#------------------------------------------------------------------------------ #$Date: 2024-07-09 00:42:20 +0300 (Tue, 09 Jul 2024) $ #$Revision: 293301 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/20/1572063.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572063 loop_ _publ_author_name 'K\"orner, Lukas' 'Bockfeld, Dirk' 'Bannenberg, Thomas' 'Tamm, Matthias' _publ_section_title ; 2,3-Diamino-4,5-diarylcyclopentadienone iron carbonyl complexes as catalysts for reductive amination reactions ; _journal_name_full 'Catalysis Science & Technology' _journal_paper_doi 10.1039/D4CY00372A _journal_year 2024 _chemical_formula_moiety 'C32 H28 F6 Fe N2 O4, C6 H12' _chemical_formula_sum 'C38 H40 F6 Fe N2 O4' _chemical_formula_weight 758.57 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-03-06 deposited with the CCDC. 2024-07-05 downloaded from the CCDC. ; _cell_angle_alpha 101.0985(12) _cell_angle_beta 99.2340(10) _cell_angle_gamma 103.2907(8) _cell_formula_units_Z 4 _cell_length_a 10.59054(12) _cell_length_b 15.4277(2) _cell_length_c 23.2167(3) _cell_measurement_reflns_used 144939 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 45.0640 _cell_measurement_theta_min 2.1100 _cell_volume 3538.47(8) _computing_cell_refinement 'CrysAlisPro 1.171.42.64a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.64a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.64a (Rigaku OD, 2022)' _computing_publication_material 'OLEX2 v1.3 (O. V. Dolomanov et al., J. Appl. Cryst., 2009, 42, 339-341)' _computing_structure_refinement 'SHELXL-2018/3 (G. M. Sheldrick, Acta Cryst., 2015, C71, 3-8)' _computing_structure_solution 'SHELXT 2018/2 (G. M. Sheldrick, Acta Cryst., 2015, A71, 3-8)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at offset/far, HyPix' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_unetI/netI 0.0396 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_l_max 42 _diffrn_reflns_limit_l_min -42 _diffrn_reflns_number 78215 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 40.327 _diffrn_reflns_theta_min 2.020 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.501 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.407 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.64a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.424 _exptl_crystal_description irregular _exptl_crystal_F_000 1576 _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.230 _exptl_crystal_size_min 0.017 _refine_diff_density_max 2.068 _refine_diff_density_min -0.969 _refine_diff_density_rms 0.138 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.049 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 976 _refine_ls_number_reflns 78215 _refine_ls_number_restraints 144 _refine_ls_restrained_S_all 1.083 _refine_ls_R_factor_all 0.1161 _refine_ls_R_factor_gt 0.0855 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1217P)^2^+3.4697P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2310 _refine_ls_wR_factor_ref 0.2484 _reflns_Friedel_coverage 0.000 _reflns_number_gt 55547 _reflns_number_total 78215 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4cy00372a3.cif _cod_data_source_block lk39db _cod_original_cell_volume 3538.46(8) _cod_database_code 1572063 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.825 _shelx_estimated_absorpt_t_max 0.992 _oxdiff_exptl_absorpt_empirical_full_min 0.825 _oxdiff_exptl_absorpt_empirical_full_max 1.379 _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _shelx_res_file ; TITL lk39db_a.res in P-1 lk39db.res created by SHELXL-2018/3 at 18:18:31 on 20-Dec-2022 REM Old TITL lk39db_twin1_hklf4 in P-1 REM SHELXT solution in P-1: R1 0.151, Rweak 0.009, 0.085 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C79 N5 O6 F11 Fe2 CELL 0.71073 10.59054 15.4277 23.2167 101.0985 99.234 103.2907 ZERR 4 0.00012 0.0002 0.0003 0.0012 0.001 0.0008 LATT 1 SFAC C H F Fe N O UNIT 152 160 24 4 8 16 RIGU 0.0001 0.0001 C94A > C99A RIGU 0.0001 0.0001 C94 > C99 ISOR 0.001 0.002 F5A F2A F6A F3A F4A F1A F5 F2 F6 F3 F4 F1 L.S. 4 0 0 PLAN 10 SIZE 0.4 0.23 0.017 TEMP -173 CONF BOND list 4 fmap 2 53 acta MERG 0 OMIT -4 6 -9 OMIT -3 -3 -3 OMIT 4 -2 3 OMIT 4 0 9 OMIT -4 4 -7 OMIT -3 -9 -3 OMIT -1 -11 6 OMIT -1 -4 -5 OMIT 0 -3 -7 REM REM REM WGHT 0.121700 3.469700 BASF 0.14933 FVAR 1.22558 0.75288 0.47197 FE1 4 0.923662 1.023874 0.167755 11.00000 0.01483 0.01351 = 0.01259 0.00269 0.00356 0.00476 F7 3 1.088983 0.532993 0.060814 11.00000 0.08129 0.02971 = 0.05736 0.01878 0.03878 0.03518 F8 3 0.903913 0.500461 0.086750 11.00000 0.05807 0.01954 = 0.15806 0.01966 0.03929 0.00484 F9 3 1.082984 0.555296 0.153712 11.00000 0.12967 0.04338 = 0.04356 0.02332 0.02119 0.05539 O1 6 0.844380 1.078751 0.031010 11.00000 0.02398 0.01750 = 0.01921 0.00784 -0.00354 0.00362 O2 6 0.718039 0.903286 0.209071 11.00000 0.03392 0.02785 = 0.05442 0.01716 0.02774 0.01077 O3 6 0.790987 1.171829 0.187220 11.00000 0.02577 0.02423 = 0.03203 0.00439 0.00728 0.01312 O4 6 1.114074 1.079834 0.284416 11.00000 0.02845 0.03134 = 0.01685 0.00318 -0.00092 0.01083 N1 5 1.219581 1.018542 0.147575 11.00000 0.01307 0.01713 = 0.01690 0.00570 0.00340 0.00385 N2 5 1.114968 1.177216 0.118898 11.00000 0.01903 0.01182 = 0.01402 0.00271 0.00167 0.00314 C1 1 0.907494 1.044827 0.065481 11.00000 0.01765 0.01381 = 0.01366 0.00321 0.00076 0.00362 C2 1 0.862852 0.953322 0.077630 11.00000 0.01581 0.01382 = 0.01304 0.00302 0.00157 0.00439 C3 1 0.977169 0.930160 0.107804 11.00000 0.01391 0.01199 = 0.01439 0.00329 0.00378 0.00306 C4 1 1.088475 1.010891 0.122532 11.00000 0.01440 0.01352 = 0.01322 0.00351 0.00367 0.00400 C5 1 1.040839 1.086539 0.107558 11.00000 0.01606 0.01330 = 0.01222 0.00268 0.00208 0.00324 C6 1 0.731436 0.891264 0.045684 11.00000 0.01472 0.01407 = 0.01503 0.00218 0.00237 0.00396 C7 1 0.717313 0.801184 0.014510 11.00000 0.01575 0.01576 = 0.02148 -0.00011 0.00159 0.00481 AFIX 43 H7 2 0.792834 0.777650 0.015744 11.00000 -1.20000 AFIX 0 C8 1 0.593686 0.745685 -0.018303 11.00000 0.01562 0.01716 = 0.02315 0.00099 0.00083 0.00352 AFIX 43 H8 2 0.585156 0.684415 -0.038846 11.00000 -1.20000 AFIX 0 C9 1 0.483140 0.779642 -0.021048 11.00000 0.01356 0.01956 = 0.01890 0.00495 0.00156 0.00280 C10 1 0.494716 0.869516 0.009730 11.00000 0.01585 0.02139 = 0.02376 0.00391 0.00220 0.00618 AFIX 43 H10 2 0.418876 0.892730 0.008093 11.00000 -1.20000 AFIX 0 C11 1 0.618018 0.924456 0.042679 11.00000 0.01887 0.01753 = 0.02228 0.00232 0.00197 0.00779 AFIX 43 H11 2 0.625892 0.985455 0.063530 11.00000 -1.20000 AFIX 0 C12 1 0.350669 0.720498 -0.056984 11.00000 0.01657 0.02420 = 0.02204 0.00689 0.00256 0.00323 C13 1 0.988099 0.835690 0.107444 11.00000 0.01609 0.01349 = 0.01402 0.00364 0.00367 0.00448 C14 1 0.936728 0.785987 0.146714 11.00000 0.02555 0.01761 = 0.02523 0.01037 0.01333 0.00914 AFIX 43 H14 2 0.894027 0.813062 0.175516 11.00000 -1.20000 AFIX 0 C15 1 0.947601 0.696873 0.143997 11.00000 0.03094 0.01893 = 0.03146 0.01362 0.01659 0.00965 AFIX 43 H15 2 0.912967 0.663631 0.171023 11.00000 -1.20000 AFIX 0 C16 1 1.009078 0.657082 0.101748 11.00000 0.02732 0.01503 = 0.02750 0.00728 0.00874 0.00755 C17 1 1.061065 0.705478 0.062407 11.00000 0.02900 0.01711 = 0.02112 0.00509 0.01009 0.01076 AFIX 43 H17 2 1.103051 0.677762 0.033538 11.00000 -1.20000 AFIX 0 C18 1 1.051499 0.794895 0.065370 11.00000 0.02327 0.01651 = 0.01720 0.00591 0.00813 0.00777 AFIX 43 H18 2 1.088047 0.828265 0.038805 11.00000 -1.20000 AFIX 0 C19 1 1.021235 0.561847 0.100875 11.00000 0.04616 0.01774 = 0.04099 0.01179 0.01877 0.01388 C20 1 1.254352 0.951405 0.179849 11.00000 0.01682 0.01901 = 0.02078 0.00744 0.00030 0.00532 AFIX 23 H20A 2 1.261555 0.897460 0.150915 11.00000 -1.20000 H20B 2 1.183953 0.930336 0.201316 11.00000 -1.20000 AFIX 0 C21 1 1.386447 0.995552 0.224725 11.00000 0.01769 0.02902 = 0.02135 0.00853 0.00084 0.00557 AFIX 23 H21A 2 1.411330 0.949811 0.245660 11.00000 -1.20000 H21B 2 1.377056 1.046821 0.255227 11.00000 -1.20000 AFIX 0 C22 1 1.495549 1.031491 0.192731 11.00000 0.01561 0.03706 = 0.02863 0.01270 0.00367 0.00731 AFIX 23 H22A 2 1.511009 0.979495 0.165005 11.00000 -1.20000 H22B 2 1.579323 1.062925 0.222677 11.00000 -1.20000 AFIX 0 C23 1 1.455288 1.098519 0.157315 11.00000 0.01549 0.03343 = 0.02907 0.01178 0.00473 0.00194 AFIX 23 H23A 2 1.451966 1.154371 0.185671 11.00000 -1.20000 H23B 2 1.522894 1.116898 0.133881 11.00000 -1.20000 AFIX 0 C24 1 1.319965 1.055356 0.114739 11.00000 0.01731 0.02520 = 0.01830 0.00742 0.00598 0.00586 AFIX 23 H24A 2 1.292102 1.102036 0.095676 11.00000 -1.20000 H24B 2 1.326616 1.005226 0.082582 11.00000 -1.20000 AFIX 0 C25 1 1.198878 1.215738 0.179783 11.00000 0.02168 0.01541 = 0.01599 0.00162 0.00050 0.00244 AFIX 23 H25A 2 1.245288 1.170713 0.191180 11.00000 -1.20000 H25B 2 1.141959 1.227075 0.208766 11.00000 -1.20000 AFIX 0 C26 1 1.300920 1.304970 0.183327 11.00000 0.02377 0.01679 = 0.02630 0.00295 0.00066 -0.00045 AFIX 23 H26A 2 1.361304 1.293229 0.156105 11.00000 -1.20000 H26B 2 1.354843 1.329323 0.224802 11.00000 -1.20000 AFIX 0 C27 1 1.232242 1.375612 0.165552 11.00000 0.02959 0.01413 = 0.02697 0.00197 0.00378 0.00183 AFIX 23 H27A 2 1.299481 1.431199 0.164211 11.00000 -1.20000 H27B 2 1.180755 1.393523 0.195677 11.00000 -1.20000 AFIX 0 C28 1 1.139070 1.334026 0.103588 11.00000 0.03032 0.01408 = 0.02213 0.00561 0.00311 0.00437 AFIX 23 H28A 2 1.087925 1.377439 0.093753 11.00000 -1.20000 H28B 2 1.192582 1.324627 0.072825 11.00000 -1.20000 AFIX 0 C29 1 1.043551 1.243242 0.101674 11.00000 0.02267 0.01331 = 0.02235 0.00491 0.00007 0.00410 AFIX 23 H29A 2 0.983718 1.253607 0.129423 11.00000 -1.20000 H29B 2 0.988256 1.217143 0.060569 11.00000 -1.20000 AFIX 0 C30 1 0.799856 0.948338 0.192879 11.00000 0.02441 0.01933 = 0.02597 0.00637 0.01092 0.00875 C31 1 0.844349 1.115662 0.178396 11.00000 0.01750 0.01909 = 0.01691 0.00291 0.00373 0.00485 C32 1 1.040047 1.058454 0.239173 11.00000 0.02160 0.02099 = 0.01440 0.00410 0.00459 0.00870 PART 1 F1 3 0.303602 0.755336 -0.102478 21.00000 0.03573 0.05226 = 0.04036 0.02780 -0.01675 -0.00866 F2 3 0.257039 0.712994 -0.025382 21.00000 0.02277 0.06733 = 0.03369 0.00437 0.01047 -0.01192 F3 3 0.351786 0.635886 -0.082525 21.00000 0.02894 0.03068 = 0.06807 -0.01320 -0.01498 0.00557 PART 2 F4 3 0.360272 0.681742 -0.109059 -21.00000 0.04340 0.05436 = 0.03943 0.00194 0.01082 0.00291 F5 3 0.257857 0.762731 -0.057474 -21.00000 0.04840 0.05214 = 0.06583 0.00681 0.00244 0.02379 F6 3 0.307110 0.651940 -0.030660 -21.00000 0.04835 0.04852 = 0.05030 0.02170 0.00443 -0.00010 PART 0 FE1A 4 1.026483 0.260029 0.401572 11.00000 0.01668 0.01880 = 0.01187 0.00309 0.00342 0.00705 F7A 3 0.802018 0.201282 0.717523 11.00000 0.11519 0.06648 = 0.04045 0.03217 0.05119 0.04578 F8A 3 0.953148 0.130906 0.707111 11.00000 0.07501 0.08473 = 0.04009 0.04256 0.01673 0.03269 F9A 3 0.753409 0.065453 0.659376 11.00000 0.07109 0.05237 = 0.05537 0.03452 0.03010 0.00547 O1A 6 1.173703 0.495236 0.445156 11.00000 0.02350 0.02368 = 0.01880 0.00750 -0.00136 -0.00448 O2A 6 1.157631 0.121092 0.431277 11.00000 0.06728 0.06370 = 0.03265 0.02416 0.02239 0.05232 O3A 6 1.207202 0.308042 0.321576 11.00000 0.02563 0.06176 = 0.02422 0.01355 0.01283 0.01368 O4A 6 0.812433 0.116869 0.313174 11.00000 0.02912 0.02297 = 0.02158 0.00139 0.00302 0.00239 N1A 5 0.738454 0.289928 0.416489 11.00000 0.01436 0.02096 = 0.01897 0.00652 0.00418 0.00412 N2A 5 0.904755 0.413467 0.352507 11.00000 0.01923 0.01662 = 0.01224 0.00405 0.00256 0.00415 C1A 1 1.086850 0.425748 0.444046 11.00000 0.01885 0.01859 = 0.01210 0.00380 0.00141 0.00319 C2A 1 1.097780 0.359978 0.481938 11.00000 0.01565 0.01923 = 0.01212 0.00398 0.00249 0.00370 C3A 1 0.965033 0.304308 0.479138 11.00000 0.01677 0.01650 = 0.01257 0.00419 0.00355 0.00499 C4A 1 0.874898 0.323367 0.432325 11.00000 0.01536 0.01657 = 0.01339 0.00380 0.00252 0.00457 C5A 1 0.952996 0.383860 0.402511 11.00000 0.01774 0.01513 = 0.01302 0.00419 0.00292 0.00421 C6A 1 1.219089 0.376913 0.528548 11.00000 0.01676 0.02188 = 0.01284 0.00309 0.00247 0.00577 C7A 1 1.214960 0.384224 0.589294 11.00000 0.01691 0.03038 = 0.01343 0.00545 0.00439 0.00619 AFIX 43 H7A 2 1.131750 0.374704 0.600890 11.00000 -1.20000 AFIX 0 C8A 1 1.331485 0.405291 0.632840 11.00000 0.01931 0.03155 = 0.01389 0.00605 0.00207 0.00668 AFIX 43 H8A 2 1.327303 0.409746 0.673840 11.00000 -1.20000 AFIX 0 C9A 1 1.453197 0.419734 0.616581 11.00000 0.01710 0.02903 = 0.01652 0.00488 0.00136 0.00638 C10A 1 1.460477 0.415234 0.556595 11.00000 0.01642 0.04799 = 0.01840 0.00468 0.00366 0.00644 AFIX 43 H10A 2 1.544300 0.427255 0.545619 11.00000 -1.20000 AFIX 0 C11A 1 1.343654 0.392945 0.512966 11.00000 0.01794 0.04464 = 0.01451 0.00612 0.00467 0.00562 AFIX 43 H11A 2 1.348425 0.388537 0.472031 11.00000 -1.20000 AFIX 0 C12A 1 1.577829 0.443762 0.664335 11.00000 0.01975 0.03923 = 0.02287 0.00587 -0.00157 0.00808 C13A 1 0.927524 0.258546 0.527232 11.00000 0.01849 0.01737 = 0.01489 0.00584 0.00455 0.00513 C14A 1 0.973728 0.185004 0.539482 11.00000 0.04396 0.03289 = 0.03125 0.01927 0.02149 0.02363 AFIX 43 H14A 2 1.023808 0.158617 0.514064 11.00000 -1.20000 AFIX 0 C15A 1 0.947429 0.149654 0.588537 11.00000 0.05224 0.03586 = 0.03532 0.02457 0.02397 0.02680 AFIX 43 H15A 2 0.979907 0.099754 0.596594 11.00000 -1.20000 AFIX 0 C16A 1 0.873803 0.187553 0.625459 11.00000 0.03622 0.02834 = 0.02117 0.01310 0.01243 0.00953 C17A 1 0.827461 0.261270 0.614177 11.00000 0.02933 0.02486 = 0.01831 0.00686 0.01056 0.00793 AFIX 43 H17A 2 0.777477 0.287413 0.639759 11.00000 -1.20000 AFIX 0 C18A 1 0.854439 0.296694 0.565326 11.00000 0.02375 0.01866 = 0.01393 0.00363 0.00599 0.00592 AFIX 43 H18A 2 0.822946 0.347211 0.557795 11.00000 -1.20000 AFIX 0 C19A 1 0.845017 0.147022 0.677292 11.00000 0.06117 0.04367 = 0.03259 0.02490 0.02453 0.02001 C20A 1 0.670607 0.206457 0.432013 11.00000 0.01752 0.02397 = 0.02309 0.00836 0.00167 -0.00028 AFIX 23 H20C 2 0.652506 0.222025 0.472733 11.00000 -1.20000 H20D 2 0.727982 0.164054 0.432131 11.00000 -1.20000 AFIX 0 C21A 1 0.539874 0.159973 0.386112 11.00000 0.01823 0.02702 = 0.02579 0.00403 0.00051 -0.00152 AFIX 23 H21C 2 0.558775 0.140757 0.345903 11.00000 -1.20000 H21D 2 0.492809 0.104433 0.397262 11.00000 -1.20000 AFIX 0 C22A 1 0.451831 0.225036 0.383732 11.00000 0.01587 0.04080 = 0.03624 0.00753 0.00343 0.00361 AFIX 23 H22C 2 0.425586 0.239529 0.422770 11.00000 -1.20000 H22D 2 0.370106 0.195211 0.352222 11.00000 -1.20000 AFIX 0 C23A 1 0.525960 0.313393 0.370016 11.00000 0.01875 0.03409 = 0.03581 0.00960 0.00206 0.01035 AFIX 23 H23C 2 0.471050 0.357413 0.372620 11.00000 -1.20000 H23D 2 0.539959 0.299756 0.328439 11.00000 -1.20000 AFIX 0 C24A 1 0.660282 0.357185 0.413561 11.00000 0.01859 0.02559 = 0.02521 0.00402 0.00508 0.00924 AFIX 23 H24C 2 0.710121 0.409504 0.400173 11.00000 -1.20000 H24D 2 0.646107 0.380947 0.454089 11.00000 -1.20000 AFIX 0 C25A 1 0.815409 0.339702 0.302413 11.00000 0.02152 0.01888 = 0.01414 0.00322 0.00011 0.00469 AFIX 23 H25C 2 0.749513 0.299694 0.318438 11.00000 -1.20000 H25D 2 0.868007 0.301756 0.283252 11.00000 -1.20000 AFIX 0 C26A 1 0.742949 0.377988 0.255459 11.00000 0.02471 0.02719 = 0.01850 0.00624 -0.00104 0.00789 AFIX 23 H26C 2 0.687115 0.413811 0.273967 11.00000 -1.20000 H26D 2 0.684106 0.326885 0.222675 11.00000 -1.20000 AFIX 0 C27A 1 0.843048 0.439512 0.229791 11.00000 0.03369 0.02840 = 0.01525 0.00875 0.00225 0.00853 AFIX 23 H27C 2 0.795913 0.467891 0.201441 11.00000 -1.20000 H27D 2 0.892959 0.402603 0.207681 11.00000 -1.20000 AFIX 0 C28A 1 0.938943 0.514166 0.281572 11.00000 0.03386 0.02177 = 0.01676 0.00810 0.00493 0.00629 AFIX 23 H28C 2 1.008431 0.551149 0.265618 11.00000 -1.20000 H28D 2 0.889857 0.555462 0.300122 11.00000 -1.20000 AFIX 0 C29A 1 1.004739 0.473521 0.329499 11.00000 0.02397 0.02214 = 0.01603 0.00725 0.00284 0.00227 AFIX 23 H29C 2 1.061815 0.437682 0.312111 11.00000 -1.20000 H29D 2 1.061988 0.523859 0.363195 11.00000 -1.20000 AFIX 0 C30A 1 1.106590 0.175988 0.421786 11.00000 0.03445 0.03757 = 0.01783 0.00823 0.00907 0.02272 C31A 1 1.135805 0.291115 0.352436 11.00000 0.01829 0.03207 = 0.01708 0.00458 0.00434 0.00834 C32A 1 0.895425 0.173062 0.346993 11.00000 0.02357 0.01869 = 0.01668 0.00375 0.00575 0.00722 PART 3 F1A 3 1.645507 0.535851 0.674598 31.00000 0.04299 0.04376 = 0.06240 0.00615 -0.02492 0.00720 F2A 3 1.672425 0.407920 0.644467 31.00000 0.02217 0.04582 = 0.03814 0.00071 -0.00316 0.01946 F3A 3 1.563483 0.429149 0.714307 31.00000 0.03555 0.08896 = 0.03075 0.02327 0.00200 0.00540 PART 4 F4A 3 1.577971 0.507759 0.709814 -31.00000 0.05701 0.06178 = 0.04849 -0.02134 -0.02384 0.03015 F5A 3 1.684276 0.461980 0.645611 -31.00000 0.03889 0.08481 = 0.04636 0.02088 0.01076 0.00048 F6A 3 1.581268 0.371523 0.691494 -31.00000 0.04667 0.04785 = 0.05790 0.02698 -0.02248 0.00586 PART 0 C94 1 0.603329 0.669032 0.196864 11.00000 0.03732 0.05881 = 0.07528 0.03941 0.01090 0.01196 AFIX 23 H94A 2 0.622084 0.667171 0.239713 11.00000 -1.20000 H94B 2 0.676832 0.716303 0.190341 11.00000 -1.20000 AFIX 0 C95 1 0.595259 0.575225 0.157256 11.00000 0.04741 0.06057 = 0.08455 0.03674 0.01714 0.01308 AFIX 23 H95A 2 0.682969 0.562428 0.165450 11.00000 -1.20000 H95B 2 0.530174 0.527271 0.168158 11.00000 -1.20000 AFIX 0 C96 1 0.554734 0.569694 0.090581 11.00000 0.06414 0.06457 = 0.08295 0.03215 0.01550 0.02116 AFIX 23 H96A 2 0.624612 0.612553 0.078356 11.00000 -1.20000 H96B 2 0.545755 0.506827 0.067367 11.00000 -1.20000 AFIX 0 C97 1 0.424783 0.593680 0.076605 11.00000 0.06320 0.07357 = 0.07493 0.03083 0.01331 0.02210 AFIX 23 H97A 2 0.352839 0.546743 0.084469 11.00000 -1.20000 H97B 2 0.403271 0.593998 0.033557 11.00000 -1.20000 AFIX 0 C98 1 0.433109 0.687496 0.115022 11.00000 0.05043 0.06984 = 0.06416 0.03682 0.01122 0.02008 AFIX 23 H98A 2 0.498730 0.734797 0.103859 11.00000 -1.20000 H98B 2 0.345651 0.700532 0.106385 11.00000 -1.20000 AFIX 0 C99 1 0.472772 0.694127 0.181697 11.00000 0.03985 0.07313 = 0.06514 0.04025 0.01293 0.01836 AFIX 23 H99A 2 0.402019 0.652240 0.194094 11.00000 -1.20000 H99B 2 0.482449 0.757436 0.204358 11.00000 -1.20000 AFIX 0 C94A 1 0.421017 0.112779 0.540541 11.00000 0.06977 0.08682 = 0.10735 0.02920 0.02748 0.02282 AFIX 23 H94C 2 0.376388 0.149290 0.517653 11.00000 -1.20000 H94D 2 0.499138 0.105425 0.523702 11.00000 -1.20000 AFIX 0 C95A 1 0.334968 0.027531 0.531722 11.00000 0.05980 0.08501 = 0.09225 0.03196 0.01409 0.02651 AFIX 23 H95C 2 0.386211 -0.013971 0.544908 11.00000 -1.20000 H95D 2 0.297420 0.003355 0.488099 11.00000 -1.20000 AFIX 0 C96A 1 0.224396 0.024349 0.563124 11.00000 0.05396 0.06900 = 0.07913 0.02035 0.00488 0.01994 AFIX 23 H96C 2 0.163127 0.056039 0.544712 11.00000 -1.20000 H96D 2 0.174469 -0.040467 0.557364 11.00000 -1.20000 AFIX 0 C97A 1 0.267199 0.066595 0.627378 11.00000 0.06603 0.07504 = 0.08042 0.01705 0.00159 0.02075 AFIX 23 H97C 2 0.187109 0.067559 0.644119 11.00000 -1.20000 H97D 2 0.313103 0.027092 0.646684 11.00000 -1.20000 AFIX 0 C98A 1 0.354072 0.158583 0.644023 11.00000 0.09170 0.08168 = 0.09405 0.00526 0.01527 0.00722 AFIX 23 H98C 2 0.395898 0.174639 0.687351 11.00000 -1.20000 H98D 2 0.301969 0.202583 0.636763 11.00000 -1.20000 AFIX 0 C99A 1 0.468724 0.165560 0.604631 11.00000 0.08976 0.10250 = 0.11472 0.01711 0.02315 0.00508 AFIX 23 H99C 2 0.506676 0.230883 0.605574 11.00000 -1.20000 H99D 2 0.540972 0.142895 0.623838 11.00000 -1.20000 AFIX 0 HKLF 5 REM lk39db_a.res in P-1 REM wR2 = 0.2484, GooF = S = 1.049, Restrained GooF = 1.083 for all data REM R1 = 0.0855 for 55547 Fo > 4sig(Fo) and 0.1161 for all 78215 data REM 976 parameters refined using 144 restraints END WGHT 0.1217 3.4737 REM Highest difference peak 2.068, deepest hole -0.969, 1-sigma level 0.138 Q1 1 0.3779 0.7796 -0.0805 11.00000 0.05 2.07 Q2 1 0.9564 0.2397 0.3801 11.00000 0.05 1.84 Q3 1 0.7390 0.4674 0.3194 11.00000 0.05 1.83 Q4 1 0.9927 1.0417 0.1838 11.00000 0.05 1.67 Q5 1 0.4499 0.1884 0.6391 11.00000 0.05 1.54 Q6 1 1.5526 0.4752 0.7202 11.00000 0.05 1.33 Q7 1 1.6247 0.3802 0.6625 11.00000 0.05 1.21 Q8 1 1.5791 0.5173 0.6575 11.00000 0.05 1.20 Q9 1 1.0944 0.2831 0.4197 11.00000 0.05 1.17 Q10 1 0.6010 0.5843 0.1829 11.00000 0.05 1.17 ; _shelx_res_checksum 34811 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24.5493 1 0 -2 -7 886.030 6.36692 1 0 2 8 9211.30 57.4448 1 0 3 7 10488.5 26.0155 -2 0 -2 -8 10488.5 26.0155 1 0 -2 -9 244.779 3.71647 1 0 4 8 10457.1 21.8326 -2 0 -2 -10 10457.1 21.8326 1 0 -2 -11 4716.13 17.2665 1 0 -4 -9 6116.20 67.6863 -2 0 2 11 6116.20 67.6863 1 0 -5 -9 168.485 6.76314 -2 0 2 12 168.485 6.76314 1 0 -2 -13 1235.92 13.7843 1 0 -5 -10 1994.25 23.2616 -2 0 2 13 1994.25 23.2616 1 0 -6 -10 403.645 8.50707 -2 0 2 14 403.645 8.50707 1 0 2 15 1163.47 14.2870 1 0 6 11 1916.64 23.5118 -2 0 -2 -15 1916.64 23.5118 1 0 -7 -11 218.507 7.48720 -2 0 2 16 218.507 7.48720 1 0 -2 -17 148.852 11.0849 1 0 -7 -12 263.597 9.23792 -2 0 2 17 263.597 9.23792 1 0 -8 -12 2731.77 20.5682 -2 0 2 18 2731.77 20.5682 1 0 8 13 920.759 12.9823 -2 0 -2 -19 920.759 12.9823 1 0 9 13 57.1657 6.48039 -2 0 -2 -20 57.1657 6.48039 1 0 -9 -14 28.3299 4.70521 -2 0 2 21 28.3299 4.70521 1 0 -10 -14 29.3332 8.31747 -2 0 2 22 29.3332 8.31747 1 0 -10 -15 395.927 11.9417 -2 0 2 23 395.927 11.9417 1 0 -2 -24 2015.26 41.3512 1 0 -11 -15 2509.37 24.4758 -2 0 2 24 2509.37 24.4758 1 0 -11 -16 1256.32 19.8551 -2 0 2 25 1256.32 19.8551 1 0 2 26 81.7810 29.0595 1 0 -12 -16 59.7167 7.90500 -2 0 2 26 59.7167 7.90500 1 0 12 17 16.5275 6.82801 -2 0 -2 -27 16.5275 6.82801 1 0 2 28 105.339 32.1641 1 0 -13 -17 109.862 11.7675 -2 0 2 28 109.862 11.7675 1 0 -13 -18 346.027 14.8007 -2 0 2 29 346.027 14.8007 1 0 2 30 32.0366 22.6146 1 0 -14 -18 88.6383 15.3861 -2 0 2 30 88.6383 15.3861 1 0 14 19 827.833 22.1632 -2 0 -2 -31 827.833 22.1632 1 0 2 32 17.6333 22.4735 1 0 15 19 50.3223 15.1328 -2 0 -2 -32 50.3223 15.1328 1 0 -15 -20 96.2705 9.48953 -2 0 2 33 96.2705 9.48953 1 0 2 34 15.9221 18.0677 1 0 -16 -20 19.3592 22.1701 -2 0 2 34 19.3592 22.1701 1 0 -16 -21 47.7727 16.2051 -2 0 2 35 47.7727 16.2051 1 0 2 36 294.243 25.9602 1 0 17 21 418.011 24.7790 -2 0 -2 -36 418.011 24.7790 1 0 -17 -22 312.323 23.7480 -2 0 2 37 312.323 23.7480 1 0 2 38 31.1691 19.8824 1 0 -18 -22 58.7595 25.4359 -2 0 2 38 58.7595 25.4359 1 0 -18 -23 147.759 21.0163 -2 0 2 39 147.759 21.0163 1 0 -21 -16 20.1318 8.57732 -2 0 -3 40 20.1318 8.57732 1 0 -3 39-3.32003 36.1538 1 0 21 15 27.6752 24.3097 -2 0 3 -39 27.6752 24.3097 1 0 20 15 126.393 22.9241 -2 0 3 -38 126.393 22.9241 1 0 -3 37 825.917 66.0070 1 0 -20 -14 913.571 34.0855 -2 0 -3 37 913.571 34.0855 1 0 19 14 488.136 25.7951 -2 0 3 -36 488.136 25.7951 1 0 -3 35 117.295 40.6942 1 0 -19 -13 187.305 20.4132 -2 0 -3 35 187.305 20.4132 1 0 -18 -13 48.4969 17.3233 -2 0 -3 34 48.4969 17.3233 1 0 -18 -12 358.913 17.3149 -2 0 -3 33 358.913 17.3149 1 0 -17 -12 189.550 15.4927 -2 0 -3 32 189.550 15.4927 1 0 -17 -11 31.2931 12.0564 -2 0 -3 31 31.2931 12.0564 1 0 16 11 306.064 14.7890 -2 0 3 -30 306.064 14.7890 1 0 -3 29 133.511 21.4035 1 0 -16 -10 190.628 13.2989 -2 0 -3 29 190.628 13.2989 1 0 -15 -10 1612.05 20.9192 -2 0 -3 28 1612.05 20.9192 1 0 -3 27 36.7708 19.2218 1 0 -15 -9 30.1670 7.64622 -2 0 -3 27 30.1670 7.64622 1 0 -14 -9 96.0160 10.4943 -2 0 -3 26 96.0160 10.4943 1 0 -14 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452.137 5.96758 1 0 3 -6 3956.67 11.0952 1 0 4 -2 1127.87 4.25743 -2 0 3 -5 1127.87 4.25743 1 0 3 -4 3263.60 8.92935 1 0 -3 3 151530. 34.7269 -2 0 -3 3 151530. 34.7269 1 0 -3 2 5925.42 9.95685 1 0 2 -4 1019.97 5.81373 -2 0 3 -1 1019.97 5.81373 1 0 -3 0 3274.62 7.71375 1 0 1 -5 20084.3 24.3727 -2 0 3 1 20084.3 24.3727 1 0 3 2 6084.46 14.0678 1 0 0 -6 168.498 4.32479 -2 0 3 3 168.498 4.32479 1 0 -3 -4 161.368 3.62964 1 0 -1 -7 3001.01 10.5644 -2 0 3 5 3001.01 10.5644 1 0 3 6 9416.73 15.7026 1 0 -2 -8 4676.30 13.2731 -2 0 3 7 4676.30 13.2731 1 0 -3 -8 236.375 4.05777 1 0 3 9 4609.91 45.0849 1 0 -3 -9 5851.74 19.3106 -2 0 3 9 5851.74 19.3106 1 0 3 10 87.5114 3.10024 1 0 3 10 143.820 23.7947 -2 0 -3 -10 143.820 23.7947 1 0 -4 -10 1253.79 8.90282 -2 0 3 11 1253.79 8.90282 1 0 -3 -12 2745.68 14.0829 1 0 4 11 3034.45 39.1118 -2 0 -3 -12 3034.45 39.1118 1 0 3 13 1589.01 14.7085 1 0 -5 -11 1850.09 15.5948 -2 0 3 13 1850.09 15.5948 1 0 3 14 5515.49 19.7120 1 0 -5 -12 7236.20 39.4214 -2 0 3 14 7236.20 39.4214 1 0 -6 -12 29.7293 4.20724 -2 0 3 15 29.7293 4.20724 1 0 3 16 13.4002 8.96114 1 0 -6 -13 16.1665 6.81891 -2 0 3 16 16.1665 6.81891 1 0 7 13 210.789 7.83509 -2 0 -3 -17 210.789 7.83509 1 0 -7 -14 13.9232 4.04453 -2 0 3 18 13.9232 4.04453 1 0 -8 -14 147.224 8.41569 -2 0 3 19 147.224 8.41569 1 0 -8 -15 203.652 9.08151 -2 0 3 20 203.652 9.08151 1 0 -9 -15 607.874 12.0486 -2 0 3 21 607.874 12.0486 1 0 -9 -16 45.6339 9.16876 -2 0 3 22 45.6339 9.16876 1 0 3 23 2217.64 76.8234 1 0 -10 -16 2719.83 24.2291 -2 0 3 23 2719.83 24.2291 1 0 10 17 17.4516 7.60708 -2 0 -3 -24 17.4516 7.60708 1 0 3 25 517.359 45.1944 1 0 11 17 659.215 15.3860 -2 0 -3 -25 659.215 15.3860 1 0 11 18 555.546 15.6568 -2 0 -3 -26 555.546 15.6568 1 0 3 27 39.7471 12.3248 1 0 12 18 17.3806 9.27946 -2 0 -3 -27 17.3806 9.27946 1 0 -12 -19 213.568 12.7239 -2 0 3 28 213.568 12.7239 1 0 3 29 63.6870 23.7296 1 0 -13 -19 97.3355 15.1206 -2 0 3 29 97.3355 15.1206 1 0 -13 -20 831.255 23.0539 -2 0 3 30 831.255 23.0539 1 0 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7.66367 -2 2 -7 -35 14.8238 7.66367 1 -2 7 34 35.9731 32.3326 1 -2 14 27 8.97465 16.2114 -2 2 -7 -34 8.97465 16.2114 1 -2 13 27 230.820 18.1487 -2 2 -7 -33 230.820 18.1487 1 2 -13 -26 517.257 21.4273 -2 -2 7 32 517.257 21.4273 1 2 -12 -26 240.166 18.2446 -2 -2 7 31 240.166 18.2446 1 -2 12 25 329.731 18.7620 -2 2 -7 -30 329.731 18.7620 1 2 -11 -25 98.3468 14.8665 -2 -2 7 29 98.3468 14.8665 1 2 -11 -24 419.424 19.5246 -2 -2 7 28 419.424 19.5246 1 2 -10 -24 18.9565 8.91752 -2 -2 7 27 18.9565 8.91752 1 -2 10 23 70.6460 11.0520 -2 2 -7 -26 70.6460 11.0520 1 -2 7 25 193.892 35.2279 1 -2 9 23 191.124 13.1591 -2 2 -7 -25 191.124 13.1591 1 2 -7 -24 167.341 17.1595 1 2 -9 -22 321.964 14.9673 -2 -2 7 24 321.964 14.9673 1 -2 7 23 1273.59 29.2638 1 2 -8 -22 2004.98 25.8371 -2 -2 7 23 2004.98 25.8371 1 2 -8 -21 94.8880 11.2953 -2 -2 7 22 94.8880 11.2953 1 2 -7 -21 300.759 10.5785 1 -2 7 21 592.847 17.8152 -2 2 -7 -21 592.847 17.8152 1 -2 7 20 75.9227 8.91232 -2 2 -7 -20 75.9227 8.91232 1 -2 7 19 3325.01 29.2121 1 2 -6 -20 4334.89 37.7803 -2 -2 7 19 4334.89 37.7803 1 -2 6 19 6.45609 3.01659 -2 2 -7 -18 6.45609 3.01659 1 2 -7 -17 592.560 12.3333 1 -2 5 19 692.836 33.2984 -2 2 -7 -17 692.836 33.2984 1 2 -5 -18 2047.93 20.1827 -2 -2 7 16 2047.93 20.1827 1 -2 7 15 223.352 5.95255 1 -2 4 18 239.659 24.8632 -2 2 -7 -15 239.659 24.8632 1 -2 4 17 3238.74 23.1456 -2 2 -7 -14 3238.74 23.1456 1 2 -7 -13 225.426 6.84173 1 -2 3 17 263.795 22.2016 -2 2 -7 -13 263.795 22.2016 1 -2 3 16 6561.84 21.1585 -2 2 -7 -12 6561.84 21.1585 1 -2 7 11 2400.99 24.4391 1 -2 2 15 6528.11 34.9554 -2 2 -7 -10 6528.11 34.9554 1 2 -7 -9 0.54609 4.30191 1 -2 1 14 7073.22 7.92507 -2 2 -7 -8 7073.22 7.92507 1 2 -7 -7 4199.51 23.0827 1 -2 0 13 395.100 5.60695 -2 2 -7 -6 395.100 5.60695 1 2 -7 -5 14.2823 4.64817 1 -2 -1 12 180.711 3.62853 -2 2 -7 -4 180.711 3.62853 1 2 -7 -3 13534.9 31.6333 1 -2 -2 11 713.950 10.2490 -2 2 -7 -2 713.950 10.2490 1 2 -7 -1 73.8711 3.44926 1 -2 -3 10 1696.21 10.1827 -2 2 -7 0 1696.21 10.1827 1 2 -7 1 4245.35 13.1682 1 -2 -4 9 2619.77 10.5477 -2 2 -7 2 2619.77 10.5477 1 -2 7 -3 17754.9 23.1263 1 -2 -5 8 262.476 4.28961 -2 2 -7 4 262.476 4.28961 1 2 -7 5 451.981 5.04853 1 -2 -6 7 555.016 7.42327 -2 2 -7 6 555.016 7.42327 1 -2 7 -7 8129.01 18.6410 1 2 7 -6 59.3672 4.10020 -2 -2 7 -8 59.3672 4.10020 1 2 -7 9 1797.73 11.7145 1 -2 -7 5 2030.45 18.8384 -2 2 -7 9 2030.45 18.8384 1 -2 -8 5 1044.26 7.69788 -2 2 -7 10 1044.26 7.69788 1 2 -7 11 1027.18 12.4785 1 -2 -8 4 1886.37 13.6928 -2 2 -7 11 1886.37 13.6928 1 -2 -9 4 1447.18 9.99224 -2 2 -7 12 1447.18 9.99224 1 -2 7 -13 94.4346 13.2005 1 -2 -9 3 155.153 5.42345 -2 2 -7 13 155.153 5.42345 1 2 10 -3 2125.62 12.2437 -2 -2 7 -14 2125.62 12.2437 1 -2 7 -15 421.360 17.0464 1 -2 -10 2 484.269 6.80233 -2 2 -7 15 484.269 6.80233 1 -2 -11 2 3005.72 13.5887 -2 2 -7 16 3005.72 13.5887 1 -2 7 -17 216.224 17.9634 1 -2 -11 1 180.314 4.94439 -2 2 -7 17 180.314 4.94439 1 -2 7 -18 43.7530 15.6286 1 2 12 -1 125.333 6.79984 -2 -2 7 -18 125.333 6.79984 1 2 12 0 1383.91 12.6746 -2 -2 7 -19 1383.91 12.6746 1 -2 7 -20 119.757 20.2194 1 2 13 0 181.893 7.50422 -2 -2 7 -20 181.893 7.50422 1 -2 -13 -1 877.057 11.7176 -2 2 -7 21 877.057 11.7176 1 2 -7 22 10.9330 10.8184 1 -2 -14 -1 49.2156 6.64062 -2 2 -7 22 49.2156 6.64062 1 2 14 2 132.615 7.28089 -2 -2 7 -23 132.615 7.28089 1 2 -7 24 1712.28 20.5788 1 -2 -15 -2 2070.78 22.6757 -2 2 -7 24 2070.78 22.6757 1 2 15 3 1089.52 17.1206 -2 -2 7 -25 1089.52 17.1206 1 2 -7 26 171.674 12.0150 1 2 16 3 184.814 12.6877 -2 -2 7 -26 184.814 12.6877 1 2 16 4 1135.81 18.2714 -2 -2 7 -27 1135.81 18.2714 1 -2 7 -28 1119.90 23.8504 1 2 17 4 1319.41 27.5914 -2 -2 7 -28 1319.41 27.5914 1 -2 -17 -5 12.9928 7.06155 -2 2 -7 29 12.9928 7.06155 1 2 -7 30 358.412 16.3814 1 2 18 5 451.997 29.0025 -2 -2 7 -30 451.997 29.0025 1 -2 -18 -6 52.0971 8.38787 -2 2 -7 31 52.0971 8.38787 1 2 -7 32 752.914 21.6627 1 2 19 6 934.486 41.2566 -2 -2 7 -32 934.486 41.2566 1 -2 -19 -7 10.0837 5.47947 -2 2 -7 33 10.0837 5.47947 1 2 -7 34 49.4005 13.2891 1 -2 -20 -7 109.105 26.1913 -2 2 -7 34 109.105 26.1913 1 2 20 8 744.859 10.4368 -2 -2 7 -35 744.859 10.4368 1 2 -7 36 128.249 17.4445 1 2 21 8 136.323 36.2687 -2 -2 7 -36 136.323 36.2687 1 2 21 9 11.8651 6.13113 -2 -2 7 -37 11.8651 6.13113 1 2 -7 38 3.27511 15.5331 1 2 22 10 41.1909 9.75496 -2 -2 7 -39 41.1909 9.75496 1 -2 7 -40 46.1244 21.6316 1 2 22 11 116.680 37.7248 -2 -2 7 -40 116.680 37.7248 1 -2 16 28 13.1789 18.3451 -2 2 -6 -38 13.1789 18.3451 1 2 -16 -27 337.922 20.7451 -2 -2 6 37 337.922 20.7451 1 2 -15 -27 21.9640 16.6856 -2 -2 6 36 21.9640 16.6856 1 2 -15 -26 13.4196 7.11783 -2 -2 6 35 13.4196 7.11783 1 2 -14 -26 315.205 20.8384 -2 -2 6 34 315.205 20.8384 1 -2 14 25 13.9896 9.57052 -2 2 -6 -33 13.9896 9.57052 1 -2 13 25 297.345 19.1314 -2 2 -6 -32 297.345 19.1314 1 -2 13 24 88.3279 16.0931 -2 2 -6 -31 88.3279 16.0931 1 -2 12 24 868.430 23.1494 -2 2 -6 -30 868.430 23.1494 1 2 -12 -23 201.501 17.6548 -2 -2 6 29 201.501 17.6548 1 -2 11 23 325.114 17.1621 -2 2 -6 -28 325.114 17.1621 1 2 -11 -22 13.1117 7.50511 -2 -2 6 27 13.1117 7.50511 1 -2 6 26 9.94163 26.9712 1 -2 10 22 33.7526 9.08663 -2 2 -6 -26 33.7526 9.08663 1 2 -10 -21 782.894 19.7495 -2 -2 6 25 782.894 19.7495 1 -2 6 24 22.8383 27.1934 1 -2 9 21 115.943 12.5713 -2 2 -6 -24 115.943 12.5713 1 2 -9 -20 14.4447 7.41784 -2 -2 6 23 14.4447 7.41784 1 -2 6 22 67.5615 37.1577 1 2 -8 -20 60.0629 12.8270 -2 -2 6 22 60.0629 12.8270 1 2 -8 -19 1370.83 27.6389 -2 -2 6 21 1370.83 27.6389 1 -2 6 20 808.796 16.4108 1 2 -7 -19 1988.06 33.6672 -2 -2 6 20 1988.06 33.6672 1 -2 6 19 4.42775 5.27295 1 -2 7 18 8.77546 2.71345 -2 2 -6 -19 8.77546 2.71345 1 2 -6 -18 1759.69 17.9850 1 -2 6 18 2274.26 34.5290 -2 2 -6 -18 2274.26 34.5290 1 2 -6 -17 176.872 9.78239 -2 -2 6 17 176.872 9.78239 1 -2 6 16 2395.33 20.9984 1 -2 5 17 2579.87 47.7856 -2 2 -6 -16 2579.87 47.7856 1 -2 5 16 777.262 10.3843 -2 2 -6 -15 777.262 10.3843 1 2 -6 -14 34.5359 7.34415 1 -2 4 16 71.7187 19.1264 -2 2 -6 -14 71.7187 19.1264 1 2 -4 -15 1506.27 16.6917 -2 -2 6 13 1506.27 16.6917 1 2 -6 -12 319.155 7.52885 1 -2 3 14 138.195 4.57035 -2 2 -6 -11 138.195 4.57035 1 2 -6 -10 2028.30 15.3475 1 -2 2 13 4820.33 8.73204 -2 2 -6 -9 4820.33 8.73204 1 2 -6 -8 6086.31 20.8435 1 -2 1 12 16202.8 27.2261 -2 2 -6 -7 16202.8 27.2261 1 2 -6 -6 842.054 11.5003 1 -2 0 11 2510.15 22.5510 -2 2 -6 -5 2510.15 22.5510 1 2 -6 -4 4815.46 17.1041 1 -2 -1 10 56.9541 4.56207 -2 2 -6 -3 56.9541 4.56207 1 -2 6 2 2580.23 12.9295 1 -2 -2 9 3718.01 17.5699 -2 2 -6 -1 3718.01 17.5699 1 2 -6 0 1639.55 9.16290 1 -2 -3 8 35918.2 36.8499 -2 2 -6 1 35918.2 36.8499 1 2 -6 2 146.295 2.94890 1 2 4 -7 4913.57 12.6645 -2 -2 6 -3 4913.57 12.6645 1 -2 6 -4 80.6915 2.81179 1 2 5 -6 1357.94 9.46501 -2 -2 6 -5 1357.94 9.46501 1 -2 6 -6 166.857 3.96968 1 2 6 -5 235.074 4.47506 -2 -2 6 -7 235.074 4.47506 1 -2 6 -8 369.419 5.45089 1 -2 -6 4 348.383 14.7742 -2 2 -6 8 348.383 14.7742 1 -2 -7 4 1367.68 10.6122 -2 2 -6 9 1367.68 10.6122 1 -2 6 -10 4619.57 34.3385 1 -2 -7 3 5033.03 20.1206 -2 2 -6 10 5033.03 20.1206 1 -2 6 -11 28.9502 7.24931 1 -2 -8 3 197.416 4.69339 -2 2 -6 11 197.416 4.69339 1 2 -6 12 64.6385 6.82468 1 -2 -8 2 274.528 5.15014 -2 2 -6 12 274.528 5.15014 1 2 9 -2 642.848 6.49015 -2 -2 6 -13 642.848 6.49015 1 -2 6 -14 2010.78 27.9503 1 -2 -9 1 2583.95 12.7259 -2 2 -6 14 2583.95 12.7259 1 2 10 -1 8.99339 2.79908 -2 -2 6 -15 8.99339 2.79908 1 -2 6 -16 132.948 15.4354 1 -2 -10 0 105.870 5.97183 -2 2 -6 16 105.870 5.97183 1 2 -6 17 587.931 46.5339 1 -2 -11 0 571.271 8.38553 -2 2 -6 17 571.271 8.38553 1 -2 -11 -1 211.106 7.26710 -2 2 -6 18 211.106 7.26710 1 -2 6 -19 2999.47 52.9498 1 2 12 1 3155.26 17.2201 -2 -2 6 -19 3155.26 17.2201 1 2 12 2 2250.72 15.8811 -2 -2 6 -20 2250.72 15.8811 1 -2 6 -21 1162.12 28.7920 1 -2 -13 -2 1178.42 11.1761 -2 2 -6 21 1178.42 11.1761 1 -2 -13 -3 49.1954 4.59121 -2 2 -6 22 49.1954 4.59121 1 2 -6 23 79.1270 7.09889 1 2 14 3 222.566 11.5116 -2 -2 6 -23 222.566 11.5116 1 2 14 4 1190.57 17.6399 -2 -2 6 -24 1190.57 17.6399 1 -2 6 -25 12.3967 10.4952 1 2 15 4 28.3989 12.1122 -2 -2 6 -25 28.3989 12.1122 1 -2 -15 -5 1837.49 23.2235 -2 2 -6 26 1837.49 23.2235 1 2 -6 27 30.8575 12.2558 1 2 16 5 70.6930 11.4660 -2 -2 6 -27 70.6930 11.4660 1 -2 -16 -6 152.526 12.2828 -2 2 -6 28 152.526 12.2828 1 2 -6 29 136.454 9.91185 1 2 17 6 251.361 32.3368 -2 -2 6 -29 251.361 32.3368 1 -2 -17 -7 26.9132 4.03753 -2 2 -6 30 26.9132 4.03753 1 2 -6 31 170.647 14.5704 1 -2 -18 -7 273.089 29.7550 -2 2 -6 31 273.089 29.7550 1 2 18 8 2.62977 5.70102 -2 -2 6 -32 2.62977 5.70102 1 2 -6 33 143.142 13.7838 1 2 19 8 204.319 29.9647 -2 -2 6 -33 204.319 29.9647 1 2 19 9 61.9593 7.61007 -2 -2 6 -34 61.9593 7.61007 1 2 -6 35 251.627 16.2837 1 2 20 9 293.250 59.1236 -2 -2 6 -35 293.250 59.1236 1 -2 -20 -10 25.7661 4.72999 -2 2 -6 36 25.7661 4.72999 1 2 -6 37-0.80078 13.7088 1 2 21 11 48.3032 4.39284 -2 -2 6 -38 48.3032 4.39284 1 -2 6 -39 503.395 25.2013 1 2 21 12 798.297 57.6074 -2 -2 6 -39 798.297 57.6074 1 2 22 12 283.364 9.73110 -2 -2 6 -40 283.364 9.73110 1 2 -17 -26 238.438 20.8103 -2 -2 5 38 238.438 20.8103 1 2 -16 -26 19.6955 12.4850 -2 -2 5 37 19.6955 12.4850 1 -2 16 25 32.9984 16.8228 -2 2 -5 -36 32.9984 16.8228 1 2 -15 -25 12.0374 11.4884 -2 -2 5 35 12.0374 11.4884 1 -2 15 24 739.450 24.4467 -2 2 -5 -34 739.450 24.4467 1 -2 14 24 97.0237 16.0935 -2 2 -5 -33 97.0237 16.0935 1 -2 14 23 37.1015 8.33930 -2 2 -5 -32 37.1015 8.33930 1 -2 13 23 862.975 23.4531 -2 2 -5 -31 862.975 23.4531 1 2 -13 -22 52.0219 11.2017 -2 -2 5 30 52.0219 11.2017 1 -2 5 29 367.938 43.9304 1 2 -12 -22 536.131 18.0273 -2 -2 5 29 536.131 18.0273 1 -2 12 21 69.9924 12.4812 -2 2 -5 -28 69.9924 12.4812 1 -2 5 27 213.237 35.2589 1 -2 11 21 204.353 13.7096 -2 2 -5 -27 204.353 13.7096 1 2 -11 -20 279.405 14.4260 -2 -2 5 26 279.405 14.4260 1 -2 5 25 193.181 32.3068 1 2 -10 -20 255.180 14.2187 -2 -2 5 25 255.180 14.2187 1 -2 10 19 15.0840 5.04561 -2 2 -5 -24 15.0840 5.04561 1 -2 5 23 53.7807 24.4577 1 2 -9 -19 121.826 12.9269 -2 -2 5 23 121.826 12.9269 1 2 -9 -18 2566.43 32.7777 -2 -2 5 22 2566.43 32.7777 1 2 -5 -21 1241.90 49.4430 1 2 -8 -18 1404.08 24.5578 -2 -2 5 21 1404.08 24.5578 1 2 -8 -17 40.3790 8.56971 -2 -2 5 20 40.3790 8.56971 1 -2 5 19 206.872 6.15760 1 -2 7 17 545.779 25.6961 -2 2 -5 -19 545.779 25.6961 1 2 -7 -16 3438.96 24.6657 -2 -2 5 18 3438.96 24.6657 1 -2 5 17 510.209 8.95189 1 -2 6 16 1057.33 35.4239 -2 2 -5 -17 1057.33 35.4239 1 2 -6 -15 921.500 14.1506 -2 -2 5 16 921.500 14.1506 1 -2 5 15 62.4855 5.88800 1 -2 5 15 109.378 25.3824 -2 2 -5 -15 109.378 25.3824 1 2 -5 -14 3.36902 1.68779 -2 -2 5 14 3.36902 1.68779 1 2 -5 -13 4198.58 23.2051 1 -2 4 13 474.130 6.29532 -2 2 -5 -12 474.130 6.29532 1 -2 5 11 763.786 11.7107 1 -2 3 12 283.565 3.55936 -2 2 -5 -10 283.565 3.55936 1 2 -5 -9 15113.0 39.6891 1 -2 2 11 12238.3 24.2314 -2 2 -5 -8 12238.3 24.2314 1 2 -5 -7 2259.53 13.7139 1 2 -1 -10 13055.6 39.1374 -2 -2 5 6 13055.6 39.1374 1 -2 5 5 2482.57 13.2152 1 2 0 -9 3994.86 14.3379 -2 -2 5 4 3994.86 14.3379 1 -2 5 3 5836.33 16.4270 1 -2 -1 8 1166.08 9.56489 -2 2 -5 -2 1166.08 9.56489 1 2 -5 -1 31925.8 35.7016 1 -2 -2 7 2192.85 9.79666 -2 2 -5 0 2192.85 9.79666 1 -2 5 -1 3246.07 10.1856 1 2 3 -6 24548.1 25.9689 -2 -2 5 -2 24548.1 25.9689 1 -2 5 -3 4149.32 8.93272 1 2 -5 4 3788.03 38.5171 1 -2 -4 5 4954.84 14.3102 -2 2 -5 4 4954.84 14.3102 1 2 -5 5 81.3582 2.62092 1 -2 -5 4 9138.35 19.1070 -2 2 -5 6 9138.35 19.1070 1 2 -5 7 86.9759 3.08957 1 -2 -5 3 125.671 9.12694 -2 2 -5 7 125.671 9.12694 1 -2 5 -8 2703.92 23.5423 1 -2 -6 3 3402.19 13.5095 -2 2 -5 8 3402.19 13.5095 1 -2 5 -9 236.127 5.13290 1 -2 -6 2 746.854 9.97404 -2 2 -5 9 746.854 9.97404 1 -2 5 -10 85.5331 8.59775 1 -2 -7 2 183.587 5.06289 -2 2 -5 10 183.587 5.06289 1 -2 5 -11 1547.99 12.8973 1 -2 -7 1 1768.54 9.86307 -2 2 -5 11 1768.54 9.86307 1 2 -5 12 336.811 12.1543 1 -2 -8 1 459.054 5.77601 -2 2 -5 12 459.054 5.77601 1 2 -5 13 794.043 12.6507 1 -2 -8 0 1251.28 9.70302 -2 2 -5 13 1251.28 9.70302 1 2 -5 14 7.09110 14.8081 1 -2 -9 0 75.6003 4.48586 -2 2 -5 14 75.6003 4.48586 1 -2 5 -15 109.685 14.8429 1 -2 -9 -1 125.368 5.47329 -2 2 -5 15 125.368 5.47329 1 2 -5 16 16.7479 16.0511 1 -2 -10 -1 104.714 5.86324 -2 2 -5 16 104.714 5.86324 1 -2 -10 -2 6889.58 23.0950 -2 2 -5 17 6889.58 23.0950 1 2 -5 18 3280.70 42.9025 1 2 11 2 3787.70 17.9040 -2 -2 5 -18 3787.70 17.9040 1 2 11 3 3976.41 20.0441 -2 -2 5 -19 3976.41 20.0441 1 -2 5 -20 1780.92 16.4868 1 -2 -12 -3 2322.39 17.6610 -2 2 -5 20 2322.39 17.6610 1 2 -5 21 271.575 35.6520 1 2 12 4 237.721 5.72514 -2 -2 5 -21 237.721 5.72514 1 2 -5 22 169.972 11.2245 1 2 13 4 198.752 10.5269 -2 -2 5 -22 198.752 10.5269 1 2 -5 23 874.429 58.7700 1 -2 -13 -5 847.980 15.2999 -2 2 -5 23 847.980 15.2999 1 2 -5 24-0.77008 8.70208 1 -2 -14 -5 1.15300 4.19607 -2 2 -5 24 1.15300 4.19607 1 2 -5 25 375.389 43.4957 1 -2 -14 -6 385.665 12.4625 -2 2 -5 25 385.665 12.4625 1 -2 5 -26 566.002 14.5935 1 2 15 6 638.185 20.7123 -2 -2 5 -26 638.185 20.7123 1 2 15 7 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26.9476 1 -7 3 -1 396.599 9.33176 1 -7 0 2 434.432 20.0587 -2 7 -3 1 434.432 20.0587 1 -7 3 -2 516.408 11.6781 1 -7 0 1 445.529 10.5196 -2 7 -3 2 445.529 10.5196 1 -7 3 -3 494.608 7.33573 1 -7 -1 0 1861.24 16.0767 -2 7 -3 4 1861.24 16.0767 1 7 -3 5 141.855 4.55792 1 -7 -2 0 378.966 37.2737 -2 7 -3 5 378.966 37.2737 1 -7 -2 -1 702.463 11.6365 -2 7 -3 6 702.463 11.6365 1 7 -3 7 8.61839 3.58875 1 7 3 2 40.1155 3.18278 -2 -7 3 -8 40.1155 3.18278 1 7 -3 9 8112.23 27.3324 1 -7 -4 -3 22.5310 2.51984 -2 7 -3 10 22.5310 2.51984 1 -7 3 -11 2328.24 16.8403 1 7 5 4 28.5518 2.49281 -2 -7 3 -12 28.5518 2.49281 1 -7 3 -13 2023.06 16.0524 1 -7 -6 -5 1015.28 7.36831 -2 7 -3 14 1015.28 7.36831 1 -7 3 -15 32.8209 5.36321 1 -7 -7 -5 81.2965 28.0893 -2 7 -3 15 81.2965 28.0893 1 -7 -7 -6 1417.60 6.59973 -2 7 -3 16 1417.60 6.59973 1 -7 3 -17 21.0007 5.15269 1 -7 -8 -6 185.350 28.8611 -2 7 -3 17 185.350 28.8611 1 7 8 7 370.469 3.82922 -2 -7 3 -18 370.469 3.82922 1 7 -3 19-0.71028 5.74031 1 -7 -8 -8 111.693 44.7312 -2 7 -3 19 111.693 44.7312 1 7 9 8 246.453 3.63572 -2 -7 3 -20 246.453 3.63572 1 7 -3 21 55.5346 6.90931 1 -7 -9 -9 83.3315 46.0186 -2 7 -3 21 83.3315 46.0186 1 -7 -10 -9 375.274 14.6463 -2 7 -3 22 375.274 14.6463 1 7 -3 23 6.21157 8.25182 1 7 10 10 40.9248 23.1661 -2 -7 3 -23 40.9248 23.1661 1 -7 -11 -10 278.314 16.6545 -2 7 -3 24 278.314 16.6545 1 7 -3 25 167.468 14.4795 1 7 11 11 271.324 26.5311 -2 -7 3 -25 271.324 26.5311 1 -7 -12 -11 40.1172 6.79819 -2 7 -3 26 40.1172 6.79819 1 7 -3 27 35.6349 18.0648 1 7 12 12 89.5838 20.2012 -2 -7 3 -27 89.5838 20.2012 1 7 13 12 377.064 20.7974 -2 -7 3 -28 377.064 20.7974 1 7 13 13 32.0670 16.9365 -2 -7 3 -29 32.0670 16.9365 1 -7 -14 -13 517.932 25.8234 -2 7 -3 30 517.932 25.8234 1 -7 -14 -14 14.3085 8.94808 -2 7 -3 31 14.3085 8.94808 1 7 15 14 18.9254 18.1869 -2 -7 3 -32 18.9254 18.1869 1 7 15 15 59.2064 21.9331 -2 -7 3 -33 59.2064 21.9331 1 -7 -16 -15 77.4819 11.4949 -2 7 -3 34 77.4819 11.4949 1 7 16 16 33.0911 11.9905 -2 -7 3 -35 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1 7 -13 -13 238.618 12.9579 -2 -7 2 24 238.618 12.9579 1 -7 2 23 987.253 15.7842 1 7 -13 -12 1243.26 27.8714 -2 -7 2 23 1243.26 27.8714 1 -7 12 12 19.9533 3.81504 -2 7 -2 -22 19.9533 3.81504 1 7 -2 -21 805.474 13.0653 1 -7 12 11 1059.34 42.0521 -2 7 -2 -21 1059.34 42.0521 1 7 -11 -11 945.984 16.2918 -2 -7 2 20 945.984 16.2918 1 -7 2 19 154.440 8.32706 1 7 -11 -10 183.044 15.2018 -2 -7 2 19 183.044 15.2018 1 7 -10 -10 2773.42 24.4261 -2 -7 2 18 2773.42 24.4261 1 -7 2 17 1299.03 16.0500 1 -7 10 9 1274.10 32.1281 -2 7 -2 -17 1274.10 32.1281 1 7 -9 -9 1286.68 18.5213 -2 -7 2 16 1286.68 18.5213 1 7 -2 -15 97.8337 9.70534 1 -7 9 8 94.0851 9.62023 -2 7 -2 -15 94.0851 9.62023 1 -7 8 8 1001.55 11.7245 -2 7 -2 -14 1001.55 11.7245 1 -7 2 13 127.740 7.42777 1 -7 8 7 153.216 7.57422 -2 7 -2 -13 153.216 7.57422 1 7 -7 -7 234.796 7.24309 -2 -7 2 12 234.796 7.24309 1 -7 2 11 229.366 7.07748 1 7 -7 -6 209.749 11.4514 -2 -7 2 11 209.749 11.4514 1 -7 2 10 57.2994 7.76366 1 7 -6 -6 113.088 6.66850 -2 -7 2 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809.800 30.7605 -2 7 -1 -36 809.800 30.7605 1 -7 19 17 16.7063 4.80833 -2 7 -1 -35 16.7063 4.80833 1 7 -1 -34 16.0604 15.4590 1 -7 18 17 12.5495 7.64430 -2 7 -1 -34 12.5495 7.64430 1 -7 18 16 23.4489 15.5036 -2 7 -1 -33 23.4489 15.5036 1 7 -1 -32 327.416 15.4390 1 -7 17 15 105.934 6.36973 -2 7 -1 -31 105.934 6.36973 1 7 -1 -30 20.6377 10.0122 1 -7 16 14 144.212 4.53680 -2 7 -1 -29 144.212 4.53680 1 7 -1 -28 32.0687 12.3504 1 -7 16 13 6.88928 24.3942 -2 7 -1 -28 6.88928 24.3942 1 -7 15 13 2316.34 37.1362 -2 7 -1 -27 2316.34 37.1362 1 7 -1 -26 9.01004 10.7913 1 7 -15 -12-1.89014 36.9911 -2 -7 1 26-1.89014 36.9911 1 7 -14 -12 1114.60 22.7449 -2 -7 1 25 1114.60 22.7449 1 7 -1 -24 945.843 20.3045 1 7 -14 -11 926.276 29.2509 -2 -7 1 24 926.276 29.2509 1 7 -13 -11 391.797 14.0032 -2 -7 1 23 391.797 14.0032 1 7 -1 -22 336.261 10.0382 1 -7 13 10 422.567 14.2898 -2 7 -1 -22 422.567 14.2898 1 -7 12 10 32.9582 5.80631 -2 7 -1 -21 32.9582 5.80631 1 7 -1 -20 1853.80 20.5236 1 -7 12 9 2501.45 28.5443 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13-3.36234 3.53905 -2 7 0 -30-3.36234 3.53905 1 7 0 -29 159.026 15.2300 1 -7 17 12 283.056 29.5336 -2 7 0 -29 283.056 29.5336 1 -7 16 12 443.142 20.8520 -2 7 0 -28 443.142 20.8520 1 7 0 -27 45.5986 12.8681 1 -7 16 11 69.5145 24.2499 -2 7 0 -27 69.5145 24.2499 1 -7 15 11 952.128 24.3728 -2 7 0 -26 952.128 24.3728 1 7 0 -25 18.7413 10.5051 1 -7 15 10 19.9266 20.9262 -2 7 0 -25 19.9266 20.9262 1 7 -14 -10 294.888 12.6366 -2 -7 0 24 294.888 12.6366 1 7 0 -23 83.0069 10.2149 1 -7 14 9 155.506 14.1683 -2 7 0 -23 155.506 14.1683 1 7 -13 -9 209.681 10.7655 -2 -7 0 22 209.681 10.7655 1 7 0 -21 498.146 15.4130 1 -7 13 8 494.639 14.9520 -2 7 0 -21 494.639 14.9520 1 7 -12 -8 700.501 12.1686 -2 -7 0 20 700.501 12.1686 1 7 0 -19 2223.68 21.3543 1 -7 12 7 2615.98 28.1653 -2 7 0 -19 2615.98 28.1653 1 -7 11 7 1118.87 14.0647 -2 7 0 -18 1118.87 14.0647 1 7 0 -17 6072.91 39.1507 1 -7 11 6 6828.99 31.0968 -2 7 0 -17 6828.99 31.0968 1 -7 10 6 59.2674 5.07804 -2 7 0 -16 59.2674 5.07804 1 -7 0 15 177.416 7.44970 1 -7 10 5 363.494 14.7095 -2 7 0 -15 363.494 14.7095 1 7 0 -14 661.105 31.0155 1 7 -9 -5 895.729 11.7823 -2 -7 0 14 895.729 11.7823 1 -7 0 13 12.5276 4.94770 1 -7 9 4 40.7144 6.66441 -2 7 0 -13 40.7144 6.66441 1 7 0 -12 776.098 34.4894 1 7 -8 -4 839.079 13.3733 -2 -7 0 12 839.079 13.3733 1 -7 0 11 967.335 11.5389 1 -7 8 3 1852.83 23.2357 -2 7 0 -11 1852.83 23.2357 1 -7 0 10 899.742 20.9273 1 7 -7 -3 1045.99 15.9469 -2 -7 0 10 1045.99 15.9469 1 -7 0 9 1351.40 20.2725 1 -7 7 2 1578.73 18.2787 -2 7 0 -9 1578.73 18.2787 1 -7 0 8 3213.91 26.6405 1 7 -6 -2 3472.04 21.0518 -2 -7 0 8 3472.04 21.0518 1 -7 0 7 835.624 21.4167 1 7 -6 -1 908.322 10.4303 -2 -7 0 7 908.322 10.4303 1 -7 0 6 1482.25 14.5051 1 -7 5 1 1584.78 18.7609 -2 7 0 -6 1584.78 18.7609 1 -7 0 5 238.443 26.0213 1 7 -5 0 292.319 6.82925 -2 -7 0 5 292.319 6.82925 1 -7 0 4 179.257 5.48947 1 7 -4 0 210.186 9.14892 -2 -7 0 4 210.186 9.14892 1 7 -4 1 10116.3 27.5054 -2 -7 0 3 10116.3 27.5054 1 -7 0 2 46.1884 4.62561 1 -7 3 -1 105.596 22.8397 -2 7 0 -2 105.596 22.8397 1 7 0 -1 14.2021 6.92189 1 7 -3 2 87.4153 6.27719 -2 -7 0 1 87.4153 6.27719 1 -7 0 0 1056.91 11.0920 1 -7 2 -2 1754.14 55.9166 -2 7 0 0 1754.14 55.9166 1 -7 2 -3 1237.25 13.0019 -2 7 0 1 1237.25 13.0019 1 7 0 2 545.750 8.55214 1 7 -1 3 740.691 16.4590 -2 -7 0 -2 740.691 16.4590 1 -7 1 -4 833.829 9.43121 -2 7 0 3 833.829 9.43121 1 -7 0 -4 144.924 4.32526 1 -7 0 -4 155.246 16.0451 -2 7 0 4 155.246 16.0451 1 7 0 5 145.388 5.58534 -2 -7 0 -5 145.388 5.58534 1 -7 0 -6 6520.64 20.0610 1 7 1 6 293.536 5.93614 -2 -7 0 -7 293.536 5.93614 1 7 0 8 198.254 6.81828 1 7 2 7 4153.83 10.9521 -2 -7 0 -9 4153.83 10.9521 1 7 0 10 1311.04 11.6975 1 7 3 8 301.432 4.44122 -2 -7 0 -11 301.432 4.44122 1 -7 0 -12 511.544 9.80198 1 7 4 8 568.965 43.8143 -2 -7 0 -12 568.965 43.8143 1 7 4 9 1547.37 5.58921 -2 -7 0 -13 1547.37 5.58921 1 7 0 14 103.841 6.61904 1 -7 -5 -10 25.8612 2.68722 -2 7 0 15 25.8612 2.68722 1 7 0 16 207.538 7.93224 1 7 6 11 35.3963 2.59506 -2 -7 0 -17 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858.060 28.4480 -2 -7 -4 -20 858.060 28.4480 1 7 6 19 3.66140 7.91697 -2 -7 -4 -21 3.66140 7.91697 1 7 4 22 521.460 27.2404 1 7 6 20 692.801 25.2944 -2 -7 -4 -22 692.801 25.2944 1 7 7 20 169.069 16.0872 -2 -7 -4 -23 169.069 16.0872 1 -7 -4 -24 114.508 24.7852 1 7 7 21 152.294 21.4130 -2 -7 -4 -24 152.294 21.4130 1 -7 -8 -21 70.1571 17.3391 -2 7 4 25 70.1571 17.3391 1 7 8 22 40.3748 17.9035 -2 -7 -4 -26 40.3748 17.9035 1 -7 -9 -22 676.041 27.5176 -2 7 4 27 676.041 27.5176 1 -7 -9 -23 123.912 20.2469 -2 7 4 28 123.912 20.2469 1 7 10 23 59.7936 22.2650 -2 -7 -4 -29 59.7936 22.2650 1 -7 -10 -24 162.988 13.7412 -2 7 4 30 162.988 13.7412 1 7 11 24 53.2333 22.5190 -2 -7 -4 -31 53.2333 22.5190 1 -7 25 11 21.6531 10.6913 -2 7 5 -41 21.6531 10.6913 1 7 5 -40 23.3242 16.1267 1 7 -24 -11 77.0064 40.2664 -2 -7 -5 40 77.0064 40.2664 1 -7 24 10 38.6790 7.23452 -2 7 5 -39 38.6790 7.23452 1 7 5 -38 173.879 13.9080 1 -7 23 9 278.452 5.62756 -2 7 5 -37 278.452 5.62756 1 7 5 -36 66.4824 12.7376 1 -7 22 8 59.4476 3.80457 -2 7 5 -35 59.4476 3.80457 1 -7 -5 34 30.6190 11.7909 1 7 -21 -7 46.0575 6.89829 -2 -7 -5 33 46.0575 6.89829 1 7 5 -32-0.57219 12.5183 1 -7 21 6-21.9275 38.7061 -2 7 5 -32-21.9275 38.7061 1 -7 20 6 32.4662 6.26955 -2 7 5 -31 32.4662 6.26955 1 7 5 -30 506.556 20.0339 1 -7 20 5 603.809 50.4504 -2 7 5 -30 603.809 50.4504 1 -7 19 5 6.10600 8.66267 -2 7 5 -29 6.10600 8.66267 1 7 5 -28 32.6721 14.2820 1 -7 19 4 14.7639 19.9002 -2 7 5 -28 14.7639 19.9002 1 -7 18 4 601.201 22.1975 -2 7 5 -27 601.201 22.1975 1 7 5 -26 357.612 18.2569 1 -7 18 3 388.255 29.9040 -2 7 5 -26 388.255 29.9040 1 -7 17 3 1892.90 27.9529 -2 7 5 -25 1892.90 27.9529 1 7 5 -24 11.0304 15.0958 1 -7 17 2 12.2314 13.5284 -2 7 5 -24 12.2314 13.5284 1 -7 16 2 83.6320 11.9650 -2 7 5 -23 83.6320 11.9650 1 7 5 -22 330.339 45.2847 1 -7 16 1 385.307 13.9139 -2 7 5 -22 385.307 13.9139 1 -7 15 1 798.236 18.1172 -2 7 5 -21 798.236 18.1172 1 7 5 -20 0.62947 16.2132 1 7 -15 0 51.5003 10.8806 -2 -7 -5 20 51.5003 10.8806 1 7 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9.28447 1 7 5 -5 3597.23 19.6109 1 7 -7 7 4149.49 30.3535 -2 -7 -5 5 4149.49 30.3535 1 -7 7 -8 9661.08 34.8334 -2 7 5 -4 9661.08 34.8334 1 -7 -5 3 507.060 10.0384 1 -7 6 -8 559.381 22.6960 -2 7 5 -3 559.381 22.6960 1 -7 6 -9 613.559 11.6323 -2 7 5 -2 613.559 11.6323 1 -7 -5 1 6.24935 5.18002 1 -7 5 -9 192.376 21.4113 -2 7 5 -1 192.376 21.4113 1 7 -5 10 14879.2 38.9412 -2 -7 -5 0 14879.2 38.9412 1 -7 -5 -1 1328.20 10.8468 1 -7 4 -10 2231.99 61.2605 -2 7 5 1 2231.99 61.2605 1 7 -4 11 309.449 5.68439 -2 -7 -5 -2 309.449 5.68439 1 -7 -5 -3 6658.80 26.1239 1 -7 3 -11 7376.19 109.495 -2 7 5 3 7376.19 109.495 1 7 -3 12 7.96519 1.95445 -2 -7 -5 -4 7.96519 1.95445 1 -7 -5 -5 2268.85 15.3732 1 -7 2 -12 2422.08 74.2488 -2 7 5 5 2422.08 74.2488 1 7 -2 13 142.188 2.23171 -2 -7 -5 -6 142.188 2.23171 1 7 5 7 240.379 5.99103 1 7 -1 13 321.501 29.8151 -2 -7 -5 -7 321.501 29.8151 1 -7 1 -14 1594.92 6.00088 -2 7 5 8 1594.92 6.00088 1 7 5 9 931.111 12.0473 1 7 0 15 64.4210 2.32123 -2 -7 -5 -10 64.4210 2.32123 1 -7 -5 -11 148.835 8.02937 1 -7 0 -16 214.741 16.3682 -2 7 5 11 214.741 16.3682 1 7 1 16 369.270 5.26001 -2 -7 -5 -12 369.270 5.26001 1 -7 -5 -13 77.4823 8.66101 1 7 1 17 79.2485 12.0143 -2 -7 -5 -13 79.2485 12.0143 1 7 2 17 2151.85 22.6851 -2 -7 -5 -14 2151.85 22.6851 1 -7 -5 -15 41.0961 9.75913 1 7 2 18 18.2378 6.37666 -2 -7 -5 -15 18.2378 6.37666 1 7 3 18 305.047 14.4643 -2 -7 -5 -16 305.047 14.4643 1 -7 -5 -17 983.435 21.2553 1 7 3 19 1249.31 30.1179 -2 -7 -5 -17 1249.31 30.1179 1 7 4 19 89.7636 12.1874 -2 -7 -5 -18 89.7636 12.1874 1 -7 -5 -19 869.278 22.7205 1 7 4 20 1026.17 30.0796 -2 -7 -5 -19 1026.17 30.0796 1 7 5 20 1.92111 5.34050 -2 -7 -5 -20 1.92111 5.34050 1 7 5 21 468.302 34.5689 1 7 5 21 553.407 23.1005 -2 -7 -5 -21 553.407 23.1005 1 7 6 21 87.0842 16.3230 -2 -7 -5 -22 87.0842 16.3230 1 7 5 23 173.050 32.8342 1 7 6 22 238.416 21.0961 -2 -7 -5 -23 238.416 21.0961 1 7 7 22 61.9074 16.9999 -2 -7 -5 -24 61.9074 16.9999 1 7 5 25 11.5631 27.1945 1 7 7 23 7.35353 7.87197 -2 -7 -5 -25 7.35353 7.87197 1 7 8 23 289.237 21.9539 -2 -7 -5 -26 289.237 21.9539 1 7 8 24 26.6042 23.8522 -2 -7 -5 -27 26.6042 23.8522 1 7 9 24 34.4169 23.1751 -2 -7 -5 -28 34.4169 23.1751 1 7 9 25 94.1205 22.6791 -2 -7 -5 -29 94.1205 22.6791 1 7 10 25 138.390 23.6809 -2 -7 -5 -30 138.390 23.6809 1 7 6 -41-2.95181 15.7496 1 7 -25 -10 13.1008 38.7156 -2 -7 -6 41 13.1008 38.7156 1 -7 25 9 17.4169 6.35400 -2 7 6 -40 17.4169 6.35400 1 7 6 -39 564.837 20.7212 1 -7 24 8 176.769 7.22828 -2 7 6 -38 176.769 7.22828 1 7 6 -37 105.041 13.3074 1 -7 23 7 56.5058 5.70053 -2 7 6 -36 56.5058 5.70053 1 7 6 -35 16.7650 11.6028 1 7 -22 -6 26.3405 5.37542 -2 -7 -6 34 26.3405 5.37542 1 7 6 -33 19.0639 12.5192 1 -7 22 5 19.0213 40.4475 -2 7 6 -33 19.0213 40.4475 1 -7 21 5 204.560 18.8039 -2 7 6 -32 204.560 18.8039 1 7 6 -31 538.843 22.8495 1 -7 21 4 537.425 39.9511 -2 7 6 -31 537.425 39.9511 1 -7 20 4 16.4285 15.9329 -2 7 6 -30 16.4285 15.9329 1 7 6 -29 20.5489 13.5661 1 -7 20 3 24.7994 29.1142 -2 7 6 -29 24.7994 29.1142 1 -7 19 3 22.4193 15.2053 -2 7 6 -28 22.4193 15.2053 1 7 6 -27 20.2355 13.2973 1 -7 19 2 58.4162 24.9184 -2 7 6 -27 58.4162 24.9184 1 -7 18 2 99.7192 12.8092 -2 7 6 -26 99.7192 12.8092 1 7 6 -25 1.86162 20.0787 1 -7 18 1 22.6006 13.2233 -2 7 6 -25 22.6006 13.2233 1 -7 17 1 515.777 17.6944 -2 7 6 -24 515.777 17.6944 1 7 6 -23 206.495 24.8099 1 -7 17 0 202.553 13.9935 -2 7 6 -23 202.553 13.9935 1 -7 16 0 327.056 14.3542 -2 7 6 -22 327.056 14.3542 1 7 6 -21 2.88408 29.2674 1 -7 16 -1 11.1341 4.12470 -2 7 6 -21 11.1341 4.12470 1 -7 15 -1 504.529 15.0953 -2 7 6 -20 504.529 15.0953 1 -7 15 -2 38.6367 10.2966 -2 7 6 -19 38.6367 10.2966 1 -7 14 -2 2909.79 24.9582 -2 7 6 -18 2909.79 24.9582 1 -7 14 -3 29.0323 5.46564 -2 7 6 -17 29.0323 5.46564 1 -7 13 -3 1298.98 15.5635 -2 7 6 -16 1298.98 15.5635 1 -7 13 -4 187.954 10.6447 -2 7 6 -15 187.954 10.6447 1 -7 12 -4 63.3393 5.35102 -2 7 6 -14 63.3393 5.35102 1 7 6 -13 3334.40 40.7173 1 -7 12 -5 4261.27 22.5680 -2 7 6 -13 4261.27 22.5680 1 -7 -6 12 535.696 16.1724 1 -7 11 -5 633.509 9.67607 -2 7 6 -12 633.509 9.67607 1 -7 11 -6 811.246 15.1397 -2 7 6 -11 811.246 15.1397 1 7 6 -10 421.603 13.4761 1 7 -10 6 558.036 14.1512 -2 -7 -6 10 558.036 14.1512 1 -7 10 -7 2602.03 23.6128 -2 7 6 -9 2602.03 23.6128 1 -7 -6 8 2714.44 29.0380 1 -7 9 -7 3433.14 28.8502 -2 7 6 -8 3433.14 28.8502 1 7 -9 8 3161.75 23.9349 -2 -7 -6 7 3161.75 23.9349 1 -7 -6 6 3782.28 23.4949 1 -7 8 -8 4909.39 34.9582 -2 7 6 -6 4909.39 34.9582 1 7 -8 9 300.978 8.04695 -2 -7 -6 5 300.978 8.04695 1 7 6 -4 1684.11 14.9043 1 -7 7 -9 1869.66 33.1859 -2 7 6 -4 1869.66 33.1859 1 7 -7 10 347.117 9.83749 -2 -7 -6 3 347.117 9.83749 1 7 6 -2 879.729 11.7635 1 -7 6 -10 1041.93 40.2403 -2 7 6 -2 1041.93 40.2403 1 -7 6 -11 5909.13 32.4595 -2 7 6 -1 5909.13 32.4595 1 7 6 0 1822.40 11.8732 1 -7 5 -11 2013.80 58.4157 -2 7 6 0 2013.80 58.4157 1 -7 5 -12 633.133 5.67189 -2 7 6 1 633.133 5.67189 1 -7 -6 -2 3345.82 18.2508 1 -7 4 -12 4754.43 49.1028 -2 7 6 2 4754.43 49.1028 1 -7 4 -13 2027.82 6.84285 -2 7 6 3 2027.82 6.84285 1 -7 -6 -4 243.411 6.75653 1 -7 3 -13 681.064 48.2894 -2 7 6 4 681.064 48.2894 1 -7 3 -14 1422.76 4.73624 -2 7 6 5 1422.76 4.73624 1 -7 -6 -6 18.4504 5.81998 1 7 -2 14 29.7251 7.80921 -2 -7 -6 -6 29.7251 7.80921 1 7 -2 15 72.8420 2.60635 -2 -7 -6 -7 72.8420 2.60635 1 7 6 8 1471.25 14.8538 1 7 -1 16 376.402 3.70313 -2 -7 -6 -9 376.402 3.70313 1 -7 -6 -10 284.762 8.54499 1 7 -1 17 277.705 26.1712 -2 -7 -6 -10 277.705 26.1712 1 7 0 17 16.9656 3.24714 -2 -7 -6 -11 16.9656 3.24714 1 -7 -6 -12 538.641 13.1292 1 7 0 18 633.777 21.1836 -2 -7 -6 -12 633.777 21.1836 1 -7 -1 -18 543.157 8.59345 -2 7 6 13 543.157 8.59345 1 -7 -6 -14 141.133 9.29103 1 7 1 19 226.941 22.5519 -2 -7 -6 -14 226.941 22.5519 1 7 2 19 497.020 15.9564 -2 -7 -6 -15 497.020 15.9564 1 -7 -6 -16 473.240 16.7743 1 7 2 20 521.709 21.7731 -2 -7 -6 -16 521.709 21.7731 1 7 3 20 418.750 17.6555 -2 -7 -6 -17 418.750 17.6555 1 7 6 18 193.952 19.9727 1 7 3 21 318.937 20.3534 -2 -7 -6 -18 318.937 20.3534 1 7 4 21 10.5732 13.9111 -2 -7 -6 -19 10.5732 13.9111 1 7 6 20 417.681 28.3642 1 7 4 22 551.533 26.0282 -2 -7 -6 -20 551.533 26.0282 1 -7 -5 -22 53.9389 15.5367 -2 7 6 21 53.9389 15.5367 1 7 6 22 203.179 32.8106 1 7 5 23 277.886 20.2677 -2 -7 -6 -22 277.886 20.2677 1 7 6 23 16.0140 9.72448 -2 -7 -6 -23 16.0140 9.72448 1 7 6 24 49.4891 13.2910 -2 -7 -6 -24 49.4891 13.2910 1 7 7 24 13.6225 7.65465 -2 -7 -6 -25 13.6225 7.65465 1 7 7 25 49.5866 11.1460 -2 -7 -6 -26 49.5866 11.1460 1 7 8 25 25.9311 20.8136 -2 -7 -6 -27 25.9311 20.8136 1 7 8 26 16.1550 11.9541 -2 -7 -6 -28 16.1550 11.9541 1 7 9 26 40.9654 11.4191 -2 -7 -6 -29 40.9654 11.4191 1 7 9 27-1.08864 22.5924 -2 -7 -6 -30-1.08864 22.5924 1 7 7 -40 385.057 19.4226 1 -7 25 7 71.7992 6.24955 -2 7 7 -39 71.7992 6.24955 1 7 7 -38 4.39503 12.5671 1 -7 24 6 29.2700 7.58873 -2 7 7 -37 29.2700 7.58873 1 7 7 -36 337.462 16.1472 1 -7 23 5 30.4091 9.22994 -2 7 7 -35 30.4091 9.22994 1 7 7 -34 9.19421 11.8878 1 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436.429 28.4634 -2 -8 25 8 436.429 28.4634 1 8 7 -39 34.5878 11.6943 -2 -8 25 7 34.5878 11.6943 1 8 7 -38 10.9795 21.4203 -2 -8 25 6 10.9795 21.4203 1 8 8 -38 26.2269 20.6747 -2 -8 25 5 26.2269 20.6747 1 -8 -8 37 65.7564 11.6618 -2 8 -25 -4 65.7564 11.6618 1 8 -25 -3 202.339 58.4176 1 8 9 -37 161.815 22.3042 -2 -8 25 3 161.815 22.3042 1 8 9 -36 32.1505 19.8065 -2 -8 25 2 32.1505 19.8065 1 -8 25 1 134.931 37.4738 1 8 10 -36 175.025 26.7884 -2 -8 25 1 175.025 26.7884 1 -8 -10 35 132.411 22.1424 -2 8 -25 0 132.411 22.1424 1 -8 25 -1 131.603 29.5745 1 8 11 -35 182.156 25.7683 -2 -8 25 -1 182.156 25.7683 1 -8 -11 34 14.8597 10.0480 -2 8 -25 2 14.8597 10.0480 1 -8 25 -3 3.69073 14.6153 1 -8 -12 34 39.8312 13.1601 -2 8 -25 3 39.8312 13.1601 1 8 12 -33 48.2281 7.64635 -2 -8 25 -4 48.2281 7.64635 1 -8 25 -5-1.18569 13.5011 1 -8 -13 33 7.82682 13.3277 -2 8 -25 5 7.82682 13.3277 1 8 13 -32 165.672 11.1030 -2 -8 25 -6 165.672 11.1030 1 -8 25 -7 1.50669 12.5421 1 8 14 -31 66.7076 6.15963 -2 -8 25 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422.248 28.4676 -2 8 -24 -5 422.248 28.4676 1 8 8 -36 67.8761 21.4762 -2 -8 24 4 67.8761 21.4762 1 -8 -8 35 14.1892 20.7718 -2 8 -24 -3 14.1892 20.7718 1 -8 24 2 113.067 28.9250 1 -8 -9 35 237.031 25.6709 -2 8 -24 -2 237.031 25.6709 1 8 9 -34 46.0160 9.83103 -2 -8 24 1 46.0160 9.83103 1 -8 24 0 33.3844 14.1260 1 -8 -10 34 76.8664 29.6400 -2 8 -24 0 76.8664 29.6400 1 8 10 -33 15.2316 16.6541 -2 -8 24 -1 15.2316 16.6541 1 -8 24 -2 2.62040 13.0552 1 -8 -11 33-28.1921 61.7110 -2 8 -24 2-28.1921 61.7110 1 8 11 -32 19.3310 8.93766 -2 -8 24 -3 19.3310 8.93766 1 -8 24 -4 26.2643 13.4323 1 -8 -12 32 114.553 39.3741 -2 8 -24 4 114.553 39.3741 1 8 12 -31 65.2580 17.8548 -2 -8 24 -5 65.2580 17.8548 1 -8 24 -6 13.4583 12.9977 1 -8 -13 31 83.9928 67.5852 -2 8 -24 6 83.9928 67.5852 1 8 13 -30 45.0910 5.38437 -2 -8 24 -7 45.0910 5.38437 1 -8 24 -8 122.088 13.6704 1 8 14 -29 41.2344 4.41255 -2 -8 24 -9 41.2344 4.41255 1 -8 24 -10 20.8728 12.5479 1 8 15 -28 29.3515 5.03610 -2 -8 24 -11 29.3515 5.03610 1 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339.110 14.2440 -2 -10 11 -28 339.110 14.2440 1 10 -11 29 180.516 25.4071 1 10 16 2 179.903 51.3387 -2 -10 11 -29 179.903 51.3387 1 10 17 2 54.5527 11.2454 -2 -10 11 -30 54.5527 11.2454 1 10 -11 31 89.2252 33.0472 1 10 17 3 152.518 33.1008 -2 -10 11 -31 152.518 33.1008 1 -10 15 29 21.4134 11.1721 -2 10 -10 -34 21.4134 11.1721 1 10 -10 -33 246.878 45.1826 1 -10 14 29 195.698 23.5756 -2 10 -10 -33 195.698 23.5756 1 10 -14 -28 10.2872 9.73436 -2 -10 10 32 10.2872 9.73436 1 10 -10 -31 1.37585 28.4831 1 10 -13 -28 12.3411 21.0243 -2 -10 10 31 12.3411 21.0243 1 10 -13 -27 24.4322 6.07983 -2 -10 10 30 24.4322 6.07983 1 10 -10 -29 804.759 40.0009 1 10 -12 -27 907.271 34.9361 -2 -10 10 29 907.271 34.9361 1 10 -12 -26 190.062 10.7688 -2 -10 10 28 190.062 10.7688 1 10 -10 -27 65.3392 20.0200 1 10 -11 -26 80.7591 28.2599 -2 -10 10 27 80.7591 28.2599 1 10 -11 -25 52.8562 7.05021 -2 -10 10 26 52.8562 7.05021 1 10 -10 -25 9.60231 15.7496 1 10 -10 -25 158.344 52.8886 -2 -10 10 25 158.344 52.8886 1 10 -10 -24 2895.33 17.7615 -2 -10 10 24 2895.33 17.7615 1 -10 10 23 28.2836 10.8181 1 -10 9 23 2115.91 13.5541 -2 10 -10 -22 2115.91 13.5541 1 -10 10 21 541.666 15.4010 1 10 -8 -22 1156.13 10.1958 -2 -10 10 20 1156.13 10.1958 1 10 -10 -19 126.067 11.9285 1 10 -8 -21 147.647 19.8016 -2 -10 10 19 147.647 19.8016 1 10 -7 -21 270.093 7.96485 -2 -10 10 18 270.093 7.96485 1 -10 10 17 164.434 10.1026 1 10 -7 -20 163.054 20.6532 -2 -10 10 17 163.054 20.6532 1 10 -6 -20 92.3242 4.76250 -2 -10 10 16 92.3242 4.76250 1 -10 10 15 62.1924 8.74367 1 10 -6 -19 114.259 19.6823 -2 -10 10 15 114.259 19.6823 1 10 -5 -19 8.63921 3.64601 -2 -10 10 14 8.63921 3.64601 1 10 -10 -13 81.0694 9.89761 1 10 -5 -18 55.2994 8.23568 -2 -10 10 13 55.2994 8.23568 1 10 -4 -18 2087.64 26.0621 -2 -10 10 12 2087.64 26.0621 1 10 -10 -11 271.747 14.3853 1 10 -4 -17 337.642 16.0473 -2 -10 10 11 337.642 16.0473 1 10 -3 -17 259.639 11.3814 -2 -10 10 10 259.639 11.3814 1 10 -10 -9 15.0843 10.9009 1 10 -3 -16 43.9299 9.61799 -2 -10 10 9 43.9299 9.61799 1 10 -2 -16 964.133 17.7760 -2 -10 10 8 964.133 17.7760 1 10 -10 -7 208.270 14.3034 1 10 -2 -15 216.005 14.8646 -2 -10 10 7 216.005 14.8646 1 -10 1 15 1000.78 16.1986 -2 10 -10 -6 1000.78 16.1986 1 10 -10 -5 2.10026 9.39680 1 10 -1 -14 7.77246 11.0431 -2 -10 10 5 7.77246 11.0431 1 10 -10 -4 71.3831 12.6958 1 10 0 -14 45.7603 6.38045 -2 -10 10 4 45.7603 6.38045 1 -10 10 3 731.295 23.4008 1 10 0 -13 838.222 16.6527 -2 -10 10 3 838.222 16.6527 1 10 -10 -2 934.878 23.1802 1 10 1 -13 1078.19 16.6756 -2 -10 10 2 1078.19 16.6756 1 -10 10 1 32.5650 14.1104 1 10 1 -12 314.254 13.4122 -2 -10 10 1 314.254 13.4122 1 10 2 -12 307.093 11.3980 -2 -10 10 0 307.093 11.3980 1 10 -10 1 932.391 36.7834 1 10 2 -11 1543.44 19.5796 -2 -10 10 -1 1543.44 19.5796 1 10 -10 2 2133.82 77.7635 1 10 3 -11 2571.34 20.3265 -2 -10 10 -2 2571.34 20.3265 1 10 -10 3 439.421 25.1836 1 10 3 -10 397.524 11.2178 -2 -10 10 -3 397.524 11.2178 1 10 -10 4 22.7128 12.6792 1 10 4 -10 31.1775 8.38089 -2 -10 10 -4 31.1775 8.38089 1 10 -10 5 554.917 26.1982 1 10 4 -9 614.310 15.1889 -2 -10 10 -5 614.310 15.1889 1 10 -10 6 1839.71 71.5962 1 10 5 -9 2128.22 18.9899 -2 -10 10 -6 2128.22 18.9899 1 10 5 -8 571.649 11.8107 -2 -10 10 -7 571.649 11.8107 1 10 -10 8 19.2064 20.2963 1 10 6 -8 14.6155 10.8383 -2 -10 10 -8 14.6155 10.8383 1 10 6 -7 606.821 15.5596 -2 -10 10 -9 606.821 15.5596 1 10 -10 10 4.14672 19.3382 1 -10 -7 7 31.6267 7.01503 -2 10 -10 10 31.6267 7.01503 1 10 7 -6 294.195 13.5418 -2 -10 10 -11 294.195 13.5418 1 10 -10 12 20.0375 13.6511 1 10 8 -6 32.6380 6.07544 -2 -10 10 -12 32.6380 6.07544 1 -10 -8 5 2112.71 28.8518 -2 10 -10 13 2112.71 28.8518 1 10 -10 14 137.866 18.4697 1 10 9 -5 297.770 17.4322 -2 -10 10 -14 297.770 17.4322 1 10 9 -4 1388.24 24.9554 -2 -10 10 -15 1388.24 24.9554 1 10 -10 16 18.5378 15.7162 1 10 10 -4 12.7298 8.57116 -2 -10 10 -16 12.7298 8.57116 1 10 10 -3 141.654 13.2503 -2 -10 10 -17 141.654 13.2503 1 10 -10 18 171.366 20.1022 1 10 11 -3 239.714 18.4569 -2 -10 10 -18 239.714 18.4569 1 10 11 -2 380.824 18.4235 -2 -10 10 -19 380.824 18.4235 1 -10 10 -20 215.034 17.3751 1 -10 -12 2 253.063 22.4566 -2 10 -10 20 253.063 22.4566 1 -10 -12 1 19.0398 4.82045 -2 10 -10 21 19.0398 4.82045 1 10 -10 22 18.4537 13.6673 1 10 13 -1 23.9820 20.5211 -2 -10 10 -22 23.9820 20.5211 1 10 13 0 474.974 7.50749 -2 -10 10 -23 474.974 7.50749 1 -10 10 -24 95.4973 15.3437 1 10 14 0 166.267 30.1682 -2 -10 10 -24 166.267 30.1682 1 10 14 1 70.9094 10.5410 -2 -10 10 -25 70.9094 10.5410 1 -10 10 -26-9.98283 14.9344 1 -10 -14 -2-29.5170 59.2178 -2 10 -10 26-29.5170 59.2178 1 10 15 2 894.390 15.6775 -2 -10 10 -27 894.390 15.6775 1 10 -10 28 9.29121 18.6335 1 -10 -15 -3-50.2164 68.0672 -2 10 -10 28-50.2164 68.0672 1 10 16 3 133.033 10.6127 -2 -10 10 -29 133.033 10.6127 1 10 -10 30 16.2535 28.6652 1 10 16 4 23.4040 31.3163 -2 -10 10 -30 23.4040 31.3163 1 10 17 4 31.6845 24.7398 -2 -10 10 -31 31.6845 24.7398 1 10 -10 32 181.175 67.7723 1 10 17 5 295.819 30.3703 -2 -10 10 -32 295.819 30.3703 1 10 -9 -34 12.3556 28.6159 1 -10 15 28 8.02445 9.42314 -2 10 -9 -34 8.02445 9.42314 1 -10 15 27 217.857 23.5678 -2 10 -9 -33 217.857 23.5678 1 10 -9 -32 62.5969 29.5151 1 10 -14 -27 74.9682 23.0357 -2 -10 9 32 74.9682 23.0357 1 10 -14 -26 233.704 23.4967 -2 -10 9 31 233.704 23.4967 1 10 -9 -30 672.979 34.8285 1 10 -13 -26 805.403 37.2790 -2 -10 9 30 805.403 37.2790 1 10 -13 -25 33.1704 9.64789 -2 -10 9 29 33.1704 9.64789 1 10 -9 -28 194.646 22.3242 1 10 -12 -25 280.101 28.7688 -2 -10 9 28 280.101 28.7688 1 10 -12 -24 186.467 10.9424 -2 -10 9 27 186.467 10.9424 1 10 -9 -26 1726.23 35.6287 1 10 -11 -24 2011.71 54.6933 -2 -10 9 26 2011.71 54.6933 1 10 -11 -23 179.501 9.64121 -2 -10 9 25 179.501 9.64121 1 -10 9 24 302.492 12.7053 1 10 -10 -22 1503.45 28.5021 -2 -10 9 23 1503.45 28.5021 1 -10 9 22 69.5839 10.5163 1 10 -9 -21 498.799 6.77793 -2 -10 9 21 498.799 6.77793 1 10 -9 -20 16.1921 9.37609 1 10 -9 -20 9.84966 9.88627 -2 -10 9 20 9.84966 9.88627 1 10 -8 -20 62.4372 2.95465 -2 -10 9 19 62.4372 2.95465 1 10 -9 -18 24.9560 8.23834 1 -10 8 19 25.4230 21.4988 -2 10 -9 -18 25.4230 21.4988 1 10 -7 -19 47.8681 3.19102 -2 -10 9 17 47.8681 3.19102 1 -10 9 16 354.882 11.8112 1 10 -7 -18 418.306 22.8410 -2 -10 9 16 418.306 22.8410 1 10 -6 -18 22.2510 2.90854 -2 -10 9 15 22.2510 2.90854 1 10 -9 -14 83.5504 9.35150 1 -10 6 17 75.1021 15.6288 -2 10 -9 -14 75.1021 15.6288 1 10 -5 -17 1487.80 21.4999 -2 -10 9 13 1487.80 21.4999 1 10 -9 -12 1185.98 22.4713 1 10 -5 -16 1526.34 23.2119 -2 -10 9 12 1526.34 23.2119 1 10 -4 -16 490.494 14.0705 -2 -10 9 11 490.494 14.0705 1 10 -9 -10 340.766 17.4201 1 10 -4 -15 362.422 11.6909 -2 -10 9 10 362.422 11.6909 1 -10 3 15 2005.56 17.4348 -2 10 -9 -9 2005.56 17.4348 1 10 -9 -8 694.331 23.3306 1 -10 3 14 903.905 17.2447 -2 10 -9 -8 903.905 17.2447 1 10 -2 -14 1158.59 17.8554 -2 -10 9 7 1158.59 17.8554 1 10 -9 -6 248.872 15.7262 1 -10 2 13 314.071 12.8477 -2 10 -9 -6 314.071 12.8477 1 -10 1 13 711.330 13.5111 -2 10 -9 -5 711.330 13.5111 1 -10 9 4 32.3789 8.56923 1 10 -1 -12 50.1281 9.40600 -2 -10 9 4 50.1281 9.40600 1 10 -9 -3 48.0998 13.4521 1 10 0 -12 89.6146 9.13494 -2 -10 9 3 89.6146 9.13494 1 -10 9 2 454.273 14.5914 1 10 0 -11 564.270 14.2170 -2 -10 9 2 564.270 14.2170 1 10 -9 -1 12.2788 14.0191 1 10 1 -11 54.8926 9.35094 -2 -10 9 1 54.8926 9.35094 1 -10 9 0 3989.56 36.9288 1 10 1 -10 4588.78 30.1488 -2 -10 9 0 4588.78 30.1488 1 10 -9 1 669.506 23.7402 1 10 2 -10 1079.84 14.9775 -2 -10 9 -1 1079.84 14.9775 1 10 2 -9 178.065 9.15407 -2 -10 9 -2 178.065 9.15407 1 -10 9 -3 553.821 26.9515 1 10 3 -9 729.238 12.9023 -2 -10 9 -3 729.238 12.9023 1 10 3 -8 90.7126 5.68356 -2 -10 9 -4 90.7126 5.68356 1 -10 9 -5 1748.51 33.8691 1 10 4 -8 2376.01 20.2677 -2 -10 9 -5 2376.01 20.2677 1 10 4 -7 214.651 11.4887 -2 -10 9 -6 214.651 11.4887 1 10 -9 7 28.6509 20.1151 1 10 5 -7 179.721 12.5801 -2 -10 9 -7 179.721 12.5801 1 10 5 -6 50.3812 5.50513 -2 -10 9 -8 50.3812 5.50513 1 10 -9 9 640.262 36.0338 1 10 6 -6 692.301 15.8715 -2 -10 9 -9 692.301 15.8715 1 10 6 -5 135.058 12.4629 -2 -10 9 -10 135.058 12.4629 1 10 -9 11 39.0799 19.0078 1 10 7 -5 33.6864 12.1681 -2 -10 9 -11 33.6864 12.1681 1 10 7 -4 478.779 16.5112 -2 -10 9 -12 478.779 16.5112 1 -10 9 -13 1090.80 31.8076 1 10 8 -4 1163.28 21.6523 -2 -10 9 -13 1163.28 21.6523 1 10 8 -3 870.390 19.9425 -2 -10 9 -14 870.390 19.9425 1 10 -9 15 184.020 17.8211 1 10 9 -3 228.644 16.7305 -2 -10 9 -15 228.644 16.7305 1 10 9 -2 405.536 16.7719 -2 -10 9 -16 405.536 16.7719 1 10 -9 17-1.31481 10.6148 1 10 10 -2 57.2167 17.8597 -2 -10 9 -17 57.2167 17.8597 1 -10 -10 1 344.404 9.57513 -2 10 -9 18 344.404 9.57513 1 10 -9 19 36.5036 11.0642 1 -10 -11 1 110.930 20.0748 -2 10 -9 19 110.930 20.0748 1 10 11 0 30.9953 5.37171 -2 -10 9 -20 30.9953 5.37171 1 10 -9 21 403.187 17.7563 1 10 12 0 466.609 24.8871 -2 -10 9 -21 466.609 24.8871 1 10 12 1 163.250 5.70698 -2 -10 9 -22 163.250 5.70698 1 -10 9 -23 187.341 15.5740 1 10 13 1 252.648 27.4267 -2 -10 9 -23 252.648 27.4267 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36.0558 1 12 15 -19 29.9330 5.04080 -2 -12 21 -17 29.9330 5.04080 1 -12 21 -18 109.173 17.9988 1 -12 -16 19 80.9287 48.8954 -2 12 -21 18 80.9287 48.8954 1 -12 -16 18 8.46234 7.53360 -2 12 -21 19 8.46234 7.53360 1 12 17 -17 26.7991 6.29519 -2 -12 21 -21 26.7991 6.29519 1 12 -3 -36 322.153 34.7676 -2 -12 20 19 322.153 34.7676 1 12 -20 -18 8.47415 30.4807 1 12 -3 -35 22.7936 34.1403 -2 -12 20 18 22.7936 34.1403 1 12 -2 -35 28.9230 22.5022 -2 -12 20 17 28.9230 22.5022 1 12 -20 -16 43.8567 25.1763 1 12 -2 -34 80.9326 39.1014 -2 -12 20 16 80.9326 39.1014 1 12 -1 -34 87.1917 33.2924 -2 -12 20 15 87.1917 33.2924 1 12 -20 -14 140.042 31.4063 1 12 -1 -33 218.564 32.6158 -2 -12 20 14 218.564 32.6158 1 12 0 -33 52.0752 12.5500 -2 -12 20 13 52.0752 12.5500 1 12 -20 -12 654.474 45.1428 1 12 0 -32 612.634 32.4724 -2 -12 20 12 612.634 32.4724 1 12 1 -32-10.6957 20.8114 -2 -12 20 11-10.6957 20.8114 1 12 -20 -10 158.537 49.5710 1 12 1 -31 160.397 25.7704 -2 -12 20 10 160.397 25.7704 1 12 2 -31 26.4617 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25.2369 1 12 10 -23 33.2336 11.6518 -2 -12 20 -7 33.2336 11.6518 1 12 10 -22 46.2832 20.4884 -2 -12 20 -8 46.2832 20.4884 1 -12 20 -9 16.9104 20.9576 1 -12 -11 22 29.4757 23.3774 -2 12 -20 9 29.4757 23.3774 1 12 11 -21 453.578 23.1379 -2 -12 20 -10 453.578 23.1379 1 -12 20 -11 31.8070 16.0543 1 -12 -12 21 25.2308 11.4168 -2 12 -20 11 25.2308 11.4168 1 12 12 -20 23.2470 6.84328 -2 -12 20 -12 23.2470 6.84328 1 -12 20 -13 16.3026 15.1188 1 -12 -13 20 105.199 34.8427 -2 12 -20 13 105.199 34.8427 1 12 13 -19 38.2740 6.07570 -2 -12 20 -14 38.2740 6.07570 1 -12 20 -15 118.494 17.8543 1 -12 -14 19 130.339 38.2288 -2 12 -20 15 130.339 38.2288 1 12 14 -18 203.972 21.9959 -2 -12 20 -16 203.972 21.9959 1 -12 20 -17 65.2408 18.1984 1 -12 -15 18 13.8238 12.3666 -2 12 -20 17 13.8238 12.3666 1 12 15 -17 19.5134 7.05032 -2 -12 20 -18 19.5134 7.05032 1 -12 20 -19 195.188 18.9650 1 -12 -16 17 287.498 73.9757 -2 12 -20 19 287.498 73.9757 1 12 16 -16 129.148 8.00173 -2 -12 20 -20 129.148 8.00173 1 -12 20 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9.29813 9.59121 2 0 -4 -30 43.1767 21.9613 2 0 -4 -32 29.8096 22.7678 2 0 -4 -34 9.03325 30.7554 2 0 -4 -36 8.45421 33.4686 2 0 -4 -38 50.4758 36.3088 2 0 5 -41 4.43454 31.4638 2 0 -5 39 7.51441 17.9688 2 0 5 -37 9.27552 17.9737 2 0 5 -35 33.3638 21.8483 2 0 5 -33 37.3344 31.6084 2 0 -5 28 127.865 45.8620 2 0 -5 26 109.482 41.3247 2 0 -5 24-2.44438 32.7925 2 0 5 -23 175.212 13.2535 2 0 -5 22 62.1051 9.81604 2 0 5 -21 68.1246 9.59295 2 0 5 -20 14.6116 4.52813 2 0 5 -19 7.34672 6.52848 2 0 5 -18 264.107 8.30413 2 0 5 -16 40.7836 3.02926 2 0 5 -14 124.113 3.56073 2 0 5 -12 101.809 3.78833 2 0 5 -10 66.1313 3.29812 2 0 5 -8 3215.37 11.6447 2 0 -5 6 272.895 4.25425 2 0 5 -4 530.097 5.50863 2 0 5 -2 70.7735 3.00146 2 0 5 0 41.7602 2.32256 2 0 5 2-0.16403 1.88663 2 0 5 4 72.8978 2.70372 2 0 5 6 44.1942 4.14995 2 0 5 8 30.5617 4.68102 2 0 5 10 754.122 11.9142 2 0 5 11 101.382 5.27041 2 0 5 12 533.904 8.56941 2 0 5 13 207.193 9.14844 2 0 -5 -14 3.10968 5.94562 2 0 5 15 21.3732 7.24093 2 0 5 16 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605.774 12.2019 2 0 10 -17 16.4617 5.97199 2 0 10 -15 407.798 7.55300 2 0 10 -13 51.2582 5.10803 2 0 -10 11 7.05497 3.45558 2 0 -10 9 9.36100 3.26239 2 0 -10 7 916.518 10.8692 2 0 10 -5 145.900 4.30679 2 0 -10 3 41.9672 4.11679 2 0 10 -1 11.3736 3.83430 2 0 10 1 13.8024 3.42508 2 0 10 3 2.37767 3.46398 2 0 10 5 79.8354 7.10505 2 0 10 7 157.780 9.71268 2 0 10 9 8.79978 9.32904 2 0 -10 -11 190.285 19.3951 2 0 -10 -16 660.777 24.8341 2 0 -10 -18 25.0584 13.7242 2 0 -10 -20 181.280 39.4969 2 0 -10 -22 20.5174 17.5282 2 0 -10 -24 37.2181 15.9539 2 0 -10 -26 0.18514 14.4320 2 0 -10 -28 31.2921 16.6857 2 0 -10 -30 29.7272 27.5314 2 0 -10 -32 17.2408 31.3206 2 0 11 -25 17.0069 12.0722 2 0 11 -24 23.5489 10.7658 2 0 11 -22 33.5873 8.57166 2 0 11 -20 180.842 9.14447 2 0 11 -18 260.775 9.06805 2 0 11 -16 1044.99 11.9599 2 0 11 -14-7.68423 5.56682 2 0 -11 12 44.3474 4.76131 2 0 -11 10 35.3872 5.84283 2 0 -11 8 44.9073 5.53037 2 0 11 -6 136.814 4.41783 2 0 11 -4 192.071 5.22064 2 0 -11 2 218.304 5.85461 2 0 11 0 7.85960 3.73700 2 0 -11 -2 74.3253 5.13586 2 0 11 4 71.8225 4.22457 2 0 11 6 9.82244 8.94082 2 0 11 8 82.9155 12.7880 2 0 -11 -10 245.171 30.2544 2 0 -11 -15 332.940 22.8126 2 0 -11 -17 55.9314 32.9248 2 0 -11 -19 4.21230 12.5829 2 0 -11 -21 18.4634 24.3877 2 0 -11 -23 44.2082 15.9902 2 0 -11 -25 7.22349 15.2339 2 0 -11 -27-2.42044 15.2461 2 0 -11 -29 30.7461 20.6854 2 0 11 31 8.10925 23.1595 2 0 11 33 52.8428 20.8236 2 0 12 -25 242.265 37.0843 2 0 12 -23 4.47090 8.67569 2 0 12 -21 4.54801 7.47257 2 0 12 -19 31.8642 6.92489 2 0 12 -17 244.645 8.21583 2 0 12 -15 6.18270 5.89272 2 0 12 -13 12.1915 5.49891 2 0 -12 11 77.2379 6.73379 2 0 -12 9 43.6463 6.27181 2 0 -12 7 9.96794 3.95972 2 0 12 -5 142.588 5.22158 2 0 -12 3 145.641 5.41048 2 0 12 -1 59.3623 5.05989 2 0 12 1 370.002 7.99820 2 0 12 3 16.7320 4.58975 2 0 -12 -4 103.770 6.18235 2 0 12 5 75.2726 9.10102 2 0 12 7-6.28152 11.9377 2 0 -12 -9 325.639 20.2434 2 0 -12 -14 41.5579 27.0147 2 0 -12 -16-19.1892 27.2725 2 0 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41.7870 41.7815 2 0 -16 -9 122.924 21.7130 2 0 -16 -10 56.8728 20.8787 2 0 -16 -12 62.6257 22.4774 2 0 -16 -13 16.8494 23.4727 2 0 -16 -16 5.93923 34.3548 2 0 -16 -18-9.67298 41.2638 2 0 -16 -20 11.2119 19.3593 2 0 -16 -22 21.3903 20.2282 2 0 -16 -24-6.09860 20.0207 2 0 -16 -26 4.49300 21.1133 2 0 17 -30 89.7611 40.6664 2 0 17 -28 20.5865 21.4707 2 0 17 -26 183.574 18.7228 2 0 17 -24 130.995 13.0003 2 0 17 -22 63.3650 11.8700 2 0 17 -20 24.3596 9.64005 2 0 17 -18 88.4189 9.23781 2 0 17 -16 174.782 9.79137 2 0 -17 14 18.2235 6.76729 2 0 -17 12 75.5032 7.44044 2 0 -17 10 38.6956 6.90693 2 0 17 -8 9.31075 6.51850 2 0 17 -6 0.07567 6.83966 2 0 17 -4 28.3492 7.18271 2 0 17 -2 25.5995 8.39802 2 0 -17 0 51.0628 13.8643 2 0 -17 -9 221.060 50.2309 2 0 -17 -19-13.2842 23.3064 2 0 -17 -21 34.4862 22.1343 2 0 -17 -23-8.80239 20.9053 2 0 -17 -25-17.2166 22.7183 2 0 18 -29 40.1328 22.2608 2 0 18 -27 60.0493 19.3726 2 0 18 -25 93.2651 14.6774 2 0 18 -23 113.983 12.1494 2 0 18 -21 20.7738 9.76254 2 0 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14.8790 2 1 4 -14 419.991 14.4953 2 -1 -4 13 1135.30 16.7814 2 1 4 -12 46.6117 7.61696 2 -1 -4 11 232.899 7.69846 2 -1 -4 10 878.643 9.93883 2 1 4 -9 355.743 8.54940 2 1 4 -8 1018.22 12.5101 2 1 4 -7 1772.55 21.4029 2 -1 -4 6 317.800 3.30794 2 1 4 -4 2319.00 9.00302 2 1 4 -2 1109.47 5.45380 2 1 4 -1 1181.06 14.2386 2 -1 -4 0 886.812 4.31260 2 1 4 1 807.120 16.3589 2 1 4 2 1877.13 7.43773 2 1 4 4 335.424 3.09539 2 -1 -4 -5 1578.38 16.7084 2 1 4 6 14.3020 2.26895 2 1 4 8 501.894 5.00820 2 -1 -4 -10 5.62544 2.58279 2 1 4 12 1708.82 8.65951 2 1 4 14 51.2127 3.50219 2 1 4 16 2.18891 4.75058 2 1 4 18 48.0596 6.25614 2 -1 -4 -20 21.7466 6.61810 2 1 4 22 6.32445 7.05598 2 -1 -4 -24 39.4207 14.6956 2 -1 -4 -26 104.647 14.0662 2 -1 -4 -28 10.7407 19.0108 2 1 5 -40 8.99245 18.7265 2 -1 -5 38-22.9724 16.6319 2 -1 -5 36 35.7050 15.0749 2 -1 -5 34 6.56920 10.6106 2 -1 -5 32 29.7386 10.8788 2 -1 -5 30 77.6839 11.6784 2 -1 -5 28 64.2759 11.8551 2 -1 -5 26 11.9340 10.5657 2 -1 -5 24 11.6420 12.3258 2 1 5 -22 101.664 6.40189 2 1 5 -20 53.0037 3.59860 2 1 5 -18 421.168 7.47225 2 1 5 -17 70.5809 4.01226 2 1 5 -16 205.855 4.29066 2 1 5 -13 19.5564 14.4420 2 1 5 -12 27.6538 15.2315 2 -1 -5 11 811.389 21.5969 2 1 5 -10 1262.87 14.7809 2 -1 -5 9 855.957 13.5152 2 1 5 -7 1712.86 9.36152 2 1 5 -5 500.327 5.58550 2 1 5 -3 1708.09 8.34825 2 -1 -5 1 2111.03 7.69695 2 -1 -5 -1 106.712 2.43560 2 1 5 3 1041.62 5.79318 2 1 5 5 189.126 4.60486 2 1 5 7 63.4577 4.26052 2 1 5 9 11.1181 3.74854 2 1 5 11 14.4209 2.96851 2 1 5 13 63.0377 3.08620 2 -1 -5 -15 12.4053 2.55585 2 -1 -5 -17 1627.90 14.6320 2 -1 -5 -19 352.222 12.4178 2 -1 -5 -21-8.32977 7.78666 2 -1 -5 -23 4.61353 13.8295 2 -1 -5 -25 52.8492 32.5011 2 -1 -5 -27 35.6766 37.1116 2 -1 -5 -34 27.6039 34.4861 2 1 6 -41-18.7253 22.9467 2 -1 -6 39-0.14273 18.2100 2 -1 -6 37 12.6293 14.4268 2 -1 -6 35 7.70112 10.9519 2 -1 -6 33 25.2305 12.1914 2 -1 -6 31 62.3921 11.7523 2 -1 -6 29 7.77295 10.2402 2 -1 -6 27 94.2607 12.3148 2 -1 -6 25 1.10191 11.3266 2 1 6 -23 3.19015 18.1536 2 1 6 -21-1.20433 5.34582 2 1 6 -19 55.2929 14.8603 2 1 6 -17 147.709 15.7856 2 1 6 -14 325.577 13.6940 2 1 6 -12 146.793 8.45557 2 1 6 -10 1094.31 10.1475 2 1 6 -8 546.833 6.20161 2 1 6 -6 403.873 4.92166 2 1 6 -4 296.483 5.36683 2 1 6 -2 405.239 4.22240 2 -1 -6 0-0.13256 2.61522 2 -1 -6 -2 1123.39 6.96680 2 1 6 4 52.2084 3.45076 2 1 6 6 235.834 5.71230 2 1 6 8 637.940 8.60129 2 1 6 10 584.657 8.98292 2 1 6 12 350.426 7.47857 2 1 6 14 2.88502 3.63094 2 1 6 16 337.264 5.94866 2 1 6 18 321.304 11.5173 2 -1 -6 -20 138.513 9.57725 2 -1 -6 -22-6.27410 20.2675 2 -1 -7 40-12.5616 17.2800 2 -1 -7 38 23.8259 16.6518 2 -1 -7 36 36.9955 13.3632 2 1 7 -34 5.15982 11.8835 2 -1 -7 32 30.5206 11.6477 2 -1 -7 30 25.2415 12.2819 2 -1 -7 28 62.7167 11.7772 2 -1 -7 26 3.79627 10.7746 2 1 7 -24 142.397 22.0606 2 1 7 -22 30.8183 13.1727 2 1 7 -20-3.95609 10.9396 2 1 7 -18 43.1795 11.0132 2 1 7 -16 271.512 14.6526 2 1 7 -15 36.5266 9.02912 2 1 7 -14 402.358 13.7991 2 -1 -7 11 1151.70 22.7580 2 -1 -7 9 297.998 6.45778 2 1 7 -7 2493.67 11.3434 2 1 7 -5 1267.49 8.15521 2 1 7 -3 554.224 4.90247 2 -1 -7 1 786.666 6.30866 2 1 7 1 73.1854 3.73260 2 1 7 3 7.26070 2.75949 2 1 7 5 856.878 8.71756 2 1 7 7 44.6642 3.45834 2 1 7 9 880.616 10.6857 2 1 7 11 77.2255 6.36263 2 1 7 13 27.1677 5.58284 2 1 7 15 197.941 5.73267 2 1 7 17 1.25512 8.58205 2 1 7 19 15.0381 14.6975 2 -1 -7 -21 29.3366 22.1886 2 -1 -7 -23 574.955 58.1833 2 -1 -7 -34 34.5886 41.4128 2 -1 -8 41 19.9737 17.9929 2 -1 -8 39 78.0988 19.2311 2 -1 -8 37 8.85566 14.8634 2 1 8 -35 18.8875 11.7904 2 1 8 -33 3.29690 10.9813 2 -1 -8 31 4.23391 10.5656 2 -1 -8 29 127.989 13.2564 2 -1 -8 27 0.01441 11.1842 2 1 8 -25 46.1396 14.1596 2 1 8 -23 134.993 16.3167 2 1 8 -21 9.76506 12.0706 2 1 8 -19 0.73221 10.3294 2 1 8 -17 25.9490 10.3325 2 1 8 -16 81.4719 9.68404 2 1 8 -15 532.851 13.3786 2 -1 -8 10 381.993 11.1028 2 1 8 -8 346.144 5.29143 2 1 8 -6 627.399 7.90043 2 1 8 -4 2445.10 10.3108 2 -1 -8 2 138.982 3.76740 2 1 8 0 87.6269 3.98813 2 1 8 2 59.1297 3.86602 2 1 8 4 91.1352 3.06440 2 1 8 6 90.6950 5.30314 2 1 8 8 551.479 7.48159 2 1 8 10 241.249 8.02982 2 1 8 12 136.650 7.39300 2 1 8 14 1173.66 13.5598 2 1 8 16 115.895 10.2847 2 1 8 18 24.8170 17.8444 2 -1 -8 -20 40.9874 23.4748 2 -1 -8 -22 245.022 48.0815 2 -1 -8 -35-24.8321 30.3330 2 -1 -9 40-2.51134 16.0125 2 -1 -9 38 39.3704 14.6123 2 1 9 -36 14.3315 14.0654 2 1 9 -34 15.4227 12.7014 2 -1 -9 32 107.707 13.6780 2 -1 -9 30 21.3790 11.1693 2 -1 -9 28-1.41237 10.4215 2 -1 -9 26 32.3114 13.5904 2 -1 -9 24-0.09171 10.4698 2 1 9 -22 9.97514 13.0531 2 1 9 -20 92.9409 13.1252 2 1 9 -18 62.5586 9.58325 2 1 9 -11 187.705 8.71362 2 1 9 -9 261.363 5.05536 2 1 9 -7 124.776 5.51272 2 1 9 -5 840.954 6.73681 2 1 9 -3 3.72534 3.35673 2 -1 -9 1 576.198 7.02424 2 1 9 1 267.764 5.42179 2 1 9 3 402.687 5.76551 2 1 9 5 2.58943 4.36170 2 1 9 7 32.3898 4.12062 2 1 9 9 27.2149 5.83228 2 1 9 11 250.712 8.37265 2 1 9 13 99.1943 7.71220 2 1 9 15 229.060 10.3860 2 1 9 17 34.8350 15.7996 2 -1 -9 -19 31.3016 23.6357 2 -1 -9 -21 11.8890 37.3348 2 -1 -9 -34 26.6605 42.1396 2 -1 -10 41 2.34476 15.4065 2 -1 -10 39 17.2779 14.2865 2 1 10 -37 14.4463 14.3083 2 1 10 -35-3.35412 11.4466 2 1 10 -33 45.1313 12.7105 2 -1 -10 31 11.0297 13.1036 2 -1 -10 29 13.7595 10.3559 2 -1 -10 27 59.6696 11.4155 2 -1 -10 25-0.63280 12.0360 2 1 10 -23-0.44863 10.8237 2 1 10 -21 32.9305 6.87789 2 -1 -10 12 48.1690 12.8208 2 -1 -10 10 1184.66 9.85569 2 1 10 -8 173.042 6.23785 2 1 10 -6 18.3824 3.49215 2 1 10 -4 10.1767 3.60925 2 -1 -10 2 153.475 5.11805 2 1 10 0 49.1887 4.32568 2 1 10 2 656.039 7.71710 2 1 10 4 51.4391 3.13927 2 1 10 6 575.981 9.55513 2 1 10 8 16.7352 5.49138 2 1 10 10 72.1748 6.87177 2 1 10 12 62.0064 7.77405 2 1 10 14 78.8082 7.50212 2 1 10 16 93.1027 13.3854 2 -1 -10 -18 0.05932 22.3384 2 -1 -10 -20 193.098 41.7304 2 -1 -10 -31 21.7285 48.9266 2 -1 -11 40 5.22286 14.4397 2 1 11 -38 3.94798 13.2684 2 1 11 -36 13.5442 12.5217 2 1 11 -34 35.7271 13.4751 2 -1 -11 32 65.5128 14.7733 2 -1 -11 30 0.52838 13.1018 2 -1 -11 28 53.5369 14.3080 2 -1 -11 26 15.2725 25.7965 2 1 11 -13 131.340 22.7038 2 1 11 -11 65.3457 6.68076 2 1 11 -9 38.3586 5.73551 2 1 11 -7 141.931 4.93722 2 -1 -11 6 3866.26 23.2938 2 -1 -11 5 164.038 5.20050 2 -1 -11 3-3.43125 4.43021 2 -1 -11 1-3.41507 4.05105 2 1 11 1 15.9644 4.46899 2 1 11 3 1.47330 3.93104 2 1 11 5 772.985 11.7407 2 1 11 7 3.02834 5.75711 2 1 11 9 140.758 7.93035 2 1 11 11-2.71421 6.58376 2 1 11 13 118.726 8.95055 2 1 11 15 4.21798 8.67938 2 1 11 17 16.3930 19.2592 2 -1 -11 -19 122.359 40.7353 2 -1 -11 -32-53.6865 46.4187 2 1 12 -39 2.35155 14.9654 2 1 12 -37 15.0467 13.7773 2 1 12 -35 20.0399 12.8381 2 1 12 -33 44.1965 13.0665 2 1 12 -31 7.00610 14.0531 2 -1 -12 29 5.92312 13.8835 2 -1 -12 27 1.86598 19.4121 2 -1 -12 25 132.096 27.4561 2 1 12 -12 189.276 8.93241 2 1 12 -10 772.698 12.3743 2 1 12 -8 566.190 9.89016 2 1 12 -6 134.589 6.24116 2 -1 -12 4 392.416 7.45322 2 -1 -12 2 26.6852 4.87244 2 -1 -12 0 143.794 5.92682 2 -1 -12 -2 2.75987 4.54895 2 1 12 4 5.46338 5.66703 2 1 12 6 7.99714 6.81330 2 1 12 8 135.227 8.17132 2 1 12 10 176.045 8.54044 2 1 12 12 96.2543 9.59005 2 1 12 14 154.455 12.1725 2 -1 -12 -16 20.4190 23.4384 2 -1 -12 -18 39.9885 33.5758 2 -1 -12 -31-23.4583 44.2770 2 1 13 -40 35.3059 36.2205 2 1 13 -38 10.2628 15.4151 2 1 13 -36-0.11037 12.5544 2 1 13 -34 23.6392 14.0045 2 1 13 -32 11.9942 14.5302 2 -1 -13 30 46.5386 14.8259 2 -1 -13 28-8.37297 18.5821 2 -1 -13 26 53.2659 25.1915 2 -1 -13 13 35.0910 7.32758 2 1 13 -11 89.2592 7.11833 2 -1 -13 9 373.699 9.48058 2 1 13 -7 52.4181 6.49433 2 1 13 -5 375.585 8.55617 2 -1 -13 3 15.4249 5.19809 2 -1 -13 1 900.814 10.8543 2 -1 -13 -1 199.589 6.56971 2 1 13 3 220.683 6.38497 2 1 13 5 80.6220 7.44281 2 1 13 7 37.8448 7.34471 2 1 13 9 292.630 11.1266 2 1 13 11 265.931 10.8865 2 1 13 13 71.4448 10.5924 2 -1 -13 -15 18.2860 15.3373 2 -1 -13 -17 57.7545 33.8279 2 -1 -13 -19-5.51454 31.9876 2 1 14 -39 14.3751 15.0075 2 1 14 -37-8.98149 14.8538 2 1 14 -35 53.4485 15.8928 2 -1 -14 33 4.62013 18.4457 2 -1 -14 31 33.1086 16.1271 2 -1 -14 29-18.9340 18.6590 2 -1 -14 27 22.8447 22.6975 2 1 14 -14 81.2668 9.41376 2 -1 -14 12 85.3219 8.16048 2 -1 -14 10 273.999 8.82264 2 1 14 -8 15.1622 6.39577 2 1 14 -6 150.034 7.03843 2 -1 -14 4 11.6795 5.95669 2 -1 -14 2 87.7153 6.07502 2 -1 -14 0 48.4039 5.06817 2 -1 -14 -2 102.577 5.89874 2 1 14 4 113.527 8.18545 2 1 14 6 40.2876 7.81680 2 1 14 8 87.4328 9.10986 2 1 14 10 36.3086 8.86645 2 1 14 12 58.9520 12.5893 2 1 14 14 20.1665 15.9416 2 1 14 16 147.499 26.4535 2 1 14 18-12.3641 21.7389 2 1 15 -38-7.53226 14.7553 2 1 15 -36 27.3959 16.3460 2 -1 -15 34 1.68228 18.0098 2 -1 -15 32 170.354 25.2148 2 -1 -15 30 35.8525 19.4261 2 -1 -15 28 76.6933 43.7985 2 1 15 -15 206.300 13.9143 2 -1 -15 13 5.37206 6.45169 2 -1 -15 11 384.763 9.27928 2 -1 -15 9-3.97136 6.45679 2 1 15 -7 49.7710 5.84669 2 1 15 -5-1.01258 5.80071 2 -1 -15 3 35.4667 5.86364 2 -1 -15 1 0.19769 4.92347 2 -1 -15 -1 114.809 6.21644 2 -1 -15 -3 111.868 5.82224 2 1 15 5 164.537 9.83876 2 1 15 7 24.9121 7.68808 2 1 15 9 83.2637 10.1824 2 1 15 11 30.9632 14.0204 2 1 15 13 25.7869 19.9916 2 1 15 15 12.0006 21.7532 2 1 15 17 20.3447 22.5752 2 1 16 -37 18.4656 15.9807 2 -1 -16 35-10.2152 14.9144 2 -1 -16 33 61.2365 20.0222 2 -1 -16 31 73.1360 21.3863 2 -1 -16 16-1.19326 11.8364 2 -1 -16 14 6.61080 6.70897 2 -1 -16 12 90.6977 7.45046 2 -1 -16 10 15.6720 6.96187 2 -1 -16 8 371.041 10.9785 2 1 16 -6 24.8657 5.97486 2 1 16 -4 55.5678 6.05632 2 -1 -16 2 5.93122 6.16958 2 -1 -16 0 12.8836 5.81720 2 -1 -16 -2-8.56190 5.76423 2 1 16 4 79.6611 8.12169 2 -1 -16 -6 160.784 10.2247 2 1 16 8 130.601 9.91483 2 1 16 10 16.1765 12.9622 2 1 16 12 36.0450 14.4205 2 1 16 14 24.4477 20.6518 2 1 16 20-31.8158 32.6516 2 1 17 -36-10.6318 14.4518 2 -1 -17 34 9.72061 16.0498 2 -1 -17 32 14.2553 21.9184 2 1 17 -22 491.008 26.9387 2 -1 -17 17 91.6055 32.5520 2 1 17 -15 19.5555 9.18850 2 -1 -17 13 9.78649 6.73735 2 -1 -17 11 6.28130 6.33442 2 -1 -17 9 252.337 9.70241 2 -1 -17 7 150.712 8.58266 2 1 17 -5 32.5028 7.30604 2 1 17 -3 101.403 7.38957 2 -1 -17 1 53.3942 6.77075 2 1 17 1 0.88969 6.19544 2 1 17 3 8.75600 7.43264 2 1 17 5 98.3834 9.86410 2 1 17 7 78.7341 11.5341 2 1 17 9 40.1336 16.9504 2 1 17 11 8.94264 16.4041 2 1 17 13 70.0797 21.4434 2 1 18 -35 78.8027 16.6878 2 -1 -18 33 0.00105 18.8084 2 -1 -18 31 20.3620 46.9243 2 1 18 -18 144.370 20.7292 2 1 18 -16 64.7118 10.1099 2 -1 -18 14 101.071 8.18758 2 -1 -18 12 97.9547 7.74982 2 -1 -18 10 20.0265 6.48276 2 -1 -18 8 54.2201 8.85719 2 1 18 -6 40.6238 7.78230 2 1 18 -4-1.57571 6.99928 2 1 18 -2 53.9839 7.68913 2 1 18 0 7.70944 6.52021 2 1 18 2 71.3909 8.70017 2 1 18 4-1.52303 9.28943 2 1 18 6-4.24924 9.77302 2 1 18 8 20.7563 16.3766 2 1 18 10 12.1698 22.2270 2 1 18 12 17.0296 22.2164 2 -1 -19 34 31.8150 30.3732 2 -1 -19 32 28.5289 34.3840 2 -1 -19 26 28.4830 30.6294 2 1 19 -21 54.3228 40.6764 2 1 19 -19 19.0365 21.1954 2 -1 -19 17 6.20058 16.1650 2 -1 -19 15 223.216 11.7971 2 -1 -19 13 31.8502 8.83195 2 -1 -19 11 204.971 11.0518 2 -1 -19 9 10.9805 7.79987 2 1 19 -7 8.51458 7.61906 2 1 19 -5 18.0257 7.30591 2 1 19 -3 41.7006 8.35456 2 1 19 -1 4.84118 8.49051 2 1 19 1 92.4177 9.50521 2 1 19 3 64.9240 10.0561 2 -1 -19 -5 44.9017 12.6194 2 -1 -19 -7 68.2195 20.3669 2 -1 -20 33 34.0416 37.1075 2 1 20 -20 6.47915 24.7580 2 -1 -20 18-1.31997 14.1680 2 1 20 -16 18.4787 12.3550 2 -1 -20 14 6.09436 9.70013 2 -1 -20 12 29.0320 9.29233 2 -1 -20 10 2.96920 8.38707 2 -1 -20 8 28.4411 9.17998 2 1 20 -6 32.7868 7.94172 2 1 20 -4 20.1679 8.05073 2 1 20 -2 1.71134 8.61184 2 1 20 0 8.56583 8.73241 2 1 20 2 84.9979 12.3802 2 -1 -20 -4 60.2101 13.8377 2 1 20 6 66.1095 19.3209 2 -1 -20 -8 12.7043 34.7832 2 1 21 -21 42.2605 42.7058 2 -1 -21 19-19.8809 36.8544 2 1 21 -17 27.1879 12.0325 2 1 21 -15 12.5460 10.5950 2 -1 -21 13 8.05969 9.39655 2 -1 -21 11-9.01502 8.82288 2 1 21 -9 89.5347 9.84144 2 1 21 -7 6.58740 8.99544 2 1 21 -5 59.6582 9.30213 2 1 21 -3 6.53132 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100.805 51.1921 2 1 24 -22-19.4437 30.9847 2 1 24 -20 80.7114 20.1713 2 1 24 -18 10.7263 12.7104 2 -1 -24 16 7.52258 12.2591 2 1 24 -14 12.9282 11.8020 2 1 24 -12 27.9325 11.8437 2 1 24 -10 4.23102 11.8160 2 1 24 -8 15.4574 12.4118 2 1 24 -6 16.8967 12.5579 2 1 24 -4-0.93347 13.1768 2 1 24 -2 6.42441 12.4863 2 1 24 0 4.02003 12.7970 2 1 24 2-13.5344 25.9203 2 -1 -24 -4-23.2902 47.8917 2 1 24 6-6.21791 37.8554 2 1 25 -23 3.33362 45.2261 2 1 25 -21 50.7953 18.8990 2 -1 -25 19 36.8551 14.8560 2 1 25 -17 6.83055 13.1486 2 1 25 -15 11.4150 14.2968 2 1 25 -13 31.6973 15.2917 2 1 25 -11 10.3611 14.7808 2 1 25 -9 23.6290 14.8758 2 1 25 -7 42.8381 14.6631 2 1 25 -5 24.6556 14.7104 2 1 25 -3 1.79725 14.6163 2 1 25 -1-2.46543 16.5549 2 1 25 1-9.31471 23.6747 2 -1 -25 -3 27.8346 54.4039 2 1 26 -20 26.0273 18.5168 2 1 26 -18 36.8061 17.9879 2 1 26 -16-0.86755 15.9708 2 1 26 -14-1.53621 15.8009 2 1 26 -12-5.39735 15.0313 2 1 26 -10 13.4489 15.8257 2 1 26 -8 46.2044 15.7146 2 1 26 -6 31.2008 14.5749 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163.872 14.3272 2 2 15 -23 85.3054 10.1686 2 2 15 -21 196.372 10.3495 2 -2 -15 19 125.880 9.13247 2 2 15 -17 7.08944 6.76836 2 2 15 -15 2.95112 6.54720 2 2 15 -13 33.7370 11.2010 2 -2 -15 6 46.0231 14.3348 2 -2 -15 2 133.858 22.7957 2 -2 -15 0 27.1051 17.0455 2 -2 -15 -2 101.104 10.5909 2 -2 -15 -4 11.6427 11.1590 2 2 15 6 24.0163 9.21856 2 2 15 8-5.33254 8.47164 2 2 15 10 67.6232 10.2884 2 2 15 12-0.58262 9.10933 2 2 15 14 75.5965 11.6049 2 2 15 16 1.67147 11.0667 2 2 15 18-14.4001 13.9159 2 2 15 20-11.1813 16.1810 2 2 15 22 37.7795 19.5464 2 -2 -15 -24-5.85921 21.7077 2 -2 -15 -26 8.64014 30.9350 2 2 16 -38 71.9229 23.4059 2 2 16 -36 10.1205 15.2097 2 2 16 -34 43.5988 15.0682 2 2 16 -32-7.62589 12.6724 2 2 16 -30 10.0551 13.0255 2 2 16 -28 19.5277 13.5536 2 2 16 -26 43.0691 13.0527 2 2 16 -24 9.62735 11.4801 2 2 16 -22 32.3442 9.35614 2 2 16 -20 49.8647 8.79218 2 2 16 -18 12.5633 7.73580 2 2 16 -16 31.8333 7.37370 2 2 16 -14 86.6072 10.8570 2 -2 -16 12 20.3492 18.1695 2 -2 -16 6 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1.62094 17.4329 2 5 -8 27 3.13796 12.9535 2 5 -8 29 66.8295 15.2065 2 5 -8 31 24.8842 14.7232 2 -5 8 -33 43.3524 15.4150 2 -5 8 -35 34.6940 18.2129 2 -5 8 -37 5.20617 18.7160 2 -5 7 23-15.8446 20.3759 2 -5 7 21 549.411 20.8715 2 -5 7 19 14.4052 11.6845 2 5 -7 -17 1031.93 18.5461 2 5 -7 -15 12.8602 7.36876 2 5 -7 -13 7.86068 6.68068 2 5 -7 -11 5.59403 3.33339 2 5 -7 -9 142.297 5.43210 2 5 -7 -7 368.512 7.85409 2 5 -7 -5 505.766 8.21247 2 5 -7 -3 279.420 5.63857 2 5 -7 -1 14.7514 3.60897 2 5 -7 1 421.232 5.66247 2 5 -7 3 487.502 6.17349 2 5 -7 5 257.485 7.42026 2 -5 7 -7 334.476 9.86432 2 5 -7 9 647.655 18.7444 2 5 -7 16 22.7477 6.16828 2 -5 7 -20 228.460 22.1092 2 -5 7 -22 4.39386 31.1267 2 5 -7 24-12.6776 19.2708 2 -5 7 -26-3.11522 11.8929 2 5 -7 28 18.3713 14.3807 2 5 -7 30 10.8764 13.8497 2 -5 7 -32 57.7532 18.0354 2 -5 7 -34 13.6181 17.7383 2 -5 7 -36 94.4467 23.2512 2 -5 7 -38 48.3912 20.2307 2 -5 6 26 91.5110 28.5028 2 -5 6 24-3.05442 23.9154 2 -5 6 22 29.3015 11.4522 2 -5 6 20 121.793 21.4600 2 5 -6 -18 355.882 14.6170 2 5 -6 -16 4.09071 7.69531 2 5 -6 -14 181.219 7.15717 2 5 -6 -12 689.924 9.08132 2 5 -6 -10 24.5066 3.76297 2 5 -6 -8 15.8338 4.43199 2 -5 6 6 45.5019 4.25220 2 5 -6 -4 722.813 7.97249 2 5 -6 -2 42.1956 4.19585 2 5 -6 0 151.650 4.94897 2 5 -6 2 92.3357 4.22392 2 5 -6 4 18.4801 4.22799 2 -5 6 -6 146.926 5.68232 2 5 -6 8 18.9817 4.54258 2 -5 6 -10 157.621 9.74838 2 -5 6 -12 399.084 15.7191 2 -5 6 -13 115.851 13.7814 2 -5 6 -14 1322.27 26.7043 2 -5 6 -15 49.0336 8.96887 2 -5 6 -17 436.169 24.8893 2 -5 6 -19 24.7491 16.4434 2 -5 6 -21 201.652 15.1812 2 -5 6 -23 15.6657 15.0213 2 -5 6 -25 33.1326 15.7446 2 5 -6 27 5.30197 14.3277 2 5 -6 29-8.21149 13.8839 2 -5 6 -31 31.5720 17.3212 2 -5 6 -33 16.8639 18.9010 2 -5 6 -35 67.3094 22.3240 2 -5 6 -37 9.17230 20.9699 2 -5 5 25 13.7287 25.5332 2 -5 5 23 208.113 31.4753 2 5 -5 -21 142.815 10.7268 2 5 -5 -19 21.4296 9.96824 2 5 -5 -17 125.809 8.61027 2 5 -5 -15 121.393 8.74203 2 5 -5 -13 662.724 9.78009 2 5 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9.71355 5.11207 2 -7 4 -16 17.8064 4.73954 2 7 -4 18 51.5143 9.03952 2 7 -4 20-0.76363 8.43967 2 7 -4 22 178.105 16.1169 2 7 -4 24 13.5453 15.4664 2 7 -4 26-2.96206 20.4556 2 7 -4 28-9.60674 24.5945 2 -7 4 -30 10.8170 39.9237 2 -7 4 -32 14.3622 40.5360 2 -7 4 -34 41.8564 44.5425 2 7 -3 -38 22.2379 52.3810 2 -7 3 36 12.1032 23.7549 2 -7 3 34 5.12391 32.5495 2 -7 3 32-17.4744 25.9512 2 -7 3 30 60.3307 22.9182 2 7 -3 -28-2.55327 12.8858 2 7 -3 -26 293.627 14.8640 2 -7 3 24 160.826 18.5672 2 -7 3 22 303.739 21.7825 2 -7 3 20 33.1819 12.3267 2 -7 3 18 0.84014 8.31474 2 -7 3 16 612.156 16.6353 2 -7 3 14 302.390 7.57509 2 -7 3 12 172.129 9.61327 2 -7 3 10 130.167 7.93978 2 7 -3 -8 472.281 15.4073 2 -7 3 7 736.626 41.1368 2 7 -3 -6-0.10142 3.69464 2 7 -3 -5 624.781 9.99750 2 -7 3 4 29.9001 6.07174 2 7 -3 -3 349.040 6.61133 2 7 -3 -2 208.720 6.14069 2 7 -3 -1 734.819 7.21468 2 7 -3 0 898.462 19.9233 2 7 -3 1 55.7814 3.97175 2 -7 3 -2 84.6235 9.73965 2 7 -3 3 75.8691 4.47143 2 7 -3 5 33.8677 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8.01466 10.6073 2 -9 15 -18 0.68239 9.67675 2 -9 15 -20 6.88844 11.9711 2 -9 15 -21 26.0263 20.7556 2 -9 15 -22 23.8659 15.4603 2 -9 15 -24 43.7955 32.0555 2 -9 15 -26-21.4383 38.4418 2 -9 14 30-3.10415 17.9366 2 -9 14 28-79.9941 44.1052 2 -9 14 26 62.3114 50.1476 2 -9 14 24 85.5107 50.9841 2 -9 14 22 2.45375 25.8797 2 -9 14 20 5.36662 26.9110 2 -9 14 18 84.8584 37.8238 2 -9 14 5 2.30485 12.3370 2 9 -14 -3 204.411 13.9814 2 9 -14 -1 0.84978 11.0882 2 -9 14 -1 398.750 14.9631 2 -9 14 -3 91.1780 11.5634 2 -9 14 -5 36.6812 10.4104 2 -9 14 -7 4.39105 9.06687 2 9 -14 9 111.936 11.2792 2 -9 14 -11 200.952 11.1350 2 -9 14 -13 5.40597 8.06109 2 -9 14 -15 170.930 11.8414 2 -9 14 -17 7.06699 9.29795 2 -9 14 -19 18.5861 10.7797 2 -9 14 -21 8.97551 17.0121 2 -9 14 -23 45.0531 31.1566 2 -9 14 -25-7.19441 39.8608 2 -9 14 -27 10.6683 40.0322 2 -9 13 31-29.1221 19.7931 2 -9 13 29 4.07106 48.4525 2 -9 13 27-28.0950 43.7404 2 -9 13 25 47.1560 50.1324 2 -9 13 23 80.4203 44.7969 2 -9 13 21 5.12869 25.3552 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230.836 18.9178 2 -9 -10 -1 4.68179 14.4415 2 9 10 3 17.1410 12.3877 2 9 10 5 10.9535 17.2961 2 9 10 7 16.2968 23.0421 2 -9 -10 -16-4.58589 52.0439 2 -9 -10 -18 54.8925 40.1189 2 -9 -10 -20-3.50688 26.2316 2 -9 -10 -22-12.0104 30.5037 2 -9 -11 26 33.7698 50.5745 2 9 11 -24 63.1011 20.6931 2 9 11 -22 49.4127 19.2668 2 9 11 -20 23.9408 14.2753 2 9 11 -18 92.7943 14.2699 2 9 11 -16 22.6831 12.0850 2 9 11 -14 12.3617 10.9382 2 9 11 -12 20.6428 11.5369 2 9 11 -10 246.826 12.8986 2 9 11 -8 18.0864 8.95966 2 9 11 -6 90.5708 10.6939 2 9 11 -4 2.96706 9.27532 2 9 11 -2 10.5612 12.8359 2 -9 -11 0 57.1318 16.6554 2 -9 -11 -2 13.1956 16.2507 2 -9 -11 -4 15.6909 17.6958 2 -9 -11 -15 100.876 42.7075 2 -9 -11 -17 9.43556 27.9752 2 -9 -11 -19 9.10621 28.8036 2 -9 -12 29-30.9176 51.4946 2 -9 -12 27 5.00032 46.8796 2 9 12 -25 56.3570 24.1397 2 9 12 -23 26.3300 18.3803 2 9 12 -21 77.3404 15.0811 2 9 12 -19 81.7479 15.3267 2 9 12 -17-3.12825 13.9416 2 9 12 -15 86.0746 13.0385 2 9 12 -13 29.3661 11.5102 2 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4.55611 16.4545 2 9 20 -15 18.4820 17.0508 2 9 20 -13 10.7169 15.1985 2 9 20 -11 54.9178 20.0681 2 9 20 -9 27.1270 35.4286 2 -9 -21 12 11.4497 47.3700 2 10 -26 -3 7.80032 15.1393 2 10 -26 -1 7.61472 15.2053 2 10 -26 1-1.37723 16.1876 2 10 -26 3 1.35112 17.6039 2 -10 26 -5 120.149 26.4951 2 -10 26 -6 24.8354 42.4335 2 -10 26 -7 30.4753 49.5533 2 -10 26 -9-8.45211 44.8408 2 -10 26 -11-12.2730 46.9081 2 -10 25 8 24.9750 16.8761 2 10 -25 -6 9.54791 15.3726 2 10 -25 -4 48.0849 15.3704 2 10 -25 -2-4.84216 14.9744 2 10 -25 0 12.5502 16.6117 2 10 -25 2 26.3775 16.7593 2 -10 25 -4 12.8942 24.5147 2 -10 25 -6-48.6802 46.5611 2 -10 25 -8 215.846 57.3487 2 -10 24 11 10.8501 15.4950 2 -10 24 9 2.67467 15.4685 2 -10 24 7 24.3083 16.7524 2 10 -24 -5 35.1249 15.1875 2 10 -24 -3 19.9273 16.2769 2 10 -24 -1 80.5249 16.9783 2 10 -24 1-1.61795 16.2531 2 10 -24 3 93.7501 22.4158 2 -10 24 -5 35.5433 48.2094 2 -10 24 -7 126.232 56.1853 2 10 -24 11 222.583 64.4980 2 -10 23 14 17.7277 21.2254 2 -10 23 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17.2310 2 -10 18 -22 93.1444 17.8812 2 -10 18 -24-11.7068 14.8948 2 -10 18 -26 47.8787 16.1720 2 -10 17 26-27.0354 41.0172 2 -10 17 24 10.2624 32.7187 2 -10 17 22-19.2020 27.2965 2 -10 17 20 13.6399 20.3928 2 -10 17 18 14.7484 19.1385 2 -10 17 16 44.4651 15.5822 2 10 -17 -14 35.8648 15.2725 2 10 -17 -12 30.9931 14.5370 2 10 -17 -10 45.2967 13.7875 2 -10 17 8 24.4130 14.4904 2 -10 17 6 11.6192 17.8095 2 -10 17 4 4.39600 19.1710 2 -10 17 2 143.233 22.4491 2 -10 17 0 52.5131 27.1417 2 -10 17 -4 105.340 21.7673 2 -10 17 -9 8.72030 36.3860 2 -10 17 -11-35.7424 34.4090 2 -10 17 -13 35.0589 32.9847 2 -10 17 -15 17.9135 25.4841 2 10 -17 17 13.8521 18.1366 2 10 -17 19 27.2429 22.1490 2 10 -17 21-42.2494 16.1463 2 -10 17 -23 15.2658 15.5304 2 -10 17 -25 68.2482 16.0231 2 10 -17 27-0.05786 16.7403 2 10 -17 29 25.5754 18.2684 2 -10 16 27-9.60508 39.3770 2 -10 16 25-12.3106 30.4862 2 -10 16 23 16.4877 23.2781 2 -10 16 21 10.3670 18.9662 2 -10 16 19 3.47503 15.6827 2 10 -16 -17-5.98887 12.4496 2 10 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30.7401 2 -10 15 -2-27.2669 29.0911 2 -10 15 -9 34.5257 35.2112 2 -10 15 -11 25.0769 25.2306 2 -10 15 -13 14.2523 25.3752 2 -10 15 -15 66.8289 22.9338 2 -10 15 -17 9.65615 13.5341 2 -10 15 -19 86.6264 12.4846 2 -10 15 -21 1.71958 10.8789 2 -10 15 -23 12.1716 15.1645 2 10 -15 25 10.6666 15.7249 2 10 -15 27 18.7885 17.0480 2 10 -15 29 0.67822 17.5470 2 -10 14 29-14.1024 36.9933 2 -10 14 27-25.9037 28.5000 2 -10 14 25 43.7058 26.7898 2 -10 14 23-11.0761 20.5792 2 -10 14 21-10.6046 17.8087 2 10 -14 -19 25.4119 10.5560 2 10 -14 -17 7.22175 9.24677 2 10 -14 -15 82.1119 13.3289 2 -10 14 13-10.6018 11.9877 2 -10 14 11 198.295 15.5847 2 -10 14 9 19.1666 13.8063 2 -10 14 7 34.6153 13.6286 2 -10 14 5-16.1040 17.8522 2 10 -14 -3 217.317 19.7577 2 10 -14 -1 19.6367 19.1862 2 -10 14 -6 93.9598 40.8779 2 -10 14 -8-8.73816 31.4873 2 -10 14 -10 30.5118 35.9263 2 -10 14 -12 22.5858 24.8743 2 10 -14 14-1.26927 17.7112 2 -10 14 -16 5.53566 13.5016 2 -10 14 -18 94.8412 14.4211 2 -10 14 -20 12.2281 10.9342 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62.4021 35.4327 2 -15 7 -14-4.05773 32.3771 2 15 -7 16 35.3950 29.6015 2 -15 6 30-4.29376 46.5272 2 -15 6 24-21.9533 35.2609 2 -15 6 22 30.9795 38.1148 2 -15 6 21 17.4087 49.3873 2 -15 6 20 43.3617 35.5696 2 -15 6 19-19.7152 31.0573 2 -15 6 18-17.7344 35.1613 2 -15 6 17 76.6055 37.3412 2 15 -6 -15 58.1382 24.6893 2 15 -6 -13 52.9041 17.9284 2 15 -6 -11 10.7987 16.2806 2 15 -6 -9 17.7590 15.1010 2 -15 6 7 7.47490 13.6161 2 15 -6 -5 0.08796 12.1912 2 15 -6 -3 17.6271 12.6794 2 15 -6 -1 3.90111 11.5164 2 15 -6 1-0.29177 14.2910 2 15 -6 3 5.47028 12.0996 2 15 -6 5 4.74245 14.6894 2 15 -6 7 5.78883 18.3156 2 -15 6 -9 23.4551 24.4843 2 -15 6 -11 51.7231 32.5629 2 -15 6 -13 29.0322 32.7921 2 15 -6 15 10.6861 47.7199 2 -15 5 29 45.7758 49.6263 2 -15 5 23 15.1207 34.5514 2 -15 5 22 72.2169 48.7646 2 -15 5 21 20.9023 32.9722 2 -15 5 20 12.7396 48.1910 2 -15 5 19 165.987 45.4207 2 -15 5 18 17.7410 32.6846 2 15 -5 -16 81.0926 25.9115 2 15 -5 -14 22.6026 23.9975 2 15 -5 -12 4.51853 12.7660 2 15 -5 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16.9404 28.0281 2 -17 2 -3-4.05758 42.5225 2 17 -1 -25 24.9278 26.6677 2 17 -1 -23-3.49767 22.8628 2 17 -1 -21 28.1776 18.1536 2 17 -1 -19 17.7317 18.5271 2 -17 1 17 11.7488 15.7314 2 17 -1 -15 26.4793 16.9720 2 -17 1 13 25.9292 22.5817 2 -17 1 11 10.1440 22.6203 2 17 -1 -9 2.11882 20.1297 2 17 -1 -7 17.2974 20.3105 2 17 -1 -5 10.2823 21.3540 2 17 -1 -3 2.88715 22.1855 2 17 -1 -1 42.9537 34.7652 2 17 -1 1-27.3320 39.0398 2 -17 1 -4 39.4320 43.5158 2 17 0 -24-7.57296 19.9252 2 17 0 -22-2.96082 19.3997 2 17 0 -20-12.6464 16.6979 2 17 0 -18 15.4736 14.9910 2 17 0 -16 16.3157 15.7596 2 17 0 -14 6.20833 22.7268 2 -17 0 12 16.7122 24.3482 2 -17 0 10 19.6296 24.4585 2 17 0 -8 5.21319 29.7536 2 17 0 -6 16.8365 29.6316 2 17 0 -4 22.6599 30.2551 2 17 0 -2 62.4378 53.0257 2 -17 0 -1 31.8204 47.1913 2 -17 0 -3 50.8212 45.5492 2 17 1 -23 12.5187 20.4808 2 17 1 -21-11.3883 16.5533 2 17 1 -19 15.7867 15.1860 2 17 1 -17 13.4858 16.5227 2 17 1 -15 30.4261 22.6723 2 17 1 -13 7.92863 20.6937 2 -17 -1 11-34.7031 24.0886 2 17 1 -9 18.8491 30.1629 2 17 1 -7-12.8867 29.1413 2 17 1 -5-8.30664 30.3562 2 17 1 -3 84.9251 52.4378 2 -17 -1 0-7.81113 45.3384 2 -17 -1 -2 23.1427 45.4322 2 17 2 -22-3.99111 18.6440 2 17 2 -20-1.16946 15.0924 2 17 2 -18 8.31815 17.3146 2 17 2 -16-2.91594 20.3484 2 17 2 -14-6.08633 20.8455 2 17 2 -12 25.0621 22.5349 2 -17 -2 10 34.6083 28.4342 2 17 2 -8-6.43772 31.5028 2 17 2 -6 7.53233 32.3714 2 17 2 -4 40.2425 53.3218 2 17 2 -2 28.0796 51.1440 2 -17 -2 1-3.82548 46.0208 2 17 2 5-26.5614 42.0237 2 17 3 -23 35.9260 24.1217 2 17 3 -21-4.10173 17.1099 2 17 3 -19-0.23335 15.7356 2 17 3 -17 6.82869 24.9349 2 17 3 -15-1.31290 22.0993 2 17 3 -13 15.1971 22.4519 2 17 3 -11 41.2945 23.7250 2 17 3 -9 41.9479 35.4660 2 17 3 -7 72.6456 37.5853 2 17 3 -5 21.6104 34.4692 2 17 4 -20 14.6970 17.5590 2 17 4 -18-18.2839 19.0084 2 17 4 -16 13.2606 26.3990 2 17 4 -14-1.94059 22.5108 2 17 4 -12-30.2527 25.3446 2 17 4 -10 55.8369 34.8612 2 17 4 -8 72.0624 48.5364 2 17 4 -6 68.9239 55.4337 2 17 4 -4 8.63350 52.6232 2 -17 -5 19-34.0443 34.4251 2 17 5 -17 20.4739 29.0681 2 17 5 -15-8.76056 26.1481 2 17 5 -13 12.2273 26.5261 2 17 5 -11 52.0448 34.1791 2 17 5 -9-48.1509 42.4910 2 17 5 -7-17.6734 52.5850 2 -17 -6 18 2.70871 33.7409 2 17 6 -16 3.87368 26.5732 2 17 6 -14 99.3121 36.6771 2 17 6 -12 22.9917 34.6676 2 17 6 -10-8.94254 54.3273 2 17 6 -8 63.0853 54.9324 2 -18 15 6-61.5267 31.6843 2 -18 15 4 11.9072 35.3253 2 -18 15 2-29.8153 36.4010 2 -18 15 0 8.31794 35.9951 2 -18 14 11 16.0569 58.0703 2 -18 14 9-16.7912 41.8261 2 -18 14 7 49.5403 46.8264 2 -18 14 5-0.65857 34.1001 2 -18 14 3-27.5043 31.9149 2 -18 14 1 4.49186 34.0631 2 -18 14 -1 20.6107 28.9444 2 -18 14 -3 5.54511 30.0310 2 -18 13 12-42.6717 52.4721 2 -18 13 10 19.6502 31.5445 2 -18 13 8 49.7290 42.7286 2 -18 13 6-13.9816 44.3827 2 -18 13 4 27.4063 34.8172 2 -18 13 2 7.51261 28.1052 2 -18 13 0-56.6366 26.9314 2 -18 13 -2 41.6306 29.7615 2 -18 13 -4 0.81377 28.4944 2 -18 12 15 15.9326 58.3461 2 -18 12 14-12.5056 47.7896 2 -18 12 13-10.5933 48.7769 2 -18 12 11-33.4657 29.6669 2 -18 12 9 14.8870 24.1107 2 -18 12 7 26.1241 41.5854 2 -18 12 5 44.8674 43.4199 2 -18 12 3-10.8602 40.7103 2 -18 12 1 1.61954 26.7648 2 -18 12 -1 43.8960 29.0133 2 -18 12 -3-38.3591 26.7251 2 -18 12 -5-58.9937 26.1284 2 18 -12 7 35.3543 18.1040 2 -18 11 16-20.9770 55.6765 2 -18 11 15-23.6564 43.6256 2 -18 11 14 5.17605 33.3172 2 -18 11 12 17.0842 32.3498 2 -18 11 10 5.08790 29.5111 2 -18 11 8 0.32667 23.5955 2 -18 11 6-14.6904 30.0106 2 -18 11 4-4.57160 30.2745 2 -18 11 2 7.95764 31.5839 2 -18 11 0 22.6417 28.9166 2 -18 11 -2-13.1577 27.2611 2 -18 11 -4 10.2670 28.0209 2 18 -11 6-18.3801 15.4388 2 -18 10 17-16.9910 31.3754 2 -18 10 16 110.723 49.6646 2 -18 10 15-26.1450 32.4232 2 -18 10 14 15.2493 43.8666 2 -18 10 13 22.0492 33.3330 2 -18 10 11 23.1955 33.6244 2 -18 10 9 7.65683 23.2928 2 -18 10 7 1.25237 23.8518 2 -18 10 5 31.5478 24.5855 2 -18 10 3-27.7444 31.7934 2 -18 10 1 60.7607 34.7772 2 -18 10 -1-17.7542 27.3665 2 -18 10 -3 35.5410 28.9342 2 18 -10 5 44.2774 16.3550 2 18 -10 7 10.7843 16.0497 2 -18 9 18-5.42906 33.7129 2 -18 9 17 54.9553 44.3930 2 -18 9 16-10.4725 34.4964 2 -18 9 15-56.7169 40.4709 2 -18 9 14 0.48712 33.7091 2 -18 9 12-11.1062 29.9822 2 -18 9 10-24.2438 35.0278 2 -18 9 8 6.06888 24.4261 2 -18 9 6 43.3801 26.0624 2 -18 9 4 30.9341 22.7406 2 -18 9 2 7.38663 29.7207 2 -18 9 0-2.10279 30.8831 2 -18 9 -2 3.76452 27.1017 2 -18 9 -4 8.27819 23.3618 2 18 -9 6 50.8216 16.1759 2 -18 9 -8 2.37278 32.4756 2 -18 8 19 31.2946 34.0486 2 -18 8 17-20.9527 34.4801 2 -18 8 16 42.5200 40.0792 2 -18 8 15-16.4188 35.6339 2 -18 8 14 13.5298 41.8706 2 -18 8 13-18.1300 32.7914 2 -18 8 11-2.25761 35.5866 2 -18 8 9 13.4385 26.8913 2 -18 8 7 33.7663 21.7888 2 -18 8 5 11.0981 21.5171 2 -18 8 3-10.8411 21.1857 2 -18 8 1-0.11470 28.2865 2 -18 8 -1-5.18087 30.4255 2 -18 8 -3 5.92238 25.7290 2 18 -8 5 23.9847 15.5355 2 -18 8 -7-32.6266 32.1337 2 -18 7 20 32.4880 35.7205 2 -18 7 18-5.39319 34.2409 2 -18 7 16 44.3027 35.4583 2 -18 7 15 37.1810 36.9472 2 -18 7 14 25.8570 34.8882 2 -18 7 12-12.7751 31.5648 2 -18 7 10-22.2837 32.7512 2 -18 7 8 32.1643 26.6309 2 -18 7 6 35.8757 22.3135 2 18 -7 -4-2.85145 18.5808 2 18 -7 -2 16.7661 16.3996 2 -18 7 0 12.3931 30.2409 2 -18 7 -2 18.8369 27.7546 2 18 -7 4-0.86048 15.7293 2 -18 7 -6 5.84863 30.9036 2 -18 7 -8 1.68808 32.1308 2 -18 6 19 13.1275 35.0928 2 -18 6 17-30.1892 32.4416 2 -18 6 15 36.7221 34.6897 2 -18 6 13 48.9426 35.6299 2 18 -6 -11 42.5573 23.5296 2 18 -6 -9 2.57612 23.1561 2 18 -6 -7 0.50670 22.1551 2 18 -6 -5-5.10807 15.9531 2 18 -6 -3-9.87369 16.0710 2 18 -6 -1-8.96164 17.8718 2 18 -6 1-8.38372 21.1418 2 18 -6 3 63.4201 18.5966 2 -18 6 -5-12.0305 24.5073 2 -18 6 -7 11.6157 30.7315 2 -18 5 20 67.3928 50.9451 2 -18 5 18-33.4464 32.4413 2 -18 5 16-19.4020 34.0967 2 -18 5 14 4.35678 34.6764 2 18 -5 -12 5.61371 21.2186 2 18 -5 -10 54.3960 23.7243 2 18 -5 -8 4.74467 19.2247 2 18 -5 -6-4.34772 18.3182 2 18 -5 -4-13.4561 16.0618 2 18 -5 -2-2.12243 16.6041 2 18 -5 0 21.3800 19.5096 2 18 -5 2 105.703 18.5965 2 -18 5 -4 18.9870 28.8293 2 -18 5 -6 46.6470 31.2905 2 -18 4 21 55.3613 36.6707 2 -18 4 19 11.7217 34.7304 2 -18 4 17-19.4160 35.3647 2 -18 4 15-11.2795 32.9647 2 18 -4 -13 40.8653 28.3233 2 18 -4 -11 39.6098 20.2388 2 18 -4 -9 65.3173 20.0145 2 18 -4 -7 7.38488 19.6055 2 18 -4 -5 22.0481 19.5045 2 18 -4 -3 1.74497 16.7898 2 18 -4 -1 3.20151 17.5093 2 18 -4 1-15.2432 15.5615 2 18 -4 3 7.67512 22.0163 2 -18 3 20 64.7006 37.1740 2 -18 3 18 18.9247 37.4843 2 -18 3 16-33.2684 31.8727 2 18 -3 -14-9.00755 26.5663 2 18 -3 -12-10.3078 23.1341 2 18 -3 -10 30.1172 23.9343 2 18 -3 -8 2.37658 18.7051 2 18 -3 -6-9.32375 18.6345 2 18 -3 -4 25.6625 19.0547 2 18 -3 -2-0.82050 20.6204 2 18 -3 0 34.9289 17.7003 2 18 -3 2-16.7042 21.6565 2 -18 2 19-9.44210 34.6622 2 -18 2 17 16.2084 34.9386 2 18 -2 -15 5.64430 27.7481 2 18 -2 -13 3.54182 28.2857 2 18 -2 -11 51.2530 24.4645 2 18 -2 -9-2.52762 22.9611 2 18 -2 -7 24.2772 18.8172 2 18 -2 -5 21.9111 19.6684 2 18 -2 -3-3.97818 19.5336 2 18 -2 -1 90.6011 19.9405 2 18 -2 1 10.0147 29.5915 2 18 -2 3 17.9782 27.7217 2 -18 1 20-7.96010 33.0531 2 -18 1 18-17.9034 33.5047 2 18 -1 -16 1.13764 27.6989 2 18 -1 -14-3.67295 28.7328 2 18 -1 -12 24.7959 24.2854 2 18 -1 -10 12.4210 19.9439 2 18 -1 -8 44.0485 21.0476 2 18 -1 -6 20.4277 20.4863 2 18 -1 -4-6.15287 19.9888 2 18 -1 -2 11.0406 16.8558 2 18 -1 0-35.7902 28.5879 2 18 -1 2 19.7314 29.8468 2 18 -1 4 66.9279 43.6963 2 -18 0 19 4.06807 33.8702 2 18 0 -17 10.0094 28.5358 2 18 0 -15-23.2655 22.6238 2 18 0 -13 0.16314 21.4708 2 18 0 -11-2.08992 20.5086 2 18 0 -9-10.8114 20.3601 2 18 0 -7 11.6974 20.0637 2 18 0 -5-0.75151 21.6593 2 18 0 -3-1.52861 18.9155 2 18 0 -1 20.5403 24.3173 2 18 0 1 2.03630 24.9016 2 18 1 -18 14.2592 28.0853 2 18 1 -16 4.01399 23.0103 2 18 1 -14-16.0292 20.9530 2 18 1 -12-20.9671 18.9463 2 18 1 -10-26.7320 21.8319 2 18 1 -8-35.9301 22.0848 2 18 1 -6 58.3145 23.4380 2 18 1 -4 18.3931 19.9257 2 18 1 -2 28.3608 26.4592 2 18 1 0 1.37418 26.5527 2 18 2 -17-5.05043 22.8292 2 18 2 -15 8.91289 21.5130 2 18 2 -13 13.2061 20.4603 2 18 2 -11 10.8314 20.6082 2 18 2 -9 4.48078 22.1533 2 18 2 -7-7.27678 22.7723 2 18 2 -5 26.1432 21.2788 2 18 2 -3-22.3656 22.1390 2 18 3 -14 32.2305 21.8880 2 18 3 -12-9.90324 20.3061 2 18 3 -10-25.6731 21.9234 2 18 3 -8 2.29053 20.5042 2 18 3 -6-20.6705 18.1213 2 -19 10 9-7.76836 44.6880 2 -19 10 7 31.8705 47.2002 2 -19 10 6 35.1096 53.9552 2 -19 10 5-4.04039 45.9711 2 -19 10 3-4.11478 47.5364 2 -19 9 10-14.6322 42.5496 2 -19 9 8-26.2219 40.7664 2 -19 9 7 4.99767 53.7630 2 -19 9 6-11.5289 43.7185 2 -19 9 5 14.6414 54.0636 2 -19 9 4 19.5217 45.6022 2 -19 9 2 7.95428 43.8391 2 -19 8 11 30.4183 39.1579 2 -19 8 9-3.50742 37.1871 2 -19 8 7-25.1542 40.7150 2 -19 8 6 87.7373 55.7243 2 -19 8 5-11.0902 40.0654 2 -19 8 4-9.55747 50.2886 2 -19 8 3 22.7104 43.0624 2 -19 7 10 41.7848 40.2847 2 -19 7 8-36.7786 40.0150 2 -19 7 7 24.1040 53.4030 2 -19 7 6-3.43493 39.8109 2 -19 7 5-80.6006 46.6417 2 -19 7 4 106.158 46.1642 2 -19 7 3-14.0164 49.3874 2 -19 7 1-11.9903 37.5633 2 -19 6 9-15.2149 38.4956 2 -19 6 7-44.4408 34.2408 2 -19 6 6 14.1561 48.2960 2 -19 6 5-13.1761 38.4558 2 -19 6 4 36.4081 36.2422 2 -19 6 3-27.0396 40.0357 2 19 -6 -2 9.85288 30.6197 2 -19 5 9 88.9940 49.9484 2 -19 5 8 20.2139 39.0483 2 -19 5 7-4.63703 50.0971 2 -19 5 6-21.0312 34.5487 2 -19 5 5-18.4490 53.7239 2 -19 5 4 9.36156 37.4736 2 19 -5 -3-4.20165 25.6789 2 19 -5 -1 28.8653 31.2724 2 -19 4 10-4.56608 47.1699 2 -19 4 8-18.3147 47.0813 2 -19 4 6-31.6945 46.3392 2 -19 4 5-22.7028 35.3359 2 19 -4 -4-37.9944 30.2298 2 -19 4 3-2.95192 35.5647 2 19 -4 -2 7.16558 23.4033 2 -19 3 11 44.2025 52.0403 2 -19 3 9 8.91154 50.9305 2 -19 3 7-8.91730 49.1840 2 -19 3 5 17.1061 35.7355 2 -19 2 8-21.6479 45.7568 2 0 0 0 0.00000 0.00000 0 TITL lk39db_twin1_hklf4 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 10.590538 15.427719 23.216728 101.0985 99.2340 103.2907 ZERR 4.00 0.000063 0.000117 0.000144 0.0006 0.0005 0.0006 LATT 1 SFAC C H N O F Fe UNIT 152.00 160.00 8.00 16.00 24.00 4.00 REM CrysAlisPro recorded range (K): Min=99.9; max=100.1; aver:100.0 TEMP -173 TREF HKLF 5 BASF 0.24867 END ; _shelx_hkl_checksum 69947 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.92366(3) 1.02387(2) 0.16775(2) 0.01347(5) Uani 1 1 d . . . . . F7 F 1.0890(3) 0.53299(13) 0.06081(11) 0.0487(5) Uani 1 1 d . . . . . F8 F 0.9039(3) 0.50046(15) 0.08675(19) 0.0778(10) Uani 1 1 d . . . . . F9 F 1.0830(4) 0.55530(16) 0.15371(11) 0.0646(8) Uani 1 1 d . . . . . O1 O 0.84438(16) 1.07875(11) 0.03101(7) 0.0210(3) Uani 1 1 d . . . . . O2 O 0.7180(2) 0.90329(14) 0.20907(11) 0.0351(4) Uani 1 1 d . . . . . O3 O 0.79099(18) 1.17183(12) 0.18722(9) 0.0265(3) Uani 1 1 d . . . . . O4 O 1.11407(18) 1.07983(13) 0.28442(7) 0.0261(3) Uani 1 1 d . . . . . N1 N 1.21958(15) 1.01854(11) 0.14757(7) 0.0155(2) Uani 1 1 d . . . . . N2 N 1.11497(16) 1.17722(11) 0.11890(7) 0.0154(2) Uani 1 1 d . . . . . C1 C 0.90749(18) 1.04483(12) 0.06548(8) 0.0155(3) Uani 1 1 d . . . . . C2 C 0.86285(17) 0.95332(12) 0.07763(8) 0.0144(2) Uani 1 1 d . . . . . C3 C 0.97717(17) 0.93016(11) 0.10780(8) 0.0134(2) Uani 1 1 d . . . . . C4 C 1.08847(17) 1.01089(12) 0.12253(8) 0.0135(2) Uani 1 1 d . . . . . C5 C 1.04084(17) 1.08654(12) 0.10756(8) 0.0141(2) Uani 1 1 d . . . . . C6 C 0.73144(17) 0.89126(12) 0.04568(8) 0.0149(2) Uani 1 1 d . . . . . C7 C 0.71731(19) 0.80118(13) 0.01451(9) 0.0185(3) Uani 1 1 d . . . . . H7 H 0.792834 0.777650 0.015744 0.022 Uiso 1 1 calc R U . . . C8 C 0.59369(19) 0.74569(14) -0.01830(10) 0.0197(3) Uani 1 1 d . . . . . H8 H 0.585156 0.684415 -0.038846 0.024 Uiso 1 1 calc R U . . . C9 C 0.48314(18) 0.77964(14) -0.02105(9) 0.0178(3) Uani 1 1 d . . . . . C10 C 0.49472(19) 0.86952(15) 0.00973(10) 0.0206(3) Uani 1 1 d . . . . . H10 H 0.418876 0.892730 0.008093 0.025 Uiso 1 1 calc R U . . . C11 C 0.6180(2) 0.92446(14) 0.04268(9) 0.0197(3) Uani 1 1 d . . . . . H11 H 0.625892 0.985455 0.063530 0.024 Uiso 1 1 calc R U . . . C12 C 0.3507(2) 0.72050(16) -0.05698(10) 0.0213(3) Uani 1 1 d . . . . . C13 C 0.98810(17) 0.83569(12) 0.10744(8) 0.0143(2) Uani 1 1 d . . . . . C14 C 0.9367(2) 0.78599(14) 0.14671(10) 0.0206(3) Uani 1 1 d . . . . . H14 H 0.894027 0.813062 0.175516 0.025 Uiso 1 1 calc R U . . . C15 C 0.9476(2) 0.69687(15) 0.14400(11) 0.0244(4) Uani 1 1 d . . . . . H15 H 0.912967 0.663631 0.171023 0.029 Uiso 1 1 calc R U . . . C16 C 1.0091(2) 0.65708(14) 0.10175(11) 0.0223(3) Uani 1 1 d . . . . . C17 C 1.0611(2) 0.70548(14) 0.06241(10) 0.0210(3) Uani 1 1 d . . . . . H17 H 1.103051 0.677762 0.033538 0.025 Uiso 1 1 calc R U . . . C18 C 1.0515(2) 0.79489(13) 0.06537(9) 0.0179(3) Uani 1 1 d . . . . . H18 H 1.088047 0.828265 0.038805 0.021 Uiso 1 1 calc R U . . . C19 C 1.0212(3) 0.56185(17) 0.10088(14) 0.0323(5) Uani 1 1 d . . . . . C20 C 1.25435(19) 0.95140(14) 0.17985(9) 0.0188(3) Uani 1 1 d . . . . . H20A H 1.261555 0.897460 0.150915 0.023 Uiso 1 1 calc R U . . . H20B H 1.183953 0.930336 0.201316 0.023 Uiso 1 1 calc R U . . . C21 C 1.3864(2) 0.99555(17) 0.22473(10) 0.0228(4) Uani 1 1 d . . . . . H21A H 1.411330 0.949811 0.245660 0.027 Uiso 1 1 calc R U . . . H21B H 1.377056 1.046821 0.255227 0.027 Uiso 1 1 calc R U . . . C22 C 1.4955(2) 1.03149(19) 0.19273(11) 0.0265(4) Uani 1 1 d . . . . . H22A H 1.511009 0.979495 0.165005 0.032 Uiso 1 1 calc R U . . . H22B H 1.579323 1.062925 0.222677 0.032 Uiso 1 1 calc R U . . . C23 C 1.4553(2) 1.09852(19) 0.15732(12) 0.0262(4) Uani 1 1 d . . . . . H23A H 1.451966 1.154371 0.185671 0.031 Uiso 1 1 calc R U . . . H23B H 1.522894 1.116898 0.133881 0.031 Uiso 1 1 calc R U . . . C24 C 1.31996(19) 1.05536(15) 0.11474(9) 0.0197(3) Uani 1 1 d . . . . . H24A H 1.292102 1.102036 0.095676 0.024 Uiso 1 1 calc R U . . . H24B H 1.326616 1.005226 0.082582 0.024 Uiso 1 1 calc R U . . . C25 C 1.1989(2) 1.21574(13) 0.17978(9) 0.0188(3) Uani 1 1 d . . . . . H25A H 1.245288 1.170713 0.191180 0.023 Uiso 1 1 calc R U . . . H25B H 1.141959 1.227075 0.208766 0.023 Uiso 1 1 calc R U . . . C26 C 1.3009(2) 1.30497(15) 0.18333(11) 0.0242(4) Uani 1 1 d . . . . . H26A H 1.361304 1.293229 0.156105 0.029 Uiso 1 1 calc R U . . . H26B H 1.354843 1.329323 0.224802 0.029 Uiso 1 1 calc R U . . . C27 C 1.2322(2) 1.37561(14) 0.16555(11) 0.0249(4) Uani 1 1 d . . . . . H27A H 1.299481 1.431199 0.164211 0.030 Uiso 1 1 calc R U . . . H27B H 1.180755 1.393523 0.195677 0.030 Uiso 1 1 calc R U . . . C28 C 1.1391(2) 1.33403(14) 0.10359(10) 0.0226(3) Uani 1 1 d . . . . . H28A H 1.087925 1.377439 0.093753 0.027 Uiso 1 1 calc R U . . . H28B H 1.192582 1.324627 0.072825 0.027 Uiso 1 1 calc R U . . . C29 C 1.0436(2) 1.24324(13) 0.10167(10) 0.0200(3) Uani 1 1 d . . . . . H29A H 0.983718 1.253607 0.129423 0.024 Uiso 1 1 calc R U . . . H29B H 0.988256 1.217143 0.060569 0.024 Uiso 1 1 calc R U . . . C30 C 0.7999(2) 0.94834(15) 0.19288(10) 0.0220(3) Uani 1 1 d . . . . . C31 C 0.84435(19) 1.11566(14) 0.17840(9) 0.0180(3) Uani 1 1 d . . . . . C32 C 1.0400(2) 1.05845(14) 0.23917(8) 0.0184(3) Uani 1 1 d . . . . . F1 F 0.3036(3) 0.7553(2) -0.10248(13) 0.0468(8) Uani 0.753(5) 1 d . U P A 1 F2 F 0.2570(2) 0.7130(2) -0.02538(12) 0.0459(8) Uani 0.753(5) 1 d . U P A 1 F3 F 0.3518(3) 0.63589(19) -0.08253(16) 0.0495(8) Uani 0.753(5) 1 d . U P A 1 F4 F 0.3603(9) 0.6817(7) -0.1091(4) 0.049(2) Uani 0.247(5) 1 d . U P A 2 F5 F 0.2579(10) 0.7627(7) -0.0575(5) 0.056(3) Uani 0.247(5) 1 d . U P A 2 F6 F 0.3071(10) 0.6519(7) -0.0307(5) 0.051(2) Uani 0.247(5) 1 d . U P A 2 Fe1A Fe 1.02648(3) 0.26003(2) 0.40157(2) 0.01543(5) Uani 1 1 d . . . . . F7A F 0.8020(3) 0.20128(19) 0.71752(10) 0.0636(8) Uani 1 1 d . . . . . F8A F 0.9531(3) 0.1309(2) 0.70711(11) 0.0603(7) Uani 1 1 d . . . . . F9A F 0.7534(3) 0.06545(18) 0.65938(11) 0.0565(6) Uani 1 1 d . . . . . O1A O 1.17370(17) 0.49524(12) 0.44516(7) 0.0242(3) Uani 1 1 d . . . . . O2A O 1.1576(3) 0.1211(2) 0.43128(10) 0.0455(6) Uani 1 1 d . . . . . O3A O 1.2072(2) 0.30804(18) 0.32158(9) 0.0355(5) Uani 1 1 d . . . . . O4A O 0.81243(19) 0.11687(12) 0.31317(8) 0.0262(3) Uani 1 1 d . . . . . N1A N 0.73845(16) 0.28993(12) 0.41649(8) 0.0179(3) Uani 1 1 d . . . . . N2A N 0.90475(17) 0.41347(11) 0.35251(7) 0.0162(2) Uani 1 1 d . . . . . C1A C 1.08685(19) 0.42575(13) 0.44405(8) 0.0170(3) Uani 1 1 d . . . . . C2A C 1.09778(18) 0.35998(13) 0.48194(8) 0.0159(3) Uani 1 1 d . . . . . C3A C 0.96503(18) 0.30431(13) 0.47914(8) 0.0150(3) Uani 1 1 d . . . . . C4A C 0.87490(17) 0.32337(13) 0.43232(8) 0.0151(3) Uani 1 1 d . . . . . C5A C 0.95300(18) 0.38386(12) 0.40251(8) 0.0153(3) Uani 1 1 d . . . . . C6A C 1.21909(19) 0.37691(14) 0.52855(8) 0.0173(3) Uani 1 1 d . . . . . C7A C 1.21496(19) 0.38422(16) 0.58929(8) 0.0201(3) Uani 1 1 d . . . . . H7A H 1.131750 0.374704 0.600890 0.024 Uiso 1 1 calc R U . . . C8A C 1.3315(2) 0.40529(17) 0.63284(9) 0.0217(3) Uani 1 1 d . . . . . H8A H 1.327303 0.409746 0.673840 0.026 Uiso 1 1 calc R U . . . C9A C 1.4532(2) 0.41973(16) 0.61658(9) 0.0212(3) Uani 1 1 d . . . . . C10A C 1.4605(2) 0.4152(2) 0.55660(10) 0.0285(5) Uani 1 1 d . . . . . H10A H 1.544300 0.427255 0.545619 0.034 Uiso 1 1 calc R U . . . C11A C 1.3437(2) 0.3929(2) 0.51297(9) 0.0262(4) Uani 1 1 d . . . . . H11A H 1.348425 0.388537 0.472031 0.031 Uiso 1 1 calc R U . . . C12A C 1.5778(2) 0.4438(2) 0.66433(11) 0.0282(4) Uani 1 1 d . . . . . C13A C 0.92752(19) 0.25855(13) 0.52723(8) 0.0165(3) Uani 1 1 d . . . . . C14A C 0.9737(3) 0.18500(19) 0.53948(12) 0.0305(5) Uani 1 1 d . . . . . H14A H 1.023808 0.158617 0.514064 0.037 Uiso 1 1 calc R U . . . C15A C 0.9474(3) 0.1497(2) 0.58854(13) 0.0346(6) Uani 1 1 d . . . . . H15A H 0.979907 0.099754 0.596594 0.042 Uiso 1 1 calc R U . . . C16A C 0.8738(3) 0.18755(17) 0.62546(10) 0.0267(4) Uani 1 1 d . . . . . C17A C 0.8275(2) 0.26127(16) 0.61418(10) 0.0232(3) Uani 1 1 d . . . . . H17A H 0.777477 0.287413 0.639759 0.028 Uiso 1 1 calc R U . . . C18A C 0.8544(2) 0.29669(14) 0.56533(8) 0.0186(3) Uani 1 1 d . . . . . H18A H 0.822946 0.347211 0.557795 0.022 Uiso 1 1 calc R U . . . C19A C 0.8450(4) 0.1470(2) 0.67729(14) 0.0409(7) Uani 1 1 d . . . . . C20A C 0.6706(2) 0.20646(16) 0.43201(10) 0.0225(3) Uani 1 1 d . . . . . H20C H 0.652506 0.222025 0.472733 0.027 Uiso 1 1 calc R U . . . H20D H 0.727982 0.164054 0.432131 0.027 Uiso 1 1 calc R U . . . C21A C 0.5399(2) 0.15997(17) 0.38611(11) 0.0258(4) Uani 1 1 d . . . . . H21C H 0.558775 0.140757 0.345903 0.031 Uiso 1 1 calc R U . . . H21D H 0.492809 0.104433 0.397262 0.031 Uiso 1 1 calc R U . . . C22A C 0.4518(2) 0.2250(2) 0.38373(13) 0.0321(5) Uani 1 1 d . . . . . H22C H 0.425586 0.239529 0.422770 0.039 Uiso 1 1 calc R U . . . H22D H 0.370106 0.195211 0.352222 0.039 Uiso 1 1 calc R U . . . C23A C 0.5260(2) 0.3134(2) 0.37002(13) 0.0293(5) Uani 1 1 d . . . . . H23C H 0.471050 0.357413 0.372620 0.035 Uiso 1 1 calc R U . . . H23D H 0.539959 0.299756 0.328439 0.035 Uiso 1 1 calc R U . . . C24A C 0.6603(2) 0.35719(16) 0.41356(10) 0.0228(3) Uani 1 1 d . . . . . H24C H 0.710121 0.409504 0.400173 0.027 Uiso 1 1 calc R U . . . H24D H 0.646107 0.380947 0.454089 0.027 Uiso 1 1 calc R U . . . C25A C 0.8154(2) 0.33970(14) 0.30241(8) 0.0188(3) Uani 1 1 d . . . . . H25C H 0.749513 0.299694 0.318438 0.023 Uiso 1 1 calc R U . . . H25D H 0.868007 0.301756 0.283252 0.023 Uiso 1 1 calc R U . . . C26A C 0.7429(2) 0.37799(17) 0.25546(10) 0.0239(4) Uani 1 1 d . . . . . H26C H 0.687115 0.413811 0.273967 0.029 Uiso 1 1 calc R U . . . H26D H 0.684106 0.326885 0.222675 0.029 Uiso 1 1 calc R U . . . C27A C 0.8430(3) 0.43951(17) 0.22979(9) 0.0256(4) Uani 1 1 d . . . . . H27C H 0.795913 0.467891 0.201441 0.031 Uiso 1 1 calc R U . . . H27D H 0.892959 0.402603 0.207681 0.031 Uiso 1 1 calc R U . . . C28A C 0.9389(3) 0.51417(16) 0.28157(10) 0.0239(4) Uani 1 1 d . . . . . H28C H 1.008431 0.551149 0.265618 0.029 Uiso 1 1 calc R U . . . H28D H 0.889857 0.555462 0.300122 0.029 Uiso 1 1 calc R U . . . C29A C 1.0047(2) 0.47352(15) 0.32950(9) 0.0212(3) Uani 1 1 d . . . . . H29C H 1.061815 0.437682 0.312111 0.025 Uiso 1 1 calc R U . . . H29D H 1.061988 0.523859 0.363195 0.025 Uiso 1 1 calc R U . . . C30A C 1.1066(3) 0.17599(19) 0.42179(10) 0.0271(4) Uani 1 1 d . . . . . C31A C 1.1358(2) 0.29111(17) 0.35244(9) 0.0223(3) Uani 1 1 d . . . . . C32A C 0.8954(2) 0.17306(14) 0.34699(9) 0.0193(3) Uani 1 1 d . . . . . F1A F 1.6455(5) 0.5359(4) 0.6746(3) 0.0557(14) Uani 0.472(5) 1 d . U P B 3 F2A F 1.6724(4) 0.4079(3) 0.64447(19) 0.0361(9) Uani 0.472(5) 1 d . U P B 3 F3A F 1.5635(5) 0.4291(5) 0.7143(2) 0.0530(13) Uani 0.472(5) 1 d . U P B 3 F4A F 1.5780(5) 0.5078(4) 0.7098(2) 0.0624(14) Uani 0.528(5) 1 d . U P B 4 F5A F 1.6843(5) 0.4620(5) 0.6456(2) 0.0585(13) Uani 0.528(5) 1 d . U P B 4 F6A F 1.5813(4) 0.3715(3) 0.6915(2) 0.0539(12) Uani 0.528(5) 1 d . U P B 4 C94 C 0.6033(4) 0.6690(3) 0.1969(2) 0.0541(6) Uani 1 1 d . . . . . H94A H 0.622084 0.667171 0.239713 0.065 Uiso 1 1 calc R U . . . H94B H 0.676832 0.716303 0.190341 0.065 Uiso 1 1 calc R U . . . C95 C 0.5953(5) 0.5752(3) 0.1573(3) 0.0613(7) Uani 1 1 d . . . . . H95A H 0.682969 0.562428 0.165450 0.074 Uiso 1 1 calc R U . . . H95B H 0.530174 0.527271 0.168158 0.074 Uiso 1 1 calc R U . . . C96 C 0.5547(5) 0.5697(4) 0.0906(3) 0.0679(8) Uani 1 1 d . . . . . H96A H 0.624612 0.612553 0.078356 0.081 Uiso 1 1 calc R U . . . H96B H 0.545755 0.506827 0.067367 0.081 Uiso 1 1 calc R U . . . C97 C 0.4248(5) 0.5937(4) 0.0766(3) 0.0683(9) Uani 1 1 d . . . . . H97A H 0.352839 0.546743 0.084469 0.082 Uiso 1 1 calc R U . . . H97B H 0.403271 0.593998 0.033557 0.082 Uiso 1 1 calc R U . . . C98 C 0.4331(5) 0.6875(4) 0.1150(2) 0.0580(7) Uani 1 1 d . . . . . H98A H 0.498730 0.734797 0.103859 0.070 Uiso 1 1 calc R U . . . H98B H 0.345651 0.700532 0.106385 0.070 Uiso 1 1 calc R U . . . C99 C 0.4728(4) 0.6941(4) 0.1817(2) 0.0553(7) Uani 1 1 d . . . . . H99A H 0.402019 0.652240 0.194094 0.066 Uiso 1 1 calc R U . . . H99B H 0.482449 0.757436 0.204358 0.066 Uiso 1 1 calc R U . . . C94A C 0.4210(6) 0.1128(5) 0.5405(4) 0.0858(12) Uani 1 1 d . . . . . H94C H 0.376388 0.149290 0.517653 0.103 Uiso 1 1 calc R U . . . H94D H 0.499138 0.105425 0.523702 0.103 Uiso 1 1 calc R U . . . C95A C 0.3350(6) 0.0275(5) 0.5317(3) 0.0766(10) Uani 1 1 d . . . . . H95C H 0.386211 -0.013971 0.544908 0.092 Uiso 1 1 calc R U . . . H95D H 0.297420 0.003355 0.488099 0.092 Uiso 1 1 calc R U . . . C96A C 0.2244(5) 0.0243(4) 0.5631(3) 0.0675(9) Uani 1 1 d . . . . . H96C H 0.163127 0.056039 0.544712 0.081 Uiso 1 1 calc R U . . . H96D H 0.174469 -0.040467 0.557364 0.081 Uiso 1 1 calc R U . . . C97A C 0.2672(6) 0.0666(4) 0.6274(3) 0.0754(10) Uani 1 1 d . . . . . H97C H 0.187109 0.067559 0.644119 0.090 Uiso 1 1 calc R U . . . H97D H 0.313103 0.027092 0.646684 0.090 Uiso 1 1 calc R U . . . C98A C 0.3541(8) 0.1586(5) 0.6440(4) 0.0947(15) Uani 1 1 d . . . . . H98C H 0.395898 0.174639 0.687351 0.114 Uiso 1 1 calc R U . . . H98D H 0.301969 0.202583 0.636763 0.114 Uiso 1 1 calc R U . . . C99A C 0.4687(8) 0.1656(6) 0.6046(4) 0.1070(18) Uani 1 1 d . . . . . H99C H 0.506676 0.230883 0.605574 0.128 Uiso 1 1 calc R U . . . H99D H 0.540972 0.142895 0.623838 0.128 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.01483(10) 0.01351(10) 0.01259(9) 0.00269(7) 0.00356(7) 0.00476(8) F7 0.0813(16) 0.0297(8) 0.0574(12) 0.0188(8) 0.0388(12) 0.0352(10) F8 0.0581(15) 0.0195(8) 0.158(3) 0.0197(13) 0.0393(18) 0.0048(9) F9 0.130(3) 0.0434(11) 0.0436(11) 0.0233(9) 0.0212(13) 0.0554(15) O1 0.0240(6) 0.0175(6) 0.0192(6) 0.0078(5) -0.0035(5) 0.0036(5) O2 0.0339(9) 0.0279(8) 0.0544(13) 0.0172(8) 0.0277(9) 0.0108(7) O3 0.0258(7) 0.0242(7) 0.0320(8) 0.0044(6) 0.0073(6) 0.0131(6) O4 0.0285(8) 0.0313(8) 0.0169(6) 0.0032(6) -0.0009(5) 0.0108(6) N1 0.0131(5) 0.0171(6) 0.0169(6) 0.0057(5) 0.0034(4) 0.0038(4) N2 0.0190(6) 0.0118(5) 0.0140(5) 0.0027(4) 0.0017(5) 0.0031(5) C1 0.0176(6) 0.0138(6) 0.0137(6) 0.0032(5) 0.0008(5) 0.0036(5) C2 0.0158(6) 0.0138(6) 0.0130(6) 0.0030(5) 0.0016(5) 0.0044(5) C3 0.0139(6) 0.0120(6) 0.0144(6) 0.0033(5) 0.0038(5) 0.0031(5) C4 0.0144(6) 0.0135(6) 0.0132(6) 0.0035(5) 0.0037(5) 0.0040(5) C5 0.0161(6) 0.0133(6) 0.0122(6) 0.0027(5) 0.0021(5) 0.0032(5) C6 0.0147(6) 0.0141(6) 0.0150(6) 0.0022(5) 0.0024(5) 0.0040(5) C7 0.0157(7) 0.0158(7) 0.0215(7) -0.0001(6) 0.0016(6) 0.0048(5) C8 0.0156(7) 0.0172(7) 0.0232(8) 0.0010(6) 0.0008(6) 0.0035(5) C9 0.0136(6) 0.0196(7) 0.0189(7) 0.0049(6) 0.0016(5) 0.0028(5) C10 0.0158(7) 0.0214(8) 0.0238(8) 0.0039(6) 0.0022(6) 0.0062(6) C11 0.0189(7) 0.0175(7) 0.0223(8) 0.0023(6) 0.0020(6) 0.0078(6) C12 0.0166(7) 0.0242(8) 0.0220(8) 0.0069(7) 0.0026(6) 0.0032(6) C13 0.0161(6) 0.0135(6) 0.0140(6) 0.0036(5) 0.0037(5) 0.0045(5) C14 0.0256(8) 0.0176(7) 0.0252(8) 0.0104(6) 0.0133(7) 0.0091(6) C15 0.0309(10) 0.0189(8) 0.0315(10) 0.0136(7) 0.0166(8) 0.0097(7) C16 0.0273(9) 0.0150(7) 0.0275(9) 0.0073(6) 0.0087(7) 0.0076(6) C17 0.0290(9) 0.0171(7) 0.0211(8) 0.0051(6) 0.0101(7) 0.0108(7) C18 0.0233(8) 0.0165(7) 0.0172(7) 0.0059(5) 0.0081(6) 0.0078(6) C19 0.0462(14) 0.0177(8) 0.0410(13) 0.0118(9) 0.0188(11) 0.0139(9) C20 0.0168(7) 0.0190(7) 0.0208(7) 0.0074(6) 0.0003(6) 0.0053(6) C21 0.0177(7) 0.0290(10) 0.0213(8) 0.0085(7) 0.0008(6) 0.0056(7) C22 0.0156(7) 0.0371(12) 0.0286(10) 0.0127(9) 0.0037(7) 0.0073(7) C23 0.0155(7) 0.0334(11) 0.0291(10) 0.0118(8) 0.0047(7) 0.0019(7) C24 0.0173(7) 0.0252(8) 0.0183(7) 0.0074(6) 0.0060(6) 0.0059(6) C25 0.0217(8) 0.0154(7) 0.0160(7) 0.0016(5) 0.0005(6) 0.0024(6) C26 0.0238(9) 0.0168(7) 0.0263(9) 0.0030(7) 0.0007(7) -0.0004(6) C27 0.0296(10) 0.0141(7) 0.0270(9) 0.0020(6) 0.0038(8) 0.0018(7) C28 0.0303(10) 0.0141(7) 0.0221(8) 0.0056(6) 0.0031(7) 0.0044(7) C29 0.0227(8) 0.0133(6) 0.0223(8) 0.0049(6) 0.0001(6) 0.0041(6) C30 0.0244(8) 0.0193(8) 0.0260(9) 0.0064(7) 0.0109(7) 0.0088(6) C31 0.0175(7) 0.0191(7) 0.0169(7) 0.0029(6) 0.0037(5) 0.0049(6) C32 0.0216(7) 0.0210(7) 0.0144(6) 0.0041(6) 0.0046(6) 0.0087(6) F1 0.0357(11) 0.0523(14) 0.0404(12) 0.0278(11) -0.0167(9) -0.0087(10) F2 0.0228(9) 0.0673(16) 0.0337(11) 0.0044(10) 0.0105(8) -0.0119(9) F3 0.0289(10) 0.0307(11) 0.0681(17) -0.0132(11) -0.0150(10) 0.0056(8) F4 0.043(3) 0.054(3) 0.039(3) 0.002(2) 0.011(2) 0.003(2) F5 0.048(3) 0.052(3) 0.066(3) 0.007(2) 0.002(2) 0.024(2) F6 0.048(3) 0.049(3) 0.050(3) 0.022(2) 0.004(2) 0.000(2) Fe1A 0.01668(11) 0.01880(11) 0.01187(10) 0.00309(8) 0.00342(8) 0.00705(9) F7A 0.115(2) 0.0665(15) 0.0405(11) 0.0322(11) 0.0512(14) 0.0458(16) F8A 0.0750(17) 0.0847(19) 0.0401(11) 0.0426(12) 0.0167(11) 0.0327(14) F9A 0.0711(15) 0.0524(13) 0.0554(13) 0.0345(11) 0.0301(12) 0.0055(11) O1A 0.0235(7) 0.0237(7) 0.0188(6) 0.0075(5) -0.0014(5) -0.0045(5) O2A 0.0673(16) 0.0637(15) 0.0326(10) 0.0242(10) 0.0224(10) 0.0523(14) O3A 0.0256(8) 0.0618(14) 0.0242(8) 0.0136(8) 0.0128(6) 0.0137(8) O4A 0.0291(8) 0.0230(7) 0.0216(7) 0.0014(5) 0.0030(6) 0.0024(6) N1A 0.0144(6) 0.0210(7) 0.0190(6) 0.0065(5) 0.0042(5) 0.0041(5) N2A 0.0192(6) 0.0166(6) 0.0122(5) 0.0041(4) 0.0026(5) 0.0042(5) C1A 0.0188(7) 0.0186(7) 0.0121(6) 0.0038(5) 0.0014(5) 0.0032(6) C2A 0.0157(6) 0.0192(7) 0.0121(6) 0.0040(5) 0.0025(5) 0.0037(5) C3A 0.0168(6) 0.0165(6) 0.0126(6) 0.0042(5) 0.0036(5) 0.0050(5) C4A 0.0154(6) 0.0166(6) 0.0134(6) 0.0038(5) 0.0025(5) 0.0046(5) C5A 0.0177(6) 0.0151(6) 0.0130(6) 0.0042(5) 0.0029(5) 0.0042(5) C6A 0.0168(7) 0.0219(8) 0.0128(6) 0.0031(5) 0.0025(5) 0.0058(6) C7A 0.0169(7) 0.0304(9) 0.0134(6) 0.0054(6) 0.0044(5) 0.0062(6) C8A 0.0193(7) 0.0315(10) 0.0139(7) 0.0061(6) 0.0021(6) 0.0067(7) C9A 0.0171(7) 0.0290(9) 0.0165(7) 0.0049(6) 0.0014(6) 0.0064(6) C10A 0.0164(8) 0.0480(14) 0.0184(8) 0.0047(8) 0.0037(6) 0.0064(8) C11A 0.0179(8) 0.0446(13) 0.0145(7) 0.0061(8) 0.0047(6) 0.0056(8) C12A 0.0198(8) 0.0392(12) 0.0229(9) 0.0059(8) -0.0016(7) 0.0081(8) C13A 0.0185(7) 0.0174(7) 0.0149(6) 0.0058(5) 0.0045(5) 0.0051(5) C14A 0.0440(13) 0.0329(11) 0.0313(11) 0.0193(9) 0.0215(10) 0.0236(10) C15A 0.0522(16) 0.0359(12) 0.0353(12) 0.0246(10) 0.0240(12) 0.0268(12) C16A 0.0362(11) 0.0283(10) 0.0212(8) 0.0131(7) 0.0124(8) 0.0095(8) C17A 0.0293(9) 0.0249(9) 0.0183(7) 0.0069(7) 0.0106(7) 0.0079(7) C18A 0.0238(8) 0.0187(7) 0.0139(6) 0.0036(5) 0.0060(6) 0.0059(6) C19A 0.0612(19) 0.0437(15) 0.0326(12) 0.0249(12) 0.0245(13) 0.0200(14) C20A 0.0175(7) 0.0240(9) 0.0231(8) 0.0084(7) 0.0017(6) -0.0003(6) C21A 0.0182(8) 0.0270(10) 0.0258(9) 0.0040(8) 0.0005(7) -0.0015(7) C22A 0.0159(8) 0.0408(14) 0.0362(12) 0.0075(10) 0.0034(8) 0.0036(8) C23A 0.0187(8) 0.0341(12) 0.0358(12) 0.0096(9) 0.0021(8) 0.0104(8) C24A 0.0186(7) 0.0256(9) 0.0252(9) 0.0040(7) 0.0051(6) 0.0092(7) C25A 0.0215(8) 0.0189(7) 0.0141(6) 0.0032(5) 0.0001(6) 0.0047(6) C26A 0.0247(9) 0.0272(9) 0.0185(8) 0.0062(7) -0.0010(6) 0.0079(7) C27A 0.0337(11) 0.0284(10) 0.0153(7) 0.0087(7) 0.0023(7) 0.0085(8) C28A 0.0339(10) 0.0218(8) 0.0168(7) 0.0081(6) 0.0049(7) 0.0063(7) C29A 0.0240(8) 0.0221(8) 0.0160(7) 0.0073(6) 0.0028(6) 0.0023(6) C30A 0.0344(11) 0.0376(12) 0.0178(8) 0.0082(8) 0.0091(7) 0.0227(10) C31A 0.0183(7) 0.0321(10) 0.0171(7) 0.0046(7) 0.0043(6) 0.0083(7) C32A 0.0236(8) 0.0187(7) 0.0167(7) 0.0038(6) 0.0057(6) 0.0072(6) F1A 0.0430(19) 0.0438(19) 0.062(2) 0.0062(17) -0.0249(16) 0.0072(15) F2A 0.0222(13) 0.0458(19) 0.0381(16) 0.0007(14) -0.0032(11) 0.0195(13) F3A 0.0355(17) 0.089(3) 0.0307(16) 0.0233(17) 0.0020(13) 0.0054(17) F4A 0.057(2) 0.062(2) 0.0485(19) -0.0213(15) -0.0238(15) 0.0301(17) F5A 0.0389(17) 0.085(3) 0.0464(19) 0.0209(19) 0.0108(14) 0.0005(17) F6A 0.0467(18) 0.0479(19) 0.058(2) 0.0270(16) -0.0225(14) 0.0059(14) C94 0.0373(11) 0.0588(14) 0.0753(14) 0.0394(12) 0.0109(11) 0.0120(10) C95 0.0474(16) 0.0606(15) 0.0846(15) 0.0367(13) 0.0171(12) 0.0131(12) C96 0.0641(17) 0.065(2) 0.0829(14) 0.0322(13) 0.0155(12) 0.0212(16) C97 0.0632(16) 0.0736(17) 0.0749(14) 0.0308(14) 0.0133(13) 0.0221(14) C98 0.0504(16) 0.0698(17) 0.0642(13) 0.0368(12) 0.0112(10) 0.0201(14) C99 0.0398(12) 0.0731(18) 0.0651(13) 0.0403(12) 0.0129(10) 0.0184(13) C94A 0.070(2) 0.087(2) 0.107(2) 0.0292(18) 0.027(2) 0.0228(17) C95A 0.0598(18) 0.085(2) 0.092(2) 0.0320(18) 0.0141(16) 0.0265(14) C96A 0.0540(16) 0.069(2) 0.0791(18) 0.0203(15) 0.0049(13) 0.0199(14) C97A 0.066(2) 0.075(2) 0.0804(18) 0.0170(15) 0.0016(14) 0.0207(16) C98A 0.092(3) 0.082(2) 0.094(2) 0.0053(19) 0.015(2) 0.0072(18) C99A 0.090(2) 0.102(3) 0.115(2) 0.017(2) 0.0232(19) 0.005(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 6 -9 -26 0.0761 -10 0 -17 0.1933 -14 5 -5 0.1876 -14 9 11 0.2027 0 7 27 0.0897 0 -20 19 0.0910 -13 -2 -3 0.1860 1 19 -18 0.0675 12 -11 15 0.1650 -5 19 -20 0.1162 6 -16 -16 0.0979 10 3 14 0.1380 6 9 18 0.1041 2 12 19 0.0851 0 14 18 0.0845 -3 16 18 0.0953 -9 17 13 0.1425 12 3 -23 0.1336 4 6 -32 0.0745 3 19 0 0.0625 11 6 7 0.1300 0 21 -1 0.0559 -2 22 -3 0.0732 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C30 Fe1 C31 93.12(9) . . ? C30 Fe1 C32 94.15(10) . . ? C31 Fe1 C32 98.33(9) . . ? C30 Fe1 C3 100.17(8) . . ? C31 Fe1 C3 146.79(8) . . ? C32 Fe1 C3 110.77(8) . . ? C30 Fe1 C2 95.14(9) . . ? C31 Fe1 C2 107.85(8) . . ? C32 Fe1 C2 151.63(8) . . ? C3 Fe1 C2 41.09(7) . . ? C30 Fe1 C4 136.25(8) . . ? C31 Fe1 C4 129.57(8) . . ? C32 Fe1 C4 89.12(8) . . ? C3 Fe1 C4 39.52(6) . . ? C2 Fe1 C4 65.92(7) . . ? C30 Fe1 C5 161.01(9) . . ? C31 Fe1 C5 91.98(8) . . ? C32 Fe1 C5 103.20(8) . . ? C3 Fe1 C5 66.61(6) . . ? C2 Fe1 C5 65.89(7) . . ? C4 Fe1 C5 38.27(6) . . ? C30 Fe1 C1 125.39(9) . . ? C31 Fe1 C1 84.11(8) . . ? C32 Fe1 C1 140.33(8) . . ? C3 Fe1 C1 63.36(6) . . ? C2 Fe1 C1 37.07(6) . . ? C4 Fe1 C1 61.09(6) . . ? C5 Fe1 C1 37.22(6) . . ? C4 N1 C20 120.85(15) . . ? C4 N1 C24 116.53(15) . . ? C20 N1 C24 113.92(15) . . ? C5 N2 C25 115.52(15) . . ? C5 N2 C29 116.74(15) . . ? C25 N2 C29 109.86(15) . . ? O1 C1 C2 126.65(17) . . ? O1 C1 C5 129.40(17) . . ? C2 C1 C5 103.84(14) . . ? O1 C1 Fe1 139.02(15) . . ? C2 C1 Fe1 58.22(9) . . ? C5 C1 Fe1 63.56(9) . . ? C3 C2 C1 108.81(15) . . ? C3 C2 C6 128.34(15) . . ? C1 C2 C6 120.27(15) . . ? C3 C2 Fe1 68.18(9) . . ? C1 C2 Fe1 84.70(10) . . ? C6 C2 Fe1 128.41(13) . . ? C4 C3 C2 107.43(14) . . ? C4 C3 C13 124.80(15) . . ? C2 C3 C13 125.55(15) . . ? C4 C3 Fe1 75.98(10) . . ? C2 C3 Fe1 70.72(10) . . ? C13 C3 Fe1 132.17(12) . . ? N1 C4 C3 127.52(16) . . ? N1 C4 C5 123.90(15) . . ? C3 C4 C5 108.57(15) . . ? N1 C4 Fe1 129.05(12) . . ? C3 C4 Fe1 64.50(9) . . ? C5 C4 Fe1 71.68(10) . . ? N2 C5 C4 126.38(16) . . ? N2 C5 C1 125.66(15) . . ? C4 C5 C1 106.61(14) . . ? N2 C5 Fe1 126.44(12) . . ? C4 C5 Fe1 70.06(9) . . ? C1 C5 Fe1 79.23(10) . . ? C7 C6 C11 118.38(17) . . ? C7 C6 C2 121.66(16) . . ? C11 C6 C2 119.81(16) . . ? C8 C7 C6 120.70(17) . . ? C9 C8 C7 120.16(18) . . ? C8 C9 C10 120.21(17) . . ? C8 C9 C12 120.19(18) . . ? C10 C9 C12 119.60(18) . . ? C11 C10 C9 119.45(18) . . ? C10 C11 C6 121.10(18) . . ? F4 C12 F5 113.8(7) . . ? F2 C12 F3 107.1(3) . . ? F4 C12 F6 105.8(7) . . ? F5 C12 F6 103.1(7) . . ? F2 C12 F1 104.3(2) . . ? F3 C12 F1 105.6(3) . . ? F4 C12 C9 110.7(4) . . ? F5 C12 C9 113.2(5) . . ? F2 C12 C9 113.3(2) . . ? F3 C12 C9 113.87(19) . . ? F6 C12 C9 109.6(4) . . ? F1 C12 C9 111.9(2) . . ? C14 C13 C18 119.01(16) . . ? C14 C13 C3 122.69(16) . . ? C18 C13 C3 118.29(15) . . ? C15 C14 C13 120.57(18) . . ? C16 C15 C14 119.77(19) . . ? C15 C16 C17 120.51(18) . . ? C15 C16 C19 118.3(2) . . ? C17 C16 C19 121.2(2) . . ? C16 C17 C18 119.88(18) . . ? C17 C18 C13 120.25(17) . . ? F8 C19 F9 106.8(3) . . ? F8 C19 F7 105.8(3) . . ? F9 C19 F7 106.4(3) . . ? F8 C19 C16 112.2(2) . . ? F9 C19 C16 112.3(2) . . ? F7 C19 C16 112.9(2) . . ? N1 C20 C21 109.44(17) . . ? C20 C21 C22 110.62(18) . . ? C21 C22 C23 110.22(18) . . ? C24 C23 C22 111.2(2) . . ? N1 C24 C23 110.64(17) . . ? N2 C25 C26 111.60(17) . . ? C25 C26 C27 110.51(19) . . ? C26 C27 C28 109.20(17) . . ? C29 C28 C27 111.71(18) . . ? N2 C29 C28 111.47(17) . . ? O2 C30 Fe1 176.9(2) . . ? O3 C31 Fe1 176.46(19) . . ? O4 C32 Fe1 179.5(2) . . ? C30A Fe1A C31A 93.24(11) . . ? C30A Fe1A C32A 91.81(11) . . ? C31A Fe1A C32A 98.68(10) . . ? C30A Fe1A C3A 101.34(9) . . ? C31A Fe1A C3A 145.51(9) . . ? C32A Fe1A C3A 111.76(8) . . ? C30A Fe1A C2A 98.34(10) . . ? C31A Fe1A C2A 106.25(9) . . ? C32A Fe1A C2A 152.38(8) . . ? C3A Fe1A C2A 41.09(7) . . ? C30A Fe1A C4A 135.94(9) . . ? C31A Fe1A C4A 130.19(9) . . ? C32A Fe1A C4A 88.78(8) . . ? C3A Fe1A C4A 39.53(7) . . ? C2A Fe1A C4A 66.13(7) . . ? C30A Fe1A C5A 164.30(9) . . ? C31A Fe1A C5A 92.31(9) . . ? C32A Fe1A C5A 101.85(8) . . ? C3A Fe1A C5A 66.53(7) . . ? C2A Fe1A C5A 65.99(7) . . ? C4A Fe1A C5A 38.34(7) . . ? C30A Fe1A C1A 129.25(10) . . ? C31A Fe1A C1A 83.57(9) . . ? C32A Fe1A C1A 138.84(8) . . ? C3A Fe1A C1A 62.97(7) . . ? C2A Fe1A C1A 36.96(7) . . ? C4A Fe1A C1A 60.97(7) . . ? C5A Fe1A C1A 37.14(6) . . ? C4A N1A C20A 121.11(16) . . ? C4A N1A C24A 117.38(17) . . ? C20A N1A C24A 114.34(17) . . ? C5A N2A C25A 114.57(15) . . ? C5A N2A C29A 116.16(16) . . ? C25A N2A C29A 110.06(15) . . ? O1A C1A C2A 126.29(18) . . ? O1A C1A C5A 129.71(17) . . ? C2A C1A C5A 103.85(15) . . ? O1A C1A Fe1A 139.31(16) . . ? C2A C1A Fe1A 57.92(10) . . ? C5A C1A Fe1A 63.16(10) . . ? C3A C2A C6A 128.06(16) . . ? C3A C2A C1A 108.43(15) . . ? C6A C2A C1A 120.10(17) . . ? C3A C2A Fe1A 68.62(10) . . ? C6A C2A Fe1A 129.62(14) . . ? C1A C2A Fe1A 85.12(11) . . ? C4A C3A C2A 107.57(15) . . ? C4A C3A C13A 126.35(16) . . ? C2A C3A C13A 123.94(16) . . ? C4A C3A Fe1A 75.68(10) . . ? C2A C3A Fe1A 70.29(10) . . ? C13A C3A Fe1A 132.51(13) . . ? N1A C4A C3A 127.50(17) . . ? N1A C4A C5A 124.26(16) . . ? C3A C4A C5A 108.24(15) . . ? N1A C4A Fe1A 128.61(13) . . ? C3A C4A Fe1A 64.80(10) . . ? C5A C4A Fe1A 71.39(10) . . ? N2A C5A C4A 126.27(16) . . ? N2A C5A C1A 125.64(16) . . ? C4A C5A C1A 106.59(15) . . ? N2A C5A Fe1A 126.37(13) . . ? C4A C5A Fe1A 70.27(10) . . ? C1A C5A Fe1A 79.70(11) . . ? C7A C6A C11A 118.28(17) . . ? C7A C6A C2A 121.82(17) . . ? C11A C6A C2A 119.73(17) . . ? C8A C7A C6A 120.73(18) . . ? C9A C8A C7A 120.19(18) . . ? C8A C9A C10A 120.30(19) . . ? C8A C9A C12A 119.37(19) . . ? C10A C9A C12A 120.3(2) . . ? C11A C10A C9A 119.4(2) . . ? C10A C11A C6A 121.05(19) . . ? F5A C12A F4A 111.5(5) . . ? F3A C12A F2A 111.7(4) . . ? F5A C12A F6A 106.5(4) . . ? F4A C12A F6A 100.9(4) . . ? F3A C12A F1A 106.7(4) . . ? F2A C12A F1A 97.6(4) . . ? F3A C12A C9A 116.3(3) . . ? F5A C12A C9A 114.6(3) . . ? F4A C12A C9A 111.9(3) . . ? F2A C12A C9A 111.9(3) . . ? F6A C12A C9A 110.3(3) . . ? F1A C12A C9A 110.9(3) . . ? C14A C13A C18A 118.70(18) . . ? C14A C13A C3A 122.41(18) . . ? C18A C13A C3A 118.56(17) . . ? C13A C14A C15A 120.9(2) . . ? C16A C15A C14A 119.7(2) . . ? C15A C16A C17A 120.3(2) . . ? C15A C16A C19A 118.6(2) . . ? C17A C16A C19A 121.2(2) . . ? C16A C17A C18A 119.9(2) . . ? C17A C18A C13A 120.56(19) . . ? F7A C19A F8A 106.8(3) . . ? F7A C19A F9A 107.4(3) . . ? F8A C19A F9A 105.4(3) . . ? F7A C19A C16A 113.0(3) . . ? F8A C19A C16A 111.6(3) . . ? F9A C19A C16A 112.2(3) . . ? N1A C20A C21A 109.53(18) . . ? C22A C21A C20A 110.7(2) . . ? C21A C22A C23A 110.1(2) . . ? C22A C23A C24A 111.9(2) . . ? N1A C24A C23A 110.80(19) . . ? N2A C25A C26A 111.78(17) . . ? C25A C26A C27A 110.10(18) . . ? C26A C27A C28A 108.86(18) . . ? C29A C28A C27A 111.78(18) . . ? N2A C29A C28A 111.42(18) . . ? O2A C30A Fe1A 176.1(2) . . ? O3A C31A Fe1A 177.3(2) . . ? O4A C32A Fe1A 178.7(2) . . ? C99 C94 C95 110.2(4) . . ? C96 C95 C94 112.9(4) . . ? C97 C96 C95 110.8(5) . . ? C96 C97 C98 110.5(5) . . ? C99 C98 C97 112.8(4) . . ? C98 C99 C94 111.1(4) . . ? C95A C94A C99A 115.0(7) . . ? C94A C95A C96A 115.4(6) . . ? C97A C96A C95A 113.5(5) . . ? C98A C97A C96A 116.2(6) . . ? C97A C98A C99A 109.9(6) . . ? C94A C99A C98A 114.3(6) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 C30 1.795(2) . ? Fe1 C31 1.803(2) . ? Fe1 C32 1.804(2) . ? Fe1 C3 2.0503(17) . ? Fe1 C2 2.0847(17) . ? Fe1 C4 2.2039(17) . ? Fe1 C5 2.2255(18) . ? Fe1 C1 2.4418(18) . ? F7 C19 1.334(3) . ? F8 C19 1.325(4) . ? F9 C19 1.328(4) . ? O1 C1 1.229(2) . ? O2 C30 1.142(3) . ? O3 C31 1.143(3) . ? O4 C32 1.145(2) . ? N1 C4 1.385(2) . ? N1 C20 1.468(2) . ? N1 C24 1.478(2) . ? N2 C5 1.389(2) . ? N2 C25 1.474(2) . ? N2 C29 1.478(3) . ? C1 C2 1.478(3) . ? C1 C5 1.503(2) . ? C2 C3 1.452(2) . ? C2 C6 1.479(2) . ? C3 C4 1.445(2) . ? C3 C13 1.487(2) . ? C4 C5 1.452(2) . ? C6 C7 1.400(3) . ? C6 C11 1.407(3) . ? C7 C8 1.393(3) . ? C8 C9 1.386(3) . ? C9 C10 1.400(3) . ? C9 C12 1.497(3) . ? C10 C11 1.389(3) . ? C12 F4 1.272(9) . ? C12 F5 1.298(10) . ? C12 F2 1.322(3) . ? C12 F3 1.329(3) . ? C12 F6 1.349(9) . ? C12 F1 1.351(3) . ? C13 C14 1.397(3) . ? C13 C18 1.403(3) . ? C14 C15 1.396(3) . ? C15 C16 1.386(3) . ? C16 C17 1.389(3) . ? C16 C19 1.501(3) . ? C17 C18 1.396(3) . ? C20 C21 1.526(3) . ? C21 C22 1.528(3) . ? C22 C23 1.531(4) . ? C23 C24 1.526(3) . ? C25 C26 1.521(3) . ? C26 C27 1.526(3) . ? C27 C28 1.534(3) . ? C28 C29 1.516(3) . ? Fe1A C30A 1.798(2) . ? Fe1A C31A 1.803(2) . ? Fe1A C32A 1.805(2) . ? Fe1A C3A 2.0591(17) . ? Fe1A C2A 2.0819(18) . ? Fe1A C4A 2.2051(18) . ? Fe1A C5A 2.2201(18) . ? Fe1A C1A 2.448(2) . ? F7A C19A 1.338(4) . ? F8A C19A 1.340(4) . ? F9A C19A 1.344(5) . ? O1A C1A 1.235(2) . ? O2A C30A 1.141(3) . ? O3A C31A 1.144(3) . ? O4A C32A 1.143(3) . ? N1A C4A 1.380(2) . ? N1A C20A 1.463(3) . ? N1A C24A 1.473(3) . ? N2A C5A 1.392(2) . ? N2A C25A 1.478(3) . ? N2A C29A 1.479(3) . ? C1A C2A 1.477(3) . ? C1A C5A 1.502(3) . ? C2A C3A 1.453(3) . ? C2A C6A 1.477(3) . ? C3A C4A 1.448(2) . ? C3A C13A 1.490(2) . ? C4A C5A 1.453(3) . ? C6A C7A 1.402(3) . ? C6A C11A 1.404(3) . ? C7A C8A 1.393(3) . ? C8A C9A 1.382(3) . ? C9A C10A 1.396(3) . ? C9A C12A 1.502(3) . ? C10A C11A 1.394(3) . ? C12A F3A 1.250(5) . ? C12A F5A 1.264(5) . ? C12A F4A 1.299(5) . ? C12A F2A 1.352(4) . ? C12A F6A 1.387(5) . ? C12A F1A 1.391(6) . ? C13A C14A 1.394(3) . ? C13A C18A 1.399(3) . ? C14A C15A 1.394(3) . ? C15A C16A 1.384(4) . ? C16A C17A 1.390(3) . ? C16A C19A 1.501(3) . ? C17A C18A 1.392(3) . ? C20A C21A 1.531(3) . ? C21A C22A 1.522(4) . ? C22A C23A 1.527(4) . ? C23A C24A 1.528(3) . ? C25A C26A 1.521(3) . ? C26A C27A 1.529(3) . ? C27A C28A 1.530(3) . ? C28A C29A 1.529(3) . ? C94 C99 1.526(5) . ? C94 C95 1.534(7) . ? C95 C96 1.519(8) . ? C96 C97 1.508(7) . ? C97 C98 1.522(8) . ? C98 C99 1.515(6) . ? C94A C95A 1.374(9) . ? C94A C99A 1.495(11) . ? C95A C96A 1.472(8) . ? C96A C97A 1.459(8) . ? C97A C98A 1.444(9) . ? C98A C99A 1.630(11) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 C3 164.96(19) . . . . ? C5 C1 C2 C3 -18.59(19) . . . . ? Fe1 C1 C2 C3 -64.79(11) . . . . ? O1 C1 C2 C6 1.7(3) . . . . ? C5 C1 C2 C6 178.15(15) . . . . ? Fe1 C1 C2 C6 131.94(17) . . . . ? O1 C1 C2 Fe1 -130.2(2) . . . . ? C5 C1 C2 Fe1 46.20(12) . . . . ? C1 C2 C3 C4 8.29(19) . . . . ? C6 C2 C3 C4 169.80(17) . . . . ? Fe1 C2 C3 C4 -67.74(12) . . . . ? C1 C2 C3 C13 -155.35(16) . . . . ? C6 C2 C3 C13 6.2(3) . . . . ? Fe1 C2 C3 C13 128.62(17) . . . . ? C1 C2 C3 Fe1 76.03(12) . . . . ? C6 C2 C3 Fe1 -122.46(18) . . . . ? C20 N1 C4 C3 -19.7(3) . . . . ? C24 N1 C4 C3 126.05(19) . . . . ? C20 N1 C4 C5 159.29(17) . . . . ? C24 N1 C4 C5 -55.0(2) . . . . ? C20 N1 C4 Fe1 66.0(2) . . . . ? C24 N1 C4 Fe1 -148.30(14) . . . . ? C2 C3 C4 N1 -174.87(17) . . . . ? C13 C3 C4 N1 -11.1(3) . . . . ? Fe1 C3 C4 N1 120.92(18) . . . . ? C2 C3 C4 C5 6.06(19) . . . . ? C13 C3 C4 C5 169.85(16) . . . . ? Fe1 C3 C4 C5 -58.16(12) . . . . ? C2 C3 C4 Fe1 64.21(11) . . . . ? C13 C3 C4 Fe1 -131.99(17) . . . . ? C25 N2 C5 C4 -46.2(2) . . . . ? C29 N2 C5 C4 -177.65(17) . . . . ? C25 N2 C5 C1 148.90(18) . . . . ? C29 N2 C5 C1 17.5(3) . . . . ? C25 N2 C5 Fe1 44.8(2) . . . . ? C29 N2 C5 Fe1 -86.65(19) . . . . ? N1 C4 C5 N2 -4.1(3) . . . . ? C3 C4 C5 N2 175.04(16) . . . . ? Fe1 C4 C5 N2 121.16(18) . . . . ? N1 C4 C5 C1 163.16(16) . . . . ? C3 C4 C5 C1 -17.72(19) . . . . ? Fe1 C4 C5 C1 -71.60(12) . . . . ? N1 C4 C5 Fe1 -125.24(17) . . . . ? C3 C4 C5 Fe1 53.87(11) . . . . ? O1 C1 C5 N2 5.6(3) . . . . ? C2 C1 C5 N2 -170.68(17) . . . . ? Fe1 C1 C5 N2 -127.41(18) . . . . ? O1 C1 C5 C4 -161.7(2) . . . . ? C2 C1 C5 C4 21.97(18) . . . . ? Fe1 C1 C5 C4 65.23(11) . . . . ? O1 C1 C5 Fe1 133.1(2) . . . . ? C2 C1 C5 Fe1 -43.26(12) . . . . ? C3 C2 C6 C7 -32.8(3) . . . . ? C1 C2 C6 C7 126.8(2) . . . . ? Fe1 C2 C6 C7 -124.12(18) . . . . ? C3 C2 C6 C11 151.60(19) . . . . ? C1 C2 C6 C11 -48.7(3) . . . . ? Fe1 C2 C6 C11 60.3(2) . . . . ? C11 C6 C7 C8 -0.5(3) . . . . ? C2 C6 C7 C8 -176.08(19) . . . . ? C6 C7 C8 C9 0.8(3) . . . . ? C7 C8 C9 C10 -0.8(3) . . . . ? C7 C8 C9 C12 179.1(2) . . . . ? C8 C9 C10 C11 0.4(3) . . . . ? C12 C9 C10 C11 -179.5(2) . . . . ? C9 C10 C11 C6 -0.1(3) . . . . ? C7 C6 C11 C10 0.1(3) . . . . ? C2 C6 C11 C10 175.79(19) . . . . ? C8 C9 C12 F4 -48.0(6) . . . . ? C10 C9 C12 F4 131.9(6) . . . . ? C8 C9 C12 F5 -177.2(6) . . . . ? C10 C9 C12 F5 2.7(7) . . . . ? C8 C9 C12 F2 124.8(3) . . . . ? C10 C9 C12 F2 -55.3(3) . . . . ? C8 C9 C12 F3 2.0(3) . . . . ? C10 C9 C12 F3 -178.0(3) . . . . ? C8 C9 C12 F6 68.3(6) . . . . ? C10 C9 C12 F6 -111.7(6) . . . . ? C8 C9 C12 F1 -117.6(3) . . . . ? C10 C9 C12 F1 62.4(3) . . . . ? C4 C3 C13 C14 115.9(2) . . . . ? C2 C3 C13 C14 -83.2(2) . . . . ? Fe1 C3 C13 C14 12.5(3) . . . . ? C4 C3 C13 C18 -64.8(2) . . . . ? C2 C3 C13 C18 96.1(2) . . . . ? Fe1 C3 C13 C18 -168.20(14) . . . . ? C18 C13 C14 C15 -0.3(3) . . . . ? C3 C13 C14 C15 179.0(2) . . . . ? C13 C14 C15 C16 -0.4(4) . . . . ? C14 C15 C16 C17 0.6(4) . . . . ? C14 C15 C16 C19 178.9(2) . . . . ? C15 C16 C17 C18 0.0(4) . . . . ? C19 C16 C17 C18 -178.2(2) . . . . ? C16 C17 C18 C13 -0.8(3) . . . . ? C14 C13 C18 C17 0.9(3) . . . . ? C3 C13 C18 C17 -178.39(18) . . . . ? C15 C16 C19 F8 64.3(4) . . . . ? C17 C16 C19 F8 -117.4(3) . . . . ? C15 C16 C19 F9 -56.0(4) . . . . ? C17 C16 C19 F9 122.3(3) . . . . ? C15 C16 C19 F7 -176.2(3) . . . . ? C17 C16 C19 F7 2.1(4) . . . . ? C4 N1 C20 C21 -154.95(17) . . . . ? C24 N1 C20 C21 58.5(2) . . . . ? N1 C20 C21 C22 -57.5(2) . . . . ? C20 C21 C22 C23 56.2(3) . . . . ? C21 C22 C23 C24 -53.9(3) . . . . ? C4 N1 C24 C23 155.33(18) . . . . ? C20 N1 C24 C23 -56.6(2) . . . . ? C22 C23 C24 N1 53.2(3) . . . . ? C5 N2 C25 C26 165.56(17) . . . . ? C29 N2 C25 C26 -59.8(2) . . . . ? N2 C25 C26 C27 58.6(2) . . . . ? C25 C26 C27 C28 -54.1(3) . . . . ? C26 C27 C28 C29 53.4(3) . . . . ? C5 N2 C29 C28 -167.63(17) . . . . ? C25 N2 C29 C28 58.4(2) . . . . ? C27 C28 C29 N2 -56.2(2) . . . . ? O1A C1A C2A C3A 163.9(2) . . . . ? C5A C1A C2A C3A -20.23(19) . . . . ? Fe1A C1A C2A C3A -65.53(12) . . . . ? O1A C1A C2A C6A 3.1(3) . . . . ? C5A C1A C2A C6A 178.96(16) . . . . ? Fe1A C1A C2A C6A 133.66(18) . . . . ? O1A C1A C2A Fe1A -130.5(2) . . . . ? C5A C1A C2A Fe1A 45.31(13) . . . . ? C6A C2A C3A C4A 168.62(18) . . . . ? C1A C2A C3A C4A 9.8(2) . . . . ? Fe1A C2A C3A C4A -67.10(12) . . . . ? C6A C2A C3A C13A 4.3(3) . . . . ? C1A C2A C3A C13A -154.49(17) . . . . ? Fe1A C2A C3A C13A 128.62(18) . . . . ? C6A C2A C3A Fe1A -124.3(2) . . . . ? C1A C2A C3A Fe1A 76.89(13) . . . . ? C20A N1A C4A C3A -20.9(3) . . . . ? C24A N1A C4A C3A 127.8(2) . . . . ? C20A N1A C4A C5A 157.70(19) . . . . ? C24A N1A C4A C5A -53.6(3) . . . . ? C20A N1A C4A Fe1A 64.8(2) . . . . ? C24A N1A C4A Fe1A -146.45(15) . . . . ? C2A C3A C4A N1A -175.94(18) . . . . ? C13A C3A C4A N1A -12.1(3) . . . . ? Fe1A C3A C4A N1A 120.54(19) . . . . ? C2A C3A C4A C5A 5.3(2) . . . . ? C13A C3A C4A C5A 169.08(17) . . . . ? Fe1A C3A C4A C5A -58.24(13) . . . . ? C2A C3A C4A Fe1A 63.52(12) . . . . ? C13A C3A C4A Fe1A -132.69(19) . . . . ? C25A N2A C5A C4A -48.6(3) . . . . ? C29A N2A C5A C4A -178.72(18) . . . . ? C25A N2A C5A C1A 147.33(18) . . . . ? C29A N2A C5A C1A 17.2(3) . . . . ? C25A N2A C5A Fe1A 42.6(2) . . . . ? C29A N2A C5A Fe1A -87.6(2) . . . . ? N1A C4A C5A N2A -3.4(3) . . . . ? C3A C4A C5A N2A 175.47(17) . . . . ? Fe1A C4A C5A N2A 121.21(18) . . . . ? N1A C4A C5A C1A 163.20(18) . . . . ? C3A C4A C5A C1A -18.0(2) . . . . ? Fe1A C4A C5A C1A -72.24(13) . . . . ? N1A C4A C5A Fe1A -124.57(18) . . . . ? C3A C4A C5A Fe1A 54.26(12) . . . . ? O1A C1A C5A N2A 5.5(3) . . . . ? C2A C1A C5A N2A -170.14(17) . . . . ? Fe1A C1A C5A N2A -127.68(19) . . . . ? O1A C1A C5A C4A -161.2(2) . . . . ? C2A C1A C5A C4A 23.20(19) . . . . ? Fe1A C1A C5A C4A 65.66(12) . . . . ? O1A C1A C5A Fe1A 133.2(2) . . . . ? C2A C1A C5A Fe1A -42.46(12) . . . . ? C3A C2A C6A C7A -35.1(3) . . . . ? C1A C2A C6A C7A 121.6(2) . . . . ? Fe1A C2A C6A C7A -127.79(19) . . . . ? C3A C2A C6A C11A 149.7(2) . . . . ? C1A C2A C6A C11A -53.6(3) . . . . ? Fe1A C2A C6A C11A 57.0(3) . . . . ? C11A C6A C7A C8A -1.1(3) . . . . ? C2A C6A C7A C8A -176.4(2) . . . . ? C6A C7A C8A C9A 0.3(4) . . . . ? C7A C8A C9A C10A 1.4(4) . . . . ? C7A C8A C9A C12A 179.1(2) . . . . ? C8A C9A C10A C11A -2.2(4) . . . . ? C12A C9A C10A C11A -179.9(3) . . . . ? C9A C10A C11A C6A 1.4(4) . . . . ? C7A C6A C11A C10A 0.2(4) . . . . ? C2A C6A C11A C10A 175.6(2) . . . . ? C8A C9A C12A F3A 15.7(5) . . . . ? C10A C9A C12A F3A -166.5(5) . . . . ? C8A C9A C12A F5A -175.2(4) . . . . ? C10A C9A C12A F5A 2.5(5) . . . . ? C8A C9A C12A F4A -47.0(5) . . . . ? C10A C9A C12A F4A 130.8(4) . . . . ? C8A C9A C12A F2A 145.7(3) . . . . ? C10A C9A C12A F2A -36.5(4) . . . . ? C8A C9A C12A F6A 64.6(4) . . . . ? C10A C9A C12A F6A -117.7(4) . . . . ? C8A C9A C12A F1A -106.4(4) . . . . ? C10A C9A C12A F1A 71.3(4) . . . . ? C4A C3A C13A C14A 129.6(2) . . . . ? C2A C3A C13A C14A -69.1(3) . . . . ? Fe1A C3A C13A C14A 24.7(3) . . . . ? C4A C3A C13A C18A -57.0(3) . . . . ? C2A C3A C13A C18A 104.3(2) . . . . ? Fe1A C3A C13A C18A -161.98(15) . . . . ? C18A C13A C14A C15A 0.3(4) . . . . ? C3A C13A C14A C15A 173.6(3) . . . . ? C13A C14A C15A C16A 0.4(5) . . . . ? C14A C15A C16A C17A -0.7(5) . . . . ? C14A C15A C16A C19A 178.9(3) . . . . ? C15A C16A C17A C18A 0.4(4) . . . . ? C19A C16A C17A C18A -179.2(3) . . . . ? C16A C17A C18A C13A 0.2(3) . . . . ? C14A C13A C18A C17A -0.6(3) . . . . ? C3A C13A C18A C17A -174.18(19) . . . . ? C15A C16A C19A F7A 165.0(3) . . . . ? C17A C16A C19A F7A -15.3(5) . . . . ? C15A C16A C19A F8A 44.6(4) . . . . ? C17A C16A C19A F8A -135.7(3) . . . . ? C15A C16A C19A F9A -73.4(4) . . . . ? C17A C16A C19A F9A 106.3(3) . . . . ? C4A N1A C20A C21A -152.40(19) . . . . ? C24A N1A C20A C21A 58.0(2) . . . . ? N1A C20A C21A C22A -57.6(3) . . . . ? C20A C21A C22A C23A 56.0(3) . . . . ? C21A C22A C23A C24A -53.3(3) . . . . ? C4A N1A C24A C23A 153.91(19) . . . . ? C20A N1A C24A C23A -55.3(3) . . . . ? C22A C23A C24A N1A 51.9(3) . . . . ? C5A N2A C25A C26A 167.48(17) . . . . ? C29A N2A C25A C26A -59.4(2) . . . . ? N2A C25A C26A C27A 59.3(2) . . . . ? C25A C26A C27A C28A -55.5(3) . . . . ? C26A C27A C28A C29A 54.4(3) . . . . ? C5A N2A C29A C28A -170.68(17) . . . . ? C25A N2A C29A C28A 57.1(2) . . . . ? C27A C28A C29A N2A -55.9(3) . . . . ? C99 C94 C95 C96 54.2(5) . . . . ? C94 C95 C96 C97 -55.7(6) . . . . ? C95 C96 C97 C98 55.2(6) . . . . ? C96 C97 C98 C99 -56.2(6) . . . . ? C97 C98 C99 C94 55.4(5) . . . . ? C95 C94 C99 C98 -53.0(5) . . . . ? C99A C94A C95A C96A 48.3(9) . . . . ? C94A C95A C96A C97A -52.6(8) . . . . ? C95A C96A C97A C98A 52.0(8) . . . . ? C96A C97A C98A C99A -44.5(9) . . . . ? C95A C94A C99A C98A -41.6(10) . . . . ? C97A C98A C99A C94A 38.8(10) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 5.5910 -9.1145 -26.3653 0.0262 0.9979 -0.0589 -10.4649 0.2292 -16.9697 0.0076 0.3356 -0.9420 -14.1059 4.7600 -5.3356 -0.0047 -0.1304 -0.9915 -14.2588 8.8667 10.5852 -0.0184 -0.6627 -0.7487 -0.1581 6.9678 27.1855 -0.0233 -0.9067 0.4212 -0.1164 -19.5998 18.9039 0.9929 -0.0262 0.1163 -13.3002 -2.1681 -3.2485 0.2875 -0.0064 -0.9578 1.4285 19.3836 -18.1676 -0.9995 0.0263 -0.0191 11.5047 -11.1685 15.4219 0.4111 -0.0119 0.9115 -5.1014 18.5678 -20.0029 -0.8709 0.0235 -0.4909 5.5496 -16.4905 -16.0621 0.4304 0.9021 0.0298 10.4505 2.8822 14.3107 -0.1614 -0.3410 0.9261 6.1892 8.6657 17.6123 -0.2949 -0.6202 0.7269 2.2152 12.4239 18.5439 -0.3726 -0.7823 0.4992 0.1356 13.9280 18.4241 -0.3999 -0.8393 0.3682 -2.8252 15.5568 17.5804 -0.4243 -0.8897 0.1685 -8.5912 16.7439 13.3312 -0.4148 -0.8685 -0.2713 11.6835 3.4678 -22.9844 -0.5657 0.6634 0.4899 4.3544 6.3449 -32.0670 -0.6455 0.7557 -0.1109 2.7246 19.0771 0.3456 -0.8310 -0.4507 0.3260 11.3329 6.0423 6.7332 -0.3799 -0.2051 0.9020 0.4437 20.5511 -1.2038 -0.8675 -0.4707 0.1611 -2.3761 21.5470 -3.0597 -0.8778 -0.4766 -0.0479