1 C5 C24 173.84(17) . . . . ? Fe1 C1 C5 C24 -135.92(19) . . . . ? O1 C1 C5 Fe1 122.4(2) . . . . ? C2 C1 C5 Fe1 -50.24(13) . . . . ? C2 N1 C6 C7 94.9(2) . . . . ? C10 N1 C6 C7 -57.0(2) . . . . ? N1 C6 C7 C8 56.3(2) . . . . ? C6 C7 C8 C9 -54.5(3) . . . . ? C7 C8 C9 C10 53.4(3) . . . . ? C2 N1 C10 C9 -95.2(2) . . . . ? C6 N1 C10 C9 56.2(2) . . . . ? C8 C9 C10 N1 -54.1(3) . . . . ? C3 N2 C11 C12 153.88(17) . . . . ? C15 N2 C11 C12 -58.8(2) . . . . ? N2 C11 C12 C13 56.7(2) . . . . ? C11 C12 C13 C14 -55.0(2) . . . . ? C12 C13 C14 C15 53.7(2) . . . . ? C3 N2 C15 C14 -154.43(17) . . . . ? C11 N2 C15 C14 57.7(2) . . . . ? C13 C14 C15 N2 -54.1(2) . . . . ? C3 C4 C16 C21 -123.4(2) . . . . ? C5 C4 C16 C21 76.9(2) . . . . ? Fe1 C4 C16 C21 -18.2(3) . . . . ? C3 C4 C16 C17 61.0(3) . . . . ? C5 C4 C16 C17 -98.6(2) . . . . ? Fe1 C4 C16 C17 166.22(15) . . . . ? C21 C16 C17 C18 0.3(3) . . . . ? C4 C16 C17 C18 175.93(18) . . . . ? C21 C16 C17 C22 179.90(19) . . . . ? C4 C16 C17 C22 -4.5(3) . . . . ? C16 C17 C18 C19 0.6(3) . . . . ? C22 C17 C18 C19 -179.1(2) . . . . ? C17 C18 C19 C20 -0.4(3) . . . . ? C18 C19 C20 C21 -0.7(3) . . . . ? C18 C19 C20 C23 177.9(2) . . . . ? C19 C20 C21 C16 1.6(3) . . . . ? C23 C20 C21 C16 -176.99(19) . . . . ? C17 C16 C21 C20 -1.4(3) . . . . ? C4 C16 C21 C20 -177.00(18) . . . . ? C4 C5 C24 C29 -87.5(3) . . . . ? C1 C5 C24 C29 115.5(2) . . . . ? Fe1 C5 C24 C29 4.7(3) . . . . ? C4 C5 C24 C25 94.6(2) . . . . ? C1 C5 C24 C25 -62.4(3) . . . . ? Fe1 C5 C24 C25 -173.28(15) . . . . ? C29 C24 C25 C26 1.7(3) . . . . ? C5 C24 C25 C26 179.70(19) . . . . ? C29 C24 C25 C30 -178.3(2) . . . . ? C5 C24 C25 C30 -0.2(3) . . . . ? C24 C25 C26 C27 -1.1(3) . . . . ? C30 C25 C26 C27 178.8(2) . . . . ? C25 C26 C27 C28 -0.1(4) . . . . ? C26 C27 C28 C29 0.7(3) . . . . ? C26 C27 C28 C31 -178.6(2) . . . . ? C25 C24 C29 C28 -1.1(3) . . . . ? C5 C24 C29 C28 -179.08(18) . . . . ? C27 C28 C29 C24 -0.1(3) . . . . ? C31 C28 C29 C24 179.2(2) . . . . ? C41A C36A C37A C38A 0.0 . . . . ? C42A C36A C37A C38A 179.1(7) . . . . ? C36A C37A C38A C39A 0.0 . . . . ? C37A C38A C39A C40A 0.0 . . . . ? C38A C39A C40A C41A 0.0 . . . . ? C39A C40A C41A C36A 0.0 . . . . ? C37A C36A C41A C40A 0.0 . . . . ? C42A C36A C41A C40A -179.1(7) . . . . ? C37B C36B C41B C40B 0.0 . . . . ? C42B C36B C41B C40B -176.3(10) . . . . ? C36B C41B C40B C39B 0.0 . . . . ? C41B C40B C39B C38B 0.0 . . . . ? C40B C39B C38B C37B 0.0 . . . . ? C39B C38B C37B C36B 0.0 . . . . ? C41B C36B C37B C38B 0.0 . . . . ? C42B C36B C37B C38B 176.7(9) . . . . ? C41C C40C C39C C38C -166(3) . . . . ? C40C C39C C38C C37C 130(6) . . . . ? C39C C38C C37C C36C 165(5) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -15.4373 5.8424 4.6887 -0.0092 -0.3955 0.9184 -7.6384 33.5485 7.5454 0.0151 0.5374 0.8432 15.4248 -6.1903 -4.7449 0.0090 0.3868 -0.9221 12.9314 -22.7282 -6.9673 -0.0037 -0.0951 -0.9955 12.8985 0.3909 -15.6385 -0.6816 0.1629 -0.7133 -11.8664 -4.4565 16.3922 0.7728 -0.1849 0.6071 11.1333 6.8515 -16.6863 -0.8201 0.1963 -0.5375 -14.3693 10.9764 11.8370 0.3533 -0.0838 0.9317 -12.4454 -2.3042 16.0323 0.7262 -0.1736 0.6652 7.7188 -10.9161 -17.4685 -0.7559 -0.3137 -0.5746 -3.4440 5.3831 -14.6095 -0.8970 -0.3712 0.2400 11.5828 -16.6520 -14.3546 -0.4810 -0.2001 -0.8536 7.0923 -10.6490 11.0036 0.7959 0.3291 -0.5082 -1.9475 2.4545 17.5128 0.9127 0.3782 0.1546 -6.7008 9.4169 17.7659 0.7995 0.3317 0.5007 -11.2412 16.1403 14.8293 0.5163 0.2147 0.8290 4.6396 34.3826 4.7433 0.0256 0.9829 0.1822 2.6114 -36.9084 -6.8915 -0.0202 -0.7915 -0.6108 -7.3435 -31.1538 -3.5536 -0.0262 -0.9996 0.0066 -9.6215 -31.3259 6.0829 0.4724 -0.8705 0.1383 -15.1542 -10.6358 8.3607 0.3399 -0.6274 0.7006