#------------------------------------------------------------------------------ #$Date: 2024-09-06 02:48:31 +0300 (Fri, 06 Sep 2024) $ #$Revision: 294473 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/20/1572088.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572088 loop_ _publ_author_name 'Chen, Zhao-Nian' 'Zhang, Le-Ping' 'Wu, Huai-Li' 'Qi, Qiao-Yan' 'Yan, Meng' 'Tian, Jia' 'Yang, Guan-Yu' 'Li, Zhan-Ting' 'Yang, Bo' _publ_section_title ; Accurate construction of monolayer, bilayer, sandwich bilayer, four-layer, multi-layer and chiral bilayer 2D pillararene-type supramolecular networks. ; _journal_issue 33 _journal_name_full 'Chemical science' _journal_page_first 13191 _journal_page_last 13200 _journal_paper_doi 10.1039/d4sc03022b _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C73 H72 Cu2 N2 O16, C3 H7 N O, H2 O' _chemical_formula_sum 'C76 H81 Cu2 N3 O18' _chemical_formula_weight 1451.51 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2024-06-21 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-06-25 deposited with the CCDC. 2024-07-04 downloaded from the CCDC. ; _cell_angle_alpha 97.3870(10) _cell_angle_beta 103.4240(10) _cell_angle_gamma 98.4550(10) _cell_formula_units_Z 2 _cell_length_a 12.3580(3) _cell_length_b 16.3529(4) _cell_length_c 17.9257(4) _cell_measurement_reflns_used 9878 _cell_measurement_temperature 150.00 _cell_measurement_theta_max 57.119 _cell_measurement_theta_min 3.254 _cell_volume 3435.12(14) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_collection 'SAINT V8.40B (?, 2016)' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 150.00 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0518 _diffrn_reflns_av_unetI/netI 0.0545 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 54142 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.436 _diffrn_reflns_theta_min 1.277 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.694 _exptl_absorpt_correction_T_max 0.7512 _exptl_absorpt_correction_T_min 0.5835 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0726 before and 0.0525 after correction. The Ratio of minimum to maximum transmission is 0.7768. The \l/2 correction factor is Not present. ; _exptl_crystal_colour green _exptl_crystal_colour_primary green _exptl_crystal_density_diffrn 1.403 _exptl_crystal_description block _exptl_crystal_F_000 1520 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.13 _refine_diff_density_max 1.017 _refine_diff_density_min -1.157 _refine_diff_density_rms 0.094 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.063 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 907 _refine_ls_number_reflns 14051 _refine_ls_number_restraints 67 _refine_ls_restrained_S_all 1.063 _refine_ls_R_factor_all 0.1013 _refine_ls_R_factor_gt 0.0765 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0918P)^2^+11.3221P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2088 _refine_ls_wR_factor_ref 0.2213 _reflns_Friedel_coverage 0.000 _reflns_number_gt 10367 _reflns_number_total 14051 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03022b2.cif _cod_data_source_block 11 _cod_depositor_comments 'Adding full bibliography for 1572083--1572100.cif.' _cod_database_code 1572088 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H,H) groups 2. Shared sites {C64, C64'} {C63, C63'} 3. Restrained distances O17-C63' 1.22 with sigma of 0.01 4. Uiso/Uaniso restraints and constraints N1 \\sim C64 \\sim C62 \\sim C63 \\sim C64' \\sim C63' \\sim O16 \\sim O17: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A Uanis(C64) = Uanis(C64') Uanis(C63) = Uanis(C63') 5. Others Sof(O17)=Sof(C64')=Sof(H64A)=Sof(H64B)=Sof(H64C)=Sof(C63')=Sof(H63')=1-FVAR(1) Sof(O16)=Sof(C64)=Sof(H64)=Sof(C63)=Sof(H63A)=Sof(H63B)=Sof(H63C)=FVAR(1) 6.a Everything fixed: H64A, H64B, H64C, O18, H18A, H18B 6.b Secondary CH2 refined with riding coordinates: C37(H37A,H37B), C61(H61A,H61B), C55(H55A,H55B), C46(H46A,H46B), C73(H73A,H73B) 6.c Aromatic/amide H refined with riding coordinates: C12(H12), C17(H17), C59(H59), C53(H53), C9(H9), C10(H10), C42(H42), C16(H16), C39(H39), C57(H57), C15(H15), C21(H21), C66(H66), C18(H18), C29(H29), C27(H27), C30(H30), C24(H24), C13(H13), C28(H28), C34(H34), C50(H50), C33(H33), C35(H35), C36(H36), C70(H70), C64(H64), C63'(H63') 6.d Idealised Me refined as rotating group: C025(H02A,H02B,H02C), C6(H6A,H6B,H6C), C44(H44A,H44B,H44C), C49(H49A,H49B, H49C), C67(H67A,H67B,H67C), C3(H3A,H3B,H3C), C60(H60A,H60B,H60C), C68(H68A, H68B,H68C), C8(H8A,H8B,H8C), C45(H45A,H45B,H45C), C54(H54A,H54B,H54C), C62(H62A,H62B,H62C), C63(H63A,H63B,H63C), C1(H1A,H1B,H1C) ; _shelx_res_file ; TITL 11_a.res in P-1 11.res created by SHELXL-2018/3 at 10:38:20 on 21-Jun-2024 REM Old TITL 11 in P-1 REM SHELXT solution in P-1 REM R1 0.193, Rweak 0.017, Alpha 0.098, Orientation as input REM Formula found by SHELXT: C78 N9 O11 Cu2 CELL 0.71073 12.358 16.3529 17.9257 97.387 103.424 98.455 ZERR 2 0.0003 0.0004 0.0004 0.001 0.001 0.001 LATT 1 SFAC C H Cu N O UNIT 152 162 4 6 36 EADP C64 C64' EADP C63 C63' SIMU 0.01 0.02 2 N1 C64 C62 C63 C64' C63' O16 O17 DFIX 1.22 0.01 O17 C63' EXYZ C64 C64' EXYZ C63 C63' L.S. 24 0 0 PLAN 2 TEMP -123.15 CONF list 4 MORE -1 fmap 2 53 acta BOND $H OMIT 0 -1 9 REM REM REM WGHT 0.091800 11.322101 FVAR 0.45743 0.59402 CU1 3 1.494180 0.866512 0.864549 11.00000 0.03134 0.04735 = 0.04134 0.00232 -0.00470 0.01409 CU2 3 1.295433 0.874940 0.772482 11.00000 0.02908 0.05602 = 0.03607 0.00314 -0.00094 0.01447 O9 5 -0.059197 0.422704 0.036896 11.00000 0.03145 0.04545 = 0.02287 -0.00083 -0.00262 0.02101 O14 5 0.329331 0.350827 0.221356 11.00000 0.02469 0.04302 = 0.02926 0.01168 0.00145 0.01231 O1 5 1.295483 0.752386 0.748248 11.00000 0.02553 0.04130 = 0.03313 -0.00115 -0.00676 0.01442 O8 5 0.366529 0.566235 0.013576 11.00000 0.04167 0.04179 = 0.02059 -0.00145 0.00204 -0.00266 O6 5 1.229584 0.858481 0.859811 11.00000 0.02654 0.05189 = 0.03005 0.00318 0.00309 0.01226 O10 5 -0.197096 0.630615 0.219976 11.00000 0.03556 0.03608 = 0.03159 0.00019 0.00518 0.01251 O2 5 1.466100 0.747391 0.823122 11.00000 0.02649 0.03643 = 0.04125 -0.00015 -0.00763 0.01244 O00A 5 1.548100 0.887662 0.770190 11.00000 0.02320 0.05743 = 0.03778 0.00909 0.00157 0.01112 O5 5 1.503247 0.986013 0.896367 11.00000 0.03744 0.04191 = 0.03734 0.00014 -0.01078 0.01713 O13 5 0.006573 0.374666 0.329913 11.00000 0.04623 0.04283 = 0.03044 0.01032 0.00448 0.01069 O11 5 -0.003305 0.922443 0.300803 11.00000 0.02291 0.04015 = 0.04529 0.00930 -0.00026 0.01202 O4 5 1.339041 0.996351 0.816123 11.00000 0.03370 0.04347 = 0.03995 0.00542 -0.00966 0.01831 O3 5 1.378749 0.891842 0.693823 11.00000 0.02400 0.07304 = 0.03160 0.01398 0.00204 0.01101 O15 5 0.569147 0.641894 0.329709 11.00000 0.04346 0.06235 = 0.02527 -0.00828 -0.00660 0.01860 O7 5 1.393526 0.840933 0.934845 11.00000 0.03416 0.06118 = 0.03804 0.01328 0.00426 0.01745 O12 5 0.114555 0.671147 0.467231 11.00000 0.04306 0.05650 = 0.03936 0.01830 0.00399 0.01753 N3 4 1.133042 0.873464 0.692354 11.00000 0.02072 0.02897 = 0.02753 0.00085 0.00149 0.00584 N2 4 -0.337024 0.872251 -0.059867 11.00000 0.02320 0.02913 = 0.02977 -0.00314 -0.00290 0.00719 C11 1 0.927339 0.866481 0.584793 11.00000 0.01249 0.02419 = 0.02258 0.00242 -0.00169 0.00656 C38 1 0.138416 0.865643 0.380753 11.00000 0.02006 0.03273 = 0.01985 -0.00236 0.00449 0.01117 C20 1 0.503265 0.856505 0.361583 11.00000 0.01429 0.02713 = 0.02381 0.00180 -0.00087 0.00512 C19 1 0.612715 0.857257 0.418519 11.00000 0.01078 0.02852 = 0.02127 -0.00047 -0.00347 0.00555 C26 1 0.189714 0.871475 0.203475 11.00000 0.01646 0.03695 = 0.01967 -0.00057 -0.00081 0.01001 C23 1 0.297301 0.866522 0.260630 11.00000 0.01308 0.02982 = 0.02349 -0.00084 -0.00237 0.00623 C14 1 0.818652 0.863315 0.526549 11.00000 0.01441 0.02804 = 0.01834 -0.00111 -0.00110 0.00752 C12 1 1.029490 0.880748 0.563851 11.00000 0.01989 0.03348 = 0.02144 0.00070 -0.00037 0.00835 AFIX 43 H12 2 1.030822 0.888490 0.512426 11.00000 -1.20000 AFIX 0 C25 1 0.480762 0.821058 0.283404 11.00000 0.01744 0.03426 = 0.02651 -0.00222 0.00038 0.00865 C17 1 0.811502 0.914643 0.470821 11.00000 0.01546 0.02750 = 0.02692 0.00323 -0.00050 0.00062 AFIX 43 H17 2 0.877119 0.951978 0.469064 11.00000 -1.20000 AFIX 0 C58 1 0.240311 0.405581 0.112756 11.00000 0.02951 0.03147 = 0.01985 -0.00212 0.00349 0.00936 C59 1 0.142479 0.422225 0.065368 11.00000 0.03440 0.03640 = 0.01930 0.00125 0.00377 0.01395 AFIX 43 H59 2 0.147055 0.447182 0.020915 11.00000 -1.20000 AFIX 0 C22 1 0.317824 0.898380 0.339347 11.00000 0.01597 0.02715 = 0.02441 -0.00031 0.00165 0.00652 C53 1 -0.139953 0.494933 0.195515 11.00000 0.02126 0.03398 = 0.02483 -0.00279 0.00252 0.00118 AFIX 43 H53 2 -0.168919 0.490660 0.140942 11.00000 -1.20000 AFIX 0 C52 1 -0.090284 0.430344 0.224794 11.00000 0.02076 0.03201 = 0.02865 0.00379 0.00626 0.00222 C9 1 1.035741 0.859530 0.712564 11.00000 0.02416 0.04338 = 0.02310 0.00614 -0.00090 0.00988 AFIX 43 H9 2 1.037610 0.851724 0.764425 11.00000 -1.20000 AFIX 0 C48 1 -0.147604 0.565250 0.244976 11.00000 0.02303 0.03208 = 0.03053 0.00139 0.00783 0.00304 C10 1 0.931969 0.855960 0.661039 11.00000 0.02042 0.04089 = 0.02622 0.00648 0.00181 0.00870 AFIX 43 H10 2 0.864328 0.846371 0.677730 11.00000 -1.20000 AFIX 0 C51 1 -0.045055 0.438776 0.304841 11.00000 0.02765 0.03632 = 0.02996 0.00510 0.00648 0.00217 C37 1 0.229788 0.935102 0.373524 11.00000 0.02171 0.03365 = 0.02795 -0.00261 0.00479 0.01053 AFIX 23 H37A 2 0.267060 0.968999 0.425490 11.00000 -1.20000 H37B 2 0.194961 0.972469 0.339586 11.00000 -1.20000 AFIX 0 C61 1 0.355607 0.431987 0.096311 11.00000 0.02684 0.03745 = 0.02544 -0.00214 0.00510 0.01114 AFIX 23 H61A 2 0.406012 0.393104 0.115123 11.00000 -1.20000 H61B 2 0.345466 0.427224 0.039393 11.00000 -1.20000 AFIX 0 C5 1 1.374977 0.715003 0.771769 11.00000 0.02329 0.03768 = 0.02605 0.00370 0.00446 0.00830 C42 1 -0.054783 0.790150 0.342493 11.00000 0.01923 0.04324 = 0.02076 -0.00454 0.00242 0.00693 AFIX 43 H42 2 -0.131549 0.786236 0.315150 11.00000 -1.20000 AFIX 0 C018 1 0.229978 0.366421 0.175990 11.00000 0.02536 0.03421 = 0.02325 0.00342 0.00137 0.01250 C69 1 0.511901 0.686381 0.209971 11.00000 0.01899 0.04313 = 0.03135 -0.00916 0.00412 0.01228 C16 1 0.620147 0.804854 0.473662 11.00000 0.01717 0.03853 = 0.02782 0.00787 -0.00090 0.00110 AFIX 43 H16 2 0.555003 0.766515 0.474645 11.00000 -1.20000 AFIX 0 C39 1 0.166692 0.803247 0.424705 11.00000 0.02266 0.04413 = 0.01861 0.00094 0.00037 0.01477 AFIX 43 H39 2 0.242483 0.807968 0.454332 11.00000 -1.20000 AFIX 0 C57 1 0.125943 0.346262 0.192612 11.00000 0.03067 0.02934 = 0.02764 0.00178 0.00309 0.00772 AFIX 43 H57 2 0.120860 0.318810 0.235603 11.00000 -1.20000 AFIX 0 C31 1 -0.013459 0.876656 0.094914 11.00000 0.01835 0.03535 = 0.02253 -0.00265 -0.00275 0.00991 C15 1 0.722090 0.807998 0.527451 11.00000 0.01784 0.03794 = 0.02895 0.01177 -0.00137 0.00413 AFIX 43 H15 2 0.726056 0.772067 0.565261 11.00000 -1.20000 AFIX 0 C21 1 0.421445 0.892931 0.388204 11.00000 0.01878 0.02960 = 0.01880 -0.00241 -0.00158 0.00511 AFIX 43 H21 2 0.436744 0.915082 0.442007 11.00000 -1.20000 AFIX 0 C66 1 0.463627 0.667813 0.130324 11.00000 0.02008 0.03805 = 0.03044 0.00093 0.00790 0.00485 AFIX 43 H66 2 0.463953 0.711950 0.100663 11.00000 -1.20000 AFIX 0 C65 1 0.411640 0.521008 0.134958 11.00000 0.02410 0.03732 = 0.02502 -0.00229 0.00527 0.01042 C18 1 0.709070 0.912225 0.417169 11.00000 0.02082 0.03286 = 0.02189 0.00678 -0.00240 0.00529 AFIX 43 H18 2 0.705051 0.948310 0.379487 11.00000 -1.20000 AFIX 0 C01J 1 0.028014 0.366188 0.146261 11.00000 0.02443 0.02743 = 0.02425 -0.00465 0.00023 0.00563 C55 1 -0.082236 0.353378 0.169884 11.00000 0.02276 0.03360 = 0.03337 0.00273 0.00197 0.00516 AFIX 23 H55A 2 -0.087263 0.303685 0.196011 11.00000 -1.20000 H55B 2 -0.146416 0.342775 0.122909 11.00000 -1.20000 AFIX 0 C47 1 -0.104844 0.573613 0.325569 11.00000 0.03203 0.03642 = 0.02876 -0.00231 0.01327 0.00089 C29 1 0.103544 0.801473 0.178918 11.00000 0.02311 0.03028 = 0.02991 0.00169 -0.00416 0.01069 AFIX 43 H29 2 0.113082 0.751252 0.198985 11.00000 -1.20000 AFIX 0 C56 1 0.038131 0.402941 0.081987 11.00000 0.02805 0.03313 = 0.02032 -0.00185 0.00075 0.01542 C71 1 0.414680 0.586247 0.092614 11.00000 0.02169 0.04281 = 0.02244 -0.00039 0.00611 0.00847 C27 1 0.173784 0.943734 0.172453 11.00000 0.01948 0.04057 = 0.02919 0.00439 -0.00130 0.00281 AFIX 43 H27 2 0.233004 0.991401 0.187299 11.00000 -1.20000 AFIX 0 N1 4 0.264175 0.585888 0.328610 11.00000 0.03565 0.05175 = 0.05837 0.00666 0.01704 0.00851 C30 1 0.003002 0.804378 0.124952 11.00000 0.01901 0.03167 = 0.03212 -0.00089 -0.00718 0.00539 AFIX 43 H30 2 -0.054952 0.755928 0.108647 11.00000 -1.20000 AFIX 0 C24 1 0.377447 0.827043 0.234117 11.00000 0.01813 0.04597 = 0.01849 -0.00465 -0.00143 0.01102 AFIX 43 H24 2 0.361156 0.803375 0.180602 11.00000 -1.20000 AFIX 0 C13 1 1.128736 0.883366 0.619628 11.00000 0.01603 0.03461 = 0.02816 0.00473 0.00078 0.00806 AFIX 43 H13 2 1.197996 0.892833 0.604913 11.00000 -1.20000 AFIX 0 C28 1 0.072773 0.947722 0.120035 11.00000 0.02506 0.03865 = 0.02765 0.00747 -0.00171 0.00781 AFIX 43 H28 2 0.062302 0.998521 0.101320 11.00000 -1.20000 AFIX 0 C43 1 0.024275 0.859395 0.340659 11.00000 0.02308 0.03652 = 0.02215 -0.00030 0.00292 0.01544 C34 1 -0.283997 0.940466 -0.007772 11.00000 0.02385 0.02936 = 0.04141 -0.00050 -0.00756 0.00983 AFIX 43 H34 2 -0.320487 0.987591 -0.004973 11.00000 -1.20000 AFIX 0 C32 1 -0.123452 0.877805 0.039382 11.00000 0.02064 0.03622 = 0.02350 0.00135 -0.00331 0.01011 C72 1 0.514827 0.620365 0.251853 11.00000 0.02346 0.05411 = 0.02360 -0.00800 -0.00015 0.01493 C40 1 0.086889 0.735107 0.425902 11.00000 0.03350 0.03811 = 0.01966 0.00465 0.00843 0.01383 C41 1 -0.025033 0.726988 0.382839 11.00000 0.03132 0.03662 = 0.02195 -0.00326 0.00973 0.00855 C7 1 1.483407 0.890978 0.706183 11.00000 0.02663 0.03121 = 0.03773 0.00227 0.00398 0.00434 C50 1 -0.053026 0.509967 0.354553 11.00000 0.03849 0.04199 = 0.02598 0.00533 0.00895 0.00449 AFIX 43 H50 2 -0.022520 0.514920 0.409044 11.00000 -1.20000 AFIX 0 C33 1 -0.178344 0.946118 0.042507 11.00000 0.02468 0.03060 = 0.03480 -0.00401 -0.00776 0.00805 AFIX 43 H33 2 -0.143826 0.996068 0.078678 11.00000 -1.20000 AFIX 0 C2 1 1.428675 1.025327 0.867752 11.00000 0.03771 0.03303 = 0.03066 0.00616 0.00428 0.01500 C025 1 -0.089881 0.383556 -0.042995 11.00000 0.03094 0.04290 = 0.02627 -0.00222 -0.00412 0.01064 AFIX 137 H02A 2 -0.037548 0.410253 -0.070021 11.00000 -1.50000 H02B 2 -0.167176 0.389761 -0.067448 11.00000 -1.50000 H02C 2 -0.085945 0.323827 -0.046261 11.00000 -1.50000 AFIX 0 C6 1 1.364347 0.625182 0.735609 11.00000 0.02748 0.03345 = 0.03689 -0.00292 0.00520 0.00796 AFIX 137 H6A 2 1.284133 0.599278 0.716784 11.00000 -1.50000 H6B 2 1.402379 0.594784 0.774530 11.00000 -1.50000 H6C 2 1.399589 0.622851 0.691909 11.00000 -1.50000 AFIX 0 C46 1 -0.112160 0.650583 0.380585 11.00000 0.03478 0.04255 = 0.03110 -0.00285 0.01694 0.00410 AFIX 23 H46A 2 -0.188669 0.664279 0.364350 11.00000 -1.20000 H46B 2 -0.102090 0.636963 0.433723 11.00000 -1.20000 AFIX 0 C35 1 -0.283467 0.808060 -0.064955 11.00000 0.02965 0.03877 = 0.03187 -0.00788 -0.01201 0.01415 AFIX 43 H35 2 -0.319141 0.759913 -0.103168 11.00000 -1.20000 AFIX 0 C36 1 -0.178008 0.807876 -0.017211 11.00000 0.03103 0.04247 = 0.03296 -0.00741 -0.01027 0.01897 AFIX 43 H36 2 -0.142874 0.760348 -0.022924 11.00000 -1.20000 AFIX 0 C70 1 0.463299 0.539441 0.214546 11.00000 0.02714 0.04638 = 0.02765 0.00182 0.00523 0.01587 AFIX 43 H70 2 0.463271 0.495292 0.244201 11.00000 -1.20000 AFIX 0 C44 1 -0.119380 0.913970 0.258155 11.00000 0.02870 0.05126 = 0.04051 0.01061 0.00025 0.02251 AFIX 137 H44A 2 -0.143238 0.859543 0.223514 11.00000 -1.50000 H44B 2 -0.126865 0.959024 0.227210 11.00000 -1.50000 H44C 2 -0.167168 0.917567 0.294668 11.00000 -1.50000 AFIX 0 C49 1 -0.252153 0.621431 0.140155 11.00000 0.04107 0.04370 = 0.03569 0.00150 0.00333 0.01628 AFIX 137 H49A 2 -0.198285 0.611775 0.109018 11.00000 -1.50000 H49B 2 -0.281268 0.672567 0.129821 11.00000 -1.50000 H49C 2 -0.315101 0.573580 0.126249 11.00000 -1.50000 AFIX 0 C73 1 0.564259 0.775417 0.251247 11.00000 0.01778 0.04822 = 0.03832 -0.01425 -0.00131 0.01273 AFIX 23 H73A 2 0.592781 0.807495 0.214345 11.00000 -1.20000 H73B 2 0.629697 0.773743 0.294660 11.00000 -1.20000 AFIX 0 C67 1 0.391598 0.626928 -0.033089 11.00000 0.04077 0.05155 = 0.03021 0.00712 0.00576 0.00218 AFIX 137 H67A 2 0.359951 0.602655 -0.088193 11.00000 -1.50000 H67B 2 0.473826 0.643872 -0.022789 11.00000 -1.50000 H67C 2 0.358285 0.676064 -0.020427 11.00000 -1.50000 AFIX 0 C4 1 1.289876 0.843648 0.922085 11.00000 0.03505 0.03080 = 0.03847 -0.00056 0.00682 0.00839 C3 1 1.232492 0.829273 0.986290 11.00000 0.05404 0.04684 = 0.04185 0.00937 0.01909 0.01665 AFIX 137 H3A 2 1.267834 0.872740 1.032011 11.00000 -1.50000 H3B 2 1.240387 0.773993 1.000109 11.00000 -1.50000 H3C 2 1.152032 0.831763 0.968400 11.00000 -1.50000 AFIX 0 C60 1 0.320857 0.293765 0.274399 11.00000 0.03787 0.06091 = 0.04342 0.02817 0.00394 0.02022 AFIX 137 H60A 2 0.270487 0.241289 0.246684 11.00000 -1.50000 H60B 2 0.290177 0.318519 0.315924 11.00000 -1.50000 H60C 2 0.396080 0.282254 0.297059 11.00000 -1.50000 AFIX 0 C68 1 0.589104 0.575169 0.372250 11.00000 0.04416 0.07089 = 0.03197 0.00447 -0.00597 0.01398 AFIX 137 H68A 2 0.632872 0.539595 0.347783 11.00000 -1.50000 H68B 2 0.516556 0.541568 0.372204 11.00000 -1.50000 H68C 2 0.631582 0.598548 0.425962 11.00000 -1.50000 AFIX 0 C8 1 1.532003 0.890443 0.637019 11.00000 0.04674 0.05398 = 0.04746 0.01283 0.02061 0.00869 AFIX 137 H8A 2 1.614818 0.901978 0.654551 11.00000 -1.50000 H8B 2 1.506489 0.933666 0.607647 11.00000 -1.50000 H8C 2 1.506505 0.835334 0.603595 11.00000 -1.50000 AFIX 0 PART 1 O16 5 0.331423 0.505325 0.418082 21.00000 0.05147 0.08083 = 0.04201 0.01790 -0.00912 -0.00160 C64 1 0.262998 0.513238 0.359421 21.00000 0.04619 0.06460 = 0.06425 0.01399 -0.00133 -0.00289 AFIX 43 H64 2 0.205563 0.466334 0.333590 21.00000 -1.20000 AFIX 0 PART 0 C45 1 0.212374 0.690316 0.532103 11.00000 0.07354 0.07375 = 0.03687 0.01570 -0.01222 0.02942 AFIX 137 H45A 2 0.280272 0.705070 0.513707 11.00000 -1.50000 H45B 2 0.218434 0.641288 0.557962 11.00000 -1.50000 H45C 2 0.205305 0.737699 0.568999 11.00000 -1.50000 AFIX 0 C54 1 0.045991 0.376232 0.410541 11.00000 0.10889 0.06462 = 0.03577 0.01840 0.01507 0.03728 AFIX 137 H54A 2 0.085251 0.329089 0.419356 11.00000 -1.50000 H54B 2 -0.018280 0.371610 0.434063 11.00000 -1.50000 H54C 2 0.098409 0.429085 0.434262 11.00000 -1.50000 AFIX 0 C62 1 0.188868 0.586332 0.254828 11.00000 0.06414 0.06339 = 0.05784 0.01620 0.00843 0.01900 AFIX 137 H62A 2 0.158273 0.528488 0.228207 11.00000 -1.50000 H62B 2 0.230132 0.616392 0.223011 11.00000 -1.50000 H62C 2 0.126634 0.614419 0.262745 11.00000 -1.50000 AFIX 0 PART 1 C63 1 0.337849 0.659912 0.370077 21.00000 0.03924 0.05287 = 0.08046 -0.01288 0.01985 0.00121 AFIX 137 H63A 2 0.375800 0.650423 0.421807 21.00000 -1.50000 H63B 2 0.294527 0.704964 0.375459 21.00000 -1.50000 H63C 2 0.394568 0.675942 0.341866 21.00000 -1.50000 AFIX 0 PART 0 C1 1 1.443893 1.113463 0.897860 11.00000 0.06159 0.06523 = 0.06308 0.01305 -0.00182 0.00974 AFIX 137 H1A 2 1.471284 1.122777 0.954690 11.00000 -1.50000 H1B 2 1.371465 1.132493 0.883314 11.00000 -1.50000 H1C 2 1.499279 1.145051 0.876048 11.00000 -1.50000 AFIX 0 PART 2 O17 5 0.395245 0.663518 0.439918 -21.00000 0.04479 0.06485 = 0.10197 -0.00774 0.02984 -0.01018 C64' 1 0.262998 0.513238 0.359421 -21.00000 0.04619 0.06460 = 0.06425 0.01399 -0.00133 -0.00289 AFIX 1 H64A 2 0.208780 0.510200 0.391540 -21.00000 -1.50000 AFIX 1 H64B 2 0.338680 0.512630 0.391460 -21.00000 -1.50000 AFIX 1 H64C 2 0.240580 0.464890 0.317060 -21.00000 -1.50000 AFIX 0 C63' 1 0.337849 0.659912 0.370077 -21.00000 0.03924 0.05287 = 0.08046 -0.01288 0.01985 0.00121 AFIX 43 H63' 2 0.345037 0.708010 0.345742 -21.00000 -1.20000 AFIX 1 PART 1 O18 5 0.505420 0.612690 0.548350 11.00000 0.21735 0.18595 = 0.14351 0.03018 0.04017 0.03033 AFIX 1 H18A 2 0.467680 0.627760 0.506620 11.00000 -1.50000 AFIX 1 H18B 2 0.470220 0.562420 0.547920 11.00000 -1.50000 AFIX 0 HKLF 4 REM 11_a.res in P-1 REM wR2 = 0.2213, GooF = S = 1.063, Restrained GooF = 1.063 for all data REM R1 = 0.0765 for 10367 Fo > 4sig(Fo) and 0.1013 for all 14051 data REM 907 parameters refined using 67 restraints END WGHT 0.0921 11.2768 REM Highest difference peak 1.017, deepest hole -1.157, 1-sigma level 0.094 Q1 1 -0.1577 0.8165 0.2942 11.00000 0.05 1.02 Q2 1 0.2623 0.8044 0.4775 11.00000 0.05 0.91 ; _shelx_res_checksum 1555 _shelx_hkl_file ; -1 0 0 443.86 22.30 1 0 0 431.86 22.30 -2 0 0 1972.80 98.89 -2 0 0 1924.01 98.79 -3 0 0 31.30 2.00 -3 0 0 33.10 2.60 3 0 0 28.50 2.50 3 0 0 30.30 3.30 -4 0 0 346.57 18.10 -4 0 0 348.87 18.40 4 0 0 364.16 19.00 4 0 0 351.86 18.40 -5 0 0 1741.83 86.39 -5 0 0 1521.65 86.69 -5 0 0 1816.02 86.69 5 0 0 1751.22 86.59 5 0 0 1667.53 87.09 -6 0 0 1044.50 54.59 -6 0 0 1072.69 54.29 6 0 0 1067.19 55.49 6 0 0 1054.39 54.49 6 0 0 1043.50 54.49 6 0 0 1100.59 54.69 -7 0 0 -1.70 2.80 7 0 0 3.00 3.00 7 0 0 4.30 5.20 7 0 0 0.50 5.40 -8 0 0 220.28 13.80 -8 0 0 224.48 12.60 -8 0 0 225.58 13.30 8 0 0 237.18 16.30 8 0 0 207.88 13.80 8 0 0 205.48 13.00 -9 0 0 533.25 28.60 -9 0 0 540.05 29.70 -9 0 0 511.35 29.30 9 0 0 528.55 29.80 9 0 0 526.45 29.30 9 0 0 627.94 35.90 -10 0 0 534.95 30.20 -10 0 0 576.74 30.30 10 0 0 530.05 31.10 10 0 0 534.25 30.50 10 0 0 512.05 32.30 -11 0 0 75.19 13.30 -11 0 0 47.40 8.60 -11 0 0 59.09 9.70 11 0 0 74.99 12.30 11 0 0 47.50 11.80 -12 0 0 22.50 7.40 -12 0 0 14.90 8.70 -12 0 0 25.60 10.40 12 0 0 14.20 10.90 12 0 0 16.40 8.50 -13 0 0 5.00 10.00 -13 0 0 -10.80 14.60 -13 0 0 7.00 9.90 13 0 0 3.20 12.10 13 0 0 -0.90 8.40 -14 0 0 68.29 10.80 14 0 0 54.09 11.10 14 -1 0 5.20 8.20 -14 1 0 5.40 6.80 13 -1 0 0.70 9.80 13 -1 0 -2.00 19.90 -13 1 0 9.70 7.00 12 -1 0 43.10 9.80 12 -1 0 51.59 12.70 -12 1 0 63.99 8.20 -12 1 0 52.69 10.00 -12 1 0 61.39 10.50 11 -1 0 290.17 23.50 11 -1 0 324.47 20.50 -11 1 0 292.17 21.00 -11 1 0 297.47 20.70 -11 1 0 310.27 20.90 10 -1 0 1142.09 61.79 10 -1 0 1124.69 60.09 10 -1 0 1135.99 62.39 -10 1 0 1162.88 60.09 -10 1 0 1137.89 59.79 9 -1 0 152.78 12.20 9 -1 0 173.98 14.60 9 -1 0 151.48 12.10 9 -1 0 131.19 10.70 -9 1 0 171.98 11.40 -9 1 0 169.18 12.20 8 -1 0 3.70 3.40 8 -1 0 3.80 6.30 8 -1 0 -6.40 6.70 8 -1 0 11.90 5.10 -8 1 0 -1.30 4.90 -8 1 0 3.70 4.90 -8 1 0 6.60 3.30 7 -1 0 380.36 21.50 7 -1 0 406.26 23.00 7 -1 0 393.36 21.50 -7 1 0 419.06 21.20 -7 1 0 417.66 21.70 -7 1 0 412.76 21.90 6 -1 0 1898.61 96.89 6 -1 0 1949.51 97.09 6 -1 0 1914.31 97.59 -6 1 0 1951.40 97.09 -6 1 0 1798.22 96.89 -6 1 0 1899.91 96.69 5 -1 0 565.04 29.00 5 -1 0 551.04 29.30 5 -1 0 583.84 29.80 -5 1 0 568.54 28.80 -5 1 0 540.55 29.10 4 -1 0 625.04 32.80 4 -1 0 637.44 32.40 -4 1 0 632.44 32.20 3 -1 0 364.86 18.90 3 -1 0 354.16 18.50 -3 1 0 361.86 18.40 2 -1 0 72.89 4.30 2 -1 0 75.39 4.00 -2 1 0 75.49 3.90 -2 1 0 73.29 4.10 0 1 0 1162.08 58.89 -1 -1 0 5.50 0.80 1 1 0 4.40 0.70 -2 -1 0 604.84 31.40 -2 -1 0 606.84 31.50 2 1 0 643.84 31.60 -3 -1 0 230.48 12.00 -3 -1 0 219.78 11.80 3 1 0 235.68 12.10 -4 -1 0 2274.27 117.89 -4 -1 0 2372.06 118.09 4 1 0 2325.67 118.09 -5 -1 0 522.25 27.30 -5 -1 0 541.65 27.90 -5 -1 0 500.35 27.50 5 1 0 561.04 28.50 5 1 0 533.25 27.60 -6 -1 0 621.34 31.50 -6 -1 0 576.14 31.30 -6 -1 0 591.24 31.00 6 1 0 587.74 32.50 6 1 0 617.24 31.40 6 1 0 633.24 31.50 6 1 0 591.14 31.30 -7 -1 0 4.00 3.90 -7 -1 0 6.50 4.00 -7 -1 0 2.10 2.90 7 1 0 2.10 3.40 7 1 0 4.40 3.70 7 1 0 5.80 6.10 7 1 0 4.00 7.00 -8 -1 0 11.10 3.70 -8 -1 0 10.20 5.40 8 1 0 13.20 5.30 8 1 0 10.60 6.80 8 1 0 10.90 4.60 8 1 0 10.90 7.70 -9 -1 0 294.07 15.50 -9 -1 0 278.97 17.20 -9 -1 0 280.87 17.10 9 1 0 231.28 15.80 9 1 0 272.07 20.30 9 1 0 251.97 17.00 9 1 0 272.47 16.70 -10 -1 0 136.39 13.60 -10 -1 0 136.49 13.40 -10 -1 0 132.09 11.00 10 1 0 172.28 18.00 10 1 0 134.69 13.30 10 1 0 117.89 15.40 -11 -1 0 215.08 17.00 -11 -1 0 231.88 17.80 11 1 0 205.78 16.30 11 1 0 198.68 20.70 -12 -1 0 135.29 15.40 -12 -1 0 139.69 16.50 -12 -1 0 149.99 13.00 12 1 0 116.49 18.70 12 1 0 145.49 14.40 -13 -1 0 14.10 10.30 -13 -1 0 -11.30 7.90 -13 -1 0 11.30 11.70 13 1 0 1.30 10.90 13 1 0 2.50 8.40 -14 -1 0 192.48 17.30 -15 2 0 20.10 10.10 14 -2 0 -0.70 9.00 -14 2 0 4.00 7.00 -14 2 0 7.30 10.80 13 -2 0 59.69 11.00 -13 2 0 20.40 10.60 -13 2 0 42.80 7.90 12 -2 0 414.86 25.50 12 -2 0 396.56 27.90 -12 2 0 423.06 24.10 -12 2 0 403.96 25.90 -12 2 0 439.16 26.10 11 -2 0 564.84 33.60 11 -2 0 566.94 31.50 -11 2 0 543.35 31.40 -11 2 0 527.05 31.40 10 -2 0 793.92 44.40 10 -2 0 741.53 45.90 -10 2 0 913.41 46.20 -10 2 0 832.12 43.20 -10 2 0 862.11 44.50 9 -2 0 76.39 7.90 9 -2 0 86.79 9.90 9 -2 0 89.29 9.80 9 -2 0 94.39 12.80 -9 2 0 84.19 9.90 -9 2 0 83.49 9.90 8 -2 0 386.56 20.80 8 -2 0 358.66 20.50 8 -2 0 384.26 22.20 8 -2 0 356.16 19.90 -8 2 0 351.26 20.40 -8 2 0 365.36 20.60 7 -2 0 185.98 12.10 7 -2 0 174.08 12.10 7 -2 0 159.08 10.60 7 -2 0 170.68 10.20 -7 2 0 175.08 10.70 -7 2 0 176.38 9.90 -7 2 0 184.38 10.90 6 -2 0 197.38 11.20 6 -2 0 192.28 11.90 6 -2 0 183.58 10.70 -6 2 0 193.08 10.40 -6 2 0 187.78 11.00 -6 2 0 197.08 11.10 5 -2 0 27.30 4.00 5 -2 0 29.70 4.60 5 -2 0 26.50 3.20 -5 2 0 35.10 2.80 -5 2 0 31.70 3.70 -5 2 0 28.70 3.60 4 -2 0 332.47 17.30 4 -2 0 321.87 17.70 -4 2 0 335.67 17.30 -4 2 0 337.77 17.10 3 -2 0 968.80 50.99 3 -2 0 984.30 51.29 -3 2 0 1026.40 51.09 -3 2 0 1031.20 50.89 2 -2 0 111.89 6.00 2 -2 0 110.49 5.80 -2 2 0 102.59 5.60 1 -2 0 1361.86 66.99 1 -2 0 1314.77 66.89 -1 2 0 1276.47 66.89 0 -2 0 38.30 2.30 0 2 0 39.20 2.30 -2 -2 0 42.00 2.50 -2 -2 0 43.40 2.90 2 2 0 40.00 3.00 -3 -2 0 1731.23 88.09 -3 -2 0 1713.63 88.29 3 2 0 1763.92 88.29 -4 -2 0 10.20 2.20 -4 -2 0 7.90 2.30 -4 -2 0 12.30 1.80 4 2 0 9.80 2.30 -5 -2 0 110.49 7.30 -5 -2 0 108.69 6.50 5 2 0 113.79 7.30 5 2 0 116.09 7.20 -6 -2 0 114.99 8.00 -6 -2 0 117.69 8.10 -6 -2 0 120.49 7.00 6 2 0 120.89 9.80 6 2 0 108.89 7.70 6 2 0 107.29 7.90 6 2 0 111.39 7.70 -7 -2 0 101.69 8.20 -7 -2 0 90.79 8.00 -7 -2 0 88.19 6.70 7 2 0 88.49 7.70 7 2 0 87.89 7.70 7 2 0 96.19 11.10 -8 -2 0 101.29 9.00 -8 -2 0 94.39 7.60 8 2 0 99.29 9.30 8 2 0 88.89 12.70 8 2 0 89.99 8.90 8 2 0 90.89 8.10 -9 -2 0 92.59 11.20 -9 -2 0 90.79 8.60 9 2 0 85.39 10.70 9 2 0 97.59 9.70 9 2 0 109.89 15.00 9 2 0 93.09 8.80 -10 -2 0 104.49 10.00 -10 -2 0 97.89 12.60 -10 -2 0 105.59 11.80 10 2 0 95.09 17.10 10 2 0 92.59 12.70 -11 -2 0 182.28 16.90 -11 -2 0 117.89 19.60 11 2 0 193.88 27.80 11 2 0 182.68 14.50 -12 -2 0 48.30 7.70 -12 -2 0 38.80 11.90 -12 -2 0 42.40 10.00 12 2 0 65.09 14.00 12 2 0 38.30 9.50 -13 -2 0 -1.30 10.20 -13 -2 0 11.20 11.00 -13 -2 0 15.40 7.40 13 2 0 17.40 8.60 -14 -2 0 0.40 9.50 -14 -2 0 11.40 7.60 15 -3 0 6.20 7.70 -15 3 0 5.80 9.80 -15 3 0 -1.80 10.10 14 -3 0 70.59 10.80 -14 3 0 69.59 11.10 -14 3 0 65.99 11.70 13 -3 0 3.30 16.50 13 -3 0 1.90 10.50 -13 3 0 -11.40 16.70 -13 3 0 4.40 7.10 -13 3 0 14.90 11.80 12 -3 0 236.68 22.30 12 -3 0 285.67 20.60 -12 3 0 268.97 17.60 -12 3 0 293.97 20.30 11 -3 0 10.10 10.10 11 -3 0 21.20 8.90 -11 3 0 19.20 8.60 -11 3 0 25.00 7.90 10 -3 0 60.09 10.90 10 -3 0 33.50 9.30 -10 3 0 54.19 10.40 -10 3 0 43.70 9.70 -10 3 0 48.40 8.10 9 -3 0 1594.04 84.69 9 -3 0 1620.24 85.69 9 -3 0 1678.63 84.79 -9 3 0 1630.04 84.59 -9 3 0 1668.93 83.99 -9 3 0 1654.13 84.39 8 -3 0 467.95 27.40 8 -3 0 485.85 26.30 8 -3 0 474.25 26.30 8 -3 0 460.85 25.60 -8 3 0 488.25 26.10 -8 3 0 507.75 26.40 -8 3 0 495.35 25.40 7 -3 0 162.28 11.60 7 -3 0 160.88 10.80 7 -3 0 162.78 9.80 -7 3 0 157.28 10.30 -7 3 0 174.88 10.60 6 -3 0 537.05 28.00 6 -3 0 528.95 28.30 6 -3 0 529.25 28.90 -6 3 0 561.24 28.20 -6 3 0 534.25 28.00 5 -3 0 70.99 5.70 5 -3 0 56.69 4.90 5 -3 0 58.99 4.40 -5 3 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-8 -3 0 34.70 6.30 8 3 0 43.60 8.30 8 3 0 52.49 10.20 8 3 0 43.40 7.40 8 3 0 36.10 9.10 -9 -3 0 402.06 21.40 9 3 0 409.76 26.30 9 3 0 398.56 22.70 9 3 0 375.96 21.90 9 3 0 338.47 21.70 9 3 0 391.66 21.80 -10 -3 0 145.99 14.70 -10 -3 0 128.19 11.60 -10 -3 0 142.29 14.10 10 3 0 145.19 13.60 10 3 0 129.39 18.60 10 3 0 135.39 16.20 -11 -3 0 82.89 14.60 -11 -3 0 88.59 13.70 11 3 0 73.89 11.60 11 3 0 87.19 18.70 -12 -3 0 3.30 11.90 -12 -3 0 2.30 7.20 -12 -3 0 -1.50 7.60 12 3 0 -0.30 5.20 12 3 0 -5.90 11.20 -13 -3 0 19.00 7.40 -13 -3 0 12.90 10.20 -14 -3 0 25.30 12.20 -14 -3 0 33.70 10.30 15 -4 0 57.09 9.40 -15 4 0 73.49 14.50 14 -4 0 91.09 15.30 -14 4 0 93.59 12.00 -14 4 0 104.89 16.50 13 -4 0 50.69 10.80 -13 4 0 75.29 11.50 -13 4 0 51.79 11.70 12 -4 0 53.39 10.60 12 -4 0 67.99 12.30 -12 4 0 74.09 12.20 -12 4 0 71.29 10.60 -12 4 0 65.19 10.80 11 -4 0 442.36 27.80 11 -4 0 451.15 26.60 -11 4 0 377.86 26.50 -11 4 0 430.66 26.20 10 -4 0 551.04 31.50 10 -4 0 552.34 33.40 -10 4 0 573.74 31.70 -10 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1537.85 74.89 9 -7 0 1393.76 75.09 -9 7 0 1357.96 73.29 -9 7 0 1405.16 74.09 -9 7 0 1442.06 74.19 8 -7 0 718.93 40.50 8 -7 0 658.73 38.60 8 -7 0 756.42 39.70 -8 7 0 805.22 41.60 -8 7 0 766.52 38.70 -8 7 0 762.32 39.50 7 -7 0 236.08 14.40 7 -7 0 268.57 15.70 7 -7 0 257.17 16.80 -7 7 0 258.17 14.40 -7 7 0 249.18 15.50 -7 7 0 270.47 15.50 6 -7 0 16.60 5.30 6 -7 0 14.60 4.40 6 -7 0 14.70 3.40 6 -7 0 15.10 3.80 -6 7 0 27.80 7.00 -6 7 0 14.30 3.20 -6 7 0 12.20 4.10 5 -7 0 1749.03 88.09 5 -7 0 1685.33 87.99 5 -7 0 1791.72 88.79 5 -7 0 1660.73 88.29 -5 7 0 1750.12 87.89 -5 7 0 1760.72 88.29 -5 7 0 1684.63 88.09 4 -7 0 772.22 37.80 4 -7 0 708.03 37.00 4 -7 0 721.63 37.00 4 -7 0 666.63 37.10 -4 7 0 720.53 36.70 -4 7 0 713.03 37.10 -4 7 0 709.23 37.10 3 -7 0 166.78 9.60 3 -7 0 157.28 9.60 -3 7 0 163.38 9.70 -3 7 0 167.68 9.20 -3 7 0 169.98 9.70 2 -7 0 11.10 2.60 2 -7 0 17.80 2.90 2 -7 0 17.70 3.40 -2 7 0 15.00 2.80 -2 7 0 12.50 2.30 1 -7 0 318.87 17.30 1 -7 0 335.67 17.50 1 -7 0 327.27 17.00 -1 7 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5.70 5.80 5 -10 4 2.30 8.30 -6 10 -4 107.29 12.00 -6 10 -4 93.49 8.10 -6 10 -4 91.69 9.80 6 -10 4 91.29 11.30 6 -10 4 91.89 13.70 -7 10 -4 871.41 44.60 -7 10 -4 857.91 43.80 -7 10 -4 859.41 44.60 7 -10 4 889.41 45.30 7 -10 4 727.53 46.70 -8 10 -4 -0.50 7.50 -8 10 -4 20.30 5.70 -8 10 -4 0.60 6.40 8 -10 4 9.50 10.50 8 -10 4 13.40 8.40 -9 10 -4 470.25 27.60 -9 10 -4 480.25 28.10 -9 10 -4 505.45 26.80 9 -10 4 490.75 29.00 9 -10 4 459.35 31.60 -10 10 -4 81.99 14.20 -10 10 -4 75.69 12.10 -10 10 -4 69.39 10.60 10 -10 4 81.19 17.90 10 -10 4 76.09 12.00 -11 10 -4 112.29 12.50 -11 10 -4 131.99 16.10 11 -10 4 122.99 16.70 -12 10 -4 14.00 8.00 -12 10 -4 2.20 10.10 12 -10 4 13.00 11.40 -13 10 -4 -7.30 9.50 13 -10 4 8.30 10.10 -12 -9 4 2.90 9.90 11 9 -4 18.80 19.60 11 9 -4 22.10 10.30 -11 -9 4 33.90 11.40 10 9 -4 -5.70 11.50 10 9 -4 -2.00 12.50 10 9 -4 1.60 8.90 -10 -9 4 1.60 12.70 -10 -9 4 6.30 8.40 9 9 -4 39.20 11.00 9 9 -4 48.30 9.70 -9 -9 4 65.59 11.50 8 9 -4 94.79 14.50 8 9 -4 103.49 14.20 -8 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4.70 -1 9 -4 49.90 6.20 -1 9 -4 39.80 5.60 1 -9 4 47.20 5.00 1 -9 4 43.50 5.70 -2 9 -4 185.68 10.90 -2 9 -4 176.78 10.60 -2 9 -4 175.18 10.00 2 -9 4 161.98 11.10 2 -9 4 176.78 10.00 -3 9 -4 1214.58 63.79 -3 9 -4 1205.48 63.39 -3 9 -4 1306.97 63.89 3 -9 4 1246.68 64.09 -4 9 -4 790.42 39.10 -4 9 -4 740.43 38.50 -4 9 -4 746.83 38.90 4 -9 4 732.73 40.50 4 -9 4 727.03 39.30 -5 9 -4 333.77 18.10 -5 9 -4 308.07 17.90 -5 9 -4 307.07 17.30 5 -9 4 348.87 21.00 5 -9 4 318.27 18.70 -6 9 -4 54.49 7.90 -6 9 -4 53.49 7.90 -6 9 -4 50.39 6.10 6 -9 4 59.59 8.50 6 -9 4 59.49 12.00 6 -9 4 60.69 9.60 -7 9 -4 1.70 4.40 -7 9 -4 3.10 5.40 -7 9 -4 11.20 6.10 7 -9 4 17.60 9.30 7 -9 4 10.10 7.00 7 -9 4 10.60 7.00 -8 9 -4 460.75 26.90 -8 9 -4 467.55 26.00 -8 9 -4 468.05 27.00 8 -9 4 539.45 30.80 8 -9 4 468.95 28.20 -9 9 -4 629.54 34.60 -9 9 -4 617.84 35.00 -9 9 -4 590.04 34.00 9 -9 4 610.34 37.50 9 -9 4 635.34 35.30 -10 9 -4 0.30 6.60 -10 9 -4 4.50 9.30 -10 9 -4 15.60 7.90 10 -9 4 13.10 12.10 10 -9 4 2.10 9.60 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4.50 -4 -8 4 6.20 4.40 3 8 -4 1284.67 66.99 3 8 -4 1302.07 66.99 3 8 -4 1335.07 66.59 -3 -8 4 1310.07 66.89 -3 -8 4 1309.07 66.89 -3 -8 4 1327.47 66.79 -3 -8 4 1236.68 66.29 2 8 -4 902.51 45.30 2 8 -4 856.31 45.30 2 8 -4 864.11 44.80 -2 -8 4 874.71 45.00 -2 -8 4 859.91 45.20 1 8 -4 1072.49 52.29 1 8 -4 1030.30 51.79 1 8 -4 978.20 52.09 -1 -8 4 882.41 52.09 -1 -8 4 1077.29 52.09 -1 -8 4 1035.50 51.99 0 8 -4 369.36 20.70 0 8 -4 406.66 20.80 0 8 -4 384.46 20.40 0 -8 4 397.06 20.50 -1 8 -4 53.49 5.40 -1 8 -4 54.69 5.40 -1 8 -4 56.69 4.40 1 -8 4 48.30 5.50 -2 8 -4 600.24 29.80 -2 8 -4 569.84 29.30 2 -8 4 571.34 29.30 2 -8 4 537.85 29.90 -3 8 -4 1163.18 59.59 -3 8 -4 1105.39 59.89 -3 8 -4 1210.58 59.99 3 -8 4 1115.19 60.19 3 -8 4 1179.08 59.89 3 -8 4 1249.47 61.09 -4 8 -4 513.65 27.40 -4 8 -4 544.15 27.90 -4 8 -4 527.05 27.80 4 -8 4 542.95 28.30 4 -8 4 545.75 28.00 4 -8 4 511.45 29.30 -5 8 -4 2.60 2.70 -5 8 -4 1.90 3.70 -5 8 -4 -1.30 3.80 5 -8 4 0.00 4.30 5 -8 4 5.70 6.80 5 -8 4 1.80 4.70 -6 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-7 4 28.80 10.10 -10 -7 4 32.80 9.20 -10 -7 4 39.50 7.50 9 7 -4 111.09 13.80 9 7 -4 86.39 12.80 9 7 -4 103.19 16.80 -9 -7 4 99.69 14.00 8 7 -4 602.14 35.20 8 7 -4 601.54 33.80 -8 -7 4 669.93 34.00 -8 -7 4 677.03 34.90 7 7 -4 305.27 18.30 7 7 -4 260.87 16.30 -7 -7 4 294.37 17.70 -7 -7 4 273.57 16.40 6 7 -4 100.99 10.40 6 7 -4 84.69 9.90 6 7 -4 74.49 7.90 -6 -7 4 97.49 9.90 -6 -7 4 99.99 9.80 -6 -7 4 85.59 7.70 5 7 -4 213.98 14.10 5 7 -4 209.68 14.00 5 7 -4 225.08 12.80 -5 -7 4 232.38 13.40 -5 -7 4 211.78 12.50 -5 -7 4 221.58 13.90 4 7 -4 347.97 19.10 4 7 -4 338.77 18.50 4 7 -4 358.86 19.30 -4 -7 4 341.07 19.00 -4 -7 4 354.96 19.00 -4 -7 4 330.67 18.20 -4 -7 4 330.37 18.80 3 7 -4 1860.11 93.69 3 7 -4 1870.71 93.29 3 7 -4 1775.82 93.59 -3 -7 4 1823.22 93.49 -3 -7 4 1752.32 93.19 -3 -7 4 1831.52 93.49 -3 -7 4 1908.91 93.59 2 7 -4 995.40 52.59 2 7 -4 1010.30 52.69 2 7 -4 1030.40 52.29 -2 -7 4 1059.39 52.49 -2 -7 4 958.00 52.59 -2 -7 4 1083.49 52.49 1 7 -4 431.16 22.10 1 7 -4 424.56 22.50 1 7 -4 400.56 22.30 -1 -7 4 448.16 22.30 -1 -7 4 416.36 22.70 0 7 -4 266.77 15.10 0 7 -4 281.27 14.90 0 -7 4 288.77 15.00 0 -7 4 297.37 15.40 -1 7 -4 349.27 18.20 -1 7 -4 327.07 18.10 -1 7 -4 354.46 17.80 1 -7 4 335.57 18.30 1 -7 4 351.26 17.90 -2 7 -4 45.30 4.20 -2 7 -4 44.20 3.80 -2 7 -4 37.60 3.10 2 -7 4 28.00 4.50 2 -7 4 35.80 3.40 2 -7 4 24.80 5.10 -3 7 -4 123.59 8.70 -3 7 -4 118.89 6.70 -3 7 -4 125.19 7.40 3 -7 4 115.09 7.50 3 -7 4 111.89 8.00 3 -7 4 117.29 9.50 -4 7 -4 253.67 14.00 -4 7 -4 248.98 13.90 -4 7 -4 245.18 13.50 4 -7 4 264.97 14.70 4 -7 4 264.97 14.30 4 -7 4 257.97 15.60 -5 7 -4 6.20 2.30 -5 7 -4 8.80 3.30 -5 7 -4 9.60 3.40 5 -7 4 8.10 5.90 5 -7 4 5.40 4.20 5 -7 4 5.20 4.30 -6 7 -4 197.78 11.80 -6 7 -4 180.48 11.60 6 -7 4 195.48 12.80 6 -7 4 201.88 12.70 6 -7 4 189.48 14.80 -7 7 -4 590.84 30.80 -7 7 -4 566.84 30.70 -7 7 -4 564.74 30.10 7 -7 4 561.04 33.10 7 -7 4 567.64 31.30 7 -7 4 610.14 31.60 -8 7 -4 63.79 8.90 -8 7 -4 67.79 9.20 -8 7 -4 57.99 7.20 8 -7 4 67.29 13.20 8 -7 4 40.00 7.80 8 -7 4 58.09 10.90 -9 7 -4 137.19 17.30 -9 7 -4 107.29 11.40 -9 7 -4 105.59 9.60 9 -7 4 115.39 13.50 9 -7 4 83.49 16.50 9 -7 4 88.89 12.90 -10 7 -4 214.38 16.40 -10 7 -4 222.28 14.30 -10 7 -4 211.18 16.00 10 -7 4 201.48 18.50 10 -7 4 196.98 20.30 10 -7 4 209.48 18.30 -11 7 -4 223.08 18.20 -11 7 -4 228.68 15.40 -11 7 -4 197.88 16.60 11 -7 4 193.58 21.50 11 -7 4 213.78 17.90 -12 7 -4 159.68 17.10 -12 7 -4 176.68 13.50 -12 7 -4 120.69 16.20 12 -7 4 165.38 26.50 12 -7 4 174.88 16.90 -13 7 -4 92.49 11.50 -13 7 -4 85.69 15.10 13 -7 4 100.09 14.80 -14 7 -4 3.40 9.40 -13 -6 4 80.49 12.10 12 6 -4 35.70 12.50 12 6 -4 5.80 6.90 -12 -6 4 33.00 11.10 -12 -6 4 26.60 8.30 -12 -6 4 22.70 11.10 11 6 -4 20.00 11.50 11 6 -4 26.60 8.80 11 6 -4 2.40 10.30 -11 -6 4 14.00 8.50 -11 -6 4 17.60 7.10 -11 -6 4 16.60 10.90 10 6 -4 143.19 14.90 10 6 -4 189.78 15.80 10 6 -4 160.68 19.30 -10 -6 4 160.18 12.90 -10 -6 4 203.88 16.90 -10 -6 4 172.18 15.60 9 6 -4 150.88 17.30 9 6 -4 160.28 14.40 9 6 -4 193.68 15.50 -9 -6 4 177.88 15.60 8 6 -4 77.79 10.30 8 6 -4 71.99 11.50 8 6 -4 61.99 7.90 -8 -6 4 77.59 11.60 -8 -6 4 74.89 8.50 7 6 -4 28.60 6.40 7 6 -4 19.80 4.50 7 6 -4 12.90 6.50 -7 -6 4 21.80 6.20 -7 -6 4 17.10 6.00 -7 -6 4 16.60 4.60 6 6 -4 6.30 5.10 6 6 -4 4.00 4.00 6 6 -4 8.00 5.20 -6 -6 4 6.80 5.10 -6 -6 4 10.50 5.20 -6 -6 4 9.60 3.70 5 6 -4 120.29 9.50 5 6 -4 117.59 7.90 5 6 -4 122.29 8.80 -5 -6 4 109.09 7.50 -5 -6 4 111.09 8.20 -5 -6 4 112.39 9.10 4 6 -4 86.99 6.40 4 6 -4 89.69 7.80 4 6 -4 84.69 7.10 -4 -6 4 102.99 7.30 -4 -6 4 83.49 7.10 -4 -6 4 94.99 6.10 -4 -6 4 84.39 6.90 3 6 -4 520.75 25.70 3 6 -4 510.75 26.10 3 6 -4 472.35 26.00 -3 -6 4 419.86 26.50 -3 -6 4 510.45 25.90 -3 -6 4 524.45 26.00 2 6 -4 18.30 2.60 2 6 -4 18.10 3.50 -2 -6 4 18.20 3.20 -2 -6 4 17.10 2.80 1 6 -4 742.83 36.30 1 6 -4 713.93 36.00 1 6 -4 639.14 36.10 -1 -6 4 695.93 36.30 -1 -6 4 722.83 36.10 0 6 -4 351.36 18.10 0 -6 4 355.56 17.90 0 -6 4 321.87 18.20 -1 6 -4 1230.78 61.59 -1 6 -4 1170.38 61.39 1 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71.09 9.50 -4 13 -9 74.79 10.90 -4 13 -9 72.89 12.30 4 -13 9 81.19 15.30 -5 13 -9 98.19 12.30 -5 13 -9 92.89 9.90 -5 13 -9 64.69 12.20 5 -13 9 82.79 15.50 -6 13 -9 90.79 10.40 -6 13 -9 88.59 12.90 -6 13 -9 79.29 10.00 6 -13 9 78.39 15.80 -7 13 -9 73.29 10.30 7 -13 9 95.99 19.40 8 -13 9 16.00 11.20 -9 13 -9 82.99 10.40 9 -13 9 83.09 16.30 10 -13 9 114.09 14.50 10 12 -9 49.00 11.60 9 12 -9 49.30 12.60 8 12 -9 3.70 10.00 8 12 -9 12.60 11.60 8 12 -9 11.30 8.10 7 12 -9 -0.10 11.00 7 12 -9 10.90 7.80 7 12 -9 17.70 10.40 6 12 -9 103.09 15.20 6 12 -9 114.59 16.60 6 12 -9 86.89 12.60 5 12 -9 25.20 8.10 5 12 -9 19.20 10.90 5 12 -9 42.50 10.10 4 12 -9 5.20 8.20 4 12 -9 12.70 9.90 4 12 -9 12.60 7.80 -4 -12 9 16.40 8.50 3 12 -9 38.10 9.90 3 12 -9 33.00 6.80 3 12 -9 38.50 8.90 -3 -12 9 22.60 8.60 2 12 -9 39.10 7.30 2 12 -9 74.99 12.10 2 12 -9 62.09 12.30 -2 -12 9 60.99 11.70 1 12 -9 318.17 20.50 1 12 -9 337.77 18.90 -1 -12 9 299.67 21.60 0 12 -9 158.88 13.80 0 12 -9 148.39 13.10 0 12 -9 157.08 11.50 0 -12 9 142.39 13.50 -1 12 -9 6.80 5.40 -1 12 -9 5.30 6.60 -1 12 -9 5.90 7.00 1 -12 9 1.60 8.10 -2 12 -9 13.50 5.20 -2 12 -9 8.80 6.90 -2 12 -9 11.40 6.40 2 -12 9 8.50 8.30 -3 12 -9 26.10 6.30 -3 12 -9 38.70 7.50 -3 12 -9 29.20 5.50 3 -12 9 17.80 8.90 -4 12 -9 158.98 12.60 -4 12 -9 171.98 11.70 4 -12 9 185.68 16.50 -5 12 -9 16.10 5.80 -5 12 -9 25.20 5.70 -5 12 -9 12.10 7.40 5 -12 9 21.20 10.50 -6 12 -9 147.49 11.80 -6 12 -9 156.78 13.40 -6 12 -9 173.48 11.90 6 -12 9 192.08 17.90 -7 12 -9 28.10 8.00 -7 12 -9 23.20 6.30 7 -12 9 22.90 11.60 -8 12 -9 3.00 6.00 8 -12 9 9.60 11.50 -9 12 -9 10.60 6.20 9 -12 9 4.70 10.40 -10 12 -9 22.10 6.30 10 -12 9 25.40 11.20 11 11 -9 2.90 11.80 10 11 -9 19.60 12.10 -10 -11 9 30.60 15.00 9 11 -9 -8.80 11.30 9 11 -9 9.70 11.80 -9 -11 9 1.80 8.40 8 11 -9 6.70 8.80 8 11 -9 3.90 11.60 8 11 -9 2.40 7.50 7 11 -9 115.39 15.30 7 11 -9 109.09 12.50 7 11 -9 123.09 16.00 6 11 -9 102.19 14.70 6 11 -9 113.29 12.80 6 11 -9 132.09 14.80 5 11 -9 100.19 11.70 5 11 -9 109.79 14.50 5 11 -9 123.39 15.20 -5 -11 9 112.49 13.60 4 11 -9 16.50 7.80 4 11 -9 20.20 6.60 4 11 -9 16.70 8.70 -4 -11 9 12.80 8.50 3 11 -9 517.55 28.60 3 11 -9 512.25 27.40 -3 -11 9 463.15 29.10 2 11 -9 294.07 20.10 2 11 -9 334.57 18.90 2 11 -9 334.27 20.20 -2 -11 9 326.17 20.90 1 11 -9 12.10 7.00 1 11 -9 10.50 6.70 1 11 -9 4.60 5.10 -1 -11 9 17.60 7.80 0 11 -9 19.00 5.90 0 11 -9 17.00 6.70 0 11 -9 20.50 5.00 0 -11 9 34.20 8.20 -1 11 -9 188.58 12.90 -1 11 -9 179.48 11.60 -1 11 -9 182.68 13.00 1 -11 9 184.88 15.20 -2 11 -9 130.29 11.30 -2 11 -9 141.69 9.80 -2 11 -9 144.89 11.00 2 -11 9 143.09 19.10 -3 11 -9 2.90 5.80 -3 11 -9 3.10 4.20 -3 11 -9 -0.60 4.90 3 -11 9 -1.70 8.60 -4 11 -9 706.73 38.40 -4 11 -9 694.73 38.00 -4 11 -9 723.23 37.60 4 -11 9 776.02 40.60 -5 11 -9 17.40 4.90 -5 11 -9 15.40 4.80 -5 11 -9 12.80 6.50 5 -11 9 13.70 6.50 5 -11 9 11.20 9.40 -6 11 -9 252.77 15.00 -6 11 -9 246.18 16.20 -6 11 -9 231.08 14.70 6 -11 9 295.57 20.60 6 -11 9 231.98 17.10 6 -11 9 232.18 22.60 -7 11 -9 293.77 17.80 7 -11 9 344.97 22.40 7 -11 9 289.67 26.30 -8 11 -9 30.30 6.00 8 -11 9 7.40 12.90 8 -11 9 20.90 10.90 9 -11 9 127.09 17.50 9 -11 9 135.49 26.10 -10 11 -9 13.50 6.00 10 -11 9 7.80 9.90 -11 11 -9 18.90 6.10 11 -11 9 10.80 12.20 12 10 -9 -11.20 9.30 11 10 -9 3.00 10.80 10 10 -9 -3.70 9.50 10 10 -9 -7.30 12.00 10 10 -9 -8.60 15.70 -10 -10 9 -9.00 10.30 9 10 -9 71.59 10.90 9 10 -9 77.39 20.50 9 10 -9 45.40 9.80 -9 -10 9 77.89 18.80 8 10 -9 -3.30 7.60 8 10 -9 2.60 8.70 8 10 -9 -5.60 10.20 -8 -10 9 3.50 9.80 -8 -10 9 -4.60 9.40 7 10 -9 19.00 9.90 7 10 -9 11.00 7.50 7 10 -9 14.10 9.60 -7 -10 9 8.70 8.60 -7 -10 9 7.30 8.00 6 10 -9 150.28 14.90 6 10 -9 163.38 12.90 6 10 -9 159.78 16.00 -6 -10 9 136.19 12.80 -6 -10 9 148.39 13.80 5 10 -9 7.00 6.40 5 10 -9 2.80 9.00 5 10 -9 6.00 7.80 4 10 -9 365.06 20.80 4 10 -9 373.36 22.40 4 10 -9 376.06 22.40 -4 -10 9 345.47 22.70 3 10 -9 535.15 28.60 3 10 -9 550.84 29.60 3 10 -9 522.85 29.70 -3 -10 9 512.85 30.00 2 10 -9 39.10 6.80 2 10 -9 39.60 7.00 2 10 -9 32.50 5.50 -2 -10 9 32.60 7.80 1 10 -9 33.00 5.10 1 10 -9 39.50 6.40 1 10 -9 44.20 8.70 -1 -10 9 32.40 7.50 0 10 -9 25.20 5.70 0 10 -9 13.40 5.10 0 10 -9 23.10 4.40 0 -10 9 15.30 7.10 -1 10 -9 375.36 21.10 -1 10 -9 381.26 20.50 -1 10 -9 384.76 21.20 1 -10 9 380.66 22.70 -2 10 -9 74.59 6.70 -2 10 -9 78.79 8.10 -2 10 -9 72.39 7.60 2 -10 9 73.09 10.90 -3 10 -9 -3.70 5.00 -3 10 -9 -2.70 4.10 -3 10 -9 -2.20 3.50 3 -10 9 -11.00 5.20 3 -10 9 -0.70 7.60 -4 10 -9 387.46 21.50 -4 10 -9 398.26 21.90 -4 10 -9 404.06 21.10 4 -10 9 392.16 26.50 4 -10 9 414.36 24.10 4 -10 9 373.76 22.10 -5 10 -9 70.39 7.40 -5 10 -9 67.99 9.10 -5 10 -9 81.99 7.10 5 -10 9 89.79 14.00 5 -10 9 71.29 10.20 5 -10 9 76.29 16.70 -6 10 -9 314.17 18.60 -6 10 -9 355.56 18.70 -6 10 -9 313.97 20.70 6 -10 9 346.47 21.00 6 -10 9 334.87 24.90 6 -10 9 362.76 23.30 -7 10 -9 186.08 12.20 7 -10 9 171.98 15.80 7 -10 9 185.08 18.10 7 -10 9 186.88 24.90 -8 10 -9 31.00 5.70 8 -10 9 21.30 10.50 8 -10 9 14.80 12.40 8 -10 9 8.10 9.30 -9 10 -9 10.60 6.10 9 -10 9 25.20 23.60 9 -10 9 18.30 10.60 -10 10 -9 158.98 12.20 10 -10 9 153.28 17.10 11 -10 9 41.30 9.10 12 9 -9 9.20 11.50 11 9 -9 61.19 12.20 10 9 -9 33.90 12.00 10 9 -9 9.20 10.50 10 9 -9 38.10 13.00 -10 -9 9 16.60 10.70 9 9 -9 13.30 9.00 9 9 -9 17.50 11.40 9 9 -9 -1.50 7.30 -9 -9 9 -1.80 7.50 -9 -9 9 13.70 10.00 8 9 -9 30.90 9.70 8 9 -9 31.20 7.70 8 9 -9 35.00 11.10 -8 -9 9 20.40 8.00 -8 -9 9 36.10 9.80 7 9 -9 -7.20 8.20 7 9 -9 -1.10 9.40 7 9 -9 -1.20 6.70 -7 -9 9 7.30 9.20 -7 -9 9 -3.90 6.90 6 9 -9 315.87 19.90 6 9 -9 290.87 17.70 6 9 -9 287.57 19.50 -6 -9 9 261.37 18.20 -6 -9 9 281.97 18.20 5 9 -9 61.29 10.90 5 9 -9 61.79 8.60 5 9 -9 53.89 10.20 -5 -9 9 62.09 10.60 -5 -9 9 37.50 6.80 4 9 -9 159.78 10.60 4 9 -9 160.18 12.00 4 9 -9 158.78 12.60 -4 -9 9 121.59 11.30 -4 -9 9 130.79 13.40 3 9 -9 11.20 6.00 3 9 -9 -1.80 4.70 3 9 -9 10.00 6.30 -3 -9 9 17.10 7.10 2 9 -9 5.00 4.90 2 9 -9 0.10 4.00 2 9 -9 4.10 5.40 -2 -9 9 3.60 6.30 1 9 -9 360.46 20.60 1 9 -9 373.26 19.90 1 9 -9 378.66 20.60 -1 -9 9 355.16 21.70 0 9 -9 310.87 16.60 0 9 -9 292.57 17.40 0 9 -9 308.87 17.20 0 -9 9 303.87 18.50 -1 9 -9 257.67 15.20 -1 9 -9 270.27 14.60 -1 9 -9 268.47 15.30 1 -9 9 272.37 16.90 -2 9 -9 7.40 4.30 -2 9 -9 10.10 3.00 -2 9 -9 8.40 3.60 2 -9 9 4.90 4.00 2 -9 9 13.00 6.70 -3 9 -9 8.10 4.40 -3 9 -9 9.80 2.90 -3 9 -9 4.70 3.40 3 -9 9 7.60 8.70 3 -9 9 11.50 7.00 3 -9 9 -0.90 5.20 -4 9 -9 35.40 5.40 -4 9 -9 32.20 3.70 -4 9 -9 38.40 6.70 4 -9 9 30.80 6.00 4 -9 9 38.40 9.70 4 -9 9 36.00 8.00 -5 9 -9 139.79 8.70 -5 9 -9 128.29 9.00 5 -9 9 151.08 14.40 5 -9 9 145.89 17.40 5 -9 9 126.39 11.90 -6 9 -9 183.68 11.60 -6 9 -9 195.88 11.80 6 -9 9 200.08 19.50 6 -9 9 222.58 15.50 6 -9 9 222.48 17.20 7 -9 9 175.28 17.10 7 -9 9 160.28 15.20 7 -9 9 155.68 19.80 -8 9 -9 32.20 5.50 8 -9 9 16.20 12.30 8 -9 9 21.60 10.00 8 -9 9 26.00 10.10 -9 9 -9 247.58 14.80 9 -9 9 249.08 23.50 9 -9 9 171.48 21.90 -10 9 -9 201.18 13.10 10 -9 9 186.68 18.30 10 -9 9 182.28 17.60 10 -9 9 164.28 21.70 -11 9 -9 40.10 6.40 11 -9 9 27.90 8.80 13 8 -9 0.30 8.90 -13 -8 9 0.70 9.50 12 8 -9 8.60 11.10 11 8 -9 48.40 10.50 11 8 -9 48.60 19.50 11 8 -9 87.39 12.70 -11 -8 9 23.90 15.60 10 8 -9 94.89 13.30 10 8 -9 96.29 16.10 10 8 -9 75.99 11.40 10 8 -9 48.70 11.60 -10 -8 9 76.29 13.40 -10 -8 9 92.09 14.30 9 8 -9 -4.10 8.50 9 8 -9 -0.90 10.30 9 8 -9 2.10 6.80 -9 -8 9 10.00 8.20 -9 -8 9 9.10 9.60 8 8 -9 7.30 6.90 8 8 -9 3.10 9.50 8 8 -9 9.70 8.70 -8 -8 9 -4.50 8.80 -8 -8 9 8.10 7.50 7 8 -9 36.50 9.40 7 8 -9 10.40 6.10 7 8 -9 15.90 7.80 -7 -8 9 20.10 9.50 -7 -8 9 8.30 7.80 6 8 -9 60.19 11.10 6 8 -9 62.39 8.60 -6 -8 9 56.79 9.70 -6 -8 9 60.79 9.40 5 8 -9 148.19 11.80 5 8 -9 138.89 10.50 5 8 -9 147.89 12.40 -5 -8 9 117.39 10.90 -5 -8 9 125.89 10.80 -5 -8 9 163.28 13.00 4 8 -9 15.60 4.50 4 8 -9 11.40 5.30 4 8 -9 14.00 5.80 -4 -8 9 3.70 6.50 -4 -8 9 10.00 4.60 3 8 -9 8.70 4.10 3 8 -9 10.50 5.10 3 8 -9 10.60 5.20 -3 -8 9 7.90 6.30 2 8 -9 22.90 4.70 2 8 -9 36.50 5.40 2 8 -9 37.30 6.80 -2 -8 9 33.60 6.60 1 8 -9 31.90 6.00 1 8 -9 30.30 6.10 -1 -8 9 30.00 6.20 0 8 -9 240.18 14.40 0 8 -9 259.27 13.80 0 8 -9 256.47 14.40 0 -8 9 263.17 15.80 -1 8 -9 38.70 5.10 -1 8 -9 31.10 5.20 -1 8 -9 38.90 4.10 1 -8 9 30.20 6.20 1 -8 9 33.90 4.60 -2 8 -9 8.10 2.30 -2 8 -9 6.30 2.80 2 -8 9 1.80 7.30 2 -8 9 14.30 6.00 2 -8 9 -3.00 3.90 -3 8 -9 303.47 16.40 -3 8 -9 306.37 16.10 3 -8 9 294.17 20.50 3 -8 9 315.07 17.40 3 -8 9 312.97 18.70 -4 8 -9 511.65 27.60 -4 8 -9 507.45 27.80 4 -8 9 551.44 29.10 4 -8 9 523.35 31.10 4 -8 9 605.74 30.20 -5 8 -9 28.80 3.50 -5 8 -9 31.10 4.30 5 -8 9 35.60 10.00 5 -8 9 19.70 8.10 5 -8 9 39.10 7.00 -6 8 -9 19.60 3.30 -6 8 -9 26.50 3.70 6 -8 9 17.40 9.50 6 -8 9 9.40 10.60 6 -8 9 28.50 8.70 -7 8 -9 7.90 4.10 7 -8 9 9.20 8.30 7 -8 9 21.60 9.20 7 -8 9 18.10 12.30 -8 8 -9 82.39 8.40 8 -8 9 96.29 14.00 8 -8 9 83.49 15.00 8 -8 9 72.79 14.10 -9 8 -9 61.29 8.60 9 -8 9 63.49 11.40 9 -8 9 35.20 13.30 9 -8 9 67.69 11.30 10 -8 9 51.59 10.40 10 -8 9 86.39 12.30 10 -8 9 52.89 14.50 -11 8 -9 5.80 5.90 11 -8 9 10.60 9.10 12 -8 9 36.40 8.60 13 7 -9 -4.40 9.70 -13 -7 9 14.60 9.70 12 7 -9 7.90 11.20 11 7 -9 41.20 11.60 11 7 -9 15.00 12.00 -11 -7 9 19.60 10.10 10 7 -9 -1.50 9.30 10 7 -9 5.80 9.90 10 7 -9 0.20 10.10 10 7 -9 6.70 6.90 -10 -7 9 -3.80 10.10 -10 -7 9 -5.60 7.50 9 7 -9 9.50 7.00 9 7 -9 2.40 9.70 9 7 -9 3.00 8.40 -9 -7 9 4.00 7.30 -9 -7 9 24.30 9.50 8 7 -9 5.10 8.40 8 7 -9 14.30 6.40 8 7 -9 6.40 9.20 -8 -7 9 11.70 7.30 7 7 -9 117.19 10.10 7 7 -9 105.99 12.70 7 7 -9 109.29 12.50 -7 -7 9 95.39 11.70 -7 -7 9 85.69 11.20 6 7 -9 22.30 6.60 6 7 -9 18.20 5.20 6 7 -9 19.10 6.60 -6 -7 9 21.20 6.30 -6 -7 9 27.00 6.20 5 7 -9 169.58 12.50 5 7 -9 162.18 12.00 5 7 -9 160.28 10.70 -5 -7 9 157.48 12.70 -5 -7 9 144.39 10.80 -5 -7 9 152.18 11.20 4 7 -9 146.59 10.90 4 7 -9 134.39 9.30 4 7 -9 141.79 11.00 -4 -7 9 128.69 11.30 -4 -7 9 132.99 9.60 3 7 -9 38.70 6.90 3 7 -9 37.10 5.30 3 7 -9 33.40 6.60 -3 -7 9 44.60 6.70 -3 -7 9 34.20 5.20 2 7 -9 56.69 6.70 2 7 -9 58.29 6.50 2 7 -9 55.99 5.40 -2 -7 9 60.69 8.60 1 7 -9 38.20 5.30 1 7 -9 30.40 5.30 1 7 -9 32.20 4.20 -1 -7 9 31.00 5.70 0 7 -9 9.30 3.00 0 7 -9 5.90 2.20 0 -7 9 3.80 2.90 0 -7 9 7.50 5.00 -1 7 -9 106.89 7.00 -1 7 -9 105.49 6.40 1 -7 9 114.39 9.70 1 -7 9 114.49 7.60 1 -7 9 111.99 10.90 -2 7 -9 81.79 5.50 -2 7 -9 67.89 5.90 -2 7 -9 83.59 4.80 2 -7 9 84.99 8.70 2 -7 9 88.59 10.70 2 -7 9 78.39 7.20 -3 7 -9 525.65 28.90 -3 7 -9 521.95 28.70 3 -7 9 581.24 31.70 3 -7 9 597.74 30.10 3 -7 9 605.54 30.70 -4 7 -9 352.96 18.90 -4 7 -9 336.87 19.00 4 -7 9 408.96 27.80 4 -7 9 373.86 20.90 4 -7 9 400.86 21.60 -5 7 -9 9.90 2.40 -5 7 -9 11.90 2.40 5 -7 9 17.70 7.40 5 -7 9 9.40 6.00 5 -7 9 7.30 8.60 -6 7 -9 193.98 11.70 -6 7 -9 217.88 11.80 6 -7 9 219.68 19.30 6 -7 9 218.88 18.50 6 -7 9 240.48 17.00 -7 7 -9 93.49 7.20 7 -7 9 78.09 13.50 7 -7 9 82.89 17.70 7 -7 9 88.79 13.20 -8 7 -9 125.69 9.40 8 -7 9 73.79 25.30 8 -7 9 125.99 15.40 8 -7 9 151.58 15.80 -9 7 -9 91.39 9.10 9 -7 9 82.39 18.50 9 -7 9 98.39 15.50 9 -7 9 78.39 14.90 -10 7 -9 8.20 5.90 10 -7 9 5.40 17.30 10 -7 9 13.70 10.00 10 -7 9 26.40 11.10 -11 7 -9 99.99 9.90 11 -7 9 88.39 14.10 11 -7 9 92.99 15.70 -12 7 -9 72.09 8.90 12 -7 9 68.99 11.90 13 6 -9 20.20 15.60 -13 -6 9 5.40 13.30 12 6 -9 -9.40 11.00 12 6 -9 5.00 9.60 11 6 -9 138.29 17.20 11 6 -9 75.59 18.70 -11 -6 9 84.89 14.10 10 6 -9 21.50 8.30 10 6 -9 11.30 10.10 10 6 -9 4.70 9.30 10 6 -9 5.70 10.20 -10 -6 9 13.70 10.10 -10 -6 9 23.40 9.20 9 6 -9 9.70 8.40 9 6 -9 8.70 6.40 9 6 -9 12.80 9.60 -9 -6 9 3.30 7.20 -9 -6 9 20.30 9.20 8 6 -9 52.19 8.80 8 6 -9 27.00 8.80 8 6 -9 29.10 7.80 -8 -6 9 42.90 8.20 -8 -6 9 51.19 7.90 7 6 -9 5.10 6.90 7 6 -9 11.70 6.60 7 6 -9 12.10 5.30 -7 -6 9 8.20 6.60 -7 -6 9 11.00 6.40 6 6 -9 5.40 6.50 6 6 -9 6.20 4.60 -6 -6 9 9.40 5.20 -6 -6 9 12.50 5.60 5 6 -9 178.68 11.00 5 6 -9 180.28 12.30 5 6 -9 166.68 11.70 -5 -6 9 182.88 13.10 -5 -6 9 177.98 11.60 -5 -6 9 171.28 11.20 4 6 -9 705.83 38.40 4 6 -9 752.72 38.90 4 6 -9 748.13 38.90 -4 -6 9 754.82 38.50 -4 -6 9 732.43 39.20 3 6 -9 284.27 16.40 3 6 -9 290.27 16.50 3 6 -9 292.67 15.80 -3 -6 9 305.47 17.40 -3 -6 9 282.47 15.60 2 6 -9 221.98 13.50 2 6 -9 243.88 13.60 2 6 -9 248.38 13.10 -2 -6 9 242.18 14.80 1 6 -9 3.50 2.30 1 6 -9 4.70 3.00 1 6 -9 -0.10 2.80 -1 -6 9 4.60 2.80 -1 -6 9 1.50 4.70 0 6 -9 137.49 7.70 0 6 -9 132.79 8.30 0 6 -9 142.29 8.30 0 -6 9 151.48 10.20 -1 6 -9 675.03 34.10 -1 6 -9 643.64 33.90 1 -6 9 685.43 35.80 1 -6 9 645.14 34.50 1 -6 9 680.73 35.10 -2 6 -9 190.88 10.60 2 -6 9 197.28 14.00 2 -6 9 207.78 13.10 2 -6 9 207.78 12.00 -3 6 -9 112.19 6.30 -3 6 -9 112.99 6.30 3 -6 9 120.29 11.20 3 -6 9 124.99 9.20 3 -6 9 128.09 10.10 -4 6 -9 53.89 3.20 -4 6 -9 49.40 3.40 4 -6 9 57.89 8.20 4 -6 9 69.89 9.30 4 -6 9 50.29 11.50 -5 6 -9 217.88 12.00 5 -6 9 223.58 15.10 5 -6 9 241.48 15.50 5 -6 9 237.58 17.40 -6 6 -9 32.40 4.00 6 -6 9 36.40 8.10 6 -6 9 34.20 7.40 6 -6 9 27.00 10.10 -7 6 -9 474.75 26.50 7 -6 9 498.55 29.00 7 -6 9 539.75 29.40 7 -6 9 538.35 32.40 -8 6 -9 181.88 12.40 8 -6 9 189.68 16.20 8 -6 9 183.08 19.40 8 -6 9 156.28 16.30 -9 6 -9 36.40 5.50 9 -6 9 20.20 13.20 9 -6 9 26.60 10.50 9 -6 9 15.20 9.20 -10 6 -9 150.68 11.60 10 -6 9 130.39 17.20 10 -6 9 155.88 16.30 -11 6 -9 88.89 9.60 11 -6 9 62.69 11.20 11 -6 9 71.09 13.20 -12 6 -9 24.30 6.00 12 -6 9 11.20 7.60 14 5 -9 5.20 7.10 -14 -5 9 15.00 8.90 13 5 -9 -4.80 10.30 -13 -5 9 -9.40 10.00 12 5 -9 73.09 12.00 12 5 -9 35.20 10.70 -12 -5 9 30.90 15.10 11 5 -9 1.30 14.60 11 5 -9 -2.20 9.00 11 5 -9 17.40 11.70 -11 -5 9 6.70 9.00 10 5 -9 20.00 8.50 10 5 -9 30.30 6.90 10 5 -9 42.20 10.90 10 5 -9 22.30 8.40 -10 -5 9 40.80 9.30 -10 -5 9 31.30 10.00 9 5 -9 17.30 7.60 9 5 -9 24.20 8.30 9 5 -9 26.90 8.60 9 5 -9 22.20 6.20 -9 -5 9 15.80 7.10 -9 -5 9 40.90 8.90 8 5 -9 2.60 5.30 8 5 -9 19.60 7.60 8 5 -9 11.40 8.60 -8 -5 9 8.40 7.20 -8 -5 9 4.10 6.30 7 5 -9 84.89 8.50 7 5 -9 90.39 9.90 7 5 -9 87.89 10.50 -7 -5 9 80.59 9.50 -7 -5 9 76.49 9.80 6 5 -9 12.70 5.60 6 5 -9 9.30 5.40 6 5 -9 11.60 4.20 -6 -5 9 6.60 5.10 -6 -5 9 8.50 5.00 5 5 -9 155.08 11.00 5 5 -9 144.59 9.70 5 5 -9 167.28 11.30 -5 -5 9 140.49 10.50 -5 -5 9 178.38 11.90 4 5 -9 92.89 6.60 4 5 -9 96.49 7.80 4 5 -9 94.09 8.30 -4 -5 9 101.29 9.30 -4 -5 9 78.69 6.30 -4 -5 9 79.59 7.00 3 5 -9 166.88 10.40 3 5 -9 170.28 10.50 3 5 -9 169.88 9.70 -3 -5 9 174.98 9.60 -3 -5 9 177.18 11.40 -3 -5 9 156.98 9.80 2 5 -9 23.90 3.60 2 5 -9 25.40 3.60 -2 -5 9 23.70 5.10 -2 -5 9 20.70 3.00 1 5 -9 440.96 23.90 1 5 -9 475.25 23.90 1 5 -9 460.15 23.60 -1 -5 9 465.05 24.80 -1 -5 9 446.76 23.90 0 5 -9 163.78 9.10 0 5 -9 179.08 9.60 0 -5 9 177.18 11.20 0 -5 9 173.48 10.10 0 -5 9 175.28 11.70 -1 5 -9 1138.79 65.59 -1 5 -9 1302.57 65.59 1 -5 9 1293.37 66.79 1 -5 9 1352.06 66.09 1 -5 9 1369.26 66.99 -2 5 -9 96.09 5.20 -2 5 -9 93.59 5.20 2 -5 9 106.29 7.50 2 -5 9 98.59 8.60 2 -5 9 95.99 9.50 3 -5 9 38.40 5.70 3 -5 9 37.50 6.30 3 -5 9 39.20 9.30 4 -5 9 133.69 10.50 4 -5 9 144.79 12.90 4 -5 9 129.19 10.90 -5 5 -9 164.08 8.90 5 -5 9 154.18 15.20 5 -5 9 180.08 12.70 5 -5 9 171.78 12.70 -6 5 -9 335.27 18.30 -6 5 -9 345.47 18.30 6 -5 9 349.57 21.40 6 -5 9 341.47 23.30 6 -5 9 378.86 21.00 -7 5 -9 60.09 5.90 -7 5 -9 65.69 5.90 7 -5 9 72.79 11.70 7 -5 9 57.49 14.80 7 -5 9 63.09 11.60 -8 5 -9 268.07 17.20 8 -5 9 317.57 20.10 8 -5 9 302.17 24.20 8 -5 9 293.97 20.80 -9 5 -9 387.06 21.00 9 -5 9 357.56 25.20 9 -5 9 389.06 24.10 9 -5 9 365.46 27.70 -10 5 -9 45.60 6.20 10 -5 9 33.30 10.70 10 -5 9 19.80 9.10 10 -5 9 44.70 15.90 -11 5 -9 77.49 9.60 11 -5 9 96.89 15.40 11 -5 9 67.39 12.60 -12 5 -9 1.50 7.40 12 -5 9 4.40 9.90 12 -5 9 7.50 11.40 14 4 -9 0.70 8.90 -14 -4 9 7.80 10.70 13 4 -9 -0.50 10.80 -13 -4 9 2.50 10.60 12 4 -9 45.20 10.50 12 4 -9 47.30 12.30 -12 -4 9 23.80 10.40 11 4 -9 -0.50 8.80 11 4 -9 14.80 10.50 -11 -4 9 2.10 8.90 10 4 -9 17.70 8.00 10 4 -9 42.40 9.60 10 4 -9 29.20 6.60 10 4 -9 38.40 9.90 -10 -4 9 23.80 9.40 -10 -4 9 24.60 8.20 9 4 -9 6.80 5.70 9 4 -9 18.80 8.50 9 4 -9 27.80 8.60 -9 -4 9 26.70 8.20 -9 -4 9 13.30 12.10 8 4 -9 28.60 7.50 8 4 -9 16.80 5.30 8 4 -9 33.60 8.00 -8 -4 9 26.00 6.90 -8 -4 9 28.50 7.20 7 4 -9 126.59 9.80 7 4 -9 132.09 11.90 -7 -4 9 133.39 10.90 -7 -4 9 132.29 10.80 6 4 -9 14.40 5.30 6 4 -9 12.10 5.70 6 4 -9 13.90 4.10 -6 -4 9 14.40 5.10 -6 -4 9 17.80 5.30 5 4 -9 99.89 7.20 5 4 -9 95.59 8.40 5 4 -9 93.49 8.40 -5 -4 9 104.09 8.00 -5 -4 9 77.69 9.40 4 4 -9 230.88 14.00 4 4 -9 251.87 14.10 4 4 -9 254.87 13.30 -4 -4 9 233.98 14.90 -4 -4 9 225.38 13.30 -4 -4 9 249.88 13.60 3 4 -9 14.60 3.40 3 4 -9 16.00 2.70 3 4 -9 13.70 3.60 -3 -4 9 11.60 3.20 -3 -4 9 13.10 2.70 -3 -4 9 8.40 4.80 2 4 -9 1147.99 58.19 2 4 -9 1103.69 58.19 2 4 -9 1133.09 57.89 -2 -4 9 1206.28 58.69 -2 -4 9 1089.29 58.29 1 4 -9 44.50 4.00 1 4 -9 42.00 3.20 1 4 -9 40.40 5.20 -1 -4 9 39.70 5.80 -1 -4 9 31.70 4.50 0 4 -9 333.37 18.10 0 4 -9 371.66 18.50 0 -4 9 352.96 19.40 0 -4 9 372.46 19.80 0 -4 9 347.37 18.90 -1 4 -9 60.49 3.60 -1 4 -9 56.49 3.90 1 -4 9 46.90 6.40 1 -4 9 61.19 5.80 1 -4 9 62.69 7.40 2 -4 9 31.40 5.80 2 -4 9 32.90 7.40 2 -4 9 28.40 5.70 3 -4 9 86.59 8.00 3 -4 9 86.39 7.40 3 -4 9 87.09 9.10 4 -4 9 501.75 27.10 4 -4 9 482.65 27.00 4 -4 9 510.85 28.40 -5 4 -9 179.38 9.70 -5 4 -9 171.88 9.50 5 -4 9 183.58 12.70 5 -4 9 194.08 12.50 5 -4 9 181.18 20.20 -6 4 -9 115.79 7.20 -6 4 -9 112.89 7.30 6 -4 9 126.19 11.50 6 -4 9 117.89 12.20 6 -4 9 134.29 15.30 -7 4 -9 13.70 3.70 -7 4 -9 21.30 3.60 7 -4 9 9.10 7.90 7 -4 9 20.30 10.70 7 -4 9 15.80 7.10 -8 4 -9 461.55 26.40 8 -4 9 472.25 31.90 8 -4 9 518.75 29.60 8 -4 9 553.94 29.10 9 -4 9 60.29 9.70 9 -4 9 54.09 13.10 9 -4 9 75.99 15.20 -10 4 -9 67.49 8.90 10 -4 9 44.80 10.90 10 -4 9 53.89 15.60 10 -4 9 64.39 10.00 -11 4 -9 15.40 6.00 11 -4 9 12.40 8.20 11 -4 9 4.10 10.40 -12 4 -9 92.59 13.20 12 -4 9 66.29 12.60 14 3 -9 9.30 9.20 -14 -3 9 -11.40 13.20 13 3 -9 -14.50 10.90 -13 -3 9 5.30 10.70 12 3 -9 -1.70 16.80 12 3 -9 13.90 8.70 -12 -3 9 1.00 8.50 -12 -3 9 26.90 16.20 11 3 -9 3.10 10.40 11 3 -9 17.40 11.50 10 3 -9 0.20 7.10 10 3 -9 8.00 9.40 10 3 -9 9.80 9.10 10 3 -9 16.00 6.20 -10 -3 9 16.60 8.60 9 3 -9 4.70 7.50 9 3 -9 2.00 6.00 9 3 -9 10.50 7.60 9 3 -9 10.20 5.50 -9 -3 9 -1.50 7.40 8 3 -9 67.19 7.90 8 3 -9 52.29 8.20 8 3 -9 69.19 10.50 8 3 -9 63.09 9.60 -8 -3 9 56.39 10.10 -8 -3 9 67.49 9.10 7 3 -9 233.98 15.00 7 3 -9 205.08 13.10 7 3 -9 226.48 14.30 -7 -3 9 209.08 14.40 6 3 -9 99.49 10.90 6 3 -9 130.39 10.40 6 3 -9 125.99 10.20 -6 -3 9 128.69 9.70 5 3 -9 56.19 5.50 5 3 -9 58.79 6.30 5 3 -9 57.99 7.00 -5 -3 9 50.79 7.80 -5 -3 9 47.20 6.50 -5 -3 9 48.40 6.20 4 3 -9 1280.67 67.19 4 3 -9 1267.17 67.19 4 3 -9 1340.07 66.79 -4 -3 9 1340.47 67.69 -4 -3 9 1345.97 66.99 -4 -3 9 1273.47 66.89 3 3 -9 464.15 24.90 3 3 -9 463.15 24.90 3 3 -9 464.55 24.50 -3 -3 9 473.35 24.80 -3 -3 9 497.95 25.60 -3 -3 9 478.55 24.60 2 3 -9 634.74 32.70 2 3 -9 604.54 32.40 -2 -3 9 694.23 33.30 -2 -3 9 599.24 32.70 1 3 -9 1492.75 72.29 1 3 -9 1404.86 71.99 -1 -3 9 1381.86 72.39 -1 -3 9 1392.16 72.69 0 3 -9 335.47 18.60 0 3 -9 384.56 18.60 0 3 -9 335.07 18.30 0 -3 9 350.46 19.10 0 -3 9 406.16 19.60 0 -3 9 353.46 19.70 -1 3 -9 657.63 34.70 -1 3 -9 648.04 34.70 1 -3 9 684.93 35.40 1 -3 9 719.93 36.00 1 -3 9 702.83 35.60 2 -3 9 567.44 30.40 2 -3 9 594.74 31.20 2 -3 9 571.24 30.50 3 -3 9 16.60 4.50 3 -3 9 26.20 6.10 3 -3 9 12.90 4.40 -4 3 -9 10.20 2.00 4 -3 9 12.50 4.60 4 -3 9 10.90 4.90 4 -3 9 12.10 6.80 -5 3 -9 8.40 1.80 -5 3 -9 11.10 2.30 5 -3 9 10.10 7.80 5 -3 9 11.80 5.40 5 -3 9 6.60 5.70 -6 3 -9 332.17 17.90 -6 3 -9 312.77 17.60 6 -3 9 334.27 20.50 6 -3 9 362.16 20.00 6 -3 9 350.46 23.10 -7 3 -9 141.09 8.90 -7 3 -9 129.19 11.10 7 -3 9 151.68 14.20 7 -3 9 147.29 13.50 7 -3 9 144.49 17.20 -8 3 -9 317.87 18.60 8 -3 9 358.36 21.20 8 -3 9 340.37 22.90 8 -3 9 328.27 25.70 -9 3 -9 31.30 7.00 -9 3 -9 41.80 5.60 9 -3 9 23.70 12.30 9 -3 9 34.40 8.50 9 -3 9 34.00 10.10 10 -3 9 29.90 10.50 10 -3 9 39.30 14.50 10 -3 9 34.30 8.30 -11 3 -9 49.20 6.70 11 -3 9 47.90 10.40 -12 3 -9 119.79 13.40 12 -3 9 103.39 17.40 14 2 -9 4.10 11.70 -14 -2 9 44.50 11.00 13 2 -9 10.20 10.50 13 2 -9 28.80 11.20 -13 -2 9 31.20 10.20 -13 -2 9 20.50 11.10 12 2 -9 13.00 9.50 12 2 -9 23.30 11.70 -12 -2 9 23.60 9.70 -12 -2 9 23.20 10.80 11 2 -9 47.00 10.30 11 2 -9 43.40 11.10 -11 -2 9 39.50 9.90 -11 -2 9 30.20 10.60 10 2 -9 29.70 8.80 10 2 -9 31.10 9.90 10 2 -9 21.20 6.40 -10 -2 9 33.00 8.50 9 2 -9 111.49 9.80 9 2 -9 131.19 12.70 9 2 -9 120.69 14.30 9 2 -9 89.99 10.00 -9 -2 9 123.09 12.60 8 2 -9 33.30 7.40 8 2 -9 25.80 6.70 8 2 -9 20.60 4.80 8 2 -9 23.10 5.00 -8 -2 9 14.30 6.10 7 2 -9 30.20 6.30 7 2 -9 23.90 6.00 7 2 -9 28.70 4.50 -7 -2 9 30.20 5.70 6 2 -9 105.09 8.40 6 2 -9 102.19 9.00 6 2 -9 102.79 7.40 -6 -2 9 107.39 8.70 -6 -2 9 91.79 8.70 5 2 -9 985.30 51.59 5 2 -9 1000.90 52.19 -5 -2 9 1002.80 51.79 -5 -2 9 1033.40 51.99 4 2 -9 3033.30 159.48 4 2 -9 3165.88 159.18 4 2 -9 3074.79 159.48 -4 -2 9 3217.48 159.78 -4 -2 9 3178.98 159.38 3 2 -9 1567.44 78.49 3 2 -9 1533.85 78.19 -3 -2 9 1496.35 78.69 -3 -2 9 1528.85 78.79 -3 -2 9 1554.34 78.29 2 2 -9 8.10 1.80 2 2 -9 6.70 2.60 -2 -2 9 5.50 3.00 -2 -2 9 7.90 3.80 1 2 -9 84.49 4.80 1 2 -9 81.49 5.30 -1 -2 9 76.29 6.90 -1 -2 9 85.99 6.50 0 2 -9 1072.89 61.69 0 2 -9 1192.78 61.49 0 2 -9 1246.08 61.69 0 -2 9 1236.48 62.29 0 -2 9 1248.18 62.19 0 -2 9 1285.37 62.39 -1 2 -9 1231.78 61.99 -1 2 -9 1127.89 61.99 1 -2 9 1251.57 62.59 1 -2 9 1200.18 62.59 1 -2 9 1288.47 63.39 -2 2 -9 369.66 18.50 -2 2 -9 341.47 18.50 2 -2 9 371.26 19.80 2 -2 9 365.06 19.60 2 -2 9 360.66 20.40 -3 2 -9 9.90 1.50 -3 2 -9 12.90 2.10 3 -2 9 11.30 4.50 3 -2 9 12.30 5.40 3 -2 9 13.10 3.90 -4 2 -9 6.30 1.30 4 -2 9 6.70 6.90 4 -2 9 6.70 4.80 4 -2 9 2.40 4.60 -5 2 -9 347.57 19.40 5 -2 9 377.66 21.90 5 -2 9 392.46 21.10 5 -2 9 397.96 23.60 -6 2 -9 174.28 9.80 -6 2 -9 170.18 10.40 6 -2 9 180.68 16.60 6 -2 9 169.38 12.50 6 -2 9 170.48 13.90 -7 2 -9 43.70 7.70 -7 2 -9 52.69 5.80 -7 2 -9 53.29 6.60 7 -2 9 65.19 12.20 7 -2 9 58.99 9.90 7 -2 9 67.19 12.80 -8 2 -9 44.70 7.20 -8 2 -9 52.69 8.40 -8 2 -9 54.29 7.60 8 -2 9 52.79 10.80 8 -2 9 72.09 13.30 8 -2 9 63.99 10.20 -9 2 -9 49.70 8.10 -9 2 -9 43.70 8.00 -9 2 -9 45.40 8.30 9 -2 9 46.60 10.50 9 -2 9 43.40 8.30 9 -2 9 31.20 12.40 -10 2 -9 58.09 11.40 -10 2 -9 72.29 9.30 10 -2 9 83.39 15.60 -11 2 -9 38.60 6.50 11 -2 9 47.40 11.10 -12 2 -9 11.50 5.90 12 -2 9 12.40 11.80 -15 -1 9 32.10 11.70 14 1 -9 137.69 16.40 -14 -1 9 162.88 16.60 13 1 -9 7.00 9.20 13 1 -9 24.50 11.20 -13 -1 9 0.60 10.80 -13 -1 9 -1.30 9.40 12 1 -9 15.50 11.70 12 1 -9 16.40 9.60 -12 -1 9 -6.50 8.70 -12 -1 9 9.10 10.80 11 1 -9 50.69 10.20 11 1 -9 50.69 11.00 -11 -1 9 56.79 10.30 -11 -1 9 41.70 10.50 10 1 -9 224.48 17.10 10 1 -9 191.28 14.00 10 1 -9 214.08 16.70 -10 -1 9 209.88 16.80 -10 -1 9 192.88 16.60 9 1 -9 82.69 11.00 9 1 -9 109.49 9.50 9 1 -9 111.19 12.80 -9 -1 9 104.79 12.30 -9 -1 9 121.59 12.70 8 1 -9 1.10 3.60 8 1 -9 2.90 4.50 8 1 -9 7.50 6.90 8 1 -9 1.80 7.80 -8 -1 9 9.40 6.70 -8 -1 9 12.30 6.40 7 1 -9 5.00 4.00 7 1 -9 3.10 5.40 7 1 -9 5.10 3.10 7 1 -9 1.50 5.70 -7 -1 9 3.30 5.60 -7 -1 9 1.80 5.10 6 1 -9 115.29 9.30 6 1 -9 121.39 7.90 6 1 -9 116.29 9.30 6 1 -9 95.99 7.00 -6 -1 9 124.79 9.20 -6 -1 9 122.69 8.90 5 1 -9 453.25 23.30 5 1 -9 421.66 23.00 5 1 -9 419.86 22.30 -5 -1 9 420.06 22.90 -5 -1 9 409.26 22.70 4 1 -9 3413.76 177.28 4 1 -9 3343.37 177.28 4 1 -9 3537.65 176.98 -4 -1 9 3541.55 177.18 -4 -1 9 3594.94 177.58 3 1 -9 115.89 7.40 3 1 -9 119.09 6.70 -3 -1 9 111.29 6.90 -3 -1 9 119.99 8.60 -3 -1 9 102.99 7.50 2 1 -9 576.24 31.40 2 1 -9 615.74 31.10 2 1 -9 626.34 32.50 -2 -1 9 617.24 31.80 -2 -1 9 601.74 31.60 1 1 -9 70.29 4.60 1 1 -9 65.69 4.10 -1 -1 9 58.49 5.40 -1 -1 9 60.49 5.80 -1 -1 9 73.99 5.90 0 1 -9 143.89 7.70 0 1 -9 133.79 7.30 0 -1 9 140.69 9.00 0 -1 9 145.99 8.90 0 -1 9 129.09 8.80 -1 1 -9 375.86 18.60 -1 1 -9 343.97 18.60 1 -1 9 361.76 19.50 1 -1 9 352.76 19.70 1 -1 9 359.86 19.30 -2 1 -9 227.28 12.20 2 -1 9 228.88 15.70 2 -1 9 245.38 14.40 2 -1 9 228.98 13.20 -3 1 -9 61.69 4.20 -3 1 -9 58.39 3.60 3 -1 9 69.99 8.90 3 -1 9 67.99 7.20 3 -1 9 68.59 6.30 -4 1 -9 46.40 3.60 -4 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50.49 9.00 6 -9 10 35.40 12.20 6 -9 10 42.00 9.90 -7 9 -10 104.49 8.60 7 -9 10 111.49 16.40 7 -9 10 104.89 19.50 7 -9 10 95.19 13.90 -8 9 -10 462.25 24.30 8 -9 10 401.56 31.10 8 -9 10 417.76 27.40 8 -9 10 515.45 29.10 -9 9 -10 347.97 19.80 9 -9 10 357.76 23.80 9 -9 10 292.97 31.50 -10 9 -10 43.80 6.30 10 -9 10 47.90 10.30 10 -9 10 58.89 11.30 -11 9 -10 51.79 6.40 11 -9 10 75.09 10.50 12 8 -10 -0.40 11.10 -12 -8 10 4.90 12.10 11 8 -10 96.89 16.80 11 8 -10 71.59 14.10 10 8 -10 3.00 9.50 10 8 -10 28.20 19.40 10 8 -10 4.20 9.80 10 8 -10 1.00 7.30 9 8 -10 2.30 9.90 9 8 -10 -6.00 7.00 9 8 -10 10.20 8.70 -9 -8 10 6.00 9.60 -9 -8 10 0.30 8.60 8 8 -10 62.39 11.50 8 8 -10 74.59 13.20 -8 -8 10 70.29 12.50 -8 -8 10 62.79 12.00 7 8 -10 3.50 8.70 7 8 -10 13.30 6.80 7 8 -10 11.70 8.00 -7 -8 10 -2.70 7.40 -7 -8 10 14.80 7.00 6 8 -10 49.80 6.60 6 8 -10 46.90 8.30 6 8 -10 45.40 8.60 -6 -8 10 30.70 8.00 -6 -8 10 30.20 6.60 5 8 -10 18.00 7.30 5 8 -10 23.20 5.70 5 8 -10 14.80 6.70 -5 -8 10 18.70 7.40 4 8 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7 -8 10 3.30 9.30 7 -8 10 9.90 16.20 -8 8 -10 53.39 7.50 8 -8 10 75.49 14.80 8 -8 10 74.19 14.60 8 -8 10 43.80 10.50 -9 8 -10 13.30 5.10 9 -8 10 7.90 10.10 9 -8 10 19.40 10.40 9 -8 10 -1.30 13.40 -10 8 -10 129.79 10.60 10 -8 10 135.89 16.60 10 -8 10 127.49 15.60 11 -8 10 60.89 10.80 13 7 -10 26.20 10.10 -13 -7 10 13.20 9.40 12 7 -10 2.90 11.30 -12 -7 10 -15.70 10.00 11 7 -10 15.30 11.60 11 7 -10 -3.00 16.40 10 7 -10 30.40 10.00 10 7 -10 80.79 15.70 10 7 -10 60.49 10.80 10 7 -10 52.99 7.80 -10 -7 10 43.40 9.20 9 7 -10 20.60 13.30 9 7 -10 57.49 8.00 9 7 -10 54.09 10.30 -9 -7 10 30.00 8.50 8 7 -10 12.30 6.90 8 7 -10 16.50 9.70 8 7 -10 5.80 7.80 -8 -7 10 -3.40 6.60 7 7 -10 133.99 10.50 7 7 -10 117.19 12.30 7 7 -10 100.39 12.20 -7 -7 10 88.89 11.50 -7 -7 10 110.49 11.40 6 7 -10 10.90 6.50 6 7 -10 12.20 7.20 6 7 -10 9.20 5.40 -6 -7 10 4.00 5.70 5 7 -10 406.16 24.20 5 7 -10 423.16 24.10 5 7 -10 451.05 23.10 -5 -7 10 412.86 24.60 -5 -7 10 419.06 23.30 4 7 -10 98.29 7.90 4 7 -10 89.29 9.50 4 7 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11.60 -9 7 -10 127.39 10.50 9 -7 10 153.18 20.10 9 -7 10 117.79 20.40 9 -7 10 173.68 19.30 -10 7 -10 247.48 14.90 10 -7 10 215.28 25.80 10 -7 10 229.38 18.70 10 -7 10 234.48 19.70 11 -7 10 80.19 14.00 11 -7 10 86.09 14.60 13 6 -10 6.90 12.40 -13 -6 10 2.80 10.90 12 6 -10 -8.40 11.10 -12 -6 10 -0.60 10.70 11 6 -10 13.60 9.00 -11 -6 10 -7.80 9.00 10 6 -10 25.60 7.10 10 6 -10 41.10 9.90 10 6 -10 30.70 10.80 -10 -6 10 22.80 16.60 9 6 -10 58.79 10.00 9 6 -10 82.29 14.60 9 6 -10 65.09 9.90 -9 -6 10 35.20 8.20 8 6 -10 50.59 9.00 8 6 -10 54.69 9.00 8 6 -10 47.60 8.90 -8 -6 10 49.80 8.60 -8 -6 10 18.00 6.80 7 6 -10 63.79 11.00 7 6 -10 59.59 8.60 -7 -6 10 50.19 7.40 6 6 -10 294.77 17.70 6 6 -10 282.07 16.00 6 6 -10 280.07 17.30 -6 -6 10 240.98 16.60 5 6 -10 117.09 10.40 5 6 -10 120.19 10.80 5 6 -10 123.59 8.90 -5 -6 10 118.99 11.30 -5 -6 10 118.29 9.50 4 6 -10 83.29 8.40 4 6 -10 85.29 7.10 4 6 -10 87.99 8.30 -4 -6 10 77.59 7.40 -4 -6 10 91.59 9.70 3 6 -10 101.29 7.90 3 6 -10 101.49 8.00 3 6 -10 100.39 7.40 -3 -6 10 85.39 6.70 -3 -6 10 91.79 9.70 2 6 -10 278.97 15.20 2 6 -10 280.67 14.60 2 6 -10 257.57 15.00 -2 -6 10 277.57 16.40 -2 -6 10 254.27 14.70 1 6 -10 56.69 5.50 1 6 -10 59.19 5.40 1 6 -10 50.79 4.60 -1 -6 10 66.59 8.50 -1 -6 10 48.30 5.60 0 6 -10 645.04 34.80 0 6 -10 680.23 35.10 0 -6 10 722.73 36.20 0 -6 10 677.43 35.30 -1 6 -10 163.08 8.90 1 -6 10 162.78 12.80 1 -6 10 172.48 12.30 1 -6 10 181.88 10.60 -2 6 -10 10.00 1.60 2 -6 10 10.90 4.80 2 -6 10 13.10 6.60 2 -6 10 4.50 5.80 3 -6 10 120.79 12.20 3 -6 10 122.99 9.70 3 -6 10 115.29 11.40 -4 6 -10 1151.08 60.69 4 -6 10 1237.68 62.59 4 -6 10 1186.58 62.09 4 -6 10 1218.58 63.79 5 -6 10 28.80 9.80 5 -6 10 28.50 7.40 5 -6 10 39.60 7.80 6 -6 10 29.60 8.80 6 -6 10 24.90 11.20 6 -6 10 29.60 8.40 7 -6 10 70.69 16.20 7 -6 10 64.89 13.20 7 -6 10 72.89 13.40 -8 6 -10 55.09 7.00 8 -6 10 64.69 10.70 8 -6 10 50.09 13.80 8 -6 10 44.90 9.90 -9 6 -10 296.67 17.00 9 -6 10 337.07 28.40 9 -6 10 312.67 27.50 9 -6 10 259.77 24.10 -10 6 -10 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5.70 -4 -5 10 -0.70 3.10 -4 -5 10 1.70 5.20 3 5 -10 1.00 2.80 3 5 -10 6.20 3.60 3 5 -10 -2.20 3.70 -3 -5 10 3.80 5.60 -3 -5 10 0.80 3.00 2 5 -10 1146.09 59.69 2 5 -10 1173.78 59.59 2 5 -10 1179.98 59.29 -2 -5 10 1111.69 59.49 -2 -5 10 1200.08 60.29 1 5 -10 225.68 13.50 1 5 -10 245.48 12.90 1 5 -10 247.68 13.30 -1 -5 10 252.77 14.70 0 5 -10 494.55 26.20 0 5 -10 453.65 24.90 0 5 -10 544.85 26.00 0 -5 10 473.65 26.50 0 -5 10 479.65 25.70 0 -5 10 477.35 26.80 -1 5 -10 177.68 9.80 1 -5 10 187.68 13.00 1 -5 10 187.98 12.30 1 -5 10 184.68 11.30 2 -5 10 12.90 5.40 2 -5 10 2.50 4.30 2 -5 10 16.30 6.10 3 -5 10 19.10 6.90 3 -5 10 7.80 5.00 3 -5 10 12.10 5.70 4 -5 10 92.39 12.90 4 -5 10 110.99 10.70 4 -5 10 107.89 10.20 5 -5 10 1113.69 58.39 5 -5 10 1098.19 58.29 5 -5 10 1127.19 59.89 -6 5 -10 71.89 5.30 6 -5 10 64.59 12.00 6 -5 10 70.19 10.00 6 -5 10 55.99 11.60 -7 5 -10 59.39 6.10 7 -5 10 70.79 13.20 7 -5 10 78.39 13.40 7 -5 10 66.59 12.90 8 -5 10 44.30 9.70 8 -5 10 39.80 12.40 8 -5 10 41.60 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17.40 6 -8 12 158.08 20.90 6 -8 12 161.88 15.90 -7 8 -12 58.49 6.50 7 -8 12 51.29 11.50 7 -8 12 53.19 10.90 7 -8 12 41.30 13.70 8 -8 12 470.05 28.70 8 -8 12 452.15 27.70 8 -8 12 380.56 42.00 -9 8 -12 193.88 12.00 9 -8 12 194.68 17.60 9 -8 12 194.28 17.90 10 -8 12 66.29 13.10 10 -8 12 39.40 10.80 12 7 -12 41.60 11.60 11 7 -12 36.50 11.30 11 7 -12 30.40 9.30 10 7 -12 0.70 8.60 10 7 -12 -11.90 18.20 10 7 -12 -1.30 7.40 9 7 -12 5.80 8.60 9 7 -12 15.30 7.40 9 7 -12 15.10 11.10 8 7 -12 40.90 7.60 8 7 -12 46.70 10.20 8 7 -12 64.19 11.60 7 7 -12 42.60 9.80 7 7 -12 25.10 7.80 7 7 -12 42.90 7.30 6 7 -12 14.60 7.00 6 7 -12 5.80 7.80 6 7 -12 5.50 6.00 5 7 -12 -2.00 6.90 5 7 -12 0.80 4.90 5 7 -12 -10.10 5.90 -5 -7 12 7.70 8.80 4 7 -12 4.60 4.70 4 7 -12 0.40 5.40 4 7 -12 9.40 6.10 -4 -7 12 1.60 7.70 3 7 -12 280.17 16.00 3 7 -12 265.47 16.70 -3 -7 12 308.17 19.20 2 7 -12 188.88 13.10 2 7 -12 213.28 12.20 2 7 -12 215.58 12.90 -2 -7 12 206.48 15.90 1 7 -12 157.08 9.60 1 7 -12 161.28 10.10 1 7 -12 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16.10 5 5 -13 53.09 9.30 5 5 -13 53.29 7.50 5 5 -13 45.20 7.70 -5 -5 13 51.99 7.80 4 5 -13 9.40 5.90 4 5 -13 12.10 5.30 4 5 -13 2.80 4.00 -4 -5 13 6.50 7.70 -4 -5 13 0.90 4.80 3 5 -13 2.40 5.10 3 5 -13 8.50 4.50 3 5 -13 1.80 3.60 -3 -5 13 9.60 7.70 -3 -5 13 -1.30 4.70 2 5 -13 48.00 6.40 2 5 -13 31.20 5.20 2 5 -13 32.80 6.70 -2 -5 13 42.40 8.10 -2 -5 13 40.10 7.10 1 5 -13 448.96 23.80 1 5 -13 448.76 24.10 1 5 -13 450.15 23.50 -1 -5 13 436.36 24.70 -1 -5 13 468.35 26.10 0 5 -13 16.40 2.70 0 5 -13 14.20 2.80 0 -5 13 13.90 7.30 0 -5 13 12.10 5.60 1 -5 13 153.88 12.70 1 -5 13 134.79 11.50 1 -5 13 137.59 13.70 2 -5 13 197.18 17.10 2 -5 13 197.78 16.20 2 -5 13 220.58 15.00 3 -5 13 163.38 14.40 3 -5 13 162.38 17.70 3 -5 13 158.08 15.70 4 -5 13 525.35 29.80 4 -5 13 511.65 29.70 4 -5 13 500.65 31.30 -5 5 -13 118.69 6.90 5 -5 13 118.39 14.80 5 -5 13 139.59 14.70 5 -5 13 91.29 17.20 6 -5 13 82.19 15.20 6 -5 13 96.69 17.70 6 -5 13 91.89 14.40 7 -5 13 9.30 11.80 7 -5 13 5.50 13.20 7 -5 13 6.00 11.80 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13 -14 20.40 7.10 -2 -13 14 14.60 13.30 1 13 -14 -1.40 6.30 1 13 -14 11.60 13.30 1 13 -14 19.80 7.30 -1 -13 14 10.20 13.10 0 13 -14 8.20 5.70 0 13 -14 11.30 6.60 0 -13 14 25.50 14.00 -1 13 -14 39.40 7.00 1 -13 14 18.40 14.70 -2 13 -14 32.60 6.30 2 -13 14 29.60 12.50 -3 13 -14 30.90 9.20 3 -13 14 22.60 12.00 -4 13 -14 17.90 5.30 4 -13 14 2.40 12.40 -5 13 -14 6.30 4.80 5 -13 14 10.10 12.10 6 -13 14 6.90 11.40 7 -13 14 2.20 12.20 9 12 -14 15.70 12.40 9 12 -14 -2.40 14.00 8 12 -14 2.60 7.00 8 12 -14 21.60 11.50 7 12 -14 7.70 11.70 7 12 -14 9.50 8.30 6 12 -14 8.50 11.40 6 12 -14 10.10 9.10 6 12 -14 8.80 8.20 5 12 -14 2.60 7.80 5 12 -14 8.30 11.80 5 12 -14 7.00 7.80 -5 -12 14 5.40 11.30 4 12 -14 26.70 10.70 4 12 -14 41.20 8.60 4 12 -14 34.00 8.10 -4 -12 14 24.60 11.30 3 12 -14 3.10 7.40 3 12 -14 -4.60 9.20 3 12 -14 -3.30 7.00 -3 -12 14 -2.80 10.50 2 12 -14 16.30 8.90 2 12 -14 6.70 7.20 2 12 -14 10.30 6.70 -2 -12 14 19.00 11.90 1 12 -14 93.49 13.60 1 12 -14 112.99 11.00 1 12 -14 115.59 11.30 -1 -12 14 91.19 17.00 0 12 -14 3.40 7.50 0 12 -14 0.00 6.10 0 12 -14 4.50 5.30 0 -12 14 6.70 11.80 -1 12 -14 50.89 6.70 1 -12 14 45.90 12.60 -2 12 -14 -1.70 5.30 2 -12 14 -0.60 12.00 -3 12 -14 6.10 5.10 3 -12 14 -0.10 19.70 -4 12 -14 239.88 15.30 4 -12 14 264.27 23.10 -5 12 -14 58.09 7.40 5 -12 14 78.99 14.20 -6 12 -14 -9.50 6.50 6 -12 14 1.80 11.60 7 -12 14 4.80 10.90 10 11 -14 29.90 16.70 9 11 -14 -4.00 8.90 9 11 -14 -3.00 11.00 8 11 -14 10.40 11.60 8 11 -14 -0.80 7.70 7 11 -14 184.08 18.70 7 11 -14 125.69 13.40 7 11 -14 78.59 15.20 6 11 -14 24.60 16.10 6 11 -14 13.50 8.40 6 11 -14 25.10 7.90 5 11 -14 11.50 10.50 5 11 -14 12.10 7.50 5 11 -14 20.70 7.90 -5 -11 14 12.80 11.30 4 11 -14 10.50 9.50 4 11 -14 1.80 7.10 4 11 -14 2.70 6.80 -4 -11 14 3.70 10.90 3 11 -14 50.89 7.70 3 11 -14 53.09 10.70 3 11 -14 60.19 9.70 -3 -11 14 45.00 11.30 2 11 -14 136.59 13.70 2 11 -14 134.99 12.10 -2 -11 14 134.59 18.10 1 11 -14 57.29 9.10 1 11 -14 34.90 6.50 1 11 -14 55.69 11.00 -1 -11 14 36.70 11.50 0 11 -14 1.90 4.70 0 11 -14 9.30 5.50 0 11 -14 -3.40 6.50 0 -11 14 3.50 11.20 -1 11 -14 2.50 5.20 1 -11 14 -4.50 11.20 -2 11 -14 15.70 5.00 2 -11 14 18.30 11.70 -3 11 -14 19.40 4.80 3 -11 14 27.70 12.20 -4 11 -14 223.98 13.40 5 -11 14 17.30 12.50 -6 11 -14 6.10 3.90 6 -11 14 6.10 12.40 7 -11 14 6.40 11.50 8 -11 14 71.79 14.40 10 10 -14 0.50 10.70 10 10 -14 7.40 7.20 9 10 -14 1.40 7.20 9 10 -14 -2.50 11.80 8 10 -14 17.30 10.40 8 10 -14 10.30 11.90 8 10 -14 44.10 13.70 7 10 -14 166.28 16.30 7 10 -14 181.78 15.00 6 10 -14 8.10 10.40 6 10 -14 -1.10 8.10 6 10 -14 6.90 7.70 5 10 -14 6.50 7.90 5 10 -14 11.80 9.90 5 10 -14 10.90 7.40 -5 -10 14 6.40 10.40 4 10 -14 18.90 11.10 4 10 -14 22.90 9.30 4 10 -14 40.20 7.30 -4 -10 14 19.50 10.60 3 10 -14 120.89 12.60 3 10 -14 136.39 11.10 3 10 -14 95.29 11.50 -3 -10 14 97.09 16.20 2 10 -14 26.70 7.70 2 10 -14 22.50 6.00 2 10 -14 38.20 6.40 -2 -10 14 26.30 10.90 1 10 -14 87.99 10.90 1 10 -14 99.69 10.50 1 10 -14 88.49 9.30 -1 -10 14 95.69 16.60 0 10 -14 5.50 4.40 0 10 -14 4.50 6.20 0 10 -14 2.10 5.80 0 -10 14 3.00 11.00 -1 10 -14 111.09 9.30 1 -10 14 127.49 16.10 -2 10 -14 233.28 13.80 2 -10 14 237.08 20.10 -3 10 -14 54.69 6.50 3 -10 14 29.70 12.20 -4 10 -14 32.00 4.20 4 -10 14 17.50 11.90 4 -10 14 14.40 5.90 -5 10 -14 37.30 4.20 5 -10 14 20.60 8.40 5 -10 14 34.10 12.20 -6 10 -14 0.40 4.20 6 -10 14 -0.20 8.00 6 -10 14 -3.20 11.80 7 -10 14 101.29 16.90 7 -10 14 96.59 13.30 8 -10 14 106.39 15.80 8 -10 14 108.39 13.30 11 9 -14 16.00 14.30 10 9 -14 13.80 11.20 10 9 -14 12.90 7.10 9 9 -14 9.60 7.60 9 9 -14 -6.10 10.90 9 9 -14 -0.30 7.90 8 9 -14 42.70 8.10 8 9 -14 54.79 10.10 8 9 -14 34.10 11.40 7 9 -14 86.39 16.20 7 9 -14 91.79 12.50 7 9 -14 84.69 13.80 6 9 -14 9.10 7.00 6 9 -14 10.70 9.80 6 9 -14 12.50 8.30 5 9 -14 110.29 13.90 5 9 -14 133.19 12.20 5 9 -14 125.69 14.70 -5 -9 14 113.59 16.90 4 9 -14 16.70 6.90 4 9 -14 23.70 6.30 4 9 -14 21.20 8.50 -4 -9 14 23.60 10.40 3 9 -14 33.60 7.90 3 9 -14 36.00 6.70 -3 -9 14 38.70 10.70 2 9 -14 24.50 5.60 2 9 -14 26.50 5.70 2 9 -14 22.00 6.80 -2 -9 14 20.40 10.30 1 9 -14 136.89 12.00 1 9 -14 130.29 10.10 1 9 -14 127.19 10.20 -1 -9 14 159.98 16.10 0 9 -14 18.70 4.50 0 9 -14 17.40 4.10 0 9 -14 7.60 8.10 0 -9 14 30.20 10.30 -1 9 -14 9.40 4.10 1 -9 14 15.40 10.50 -2 9 -14 30.20 5.00 2 -9 14 72.89 9.30 2 -9 14 24.10 11.30 -3 9 -14 37.10 4.40 3 -9 14 16.00 7.60 3 -9 14 45.10 11.90 -4 9 -14 63.19 5.80 4 -9 14 69.89 12.90 4 -9 14 61.39 11.50 -5 9 -14 62.39 5.50 5 -9 14 45.60 10.20 5 -9 14 70.49 13.20 6 -9 14 13.20 9.30 6 -9 14 21.40 18.80 6 -9 14 19.30 12.20 7 -9 14 53.59 12.40 7 -9 14 40.50 10.00 8 -9 14 18.30 13.50 8 -9 14 8.80 10.50 11 8 -14 18.20 11.40 11 8 -14 -1.20 11.80 10 8 -14 15.30 11.50 10 8 -14 9.60 7.00 9 8 -14 -1.00 10.00 9 8 -14 13.90 11.10 9 8 -14 4.70 7.20 8 8 -14 -11.50 10.60 8 8 -14 10.00 7.60 8 8 -14 -1.00 9.20 7 8 -14 52.59 9.80 7 8 -14 61.89 8.60 7 8 -14 59.69 11.60 6 8 -14 21.30 11.40 6 8 -14 8.40 6.60 6 8 -14 0.60 9.30 5 8 -14 8.90 8.50 5 8 -14 3.70 7.00 5 8 -14 8.90 6.00 -5 -8 14 11.30 9.70 4 8 -14 4.20 5.70 4 8 -14 5.90 6.20 4 8 -14 -0.90 7.50 -4 -8 14 2.70 9.30 3 8 -14 2.80 7.20 3 8 -14 -1.00 5.30 3 8 -14 2.00 5.20 -3 -8 14 -2.10 9.60 2 8 -14 6.60 4.70 2 8 -14 5.10 6.10 2 8 -14 5.60 4.80 -2 -8 14 1.60 9.40 1 8 -14 11.90 4.40 1 8 -14 18.30 4.40 1 8 -14 9.10 5.60 -1 -8 14 7.20 9.60 0 8 -14 10.20 5.40 0 8 -14 4.30 3.70 0 -8 14 3.70 5.60 0 -8 14 8.20 9.60 -1 8 -14 427.76 22.50 1 -8 14 412.36 24.00 1 -8 14 436.36 27.00 -2 8 -14 30.80 3.80 2 -8 14 39.40 7.70 2 -8 14 37.30 10.70 -3 8 -14 11.70 2.90 3 -8 14 19.30 11.00 3 -8 14 8.50 7.50 -4 8 -14 81.59 6.00 4 -8 14 77.99 12.70 4 -8 14 62.89 12.90 4 -8 14 91.89 16.40 5 -8 14 0.10 11.80 5 -8 14 24.90 9.50 5 -8 14 9.90 12.00 6 -8 14 0.40 9.70 6 -8 14 4.00 12.90 6 -8 14 5.20 11.40 7 -8 14 17.30 12.30 7 -8 14 1.70 9.70 7 -8 14 8.60 11.10 8 -8 14 64.69 11.10 8 -8 14 74.99 11.60 9 -8 14 83.79 12.90 9 -8 14 115.89 13.50 12 7 -14 29.40 14.80 11 7 -14 19.60 11.60 11 7 -14 -0.10 11.50 10 7 -14 6.30 8.00 10 7 -14 15.30 9.90 10 7 -14 7.90 11.60 9 7 -14 5.50 7.50 9 7 -14 6.80 12.90 9 7 -14 12.90 8.60 8 7 -14 -4.10 7.90 8 7 -14 -11.30 10.20 8 7 -14 4.60 7.30 7 7 -14 311.67 18.90 7 7 -14 225.88 23.20 7 7 -14 324.17 21.10 6 7 -14 15.40 9.00 6 7 -14 7.20 7.50 6 7 -14 5.30 6.30 5 7 -14 5.90 6.00 5 7 -14 4.60 6.50 5 7 -14 9.50 8.00 -5 -7 14 10.60 9.10 4 7 -14 26.80 5.70 4 7 -14 39.10 6.70 4 7 -14 36.00 7.70 -4 -7 14 29.90 9.50 3 7 -14 9.90 4.90 3 7 -14 2.30 6.30 3 7 -14 5.60 5.30 -3 -7 14 7.50 9.40 2 7 -14 97.69 7.80 2 7 -14 86.69 9.20 2 7 -14 77.99 8.50 -2 -7 14 91.59 13.30 -2 -7 14 71.49 8.60 1 7 -14 251.27 15.30 1 7 -14 214.68 14.60 1 7 -14 244.68 13.80 -1 -7 14 265.67 18.40 -1 -7 14 237.28 15.10 0 7 -14 29.80 3.80 0 7 -14 30.20 4.70 0 -7 14 22.60 9.30 0 -7 14 19.90 6.00 -1 7 -14 27.20 4.50 1 -7 14 34.50 9.90 1 -7 14 32.00 6.90 -2 7 -14 734.93 38.00 2 -7 14 731.93 39.90 2 -7 14 760.32 41.40 -3 7 -14 251.77 14.20 3 -7 14 286.97 22.30 3 -7 14 283.47 21.40 3 -7 14 292.07 18.90 4 -7 14 288.87 22.00 4 -7 14 283.67 20.10 4 -7 14 292.57 31.10 5 -7 14 42.50 13.10 5 -7 14 49.20 10.40 5 -7 14 43.00 11.60 6 -7 14 0.70 14.90 6 -7 14 2.90 11.90 7 -7 14 16.90 12.90 7 -7 14 3.00 10.10 7 -7 14 17.90 10.00 8 -7 14 126.59 15.90 8 -7 14 132.49 16.70 9 -7 14 48.20 9.30 9 -7 14 76.19 13.30 12 6 -14 37.70 11.80 11 6 -14 58.49 12.10 11 6 -14 34.40 7.60 10 6 -14 -4.70 11.70 10 6 -14 1.90 7.40 10 6 -14 10.60 13.40 9 6 -14 -6.00 9.00 9 6 -14 1.60 10.40 9 6 -14 1.90 6.90 8 6 -14 -0.80 9.80 8 6 -14 6.30 8.70 8 6 -14 -1.30 6.80 7 6 -14 182.18 16.30 7 6 -14 215.98 14.70 7 6 -14 212.58 18.00 6 6 -14 29.50 7.80 6 6 -14 15.30 8.20 6 6 -14 23.40 8.60 5 6 -14 7.00 5.50 5 6 -14 2.80 6.50 5 6 -14 3.60 7.50 -5 -6 14 6.80 9.10 4 6 -14 3.10 6.70 4 6 -14 6.00 5.60 4 6 -14 3.30 4.80 -4 -6 14 4.60 8.80 -4 -6 14 0.80 4.80 3 6 -14 123.59 8.90 3 6 -14 105.09 9.70 3 6 -14 115.59 10.20 -3 -6 14 100.09 9.70 -3 -6 14 116.79 13.60 2 6 -14 81.49 8.50 2 6 -14 93.19 7.30 2 6 -14 78.29 8.10 -2 -6 14 87.79 14.00 -2 -6 14 78.89 9.40 1 6 -14 256.57 16.10 1 6 -14 268.67 15.50 1 6 -14 288.97 15.20 -1 -6 14 290.27 16.80 -1 -6 14 266.37 20.40 0 6 -14 101.59 6.70 0 6 -14 87.99 6.20 0 -6 14 76.89 14.10 0 -6 14 97.69 10.50 -1 6 -14 12.40 2.70 1 -6 14 7.30 8.50 1 -6 14 13.70 6.60 -2 6 -14 352.86 19.70 2 -6 14 373.36 25.10 2 -6 14 401.06 24.30 2 -6 14 419.76 22.90 3 -6 14 205.48 16.70 3 -6 14 203.78 19.10 3 -6 14 232.18 18.00 4 -6 14 312.47 21.90 4 -6 14 300.67 24.10 4 -6 14 317.97 21.40 5 -6 14 113.39 18.40 5 -6 14 111.59 15.70 5 -6 14 107.79 14.10 6 -6 14 -6.60 12.20 6 -6 14 8.70 13.40 6 -6 14 13.10 11.90 7 -6 14 59.49 11.10 7 -6 14 72.89 11.60 7 -6 14 61.79 15.10 8 -6 14 -1.60 10.30 8 -6 14 12.80 9.80 9 -6 14 31.10 9.80 13 5 -14 26.60 10.30 12 5 -14 26.70 12.40 11 5 -14 1.40 11.40 11 5 -14 5.00 7.20 11 5 -14 2.50 9.60 10 5 -14 4.20 7.70 10 5 -14 -3.50 15.80 10 5 -14 16.50 9.20 9 5 -14 12.80 10.60 9 5 -14 -0.90 8.60 9 5 -14 -5.40 7.50 8 5 -14 14.90 11.80 8 5 -14 10.40 10.10 8 5 -14 4.70 6.80 7 5 -14 34.80 9.70 7 5 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15 -1.20 15.30 -2 12 -15 1.70 5.00 2 -12 15 6.40 12.70 3 -12 15 21.40 12.20 -4 12 -15 122.59 9.20 4 -12 15 159.88 17.70 5 -12 15 6.90 11.50 6 -12 15 -4.40 10.20 7 -12 15 110.99 14.80 9 11 -15 -11.00 10.50 9 11 -15 2.10 8.70 8 11 -15 39.60 11.50 8 11 -15 26.50 7.70 7 11 -15 179.38 18.50 7 11 -15 136.59 16.60 7 11 -15 129.49 14.20 6 11 -15 11.20 10.90 6 11 -15 2.90 7.40 6 11 -15 4.70 8.70 5 11 -15 7.00 7.30 5 11 -15 6.00 7.70 -5 -11 15 8.80 16.70 4 11 -15 -3.80 6.60 4 11 -15 -7.30 7.00 4 11 -15 2.70 9.80 -4 -11 15 -0.20 11.00 3 11 -15 161.98 14.00 3 11 -15 194.08 16.80 3 11 -15 201.38 14.30 -3 -11 15 181.88 18.40 2 11 -15 13.00 6.40 2 11 -15 12.60 8.30 2 11 -15 13.60 5.90 -2 -11 15 18.70 11.50 1 11 -15 -1.70 5.00 1 11 -15 -0.50 5.90 1 11 -15 -9.60 7.20 -1 -11 15 11.50 11.40 0 11 -15 34.00 5.90 0 -11 15 31.40 12.00 -1 11 -15 4.90 4.90 1 -11 15 8.30 12.30 -2 11 -15 59.69 7.60 2 -11 15 44.30 12.90 -3 11 -15 39.50 6.60 3 -11 15 29.10 12.50 4 -11 15 1.80 11.80 5 -11 15 7.00 12.30 6 -11 15 13.30 11.30 7 -11 15 82.39 14.10 10 10 -15 -2.10 14.30 9 10 -15 21.40 11.80 9 10 -15 15.30 7.50 8 10 -15 76.19 11.60 8 10 -15 97.49 17.20 7 10 -15 2.50 11.00 7 10 -15 4.70 7.80 6 10 -15 -2.60 7.80 6 10 -15 9.10 8.20 5 10 -15 29.80 7.40 5 10 -15 24.70 10.20 5 10 -15 16.40 7.30 -5 -10 15 23.00 11.70 4 10 -15 52.49 9.90 4 10 -15 55.89 10.90 4 10 -15 52.49 7.70 -4 -10 15 59.39 12.00 3 10 -15 17.30 6.40 3 10 -15 15.20 6.50 3 10 -15 0.60 8.40 -3 -10 15 18.60 11.20 2 10 -15 84.79 11.80 2 10 -15 81.29 9.90 -2 -10 15 60.89 12.40 1 10 -15 8.00 4.80 1 10 -15 6.80 5.50 1 10 -15 -4.90 6.40 -1 -10 15 2.30 11.10 0 10 -15 15.40 5.10 0 -10 15 6.70 12.20 -1 10 -15 14.60 4.50 1 -10 15 7.60 11.70 -2 10 -15 96.39 8.00 2 -10 15 106.79 17.60 -3 10 -15 10.10 3.80 3 -10 15 0.60 12.20 -4 10 -15 59.79 5.70 4 -10 15 67.39 13.60 5 -10 15 -3.90 11.60 5 -10 15 18.10 7.20 6 -10 15 -3.10 11.70 6 -10 15 3.30 8.70 7 -10 15 14.50 10.80 7 -10 15 16.20 8.20 11 9 -15 7.00 10.70 10 9 -15 -6.20 10.90 10 9 -15 -7.30 11.40 9 9 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8.00 9 8 -15 17.50 11.30 9 8 -15 1.60 8.30 8 8 -15 27.10 7.90 8 8 -15 8.80 8.10 8 8 -15 21.90 10.80 7 8 -15 108.99 12.20 7 8 -15 83.49 13.30 7 8 -15 104.19 16.50 6 8 -15 137.09 16.00 6 8 -15 103.39 12.30 6 8 -15 112.79 13.40 5 8 -15 54.19 9.70 5 8 -15 40.70 9.00 5 8 -15 75.89 10.00 -5 -8 15 42.90 11.00 4 8 -15 13.80 8.10 4 8 -15 18.80 6.70 4 8 -15 30.20 6.40 -4 -8 15 23.60 10.40 3 8 -15 2.90 7.10 3 8 -15 9.60 5.50 3 8 -15 8.80 5.60 -3 -8 15 -2.50 9.90 2 8 -15 50.89 8.10 2 8 -15 53.89 7.40 -2 -8 15 57.89 11.40 1 8 -15 22.90 9.70 1 8 -15 15.80 5.10 1 8 -15 17.00 4.40 -1 -8 15 24.10 10.80 0 8 -15 18.60 4.40 0 -8 15 3.00 10.30 1 -8 15 63.89 11.60 1 -8 15 54.09 10.60 2 -8 15 8.80 7.60 2 -8 15 7.50 10.60 -3 8 -15 30.90 4.10 3 -8 15 31.00 8.60 3 -8 15 42.20 11.60 4 -8 15 -0.20 8.60 4 -8 15 14.20 11.20 5 -8 15 36.80 12.40 5 -8 15 43.40 9.50 5 -8 15 40.30 16.60 6 -8 15 24.40 9.40 6 -8 15 -2.40 11.80 6 -8 15 13.70 11.50 7 -8 15 53.59 11.30 7 -8 15 84.69 13.80 8 -8 15 18.60 8.80 8 -8 15 8.70 8.80 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15 -17.00 10.70 5 -7 15 14.70 14.80 5 -7 15 12.70 15.30 5 -7 15 12.60 12.30 6 -7 15 1.80 11.10 6 -7 15 5.10 10.00 6 -7 15 -1.60 10.20 7 -7 15 73.49 14.40 7 -7 15 51.29 10.50 8 -7 15 11.00 8.90 8 -7 15 9.10 11.50 12 6 -15 -1.50 11.20 11 6 -15 11.70 11.90 11 6 -15 -5.30 8.40 10 6 -15 10.70 10.10 10 6 -15 0.30 7.70 10 6 -15 0.70 11.70 9 6 -15 6.00 9.90 9 6 -15 7.50 12.60 9 6 -15 4.20 7.70 8 6 -15 -2.00 7.00 8 6 -15 10.50 10.20 8 6 -15 15.50 8.50 7 6 -15 9.90 9.30 7 6 -15 3.90 7.00 7 6 -15 9.30 8.70 6 6 -15 14.70 9.10 6 6 -15 14.60 6.50 6 6 -15 12.60 7.90 5 6 -15 7.40 7.80 5 6 -15 2.70 6.50 5 6 -15 19.80 9.00 -5 -6 15 1.70 9.90 4 6 -15 77.79 10.00 4 6 -15 84.69 8.80 4 6 -15 69.49 11.30 -4 -6 15 62.69 10.70 -4 -6 15 68.59 8.90 3 6 -15 114.89 10.70 3 6 -15 133.49 9.80 -3 -6 15 118.99 15.60 -3 -6 15 125.39 11.00 2 6 -15 264.57 14.50 2 6 -15 240.38 14.80 2 6 -15 231.38 15.40 -2 -6 15 238.08 16.00 -2 -6 15 262.77 19.40 1 6 -15 11.40 5.30 1 6 -15 6.60 3.80 1 6 -15 4.70 3.80 -1 -6 15 6.00 6.50 -1 -6 15 1.00 9.40 0 6 -15 177.28 10.30 0 -6 15 150.48 14.90 0 -6 15 185.18 17.10 -1 6 -15 6.90 2.90 1 -6 15 -0.50 10.00 1 -6 15 -2.90 6.90 -2 6 -15 169.48 9.50 2 -6 15 172.98 17.30 2 -6 15 170.38 15.10 3 -6 15 148.29 15.60 3 -6 15 155.98 18.30 3 -6 15 159.78 16.40 4 -6 15 184.98 17.30 4 -6 15 172.78 17.30 4 -6 15 155.28 18.80 5 -6 15 157.98 20.20 5 -6 15 258.57 23.00 5 -6 15 226.28 23.00 6 -6 15 10.00 9.80 6 -6 15 -13.40 9.90 6 -6 15 -1.40 14.50 7 -6 15 12.00 9.50 7 -6 15 -3.00 10.30 8 -6 15 23.50 13.00 8 -6 15 25.90 10.20 12 5 -15 15.60 11.10 11 5 -15 42.10 12.10 11 5 -15 8.40 7.40 10 5 -15 21.30 10.90 10 5 -15 22.20 10.90 9 5 -15 -4.80 7.00 9 5 -15 0.40 8.90 9 5 -15 4.90 11.10 8 5 -15 423.66 24.70 8 5 -15 454.05 27.60 8 5 -15 404.76 26.90 7 5 -15 231.28 18.30 7 5 -15 233.38 15.80 7 5 -15 197.38 25.50 6 5 -15 9.30 6.30 6 5 -15 4.50 8.30 6 5 -15 2.00 7.20 -6 -5 15 12.90 7.40 5 5 -15 31.40 7.10 5 5 -15 39.00 8.20 5 5 -15 29.50 6.00 -5 -5 15 35.60 6.50 -5 -5 15 24.50 9.50 4 5 -15 82.29 10.20 4 5 -15 83.69 8.40 4 5 -15 77.89 14.50 -4 -5 15 57.69 9.70 -4 -5 15 80.49 14.50 3 5 -15 37.00 6.60 3 5 -15 49.00 8.20 3 5 -15 40.00 5.30 -3 -5 15 23.90 6.30 -3 -5 15 28.00 9.30 2 5 -15 163.68 10.60 2 5 -15 159.68 11.10 2 5 -15 154.28 11.70 -2 -5 15 167.38 13.00 -2 -5 15 165.98 15.20 1 5 -15 66.49 8.30 1 5 -15 85.99 6.90 -1 -5 15 91.69 10.70 -1 -5 15 75.19 13.10 0 5 -15 16.20 3.30 0 -5 15 4.40 9.20 0 -5 15 15.50 7.50 -1 5 -15 29.80 4.30 1 -5 15 19.40 9.40 1 -5 15 22.00 7.70 -2 5 -15 95.79 5.90 2 -5 15 78.09 14.80 2 -5 15 89.99 13.20 2 -5 15 122.19 14.80 3 -5 15 63.59 15.20 3 -5 15 107.69 14.10 3 -5 15 92.59 13.70 4 -5 15 98.19 14.40 4 -5 15 91.29 15.00 4 -5 15 71.69 13.10 5 -5 15 116.39 18.60 5 -5 15 150.28 16.40 5 -5 15 127.99 15.60 6 -5 15 1.10 9.30 6 -5 15 -1.50 12.60 6 -5 15 1.50 10.60 7 -5 15 25.40 9.10 7 -5 15 22.90 10.20 8 -5 15 35.00 10.60 12 4 -15 22.00 11.60 11 4 -15 15.70 11.80 11 4 -15 7.60 7.80 11 4 -15 -10.60 13.20 10 4 -15 19.90 8.00 10 4 -15 26.60 11.90 10 4 -15 23.70 14.30 9 4 -15 14.60 11.30 9 4 -15 15.30 7.40 9 4 -15 -16.50 8.40 8 4 -15 16.00 10.10 8 4 -15 18.90 7.50 8 4 -15 15.70 9.50 -8 -4 15 8.90 6.60 7 4 -15 181.18 16.80 7 4 -15 165.18 13.10 7 4 -15 175.28 15.50 -7 -4 15 122.69 13.00 6 4 -15 221.98 16.90 6 4 -15 212.98 16.40 -6 -4 15 207.78 15.20 5 4 -15 76.19 11.10 5 4 -15 94.39 9.30 5 4 -15 79.69 12.00 -5 -4 15 80.79 11.30 -5 -4 15 78.39 13.30 4 4 -15 19.80 10.70 4 4 -15 14.80 6.00 4 4 -15 12.70 4.80 -4 -4 15 15.70 8.90 -4 -4 15 17.90 6.60 3 4 -15 47.00 6.10 3 4 -15 43.00 6.70 3 4 -15 44.70 6.70 -3 -4 15 32.30 6.90 -3 -4 15 35.30 8.90 2 4 -15 33.90 4.50 2 4 -15 29.90 4.90 2 4 -15 31.00 5.70 -2 -4 15 28.60 8.60 -2 -4 15 24.60 6.90 1 4 -15 72.99 8.00 1 4 -15 73.69 6.70 1 4 -15 76.19 6.50 -1 -4 15 65.49 13.00 -1 -4 15 84.69 12.60 0 4 -15 1.80 3.00 0 -4 15 9.10 7.30 0 -4 15 -0.90 8.00 -1 4 -15 189.08 10.70 1 -4 15 190.18 15.80 1 -4 15 192.48 16.60 -2 4 -15 16.60 2.60 2 -4 15 15.70 8.60 2 -4 15 15.10 8.80 2 -4 15 12.40 8.80 -3 4 -15 439.26 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8.20 4 14 -16 41.60 14.10 4 14 -16 48.40 8.10 3 14 -16 7.10 7.60 3 14 -16 5.20 9.40 -3 -14 16 4.00 10.30 2 14 -16 52.09 10.90 2 14 -16 40.80 7.90 -2 -14 16 47.60 12.00 1 14 -16 13.20 10.50 1 14 -16 0.70 6.60 -1 -14 16 -0.80 11.30 0 14 -16 -9.30 6.10 0 -14 16 13.10 11.30 -1 14 -16 6.10 5.60 1 -14 16 4.20 10.90 2 -14 16 4.40 10.90 -3 14 -16 29.50 5.30 3 -14 16 25.00 11.80 4 -14 16 14.40 15.50 7 13 -16 7.60 12.20 7 13 -16 -0.10 6.80 6 13 -16 29.50 7.70 6 13 -16 15.70 10.90 5 13 -16 -0.90 7.40 5 13 -16 3.50 10.30 4 13 -16 -3.30 9.90 4 13 -16 4.90 7.30 -4 -13 16 7.20 10.80 3 13 -16 90.09 11.80 3 13 -16 87.89 14.80 -3 -13 16 65.49 12.20 2 13 -16 112.49 14.70 2 13 -16 132.29 12.30 -2 -13 16 120.39 17.50 1 13 -16 10.30 6.80 1 13 -16 15.20 8.20 -1 -13 16 16.00 12.10 0 13 -16 10.70 6.20 0 -13 16 12.40 12.00 -1 13 -16 24.70 5.90 1 -13 16 28.70 12.90 -2 13 -16 29.80 5.10 2 -13 16 19.30 12.30 3 -13 16 264.57 22.60 4 -13 16 6.30 12.30 5 -13 16 -3.80 10.70 8 12 -16 24.90 12.80 8 12 -16 5.80 6.70 7 12 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145.89 12.30 -3 -11 16 135.09 23.00 2 11 -16 151.48 11.90 2 11 -16 121.99 11.00 -2 -11 16 102.99 22.70 1 11 -16 86.09 10.00 -1 -11 16 91.29 24.40 0 11 -16 20.20 5.70 0 -11 16 -0.90 19.10 -1 11 -16 309.87 18.10 1 -11 16 335.47 24.10 -2 11 -16 21.00 7.40 2 -11 16 13.90 12.50 -3 11 -16 6.70 3.80 3 -11 16 3.20 12.30 4 -11 16 13.60 11.90 5 -11 16 22.10 11.90 6 -11 16 23.30 12.00 9 10 -16 21.90 8.10 9 10 -16 45.50 11.20 8 10 -16 6.30 7.00 8 10 -16 -5.20 10.60 7 10 -16 0.80 9.30 7 10 -16 14.10 7.60 7 10 -16 9.20 10.80 6 10 -16 20.80 7.80 6 10 -16 22.00 10.60 5 10 -16 18.70 7.50 5 10 -16 10.00 7.10 5 10 -16 20.60 13.30 -5 -10 16 23.20 13.10 4 10 -16 2.00 6.50 4 10 -16 9.60 6.90 4 10 -16 6.10 10.10 -4 -10 16 -5.50 10.80 3 10 -16 22.00 8.70 3 10 -16 28.00 6.70 3 10 -16 6.40 6.10 -3 -10 16 11.00 11.80 2 10 -16 3.30 5.30 2 10 -16 5.30 6.10 2 10 -16 7.10 7.70 -2 -10 16 7.20 11.50 1 10 -16 20.70 5.80 -1 -10 16 9.70 11.60 0 10 -16 300.77 17.40 0 -10 16 298.97 24.30 -1 10 -16 9.20 4.40 1 -10 16 15.00 12.80 -2 10 -16 75.59 7.10 2 -10 16 70.79 16.30 3 -10 16 57.19 13.10 4 -10 16 -0.40 12.50 5 -10 16 24.00 11.20 6 -10 16 4.80 9.80 7 -10 16 19.70 9.30 10 9 -16 4.60 12.40 10 9 -16 6.10 7.30 9 9 -16 13.70 7.20 9 9 -16 3.10 10.70 8 9 -16 56.99 13.80 8 9 -16 116.99 12.10 8 9 -16 112.29 16.40 7 9 -16 106.39 16.10 7 9 -16 89.19 12.40 6 9 -16 5.10 7.20 6 9 -16 -15.10 13.00 6 9 -16 0.40 7.60 5 9 -16 0.90 6.90 5 9 -16 4.50 9.50 5 9 -16 3.20 6.80 -5 -9 16 -4.20 11.10 4 9 -16 0.60 6.20 4 9 -16 1.80 8.70 4 9 -16 -0.30 6.30 -4 -9 16 1.20 10.90 3 9 -16 11.80 6.30 3 9 -16 20.20 8.30 3 9 -16 8.20 5.80 -3 -9 16 5.20 11.10 2 9 -16 170.98 12.10 2 9 -16 156.58 13.60 -2 -9 16 167.48 19.20 1 9 -16 53.09 8.10 -1 -9 16 58.39 12.50 0 9 -16 -0.90 4.40 0 -9 16 13.30 11.40 -1 9 -16 182.08 11.30 1 -9 16 174.18 18.90 -2 9 -16 36.20 4.30 2 -9 16 31.70 13.00 -3 9 -16 81.99 7.50 3 -9 16 99.99 16.00 4 -9 16 -10.40 11.30 4 -9 16 3.60 8.20 5 -9 16 2.00 8.40 5 -9 16 6.80 10.90 6 -9 16 29.10 10.40 6 -9 16 30.30 10.60 7 -9 16 42.70 9.40 7 -9 16 33.20 8.20 11 8 -16 -1.10 10.50 10 8 -16 0.50 11.40 10 8 -16 -2.50 9.30 9 8 -16 16.20 11.30 9 8 -16 21.40 7.20 8 8 -16 34.30 9.20 8 8 -16 33.20 11.20 8 8 -16 25.10 9.30 7 8 -16 59.69 9.70 7 8 -16 64.69 14.60 7 8 -16 68.09 11.60 6 8 -16 13.50 7.90 6 8 -16 22.40 7.50 6 8 -16 17.90 9.90 5 8 -16 132.99 11.60 5 8 -16 112.69 15.00 5 8 -16 105.99 12.50 -5 -8 16 111.09 16.50 4 8 -16 6.60 8.10 4 8 -16 9.90 6.40 4 8 -16 9.70 6.20 -4 -8 16 10.50 11.20 3 8 -16 155.18 13.70 3 8 -16 193.38 14.40 3 8 -16 178.48 12.70 -3 -8 16 176.68 18.60 2 8 -16 80.19 9.10 2 8 -16 87.59 11.00 2 8 -16 99.79 9.20 -2 -8 16 89.19 16.80 1 8 -16 214.48 13.50 -1 -8 16 232.08 20.40 0 8 -16 17.00 4.40 0 -8 16 15.00 11.10 -1 8 -16 268.27 15.10 1 -8 16 258.47 21.20 1 -8 16 277.77 17.90 -2 8 -16 29.00 3.60 2 -8 16 31.20 8.30 2 -8 16 47.80 12.60 3 -8 16 78.69 14.20 3 -8 16 69.09 13.40 4 -8 16 49.80 12.50 4 -8 16 54.79 9.70 5 -8 16 16.40 10.60 5 -8 16 12.10 9.10 6 -8 16 73.09 12.00 6 -8 16 79.19 13.50 7 -8 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-7 -1 20 30.70 8.90 6 1 -20 -0.50 6.90 6 1 -20 -1.20 9.80 -6 -1 20 6.40 8.60 5 1 -20 92.99 15.30 5 1 -20 86.79 11.20 -5 -1 20 93.39 13.90 4 1 -20 51.59 9.90 4 1 -20 43.50 7.80 -4 -1 20 30.70 9.50 3 1 -20 13.50 8.50 3 1 -20 -4.10 7.90 -3 -1 20 15.20 10.20 2 1 -20 4.70 5.90 -2 -1 20 -3.80 9.50 1 1 -20 5.00 5.10 -1 -1 20 2.50 9.90 0 1 -20 20.20 5.00 0 -1 20 16.50 10.10 -1 1 -20 28.50 6.40 1 -1 20 23.00 9.90 2 -1 20 -2.60 10.50 3 -1 20 22.60 9.20 10 0 -20 35.20 10.90 9 0 -20 5.20 14.30 -9 0 20 5.50 8.20 8 0 -20 11.60 10.70 8 0 -20 2.50 7.20 -8 0 20 3.10 8.20 7 0 -20 -2.50 7.00 7 0 -20 12.80 10.60 -7 0 20 3.30 9.10 6 0 -20 1.60 10.00 6 0 -20 2.90 7.00 -6 0 20 11.00 9.20 5 0 -20 30.20 10.10 5 0 -20 19.50 7.20 -5 0 20 21.50 9.90 4 0 -20 50.79 7.90 4 0 -20 49.80 9.90 -4 0 20 25.00 9.80 3 0 -20 23.80 8.70 3 0 -20 17.60 6.70 -3 0 20 23.30 10.90 2 0 -20 90.29 10.10 -2 0 20 75.99 15.10 1 0 -20 48.00 8.10 -1 0 20 33.90 10.80 0 0 -20 221.08 14.20 0 0 20 241.58 19.40 1 0 20 10.70 10.60 2 0 20 11.10 9.60 9 -1 -20 -0.20 12.50 9 -1 -20 -4.20 11.30 -9 1 20 8.10 8.80 8 -1 -20 4.60 10.70 8 -1 -20 18.10 8.00 -8 1 20 13.60 8.70 7 -1 -20 -2.70 7.40 7 -1 -20 -6.10 10.20 -7 1 20 5.90 10.10 6 -1 -20 -1.70 7.60 6 -1 -20 -8.50 10.20 -6 1 20 8.30 9.30 5 -1 -20 8.20 9.90 5 -1 -20 20.10 7.80 -5 1 20 6.30 9.30 4 -1 -20 104.99 11.90 4 -1 -20 86.09 11.50 -4 1 20 105.69 15.50 3 -1 -20 15.10 6.60 3 -1 -20 7.40 8.50 -3 1 20 6.80 10.30 2 -1 -20 62.49 7.40 -2 1 20 60.99 11.90 1 -1 -20 7.30 5.80 -1 1 20 10.90 11.40 0 -1 -20 8.80 5.30 0 1 20 4.40 10.70 1 1 20 20.30 10.10 2 1 20 -2.90 11.50 9 -2 -20 26.20 8.30 9 -2 -20 22.40 11.90 -9 2 20 32.40 9.30 8 -2 -20 13.80 8.00 8 -2 -20 18.10 11.20 -8 2 20 17.40 10.20 7 -2 -20 -1.10 7.70 7 -2 -20 7.70 10.70 -7 2 20 6.10 9.40 6 -2 -20 9.70 10.70 6 -2 -20 11.90 7.60 -6 2 20 20.90 10.90 5 -2 -20 48.30 7.90 5 -2 -20 30.00 10.60 -5 2 20 47.70 11.10 4 -2 -20 84.09 14.60 4 -2 -20 85.59 11.50 -4 2 20 94.79 14.40 3 -2 -20 18.10 9.10 3 -2 -20 33.70 7.10 -3 2 20 41.60 11.80 2 -2 -20 -1.00 11.50 2 -2 -20 8.90 6.30 -2 2 20 -6.70 11.40 1 -2 -20 14.20 6.00 -1 2 20 6.70 11.60 0 -2 -20 68.19 8.80 0 2 20 75.99 12.30 -1 -2 -20 86.39 12.90 1 2 20 74.29 14.60 2 2 20 -12.20 9.30 9 -3 -20 81.49 11.60 9 -3 -20 94.09 17.00 -9 3 20 83.79 13.80 8 -3 -20 40.00 12.50 8 -3 -20 14.20 8.90 -8 3 20 15.50 11.50 7 -3 -20 35.90 8.10 7 -3 -20 37.60 11.40 -7 3 20 26.40 10.30 6 -3 -20 24.20 7.50 6 -3 -20 24.30 11.10 -6 3 20 39.70 11.70 5 -3 -20 75.59 15.30 5 -3 -20 79.99 11.30 -5 3 20 91.59 15.80 4 -3 -20 159.28 16.10 4 -3 -20 145.29 13.50 -4 3 20 166.78 16.70 3 -3 -20 13.70 8.80 3 -3 -20 2.30 6.70 -3 3 20 -5.90 11.20 2 -3 -20 12.70 6.40 -2 3 20 36.20 11.70 1 -3 -20 5.60 6.20 -1 3 20 11.50 11.60 0 3 20 29.00 10.60 -1 -3 -20 17.90 5.40 1 3 20 13.90 12.10 8 -4 -20 3.00 11.70 8 -4 -20 -13.40 9.20 -8 4 20 3.50 16.10 7 -4 -20 6.30 9.10 7 -4 -20 21.00 11.20 -7 4 20 9.00 9.90 6 -4 -20 -2.00 7.20 6 -4 -20 14.00 10.50 -6 4 20 4.50 10.60 5 -4 -20 20.10 7.10 5 -4 -20 27.20 10.10 -5 4 20 35.30 10.80 4 -4 -20 21.50 7.10 4 -4 -20 4.90 9.30 -4 4 20 4.20 11.00 3 -4 -20 3.00 10.40 3 -4 -20 4.50 6.60 -3 4 20 7.00 10.60 2 -4 -20 40.80 9.80 2 -4 -20 45.50 7.30 -2 4 20 32.20 10.80 1 -4 -20 -10.30 12.90 1 -4 -20 -1.40 9.10 -1 4 20 10.10 10.30 0 -4 -20 52.29 9.70 0 4 20 70.39 16.60 8 -5 -20 62.19 10.20 8 -5 -20 43.20 10.90 -8 5 20 49.10 10.10 7 -5 -20 21.90 9.10 7 -5 -20 12.60 12.30 -7 5 20 17.00 12.40 6 -5 -20 -16.40 11.60 6 -5 -20 1.30 15.70 -6 5 20 0.70 10.80 5 -5 -20 3.60 7.10 5 -5 -20 -12.70 13.10 -5 5 20 3.70 11.20 4 -5 -20 134.09 11.90 -4 5 20 105.29 16.20 3 -5 -20 13.20 7.10 3 -5 -20 21.40 9.80 -3 5 20 22.40 12.00 2 -5 -20 -3.00 8.30 -2 5 20 4.60 11.50 1 -5 -20 -2.90 11.70 1 -5 -20 -2.90 8.40 -1 5 20 6.00 15.10 7 -6 -20 41.30 10.30 -7 6 20 33.80 10.90 6 -6 -20 4.30 7.30 6 -6 -20 6.00 9.70 -6 6 20 -1.90 13.70 5 -6 -20 21.20 7.50 5 -6 -20 21.60 9.70 -5 6 20 31.20 16.00 4 -6 -20 41.20 9.90 -4 6 20 52.29 13.10 3 -6 -20 4.90 8.30 3 -6 -20 7.20 9.30 -3 6 20 -0.30 17.30 2 -6 -20 8.40 8.60 2 -6 -20 6.10 6.50 -2 6 20 3.40 11.30 4 9 -21 -4.30 6.00 3 9 -21 -2.70 5.50 -1 -9 21 23.80 10.30 5 8 -21 0.40 5.20 4 8 -21 10.90 5.60 3 8 -21 6.60 6.70 2 8 -21 11.70 4.40 -1 -8 21 18.00 9.40 0 -8 21 3.30 9.00 6 7 -21 11.90 7.70 6 7 -21 7.10 7.10 -1 -7 21 14.70 10.80 0 -7 21 143.49 15.20 1 -7 21 37.60 9.50 7 6 -21 2.70 6.20 7 6 -21 6.00 8.00 6 6 -21 28.30 8.40 5 6 -21 9.90 5.90 5 6 -21 3.80 7.80 4 6 -21 -9.30 5.30 3 6 -21 49.40 8.50 1 6 -21 37.00 6.80 0 -6 21 81.79 13.10 1 -6 21 14.80 12.10 7 5 -21 8.70 7.90 7 5 -21 17.00 8.60 6 5 -21 4.30 8.50 6 5 -21 14.00 7.00 5 5 -21 38.10 6.40 5 5 -21 29.40 8.50 4 5 -21 8.80 5.60 3 5 -21 33.40 5.60 -3 -5 21 22.70 11.80 2 5 -21 9.80 4.70 -2 -5 21 12.90 7.70 -1 -5 21 47.30 8.50 0 -5 21 5.10 7.80 1 -5 21 5.40 7.50 8 4 -21 92.19 13.90 8 4 -21 91.49 10.70 7 4 -21 27.50 9.00 6 4 -21 -0.70 6.10 6 4 -21 21.40 10.30 5 4 -21 -2.20 12.00 5 4 -21 5.10 6.00 -5 -4 21 -9.20 12.40 4 4 -21 31.80 6.20 -4 -4 21 25.80 12.00 3 4 -21 16.20 5.40 -3 -4 21 15.30 9.40 2 4 -21 14.90 5.10 -2 -4 21 21.60 11.80 -1 -4 21 48.50 13.30 0 -4 21 13.80 9.80 1 -4 21 42.30 9.00 8 3 -21 23.00 9.30 8 3 -21 12.60 7.20 7 3 -21 -9.50 11.20 7 3 -21 10.80 8.30 6 3 -21 2.90 6.10 6 3 -21 -0.10 9.50 -6 -3 21 1.70 7.60 5 3 -21 23.10 6.50 5 3 -21 42.50 15.40 4 3 -21 51.99 6.60 -4 -3 21 30.80 9.20 3 3 -21 3.30 5.70 -3 -3 21 11.70 8.40 2 3 -21 2.50 5.20 -2 -3 21 -0.50 9.00 -1 -3 21 5.70 8.50 0 3 -21 62.29 6.70 0 -3 21 36.70 9.50 1 -3 21 25.80 8.40 8 2 -21 -6.40 9.40 8 2 -21 -3.70 7.40 -8 -2 21 10.10 9.70 7 2 -21 7.60 14.60 7 2 -21 10.00 7.40 -7 -2 21 6.00 7.20 6 2 -21 5.40 9.50 6 2 -21 8.60 6.60 -6 -2 21 0.10 12.50 5 2 -21 71.19 10.60 5 2 -21 66.19 16.40 -5 -2 21 58.99 9.80 4 2 -21 9.90 6.20 -4 -2 21 2.30 8.80 3 2 -21 45.30 6.50 -3 -2 21 33.30 10.10 2 2 -21 4.70 5.20 -2 -2 21 2.90 8.80 1 2 -21 4.40 7.30 -1 -2 21 5.60 9.60 0 2 -21 20.30 4.80 0 -2 21 40.20 11.40 1 -2 21 -8.70 8.90 8 1 -21 1.50 9.00 8 1 -21 7.90 9.50 -8 -1 21 4.80 7.20 7 1 -21 17.40 11.90 7 1 -21 0.30 7.40 -7 -1 21 -4.00 7.30 6 1 -21 39.10 7.40 6 1 -21 42.50 16.40 -6 -1 21 23.70 11.00 5 1 -21 -0.80 14.00 5 1 -21 14.60 7.00 -5 -1 21 12.20 8.50 4 1 -21 12.80 6.50 -4 -1 21 4.70 9.00 3 1 -21 72.49 9.70 -3 -1 21 62.69 10.50 2 1 -21 5.50 5.40 -2 -1 21 10.80 9.80 -1 -1 21 31.60 10.70 0 1 -21 7.90 4.90 0 -1 21 11.20 11.40 1 -1 21 6.50 9.30 8 0 -21 19.60 9.60 8 0 -21 37.30 8.20 -8 0 21 21.10 8.20 7 0 -21 6.70 14.60 7 0 -21 2.40 9.00 -7 0 21 2.70 8.90 6 0 -21 -2.30 7.00 6 0 -21 2.20 10.10 -6 0 21 1.70 8.10 5 0 -21 2.00 6.80 5 0 -21 3.10 11.50 -5 0 21 4.30 8.90 4 0 -21 5.70 10.00 4 0 -21 11.60 6.50 -4 0 21 9.30 9.30 3 0 -21 36.90 6.40 -3 0 21 3.40 10.00 2 0 -21 3.60 5.40 -2 0 21 1.70 9.70 -1 0 21 61.89 10.80 0 0 -21 104.09 8.40 0 0 21 87.19 15.70 1 0 21 15.10 8.90 8 -1 -21 0.00 6.70 8 -1 -21 7.70 10.30 -8 1 21 -9.20 8.00 7 -1 -21 0.60 7.80 7 -1 -21 -8.40 11.40 -7 1 21 1.40 10.00 6 -1 -21 6.00 7.00 6 -1 -21 22.80 11.80 -6 1 21 13.00 9.80 5 -1 -21 20.30 10.00 5 -1 -21 28.00 7.00 -5 1 21 17.80 9.10 4 -1 -21 218.78 21.10 4 -1 -21 217.58 15.20 -4 1 21 209.18 18.20 3 -1 -21 4.90 6.00 -3 1 21 7.80 9.80 2 -1 -21 3.40 6.40 -2 1 21 -5.20 10.70 -1 1 21 -5.80 10.50 0 -1 -21 81.59 9.60 0 1 21 88.29 16.60 8 -2 -21 4.20 10.00 7 -2 -21 49.70 9.20 7 -2 -21 59.59 10.90 -7 2 21 48.90 9.90 6 -2 -21 5.30 11.30 6 -2 -21 10.40 9.40 -6 2 21 4.60 12.60 5 -2 -21 35.80 7.20 5 -2 -21 36.70 10.50 -5 2 21 24.40 9.60 4 -2 -21 27.30 8.80 4 -2 -21 35.10 6.90 -4 2 21 30.60 9.80 3 -2 -21 8.60 8.00 3 -2 -21 17.80 6.60 -3 2 21 5.00 10.30 -2 2 21 31.00 10.80 1 -2 -21 19.30 7.40 0 2 21 -2.00 10.50 7 -3 -21 2.00 9.40 7 -3 -21 2.20 6.50 -7 3 21 3.70 9.00 6 -3 -21 11.00 9.40 -6 3 21 29.30 14.00 5 -3 -21 28.20 9.10 -5 3 21 49.80 14.40 4 -3 -21 20.80 8.50 4 -3 -21 17.70 8.80 -4 3 21 7.30 9.80 3 -3 -21 117.49 13.30 -3 3 21 120.89 18.40 2 -3 -21 2.30 7.50 -2 3 21 1.70 13.10 1 -3 -21 -4.00 6.70 -1 3 21 6.50 10.60 6 -4 -21 5.50 8.80 6 -4 -21 8.40 6.50 -6 4 21 1.20 8.80 5 -4 -21 8.70 8.40 5 -4 -21 10.80 7.10 -5 4 21 15.10 10.10 4 -4 -21 122.19 13.70 4 -4 -21 114.89 14.30 -4 4 21 156.48 18.50 3 -4 -21 26.00 11.20 3 -4 -21 30.70 6.70 -3 4 21 38.00 10.10 5 5 -22 14.30 5.40 4 5 -22 109.29 9.40 3 5 -22 0.80 6.70 5 4 -22 65.89 9.30 4 4 -22 68.69 9.20 3 4 -22 23.10 5.30 -3 -4 22 16.50 8.10 -2 -4 22 -3.50 7.20 -1 -4 22 2.00 7.70 6 3 -22 -0.30 5.90 6 3 -22 -1.90 13.20 5 3 -22 15.40 6.50 -5 -3 22 4.70 8.20 4 3 -22 3.70 7.80 -4 -3 22 9.20 7.50 3 3 -22 14.80 5.90 -3 -3 22 15.40 7.90 -2 -3 22 5.20 7.40 -1 -3 22 17.00 7.50 6 2 -22 16.30 6.20 6 2 -22 14.30 9.30 -6 -2 22 7.30 9.10 5 2 -22 9.30 7.10 -5 -2 22 4.80 7.70 4 2 -22 13.00 6.40 -4 -2 22 10.90 8.00 3 2 -22 13.40 5.80 -3 -2 22 13.10 8.30 2 2 -22 26.70 8.10 -2 -2 22 9.90 8.00 -1 -2 22 13.60 8.10 6 1 -22 -5.60 6.10 6 1 -22 4.50 8.10 -6 -1 22 8.70 7.30 5 1 -22 25.80 7.30 5 1 -22 36.00 14.40 -5 -1 22 25.90 8.40 4 1 -22 35.20 7.20 -4 -1 22 21.60 8.70 3 1 -22 26.00 5.70 -3 -1 22 8.10 8.80 2 1 -22 -3.60 7.70 -2 -1 22 4.80 8.50 6 0 -22 4.50 9.10 5 0 -22 33.70 10.90 5 0 -22 60.59 9.60 -5 0 22 72.09 11.80 4 0 -22 62.69 9.20 -4 0 22 39.70 9.10 3 0 -22 22.70 5.60 -3 0 22 19.90 9.40 -2 0 22 -0.30 8.40 5 -1 -22 49.00 6.90 5 -1 -22 39.80 10.80 -5 1 22 43.70 9.80 4 -1 -22 6.10 5.60 -4 1 22 34.70 9.60 3 -1 -22 -8.40 7.80 -3 1 22 -9.10 8.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 34620 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 1.49418(5) 0.86651(4) 0.86455(4) 0.04213(19) Uani 1 1 d . . . . . Cu2 Cu 1.29543(5) 0.87494(4) 0.77248(4) 0.04168(19) Uani 1 1 d . . . . . O9 O -0.0592(3) 0.4227(2) 0.03690(17) 0.0340(7) Uani 1 1 d . . . . . O14 O 0.3293(3) 0.3508(2) 0.22136(18) 0.0321(7) Uani 1 1 d . . . . . O1 O 1.2955(3) 0.7524(2) 0.74825(18) 0.0355(8) Uani 1 1 d . . . . . O8 O 0.3665(3) 0.5662(2) 0.01358(17) 0.0374(8) Uani 1 1 d . . . . . O6 O 1.2296(3) 0.8585(2) 0.85981(18) 0.0367(8) Uani 1 1 d . . . . . O10 O -0.1971(3) 0.6306(2) 0.21998(18) 0.0349(7) Uani 1 1 d . . . . . O2 O 1.4661(3) 0.7474(2) 0.8231(2) 0.0374(8) Uani 1 1 d . . . . . O00A O 1.5481(3) 0.8877(2) 0.7702(2) 0.0400(8) Uani 1 1 d . . . . . O5 O 1.5032(3) 0.9860(2) 0.8964(2) 0.0419(9) Uani 1 1 d . . . . . O13 O 0.0066(3) 0.3747(2) 0.32991(19) 0.0401(8) Uani 1 1 d . . . . . O11 O -0.0033(3) 0.9224(2) 0.3008(2) 0.0368(8) Uani 1 1 d . . . . . O4 O 1.3390(3) 0.9964(2) 0.8161(2) 0.0412(8) Uani 1 1 d . . . . . O3 O 1.3787(3) 0.8918(3) 0.69382(19) 0.0430(9) Uani 1 1 d . . . . . O15 O 0.5691(3) 0.6419(2) 0.32971(19) 0.0468(9) Uani 1 1 d . . . . . O7 O 1.3935(3) 0.8409(2) 0.9348(2) 0.0439(9) Uani 1 1 d . . . . . O12 O 0.1146(3) 0.6711(2) 0.4672(2) 0.0456(9) Uani 1 1 d . . . . . N3 N 1.1330(3) 0.8735(2) 0.6924(2) 0.0268(8) Uani 1 1 d . . . . . N2 N -0.3370(3) 0.8723(2) -0.0599(2) 0.0295(8) Uani 1 1 d . . . . . C11 C 0.9273(3) 0.8665(2) 0.5848(2) 0.0206(8) Uani 1 1 d . . . . . C38 C 0.1384(3) 0.8656(3) 0.3808(2) 0.0243(9) Uani 1 1 d . . . . . C20 C 0.5033(3) 0.8565(3) 0.3616(2) 0.0228(8) Uani 1 1 d . . . . . C19 C 0.6127(3) 0.8573(3) 0.4185(2) 0.0217(8) Uani 1 1 d . . . . . C26 C 0.1897(3) 0.8715(3) 0.2035(2) 0.0252(9) Uani 1 1 d . . . . . C23 C 0.2973(3) 0.8665(3) 0.2606(2) 0.0236(9) Uani 1 1 d . . . . . C14 C 0.8187(3) 0.8633(3) 0.5265(2) 0.0212(8) Uani 1 1 d . . . . . C12 C 1.0295(3) 0.8807(3) 0.5639(2) 0.0259(9) Uani 1 1 d . . . . . H12 H 1.030822 0.888490 0.512426 0.031 Uiso 1 1 calc R U . . . C25 C 0.4808(3) 0.8211(3) 0.2834(2) 0.0272(9) Uani 1 1 d . . . . . C17 C 0.8115(3) 0.9146(3) 0.4708(2) 0.0248(9) Uani 1 1 d . . . . . H17 H 0.877119 0.951978 0.469064 0.030 Uiso 1 1 calc R U . . . C58 C 0.2403(4) 0.4056(3) 0.1128(2) 0.0276(9) Uani 1 1 d . . . . . C59 C 0.1425(4) 0.4222(3) 0.0654(2) 0.0301(10) Uani 1 1 d . . . . . H59 H 0.147055 0.447182 0.020915 0.036 Uiso 1 1 calc R U . . . C22 C 0.3178(3) 0.8984(3) 0.3393(2) 0.0233(8) Uani 1 1 d . . . . . C53 C -0.1400(3) 0.4949(3) 0.1955(3) 0.0284(9) Uani 1 1 d . . . . . H53 H -0.168919 0.490660 0.140942 0.034 Uiso 1 1 calc R U . . . C52 C -0.0903(3) 0.4303(3) 0.2248(3) 0.0276(9) Uani 1 1 d . . . . . C9 C 1.0357(4) 0.8595(3) 0.7126(3) 0.0309(10) Uani 1 1 d . . . . . H9 H 1.037610 0.851724 0.764425 0.037 Uiso 1 1 calc R U . . . C48 C -0.1476(4) 0.5652(3) 0.2450(3) 0.0289(9) Uani 1 1 d . . . . . C10 C 0.9320(4) 0.8560(3) 0.6610(2) 0.0295(10) Uani 1 1 d . . . . . H10 H 0.864328 0.846371 0.677730 0.035 Uiso 1 1 calc R U . . . C51 C -0.0451(4) 0.4388(3) 0.3048(3) 0.0319(10) Uani 1 1 d . . . . . C37 C 0.2298(3) 0.9351(3) 0.3735(3) 0.0282(9) Uani 1 1 d . . . . . H37A H 0.267060 0.968999 0.425490 0.034 Uiso 1 1 calc R U . . . H37B H 0.194961 0.972469 0.339586 0.034 Uiso 1 1 calc R U . . . C61 C 0.3556(4) 0.4320(3) 0.0963(3) 0.0303(10) Uani 1 1 d . . . . . H61A H 0.406012 0.393104 0.115123 0.036 Uiso 1 1 calc R U . . . H61B H 0.345466 0.427224 0.039393 0.036 Uiso 1 1 calc R U . . . C5 C 1.3750(4) 0.7150(3) 0.7718(2) 0.0292(9) Uani 1 1 d . . . . . C42 C -0.0548(4) 0.7902(3) 0.3425(2) 0.0290(10) Uani 1 1 d . . . . . H42 H -0.131549 0.786236 0.315150 0.035 Uiso 1 1 calc R U . . . C018 C 0.2300(4) 0.3664(3) 0.1760(2) 0.0278(9) Uani 1 1 d . . . . . C69 C 0.5119(4) 0.6864(3) 0.2100(3) 0.0323(10) Uani 1 1 d . . . . . C16 C 0.6201(3) 0.8049(3) 0.4737(2) 0.0292(9) Uani 1 1 d . . . . . H16 H 0.555003 0.766515 0.474645 0.035 Uiso 1 1 calc R U . . . C39 C 0.1667(4) 0.8032(3) 0.4247(2) 0.0288(10) Uani 1 1 d . . . . . H39 H 0.242483 0.807968 0.454332 0.035 Uiso 1 1 calc R U . . . C57 C 0.1259(4) 0.3463(3) 0.1926(3) 0.0300(10) Uani 1 1 d . . . . . H57 H 0.120860 0.318810 0.235603 0.036 Uiso 1 1 calc R U . . . C31 C -0.0135(3) 0.8767(3) 0.0949(2) 0.0269(9) Uani 1 1 d . . . . . C15 C 0.7221(3) 0.8080(3) 0.5275(3) 0.0290(9) Uani 1 1 d . . . . . H15 H 0.726056 0.772067 0.565261 0.035 Uiso 1 1 calc R U . . . C21 C 0.4214(3) 0.8929(3) 0.3882(2) 0.0240(9) Uani 1 1 d . . . . . H21 H 0.436744 0.915082 0.442007 0.029 Uiso 1 1 calc R U . . . C66 C 0.4636(3) 0.6678(3) 0.1303(3) 0.0298(10) Uani 1 1 d . . . . . H66 H 0.463953 0.711950 0.100663 0.036 Uiso 1 1 calc R U . . . C65 C 0.4116(4) 0.5210(3) 0.1350(2) 0.0292(10) Uani 1 1 d . . . . . C18 C 0.7091(3) 0.9122(3) 0.4172(2) 0.0263(9) Uani 1 1 d . . . . . H18 H 0.705051 0.948310 0.379487 0.032 Uiso 1 1 calc R U . . . C01J C 0.0280(4) 0.3662(3) 0.1463(2) 0.0271(9) Uani 1 1 d . . . . . C55 C -0.0822(4) 0.3534(3) 0.1699(3) 0.0311(10) Uani 1 1 d . . . . . H55A H -0.087263 0.303685 0.196011 0.037 Uiso 1 1 calc R U . . . H55B H -0.146416 0.342775 0.122909 0.037 Uiso 1 1 calc R U . . . C47 C -0.1048(4) 0.5736(3) 0.3256(3) 0.0328(10) Uani 1 1 d . . . . . C29 C 0.1035(4) 0.8015(3) 0.1789(3) 0.0293(10) Uani 1 1 d . . . . . H29 H 0.113082 0.751252 0.198985 0.035 Uiso 1 1 calc R U . . . C56 C 0.0381(4) 0.4029(3) 0.0820(2) 0.0276(9) Uani 1 1 d . . . . . C71 C 0.4147(4) 0.5862(3) 0.0926(2) 0.0292(10) Uani 1 1 d . . . . . C27 C 0.1738(4) 0.9437(3) 0.1725(3) 0.0314(10) Uani 1 1 d . . . . . H27 H 0.233004 0.991401 0.187299 0.038 Uiso 1 1 calc R U . . . N1 N 0.2642(4) 0.5859(3) 0.3286(3) 0.0479(11) Uani 1 1 d . U . . . C30 C 0.0030(4) 0.8044(3) 0.1250(3) 0.0304(10) Uani 1 1 d . . . . . H30 H -0.054952 0.755928 0.108647 0.037 Uiso 1 1 calc R U . . . C24 C 0.3774(3) 0.8270(3) 0.2341(2) 0.0290(10) Uani 1 1 d . . . . . H24 H 0.361156 0.803375 0.180602 0.035 Uiso 1 1 calc R U . . . C13 C 1.1287(3) 0.8834(3) 0.6196(2) 0.0268(9) Uani 1 1 d . . . . . H13 H 1.197996 0.892833 0.604913 0.032 Uiso 1 1 calc R U . . . C28 C 0.0728(4) 0.9477(3) 0.1200(3) 0.0315(10) Uani 1 1 d . . . . . H28 H 0.062302 0.998521 0.101320 0.038 Uiso 1 1 calc R U . . . C43 C 0.0243(4) 0.8594(3) 0.3407(2) 0.0272(9) Uani 1 1 d . . . . . C34 C -0.2840(4) 0.9405(3) -0.0078(3) 0.0343(11) Uani 1 1 d . . . . . H34 H -0.320487 0.987591 -0.004973 0.041 Uiso 1 1 calc R U . . . C32 C -0.1235(3) 0.8778(3) 0.0394(2) 0.0281(9) Uani 1 1 d . . . . . C72 C 0.5148(4) 0.6204(3) 0.2519(3) 0.0353(11) Uani 1 1 d . . . . . C40 C 0.0869(4) 0.7351(3) 0.4259(2) 0.0294(10) Uani 1 1 d . . . . . C41 C -0.0250(4) 0.7270(3) 0.3828(2) 0.0300(10) Uani 1 1 d . . . . . C7 C 1.4834(4) 0.8910(3) 0.7062(3) 0.0330(10) Uani 1 1 d . . . . . C50 C -0.0530(4) 0.5100(3) 0.3546(3) 0.0357(11) Uani 1 1 d . . . . . H50 H -0.022520 0.514920 0.409044 0.043 Uiso 1 1 calc R U . . . C33 C -0.1783(4) 0.9461(3) 0.0425(3) 0.0332(10) Uani 1 1 d . . . . . H33 H -0.143826 0.996068 0.078678 0.040 Uiso 1 1 calc R U . . . C2 C 1.4287(4) 1.0253(3) 0.8678(3) 0.0336(10) Uani 1 1 d . . . . . C025 C -0.0899(4) 0.3836(3) -0.0430(3) 0.0356(11) Uani 1 1 d . . . . . H02A H -0.037548 0.410253 -0.070021 0.053 Uiso 1 1 calc R U . . . H02B H -0.167176 0.389761 -0.067448 0.053 Uiso 1 1 calc R U . . . H02C H -0.085945 0.323827 -0.046261 0.053 Uiso 1 1 calc R U . . . C6 C 1.3643(4) 0.6252(3) 0.7356(3) 0.0337(10) Uani 1 1 d . . . . . H6A H 1.284133 0.599278 0.716784 0.051 Uiso 1 1 calc R U . . . H6B H 1.402379 0.594784 0.774530 0.051 Uiso 1 1 calc R U . . . H6C H 1.399589 0.622851 0.691909 0.051 Uiso 1 1 calc R U . . . C46 C -0.1122(4) 0.6506(3) 0.3806(3) 0.0359(11) Uani 1 1 d . . . . . H46A H -0.188669 0.664279 0.364350 0.043 Uiso 1 1 calc R U . . . H46B H -0.102090 0.636963 0.433723 0.043 Uiso 1 1 calc R U . . . C35 C -0.2835(4) 0.8081(3) -0.0650(3) 0.0372(11) Uani 1 1 d . . . . . H35 H -0.319141 0.759913 -0.103168 0.045 Uiso 1 1 calc R U . . . C36 C -0.1780(4) 0.8079(3) -0.0172(3) 0.0386(12) Uani 1 1 d . . . . . H36 H -0.142874 0.760348 -0.022924 0.046 Uiso 1 1 calc R U . . . C70 C 0.4633(4) 0.5394(3) 0.2145(3) 0.0335(10) Uani 1 1 d . . . . . H70 H 0.463271 0.495292 0.244201 0.040 Uiso 1 1 calc R U . . . C44 C -0.1194(4) 0.9140(3) 0.2582(3) 0.0398(12) Uani 1 1 d . . . . . H44A H -0.143238 0.859543 0.223514 0.060 Uiso 1 1 calc R U . . . H44B H -0.126865 0.959024 0.227210 0.060 Uiso 1 1 calc R U . . . H44C H -0.167168 0.917567 0.294668 0.060 Uiso 1 1 calc R U . . . C49 C -0.2522(4) 0.6214(3) 0.1402(3) 0.0408(12) Uani 1 1 d . . . . . H49A H -0.198285 0.611775 0.109018 0.061 Uiso 1 1 calc R U . . . H49B H -0.281268 0.672567 0.129821 0.061 Uiso 1 1 calc R U . . . H49C H -0.315101 0.573580 0.126249 0.061 Uiso 1 1 calc R U . . . C73 C 0.5643(4) 0.7754(3) 0.2512(3) 0.0375(12) Uani 1 1 d . . . . . H73A H 0.592781 0.807495 0.214345 0.045 Uiso 1 1 calc R U . . . H73B H 0.629697 0.773743 0.294660 0.045 Uiso 1 1 calc R U . . . C67 C 0.3916(5) 0.6269(3) -0.0331(3) 0.0420(12) Uani 1 1 d . . . . . H67A H 0.359951 0.602655 -0.088193 0.063 Uiso 1 1 calc R U . . . H67B H 0.473826 0.643872 -0.022789 0.063 Uiso 1 1 calc R U . . . H67C H 0.358285 0.676064 -0.020427 0.063 Uiso 1 1 calc R U . . . C4 C 1.2899(4) 0.8436(3) 0.9221(3) 0.0356(11) Uani 1 1 d . . . . . C3 C 1.2325(5) 0.8293(4) 0.9863(3) 0.0455(13) Uani 1 1 d . . . . . H3A H 1.267834 0.872740 1.032011 0.068 Uiso 1 1 calc R U . . . H3B H 1.240387 0.773993 1.000109 0.068 Uiso 1 1 calc R U . . . H3C H 1.152032 0.831763 0.968400 0.068 Uiso 1 1 calc R U . . . C60 C 0.3209(4) 0.2938(4) 0.2744(3) 0.0455(13) Uani 1 1 d . . . . . H60A H 0.270487 0.241289 0.246684 0.068 Uiso 1 1 calc R U . . . H60B H 0.290177 0.318519 0.315924 0.068 Uiso 1 1 calc R U . . . H60C H 0.396080 0.282254 0.297059 0.068 Uiso 1 1 calc R U . . . C68 C 0.5891(5) 0.5752(4) 0.3723(3) 0.0517(15) Uani 1 1 d . . . . . H68A H 0.632872 0.539595 0.347783 0.078 Uiso 1 1 calc R U . . . H68B H 0.516556 0.541568 0.372204 0.078 Uiso 1 1 calc R U . . . H68C H 0.631582 0.598548 0.425962 0.078 Uiso 1 1 calc R U . . . C8 C 1.5320(5) 0.8904(4) 0.6370(3) 0.0476(13) Uani 1 1 d . . . . . H8A H 1.614818 0.901978 0.654551 0.071 Uiso 1 1 calc R U . . . H8B H 1.506489 0.933666 0.607647 0.071 Uiso 1 1 calc R U . . . H8C H 1.506505 0.835334 0.603595 0.071 Uiso 1 1 calc R U . . . O16 O 0.3314(6) 0.5053(5) 0.4181(4) 0.062(2) Uani 0.594(11) 1 d . U P A 1 C64 C 0.2630(5) 0.5132(4) 0.3594(4) 0.0620(16) Uani 0.594(11) 1 d . U P A 1 H64 H 0.205563 0.466334 0.333590 0.074 Uiso 0.594(11) 1 calc R U P A 1 C45 C 0.2124(6) 0.6903(4) 0.5321(3) 0.0636(18) Uani 1 1 d . . . . . H45A H 0.280272 0.705070 0.513707 0.095 Uiso 1 1 calc R U . . . H45B H 0.218434 0.641288 0.557962 0.095 Uiso 1 1 calc R U . . . H45C H 0.205305 0.737699 0.568999 0.095 Uiso 1 1 calc R U . . . C54 C 0.0460(7) 0.3762(4) 0.4105(3) 0.0672(19) Uani 1 1 d . . . . . H54A H 0.085251 0.329089 0.419356 0.101 Uiso 1 1 calc R U . . . H54B H -0.018280 0.371610 0.434063 0.101 Uiso 1 1 calc R U . . . H54C H 0.098409 0.429085 0.434262 0.101 Uiso 1 1 calc R U . . . C62 C 0.1889(6) 0.5863(4) 0.2548(4) 0.0617(16) Uani 1 1 d . U . . . H62A H 0.158273 0.528488 0.228207 0.093 Uiso 1 1 calc R U . . . H62B H 0.230132 0.616392 0.223011 0.093 Uiso 1 1 calc R U . . . H62C H 0.126634 0.614419 0.262745 0.093 Uiso 1 1 calc R U . . . C63 C 0.3378(5) 0.6599(4) 0.3701(4) 0.0597(16) Uani 0.594(11) 1 d . U P A 1 H63A H 0.375800 0.650423 0.421807 0.090 Uiso 0.594(11) 1 calc R U P A 1 H63B H 0.294527 0.704964 0.375459 0.090 Uiso 0.594(11) 1 calc R U P A 1 H63C H 0.394568 0.675942 0.341866 0.090 Uiso 0.594(11) 1 calc R U P A 1 C1 C 1.4439(6) 1.1135(4) 0.8979(4) 0.0663(18) Uani 1 1 d . . . . . H1A H 1.471284 1.122777 0.954690 0.099 Uiso 1 1 calc R U . . . H1B H 1.371465 1.132493 0.883314 0.099 Uiso 1 1 calc R U . . . H1C H 1.499279 1.145051 0.876048 0.099 Uiso 1 1 calc R U . . . O17 O 0.3952(9) 0.6635(7) 0.4399(6) 0.073(4) Uani 0.406(11) 1 d D U P A 2 C64' C 0.2630(5) 0.5132(4) 0.3594(4) 0.0620(16) Uani 0.406(11) 1 d . U P A 2 H64A H 0.208780 0.510200 0.391540 0.093 Uiso 0.406 1 d . U P A 2 H64B H 0.338680 0.512630 0.391460 0.093 Uiso 0.406 1 d . U P A 2 H64C H 0.240580 0.464890 0.317060 0.093 Uiso 0.406 1 d . U P A 2 C63' C 0.3378(5) 0.6599(4) 0.3701(4) 0.0597(16) Uani 0.406(11) 1 d D U P A 2 H63' H 0.345037 0.708010 0.345742 0.072 Uiso 0.406(11) 1 calc R U P A 2 O18 O 0.505420 0.612690 0.548350 0.184 Uani 1 1 d . . . B 1 H18A H 0.467680 0.627760 0.506620 0.276 Uiso 1 1 d . U . C 1 H18B H 0.470220 0.562420 0.547920 0.276 Uiso 1 1 d . U . D 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.0313(3) 0.0474(4) 0.0413(4) 0.0023(3) -0.0047(3) 0.0141(3) Cu2 0.0291(3) 0.0560(4) 0.0361(3) 0.0031(3) -0.0009(2) 0.0145(3) O9 0.0315(17) 0.0454(19) 0.0229(15) -0.0008(13) -0.0026(13) 0.0210(15) O14 0.0247(15) 0.0430(19) 0.0293(16) 0.0117(14) 0.0015(13) 0.0123(14) O1 0.0255(16) 0.0413(19) 0.0331(17) -0.0011(14) -0.0068(13) 0.0144(14) O8 0.0417(19) 0.0418(19) 0.0206(15) -0.0015(14) 0.0020(14) -0.0027(15) O6 0.0265(16) 0.052(2) 0.0301(17) 0.0032(15) 0.0031(13) 0.0123(15) O10 0.0356(18) 0.0361(18) 0.0316(17) 0.0002(14) 0.0052(14) 0.0125(14) O2 0.0265(16) 0.0364(18) 0.0413(19) -0.0002(15) -0.0076(14) 0.0124(14) O00A 0.0232(16) 0.057(2) 0.0378(19) 0.0091(16) 0.0016(14) 0.0111(15) O5 0.0374(19) 0.042(2) 0.0373(19) 0.0001(15) -0.0108(15) 0.0171(16) O13 0.046(2) 0.043(2) 0.0304(17) 0.0103(15) 0.0045(15) 0.0107(16) O11 0.0229(16) 0.0401(19) 0.0453(19) 0.0093(15) -0.0003(14) 0.0120(14) O4 0.0337(18) 0.043(2) 0.0399(19) 0.0054(15) -0.0097(15) 0.0183(15) O3 0.0240(17) 0.073(3) 0.0316(18) 0.0140(17) 0.0020(14) 0.0110(16) O15 0.043(2) 0.062(2) 0.0253(17) -0.0083(16) -0.0066(15) 0.0186(18) O7 0.0342(19) 0.061(2) 0.0380(19) 0.0133(17) 0.0043(15) 0.0174(17) O12 0.043(2) 0.056(2) 0.039(2) 0.0183(17) 0.0040(16) 0.0175(18) N3 0.0207(17) 0.0290(19) 0.0275(19) 0.0009(15) 0.0015(14) 0.0058(15) N2 0.0232(18) 0.029(2) 0.0298(19) -0.0031(15) -0.0029(15) 0.0072(15) C11 0.0125(18) 0.024(2) 0.023(2) 0.0024(16) -0.0017(15) 0.0066(15) C38 0.0201(19) 0.033(2) 0.0199(19) -0.0024(17) 0.0045(16) 0.0112(17) C20 0.0143(18) 0.027(2) 0.024(2) 0.0018(16) -0.0009(15) 0.0051(16) C19 0.0108(17) 0.029(2) 0.0213(19) -0.0005(16) -0.0035(15) 0.0056(15) C26 0.0165(19) 0.037(2) 0.0197(19) -0.0006(17) -0.0008(15) 0.0100(17) C23 0.0131(18) 0.030(2) 0.023(2) -0.0008(17) -0.0024(15) 0.0062(16) C14 0.0144(18) 0.028(2) 0.0183(19) -0.0011(16) -0.0011(15) 0.0075(16) C12 0.020(2) 0.033(2) 0.021(2) 0.0007(17) -0.0004(16) 0.0084(17) C25 0.0174(19) 0.034(2) 0.027(2) -0.0022(18) 0.0004(16) 0.0087(17) C17 0.0155(19) 0.028(2) 0.027(2) 0.0032(17) -0.0005(16) 0.0006(16) C58 0.030(2) 0.031(2) 0.020(2) -0.0021(17) 0.0035(17) 0.0094(18) C59 0.034(2) 0.036(3) 0.019(2) 0.0012(18) 0.0038(17) 0.014(2) C22 0.0160(19) 0.027(2) 0.024(2) -0.0003(16) 0.0017(16) 0.0065(16) C53 0.021(2) 0.034(2) 0.025(2) -0.0028(18) 0.0025(17) 0.0012(18) C52 0.021(2) 0.032(2) 0.029(2) 0.0038(18) 0.0063(17) 0.0022(17) C9 0.024(2) 0.043(3) 0.023(2) 0.0061(19) -0.0009(17) 0.0099(19) C48 0.023(2) 0.032(2) 0.031(2) 0.0014(18) 0.0078(18) 0.0030(18) C10 0.020(2) 0.041(3) 0.026(2) 0.0065(19) 0.0018(17) 0.0087(19) C51 0.028(2) 0.036(3) 0.030(2) 0.0051(19) 0.0065(18) 0.0022(19) C37 0.022(2) 0.034(2) 0.028(2) -0.0026(18) 0.0048(17) 0.0105(18) C61 0.027(2) 0.037(3) 0.025(2) -0.0021(18) 0.0051(17) 0.0111(19) C5 0.023(2) 0.038(3) 0.026(2) 0.0037(18) 0.0045(17) 0.0083(19) C42 0.019(2) 0.043(3) 0.021(2) -0.0045(18) 0.0024(16) 0.0069(18) C018 0.025(2) 0.034(2) 0.023(2) 0.0034(18) 0.0014(17) 0.0125(18) C69 0.019(2) 0.043(3) 0.031(2) -0.009(2) 0.0041(17) 0.0123(19) C16 0.017(2) 0.039(3) 0.028(2) 0.0079(19) -0.0009(17) 0.0011(18) C39 0.023(2) 0.044(3) 0.019(2) 0.0009(18) 0.0004(16) 0.0148(19) C57 0.031(2) 0.029(2) 0.028(2) 0.0018(18) 0.0031(18) 0.0077(19) C31 0.018(2) 0.035(2) 0.023(2) -0.0027(17) -0.0028(16) 0.0099(18) C15 0.018(2) 0.038(3) 0.029(2) 0.0118(19) -0.0014(17) 0.0041(18) C21 0.0188(19) 0.030(2) 0.0188(19) -0.0024(16) -0.0016(15) 0.0051(17) C66 0.020(2) 0.038(3) 0.030(2) 0.0009(19) 0.0079(17) 0.0048(18) C65 0.024(2) 0.037(3) 0.025(2) -0.0023(18) 0.0053(17) 0.0104(19) C18 0.021(2) 0.033(2) 0.022(2) 0.0068(17) -0.0024(16) 0.0053(17) C01J 0.024(2) 0.027(2) 0.024(2) -0.0046(17) 0.0002(17) 0.0056(17) C55 0.023(2) 0.034(2) 0.033(2) 0.0027(19) 0.0020(18) 0.0052(18) C47 0.032(2) 0.036(3) 0.029(2) -0.0023(19) 0.0133(19) 0.001(2) C29 0.023(2) 0.030(2) 0.030(2) 0.0017(18) -0.0042(17) 0.0107(18) C56 0.028(2) 0.033(2) 0.020(2) -0.0018(17) 0.0008(17) 0.0154(18) C71 0.022(2) 0.043(3) 0.022(2) -0.0004(18) 0.0061(17) 0.0085(19) C27 0.019(2) 0.041(3) 0.029(2) 0.0044(19) -0.0013(17) 0.0028(19) N1 0.036(2) 0.052(3) 0.058(3) 0.007(2) 0.017(2) 0.0085(19) C30 0.019(2) 0.032(2) 0.032(2) -0.0009(18) -0.0072(17) 0.0054(18) C24 0.018(2) 0.046(3) 0.018(2) -0.0046(18) -0.0014(16) 0.0110(19) C13 0.0160(19) 0.035(2) 0.028(2) 0.0047(18) 0.0008(16) 0.0081(17) C28 0.025(2) 0.039(3) 0.028(2) 0.0075(19) -0.0017(18) 0.0078(19) C43 0.023(2) 0.037(2) 0.022(2) -0.0003(17) 0.0029(16) 0.0154(18) C34 0.024(2) 0.029(2) 0.041(3) 0.000(2) -0.0076(19) 0.0098(18) C32 0.021(2) 0.036(2) 0.024(2) 0.0013(18) -0.0033(16) 0.0101(18) C72 0.023(2) 0.054(3) 0.024(2) -0.008(2) -0.0002(17) 0.015(2) C40 0.034(2) 0.038(3) 0.020(2) 0.0046(18) 0.0084(18) 0.014(2) C41 0.031(2) 0.037(3) 0.022(2) -0.0033(18) 0.0097(18) 0.0085(19) C7 0.027(2) 0.031(2) 0.038(3) 0.002(2) 0.0040(19) 0.0043(19) C50 0.038(3) 0.042(3) 0.026(2) 0.005(2) 0.009(2) 0.004(2) C33 0.025(2) 0.031(2) 0.035(2) -0.0040(19) -0.0078(18) 0.0081(18) C2 0.038(3) 0.033(2) 0.031(2) 0.0062(19) 0.004(2) 0.015(2) C025 0.031(2) 0.043(3) 0.026(2) -0.002(2) -0.0041(18) 0.011(2) C6 0.027(2) 0.033(3) 0.037(3) -0.003(2) 0.0052(19) 0.0080(19) C46 0.035(3) 0.043(3) 0.031(2) -0.003(2) 0.017(2) 0.004(2) C35 0.030(2) 0.039(3) 0.032(2) -0.008(2) -0.0120(19) 0.014(2) C36 0.031(2) 0.042(3) 0.033(2) -0.007(2) -0.010(2) 0.019(2) C70 0.027(2) 0.046(3) 0.028(2) 0.002(2) 0.0052(18) 0.016(2) C44 0.029(2) 0.051(3) 0.041(3) 0.011(2) 0.000(2) 0.023(2) C49 0.041(3) 0.044(3) 0.036(3) 0.001(2) 0.003(2) 0.016(2) C73 0.018(2) 0.048(3) 0.038(3) -0.014(2) -0.0013(18) 0.013(2) C67 0.041(3) 0.052(3) 0.030(2) 0.007(2) 0.006(2) 0.002(2) C4 0.035(3) 0.031(2) 0.038(3) -0.001(2) 0.007(2) 0.008(2) C3 0.054(3) 0.047(3) 0.042(3) 0.009(2) 0.019(3) 0.017(3) C60 0.038(3) 0.061(4) 0.043(3) 0.028(3) 0.004(2) 0.020(3) C68 0.044(3) 0.071(4) 0.032(3) 0.004(3) -0.006(2) 0.014(3) C8 0.047(3) 0.054(3) 0.047(3) 0.013(3) 0.021(3) 0.009(3) O16 0.051(4) 0.081(5) 0.042(4) 0.018(3) -0.009(3) -0.002(4) C64 0.046(3) 0.065(4) 0.064(4) 0.014(3) -0.001(3) -0.003(3) C45 0.074(4) 0.074(4) 0.037(3) 0.016(3) -0.012(3) 0.029(4) C54 0.109(6) 0.065(4) 0.036(3) 0.018(3) 0.015(3) 0.037(4) C62 0.064(4) 0.063(4) 0.058(4) 0.016(3) 0.008(3) 0.019(3) C63 0.039(3) 0.053(3) 0.080(4) -0.013(3) 0.020(3) 0.001(3) C1 0.062(4) 0.065(4) 0.063(4) 0.013(3) -0.002(3) 0.010(3) O17 0.045(6) 0.065(7) 0.102(8) -0.008(6) 0.030(6) -0.010(5) C64' 0.046(3) 0.065(4) 0.064(4) 0.014(3) -0.001(3) -0.003(3) C63' 0.039(3) 0.053(3) 0.080(4) -0.013(3) 0.020(3) 0.001(3) O18 0.217 0.186 0.144 0.030 0.040 0.030 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Cu1 Cu2 88.26(9) . . ? O2 Cu1 O00A 87.83(15) . . ? O2 Cu1 O7 88.59(16) . . ? O2 Cu1 N2 96.66(13) . 1_756 ? O00A Cu1 Cu2 82.37(9) . . ? O00A Cu1 N2 95.42(14) . 1_756 ? O5 Cu1 Cu2 84.12(9) . . ? O5 Cu1 O2 172.37(13) . . ? O5 Cu1 O00A 90.82(16) . . ? O5 Cu1 O7 90.41(16) . . ? O5 Cu1 N2 90.94(13) . 1_756 ? O7 Cu1 Cu2 80.02(10) . . ? O7 Cu1 O00A 162.12(13) . . ? O7 Cu1 N2 102.40(14) . 1_756 ? N2 Cu1 Cu2 174.53(11) 1_756 . ? O1 Cu2 Cu1 79.68(9) . . ? O1 Cu2 N3 96.53(13) . . ? O6 Cu2 Cu1 87.72(9) . . ? O6 Cu2 O1 91.10(15) . . ? O6 Cu2 O4 88.67(15) . . ? O6 Cu2 N3 93.75(14) . . ? O4 Cu2 Cu1 83.73(9) . . ? O4 Cu2 O1 163.40(13) . . ? O4 Cu2 N3 100.04(13) . . ? O3 Cu2 Cu1 85.46(10) . . ? O3 Cu2 O1 88.25(16) . . ? O3 Cu2 O6 173.15(13) . . ? O3 Cu2 O4 90.00(17) . . ? O3 Cu2 N3 93.10(14) . . ? N3 Cu2 Cu1 175.97(10) . . ? C56 O9 C025 114.8(3) . . ? C018 O14 C60 118.0(4) . . ? C5 O1 Cu2 127.1(3) . . ? C71 O8 C67 117.6(4) . . ? C4 O6 Cu2 120.0(3) . . ? C48 O10 C49 117.6(4) . . ? C5 O2 Cu1 119.3(3) . . ? C7 O00A Cu1 123.6(3) . . ? C2 O5 Cu1 123.2(3) . . ? C51 O13 C54 118.8(4) . . ? C43 O11 C44 117.0(4) . . ? C2 O4 Cu2 121.6(3) . . ? C7 O3 Cu2 122.5(3) . . ? C72 O15 C68 117.4(4) . . ? C4 O7 Cu1 126.7(3) . . ? C40 O12 C45 118.2(4) . . ? C9 N3 Cu2 122.5(3) . . ? C13 N3 Cu2 119.6(3) . . ? C13 N3 C9 117.9(4) . . ? C34 N2 Cu1 121.4(3) . 1_354 ? C35 N2 Cu1 120.9(3) . 1_354 ? C35 N2 C34 117.7(4) . . ? C12 C11 C14 120.2(4) . . ? C10 C11 C14 122.3(4) . . ? C10 C11 C12 117.6(4) . . ? C39 C38 C37 120.5(4) . . ? C39 C38 C43 118.0(4) . . ? C43 C38 C37 121.3(4) . . ? C25 C20 C19 122.4(4) . . ? C21 C20 C19 118.2(4) . . ? C21 C20 C25 119.4(3) . . ? C16 C19 C20 121.3(4) . . ? C16 C19 C18 119.1(4) . . ? C18 C19 C20 119.6(4) . . ? C29 C26 C23 119.6(4) . . ? C27 C26 C23 122.0(4) . . ? C27 C26 C29 118.4(4) . . ? C22 C23 C26 121.6(4) . . ? C22 C23 C24 119.5(3) . . ? C24 C23 C26 118.9(4) . . ? C17 C14 C11 121.0(4) . . ? C17 C14 C15 118.9(4) . . ? C15 C14 C11 120.1(4) . . ? C11 C12 H12 120.8 . . ? C13 C12 C11 118.5(4) . . ? C13 C12 H12 120.8 . . ? C20 C25 C24 117.9(4) . . ? C20 C25 C73 122.0(4) . . ? C24 C25 C73 120.1(4) . . ? C14 C17 H17 119.7 . . ? C14 C17 C18 120.7(4) . . ? C18 C17 H17 119.7 . . ? C59 C58 C61 120.4(4) . . ? C59 C58 C018 117.9(4) . . ? C018 C58 C61 121.7(4) . . ? C58 C59 H59 119.4 . . ? C56 C59 C58 121.1(4) . . ? C56 C59 H59 119.4 . . ? C23 C22 C37 122.3(3) . . ? C23 C22 C21 117.8(4) . . ? C21 C22 C37 119.8(4) . . ? C52 C53 H53 119.5 . . ? C48 C53 H53 119.5 . . ? C48 C53 C52 121.0(4) . . ? C53 C52 C55 120.5(4) . . ? C51 C52 C53 118.8(4) . . ? C51 C52 C55 120.7(4) . . ? N3 C9 H9 118.7 . . ? N3 C9 C10 122.6(4) . . ? C10 C9 H9 118.7 . . ? O10 C48 C53 123.9(4) . . ? O10 C48 C47 115.3(4) . . ? C53 C48 C47 120.8(4) . . ? C11 C10 H10 120.2 . . ? C9 C10 C11 119.6(4) . . ? C9 C10 H10 120.2 . . ? O13 C51 C52 116.1(4) . . ? O13 C51 C50 123.9(4) . . ? C52 C51 C50 120.0(4) . . ? C38 C37 C22 110.6(3) . . ? C38 C37 H37A 109.5 . . ? C38 C37 H37B 109.5 . . ? C22 C37 H37A 109.5 . . ? C22 C37 H37B 109.5 . . ? H37A C37 H37B 108.1 . . ? C58 C61 H61A 109.1 . . ? C58 C61 H61B 109.1 . . ? H61A C61 H61B 107.8 . . ? C65 C61 C58 112.7(3) . . ? C65 C61 H61A 109.1 . . ? C65 C61 H61B 109.1 . . ? O1 C5 O2 125.3(4) . . ? O1 C5 C6 118.1(4) . . ? O2 C5 C6 116.6(4) . . ? C43 C42 H42 119.0 . . ? C41 C42 H42 119.0 . . ? C41 C42 C43 122.0(4) . . ? O14 C018 C58 116.0(4) . . ? O14 C018 C57 122.7(4) . . ? C57 C018 C58 121.3(4) . . ? C66 C69 C72 118.2(4) . . ? C66 C69 C73 121.9(5) . . ? C72 C69 C73 119.9(4) . . ? C19 C16 H16 119.8 . . ? C19 C16 C15 120.4(4) . . ? C15 C16 H16 119.8 . . ? C38 C39 H39 119.2 . . ? C40 C39 C38 121.5(4) . . ? C40 C39 H39 119.2 . . ? C018 C57 H57 119.7 . . ? C018 C57 C01J 120.5(4) . . ? C01J C57 H57 119.7 . . ? C30 C31 C28 118.7(4) . . ? C30 C31 C32 119.2(4) . . ? C28 C31 C32 122.0(4) . . ? C14 C15 H15 119.7 . . ? C16 C15 C14 120.6(4) . . ? C16 C15 H15 119.7 . . ? C20 C21 C22 122.9(4) . . ? C20 C21 H21 118.6 . . ? C22 C21 H21 118.6 . . ? C69 C66 H66 119.1 . . ? C69 C66 C71 121.9(5) . . ? C71 C66 H66 119.1 . . ? C71 C65 C61 121.5(4) . . ? C71 C65 C70 117.9(4) . . ? C70 C65 C61 120.6(4) . . ? C19 C18 C17 120.3(4) . . ? C19 C18 H18 119.9 . . ? C17 C18 H18 119.9 . . ? C57 C01J C55 120.3(4) . . ? C56 C01J C57 118.0(4) . . ? C56 C01J C55 121.6(4) . . ? C52 C55 H55A 109.5 . . ? C52 C55 H55B 109.5 . . ? C01J C55 C52 110.7(4) . . ? C01J C55 H55A 109.5 . . ? C01J C55 H55B 109.5 . . ? H55A C55 H55B 108.1 . . ? C48 C47 C46 121.4(4) . . ? C50 C47 C48 118.1(4) . . ? C50 C47 C46 120.4(4) . . ? C26 C29 H29 119.7 . . ? C26 C29 C30 120.5(4) . . ? C30 C29 H29 119.7 . . ? C59 C56 O9 121.5(4) . . ? C01J C56 O9 117.4(4) . . ? C01J C56 C59 121.1(4) . . ? O8 C71 C66 122.9(4) . . ? O8 C71 C65 117.0(4) . . ? C65 C71 C66 120.0(4) . . ? C26 C27 H27 119.3 . . ? C26 C27 C28 121.4(4) . . ? C28 C27 H27 119.3 . . ? C64 N1 C62 119.8(5) . . ? C64 N1 C63 120.0(5) . . ? C63 N1 C62 120.2(5) . . ? C64' N1 C62 119.8(5) . . ? C64' N1 C63' 120.0(5) . . ? C63' N1 C62 120.2(5) . . ? C31 C30 C29 121.0(4) . . ? C31 C30 H30 119.5 . . ? C29 C30 H30 119.5 . . ? C23 C24 C25 122.5(4) . . ? C23 C24 H24 118.8 . . ? C25 C24 H24 118.8 . . ? N3 C13 C12 123.9(4) . . ? N3 C13 H13 118.0 . . ? C12 C13 H13 118.0 . . ? C31 C28 H28 120.0 . . ? C27 C28 C31 119.9(4) . . ? C27 C28 H28 120.0 . . ? O11 C43 C38 117.6(4) . . ? O11 C43 C42 122.9(4) . . ? C42 C43 C38 119.5(4) . . ? N2 C34 H34 118.3 . . ? N2 C34 C33 123.4(4) . . ? C33 C34 H34 118.3 . . ? C33 C32 C31 122.6(4) . . ? C33 C32 C36 116.9(4) . . ? C36 C32 C31 120.6(4) . . ? O15 C72 C69 115.6(4) . . ? O15 C72 C70 124.6(5) . . ? C70 C72 C69 119.8(4) . . ? O12 C40 C41 117.6(4) . . ? C39 C40 O12 122.2(4) . . ? C39 C40 C41 120.2(4) . . ? C42 C41 C40 118.7(4) . . ? C42 C41 C46 120.6(4) . . ? C40 C41 C46 120.7(4) . . ? O00A C7 O3 125.6(5) . . ? O00A C7 C8 117.8(4) . . ? O3 C7 C8 116.5(4) . . ? C51 C50 H50 119.4 . . ? C47 C50 C51 121.3(4) . . ? C47 C50 H50 119.4 . . ? C34 C33 C32 119.2(4) . . ? C34 C33 H33 120.4 . . ? C32 C33 H33 120.4 . . ? O5 C2 C1 117.8(5) . . ? O4 C2 O5 127.2(4) . . ? O4 C2 C1 114.9(4) . . ? O9 C025 H02A 109.5 . . ? O9 C025 H02B 109.5 . . ? O9 C025 H02C 109.5 . . ? H02A C025 H02B 109.5 . . ? H02A C025 H02C 109.5 . . ? H02B C025 H02C 109.5 . . ? C5 C6 H6A 109.5 . . ? C5 C6 H6B 109.5 . . ? C5 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C47 C46 H46A 108.9 . . ? C47 C46 H46B 108.9 . . ? C41 C46 C47 113.6(4) . . ? C41 C46 H46A 108.9 . . ? C41 C46 H46B 108.9 . . ? H46A C46 H46B 107.7 . . ? N2 C35 H35 118.5 . . ? N2 C35 C36 123.1(4) . . ? C36 C35 H35 118.5 . . ? C32 C36 H36 120.1 . . ? C35 C36 C32 119.7(4) . . ? C35 C36 H36 120.1 . . ? C65 C70 H70 119.0 . . ? C72 C70 C65 122.1(5) . . ? C72 C70 H70 119.0 . . ? O11 C44 H44A 109.5 . . ? O11 C44 H44B 109.5 . . ? O11 C44 H44C 109.5 . . ? H44A C44 H44B 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? O10 C49 H49A 109.5 . . ? O10 C49 H49B 109.5 . . ? O10 C49 H49C 109.5 . . ? H49A C49 H49B 109.5 . . ? H49A C49 H49C 109.5 . . ? H49B C49 H49C 109.5 . . ? C25 C73 H73A 109.0 . . ? C25 C73 H73B 109.0 . . ? C69 C73 C25 112.9(4) . . ? C69 C73 H73A 109.0 . . ? C69 C73 H73B 109.0 . . ? H73A C73 H73B 107.8 . . ? O8 C67 H67A 109.5 . . ? O8 C67 H67B 109.5 . . ? O8 C67 H67C 109.5 . . ? H67A C67 H67B 109.5 . . ? H67A C67 H67C 109.5 . . ? H67B C67 H67C 109.5 . . ? O6 C4 C3 117.1(4) . . ? O7 C4 O6 125.1(5) . . ? O7 C4 C3 117.8(5) . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? C4 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? O14 C60 H60A 109.5 . . ? O14 C60 H60B 109.5 . . ? O14 C60 H60C 109.5 . . ? H60A C60 H60B 109.5 . . ? H60A C60 H60C 109.5 . . ? H60B C60 H60C 109.5 . . ? O15 C68 H68A 109.5 . . ? O15 C68 H68B 109.5 . . ? O15 C68 H68C 109.5 . . ? H68A C68 H68B 109.5 . . ? H68A C68 H68C 109.5 . . ? H68B C68 H68C 109.5 . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? N1 C64 H64 118.1 . . ? O16 C64 N1 123.9(7) . . ? O16 C64 H64 118.1 . . ? O12 C45 H45A 109.5 . . ? O12 C45 H45B 109.5 . . ? O12 C45 H45C 109.5 . . ? H45A C45 H45B 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? O13 C54 H54A 109.5 . . ? O13 C54 H54B 109.5 . . ? O13 C54 H54C 109.5 . . ? H54A C54 H54B 109.5 . . ? H54A C54 H54C 109.5 . . ? H54B C54 H54C 109.5 . . ? N1 C62 H62A 109.5 . . ? N1 C62 H62B 109.5 . . ? N1 C62 H62C 109.5 . . ? H62A C62 H62B 109.5 . . ? H62A C62 H62C 109.5 . . ? H62B C62 H62C 109.5 . . ? N1 C63 H63A 109.5 . . ? N1 C63 H63B 109.5 . . ? N1 C63 H63C 109.5 . . ? H63A C63 H63B 109.5 . . ? H63A C63 H63C 109.5 . . ? H63B C63 H63C 109.5 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? N1 C64' H64A 109.5 . . ? N1 C64' H64B 109.5 . . ? N1 C64' H64C 109.4 . . ? H64A C64' H64B 109.5 . . ? H64A C64' H64C 109.4 . . ? H64B C64' H64C 109.4 . . ? N1 C63' H63' 119.5 . . ? O17 C63' N1 121.1(8) . . ? O17 C63' H63' 119.5 . . ? H18A O18 H18B 104.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 Cu2 2.6554(8) . ? Cu1 O2 1.943(3) . ? Cu1 O00A 2.008(4) . ? Cu1 O5 1.943(3) . ? Cu1 O7 2.005(4) . ? Cu1 N2 2.189(3) 1_756 ? Cu2 O1 1.995(3) . ? Cu2 O6 1.955(3) . ? Cu2 O4 1.984(4) . ? Cu2 O3 1.953(3) . ? Cu2 N3 2.175(3) . ? O9 C56 1.391(5) . ? O9 C025 1.430(5) . ? O14 C018 1.384(5) . ? O14 C60 1.425(6) . ? O1 C5 1.252(5) . ? O8 C71 1.379(5) . ? O8 C67 1.423(6) . ? O6 C4 1.264(6) . ? O10 C48 1.380(5) . ? O10 C49 1.413(6) . ? O2 C5 1.270(5) . ? O00A C7 1.250(6) . ? O5 C2 1.251(5) . ? O13 C51 1.376(6) . ? O13 C54 1.410(6) . ? O11 C43 1.367(5) . ? O11 C44 1.438(5) . ? O4 C2 1.251(6) . ? O3 C7 1.263(6) . ? O15 C72 1.375(5) . ? O15 C68 1.428(7) . ? O7 C4 1.256(6) . ? O12 C40 1.395(6) . ? O12 C45 1.433(6) . ? N3 C9 1.331(6) . ? N3 C13 1.324(6) . ? N2 C34 1.334(6) . ? N2 C35 1.325(6) . ? C11 C14 1.487(5) . ? C11 C12 1.395(6) . ? C11 C10 1.388(6) . ? C38 C37 1.520(6) . ? C38 C39 1.403(6) . ? C38 C43 1.409(6) . ? C20 C19 1.491(5) . ? C20 C25 1.393(6) . ? C20 C21 1.390(6) . ? C19 C16 1.385(6) . ? C19 C18 1.389(6) . ? C26 C23 1.498(5) . ? C26 C29 1.390(6) . ? C26 C27 1.390(6) . ? C23 C22 1.390(6) . ? C23 C24 1.397(6) . ? C14 C17 1.381(6) . ? C14 C15 1.392(6) . ? C12 H12 0.9500 . ? C12 C13 1.382(5) . ? C25 C24 1.398(5) . ? C25 C73 1.532(6) . ? C17 H17 0.9500 . ? C17 C18 1.393(5) . ? C58 C59 1.392(6) . ? C58 C61 1.533(6) . ? C58 C018 1.393(6) . ? C59 H59 0.9500 . ? C59 C56 1.391(6) . ? C22 C37 1.525(5) . ? C22 C21 1.396(5) . ? C53 H53 0.9500 . ? C53 C52 1.397(6) . ? C53 C48 1.388(6) . ? C52 C51 1.394(6) . ? C52 C55 1.525(6) . ? C9 H9 0.9500 . ? C9 C10 1.384(6) . ? C48 C47 1.399(6) . ? C10 H10 0.9500 . ? C51 C50 1.402(7) . ? C37 H37A 0.9900 . ? C37 H37B 0.9900 . ? C61 H61A 0.9900 . ? C61 H61B 0.9900 . ? C61 C65 1.517(6) . ? C5 C6 1.501(6) . ? C42 H42 0.9500 . ? C42 C43 1.392(7) . ? C42 C41 1.380(7) . ? C018 C57 1.389(6) . ? C69 C66 1.388(6) . ? C69 C72 1.392(7) . ? C69 C73 1.520(7) . ? C16 H16 0.9500 . ? C16 C15 1.387(6) . ? C39 H39 0.9500 . ? C39 C40 1.381(7) . ? C57 H57 0.9500 . ? C57 C01J 1.407(6) . ? C31 C30 1.383(6) . ? C31 C28 1.403(6) . ? C31 C32 1.491(5) . ? C15 H15 0.9500 . ? C21 H21 0.9500 . ? C66 H66 0.9500 . ? C66 C71 1.394(6) . ? C65 C71 1.388(7) . ? C65 C70 1.394(6) . ? C18 H18 0.9500 . ? C01J C55 1.512(6) . ? C01J C56 1.388(6) . ? C55 H55A 0.9900 . ? C55 H55B 0.9900 . ? C47 C50 1.394(7) . ? C47 C46 1.523(6) . ? C29 H29 0.9500 . ? C29 C30 1.397(6) . ? C27 H27 0.9500 . ? C27 C28 1.393(6) . ? N1 C64 1.373(8) . ? N1 C62 1.431(8) . ? N1 C63 1.406(7) . ? N1 C64' 1.373(8) . ? N1 C63' 1.406(7) . ? C30 H30 0.9500 . ? C24 H24 0.9500 . ? C13 H13 0.9500 . ? C28 H28 0.9500 . ? C34 H34 0.9500 . ? C34 C33 1.386(6) . ? C32 C33 1.391(6) . ? C32 C36 1.396(6) . ? C72 C70 1.390(7) . ? C40 C41 1.397(6) . ? C41 C46 1.514(7) . ? C7 C8 1.497(7) . ? C50 H50 0.9500 . ? C33 H33 0.9500 . ? C2 C1 1.441(8) . ? C025 H02A 0.9800 . ? C025 H02B 0.9800 . ? C025 H02C 0.9800 . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C46 H46A 0.9900 . ? C46 H46B 0.9900 . ? C35 H35 0.9500 . ? C35 C36 1.384(6) . ? C36 H36 0.9500 . ? C70 H70 0.9500 . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C49 H49A 0.9800 . ? C49 H49B 0.9800 . ? C49 H49C 0.9800 . ? C73 H73A 0.9900 . ? C73 H73B 0.9900 . ? C67 H67A 0.9800 . ? C67 H67B 0.9800 . ? C67 H67C 0.9800 . ? C4 C3 1.511(7) . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 H3C 0.9800 . ? C60 H60A 0.9800 . ? C60 H60B 0.9800 . ? C60 H60C 0.9800 . ? C68 H68A 0.9800 . ? C68 H68B 0.9800 . ? C68 H68C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? O16 C64 1.221(9) . ? C64 H64 0.9500 . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C54 H54A 0.9800 . ? C54 H54B 0.9800 . ? C54 H54C 0.9800 . ? C62 H62A 0.9800 . ? C62 H62B 0.9800 . ? C62 H62C 0.9800 . ? C63 H63A 0.9800 . ? C63 H63B 0.9800 . ? C63 H63C 0.9800 . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? O17 C63' 1.277(8) . ? C64' H64A 0.9796 . ? C64' H64B 0.9795 . ? C64' H64C 0.9808 . ? C63' H63' 0.9500 . ? O18 H18A 0.8701 . ? O18 H18B 0.8699 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 O2 C5 O1 -5.2(7) . . . . ? Cu1 O2 C5 C6 173.2(3) . . . . ? Cu1 O00A C7 O3 9.0(7) . . . . ? Cu1 O00A C7 C8 -168.3(4) . . . . ? Cu1 O5 C2 O4 0.1(8) . . . . ? Cu1 O5 C2 C1 178.4(4) . . . . ? Cu1 O7 C4 O6 4.4(7) . . . . ? Cu1 O7 C4 C3 -174.7(3) . . . . ? Cu1 N2 C34 C33 178.4(4) 1_354 . . . ? Cu1 N2 C35 C36 -178.3(4) 1_354 . . . ? Cu2 O1 C5 O2 8.8(7) . . . . ? Cu2 O1 C5 C6 -169.6(3) . . . . ? Cu2 O6 C4 O7 2.5(7) . . . . ? Cu2 O6 C4 C3 -178.4(3) . . . . ? Cu2 O4 C2 O5 3.1(7) . . . . ? Cu2 O4 C2 C1 -175.2(4) . . . . ? Cu2 O3 C7 O00A -7.3(7) . . . . ? Cu2 O3 C7 C8 170.1(4) . . . . ? Cu2 N3 C9 C10 -177.9(3) . . . . ? Cu2 N3 C13 C12 177.9(3) . . . . ? O14 C018 C57 C01J 177.7(4) . . . . ? O10 C48 C47 C50 -179.5(4) . . . . ? O10 C48 C47 C46 -0.7(6) . . . . ? O13 C51 C50 C47 179.0(4) . . . . ? O15 C72 C70 C65 -178.5(4) . . . . ? O12 C40 C41 C42 179.0(4) . . . . ? O12 C40 C41 C46 -0.9(6) . . . . ? N3 C9 C10 C11 0.6(7) . . . . ? N2 C34 C33 C32 0.0(8) . . . . ? N2 C35 C36 C32 -0.1(9) . . . . ? C11 C14 C17 C18 -179.1(4) . . . . ? C11 C14 C15 C16 179.7(4) . . . . ? C11 C12 C13 N3 -0.3(7) . . . . ? C38 C39 C40 O12 177.8(4) . . . . ? C38 C39 C40 C41 -0.1(6) . . . . ? C20 C19 C16 C15 -178.3(4) . . . . ? C20 C19 C18 C17 178.9(4) . . . . ? C20 C25 C24 C23 -0.3(7) . . . . ? C20 C25 C73 C69 124.4(5) . . . . ? C19 C20 C25 C24 -177.1(4) . . . . ? C19 C20 C25 C73 3.8(7) . . . . ? C19 C20 C21 C22 177.6(4) . . . . ? C19 C16 C15 C14 -0.5(7) . . . . ? C26 C23 C22 C37 4.1(7) . . . . ? C26 C23 C22 C21 -178.5(4) . . . . ? C26 C23 C24 C25 178.9(4) . . . . ? C26 C29 C30 C31 -0.2(7) . . . . ? C26 C27 C28 C31 -2.9(7) . . . . ? C23 C26 C29 C30 -179.2(4) . . . . ? C23 C26 C27 C28 -179.3(4) . . . . ? C23 C22 C37 C38 76.0(5) . . . . ? C23 C22 C21 C20 -0.7(7) . . . . ? C14 C11 C12 C13 179.9(4) . . . . ? C14 C11 C10 C9 180.0(4) . . . . ? C14 C17 C18 C19 -0.7(6) . . . . ? C12 C11 C14 C17 -35.7(6) . . . . ? C12 C11 C14 C15 144.2(4) . . . . ? C12 C11 C10 C9 -0.3(6) . . . . ? C25 C20 C19 C16 -106.3(5) . . . . ? C25 C20 C19 C18 74.5(6) . . . . ? C25 C20 C21 C22 -2.2(7) . . . . ? C17 C14 C15 C16 -0.5(7) . . . . ? C58 C59 C56 O9 177.1(4) . . . . ? C58 C59 C56 C01J -0.2(7) . . . . ? C58 C61 C65 C71 -104.5(5) . . . . ? C58 C61 C65 C70 76.4(5) . . . . ? C58 C018 C57 C01J -0.9(7) . . . . ? C59 C58 C61 C65 87.3(5) . . . . ? C59 C58 C018 O14 179.8(4) . . . . ? C59 C58 C018 C57 -1.5(6) . . . . ? C22 C23 C24 C25 -2.7(7) . . . . ? C53 C52 C51 O13 -177.6(4) . . . . ? C53 C52 C51 C50 1.9(7) . . . . ? C53 C52 C55 C01J 90.9(5) . . . . ? C53 C48 C47 C50 0.9(7) . . . . ? C53 C48 C47 C46 179.7(4) . . . . ? C52 C53 C48 O10 -179.0(4) . . . . ? C52 C53 C48 C47 0.5(7) . . . . ? C52 C51 C50 C47 -0.5(7) . . . . ? C9 N3 C13 C12 0.5(7) . . . . ? C48 C53 C52 C51 -2.0(6) . . . . ? C48 C53 C52 C55 -179.9(4) . . . . ? C48 C47 C50 C51 -0.9(7) . . . . ? C48 C47 C46 C41 -77.4(6) . . . . ? C10 C11 C14 C17 144.1(4) . . . . ? C10 C11 C14 C15 -36.0(6) . . . . ? C10 C11 C12 C13 0.2(6) . . . . ? C51 C52 C55 C01J -87.0(5) . . . . ? C37 C38 C39 C40 -173.5(4) . . . . ? C37 C38 C43 O11 -6.0(6) . . . . ? C37 C38 C43 C42 173.5(4) . . . . ? C37 C22 C21 C20 176.8(4) . . . . ? C61 C58 C59 C56 -176.4(4) . . . . ? C61 C58 C018 O14 -1.8(6) . . . . ? C61 C58 C018 C57 176.9(4) . . . . ? C61 C65 C71 O8 -1.3(6) . . . . ? C61 C65 C71 C66 177.9(4) . . . . ? C61 C65 C70 C72 -179.6(4) . . . . ? C42 C41 C46 C47 101.4(5) . . . . ? C018 C58 C59 C56 2.1(6) . . . . ? C018 C58 C61 C65 -91.1(5) . . . . ? C018 C57 C01J C55 -172.9(4) . . . . ? C018 C57 C01J C56 2.8(6) . . . . ? C69 C66 C71 O8 -179.8(4) . . . . ? C69 C66 C71 C65 1.0(6) . . . . ? C69 C72 C70 C65 2.5(7) . . . . ? C16 C19 C18 C17 -0.2(6) . . . . ? C39 C38 C37 C22 57.8(5) . . . . ? C39 C38 C43 O11 177.2(4) . . . . ? C39 C38 C43 C42 -3.4(6) . . . . ? C39 C40 C41 C42 -3.1(6) . . . . ? C39 C40 C41 C46 177.1(4) . . . . ? C57 C01J C55 C52 87.0(5) . . . . ? C57 C01J C56 O9 -179.7(4) . . . . ? C57 C01J C56 C59 -2.2(6) . . . . ? C31 C32 C33 C34 -175.7(5) . . . . ? C31 C32 C36 C35 175.8(5) . . . . ? C15 C14 C17 C18 1.1(6) . . . . ? C21 C20 C19 C16 73.8(5) . . . . ? C21 C20 C19 C18 -105.3(5) . . . . ? C21 C20 C25 C24 2.7(7) . . . . ? C21 C20 C25 C73 -176.3(4) . . . . ? C21 C22 C37 C38 -101.4(4) . . . . ? C66 C69 C72 O15 176.6(4) . . . . ? C66 C69 C72 C70 -4.3(6) . . . . ? C66 C69 C73 C25 92.7(5) . . . . ? C18 C19 C16 C15 0.8(7) . . . . ? C55 C52 C51 O13 0.4(6) . . . . ? C55 C52 C51 C50 179.9(4) . . . . ? C55 C01J C56 O9 -4.1(6) . . . . ? C55 C01J C56 C59 173.4(4) . . . . ? C29 C26 C23 C22 -100.1(5) . . . . ? C29 C26 C23 C24 78.3(6) . . . . ? C29 C26 C27 C28 2.2(7) . . . . ? C56 C01J C55 C52 -88.5(5) . . . . ? C71 C65 C70 C72 1.2(6) . . . . ? C27 C26 C23 C22 81.4(6) . . . . ? C27 C26 C23 C24 -100.2(5) . . . . ? C27 C26 C29 C30 -0.7(7) . . . . ? C30 C31 C28 C27 1.9(7) . . . . ? C30 C31 C32 C33 138.6(5) . . . . ? C30 C31 C32 C36 -39.3(7) . . . . ? C24 C23 C22 C37 -174.3(4) . . . . ? C24 C23 C22 C21 3.1(6) . . . . ? C24 C25 C73 C69 -54.7(6) . . . . ? C13 N3 C9 C10 -0.7(7) . . . . ? C28 C31 C30 C29 -0.4(7) . . . . ? C28 C31 C32 C33 -39.1(7) . . . . ? C28 C31 C32 C36 143.1(5) . . . . ? C43 C38 C37 C22 -118.9(4) . . . . ? C43 C38 C39 C40 3.3(6) . . . . ? C43 C42 C41 C40 3.0(6) . . . . ? C43 C42 C41 C46 -177.2(4) . . . . ? C34 N2 C35 C36 2.3(8) . . . . ? C32 C31 C30 C29 -178.1(4) . . . . ? C32 C31 C28 C27 179.5(4) . . . . ? C72 C69 C66 C71 2.7(6) . . . . ? C72 C69 C73 C25 -89.4(5) . . . . ? C40 C41 C46 C47 -78.7(5) . . . . ? C41 C42 C43 O11 179.7(4) . . . . ? C41 C42 C43 C38 0.3(6) . . . . ? C50 C47 C46 C41 101.4(5) . . . . ? C33 C32 C36 C35 -2.2(8) . . . . ? C025 O9 C56 C59 61.0(6) . . . . ? C025 O9 C56 C01J -121.5(4) . . . . ? C46 C47 C50 C51 -179.8(4) . . . . ? C35 N2 C34 C33 -2.3(8) . . . . ? C36 C32 C33 C34 2.2(7) . . . . ? C70 C65 C71 O8 177.8(4) . . . . ? C70 C65 C71 C66 -2.9(6) . . . . ? C44 O11 C43 C38 178.1(4) . . . . ? C44 O11 C43 C42 -1.4(6) . . . . ? C49 O10 C48 C53 6.1(6) . . . . ? C49 O10 C48 C47 -173.5(4) . . . . ? C73 C25 C24 C23 178.8(5) . . . . ? C73 C69 C66 C71 -179.4(4) . . . . ? C73 C69 C72 O15 -1.4(6) . . . . ? C73 C69 C72 C70 177.7(4) . . . . ? C67 O8 C71 C66 15.2(6) . . . . ? C67 O8 C71 C65 -165.6(4) . . . . ? C60 O14 C018 C58 -165.1(4) . . . . ? C60 O14 C018 C57 16.2(6) . . . . ? C68 O15 C72 C69 -170.8(4) . . . . ? C68 O15 C72 C70 10.2(7) . . . . ? C45 O12 C40 C39 24.5(7) . . . . ? C45 O12 C40 C41 -157.5(5) . . . . ? C54 O13 C51 C52 -175.0(5) . . . . ? C54 O13 C51 C50 5.5(7) . . . . ? C62 N1 C64 O16 172.7(7) . . . . ? C62 N1 C63' O17 171.1(8) . . . . ? C63 N1 C64 O16 -8.4(11) . . . . ? C64' N1 C63' O17 -7.8(11) . . . . ?