#------------------------------------------------------------------------------ #$Date: 2024-07-09 01:18:42 +0300 (Tue, 09 Jul 2024) $ #$Revision: 293306 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/20/1572090.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572090 loop_ _publ_author_name 'Chen, Zhao-Nian' 'Zhang, Le-Ping' 'Wu, Huai-Li' 'Qi, Qiao-Yan' 'Yan, Meng' 'Tian, Jia' 'Yang, Guanyu' 'Li, Zhan-Ting' 'Yang, Bo' _publ_section_title ; Accurate Construction of Monolayer, Bilayer, Sandwich Bilayer, Four-layer, Multi-layer and Chiral Bilayer 2D Pillararene-Type Supramolecular Networks ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC03022B _journal_year 2024 _chemical_formula_moiety 'C85 H72 Co N5 O10, C3 H7 N O, 1(N1 O3), 4[C3H7NO], 1[H2O]' _chemical_formula_sum 'C100 H109 Co N11 O19' _chemical_formula_weight 1827.91 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2024-06-18 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-06-25 deposited with the CCDC. 2024-07-04 downloaded from the CCDC. ; _cell_angle_alpha 112.3290(10) _cell_angle_beta 103.5880(10) _cell_angle_gamma 92.9400(10) _cell_formula_units_Z 2 _cell_length_a 13.9766(5) _cell_length_b 18.8234(8) _cell_length_c 24.3526(9) _cell_measurement_reflns_used 8287 _cell_measurement_temperature 193.00 _cell_measurement_theta_max 25.18 _cell_measurement_theta_min 2.36 _cell_volume 5689.8(4) _computing_cell_refinement 'SAINT V8.40B (Bruker, 2019)' _computing_data_collection 'APEX4 V2022.1-1 (Bruker, 2022)' _computing_data_reduction 'SAINT V8.40B (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 193.00 _diffrn_detector CPAD _diffrn_detector_area_resol_mean 7.41 _diffrn_detector_type 'Bruker PHOTON II' _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE TXS PHOTON II' _diffrn_measurement_method '\w and \f shutterless scans' _diffrn_measurement_specimen_support 'nylon loop' _diffrn_radiation_monochromator 'Helios Multi-layer Optic' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0667 _diffrn_reflns_av_unetI/netI 0.1122 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.991 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 44378 _diffrn_reflns_point_group_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.379 _diffrn_reflns_theta_min 1.772 _diffrn_source TXS _diffrn_source_current 40.0 _diffrn_source_power 2.0 _diffrn_source_type 'Rotaing Anode' _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.213 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.6690 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0897 before and 0.0610 after correction. The Ratio of minimum to maximum transmission is 0.8977. The \l/2 correction factor is Not present. ; _exptl_crystal_colour pink _exptl_crystal_colour_primary pink _exptl_crystal_density_diffrn 1.067 _exptl_crystal_description block _exptl_crystal_F_000 1930 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.945 _refine_diff_density_min -0.508 _refine_diff_density_rms 0.072 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.022 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1134 _refine_ls_number_reflns 20744 _refine_ls_number_restraints 238 _refine_ls_restrained_S_all 1.030 _refine_ls_R_factor_all 0.1353 _refine_ls_R_factor_gt 0.0845 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1359P)^2^+1.7927P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2301 _refine_ls_wR_factor_ref 0.2653 _reflns_Friedel_coverage 0.000 _reflns_number_gt 11900 _reflns_number_total 20744 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03022b2.cif _cod_data_source_block 230106_wqangz_038351_0m _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_radiation_probe' value 'X-ray' was changed to 'x-ray' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas ; _cod_database_code 1572090 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.979 _shelx_estimated_absorpt_t_min 0.973 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H,H) groups 2. Restrained distances N6-O13 = N6-O14 1.25 with sigma of 0.02 N6-O12 1.24 with sigma of 0.02 N6A-O13A = N6A-O12A 1.25 with sigma of 0.02 N6A-O14A 1.24 with sigma of 0.02 O9A-C59A \\sim O9-C59 \\sim O10A-C60A \\sim O10-C60 with sigma of 0.02 O13A-O14A \\sim O14A-O12A \\sim O12A-O13A with sigma of 0.04 N6-O13 \\sim N6-O12 \\sim N6-O14 with sigma of 0.02 O13-O12 \\sim O12-O14 \\sim O14-O13 with sigma of 0.04 N6A-O13A \\sim N6A-O14A \\sim N6A-O12A with sigma of 0.02 O3A-N5 \\sim O3B-N5 with sigma of 0.02 3. Restrained planarity O12A, O13A, O14A, N6A with sigma of 0.1 O12, O13, O14, N6 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints O9 \\sim O9A \\sim O10 \\sim O10A \\sim C59 \\sim C59A \\sim C60 \\sim C60A: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 within 2A O12A \\sim O13A \\sim N6A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A O12 \\sim O13 \\sim O14 \\sim N6: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A O12 \\sim O13 \\sim O14 \\sim N6 \\sim O14A \\sim O12A \\sim O13A \\sim N6A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A C45 \\sim C45A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A O12A \\sim O14A \\sim N6A \\sim O13A \\sim N6B \\sim O13B \\sim O14B \\sim O12B: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A O3A \\sim O3B: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A Uanis(O13A) \\sim Ueq, Uanis(N6A) \\sim Ueq, Uanis(O14A) \\sim Ueq, Uanis(O12A) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04 5. Rigid body (RIGU) restrains O12, O13, O14, N6 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 O12A, O13A, N6A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Same fragment restrains {O13B, O14B, O12B, N6B} sigma for 1-2: 0.02, 1-3: 0.02 as in {O14A, O12A, O13A, N6A} 7. Others 1*[Sof(O12)+Sof(O13)+Sof(O14)+Sof(N6)]+1*[Sof(O14A)+Sof(O12A)+Sof(O13A)+ Sof(N6A)]+1*[Sof(O13B)+Sof(O14B)+Sof(O12B)+Sof(N6B)]=1 with esd of 0 Sof(O9)=Sof(O10)=Sof(H54)=Sof(H57)=Sof(C59)=Sof(H59A)=Sof(H59B)=Sof(H59C)= Sof(C60)=Sof(H60A)=Sof(H60B)=Sof(H60C)=1-FVAR(1) Sof(O9A)=Sof(O10A)=Sof(H55)=Sof(H58)=Sof(C59A)=Sof(H59D)=Sof(H59E)=Sof(H59F)= Sof(C60A)=Sof(H60D)=Sof(H60E)=Sof(H60F)=FVAR(1) Sof(O12)=Sof(O13)=Sof(O14)=Sof(N6)=FVAR(2) Sof(C45A)=Sof(H45D)=Sof(H45E)=Sof(H45F)=1-FVAR(3) Sof(C45)=Sof(H45A)=Sof(H45B)=Sof(H45C)=FVAR(3) Sof(O14A)=Sof(O12A)=Sof(O13A)=Sof(N6A)=FVAR(4) Sof(O13B)=Sof(O14B)=Sof(O12B)=Sof(N6B)=FVAR(5) Sof(O3B)=1-FVAR(6) Sof(O3A)=FVAR(6) 8.a Riding coordinates: C59(H59A,H59B,H59C) 8.b Rotating group: O4(H4A,H4B) 8.c Secondary CH2 refined with riding coordinates: C29(H29A,H29B), C38(H38A,H38B), C47(H47A,H47B), C52(H52A,H52B), C61(H61A,H61B) 8.d Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C4(H4), C5(H5), C7(H7), C8(H8), C10(H10), C11(H11), C14(H14), C17(H17), C19(H19), C20(H20), C22(H22), C23(H23), C25(H25), C26(H26), C27(H27), C28(H28), C31(H31), C34(H34), C40(H40), C43(H43), C49(H49), C54(H54), C55(H55), C57(H57), C58(H58), C62(H62), C65(H65), C66(H66), C68(H68), C69(H69), C71(H71), C72(H72), C73(H73), C74(H74), C76(H76), C77(H77), C79(H79), C80(H80), C82(H82), C83(H83), C84(H84), C85(H85), C88(H88) 8.e Idealised Me refined as rotating group: C36(H36A,H36B,H36C), C37(H37A,H37B,H37C), C45(H45A,H45B,H45C), C45A(H45D,H45E, H45F), C46(H46A,H46B,H46C), C59A(H59D,H59E,H59F), C60(H60A,H60B,H60C), C60A(H60D,H60E,H60F), C86(H86A,H86B,H86C), C87(H87A,H87B,H87C) ; _smtbx_masks_special_details ; A solvent mask was calculated and 348 electrons were found in a volume of 2244\%A^3^ in 2 voids per unit cell. This is consistent with the presence of 4[C3H7NO], 1[H2O] per formula unit which account for 340 electrons per unit cell. ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL 230106_wqangz_038351_0m_a.res in P-1 230106_wqangz_038351_0m.res created by SHELXL-2019/3 at 20:40:20 on 18-Jun-2024 REM Old TITL 230106_WQANGZ_038351_0m in P-1 REM SHELXT solution in P-1: R1 0.272, Rweak 0.042, Alpha 0.095 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C89 N6 O13A Co CELL 0.71073 13.9766 18.8234 24.3526 112.329 103.588 92.94 ZERR 2 0.0005 0.0008 0.0009 0.001 0.001 0.001 LATT 1 SFAC C H Co N O UNIT 200 218 2 22 38 DFIX 1.25 N6 O13 N6 O14 SADI O9A C59A O9 C59 O10A C60A O10 C60 RIGU O12 > N6 SIMU 0.005 0.01 2 O9 > O10A C59 > C60A DFIX 1.24 N6 O12 DFIX 1.25 N6A O13A N6A O12A SIMU O12A > N6A FLAT O12A O13A O14A N6A SADI 0.04 O13A O14A O14A O12A O12A O13A RIGU O12A > N6A FLAT O12 O13 O14 N6 DFIX 1.24 N6A O14A SIMU O12 > N6 SADI N6 O13 N6 O12 N6 O14 SADI 0.04 O13 O12 O12 O14 O14 O13 SADI N6A O13A N6A O14A N6A O12A SIMU 0.01 0.02 2 O12 > N6A ISOR 0.02 0.04 O13A N6A O14A O12A SIMU 0.01 0.02 2 C45 C45A SIMU 0.01 0.02 2 O12A O14A N6A O13A N6B O13B O14B O12B SADI O3A N5 O3B N5 SIMU 0.01 0.02 2 O3A O3B SUMP 1 0 1 3 1 5 1 6 L.S. 10 0 0 PLAN 20 SIZE 0.1 0.12 0.13 TEMP -80.15 CONF BOND list 4 MORE -1 ABIN BOND $H fmap 2 53 acta OMIT -4 5 5 OMIT -3 5 1 OMIT -2 -1 2 OMIT -1 0 2 OMIT 0 3 0 OMIT 1 -2 1 OMIT 1 0 1 OMIT 1 0 2 OMIT 2 -3 1 OMIT 2 0 1 OMIT 3 -1 1 REM REM REM WGHT 0.135900 1.792700 FVAR 0.31251 0.55374 0.43560 0.69945 0.41789 0.14653 0.28615 CO1 3 0.933212 0.765001 -0.132810 11.00000 0.04550 0.03685 = 0.02364 0.01767 0.01428 0.01758 O1 5 1.066705 0.849007 -0.082423 11.00000 0.04955 0.04542 = 0.03153 0.02124 0.01040 0.01684 O2 5 1.081124 0.957588 -0.092359 11.00000 0.06967 0.05390 = 0.06495 0.03438 0.01878 0.01685 PART 2 O3B 5 1.177101 0.875951 -0.123170 -71.00000 0.09686 0.06207 = 0.10790 0.04452 0.07431 0.02866 PART 0 O4 5 0.804741 0.680763 -0.178393 11.00000 0.07432 0.04923 = 0.03867 0.01721 0.01891 0.02299 AFIX 7 H4A 2 0.758583 0.695160 -0.159650 11.00000 -1.50000 H4B 2 0.817272 0.637851 -0.174296 11.00000 -1.50000 AFIX 0 O5 5 0.672002 0.949605 0.266130 11.00000 0.06745 0.06888 = 0.03461 0.02034 0.01817 -0.00074 O6 5 0.655547 0.871840 0.021284 11.00000 0.05828 0.05562 = 0.03320 0.02273 0.01370 0.00371 O7 5 0.955273 0.967780 0.421221 11.00000 0.08662 0.07561 = 0.03198 0.02289 0.01858 0.00622 O8 5 0.972682 0.975850 0.199793 11.00000 0.06188 0.06115 = 0.03464 0.03019 0.01667 0.01008 PART 1 O9 5 0.482793 0.726402 0.254408 -21.00000 0.23835 0.05363 = 0.06932 0.02988 0.02980 0.05934 PART 2 O9A 5 0.662912 0.771253 0.347156 21.00000 0.12630 0.05008 = 0.06735 0.02315 0.01547 0.00736 PART 1 O10 5 0.695745 0.499975 0.286889 -21.00000 0.08119 0.11192 = 0.07498 0.05189 0.00488 0.04277 PART 2 O10A 5 0.522311 0.463707 0.195008 21.00000 0.07964 0.04572 = 0.06534 0.02778 0.00976 0.02445 PART 0 N1 4 0.932043 0.764136 -0.044377 11.00000 0.04364 0.04160 = 0.02758 0.01887 0.01359 0.01541 N2 4 0.938005 0.764983 0.779155 11.00000 0.04942 0.03710 = 0.02734 0.01853 0.01410 0.01791 N3 4 0.969608 0.322030 0.142885 11.00000 0.04927 0.04086 = 0.03093 0.02029 0.02163 0.01747 N4 4 0.148927 1.138634 0.117607 11.00000 0.04565 0.04249 = 0.02836 0.01907 0.01417 0.01981 N5 4 1.107929 0.893749 -0.097262 11.00000 0.04776 0.03957 = 0.03222 0.00889 0.00986 0.01445 C1 1 0.847094 0.761353 -0.028190 11.00000 0.04155 0.05259 = 0.03048 0.02279 0.01410 0.02026 AFIX 43 H1 2 0.786925 0.761784 -0.055971 11.00000 -1.20000 AFIX 0 C2 1 0.842578 0.757904 0.026576 11.00000 0.05074 0.05345 = 0.03158 0.02157 0.02194 0.01732 AFIX 43 H2 2 0.780134 0.755757 0.035488 11.00000 -1.20000 AFIX 0 C3 1 0.927980 0.757530 0.068785 11.00000 0.04787 0.04334 = 0.02260 0.01930 0.01146 0.01758 C4 1 1.015733 0.759590 0.051043 11.00000 0.04886 0.05708 = 0.03202 0.02556 0.01231 0.01965 AFIX 43 H4 2 1.076914 0.758597 0.077677 11.00000 -1.20000 AFIX 0 C5 1 1.014760 0.763006 -0.003972 11.00000 0.04609 0.05387 = 0.02727 0.02241 0.01469 0.02152 AFIX 43 H5 2 1.076148 0.764675 -0.014187 11.00000 -1.20000 AFIX 0 C6 1 0.924823 0.755196 0.128816 11.00000 0.05217 0.04377 = 0.02574 0.01903 0.01186 0.00954 C7 1 0.854134 0.785924 0.158059 11.00000 0.04683 0.04809 = 0.02690 0.02053 0.01290 0.00897 AFIX 43 H7 2 0.803442 0.807152 0.138549 11.00000 -1.20000 AFIX 0 C8 1 0.855181 0.786609 0.214865 11.00000 0.05045 0.04869 = 0.02830 0.01882 0.01412 0.00507 AFIX 43 H8 2 0.805028 0.807879 0.233706 11.00000 -1.20000 AFIX 0 C9 1 0.928001 0.756859 0.244921 11.00000 0.06565 0.04392 = 0.02556 0.01702 0.01321 0.00313 C10 1 0.999331 0.723665 0.215906 11.00000 0.06277 0.07127 = 0.03806 0.03406 0.01206 0.01799 AFIX 43 H10 2 1.048852 0.701665 0.235496 11.00000 -1.20000 AFIX 0 C11 1 0.998213 0.722674 0.158903 11.00000 0.06358 0.06302 = 0.03509 0.02796 0.02590 0.02922 AFIX 43 H11 2 1.047145 0.699952 0.139487 11.00000 -1.20000 AFIX 0 C12 1 0.932265 0.760477 0.308307 11.00000 0.06482 0.04713 = 0.02794 0.02163 0.01642 0.00985 C13 1 1.004580 0.810459 0.361118 11.00000 0.06091 0.05832 = 0.03102 0.02556 0.01261 0.00600 C14 1 1.003652 0.806293 0.417145 11.00000 0.06259 0.05725 = 0.02612 0.02090 0.00852 0.00717 AFIX 43 H14 2 1.053745 0.839012 0.453458 11.00000 -1.20000 AFIX 0 C15 1 0.932138 0.756034 0.421837 11.00000 0.06493 0.05738 = 0.03103 0.02475 0.01387 0.00863 C16 1 0.856880 0.709413 0.369151 11.00000 0.06464 0.05838 = 0.02756 0.02158 0.00973 0.00166 C17 1 0.859867 0.711956 0.313741 11.00000 0.07297 0.06020 = 0.02834 0.02200 0.00961 0.00294 AFIX 43 H17 2 0.809983 0.678917 0.277441 11.00000 -1.20000 AFIX 0 C18 1 0.934805 0.757183 0.484148 11.00000 0.06455 0.05655 = 0.02356 0.01883 0.01184 0.00394 C19 1 0.934209 0.825857 0.532832 11.00000 0.09631 0.04963 = 0.03103 0.02245 0.01932 0.00568 AFIX 43 H19 2 0.933606 0.872825 0.526785 11.00000 -1.20000 AFIX 0 C20 1 0.934475 0.827356 0.590329 11.00000 0.09419 0.04533 = 0.02315 0.01619 0.01412 0.00135 AFIX 43 H20 2 0.932613 0.874907 0.622851 11.00000 -1.20000 AFIX 0 C21 1 0.937484 0.758890 0.600571 11.00000 0.06057 0.04733 = 0.02891 0.02109 0.01297 0.00703 C22 1 0.940520 0.690679 0.551895 11.00000 0.09369 0.05007 = 0.03440 0.02602 0.02932 0.02294 AFIX 43 H22 2 0.944227 0.643904 0.558086 11.00000 -1.20000 AFIX 0 C23 1 0.938246 0.689771 0.494832 11.00000 0.08856 0.04954 = 0.03270 0.01876 0.02035 0.01794 AFIX 43 H23 2 0.939043 0.642111 0.462085 11.00000 -1.20000 AFIX 0 C24 1 0.939117 0.760466 0.662520 11.00000 0.05683 0.04029 = 0.02375 0.01360 0.01057 0.00722 C25 1 0.923948 0.692911 0.671788 11.00000 0.11219 0.04361 = 0.03202 0.01859 0.02829 0.01413 AFIX 43 H25 2 0.913525 0.643538 0.638391 11.00000 -1.20000 AFIX 0 C26 1 0.924105 0.697919 0.729762 11.00000 0.09564 0.04545 = 0.03331 0.02585 0.02930 0.02076 AFIX 43 H26 2 0.913704 0.650861 0.734964 11.00000 -1.20000 AFIX 0 C27 1 0.951530 0.829738 0.770032 11.00000 0.05620 0.03450 = 0.02606 0.01141 0.01076 0.01046 AFIX 43 H27 2 0.961997 0.878329 0.804262 11.00000 -1.20000 AFIX 0 C28 1 0.951101 0.829769 0.713587 11.00000 0.06443 0.04201 = 0.02738 0.02139 0.01299 0.00632 AFIX 43 H28 2 0.959098 0.877772 0.709481 11.00000 -1.20000 AFIX 0 C29 1 1.077623 0.872925 0.360762 11.00000 0.05912 0.06803 = 0.03652 0.02996 0.00877 0.00433 AFIX 23 H29A 2 1.120847 0.902902 0.403203 11.00000 -1.20000 H29B 2 1.120704 0.847978 0.334288 11.00000 -1.20000 AFIX 0 C30 1 1.023802 0.927796 0.336983 11.00000 0.05158 0.05142 = 0.03158 0.01995 0.00473 -0.00417 C31 1 1.033327 0.933920 0.283294 11.00000 0.05122 0.04845 = 0.03527 0.02115 0.01086 0.00103 AFIX 43 H31 2 1.084894 0.912344 0.266093 11.00000 -1.20000 AFIX 0 C32 1 0.969749 0.970510 0.254592 11.00000 0.05306 0.04354 = 0.03321 0.01874 0.01339 -0.00021 C33 1 0.894527 1.004104 0.278500 11.00000 0.06447 0.03819 = 0.03475 0.01761 0.01231 0.00048 C34 1 0.890087 1.002900 0.335862 11.00000 0.05668 0.05009 = 0.03570 0.01495 0.01288 0.00041 AFIX 43 H34 2 0.841437 1.027364 0.354675 11.00000 -1.20000 AFIX 0 C35 1 0.954146 0.967397 0.364363 11.00000 0.06058 0.05209 = 0.03393 0.02147 0.01265 0.00294 C36 1 1.056158 0.953501 0.177704 11.00000 0.06592 0.06657 = 0.04784 0.03323 0.02186 0.00789 AFIX 137 H36A 2 1.050971 0.961912 0.139858 11.00000 -1.50000 H36B 2 1.058050 0.898348 0.168850 11.00000 -1.50000 H36C 2 1.117287 0.984761 0.209099 11.00000 -1.50000 AFIX 0 C37 1 0.865492 0.972924 0.438151 11.00000 0.10554 0.14485 = 0.06803 0.06044 0.04786 0.02847 AFIX 137 H37A 2 0.816814 0.926532 0.410003 11.00000 -1.50000 H37B 2 0.839391 1.019309 0.435742 11.00000 -1.50000 H37C 2 0.877729 0.976514 0.480500 11.00000 -1.50000 AFIX 0 C38 1 0.816467 1.036126 0.243738 11.00000 0.06351 0.05075 = 0.04059 0.02315 0.01778 0.00838 AFIX 23 H38A 2 0.849369 1.067217 0.226497 11.00000 -1.20000 H38B 2 0.783299 1.071078 0.272793 11.00000 -1.20000 AFIX 0 C39 1 0.738674 0.972060 0.191726 11.00000 0.05324 0.03788 = 0.03802 0.01372 0.01232 0.00510 C40 1 0.735109 0.952336 0.130216 11.00000 0.04688 0.04697 = 0.03810 0.02667 0.01611 0.00965 AFIX 43 H40 2 0.780871 0.981032 0.120057 11.00000 -1.20000 AFIX 0 C41 1 0.666724 0.892155 0.083759 11.00000 0.04539 0.04445 = 0.02979 0.02073 0.00938 0.01217 C42 1 0.601313 0.845764 0.096400 11.00000 0.04141 0.04330 = 0.03732 0.02397 0.01661 0.02006 C43 1 0.605185 0.865091 0.157501 11.00000 0.05177 0.04197 = 0.03905 0.01711 0.01877 0.00698 AFIX 43 H43 2 0.561934 0.834208 0.167473 11.00000 -1.20000 AFIX 0 C44 1 0.669558 0.927567 0.204462 11.00000 0.05631 0.05834 = 0.03276 0.02132 0.01961 0.01449 PART 1 C45 1 0.585340 0.985536 0.279364 41.00000 0.12863 0.10211 = 0.06572 0.02843 0.05193 0.04351 AFIX 137 H45A 2 0.593777 1.038579 0.281425 41.00000 -1.50000 H45B 2 0.578816 0.987135 0.318999 41.00000 -1.50000 H45C 2 0.525238 0.955018 0.246554 41.00000 -1.50000 AFIX 0 PART 3 C45A 1 0.614132 0.901448 0.282048 -41.00000 0.09938 0.10138 = 0.05690 0.04398 0.04651 0.02340 AFIX 137 H45D 2 0.543365 0.902925 0.266105 -41.00000 -1.50000 H45E 2 0.631276 0.919771 0.327097 -41.00000 -1.50000 H45F 2 0.627302 0.847985 0.264071 -41.00000 -1.50000 AFIX 0 PART 0 C46 1 0.717265 0.918675 0.004932 11.00000 0.07721 0.06679 = 0.04521 0.03161 0.02250 0.00828 AFIX 137 H46A 2 0.704865 0.897085 -0.040049 11.00000 -1.50000 H46B 2 0.787421 0.919326 0.024235 11.00000 -1.50000 H46C 2 0.701960 0.971828 0.019362 11.00000 -1.50000 AFIX 0 C47 1 0.530548 0.776969 0.043403 11.00000 0.04237 0.04340 = 0.03572 0.01929 0.01563 0.01805 AFIX 23 H47A 2 0.473991 0.796167 0.023155 11.00000 -1.20000 H47B 2 0.566020 0.750491 0.012383 11.00000 -1.20000 AFIX 0 C48 1 0.491142 0.719574 0.065124 11.00000 0.04075 0.03701 = 0.03147 0.01268 0.00688 0.01241 C49 1 0.549773 0.663874 0.071152 11.00000 0.04341 0.03594 = 0.03449 0.01288 0.01202 0.01506 AFIX 43 H49 2 0.606154 0.659062 0.055277 11.00000 -1.20000 AFIX 0 C50 1 0.529970 0.615093 0.099167 11.00000 0.04671 0.03639 = 0.03351 0.01455 0.00513 0.01370 C51 1 0.446109 0.620577 0.122384 11.00000 0.04482 0.03043 = 0.04062 0.01650 0.00691 0.01086 C52 1 0.426551 0.575974 0.159646 11.00000 0.05209 0.04455 = 0.06069 0.02719 0.01834 0.00642 AFIX 23 H52A 2 0.418185 0.519534 0.134116 11.00000 -1.20000 H52B 2 0.363741 0.587377 0.170930 11.00000 -1.20000 AFIX 0 C53 1 0.510566 0.596848 0.217716 11.00000 0.05317 0.04262 = 0.04261 0.02285 0.01439 0.00883 C54 1 0.559910 0.540337 0.230172 11.00000 0.05876 0.04775 = 0.05301 0.02493 0.01712 0.00903 PART 1 AFIX 43 H54 2 0.536653 0.487179 0.203484 -21.00000 -1.20000 AFIX 0 PART 0 C55 1 0.642414 0.559456 0.280638 11.00000 0.06078 0.06534 = 0.04922 0.03396 0.01788 0.01246 PART 2 AFIX 43 H55 2 0.674997 0.519571 0.288019 21.00000 -1.20000 AFIX 0 PART 0 C56 1 0.677822 0.637557 0.320788 11.00000 0.07289 0.06873 = 0.04386 0.03504 0.01384 -0.00734 C57 1 0.627275 0.694130 0.309606 11.00000 0.09671 0.04993 = 0.04724 0.02042 0.00884 -0.00014 PART 1 AFIX 43 H57 2 0.649462 0.747324 0.336539 -21.00000 -1.20000 AFIX 0 PART 0 C58 1 0.544536 0.673508 0.259340 11.00000 0.08080 0.04110 = 0.05596 0.02209 0.01614 0.01135 PART 2 AFIX 43 H58 2 0.509828 0.713108 0.253103 21.00000 -1.20000 AFIX 0 PART 1 C59 1 0.431933 0.778222 0.298590 -21.00000 0.28174 0.10320 = 0.11797 0.01318 0.01664 0.04777 AFIX 3 H59A 2 0.448943 0.772752 0.338030 -21.00000 -1.50000 H59B 2 0.362763 0.754002 0.275860 -21.00000 -1.50000 H59C 2 0.439573 0.833552 0.306330 -21.00000 -1.50000 AFIX 0 PART 2 C59A 1 0.622352 0.824514 0.320702 21.00000 0.18413 0.06126 = 0.12975 0.00617 0.00876 0.01192 AFIX 137 H59D 2 0.639827 0.814030 0.281962 21.00000 -1.50000 H59E 2 0.650253 0.878182 0.349790 21.00000 -1.50000 H59F 2 0.549671 0.817189 0.312546 21.00000 -1.50000 AFIX 0 PART 1 C60 1 0.651227 0.419258 0.250081 -21.00000 0.10346 0.09312 = 0.08100 0.04182 0.00092 0.03794 AFIX 137 H60A 2 0.653122 0.405240 0.207303 -21.00000 -1.50000 H60B 2 0.581891 0.412058 0.251228 -21.00000 -1.50000 H60C 2 0.688601 0.385958 0.266851 -21.00000 -1.50000 AFIX 0 PART 2 C60A 1 0.577193 0.404628 0.206613 21.00000 0.11063 0.06095 = 0.07678 0.03240 0.00376 0.02822 AFIX 137 H60D 2 0.551646 0.354241 0.171670 21.00000 -1.50000 H60E 2 0.568686 0.401065 0.244347 21.00000 -1.50000 H60F 2 0.648105 0.418903 0.211615 21.00000 -1.50000 AFIX 0 PART 0 C61 1 0.771641 0.659113 0.373866 11.00000 0.08423 0.09424 = 0.05124 0.04671 0.00109 -0.01880 AFIX 23 H61A 2 0.794797 0.610816 0.375209 11.00000 -1.20000 H61B 2 0.755217 0.687616 0.413113 11.00000 -1.20000 AFIX 0 C62 1 0.386931 0.675290 0.115273 11.00000 0.04174 0.04064 = 0.04813 0.01653 0.01344 0.01213 AFIX 43 H62 2 0.329137 0.678519 0.129729 11.00000 -1.20000 AFIX 0 C63 1 0.406734 0.725547 0.088425 11.00000 0.03675 0.03902 = 0.03037 0.01522 0.00945 0.01065 C64 1 0.349384 0.789751 0.090146 11.00000 0.04398 0.04212 = 0.03876 0.02010 0.01446 0.01565 C65 1 0.307247 0.803539 0.037988 11.00000 0.04578 0.04200 = 0.03696 0.01482 0.00784 0.01734 AFIX 43 H65 2 0.306366 0.766525 -0.001728 11.00000 -1.20000 AFIX 0 C66 1 0.266524 0.870893 0.043518 11.00000 0.04315 0.04980 = 0.03085 0.02138 0.00923 0.02198 AFIX 43 H66 2 0.238272 0.879073 0.007320 11.00000 -1.20000 AFIX 0 C67 1 0.266037 0.926959 0.100980 11.00000 0.04042 0.04628 = 0.03883 0.02283 0.01354 0.01636 C68 1 0.302892 0.910644 0.152274 11.00000 0.05331 0.05058 = 0.03479 0.02489 0.01746 0.02800 AFIX 43 H68 2 0.300231 0.946284 0.191680 11.00000 -1.20000 AFIX 0 C69 1 0.343352 0.843814 0.147389 11.00000 0.05369 0.04979 = 0.03883 0.02732 0.01393 0.02374 AFIX 43 H69 2 0.367533 0.834244 0.183394 11.00000 -1.20000 AFIX 0 C70 1 0.227841 0.999721 0.106113 11.00000 0.03847 0.04470 = 0.03233 0.02313 0.01596 0.01740 C71 1 0.149974 1.003549 0.060250 11.00000 0.05006 0.03746 = 0.03055 0.01900 0.01764 0.02001 AFIX 43 H71 2 0.121250 0.958222 0.023648 11.00000 -1.20000 AFIX 0 C72 1 0.114262 1.072052 0.067326 11.00000 0.04018 0.04652 = 0.02745 0.02183 0.01069 0.01614 AFIX 43 H72 2 0.061759 1.072369 0.034614 11.00000 -1.20000 AFIX 0 C73 1 0.226791 1.136200 0.161969 11.00000 0.04634 0.04199 = 0.03338 0.01435 0.00850 0.01416 AFIX 43 H73 2 0.255405 1.182631 0.197644 11.00000 -1.20000 AFIX 0 C74 1 0.266402 1.068433 0.157304 11.00000 0.04636 0.05446 = 0.03309 0.02246 0.00644 0.02172 AFIX 43 H74 2 0.320580 1.069499 0.189721 11.00000 -1.20000 AFIX 0 C75 1 0.603034 0.562362 0.106610 11.00000 0.04958 0.03593 = 0.03067 0.01277 0.01066 0.01776 C76 1 0.580322 0.482091 0.080395 11.00000 0.04858 0.03748 = 0.03955 0.00979 0.00556 0.01325 AFIX 43 H76 2 0.514237 0.457871 0.056472 11.00000 -1.20000 AFIX 0 C77 1 0.652412 0.436655 0.088519 11.00000 0.05867 0.02899 = 0.04468 0.01084 0.01088 0.01302 AFIX 43 H77 2 0.634593 0.381684 0.070545 11.00000 -1.20000 AFIX 0 C78 1 0.750540 0.469519 0.122420 11.00000 0.04848 0.03407 = 0.03597 0.01682 0.01113 0.01360 C79 1 0.774324 0.550570 0.148436 11.00000 0.04139 0.03619 = 0.03419 0.01474 0.00404 0.01205 AFIX 43 H79 2 0.840632 0.574414 0.172124 11.00000 -1.20000 AFIX 0 C80 1 0.703216 0.596473 0.140307 11.00000 0.04603 0.03110 = 0.04323 0.01592 0.00938 0.01453 AFIX 43 H80 2 0.721407 0.651379 0.157393 11.00000 -1.20000 AFIX 0 C81 1 0.826188 0.419797 0.131189 11.00000 0.04981 0.02997 = 0.03557 0.01402 0.01540 0.01920 C82 1 0.801781 0.349537 0.134895 11.00000 0.04594 0.03684 = 0.04803 0.02072 0.02079 0.01827 AFIX 43 H82 2 0.735214 0.332811 0.132781 11.00000 -1.20000 AFIX 0 C83 1 0.874674 0.303906 0.141678 11.00000 0.06366 0.03348 = 0.04616 0.02593 0.02577 0.01666 AFIX 43 H83 2 0.856477 0.257169 0.145701 11.00000 -1.20000 AFIX 0 C84 1 0.993576 0.390097 0.140148 11.00000 0.04217 0.03939 = 0.03789 0.02080 0.00905 0.00984 AFIX 43 H84 2 1.060716 0.404647 0.141964 11.00000 -1.20000 AFIX 0 C85 1 0.926948 0.440910 0.134834 11.00000 0.04962 0.03200 = 0.04145 0.01710 0.00752 0.00915 AFIX 43 H85 2 0.948508 0.488877 0.133666 11.00000 -1.20000 AFIX 0 O11 5 0.885289 0.447455 -0.125899 11.00000 0.11814 0.18601 = 0.12268 0.07930 0.06493 0.04595 N7 4 0.828949 0.489145 -0.040580 11.00000 0.09190 0.10260 = 0.05893 0.03550 0.01490 -0.00602 C86 1 0.768940 0.542681 -0.005994 11.00000 0.18454 0.09993 = 0.09870 0.02419 0.06224 -0.00236 AFIX 137 H86A 2 0.745736 0.576543 -0.026886 11.00000 -1.50000 H86B 2 0.810063 0.574506 0.036074 11.00000 -1.50000 H86C 2 0.711391 0.512349 -0.004329 11.00000 -1.50000 AFIX 0 C88 1 0.840417 0.491572 -0.092860 11.00000 0.07738 0.12705 = 0.08692 0.05638 0.02968 0.00814 AFIX 43 H88 2 0.812132 0.529765 -0.105266 11.00000 -1.20000 AFIX 0 C87 1 0.873394 0.433206 -0.019862 11.00000 0.12932 0.13155 = 0.09860 0.07590 0.01044 0.01833 AFIX 137 H87A 2 0.938282 0.457774 0.010221 11.00000 -1.50000 H87B 2 0.882408 0.389358 -0.055229 11.00000 -1.50000 H87C 2 0.829747 0.414407 -0.000474 11.00000 -1.50000 AFIX 0 PART 1 O12 5 0.380110 0.300104 0.129117 31.00000 0.08560 0.08799 = 0.14810 0.00875 -0.02475 0.03816 O13 5 0.292465 0.384415 0.127170 31.00000 0.11040 0.05120 = 0.09146 0.02599 0.03709 0.01767 O14 5 0.386946 0.360177 0.071348 31.00000 0.14028 0.05809 = 0.12824 -0.02873 0.07861 -0.02956 N6 4 0.359291 0.350919 0.110060 31.00000 0.08800 0.03831 = 0.12187 -0.00472 0.05347 -0.00226 SAME 0.02 0.02 O13B O14B O12B N6B PART 2 O14A 5 0.526619 1.066025 0.141539 51.00000 0.08470 0.13517 = 0.29958 0.06444 0.04283 0.03257 O12A 5 0.545251 1.152241 0.111263 51.00000 0.11299 0.21332 = 0.24489 0.05319 -0.00111 0.01197 O13A 5 0.504765 1.187831 0.194151 51.00000 0.12383 0.17302 = 0.27745 0.03290 0.01368 -0.01473 N6A 4 0.528321 1.134949 0.152206 51.00000 0.10773 0.18743 = 0.25715 0.05518 0.01820 0.01796 PART 3 O13B 5 0.533297 1.123331 0.125367 61.00000 0.09374 0.17635 = 0.25679 0.06793 0.02372 0.01186 O14B 5 0.616810 1.114557 0.066206 61.00000 0.12748 0.21109 = 0.24237 0.05528 0.00720 0.02032 O12B 5 0.587783 1.226548 0.107711 61.00000 0.10442 0.18132 = 0.21489 0.07051 -0.00052 -0.01469 N6B 4 0.578182 1.159223 0.103300 61.00000 0.10814 0.19398 = 0.24755 0.05665 0.00853 0.01669 PART 1 O3A 5 1.195276 0.883583 -0.099593 71.00000 0.07166 0.08872 = 0.12669 0.04985 0.04755 0.01892 HKLF 4 REM 230106_wqangz_038351_0m_a.res in P-1 REM wR2 = 0.2653, GooF = S = 1.022, Restrained GooF = 1.030 for all data REM R1 = 0.0845 for 11900 Fo > 4sig(Fo) and 0.1353 for all 20744 data REM 1134 parameters refined using 238 restraints END WGHT 0.1360 1.7660 REM Highest difference peak 0.945, deepest hole -0.508, 1-sigma level 0.072 Q1 1 0.4819 0.3386 0.1180 11.00000 0.05 0.95 Q2 1 0.3296 0.2969 0.1633 11.00000 0.05 0.63 Q3 1 0.3727 0.3050 0.1000 11.00000 0.05 0.59 Q4 1 0.7381 0.6540 -0.1765 11.00000 0.05 0.58 Q5 1 0.4287 0.3411 0.1217 11.00000 0.05 0.56 Q6 1 0.5531 1.1038 0.1170 11.00000 0.05 0.56 Q7 1 0.5392 0.8028 0.2847 11.00000 0.05 0.55 Q8 1 0.5236 1.0324 0.0865 11.00000 0.05 0.51 Q9 1 0.4642 1.1958 0.2228 11.00000 0.05 0.49 Q10 1 0.5408 1.1353 0.2172 11.00000 0.05 0.48 Q11 1 0.7366 0.6575 -0.2161 11.00000 0.05 0.48 Q12 1 0.5249 1.2643 0.1159 11.00000 0.05 0.47 Q13 1 0.5177 1.1989 0.1176 11.00000 0.05 0.45 Q14 1 0.4563 1.1920 0.1472 11.00000 0.05 0.44 Q15 1 0.5784 1.0967 0.1774 11.00000 0.05 0.43 Q16 1 0.3824 0.2694 0.1339 11.00000 0.05 0.40 Q17 1 0.2323 0.3805 0.1368 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1.50 2.60 -2 -9 0 52.89 6.80 -3 -9 0 338.77 19.90 -4 -9 0 634.34 30.30 -4 -9 0 626.84 32.30 -5 -9 0 98.99 8.10 -5 -9 0 99.89 9.90 5 9 0 92.59 12.60 -6 -9 0 240.48 14.70 -6 -9 0 262.57 17.70 6 9 0 291.67 23.80 -7 -9 0 161.78 10.90 -7 -9 0 160.68 13.80 7 9 0 184.58 19.50 -8 -9 0 34.80 7.40 -8 -9 0 28.10 4.40 8 9 0 46.30 13.40 -9 -9 0 9.70 5.60 9 9 0 2.80 7.40 -10 -9 0 9.40 5.90 10 9 0 6.60 7.90 -11 -9 0 33.00 8.00 11 9 0 28.20 11.80 -12 -9 0 9.50 5.80 12 9 0 -4.80 7.60 13 9 0 34.00 12.60 15 -10 0 31.10 13.40 14 -10 0 1.60 8.00 13 -10 0 31.00 12.20 12 -10 0 188.18 22.20 11 -10 0 67.79 14.20 10 -10 0 62.59 14.10 10 -10 0 52.29 4.80 -10 10 0 42.10 4.00 9 -10 0 93.89 15.30 9 -10 0 86.99 7.10 -9 10 0 102.69 6.50 8 -10 0 157.18 16.30 8 -10 0 139.79 9.50 -8 10 0 146.19 8.80 7 -10 0 641.94 37.40 7 -10 0 616.44 28.60 -7 10 0 574.94 27.30 6 -10 0 610.54 28.40 6 -10 0 540.25 34.40 -6 10 0 616.44 27.50 5 -10 0 209.78 18.00 5 -10 0 226.38 13.30 -5 10 0 223.88 12.70 4 -10 0 21.80 7.10 4 -10 0 21.50 4.50 -4 10 0 22.50 4.50 3 -10 0 28.90 5.10 2 -10 0 5.60 3.00 1 -10 0 2.30 2.80 0 -10 0 291.27 17.30 -1 -10 0 371.86 21.10 -2 -10 0 112.09 10.00 -3 -10 0 323.57 19.80 -4 -10 0 42.10 6.80 -4 -10 0 40.70 7.00 -5 -10 0 126.39 9.90 -5 -10 0 125.79 11.60 -6 -10 0 41.50 6.70 -6 -10 0 56.09 9.40 6 10 0 47.90 11.60 -7 -10 0 84.79 10.40 -7 -10 0 71.99 7.40 7 10 0 56.99 14.20 -8 -10 0 54.49 9.90 -8 -10 0 51.99 6.10 8 10 0 49.70 13.80 -9 -10 0 21.00 3.90 -9 -10 0 10.90 6.00 9 10 0 24.00 10.40 -10 -10 0 71.59 12.10 10 10 0 59.89 14.40 -11 -10 0 17.20 6.80 11 10 0 8.00 9.30 -12 -10 0 -9.30 4.40 12 10 0 10.50 8.40 -13 -10 0 -12.70 4.60 15 -11 0 11.60 11.40 14 -11 0 1.90 8.10 13 -11 0 8.60 8.40 12 -11 0 5.30 6.30 11 -11 0 55.39 13.30 10 -11 0 210.88 22.30 10 -11 0 201.18 11.70 -10 11 0 232.38 11.30 9 -11 0 494.95 24.70 9 -11 0 485.35 34.70 -9 11 0 567.84 24.10 8 -11 0 349.07 27.30 8 -11 0 369.66 19.10 -8 11 0 365.56 18.00 7 -11 0 265.97 15.90 7 -11 0 310.47 23.90 -7 11 0 285.37 15.10 6 -11 0 40.10 8.60 6 -11 0 44.20 6.30 -6 11 0 53.29 5.70 5 -11 0 2.60 4.20 5 -11 0 6.50 2.80 4 -11 0 7.50 3.10 4 -11 0 -0.70 3.20 3 -11 0 236.08 14.70 2 -11 0 210.58 14.00 1 -11 0 589.14 30.00 0 -11 0 569.54 29.30 -1 -11 0 91.59 9.20 -2 -11 0 0.90 3.00 -3 -11 0 9.10 5.00 -4 -11 0 43.00 8.20 -5 -11 0 76.29 9.30 -6 -11 0 11.70 4.70 -7 -11 0 21.60 6.60 -7 -11 0 12.20 4.40 7 11 0 8.40 6.40 -8 -11 0 40.10 8.70 -8 -11 0 30.00 5.20 -9 -11 0 5.90 3.40 -9 -11 0 -1.70 4.40 9 11 0 -7.30 6.20 -10 -11 0 4.90 5.50 10 11 0 2.10 7.80 -11 -11 0 32.70 8.70 11 11 0 12.70 12.60 -12 -11 0 12.20 7.60 12 11 0 26.90 12.40 14 -12 0 35.80 12.80 13 -12 0 17.30 10.80 12 -12 0 79.69 16.90 11 -12 0 27.00 10.60 11 -12 0 23.70 3.30 11 -12 0 17.60 3.00 10 -12 0 98.69 7.50 10 -12 0 78.39 15.50 9 -12 0 16.50 4.40 9 -12 0 23.70 9.00 -9 12 0 17.40 3.80 8 -12 0 9.30 6.30 8 -12 0 18.10 4.20 -8 12 0 22.30 3.90 7 -12 0 36.10 6.20 6 -12 0 50.59 10.80 6 -12 0 40.00 6.10 5 -12 0 18.20 6.80 5 -12 0 15.50 4.40 4 -12 0 111.59 12.80 4 -12 0 88.29 8.50 3 -12 0 70.29 7.60 2 -12 0 37.50 6.70 1 -12 0 5.50 3.80 0 -12 0 41.70 7.50 -1 -12 0 357.36 21.60 -2 -12 0 211.18 15.80 -3 -12 0 125.99 12.30 -4 -12 0 25.20 6.90 -5 -12 0 0.10 3.80 -6 -12 0 65.99 10.90 -7 -12 0 0.80 3.40 -8 -12 0 153.48 12.30 -8 -12 0 115.79 13.50 -9 -12 0 109.39 13.30 -9 -12 0 85.99 8.90 9 12 0 90.69 19.00 -10 -12 0 16.00 7.50 10 12 0 32.00 12.20 -11 -12 0 12.00 6.50 11 12 0 14.20 10.70 14 -13 0 -1.00 8.20 13 -13 0 13.20 9.60 12 -13 0 17.50 8.80 11 -13 0 61.89 5.50 11 -13 0 49.99 5.50 11 -13 0 50.39 12.70 10 -13 0 250.67 25.00 10 -13 0 245.08 14.40 10 -13 0 256.17 14.10 9 -13 0 120.69 9.80 9 -13 0 131.69 17.50 8 -13 0 82.39 8.30 8 -13 0 87.29 15.30 7 -13 0 8.20 6.60 7 -13 0 6.50 3.10 6 -13 0 40.80 10.50 6 -13 0 52.89 6.80 5 -13 0 13.60 6.60 4 -13 0 89.39 12.60 4 -13 0 105.09 9.70 3 -13 0 110.89 10.10 2 -13 0 305.07 19.20 1 -13 0 171.38 13.60 0 -13 0 298.47 19.70 -1 -13 0 127.59 11.90 -2 -13 0 5.10 4.20 -3 -13 0 46.40 8.90 -4 -13 0 154.58 14.20 -5 -13 0 344.97 23.50 -6 -13 0 190.98 17.40 -7 -13 0 98.69 12.80 -8 -13 0 9.10 5.10 -9 -13 0 2.90 4.50 -9 -13 0 0.80 4.00 -10 -13 0 -6.00 4.20 -11 -13 0 3.70 6.00 11 13 0 -15.60 7.10 13 -14 0 27.30 13.40 12 -14 0 37.30 12.60 11 -14 0 74.29 16.60 11 -14 0 78.89 6.50 11 -14 0 57.99 6.70 10 -14 0 81.09 7.90 10 -14 0 62.69 7.00 10 -14 0 65.19 14.20 9 -14 0 -4.00 5.60 9 -14 0 15.90 4.60 8 -14 0 131.89 11.10 8 -14 0 128.29 16.70 7 -14 0 83.59 8.80 7 -14 0 88.39 15.50 6 -14 0 330.67 19.60 6 -14 0 310.97 25.80 5 -14 0 188.08 19.80 5 -14 0 188.68 14.10 4 -14 0 -0.80 3.30 4 -14 0 -2.10 3.60 3 -14 0 123.09 11.30 2 -14 0 0.90 3.10 1 -14 0 2.40 3.70 0 -14 0 46.50 8.20 -1 -14 0 331.07 22.00 -2 -14 0 382.86 24.70 -3 -14 0 253.37 19.10 -4 -14 0 229.78 18.60 -5 -14 0 49.90 9.60 -6 -14 0 5.10 5.60 -7 -14 0 20.80 7.40 -8 -14 0 2.70 5.80 -9 -14 0 24.80 8.00 -10 -14 0 29.00 9.20 13 -15 0 13.70 9.50 12 -15 0 -3.30 6.90 11 -15 0 51.69 5.90 11 -15 0 34.50 6.20 11 -15 0 46.80 13.90 10 -15 0 78.79 17.10 10 -15 0 86.19 8.30 9 -15 0 243.28 24.40 9 -15 0 214.68 15.30 8 -15 0 316.47 27.90 8 -15 0 318.57 19.60 7 -15 0 155.18 12.60 7 -15 0 160.28 18.40 6 -15 0 13.30 4.80 5 -15 0 -1.50 5.40 5 -15 0 1.20 3.90 4 -15 0 35.20 10.00 4 -15 0 28.70 6.60 3 -15 0 123.99 11.80 2 -15 0 113.99 11.50 1 -15 0 472.85 27.90 0 -15 0 94.49 11.30 -1 -15 0 110.29 12.70 -2 -15 0 62.39 11.20 -3 -15 0 10.40 5.70 -4 -15 0 62.09 11.60 -5 -15 0 45.30 9.60 -6 -15 0 56.39 11.40 -7 -15 0 69.99 12.50 -8 -15 0 18.10 7.20 -9 -15 0 1.40 5.60 12 -16 0 35.40 11.60 12 -16 0 32.10 4.70 11 -16 0 77.59 17.00 11 -16 0 54.69 7.20 10 -16 0 46.30 12.50 10 -16 0 72.19 7.50 9 -16 0 -1.30 6.20 9 -16 0 12.30 5.10 8 -16 0 4.70 7.30 8 -16 0 -1.50 4.10 7 -16 0 54.29 13.40 7 -16 0 54.89 8.40 6 -16 0 107.09 10.80 6 -16 0 99.59 17.00 5 -16 0 79.99 10.00 5 -16 0 61.29 12.70 4 -16 0 535.15 30.80 4 -16 0 592.64 38.30 3 -16 0 70.79 10.80 2 -16 0 11.50 5.20 1 -16 0 15.90 6.10 0 -16 0 26.40 7.60 -1 -16 0 62.29 11.20 -2 -16 0 13.60 6.70 -3 -16 0 111.99 14.20 -4 -16 0 117.89 14.30 -5 -16 0 28.30 8.30 -6 -16 0 2.60 4.80 -7 -16 0 -3.10 4.80 -8 -16 0 0.90 6.50 11 -17 0 16.50 9.10 11 -17 0 14.50 4.30 10 -17 0 35.70 11.50 9 -17 0 71.09 8.80 9 -17 0 43.50 12.90 8 -17 0 73.89 10.60 8 -17 0 78.79 16.50 7 -17 0 73.49 9.50 7 -17 0 62.39 15.00 6 -17 0 -4.00 5.30 6 -17 0 0.80 3.80 5 -17 0 12.60 9.70 4 -17 0 -3.00 3.70 4 -17 0 3.60 6.60 3 -17 0 12.00 5.40 2 -17 0 36.70 8.00 1 -17 0 121.89 13.10 0 -17 0 63.89 11.10 -1 -17 0 72.19 12.90 -2 -17 0 13.50 6.20 -3 -17 0 19.70 8.10 -4 -17 0 15.10 7.30 -5 -17 0 15.70 7.70 -6 -17 0 34.00 9.00 -7 -17 0 6.90 6.20 10 -18 0 28.10 11.00 10 -18 0 34.20 6.60 9 -18 0 6.10 4.80 9 -18 0 -5.40 7.10 8 -18 0 -11.40 4.10 8 -18 0 -9.10 5.20 7 -18 0 13.10 5.40 7 -18 0 0.60 5.70 6 -18 0 19.90 6.20 6 -18 0 22.90 10.40 5 -18 0 28.70 10.50 5 -18 0 28.80 7.30 4 -18 0 78.89 15.10 4 -18 0 81.09 10.60 3 -18 0 100.29 11.80 2 -18 0 53.39 9.80 1 -18 0 2.30 4.90 0 -18 0 3.10 4.10 -1 -18 0 81.39 13.30 -2 -18 0 -0.70 5.30 -3 -18 0 90.79 15.70 -4 -18 0 30.20 9.60 -5 -18 0 9.50 7.90 -6 -18 0 -16.80 6.00 9 -19 0 15.50 6.30 9 -19 0 13.00 10.80 8 -19 0 6.80 8.40 8 -19 0 4.80 5.20 7 -19 0 36.90 11.40 7 -19 0 34.10 8.20 6 -19 0 5.90 5.20 6 -19 0 4.60 7.30 5 -19 0 -8.40 4.10 5 -19 0 -2.20 5.60 4 -19 0 22.40 7.30 4 -19 0 19.80 8.50 3 -19 0 19.30 8.60 3 -19 0 12.70 5.50 2 -19 0 15.80 6.50 1 -19 0 53.39 10.60 0 -19 0 52.99 11.00 -1 -19 0 11.90 7.40 -2 -19 0 26.70 9.30 -3 -19 0 -4.80 5.60 -4 -19 0 2.70 5.90 7 -20 0 4.40 8.40 7 -20 0 8.20 5.80 6 -20 0 -0.20 4.70 5 -20 0 42.90 13.20 5 -20 0 39.20 9.20 4 -20 0 37.90 9.20 4 -20 0 26.60 10.30 3 -20 0 33.90 11.10 3 -20 0 26.10 8.10 2 -20 0 46.30 10.00 1 -20 0 -1.00 4.70 0 -20 0 10.90 7.00 -1 -20 0 14.40 7.30 -2 -20 0 5.30 6.70 0 -21 1 22.60 8.30 1 -21 1 -12.90 4.50 2 -21 1 5.70 6.60 3 -21 1 5.00 5.10 3 -21 1 12.40 7.70 4 -21 1 7.20 7.70 4 -21 1 6.10 4.60 -3 -20 1 -5.00 6.30 -2 -20 1 -8.60 4.90 -1 -20 1 -2.70 4.70 0 -20 1 -3.30 5.40 1 -20 1 -4.40 4.80 2 -20 1 2.70 5.30 3 -20 1 -8.80 3.70 3 -20 1 -0.40 5.70 4 -20 1 9.20 6.90 4 -20 1 -7.50 4.50 5 -20 1 -4.70 4.10 5 -20 1 6.10 7.50 6 -20 1 -5.00 4.70 6 -20 1 -10.90 5.50 7 -20 1 -0.80 8.70 7 -20 1 7.70 5.90 -5 -19 1 3.40 6.90 -4 -19 1 18.50 7.80 -3 -19 1 3.70 5.30 -2 -19 1 20.20 7.40 -1 -19 1 -10.50 3.70 0 -19 1 -0.10 6.10 1 -19 1 11.00 6.20 2 -19 1 7.30 5.20 3 -19 1 25.60 9.80 3 -19 1 42.80 8.70 4 -19 1 15.30 6.10 4 -19 1 19.10 8.20 5 -19 1 7.20 8.00 5 -19 1 15.90 6.20 6 -19 1 10.20 5.50 6 -19 1 8.90 6.60 7 -19 1 7.70 4.80 7 -19 1 0.10 6.40 8 -19 1 -2.70 5.90 8 -19 1 -0.60 4.70 9 -19 1 13.90 8.10 -6 -18 1 -3.50 5.00 -5 -18 1 -0.10 4.80 -4 -18 1 1.30 5.60 -3 -18 1 15.60 7.30 -2 -18 1 10.40 7.00 -1 -18 1 4.00 6.30 0 -18 1 33.90 8.40 1 -18 1 27.30 8.00 2 -18 1 56.49 10.30 3 -18 1 44.70 8.80 4 -18 1 27.60 7.90 4 -18 1 -0.60 6.90 5 -18 1 3.60 5.10 5 -18 1 -0.50 5.10 6 -18 1 23.20 6.40 6 -18 1 10.50 8.00 7 -18 1 35.60 7.70 7 -18 1 5.80 7.80 8 -18 1 44.90 8.90 8 -18 1 41.60 12.60 9 -18 1 19.80 10.60 9 -18 1 15.40 6.50 10 -18 1 37.00 11.90 10 -18 1 23.00 5.70 -7 -17 1 2.70 5.40 -6 -17 1 16.90 7.30 -5 -17 1 29.70 9.30 -4 -17 1 24.70 7.90 -3 -17 1 -7.40 3.70 -2 -17 1 0.70 5.10 -1 -17 1 13.50 6.00 0 -17 1 0.80 4.90 1 -17 1 5.80 5.00 2 -17 1 26.10 7.30 3 -17 1 108.99 12.30 4 -17 1 39.10 8.10 4 -17 1 29.00 8.80 5 -17 1 176.48 14.80 5 -17 1 162.68 20.40 6 -17 1 10.90 5.30 6 -17 1 6.40 6.50 7 -17 1 31.80 10.50 7 -17 1 41.80 8.60 8 -17 1 8.60 5.60 8 -17 1 7.20 8.10 9 -17 1 10.10 8.40 9 -17 1 9.60 5.00 10 -17 1 -4.50 5.80 10 -17 1 4.50 3.90 11 -17 1 19.60 5.30 11 -17 1 14.20 9.00 -8 -16 1 14.00 7.50 -7 -16 1 16.70 7.00 -6 -16 1 22.80 8.30 -5 -16 1 12.20 6.70 -4 -16 1 -6.80 4.10 -3 -16 1 12.80 6.30 -2 -16 1 37.00 8.80 -1 -16 1 6.70 5.20 0 -16 1 82.89 10.70 1 -16 1 16.40 6.00 2 -16 1 115.09 12.10 3 -16 1 7.30 3.90 4 -16 1 21.60 8.10 4 -16 1 19.10 6.10 5 -16 1 9.60 6.90 5 -16 1 26.20 6.60 6 -16 1 21.20 9.20 6 -16 1 15.30 5.20 7 -16 1 18.20 9.40 7 -16 1 24.40 6.30 8 -16 1 9.10 8.20 8 -16 1 17.50 5.60 9 -16 1 12.00 8.80 9 -16 1 27.30 6.40 10 -16 1 28.10 10.40 10 -16 1 16.70 5.10 11 -16 1 24.60 5.20 11 -16 1 9.90 8.50 12 -16 1 9.30 3.80 12 -16 1 4.80 7.00 -9 -15 1 13.50 6.90 -8 -15 1 9.30 6.10 -7 -15 1 5.70 5.10 -6 -15 1 -2.90 4.40 -5 -15 1 27.30 8.10 -4 -15 1 6.20 5.60 -3 -15 1 73.69 12.50 -2 -15 1 100.29 11.70 -1 -15 1 38.10 8.50 0 -15 1 0.60 3.80 1 -15 1 150.28 13.20 2 -15 1 5.60 4.20 3 -15 1 65.09 9.80 4 -15 1 107.89 13.80 4 -15 1 96.49 10.20 5 -15 1 114.29 15.50 5 -15 1 107.19 10.40 6 -15 1 6.10 6.20 6 -15 1 1.40 3.20 7 -15 1 16.40 8.50 7 -15 1 33.10 6.40 8 -15 1 19.90 8.90 9 -15 1 -1.80 5.80 9 -15 1 9.80 4.20 10 -15 1 17.90 4.90 10 -15 1 18.10 9.40 11 -15 1 -0.30 3.10 11 -15 1 2.40 4.40 11 -15 1 11.50 7.30 12 -15 1 29.80 11.00 12 -15 1 22.80 4.20 13 -15 1 20.10 11.40 -10 -14 1 6.60 5.50 -9 -14 1 -4.00 4.10 -8 -14 1 35.10 9.30 -7 -14 1 4.40 4.60 -6 -14 1 12.70 6.30 -5 -14 1 8.00 4.80 -4 -14 1 8.80 5.60 -3 -14 1 14.20 6.20 -2 -14 1 7.80 5.50 -1 -14 1 22.30 6.10 0 -14 1 103.59 11.50 1 -14 1 81.79 9.50 2 -14 1 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15.20 5.20 2 -14 3 17.60 5.20 3 -14 3 9.30 6.10 3 -14 3 15.90 5.30 4 -14 3 8.70 5.50 4 -14 3 10.80 5.10 5 -14 3 94.39 12.80 5 -14 3 82.89 9.60 6 -14 3 98.49 10.30 7 -14 3 13.90 7.40 7 -14 3 7.20 4.30 8 -14 3 -1.60 3.10 8 -14 3 -6.30 3.80 9 -14 3 14.10 7.80 9 -14 3 18.30 5.30 10 -14 3 6.80 4.80 10 -14 3 8.60 6.70 11 -14 3 30.70 5.70 11 -14 3 17.20 9.20 -12 14 -3 10.60 4.80 12 -14 3 -11.20 6.10 13 -14 3 13.60 10.30 -12 -13 3 12.70 6.20 11 13 -3 5.00 9.50 -11 -13 3 -2.70 4.40 10 13 -3 -14.80 6.30 -10 -13 3 1.60 5.70 -9 -13 3 18.40 7.30 -8 -13 3 7.70 5.50 -7 -13 3 30.10 7.90 -6 -13 3 14.60 5.70 -5 -13 3 8.90 4.90 -4 -13 3 93.89 10.50 -3 -13 3 5.80 4.80 -2 -13 3 129.49 12.30 -1 -13 3 3.90 3.90 0 -13 3 19.40 5.60 1 -13 3 21.40 5.80 2 -13 3 30.40 6.20 3 -13 3 148.29 12.20 3 -13 3 156.38 15.60 4 -13 3 26.90 5.80 4 -13 3 24.90 8.30 5 -13 3 4.10 5.50 5 -13 3 8.70 4.00 6 -13 3 5.90 6.40 6 -13 3 -1.10 3.50 7 -13 3 8.00 4.40 7 -13 3 22.10 8.20 8 -13 3 181.28 13.50 8 -13 3 196.48 20.10 9 -13 3 18.60 5.10 9 -13 3 7.70 6.60 10 -13 3 55.09 7.20 10 -13 3 55.49 13.30 -11 13 -3 35.40 6.40 11 -13 3 47.60 12.20 11 -13 3 58.99 6.90 -12 13 -3 1.20 3.70 12 -13 3 2.20 2.90 12 -13 3 -12.90 5.40 13 -13 3 -5.20 2.70 13 -13 3 1.90 8.20 14 -13 3 17.00 10.80 12 12 -3 13.60 9.70 -12 -12 3 3.50 6.30 11 12 -3 31.80 13.00 -11 -12 3 16.30 7.00 10 12 -3 13.40 9.60 -10 -12 3 -0.30 5.10 9 12 -3 37.80 13.10 -9 -12 3 37.90 9.10 8 12 -3 18.50 9.70 -8 -12 3 -6.90 4.80 -7 -12 3 -2.60 3.90 -6 -12 3 4.40 4.00 -5 -12 3 -2.00 3.40 -4 -12 3 7.40 4.00 -3 -12 3 46.70 8.00 -2 -12 3 6.10 4.00 -1 -12 3 25.40 6.10 0 -12 3 40.00 6.90 1 -12 3 -0.50 2.90 2 -12 3 38.10 7.10 3 -12 3 54.79 7.00 3 -12 3 69.39 11.60 4 -12 3 8.30 5.30 4 -12 3 6.60 3.50 5 -12 3 102.09 9.40 5 -12 3 94.69 12.70 6 -12 3 79.79 8.00 6 -12 3 61.49 12.10 7 -12 3 195.38 13.10 7 -12 3 134.19 17.00 8 -12 3 223.28 20.20 8 -12 3 169.28 12.70 9 -12 3 -0.60 5.60 9 -12 3 2.00 3.80 -10 12 -3 -3.60 3.60 10 -12 3 3.00 3.30 10 -12 3 -3.00 4.60 -11 12 -3 2.40 3.80 11 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6.70 -12 11 -3 10.60 3.90 12 -11 3 12.70 3.60 12 -11 3 3.60 8.30 -13 11 -3 17.40 3.80 13 -11 3 11.90 3.30 13 -11 3 0.40 8.80 14 -11 3 2.50 10.50 14 -11 3 4.70 2.80 13 10 -3 8.20 9.00 12 10 -3 -3.20 9.90 -12 -10 3 -3.90 4.50 11 10 -3 -14.40 6.70 -11 -10 3 7.80 5.60 10 10 -3 11.20 9.70 -10 -10 3 17.80 6.30 9 10 -3 54.69 13.70 -9 -10 3 56.19 9.90 8 10 -3 5.30 6.60 -8 -10 3 6.80 4.30 7 10 -3 133.69 16.90 -7 -10 3 128.09 11.80 6 10 -3 19.90 7.90 -6 -10 3 32.10 6.50 -5 -10 3 23.20 5.80 -4 -10 3 0.40 2.60 -3 -10 3 59.69 8.90 -2 -10 3 194.68 13.80 -1 -10 3 321.07 18.90 0 -10 3 81.69 7.90 1 -10 3 0.80 2.40 2 -10 3 23.10 5.10 3 -10 3 63.79 6.80 3 -10 3 66.59 8.90 4 -10 3 8.30 4.30 4 -10 3 8.70 3.30 -5 10 -3 281.67 15.90 5 -10 3 290.57 16.80 5 -10 3 302.67 21.40 -6 10 -3 177.08 11.10 6 -10 3 171.08 12.00 6 -10 3 181.78 16.50 -7 10 -3 5.10 3.10 7 -10 3 2.10 2.70 7 -10 3 11.10 6.00 -8 10 -3 76.79 6.80 8 -10 3 71.19 7.50 8 -10 3 75.49 13.00 -9 10 -3 50.09 5.60 9 -10 3 60.49 12.20 9 -10 3 33.20 5.90 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11.30 3.60 4 -9 3 16.60 6.00 -5 9 -3 398.46 20.10 5 -9 3 395.06 25.40 5 -9 3 419.96 21.20 -6 9 -3 14.70 3.60 6 -9 3 13.60 3.80 6 -9 3 12.70 5.80 -7 9 -3 273.67 14.70 7 -9 3 260.17 15.30 7 -9 3 257.47 20.80 -8 9 -3 18.10 3.70 8 -9 3 18.50 7.20 8 -9 3 19.20 4.40 9 -9 3 13.90 3.70 9 -9 3 17.60 7.60 -10 9 -3 14.00 3.50 10 -9 3 1.00 5.40 10 -9 3 15.60 4.20 -11 9 -3 59.19 6.60 11 -9 3 74.49 15.20 11 -9 3 61.99 6.80 -12 9 -3 52.19 7.00 12 -9 3 78.49 7.10 12 -9 3 90.99 17.30 -13 9 -3 31.80 5.50 13 -9 3 33.80 5.10 13 -9 3 40.20 13.70 14 -9 3 -4.80 6.80 14 -9 3 -3.00 2.80 -15 9 -3 -5.60 3.00 15 -9 3 -5.50 9.20 14 8 -3 1.50 7.80 -14 -8 3 -5.20 4.50 13 8 -3 -13.00 6.80 -13 -8 3 8.00 5.20 12 8 -3 -9.20 5.20 -12 -8 3 -2.00 3.80 11 8 -3 13.10 9.30 -11 -8 3 15.90 5.90 10 8 -3 -0.20 7.40 -10 -8 3 3.80 4.80 9 8 -3 11.90 8.70 -9 -8 3 19.10 6.00 -9 -8 3 23.20 4.50 8 8 -3 41.60 11.40 -8 -8 3 33.50 6.70 -8 -8 3 43.00 6.70 7 8 -3 3.90 5.50 -7 -8 3 9.10 3.40 -7 -8 3 9.00 4.00 6 8 -3 89.69 14.00 -6 -8 3 96.19 8.30 -6 -8 3 91.09 8.90 5 8 -3 14.80 6.50 -5 -8 3 26.40 5.50 -5 -8 3 23.40 4.70 4 8 -3 1.20 4.20 -4 -8 3 2.70 2.50 -4 -8 3 3.20 2.90 -3 -8 3 84.19 7.70 -3 -8 3 67.69 7.00 -2 -8 3 14.00 3.80 -1 -8 3 85.79 7.80 0 8 -3 41.40 4.80 0 -8 3 37.00 5.90 -1 8 -3 92.39 7.20 1 -8 3 92.49 7.80 -2 8 -3 304.17 16.10 2 -8 3 327.37 16.80 2 -8 3 282.87 18.70 -3 8 -3 128.59 8.50 3 -8 3 112.99 10.70 3 -8 3 122.69 9.00 -4 8 -3 2.60 2.10 4 -8 3 5.30 2.60 4 -8 3 3.20 3.50 -5 8 -3 324.77 16.60 5 -8 3 318.37 21.60 5 -8 3 326.87 17.50 -6 8 -3 165.18 10.10 6 -8 3 159.48 10.60 6 -8 3 140.59 14.10 -7 8 -3 51.79 5.10 7 -8 3 45.50 5.70 7 -8 3 50.69 10.00 -8 8 -3 4.40 2.50 8 -8 3 -0.70 2.30 8 -8 3 6.40 4.80 -9 8 -3 8.40 3.20 9 -8 3 6.10 5.70 -10 8 -3 5.40 3.10 10 -8 3 6.80 2.90 10 -8 3 5.80 6.30 -11 8 -3 -3.50 3.20 11 -8 3 -0.60 2.90 11 -8 3 5.80 6.90 12 -8 3 28.30 5.30 12 -8 3 31.10 11.10 -13 8 -3 1.40 4.10 13 -8 3 -2.30 8.60 13 -8 3 -7.50 3.30 -14 8 -3 20.00 6.00 14 -8 3 25.80 4.50 -15 8 -3 6.20 3.60 15 -8 3 -4.30 9.20 15 7 -3 20.50 12.70 14 7 -3 4.50 9.80 -14 -7 3 8.90 5.70 13 7 -3 -6.10 3.40 13 7 -3 11.50 9.30 -13 -7 3 3.70 4.40 12 7 -3 20.50 5.20 12 7 -3 24.30 10.60 -12 -7 3 29.20 6.70 11 7 -3 19.90 10.60 11 7 -3 41.40 6.30 -11 -7 3 29.80 6.70 10 7 -3 -2.00 6.90 10 7 -3 6.10 3.70 -10 -7 3 3.60 4.00 9 7 -3 26.80 9.50 9 7 -3 34.60 5.70 -9 -7 3 27.30 6.70 8 7 -3 3.30 5.10 8 7 -3 3.70 2.80 -8 -7 3 1.90 2.90 7 7 -3 20.10 7.80 7 7 -3 14.20 3.90 -7 -7 3 19.40 4.10 -7 -7 3 13.50 4.40 6 7 -3 229.98 19.50 -6 -7 3 243.88 15.50 -6 -7 3 254.67 14.60 5 7 -3 341.17 23.10 -5 -7 3 345.27 19.00 -5 -7 3 311.47 17.70 4 7 -3 990.30 49.60 -4 -7 3 1090.79 45.90 -4 -7 3 944.21 44.80 -3 -7 3 376.36 19.60 -3 -7 3 352.16 19.10 2 7 -3 51.89 5.50 -2 -7 3 41.80 6.00 -2 -7 3 49.10 7.90 -2 -7 3 42.50 5.20 1 7 -3 455.25 22.40 -1 -7 3 465.85 22.90 0 7 -3 62.99 5.50 0 -7 3 61.39 5.90 -1 7 -3 14.10 3.40 1 -7 3 14.40 3.70 -2 7 -3 0.30 1.60 2 -7 3 1.90 2.20 2 -7 3 0.20 2.60 -3 7 -3 310.17 15.80 3 -7 3 291.57 18.70 3 -7 3 325.37 16.60 -4 7 -3 677.43 30.80 4 -7 3 645.94 31.20 4 -7 3 742.13 35.80 -5 7 -3 179.48 10.60 5 -7 3 185.98 11.30 5 -7 3 177.08 14.50 -6 7 -3 1.70 2.10 6 -7 3 7.40 4.80 6 -7 3 7.10 2.90 -7 7 -3 8.60 2.90 7 -7 3 10.00 3.10 7 -7 3 6.10 5.10 -8 7 -3 22.00 4.20 8 -7 3 28.70 8.00 8 -7 3 24.40 4.50 -9 7 -3 22.40 4.50 9 -7 3 11.90 7.20 9 -7 3 33.10 5.20 -10 7 -3 197.08 12.40 10 -7 3 177.58 20.10 10 -7 3 190.58 12.20 11 -7 3 -0.90 2.80 11 -7 3 28.60 9.80 -12 7 -3 1.80 4.30 12 -7 3 4.90 3.30 12 -7 3 -9.10 6.10 13 -7 3 38.40 13.20 13 -7 3 28.80 5.50 14 -7 3 2.50 3.00 14 -7 3 -5.00 7.40 -15 7 -3 -5.90 3.50 15 -7 3 14.40 10.70 15 6 -3 5.30 5.60 15 6 -3 11.20 12.50 -15 -6 3 13.30 5.90 14 6 -3 16.30 5.40 14 6 -3 12.40 11.70 -14 -6 3 13.60 6.00 13 6 -3 15.80 5.40 13 6 -3 21.60 11.70 -13 -6 3 23.30 6.50 12 6 -3 74.59 16.80 12 6 -3 28.20 5.90 -12 -6 3 49.80 8.50 11 6 -3 5.70 7.80 11 6 -3 0.10 3.00 -11 -6 3 9.80 4.10 10 6 -3 2.20 6.80 10 6 -3 9.70 3.90 -10 -6 3 10.30 4.60 9 6 -3 11.60 3.90 9 6 -3 17.50 8.30 -9 -6 3 9.90 4.10 8 6 -3 17.60 4.10 8 6 -3 16.30 7.70 -8 -6 3 16.30 3.90 -8 -6 3 20.40 5.00 7 6 -3 21.70 4.30 7 6 -3 7.20 5.90 -7 -6 3 20.80 3.90 -7 -6 3 13.70 4.40 6 6 -3 359.86 19.10 6 6 -3 369.76 24.80 -6 -6 3 365.96 19.00 -6 -6 3 356.46 19.90 5 6 -3 962.90 51.19 5 6 -3 1071.09 46.60 -5 -6 3 1141.79 47.50 -5 -6 3 1027.30 46.40 4 6 -3 108.29 10.70 -4 -6 3 87.19 7.60 -4 -6 3 97.59 7.70 3 6 -3 200.78 14.30 3 6 -3 178.28 11.20 -3 -6 3 183.08 14.00 -3 -6 3 178.08 11.30 -3 -6 3 197.38 11.80 2 6 -3 76.49 6.10 -2 -6 3 69.89 6.10 -2 -6 3 55.09 7.10 -2 -6 3 65.79 6.00 1 6 -3 101.09 7.00 -1 -6 3 85.19 7.00 0 6 -3 5.60 2.10 0 -6 3 3.50 2.20 -1 6 -3 197.68 10.80 1 -6 3 190.38 11.00 -2 6 -3 41.30 4.40 2 -6 3 48.00 6.10 2 -6 3 42.40 4.70 -3 6 -3 101.19 8.60 -3 6 -3 80.89 6.40 3 -6 3 90.69 8.80 3 -6 3 95.79 7.00 -4 6 -3 227.48 15.70 -4 6 -3 252.37 13.30 4 -6 3 270.57 14.00 4 -6 3 269.47 17.20 -5 6 -3 10.80 3.00 5 -6 3 13.90 5.50 5 -6 3 11.70 3.30 -6 6 -3 2.20 2.00 6 -6 3 5.40 4.10 6 -6 3 -0.20 2.10 -7 6 -3 99.59 7.70 7 -6 3 95.39 7.90 7 -6 3 126.29 13.30 -8 6 -3 73.79 7.10 8 -6 3 122.19 14.10 8 -6 3 100.29 7.70 -9 6 -3 143.49 10.20 9 -6 3 157.28 10.60 9 -6 3 153.18 17.10 -10 6 -3 37.30 6.00 10 -6 3 37.10 5.80 10 -6 3 35.80 10.70 -11 6 -3 32.00 5.80 11 -6 3 40.20 12.40 11 -6 3 33.80 5.70 12 -6 3 14.70 4.60 12 -6 3 31.50 12.80 13 -6 3 11.30 9.40 14 -6 3 6.70 9.00 15 -6 3 20.20 12.30 15 5 -3 -3.70 8.40 15 5 -3 14.20 5.80 -15 -5 3 -0.80 5.40 14 5 -3 10.80 4.90 14 5 -3 7.00 10.10 -14 -5 3 -1.10 4.20 13 5 -3 1.20 3.90 13 5 -3 -6.00 6.80 -13 -5 3 3.60 3.90 12 5 -3 -1.80 6.90 12 5 -3 10.50 4.50 -12 -5 3 3.90 4.20 11 5 -3 14.10 8.30 11 5 -3 10.30 4.20 -11 -5 3 2.10 4.30 10 5 -3 49.10 12.80 10 5 -3 58.59 7.20 -10 -5 3 51.09 7.60 9 5 -3 82.09 8.00 9 5 -3 63.69 13.40 -9 -5 3 62.39 7.40 8 5 -3 42.30 10.40 8 5 -3 35.30 5.60 -8 -5 3 29.90 5.50 7 5 -3 10.10 3.60 7 5 -3 16.40 7.10 -7 -5 3 13.70 3.80 -7 -5 3 18.30 3.90 6 5 -3 66.89 11.40 6 5 -3 70.29 6.80 -6 -5 3 83.39 7.30 -6 -5 3 64.59 6.20 5 5 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4 1.40 4.60 6 -19 4 6.80 5.90 7 -19 4 -0.50 5.20 7 -19 4 9.80 8.10 8 -19 4 19.10 8.40 8 -19 4 -10.00 5.30 9 -19 4 13.60 6.30 9 -19 4 18.00 9.30 -7 -18 4 -9.40 4.90 -6 -18 4 20.60 7.70 -5 -18 4 11.80 6.70 -4 -18 4 8.80 6.00 -3 -18 4 5.10 5.90 -2 -18 4 5.70 5.60 -1 -18 4 0.80 4.50 0 -18 4 30.60 8.80 1 -18 4 14.10 6.70 2 -18 4 9.40 5.60 3 -18 4 53.69 10.00 3 -18 4 45.50 11.80 4 -18 4 36.10 11.40 4 -18 4 40.50 8.60 5 -18 4 9.40 4.70 5 -18 4 19.90 8.40 6 -18 4 9.90 6.10 6 -18 4 10.70 5.10 7 -18 4 13.30 8.90 7 -18 4 9.90 4.90 8 -18 4 14.90 5.80 8 -18 4 2.20 7.80 9 -18 4 8.20 5.30 9 -18 4 -6.80 7.00 10 -18 4 11.10 8.90 10 -18 4 21.90 5.40 -8 -17 4 7.70 6.30 -7 -17 4 -2.30 4.10 -6 -17 4 2.60 5.60 -5 -17 4 9.50 5.70 -4 -17 4 14.20 6.10 -3 -17 4 -10.10 3.60 -2 -17 4 14.10 6.50 -1 -17 4 109.89 13.20 0 -17 4 -1.70 3.80 1 -17 4 30.80 8.70 2 -17 4 49.30 9.50 3 -17 4 -2.10 3.90 3 -17 4 3.70 5.00 4 -17 4 13.90 7.10 4 -17 4 -2.10 3.60 5 -17 4 8.20 7.40 5 -17 4 8.20 5.70 6 -17 4 4.80 5.70 6 -17 4 -3.00 4.30 7 -17 4 1.10 6.00 7 -17 4 17.80 6.50 8 -17 4 21.10 9.20 8 -17 4 27.90 7.80 9 -17 4 0.40 5.80 9 -17 4 0.00 8.40 10 -17 4 -7.70 4.30 10 -17 4 -6.30 7.20 11 -17 4 10.70 5.70 11 -17 4 11.40 9.90 -9 -16 4 4.90 5.70 -8 -16 4 8.50 5.80 -7 -16 4 5.70 5.00 -6 -16 4 1.90 4.80 -5 -16 4 11.40 5.90 -4 -16 4 67.99 11.30 -3 -16 4 -0.60 4.10 -2 -16 4 -0.20 4.10 -1 -16 4 4.80 5.40 0 -16 4 -0.50 3.50 1 -16 4 29.50 7.70 2 -16 4 83.79 12.30 3 -16 4 85.79 11.90 3 -16 4 56.59 12.00 4 -16 4 8.90 4.30 4 -16 4 -0.50 5.00 5 -16 4 -4.10 4.70 5 -16 4 3.10 3.80 6 -16 4 78.49 10.00 6 -16 4 87.39 16.20 7 -16 4 -4.00 3.30 7 -16 4 -7.50 4.70 8 -16 4 10.00 5.30 8 -16 4 -4.80 6.20 9 -16 4 -5.00 5.30 9 -16 4 2.00 4.20 10 -16 4 15.90 5.50 10 -16 4 -14.70 7.50 11 -16 4 -10.40 9.70 12 -16 4 9.20 4.60 12 -16 4 7.40 9.20 -10 -15 4 2.10 5.70 -9 -15 4 4.60 6.40 -8 -15 4 21.70 7.90 -7 -15 4 -9.20 3.40 -6 -15 4 -1.20 4.60 -5 -15 4 73.19 11.60 -4 -15 4 1.20 4.60 -3 -15 4 125.29 13.10 -2 -15 4 11.50 5.90 -1 -15 4 46.10 9.40 0 -15 4 53.49 9.30 1 -15 4 9.90 4.80 2 -15 4 88.29 10.40 3 -15 4 48.00 10.50 3 -15 4 45.30 8.00 4 -15 4 138.59 12.20 4 -15 4 110.09 14.90 5 -15 4 10.10 4.90 5 -15 4 14.10 6.90 6 -15 4 25.80 9.00 7 -15 4 62.79 8.20 7 -15 4 39.50 12.50 8 -15 4 55.49 13.00 8 -15 4 72.89 9.00 9 -15 4 -3.40 3.90 10 -15 4 -11.00 6.20 10 -15 4 0.30 4.20 11 -15 4 0.90 7.10 11 -15 4 10.90 4.20 12 -15 4 7.00 8.40 13 -15 4 -0.20 3.60 13 -15 4 -5.30 9.00 -11 -14 4 -1.80 5.20 -10 -14 4 4.30 4.80 -9 -14 4 -0.10 5.00 -8 -14 4 4.20 4.50 -7 -14 4 7.70 5.40 -6 -14 4 11.80 6.70 -5 -14 4 44.50 9.50 -4 -14 4 8.60 4.80 -3 -14 4 80.69 10.10 -2 -14 4 21.20 6.20 -1 -14 4 33.40 7.90 0 -14 4 0.10 3.40 1 -14 4 -4.50 2.70 2 -14 4 70.79 9.10 3 -14 4 3.70 4.30 3 -14 4 5.60 3.70 4 -14 4 15.70 5.00 4 -14 4 9.40 5.80 5 -14 4 51.29 8.20 5 -14 4 46.60 11.00 6 -14 4 59.59 12.20 6 -14 4 77.09 8.90 7 -14 4 -1.40 4.20 7 -14 4 9.20 7.20 8 -14 4 -1.10 5.10 8 -14 4 -2.80 3.40 9 -14 4 35.60 7.00 9 -14 4 39.90 11.80 10 -14 4 5.20 6.70 11 -14 4 26.40 9.90 11 -14 4 14.30 5.10 12 -14 4 14.10 8.70 13 -14 4 2.30 3.70 13 -14 4 4.20 9.20 12 13 -4 9.10 9.30 11 13 -4 21.50 11.30 -11 -13 4 12.20 6.00 10 13 -4 8.60 8.40 -10 -13 4 7.40 5.40 9 13 -4 -11.40 5.10 -9 -13 4 -7.20 3.70 -8 -13 4 23.70 6.90 -7 -13 4 19.10 8.00 -6 -13 4 1.80 4.00 -5 -13 4 -2.30 3.20 -4 -13 4 47.40 9.10 -3 -13 4 6.60 4.60 -2 -13 4 3.10 3.80 -1 -13 4 53.99 9.20 0 -13 4 26.50 6.50 1 -13 4 5.40 3.70 2 -13 4 18.20 5.70 3 -13 4 49.80 8.10 3 -13 4 48.00 10.30 4 -13 4 10.20 5.60 4 -13 4 26.50 6.30 5 -13 4 8.30 5.80 5 -13 4 14.60 4.80 6 -13 4 30.20 8.90 6 -13 4 40.00 6.90 7 -13 4 13.20 4.30 7 -13 4 4.50 5.50 8 -13 4 162.38 17.80 8 -13 4 136.99 11.80 9 -13 4 9.80 4.60 9 -13 4 14.40 8.00 10 -13 4 15.70 7.90 10 -13 4 -1.00 3.80 11 -13 4 4.50 3.80 11 -13 4 12.20 8.50 12 -13 4 7.60 8.50 12 -13 4 6.90 3.60 13 -13 4 11.30 3.90 13 -13 4 12.70 8.30 14 -13 4 3.60 9.60 14 -13 4 3.00 3.30 12 12 -4 5.30 9.90 -12 -12 4 8.80 5.70 11 12 -4 7.40 9.50 -11 -12 4 13.80 6.00 10 12 -4 3.60 7.80 -10 -12 4 6.70 5.10 9 12 -4 11.20 9.00 -9 -12 4 30.60 8.30 8 12 -4 -2.30 7.80 -8 -12 4 17.80 6.60 -7 -12 4 41.50 8.80 -6 -12 4 -4.10 3.60 -5 -12 4 13.60 5.30 -4 -12 4 5.30 4.00 -3 -12 4 49.20 8.20 -2 -12 4 -3.40 2.60 -1 -12 4 15.30 5.10 0 -12 4 111.49 10.30 1 -12 4 302.97 18.90 2 -12 4 112.89 10.10 3 -12 4 41.40 7.10 3 -12 4 50.99 9.50 4 -12 4 141.29 11.70 4 -12 4 162.08 15.40 5 -12 4 172.48 16.90 5 -12 4 193.18 13.60 6 -12 4 29.70 8.20 6 -12 4 28.70 5.90 7 -12 4 7.20 5.90 7 -12 4 21.10 5.20 8 -12 4 83.59 8.60 8 -12 4 78.19 13.40 9 -12 4 12.50 4.40 9 -12 4 25.80 9.50 10 -12 4 60.89 13.20 10 -12 4 65.59 7.70 11 -12 4 20.40 9.20 12 -12 4 12.50 8.80 -13 12 -4 15.40 6.80 13 -12 4 17.80 10.70 14 -12 4 17.90 10.00 13 11 -4 31.20 12.20 12 11 -4 9.50 8.40 -12 -11 4 3.60 5.50 11 11 -4 -8.30 6.20 -11 -11 4 2.10 4.80 10 11 -4 2.60 6.80 -10 -11 4 6.10 4.80 9 11 -4 76.39 16.10 -9 -11 4 107.99 12.70 8 11 -4 24.80 9.70 -8 -11 4 18.60 7.40 7 11 -4 32.10 9.90 -7 -11 4 39.30 8.20 -6 -11 4 96.49 10.40 -5 -11 4 -2.30 2.50 -4 -11 4 11.30 4.70 -3 -11 4 16.40 4.80 -2 -11 4 23.30 5.40 -1 -11 4 370.76 21.40 0 -11 4 115.39 10.10 1 -11 4 276.17 17.10 2 -11 4 280.67 17.20 3 -11 4 52.99 6.60 3 -11 4 41.80 8.70 4 -11 4 31.80 7.70 4 -11 4 38.10 6.70 5 -11 4 10.10 4.00 5 -11 4 10.10 5.60 6 -11 4 242.18 19.70 6 -11 4 207.78 14.40 7 -11 4 89.99 8.90 7 -11 4 98.39 12.90 8 -11 4 6.70 6.00 9 -11 4 91.19 9.20 10 -11 4 1.90 6.20 10 -11 4 -1.40 3.30 11 -11 4 0.40 6.30 11 -11 4 9.90 3.90 -12 11 -4 6.00 7.10 12 -11 4 -1.90 6.70 12 -11 4 1.30 3.50 -13 11 -4 -4.20 5.00 13 -11 4 9.00 3.90 13 -11 4 -6.30 7.20 14 -11 4 20.40 4.10 14 -11 4 16.20 12.00 13 10 -4 12.80 10.40 12 10 -4 15.30 9.90 -12 -10 4 21.70 6.70 11 10 -4 101.39 20.00 -11 -10 4 97.89 12.00 10 10 -4 5.40 8.20 -10 -10 4 0.00 4.50 9 10 -4 220.78 23.00 -9 -10 4 179.78 15.90 8 10 -4 -0.10 5.10 -8 -10 4 1.00 4.20 7 10 -4 32.00 10.40 -7 -10 4 14.50 5.50 6 10 -4 58.69 12.40 -6 -10 4 67.39 8.80 -5 -10 4 6.40 4.00 -4 -10 4 75.59 8.80 -3 -10 4 10.10 4.20 -2 -10 4 56.09 7.30 -1 -10 4 181.38 12.80 0 -10 4 100.99 9.30 1 -10 4 4.70 3.10 2 -10 4 11.80 3.70 3 -10 4 30.00 7.30 3 -10 4 43.70 6.60 4 -10 4 122.39 12.20 4 -10 4 109.99 9.30 5 -10 4 386.96 25.40 5 -10 4 387.16 21.10 -6 10 -4 320.77 23.80 6 -10 4 373.96 20.20 6 -10 4 387.96 25.80 -7 10 -4 70.69 7.60 7 -10 4 73.79 7.60 7 -10 4 65.29 12.10 -8 10 -4 11.80 4.40 8 -10 4 15.50 4.40 8 -10 4 14.50 6.10 -9 10 -4 62.19 8.00 9 -10 4 62.99 7.10 9 -10 4 87.49 15.40 -10 10 -4 -0.20 3.70 10 -10 4 -3.10 5.20 11 -10 4 23.40 10.00 11 -10 4 21.60 5.20 12 -10 4 71.09 7.80 12 -10 4 75.29 16.00 -13 10 -4 20.00 7.20 13 -10 4 10.50 4.20 13 -10 4 44.20 13.60 14 -10 4 8.60 10.00 14 -10 4 6.10 3.70 14 9 -4 2.40 7.30 -14 -9 4 9.50 6.10 13 9 -4 27.40 10.80 12 9 -4 40.20 13.50 -12 -9 4 31.80 7.60 -11 -9 4 4.90 4.20 10 9 -4 7.50 8.20 -10 -9 4 17.30 5.90 -9 -9 4 5.20 4.30 8 9 -4 128.39 16.50 -8 -9 4 114.59 11.10 7 9 -4 130.89 15.40 -7 -9 4 115.19 11.30 6 9 -4 28.90 8.20 -6 -9 4 24.00 5.50 5 9 -4 136.29 14.70 -5 -9 4 137.29 11.40 -4 -9 4 197.08 14.00 -3 -9 4 22.40 5.00 -2 -9 4 248.18 15.50 -1 -9 4 1.70 2.50 0 -9 4 -3.10 2.20 1 -9 4 138.19 10.40 -2 9 -4 41.40 8.40 2 -9 4 35.90 5.70 2 -9 4 41.00 7.40 -3 9 -4 -0.70 1.80 3 -9 4 1.20 2.70 3 -9 4 -0.30 2.90 -4 9 -4 79.69 6.80 4 -9 4 72.59 7.20 4 -9 4 79.79 9.70 -5 9 -4 18.40 3.70 5 -9 4 14.00 4.10 5 -9 4 18.00 6.40 6 -9 4 25.00 6.90 6 -9 4 25.40 5.20 -7 9 -4 263.07 15.00 7 -9 4 267.77 21.30 7 -9 4 273.47 16.10 -8 9 -4 3.00 2.90 8 -9 4 -0.70 4.40 8 -9 4 2.10 2.60 -9 9 -4 0.20 3.50 9 -9 4 -0.70 5.10 9 -9 4 4.90 3.30 -10 9 -4 -3.40 3.30 10 -9 4 4.60 6.00 10 -9 4 10.40 3.50 11 -9 4 68.49 7.50 11 -9 4 52.99 13.70 12 -9 4 22.30 5.30 12 -9 4 19.30 10.30 13 -9 4 -3.80 3.00 13 -9 4 0.30 8.20 14 -9 4 9.50 9.60 14 -9 4 4.70 4.10 15 -9 4 2.20 10.20 14 8 -4 -3.50 7.60 -14 -8 4 4.70 5.00 13 8 -4 2.70 9.30 -13 -8 4 11.10 6.30 12 8 -4 12.90 10.60 -12 -8 4 14.20 5.60 11 8 -4 49.10 8.00 11 8 -4 58.19 15.00 -11 -8 4 56.69 9.10 10 8 -4 25.00 10.80 10 8 -4 23.00 5.50 -10 -8 4 17.20 6.00 9 8 -4 3.40 3.60 9 8 -4 9.50 7.00 -9 -8 4 14.20 5.10 8 8 -4 304.07 24.50 -8 -8 4 275.07 18.30 7 8 -4 -2.10 4.60 -7 -8 4 0.70 3.10 6 8 -4 14.60 6.90 -6 -8 4 16.30 4.30 -6 -8 4 9.00 3.80 5 8 -4 0.70 4.20 -5 -8 4 4.20 3.00 -5 -8 4 2.40 3.10 4 8 -4 74.79 11.40 -4 -8 4 66.79 7.20 -4 -8 4 67.99 7.10 -3 -8 4 1.30 2.40 -3 -8 4 -0.20 2.60 -2 -8 4 13.40 3.50 -2 -8 4 12.60 3.80 -1 -8 4 323.87 17.90 0 8 -4 69.59 6.30 0 -8 4 69.49 7.00 -1 8 -4 16.70 3.80 1 -8 4 10.20 3.70 -2 8 -4 158.98 10.40 2 -8 4 163.58 11.00 2 -8 4 182.38 13.00 -3 8 -4 776.02 35.50 3 -8 4 824.52 36.60 3 -8 4 766.32 38.80 -4 8 -4 1520.95 66.09 4 -8 4 1579.04 66.99 4 -8 4 1574.84 70.79 -5 8 -4 115.99 8.20 5 -8 4 128.99 12.20 5 -8 4 108.69 9.00 -6 8 -4 170.78 10.80 6 -8 4 160.88 11.30 6 -8 4 171.68 15.30 -7 8 -4 105.09 8.00 7 -8 4 89.49 8.10 7 -8 4 98.89 12.10 -8 8 -4 4.30 3.00 8 -8 4 -0.40 4.50 8 -8 4 5.50 3.10 -9 8 -4 23.80 5.30 9 -8 4 20.70 8.00 9 -8 4 23.90 5.00 -10 8 -4 -3.20 3.50 10 -8 4 0.60 7.00 10 -8 4 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1 7 -4 39.40 4.70 -1 -7 4 35.90 4.70 0 7 -4 32.70 5.10 0 -7 4 26.60 4.80 -1 7 -4 680.43 31.40 1 -7 4 704.03 32.00 -2 7 -4 340.67 17.60 2 -7 4 332.27 18.10 2 -7 4 376.26 20.20 -3 7 -4 1715.93 73.09 3 -7 4 1805.32 76.69 3 -7 4 1713.53 73.69 -4 7 -4 1533.45 65.89 4 -7 4 1636.14 70.69 4 -7 4 1517.05 66.59 -5 7 -4 61.29 5.80 5 -7 4 65.19 6.30 5 -7 4 55.29 9.40 -6 7 -4 19.00 4.00 6 -7 4 14.20 3.80 6 -7 4 6.20 4.90 -7 7 -4 10.30 3.70 7 -7 4 17.60 4.30 7 -7 4 28.40 8.10 -8 7 -4 55.59 6.30 8 -7 4 47.40 6.10 8 -7 4 56.49 11.30 -9 7 -4 6.50 3.20 9 -7 4 8.00 3.10 -10 7 -4 32.80 8.70 10 -7 4 16.70 4.80 10 -7 4 18.30 9.50 11 -7 4 0.00 3.10 11 -7 4 9.20 7.50 12 -7 4 28.20 5.50 12 -7 4 1.60 8.20 13 -7 4 29.80 12.20 13 -7 4 37.80 6.50 14 -7 4 10.70 9.50 15 -7 4 -19.80 10.00 15 6 -4 7.10 4.70 15 6 -4 11.80 9.90 14 6 -4 0.20 4.20 14 6 -4 -7.20 7.80 -14 -6 4 0.40 4.60 13 6 -4 11.60 5.50 13 6 -4 6.20 9.80 -13 -6 4 4.30 4.50 12 6 -4 7.10 6.90 -12 -6 4 6.90 4.60 11 6 -4 16.20 8.70 11 6 -4 27.00 6.10 -11 -6 4 22.60 5.70 10 6 -4 92.39 16.50 10 6 -4 77.89 8.30 -10 -6 4 64.79 9.20 9 6 -4 138.29 16.70 9 6 -4 132.89 11.00 -9 -6 4 136.49 11.10 8 6 -4 43.70 10.30 8 6 -4 27.60 5.60 -8 -6 4 21.40 5.10 7 6 -4 -0.90 4.10 7 6 -4 3.70 2.90 -7 -6 4 3.70 2.40 -7 -6 4 7.30 3.40 6 6 -4 67.69 6.80 6 6 -4 63.39 11.10 -6 -6 4 52.29 6.00 -6 -6 4 61.29 6.80 5 6 -4 128.49 12.30 5 6 -4 118.79 9.10 -5 -6 4 115.09 9.10 -5 -6 4 115.39 8.90 4 6 -4 20.10 6.20 4 6 -4 19.00 4.50 4 6 -4 30.80 5.20 -4 -6 4 22.90 6.40 -4 -6 4 20.10 4.50 -4 -6 4 19.40 4.20 3 6 -4 17.40 3.50 3 6 -4 11.70 4.20 -3 -6 4 6.30 3.50 -3 -6 4 10.10 3.40 -3 -6 4 12.60 3.60 2 6 -4 126.79 8.00 -2 -6 4 92.79 7.70 -2 -6 4 121.79 8.20 -2 -6 4 91.79 8.60 1 6 -4 1023.00 47.90 -1 -6 4 1140.59 48.60 -1 -6 4 1196.68 49.20 0 6 -4 108.69 7.30 0 -6 4 97.49 7.50 -1 6 -4 23.80 3.80 1 -6 4 13.60 3.50 -2 6 -4 -2.20 1.50 2 -6 4 -0.50 2.20 2 -6 4 1.40 2.20 -3 6 -4 1.10 2.50 -3 6 -4 1.80 2.00 3 -6 4 3.20 2.90 3 -6 4 2.70 2.60 -4 6 -4 430.36 21.80 -4 6 -4 439.86 24.30 4 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22.90 -7 -5 4 299.47 17.20 -7 -5 4 329.67 17.40 6 5 -4 122.59 9.40 6 5 -4 122.99 13.00 -6 -5 4 125.69 9.10 -6 -5 4 127.79 9.30 5 5 -4 53.09 9.00 5 5 -4 50.09 5.40 5 5 -4 59.49 6.20 -5 -5 4 47.60 5.50 -5 -5 4 50.59 5.80 4 5 -4 30.40 4.80 4 5 -4 26.90 4.50 4 5 -4 32.60 6.70 -4 -5 4 28.60 4.80 -4 -5 4 29.90 5.00 -4 -5 4 30.40 6.40 3 5 -4 217.68 12.30 3 5 -4 238.18 14.80 3 5 -4 211.38 12.80 -3 -5 4 213.08 12.60 -3 -5 4 244.68 13.20 -3 -5 4 241.98 14.70 2 5 -4 55.39 5.40 2 5 -4 42.60 4.60 -2 -5 4 51.39 6.00 -2 -5 4 52.49 5.40 -2 -5 4 46.20 4.80 1 5 -4 271.27 14.80 -1 -5 4 305.17 15.50 -1 -5 4 329.27 16.10 0 5 -4 198.98 10.70 0 -5 4 178.18 10.60 -1 5 -4 2.80 2.10 1 -5 4 1.10 2.20 -2 5 -4 691.83 33.30 -2 5 -4 745.13 32.60 2 -5 4 721.83 33.80 2 -5 4 773.12 33.00 -3 5 -4 304.67 16.10 -3 5 -4 323.17 17.80 3 -5 4 306.77 18.00 3 -5 4 345.27 16.80 -4 5 -4 289.97 17.60 -4 5 -4 294.77 15.40 4 -5 4 299.27 15.90 4 -5 4 292.87 18.20 -5 5 -4 1.20 1.90 5 -5 4 1.80 2.30 5 -5 4 -3.30 2.40 -6 5 -4 253.37 14.30 6 -5 4 239.68 14.50 6 -5 4 277.37 19.30 -7 5 -4 13.40 3.50 7 -5 4 8.40 6.00 7 -5 4 3.90 3.00 -8 5 -4 37.30 6.10 8 -5 4 39.50 9.10 8 -5 4 39.60 6.10 9 -5 4 46.30 5.90 9 -5 4 39.70 11.40 10 -5 4 6.20 3.40 10 -5 4 5.50 6.40 11 -5 4 5.80 8.70 11 -5 4 4.40 3.30 12 -5 4 -2.20 3.20 12 -5 4 5.80 8.10 13 -5 4 -8.70 6.10 13 -5 4 4.30 4.30 14 -5 4 8.30 9.90 14 -5 4 15.00 5.20 15 -5 4 0.00 8.90 16 4 -4 20.00 6.70 16 4 -4 3.50 9.30 -16 -4 4 7.30 5.40 15 4 -4 -0.10 7.90 15 4 -4 3.70 5.40 -15 -4 4 2.50 4.80 14 4 -4 21.60 6.80 14 4 -4 10.60 9.50 -14 -4 4 14.60 5.20 13 4 -4 14.50 5.10 13 4 -4 18.10 10.20 -13 -4 4 12.80 5.00 12 4 -4 -5.30 6.80 12 4 -4 15.20 5.20 -12 -4 4 -1.60 3.70 11 4 -4 10.70 8.30 11 4 -4 -4.90 3.40 -11 -4 4 -2.60 2.60 10 4 -4 103.39 9.90 10 4 -4 87.39 16.00 -10 -4 4 109.19 9.20 9 4 -4 245.68 15.60 9 4 -4 220.28 21.00 -9 -4 4 239.98 14.50 8 4 -4 3.10 3.00 8 4 -4 -0.50 4.20 -8 -4 4 1.70 2.40 7 4 -4 272.37 15.40 7 4 -4 229.88 19.20 -7 -4 4 240.58 14.10 -7 -4 4 239.88 16.20 6 4 -4 227.88 13.10 6 4 -4 199.48 17.10 6 4 -4 250.57 14.30 -6 -4 4 234.88 13.70 -6 -4 4 253.37 13.70 5 4 -4 77.49 6.40 5 4 -4 80.89 7.30 5 4 -4 72.79 9.30 -5 -4 4 95.19 7.20 -5 -4 4 82.89 6.80 -5 -4 4 95.69 9.30 4 4 -4 203.88 11.60 4 4 -4 221.48 12.60 4 4 -4 234.08 14.90 -4 -4 4 206.88 14.00 -4 -4 4 204.78 11.90 -4 -4 4 212.58 12.30 3 4 -4 160.08 10.20 3 4 -4 154.98 11.20 3 4 -4 182.38 9.70 -3 -4 4 176.78 11.60 -3 -4 4 157.18 10.10 -3 -4 4 156.48 9.70 2 4 -4 197.08 10.10 2 4 -4 175.68 10.50 2 4 -4 177.08 11.00 -2 -4 4 173.78 10.40 -2 -4 4 180.58 11.20 -2 -4 4 156.18 9.80 1 4 -4 254.67 12.00 1 4 -4 204.68 12.10 -1 -4 4 212.58 12.10 -1 -4 4 222.18 12.20 0 4 -4 1459.95 63.59 0 -4 4 1454.15 63.79 0 -4 4 1691.13 64.49 -1 4 -4 64.89 5.20 1 -4 4 54.89 5.00 1 -4 4 49.30 5.10 -2 4 -4 33.50 4.80 -2 4 -4 24.90 3.80 2 -4 4 28.70 4.70 2 -4 4 24.60 4.00 -3 4 -4 15.70 3.70 -3 4 -4 17.40 3.40 3 -4 4 21.50 4.70 3 -4 4 17.30 3.70 -4 4 -4 248.58 14.00 -4 4 -4 271.97 16.10 4 -4 4 264.57 16.70 -5 4 -4 13.30 3.50 5 -4 4 10.60 3.50 5 -4 4 10.50 4.70 -6 4 -4 41.00 5.30 6 -4 4 41.90 8.50 6 -4 4 44.70 6.20 -7 4 -4 4.70 3.00 7 -4 4 7.20 5.90 7 -4 4 7.90 3.40 -8 4 -4 21.90 4.90 8 -4 4 22.10 8.30 8 -4 4 28.20 5.50 9 -4 4 13.50 4.20 9 -4 4 8.80 7.00 10 -4 4 24.00 9.50 10 -4 4 29.90 6.00 11 -4 4 111.19 10.00 11 -4 4 97.09 17.60 12 -4 4 35.80 6.80 12 -4 4 31.00 11.60 13 -4 4 6.80 4.60 13 -4 4 2.70 8.00 14 -4 4 14.40 6.10 14 -4 4 3.50 9.40 -15 4 -4 21.30 5.30 15 -4 4 15.10 5.60 15 -4 4 5.90 8.80 16 3 -4 -4.50 8.40 16 3 -4 0.60 5.00 -16 -3 4 3.70 4.60 15 3 -4 -7.00 9.20 15 3 -4 5.00 5.00 -15 -3 4 -3.60 3.80 14 3 -4 9.50 4.90 14 3 -4 -2.90 6.20 -14 -3 4 -2.20 3.50 13 3 -4 1.60 4.40 13 3 -4 2.30 7.70 -13 -3 4 -7.70 3.20 12 3 -4 3.80 8.20 12 3 -4 -1.80 3.90 -12 -3 4 9.80 4.10 11 3 -4 17.70 5.30 11 3 -4 12.70 7.80 10 3 -4 57.69 8.40 10 3 -4 74.39 14.00 -10 -3 4 58.79 6.70 9 3 -4 42.70 6.80 9 3 -4 34.80 9.30 -9 -3 4 49.00 5.60 8 3 -4 28.10 5.60 8 3 -4 18.70 7.80 -8 -3 4 22.70 4.20 -8 -3 4 19.10 4.30 7 3 -4 272.27 15.70 7 3 -4 220.48 18.70 -7 -3 4 266.17 14.80 -7 -3 4 257.87 14.10 6 3 -4 1.30 2.40 6 3 -4 3.70 4.20 6 3 -4 2.20 2.00 -6 -3 4 0.10 1.90 5 3 -4 45.20 7.70 5 3 -4 59.89 6.20 5 3 -4 57.49 4.90 -5 -3 4 68.89 5.50 -5 -3 4 47.80 5.30 -5 -3 4 60.79 7.60 4 3 -4 620.54 33.10 4 3 -4 638.74 31.40 4 3 -4 776.22 30.70 -4 -3 4 718.33 30.70 -4 -3 4 731.73 33.50 -4 -3 4 668.33 31.30 3 3 -4 251.37 12.90 3 3 -4 238.98 13.80 3 3 -4 260.07 14.90 -3 -3 4 264.47 13.90 -3 -3 4 284.77 15.10 -3 -3 4 274.67 13.30 2 3 -4 376.46 18.70 2 3 -4 381.96 17.90 2 3 -4 382.86 18.70 -2 -3 4 386.06 18.70 -2 -3 4 380.06 18.70 -2 -3 4 412.86 18.30 1 3 -4 581.14 25.20 1 3 -4 514.55 24.30 -1 -3 4 538.35 24.10 -1 -3 4 597.34 25.20 -1 -3 4 531.55 24.50 0 3 -4 178.48 9.80 0 3 -4 178.18 9.40 0 -3 4 157.78 9.30 0 -3 4 156.08 9.30 -1 3 -4 533.55 24.80 -1 3 -4 551.34 24.50 1 -3 4 576.04 25.30 1 -3 4 552.14 24.70 -2 3 -4 1017.00 44.20 -2 3 -4 1057.69 44.80 2 -3 4 1091.19 45.10 2 -3 4 968.40 44.20 -3 3 -4 5.10 2.30 -3 3 -4 0.90 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5.00 7 -13 5 3.20 5.90 8 -13 5 12.10 7.90 8 -13 5 18.40 4.80 9 -13 5 0.80 6.30 9 -13 5 3.50 3.80 10 -13 5 12.50 4.90 10 -13 5 11.90 7.40 11 -13 5 12.00 4.50 11 -13 5 -13.30 5.10 12 -13 5 18.90 4.90 12 -13 5 4.80 7.60 13 -13 5 20.90 4.80 13 -13 5 17.50 10.30 13 12 -5 10.00 10.90 -13 -12 5 5.00 5.70 12 12 -5 -3.50 7.60 -12 -12 5 10.80 5.90 11 12 -5 11.70 9.20 -11 -12 5 5.10 5.10 10 12 -5 7.00 6.50 -10 -12 5 -5.80 5.20 9 12 -5 6.40 6.70 -9 -12 5 5.90 5.20 8 12 -5 -5.70 4.80 -8 -12 5 6.90 5.60 -7 -12 5 8.60 4.80 -6 -12 5 5.40 4.50 -5 -12 5 73.69 9.70 -3 -12 5 36.30 7.20 -2 -12 5 23.60 6.00 -1 -12 5 -4.30 2.10 0 -12 5 11.90 4.60 1 -12 5 71.19 8.10 2 -12 5 2.50 3.00 3 -12 5 10.70 4.10 3 -12 5 6.80 4.70 4 -12 5 133.59 14.00 4 -12 5 131.49 11.20 5 -12 5 86.79 9.00 5 -12 5 73.79 12.80 6 -12 5 -4.10 2.60 6 -12 5 -1.50 3.70 7 -12 5 36.70 9.40 7 -12 5 47.10 7.70 8 -12 5 0.10 5.20 8 -12 5 7.50 3.90 9 -12 5 18.10 5.30 9 -12 5 -4.20 5.30 10 -12 5 65.89 13.90 10 -12 5 63.59 8.30 11 -12 5 -1.50 6.80 11 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16.20 13 -11 5 54.49 7.70 14 -11 5 31.80 13.80 14 -11 5 42.20 6.50 14 10 -5 6.20 8.70 -14 -10 5 1.50 5.90 13 10 -5 -0.40 7.10 -13 -10 5 8.30 5.80 12 10 -5 7.70 8.40 -12 -10 5 -2.30 4.20 11 10 -5 62.59 15.50 -11 -10 5 34.20 8.60 10 10 -5 9.60 7.80 -10 -10 5 5.80 4.30 9 10 -5 65.39 14.10 -9 -10 5 52.69 9.50 8 10 -5 6.30 6.40 -8 -10 5 15.70 6.00 7 10 -5 13.20 6.90 -7 -10 5 12.50 5.40 6 10 -5 12.90 6.90 -6 -10 5 13.00 4.80 -5 -10 5 37.20 7.10 -4 -10 5 80.59 8.70 -3 -10 5 250.37 16.30 -2 -10 5 -0.10 2.50 -1 -10 5 77.19 8.30 0 -10 5 318.97 18.80 1 -10 5 573.54 29.00 2 -10 5 135.99 12.20 2 -10 5 142.19 10.80 3 -10 5 224.28 16.70 3 -10 5 211.28 14.10 4 -10 5 164.98 11.90 4 -10 5 147.59 13.70 5 -10 5 49.20 7.40 5 -10 5 36.20 8.10 6 -10 5 3.10 4.00 6 -10 5 1.40 3.10 7 -10 5 3.50 5.00 7 -10 5 3.90 3.00 8 -10 5 1.90 4.70 8 -10 5 2.60 3.20 9 -10 5 11.30 6.40 10 -10 5 54.29 13.40 10 -10 5 75.59 8.20 11 -10 5 70.89 15.30 11 -10 5 88.39 8.90 12 -10 5 66.59 16.00 12 -10 5 52.99 7.70 13 -10 5 9.70 4.50 13 -10 5 7.40 8.30 14 -10 5 8.70 8.40 14 -10 5 -1.30 3.90 14 9 -5 15.00 12.20 -14 -9 5 0.70 5.20 13 9 -5 -3.10 8.60 -13 -9 5 5.10 5.30 12 9 -5 -8.80 6.30 -12 -9 5 -4.00 3.50 11 9 -5 7.10 8.70 -11 -9 5 -1.80 3.40 -10 -9 5 27.20 7.50 9 9 -5 8.90 7.10 -9 -9 5 -0.70 3.80 8 9 -5 11.40 7.70 -8 -9 5 18.20 5.70 7 9 -5 66.59 12.80 -7 -9 5 66.99 8.50 6 9 -5 3.70 5.10 -6 -9 5 9.00 4.30 5 9 -5 101.79 11.90 -5 -9 5 97.99 9.50 -4 -9 5 26.90 5.60 -3 -9 5 709.93 34.70 -2 -9 5 81.99 8.30 -1 -9 5 163.18 11.70 0 -9 5 179.28 12.50 1 -9 5 167.78 11.70 2 -9 5 11.20 3.90 2 -9 5 0.60 3.20 3 -9 5 108.99 10.70 3 -9 5 107.39 9.20 -4 9 -5 44.60 6.20 4 -9 5 40.10 6.30 4 -9 5 30.50 7.30 -5 9 -5 225.48 13.50 5 -9 5 228.08 14.30 5 -9 5 209.28 17.30 -6 9 -5 37.90 6.50 6 -9 5 50.79 6.30 6 -9 5 40.40 9.10 7 -9 5 80.69 8.00 7 -9 5 68.69 12.20 8 -9 5 -0.70 3.10 8 -9 5 7.80 5.30 9 -9 5 14.70 4.90 9 -9 5 23.40 9.60 10 -9 5 7.50 7.30 10 -9 5 5.60 3.40 11 -9 5 5.30 6.80 11 -9 5 0.60 3.60 12 -9 5 -2.20 6.60 12 -9 5 13.00 4.20 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2.50 -8 -7 5 -1.50 2.80 7 7 -5 118.49 10.00 7 7 -5 118.79 14.00 -7 -7 5 124.89 10.20 6 7 -5 288.07 17.30 6 7 -5 291.27 21.20 -6 -7 5 273.17 16.80 -6 -7 5 316.07 17.90 5 7 -5 14.20 6.00 5 7 -5 13.50 4.20 -5 -7 5 13.10 4.00 -5 -7 5 19.20 4.30 4 7 -5 8.00 3.80 -4 -7 5 2.80 3.20 -4 -7 5 4.20 3.00 -3 -7 5 349.57 19.50 -3 -7 5 351.86 21.40 -3 -7 5 374.26 19.50 2 7 -5 141.29 9.30 -2 -7 5 116.99 9.20 -2 -7 5 121.79 10.40 -2 -7 5 126.39 9.30 1 7 -5 175.08 10.90 -1 -7 5 184.58 11.60 -1 -7 5 165.68 11.50 0 7 -5 45.60 4.90 0 -7 5 45.20 5.30 -1 7 -5 398.46 19.50 1 -7 5 370.26 19.90 -2 7 -5 223.68 12.90 2 -7 5 223.68 14.40 2 -7 5 230.28 13.50 -3 7 -5 78.79 7.90 -3 7 -5 67.69 6.20 3 -7 5 67.19 6.90 3 -7 5 75.09 8.20 -4 7 -5 568.84 27.30 4 -7 5 610.74 30.90 4 -7 5 538.95 27.70 -5 7 -5 0.10 2.50 5 -7 5 3.40 3.60 5 -7 5 -2.00 2.20 -6 7 -5 16.00 3.80 6 -7 5 16.40 5.70 6 -7 5 11.20 3.90 -7 7 -5 185.78 12.50 7 -7 5 196.38 17.20 7 -7 5 197.18 13.00 8 -7 5 70.89 7.50 8 -7 5 78.89 13.60 9 -7 5 20.60 5.00 9 -7 5 15.70 7.90 10 -7 5 1.10 3.40 10 -7 5 -5.70 5.80 11 -7 5 3.20 3.60 11 -7 5 5.00 6.80 12 -7 5 60.69 8.70 12 -7 5 46.20 13.70 13 -7 5 11.80 10.30 14 -7 5 10.80 5.10 14 -7 5 6.60 9.00 15 -7 5 19.50 11.50 15 -7 5 5.30 5.10 15 6 -5 4.40 5.50 15 6 -5 16.10 9.10 14 6 -5 15.20 9.60 14 6 -5 13.60 6.10 -14 -6 5 8.80 5.40 13 6 -5 35.30 11.60 13 6 -5 22.90 6.80 -13 -6 5 31.50 7.20 12 6 -5 -0.60 7.60 12 6 -5 9.60 5.20 -12 -6 5 6.10 4.50 11 6 -5 11.80 4.50 11 6 -5 0.80 6.80 -11 -6 5 -2.70 3.30 10 6 -5 37.30 11.70 10 6 -5 26.60 6.10 -10 -6 5 34.60 6.80 9 6 -5 70.89 8.30 9 6 -5 62.09 12.70 -9 -6 5 69.39 8.00 8 6 -5 -3.60 4.10 8 6 -5 3.90 3.10 -8 -6 5 3.50 3.00 7 6 -5 3.70 3.10 7 6 -5 17.10 6.30 -7 -6 5 0.60 2.70 -7 -6 5 0.60 2.60 6 6 -5 17.20 6.20 6 6 -5 24.00 5.10 -6 -6 5 20.20 4.50 -6 -6 5 32.40 5.40 5 6 -5 185.48 14.80 5 6 -5 183.18 12.30 -5 -6 5 191.08 12.40 -5 -6 5 180.18 12.10 4 6 -5 479.15 24.40 4 6 -5 499.25 26.90 4 6 -5 462.05 23.50 -4 -6 5 492.45 26.90 -4 -6 5 492.05 24.10 -4 -6 5 488.75 24.40 3 6 -5 4.20 2.50 3 6 -5 14.60 4.60 -3 -6 5 11.20 4.20 -3 -6 5 7.30 2.80 -3 -6 5 2.10 2.80 2 6 -5 66.89 6.00 -2 -6 5 75.59 7.30 -2 -6 5 69.09 6.40 -2 -6 5 72.09 6.50 1 6 -5 161.88 10.20 -1 -6 5 159.18 10.40 -1 -6 5 186.08 11.20 0 6 -5 40.10 4.70 0 -6 5 35.00 4.50 -1 6 -5 173.38 10.40 1 -6 5 189.58 11.30 1 -6 5 157.18 10.70 -2 6 -5 244.38 13.40 2 -6 5 224.58 13.50 2 -6 5 245.58 14.50 -3 6 -5 55.19 5.60 -3 6 -5 57.99 6.60 3 -6 5 66.29 7.30 3 -6 5 51.49 5.90 -4 6 -5 47.80 7.40 -4 6 -5 39.70 5.50 4 -6 5 30.00 6.30 4 -6 5 37.30 6.00 -5 6 -5 178.78 11.80 5 -6 5 206.38 12.90 5 -6 5 202.48 15.40 -6 6 -5 35.10 5.40 6 -6 5 20.60 6.80 6 -6 5 27.30 5.10 -7 6 -5 80.79 7.50 7 -6 5 82.19 13.40 7 -6 5 79.29 7.90 8 -6 5 25.30 8.70 8 -6 5 22.90 5.00 9 -6 5 32.80 6.30 9 -6 5 49.90 11.50 10 -6 5 7.30 3.90 10 -6 5 6.20 7.00 11 -6 5 65.79 8.50 11 -6 5 71.69 15.30 12 -6 5 5.80 4.90 12 -6 5 1.00 8.80 13 -6 5 7.30 7.60 13 -6 5 8.50 4.40 14 -6 5 13.90 9.60 14 -6 5 15.60 5.00 15 -6 5 1.70 10.20 15 -6 5 6.20 4.40 15 5 -5 20.40 7.00 15 5 -5 18.10 11.10 14 5 -5 -5.70 4.40 14 5 -5 7.00 8.60 -14 -5 5 -0.80 4.40 13 5 -5 37.80 7.90 13 5 -5 44.70 13.90 -13 -5 5 26.70 7.10 12 5 -5 9.80 8.40 12 5 -5 10.20 5.50 -12 -5 5 5.30 4.40 11 5 -5 -7.60 4.30 11 5 -5 -1.30 3.70 -11 -5 5 -3.60 2.80 10 5 -5 4.50 4.30 10 5 -5 7.30 6.50 -10 -5 5 5.70 3.60 9 5 -5 24.50 8.50 9 5 -5 26.40 5.80 -9 -5 5 24.80 5.30 8 5 -5 41.20 9.80 8 5 -5 35.70 6.30 -8 -5 5 43.10 6.50 7 5 -5 386.26 25.10 7 5 -5 349.07 20.10 -7 -5 5 385.26 19.80 -7 -5 5 324.37 19.00 6 5 -5 242.08 17.60 6 5 -5 214.38 13.80 -6 -5 5 216.08 13.60 -6 -5 5 209.18 13.20 5 5 -5 39.80 8.00 5 5 -5 41.20 6.20 5 5 -5 30.70 4.80 -5 -5 5 38.70 5.80 -5 -5 5 38.40 5.50 -5 -5 5 46.80 8.30 4 5 -5 100.39 9.60 4 5 -5 102.39 8.30 4 5 -5 108.89 7.50 -4 -5 5 89.19 7.80 -4 -5 5 100.29 7.60 -4 -5 5 86.59 8.90 3 5 -5 880.41 37.90 3 5 -5 856.01 38.80 3 5 -5 893.51 40.00 -3 -5 5 872.31 40.00 -3 -5 5 879.01 38.30 -3 -5 5 770.72 38.30 2 5 -5 262.97 15.80 2 5 -5 333.57 15.60 -2 -5 5 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4 -7 13.50 5.70 11 4 -7 15.40 7.70 -11 -4 7 7.20 3.70 10 4 -7 1.10 5.60 -10 -4 7 1.10 2.80 9 4 -7 6.10 4.00 9 4 -7 7.80 5.90 -9 -4 7 -0.50 2.60 8 4 -7 41.20 7.20 8 4 -7 54.79 5.90 8 4 -7 52.19 10.60 -8 -4 7 51.59 6.00 7 4 -7 28.50 6.00 7 4 -7 20.40 3.80 7 4 -7 10.40 4.90 -7 -4 7 19.80 4.30 6 4 -7 62.59 7.50 6 4 -7 58.89 5.50 6 4 -7 54.79 8.90 -6 -4 7 73.89 8.80 -6 -4 7 50.99 5.70 5 4 -7 385.06 21.70 5 4 -7 414.06 22.80 5 4 -7 388.76 19.60 -5 -4 7 417.26 21.60 -5 -4 7 432.06 20.30 -5 -4 7 352.16 21.50 4 4 -7 61.29 5.40 4 4 -7 60.69 6.60 4 4 -7 61.59 6.70 -4 -4 7 63.39 5.80 -4 -4 7 56.19 6.30 -4 -4 7 58.39 6.50 3 4 -7 32.60 4.20 3 4 -7 29.10 5.20 3 4 -7 30.80 4.70 -3 -4 7 32.50 4.70 -3 -4 7 43.00 5.00 -3 -4 7 26.40 4.90 2 4 -7 10.10 3.40 2 4 -7 15.50 3.40 -2 -4 7 8.00 3.30 -2 -4 7 11.30 2.60 -2 -4 7 16.40 3.50 1 4 -7 3.80 2.30 1 4 -7 4.80 2.90 -1 -4 7 3.00 2.70 0 4 -7 240.58 13.80 0 4 -7 254.77 13.60 0 -4 7 238.18 13.90 0 -4 7 215.88 13.30 0 -4 7 240.58 11.60 -1 4 -7 169.48 11.30 -1 4 -7 185.08 10.10 1 -4 7 173.68 10.20 1 -4 7 187.38 11.80 1 -4 7 195.28 11.30 -2 4 -7 20.80 4.00 -2 4 -7 28.60 4.80 2 -4 7 24.10 4.50 2 -4 7 17.20 3.70 2 -4 7 17.90 4.20 -3 4 -7 -1.00 2.00 -3 4 -7 -3.50 2.10 3 -4 7 -0.90 2.20 3 -4 7 1.10 2.90 -4 4 -7 76.19 8.00 -4 4 -7 67.29 7.10 4 -4 7 70.49 7.40 4 -4 7 75.39 9.10 5 -4 7 32.40 5.80 5 -4 7 38.70 7.90 6 -4 7 409.96 23.50 6 -4 7 445.86 27.50 7 -4 7 251.37 21.10 7 -4 7 280.07 17.60 8 -4 7 118.89 11.00 8 -4 7 98.69 15.70 9 -4 7 21.70 6.40 9 -4 7 50.69 12.20 10 -4 7 145.89 13.10 10 -4 7 139.49 18.20 11 -4 7 -9.30 3.90 11 -4 7 -4.00 6.90 12 -4 7 6.80 4.60 12 -4 7 15.20 8.40 13 -4 7 17.40 11.00 13 -4 7 22.20 7.70 14 -4 7 -7.30 5.40 14 -4 7 7.70 9.80 16 3 -7 -3.50 5.90 -16 -3 7 -4.40 3.80 15 3 -7 1.70 8.90 -15 -3 7 3.70 3.60 14 3 -7 13.90 9.80 14 3 -7 12.70 6.40 -14 -3 7 9.90 4.30 13 3 -7 8.50 8.90 13 3 -7 6.50 4.80 -13 -3 7 3.00 3.30 12 3 -7 46.50 9.20 12 3 -7 46.40 12.10 -12 -3 7 46.40 6.80 11 3 -7 14.90 8.00 11 3 -7 20.50 6.60 -11 -3 7 22.30 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8 -14 8 77.19 9.70 9 -14 8 41.40 8.60 9 -14 8 42.40 11.50 10 -14 8 40.40 12.00 10 -14 8 28.70 7.20 11 -14 8 -1.60 8.30 11 -14 8 21.90 6.30 12 -14 8 0.20 4.80 12 -14 8 -3.70 9.10 13 -14 8 1.90 9.80 -13 -13 8 4.50 6.00 12 13 -8 1.80 7.70 -12 -13 8 -0.90 4.60 11 13 -8 -0.90 7.90 10 13 -8 36.90 11.70 -10 -13 8 30.40 8.20 9 13 -8 -9.80 5.10 -9 -13 8 0.20 3.40 -8 -13 8 -1.30 3.90 -7 -13 8 4.40 4.10 -6 -13 8 3.40 4.30 -5 -13 8 28.20 7.40 -4 -13 8 30.40 7.70 -3 -13 8 43.30 8.50 -2 -13 8 -4.40 2.20 -1 -13 8 65.09 10.00 0 -13 8 80.49 9.90 1 -13 8 0.20 2.90 2 -13 8 213.38 15.90 2 -13 8 198.38 16.70 3 -13 8 98.09 10.80 3 -13 8 107.49 11.80 4 -13 8 22.00 6.90 4 -13 8 22.70 6.40 5 -13 8 7.60 4.40 5 -13 8 0.60 4.50 6 -13 8 86.89 10.20 6 -13 8 77.29 13.00 7 -13 8 32.30 7.10 7 -13 8 18.60 8.00 8 -13 8 17.80 8.20 8 -13 8 7.50 5.40 9 -13 8 16.20 5.60 9 -13 8 12.00 7.60 10 -13 8 8.00 6.80 10 -13 8 13.40 5.90 11 -13 8 -5.50 4.00 11 -13 8 -1.50 6.40 12 -13 8 9.70 4.40 12 -13 8 7.40 8.40 13 -13 8 15.90 11.60 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3.40 6.20 -11 -11 8 10.80 5.50 10 11 -8 -0.80 6.00 -10 -11 8 -0.20 3.80 9 11 -8 102.59 16.90 -9 -11 8 105.39 12.10 8 11 -8 58.79 12.50 -8 -11 8 30.10 7.50 -7 -11 8 19.90 6.10 -6 -11 8 4.80 3.90 -5 -11 8 4.90 4.00 -4 -11 8 92.09 10.10 -3 -11 8 2.40 3.50 -2 -11 8 2.60 3.00 -1 -11 8 48.30 8.30 0 -11 8 159.28 12.80 1 -11 8 44.80 8.20 2 -11 8 6.80 4.00 2 -11 8 -1.80 2.10 3 -11 8 21.80 6.00 3 -11 8 19.10 5.00 4 -11 8 3.90 3.90 4 -11 8 6.60 4.30 5 -11 8 49.60 9.20 5 -11 8 52.09 8.70 6 -11 8 69.89 12.30 6 -11 8 37.80 7.60 7 -11 8 20.90 5.70 7 -11 8 23.20 7.70 8 -11 8 1.30 5.70 8 -11 8 2.50 3.70 9 -11 8 57.49 12.80 9 -11 8 43.90 7.90 10 -11 8 -2.50 6.70 10 -11 8 6.70 4.20 11 -11 8 -0.70 5.90 12 -11 8 -5.80 3.90 12 -11 8 2.60 9.70 13 -11 8 9.30 5.30 13 -11 8 4.80 9.70 14 -11 8 1.50 4.90 14 10 -8 -1.50 7.90 14 10 -8 -6.50 4.60 13 10 -8 13.70 6.40 13 10 -8 8.60 8.60 -13 -10 8 14.70 6.20 12 10 -8 5.80 7.10 -12 -10 8 2.50 4.50 11 10 -8 20.60 7.10 11 10 -8 10.00 7.60 -11 -10 8 32.90 7.90 10 10 -8 1.10 5.10 10 10 -8 4.90 8.20 -10 -10 8 7.50 4.90 9 10 -8 7.20 6.40 9 10 -8 17.20 5.30 -9 -10 8 7.10 4.50 8 10 -8 9.80 6.40 8 10 -8 -1.30 3.60 -8 -10 8 -0.40 3.30 7 10 -8 14.60 6.50 7 10 -8 12.20 5.10 -7 -10 8 19.80 5.60 6 10 -8 -4.60 3.80 -6 -10 8 1.40 3.40 -5 -10 8 97.19 10.20 -4 -10 8 83.69 9.00 -3 -10 8 28.80 6.10 -2 -10 8 0.20 2.60 -1 -10 8 23.60 5.30 0 -10 8 419.16 23.70 1 -10 8 14.40 4.60 2 -10 8 16.30 4.90 2 -10 8 15.20 5.10 3 -10 8 232.18 16.60 3 -10 8 209.68 15.00 4 -10 8 376.16 21.80 4 -10 8 345.47 23.00 5 -10 8 49.80 8.10 5 -10 8 62.99 10.40 6 -10 8 35.10 6.90 6 -10 8 29.40 8.10 7 -10 8 24.50 8.40 7 -10 8 44.30 7.90 8 -10 8 16.90 5.10 8 -10 8 15.40 8.20 9 -10 8 -7.00 3.20 9 -10 8 -6.10 5.80 10 -10 8 -9.30 3.90 10 -10 8 1.70 6.50 11 -10 8 86.59 17.80 11 -10 8 87.99 12.20 12 -10 8 36.90 13.10 12 -10 8 30.70 7.90 13 -10 8 -10.20 4.90 13 -10 8 9.50 10.00 14 -10 8 20.80 11.60 14 9 -8 -14.60 7.60 14 9 -8 17.10 6.60 -14 -9 8 11.90 6.20 13 9 -8 27.20 10.50 13 9 -8 26.70 7.50 -13 -9 8 22.00 7.20 12 9 -8 9.30 5.60 12 9 -8 16.60 8.80 11 9 -8 11.10 5.00 11 9 -8 2.30 6.10 -11 -9 8 3.50 3.90 10 9 -8 46.90 8.50 10 9 -8 21.80 9.70 -10 -9 8 47.20 8.40 9 9 -8 31.60 9.20 9 9 -8 9.30 4.90 -9 -9 8 9.70 5.30 8 9 -8 6.10 5.80 8 9 -8 -0.50 3.50 -8 -9 8 10.90 4.40 7 9 -8 68.49 10.00 7 9 -8 82.49 13.50 -7 -9 8 84.39 9.20 6 9 -8 461.15 26.20 6 9 -8 456.95 28.90 -6 -9 8 479.25 26.10 5 9 -8 32.20 6.60 5 9 -8 22.30 6.40 -5 -9 8 24.70 6.30 -4 -9 8 43.10 7.40 -3 -9 8 210.38 14.40 -2 -9 8 1.90 2.80 -2 -9 8 8.00 4.00 -1 -9 8 108.69 9.70 0 -9 8 82.29 8.40 1 -9 8 269.77 17.70 1 -9 8 314.07 18.00 2 -9 8 239.58 15.70 2 -9 8 234.18 15.90 3 -9 8 290.87 19.10 3 -9 8 306.57 18.60 4 -9 8 -1.20 3.20 4 -9 8 3.20 3.00 5 -9 8 -0.90 3.00 5 -9 8 -1.50 3.40 6 -9 8 5.90 4.70 6 -9 8 2.40 3.40 7 -9 8 50.79 10.80 7 -9 8 39.80 7.90 8 -9 8 122.39 11.80 8 -9 8 154.08 17.20 9 -9 8 -1.10 6.70 9 -9 8 8.00 5.00 10 -9 8 9.20 4.40 10 -9 8 3.80 8.10 11 -9 8 53.59 9.30 11 -9 8 49.30 13.40 12 -9 8 16.40 9.90 12 -9 8 12.10 5.80 13 -9 8 8.20 5.60 13 -9 8 -4.00 10.10 14 -9 8 4.30 9.30 15 8 -8 1.60 8.90 15 8 -8 1.70 6.20 -15 -8 8 -4.50 5.20 14 8 -8 10.20 6.10 14 8 -8 13.10 7.90 13 8 -8 2.60 5.00 13 8 -8 3.40 7.70 -13 -8 8 -1.80 4.00 12 8 -8 1.70 6.30 12 8 -8 3.10 5.20 -12 -8 8 4.50 4.30 11 8 -8 7.80 7.10 11 8 -8 0.10 5.00 -11 -8 8 3.40 4.00 10 8 -8 11.90 5.10 10 8 -8 1.60 6.40 -10 -8 8 2.10 3.60 9 8 -8 -1.40 3.30 -9 -8 8 9.50 4.30 8 8 -8 -4.00 3.90 8 8 -8 4.50 3.90 -8 -8 8 7.60 4.00 7 8 -8 -0.20 4.20 7 8 -8 5.40 3.60 -7 -8 8 5.60 3.30 6 8 -8 13.10 4.60 6 8 -8 9.30 5.00 -6 -8 8 6.70 4.10 5 8 -8 97.39 9.80 5 8 -8 108.89 11.20 -5 -8 8 95.39 9.30 4 8 -8 11.70 4.50 -4 -8 8 14.30 4.50 -4 -8 8 15.40 5.00 3 8 -8 140.79 11.80 -3 -8 8 159.78 12.40 -3 -8 8 152.98 11.40 -2 -8 8 343.97 19.80 -2 -8 8 359.36 20.10 -1 -8 8 49.90 7.60 0 -8 8 4.40 3.40 1 -8 8 12.10 3.90 1 -8 8 6.40 3.50 2 -8 8 25.10 5.60 2 -8 8 32.30 5.80 -3 8 -8 221.08 14.50 3 -8 8 194.18 14.50 3 -8 8 211.08 14.40 4 -8 8 33.20 6.80 4 -8 8 21.20 5.50 5 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8.40 4 7 -8 68.39 8.20 4 7 -8 79.29 8.40 -4 -7 8 92.49 8.80 3 7 -8 2.40 3.10 -3 -7 8 -4.00 2.80 -3 -7 8 1.10 2.60 2 7 -8 1.60 2.70 -2 -7 8 3.10 2.80 -2 -7 8 2.90 2.40 -1 -7 8 31.80 6.00 0 -7 8 48.00 7.00 1 -7 8 132.09 10.60 1 -7 8 146.39 10.10 2 -7 8 136.09 10.40 2 -7 8 127.79 10.50 -3 7 -8 51.39 6.40 3 -7 8 60.89 7.30 3 -7 8 54.89 6.90 4 -7 8 246.88 16.20 4 -7 8 186.38 14.20 5 -7 8 6.90 4.10 5 -7 8 15.90 5.50 6 -7 8 10.60 4.30 6 -7 8 10.20 5.40 7 -7 8 195.88 18.00 7 -7 8 183.58 14.20 8 -7 8 3.60 3.50 8 -7 8 -5.70 4.50 9 -7 8 2.60 4.00 9 -7 8 6.30 7.10 10 -7 8 70.29 10.40 11 -7 8 5.40 4.30 11 -7 8 -5.10 6.90 12 -7 8 23.00 7.40 12 -7 8 0.30 9.90 13 -7 8 -0.40 7.60 13 -7 8 -8.20 5.20 14 -7 8 13.70 9.30 14 -7 8 2.10 5.10 15 6 -8 10.60 6.40 -15 -6 8 -5.90 4.60 14 6 -8 7.20 7.20 14 6 -8 2.10 5.10 -14 -6 8 -2.10 4.00 13 6 -8 17.70 6.30 13 6 -8 4.10 6.50 -13 -6 8 7.10 5.00 12 6 -8 -1.30 4.30 12 6 -8 11.20 7.80 -12 -6 8 8.60 4.00 11 6 -8 15.20 5.70 11 6 -8 19.20 8.60 10 6 -8 -5.60 3.60 10 6 -8 -2.00 5.10 -10 -6 8 -4.70 2.50 9 6 -8 136.49 15.60 9 6 -8 135.79 12.70 -9 -6 8 148.89 11.40 8 6 -8 253.47 19.80 8 6 -8 226.78 16.40 -8 -6 8 224.98 14.90 7 6 -8 2.10 4.30 7 6 -8 7.10 4.00 -7 -6 8 7.70 3.30 6 6 -8 30.60 6.00 6 6 -8 24.40 6.60 -6 -6 8 24.70 4.90 5 6 -8 17.30 5.30 -5 -6 8 17.70 4.20 -5 -6 8 13.10 4.70 4 6 -8 378.86 21.30 4 6 -8 369.76 20.70 -4 -6 8 338.67 20.50 -4 -6 8 403.06 20.30 3 6 -8 102.09 7.90 3 6 -8 91.09 8.70 -3 -6 8 88.39 9.50 -3 -6 8 95.49 8.20 -3 -6 8 113.89 8.90 2 6 -8 319.97 18.40 2 6 -8 326.17 17.40 -2 -6 8 324.47 18.40 -2 -6 8 291.77 17.50 -2 -6 8 332.17 17.00 1 6 -8 521.95 25.60 1 6 -8 498.65 26.40 -1 -6 8 520.05 26.20 -1 -6 8 553.34 26.70 0 6 -8 178.58 11.90 0 -6 8 190.58 12.30 0 -6 8 182.08 10.60 0 -6 8 177.48 12.10 -1 6 -8 49.70 6.80 1 -6 8 46.90 5.60 1 -6 8 52.79 5.40 1 -6 8 46.00 6.00 -2 6 -8 25.00 5.00 -2 6 -8 32.60 5.20 2 -6 8 33.90 5.50 2 -6 8 21.60 5.20 2 -6 8 31.70 5.20 -3 6 -8 137.09 10.50 3 -6 8 134.89 11.00 3 -6 8 163.38 11.80 -4 6 -8 517.05 27.50 4 -6 8 513.75 28.40 4 -6 8 529.55 27.50 5 -6 8 123.09 10.50 5 -6 8 99.29 11.30 6 -6 8 109.09 12.80 6 -6 8 129.89 11.10 7 -6 8 7.50 4.00 7 -6 8 3.40 5.60 8 -6 8 87.79 15.20 8 -6 8 87.19 9.90 9 -6 8 9.90 5.40 9 -6 8 20.30 8.80 10 -6 8 5.20 4.60 10 -6 8 2.90 8.20 11 -6 8 -15.40 6.30 11 -6 8 -0.90 3.80 12 -6 8 8.80 5.60 12 -6 8 -5.60 7.40 13 -6 8 57.29 15.80 13 -6 8 45.00 9.10 14 -6 8 -3.70 4.70 14 -6 8 9.20 10.20 16 5 -8 9.60 6.60 -16 -5 8 21.10 6.30 15 5 -8 21.90 10.90 15 5 -8 12.70 7.30 -15 -5 8 26.20 6.20 14 5 -8 -2.60 5.30 14 5 -8 16.10 8.10 -14 -5 8 6.30 4.20 13 5 -8 1.70 6.90 13 5 -8 2.10 5.40 -13 -5 8 -0.50 4.00 12 5 -8 15.70 9.00 12 5 -8 1.30 5.10 -12 -5 8 10.40 4.70 11 5 -8 31.90 7.30 11 5 -8 19.90 9.40 -11 -5 8 16.70 4.90 10 5 -8 8.80 4.60 10 5 -8 -2.60 5.10 -10 -5 8 0.20 2.90 9 5 -8 21.70 7.70 9 5 -8 17.70 6.00 -9 -5 8 19.80 4.70 8 5 -8 2.50 4.20 8 5 -8 2.40 3.00 7 5 -8 182.28 15.70 7 5 -8 200.38 14.50 -7 -5 8 209.28 13.00 6 5 -8 144.19 11.90 6 5 -8 145.09 12.90 6 5 -8 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9.30 4.80 3 -13 9 -1.10 3.60 3 -13 9 1.40 3.50 4 -13 9 19.70 6.40 4 -13 9 32.10 7.60 5 -13 9 21.10 7.20 5 -13 9 36.00 7.90 6 -13 9 167.28 14.80 6 -13 9 177.88 17.60 7 -13 9 51.99 11.40 7 -13 9 41.70 8.60 8 -13 9 17.80 7.60 8 -13 9 15.70 6.30 9 -13 9 1.90 7.10 10 -13 9 5.20 8.60 10 -13 9 -2.20 4.70 11 -13 9 35.40 8.20 11 -13 9 14.30 9.90 12 -13 9 31.70 13.60 12 -13 9 23.60 6.70 13 -13 9 34.10 12.90 13 -13 9 21.00 6.00 13 12 -9 -8.00 7.60 -13 -12 9 10.30 6.70 12 12 -9 18.90 9.70 11 12 -9 23.70 10.50 -11 -12 9 9.00 5.50 10 12 -9 22.50 8.90 9 12 -9 -8.70 4.10 -9 -12 9 8.20 4.70 8 12 -9 0.10 5.80 -8 -12 9 -0.30 4.40 -7 -12 9 6.50 4.60 -6 -12 9 43.80 8.50 -5 -12 9 1.80 4.00 -4 -12 9 73.69 10.70 -3 -12 9 88.59 10.10 -2 -12 9 16.40 5.60 -1 -12 9 63.69 9.70 0 -12 9 86.89 10.20 1 -12 9 132.79 12.30 1 -12 9 128.49 11.90 2 -12 9 17.10 5.50 2 -12 9 33.70 6.80 3 -12 9 79.29 10.00 3 -12 9 53.89 9.40 4 -12 9 11.60 5.30 4 -12 9 18.90 6.00 5 -12 9 51.59 10.00 5 -12 9 30.20 7.60 6 -12 9 5.80 5.80 6 -12 9 18.60 5.80 7 -12 9 7.40 6.30 7 -12 9 12.10 5.90 8 -12 9 18.30 6.40 8 -12 9 17.70 9.40 9 -12 9 6.20 3.80 9 -12 9 -6.70 5.20 10 -12 9 26.40 11.30 10 -12 9 35.80 8.40 11 -12 9 27.00 12.50 11 -12 9 29.00 8.00 12 -12 9 19.80 11.90 12 -12 9 5.20 5.30 13 -12 9 9.60 5.00 13 -12 9 2.80 9.10 14 11 -9 13.70 10.20 -14 -11 9 1.70 5.70 13 11 -9 12.00 9.70 -13 -11 9 1.10 5.90 12 11 -9 8.00 7.40 11 11 -9 -3.80 7.40 11 11 -9 5.50 5.70 -11 -11 9 17.50 6.20 10 11 -9 1.90 7.20 10 11 -9 18.70 6.10 -10 -11 9 10.60 5.30 9 11 -9 114.99 16.10 -9 -11 9 129.39 12.80 8 11 -9 51.49 11.30 -8 -11 9 37.60 8.40 7 11 -9 98.59 13.80 -7 -11 9 119.49 12.20 -6 -11 9 2.10 3.80 -5 -11 9 22.30 6.20 -4 -11 9 6.70 4.10 -3 -11 9 -1.60 2.10 -2 -11 9 393.06 23.40 -1 -11 9 33.00 6.80 0 -11 9 4.90 4.20 1 -11 9 16.80 5.50 1 -11 9 25.60 5.90 2 -11 9 2.60 3.30 2 -11 9 5.20 3.70 3 -11 9 72.39 9.20 3 -11 9 76.39 9.20 4 -11 9 91.29 11.10 4 -11 9 105.69 10.50 5 -11 9 268.97 18.20 5 -11 9 237.28 18.80 6 -11 9 38.10 8.80 6 -11 9 43.70 8.30 7 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10.70 4 -10 9 473.35 25.00 4 -10 9 352.26 24.20 5 -10 9 57.09 9.10 5 -10 9 56.49 10.10 6 -10 9 11.20 5.70 6 -10 9 1.90 3.80 7 -10 9 136.49 15.60 7 -10 9 162.18 13.80 8 -10 9 4.70 3.90 8 -10 9 -8.10 4.80 9 -10 9 -0.40 4.40 9 -10 9 6.50 7.80 10 -10 9 33.50 7.50 10 -10 9 45.80 13.30 11 -10 9 51.59 9.40 11 -10 9 67.19 15.70 12 -10 9 9.30 5.50 12 -10 9 -8.20 9.20 13 -10 9 -0.50 5.10 13 -10 9 8.10 9.70 14 -10 9 -8.50 4.90 15 9 -9 3.10 6.10 -15 -9 9 6.70 6.10 14 9 -9 -12.60 6.40 14 9 -9 0.70 5.60 -14 -9 9 -4.80 4.90 13 9 -9 -1.30 6.00 13 9 -9 0.80 5.10 -13 -9 9 4.40 5.20 12 9 -9 7.00 5.50 12 9 -9 -6.90 6.70 -12 -9 9 14.50 5.70 11 9 -9 -4.00 5.30 11 9 -9 1.20 5.30 -11 -9 9 6.40 4.20 10 9 -9 -2.30 6.80 10 9 -9 4.00 4.40 -10 -9 9 -2.30 3.60 9 9 -9 54.29 9.10 9 9 -9 40.90 10.70 -9 -9 9 42.20 8.30 8 9 -9 13.40 6.80 8 9 -9 -0.60 3.60 -8 -9 9 8.80 4.30 7 9 -9 71.09 11.70 7 9 -9 90.19 10.00 -7 -9 9 67.59 8.80 6 9 -9 6.00 4.90 6 9 -9 17.60 5.30 -6 -9 9 18.10 5.30 5 9 -9 2.60 3.50 5 9 -9 4.30 3.40 -5 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4.80 8 8 -9 7.60 5.60 -8 -8 9 8.10 4.30 7 8 -9 150.08 13.10 7 8 -9 149.69 14.90 -7 -8 9 156.88 12.30 6 8 -9 116.59 12.00 6 8 -9 106.29 10.40 -6 -8 9 107.09 10.20 5 8 -9 374.16 23.20 5 8 -9 405.86 23.30 -5 -8 9 386.86 22.00 4 8 -9 310.27 18.60 -4 -8 9 258.47 17.70 -4 -8 9 261.17 16.80 3 8 -9 76.49 8.80 -3 -8 9 81.39 8.30 -3 -8 9 66.59 7.90 -2 -8 9 271.47 16.10 -2 -8 9 208.28 14.30 -1 -8 9 9.90 4.10 0 -8 9 72.69 6.90 0 -8 9 63.09 7.50 1 -8 9 248.18 15.20 1 -8 9 251.57 16.40 2 -8 9 203.78 14.10 2 -8 9 184.88 13.20 -3 8 -9 282.47 17.90 3 -8 9 309.67 19.10 3 -8 9 321.87 19.00 4 -8 9 95.69 9.70 4 -8 9 115.69 11.10 5 -8 9 49.20 8.10 5 -8 9 53.59 9.40 6 -8 9 17.80 7.00 6 -8 9 22.40 5.90 7 -8 9 4.70 5.60 7 -8 9 7.80 4.70 8 -8 9 11.00 4.80 8 -8 9 14.70 8.20 9 -8 9 212.28 16.70 9 -8 9 224.98 22.10 10 -8 9 26.60 7.20 10 -8 9 12.60 9.00 11 -8 9 16.00 10.10 11 -8 9 31.10 7.30 12 -8 9 -10.90 4.40 12 -8 9 -3.60 8.00 13 -8 9 1.70 5.20 13 -8 9 12.40 9.80 14 -8 9 14.00 10.10 14 -8 9 11.10 5.80 15 7 -9 11.40 6.70 15 7 -9 13.40 9.30 -15 -7 9 3.70 5.10 14 7 -9 28.60 8.90 14 7 -9 26.40 10.80 -14 -7 9 39.50 8.40 13 7 -9 12.50 5.90 13 7 -9 -3.70 7.30 -13 -7 9 1.50 4.30 12 7 -9 5.00 5.30 12 7 -9 -0.20 7.00 -12 -7 9 6.50 4.50 11 7 -9 3.50 6.20 11 7 -9 1.80 4.30 -11 -7 9 2.80 3.90 10 7 -9 5.50 4.00 10 7 -9 -3.30 5.20 -10 -7 9 1.50 3.30 9 7 -9 66.69 12.60 9 7 -9 59.79 10.00 -9 -7 9 69.19 8.20 8 7 -9 7.10 4.20 8 7 -9 1.70 5.30 -8 -7 9 10.30 4.40 7 7 -9 41.30 9.00 7 7 -9 45.30 8.00 -7 -7 9 48.40 7.60 6 7 -9 30.30 6.30 6 7 -9 23.30 6.30 5 7 -9 33.70 6.60 5 7 -9 38.00 7.20 -5 -7 9 31.60 5.90 -5 -7 9 42.60 7.20 4 7 -9 1.50 2.90 4 7 -9 -2.20 2.30 -4 -7 9 7.00 3.50 -4 -7 9 5.00 3.40 3 7 -9 162.48 13.00 -3 -7 9 178.58 12.50 -3 -7 9 177.58 12.10 2 7 -9 104.59 9.80 -2 -7 9 127.59 9.10 -2 -7 9 114.09 9.70 -1 -7 9 60.49 7.40 0 -7 9 155.78 10.20 0 -7 9 173.18 12.20 1 -7 9 155.08 11.80 1 -7 9 133.29 9.70 -2 7 -9 16.20 3.70 2 -7 9 12.40 5.00 -3 7 -9 -2.20 2.30 3 -7 9 1.50 3.20 3 -7 9 2.00 3.00 4 -7 9 52.09 8.70 4 -7 9 56.79 8.80 5 -7 9 71.89 9.80 5 -7 9 81.59 9.20 6 -7 9 3.70 4.50 6 -7 9 0.10 3.30 7 -7 9 142.69 12.80 7 -7 9 155.48 16.30 8 -7 9 103.79 11.60 8 -7 9 115.49 14.80 9 -7 9 15.20 8.80 9 -7 9 12.30 5.40 10 -7 9 5.60 8.90 10 -7 9 19.10 6.40 11 -7 9 -9.40 3.40 11 -7 9 -6.10 5.50 12 -7 9 62.59 16.90 12 -7 9 71.79 11.40 13 -7 9 -11.90 4.70 13 -7 9 13.70 10.00 14 -7 9 15.20 10.70 14 -7 9 11.40 6.50 15 6 -9 -11.70 6.90 15 6 -9 -10.90 5.60 -15 -6 9 7.60 4.80 14 6 -9 -0.20 6.30 14 6 -9 26.50 10.20 -14 -6 9 16.30 5.30 13 6 -9 13.40 6.00 13 6 -9 3.50 6.70 -13 -6 9 11.00 5.10 12 6 -9 25.20 10.20 12 6 -9 17.90 7.00 -12 -6 9 14.90 4.90 11 6 -9 0.30 5.70 11 6 -9 0.60 3.60 -11 -6 9 4.00 3.50 10 6 -9 -1.10 4.10 10 6 -9 1.10 5.40 -10 -6 9 0.20 3.00 9 6 -9 8.60 4.80 -9 -6 9 11.10 4.40 8 6 -9 19.90 6.70 8 6 -9 15.70 5.10 -8 -6 9 12.00 4.20 7 6 -9 90.29 10.20 7 6 -9 108.79 11.50 -7 -6 9 99.69 8.90 6 6 -9 123.39 12.00 6 6 -9 138.29 11.70 -6 -6 9 136.39 10.40 5 6 -9 16.60 4.70 5 6 -9 12.00 4.80 -5 -6 9 11.90 5.00 -5 -6 9 13.80 4.30 4 6 -9 90.49 8.50 4 6 -9 101.79 9.90 -4 -6 9 95.39 8.60 -4 -6 9 108.79 9.10 3 6 -9 4.20 3.10 -3 -6 9 3.70 3.00 -3 -6 9 5.20 3.40 2 6 -9 121.79 10.80 2 6 -9 140.19 11.00 -2 -6 9 157.28 11.20 -2 -6 9 144.59 9.20 1 6 -9 11.10 4.10 1 6 -9 9.40 3.60 -1 -6 9 14.90 4.10 -1 -6 9 13.00 3.80 0 -6 9 42.80 4.50 0 -6 9 54.69 7.70 0 -6 9 43.50 6.70 1 -6 9 214.28 12.10 1 -6 9 208.58 13.40 1 -6 9 176.08 13.30 -2 6 -9 611.54 28.10 2 -6 9 539.55 28.40 2 -6 9 582.44 29.90 2 -6 9 596.94 28.50 -3 6 -9 46.00 5.80 3 -6 9 45.30 5.90 3 -6 9 58.09 7.40 3 -6 9 53.99 8.20 -4 6 -9 192.58 15.00 4 -6 9 166.58 13.10 4 -6 9 178.88 14.10 5 -6 9 49.50 9.00 5 -6 9 40.60 7.60 6 -6 9 61.99 9.60 6 -6 9 56.49 10.00 7 -6 9 15.10 5.50 7 -6 9 20.00 7.80 8 -6 9 28.20 7.40 8 -6 9 38.60 9.80 9 -6 9 4.00 4.50 9 -6 9 0.30 6.50 10 -6 9 5.40 4.60 10 -6 9 4.20 7.00 11 -6 9 -4.50 4.20 11 -6 9 0.80 6.60 12 -6 9 19.20 6.80 12 -6 9 11.60 9.30 13 -6 9 9.10 9.50 13 -6 9 16.70 7.10 14 -6 9 -3.70 5.80 14 -6 9 -15.20 7.00 16 5 -9 16.90 8.40 16 5 -9 14.40 10.40 -16 -5 9 15.90 5.90 15 5 -9 42.30 14.00 15 5 -9 26.10 7.90 -15 -5 9 19.70 5.60 14 5 -9 4.40 7.00 13 5 -9 32.30 11.00 13 5 -9 14.60 6.40 -13 -5 9 13.20 4.70 12 5 -9 8.30 5.10 12 5 -9 2.00 6.10 -12 -5 9 1.20 3.60 11 5 -9 31.50 11.60 -11 -5 9 8.60 3.90 10 5 -9 14.40 5.70 10 5 -9 11.50 6.70 -10 -5 9 12.50 4.30 9 5 -9 10.40 6.30 9 5 -9 3.40 4.00 -9 -5 9 6.90 3.20 8 5 -9 120.49 11.20 8 5 -9 97.69 12.20 -8 -5 9 93.99 8.50 7 5 -9 398.96 24.90 7 5 -9 423.86 24.10 -7 -5 9 388.26 21.20 6 5 -9 256.87 17.50 6 5 -9 271.97 17.70 -6 -5 9 267.97 17.40 -6 -5 9 254.37 15.30 5 5 -9 86.49 8.80 5 5 -9 68.29 6.80 5 5 -9 82.19 8.30 -5 -5 9 81.19 7.70 -5 -5 9 87.79 8.70 4 5 -9 226.78 14.30 4 5 -9 242.98 14.30 4 5 -9 253.37 16.40 -4 -5 9 262.27 14.70 -4 -5 9 262.27 15.20 3 5 -9 66.79 5.70 3 5 -9 67.39 7.60 3 5 -9 65.49 6.30 -3 -5 9 62.69 6.80 -3 -5 9 60.89 5.70 2 5 -9 202.58 13.50 2 5 -9 173.58 11.90 -2 -5 9 206.38 10.60 -2 -5 9 211.38 13.20 -2 -5 9 190.88 13.00 1 5 -9 230.48 13.90 1 5 -9 201.48 14.00 -1 -5 9 240.98 11.20 -1 -5 9 244.18 14.60 -1 -5 9 236.58 14.60 0 5 -9 661.73 32.50 0 5 -9 715.73 32.70 0 -5 9 683.33 29.60 0 -5 9 671.13 32.50 0 -5 9 673.43 33.10 -1 5 -9 235.18 12.30 -1 5 -9 208.28 15.20 1 -5 9 219.18 13.80 1 -5 9 224.58 12.50 1 -5 9 235.68 15.00 -2 5 -9 5.00 2.30 2 -5 9 2.50 3.20 2 -5 9 7.70 3.50 -3 5 -9 19.20 4.60 3 -5 9 18.10 5.20 3 -5 9 25.00 5.80 3 -5 9 19.40 4.30 -4 5 -9 8.20 3.40 4 -5 9 11.50 4.90 4 -5 9 2.40 3.40 4 -5 9 1.80 2.60 5 -5 9 27.40 6.20 5 -5 9 14.60 6.30 6 -5 9 30.70 7.10 6 -5 9 46.00 9.10 7 -5 9 187.48 15.00 7 -5 9 196.68 18.20 8 -5 9 115.49 17.60 8 -5 9 92.19 10.80 9 -5 9 191.18 20.30 9 -5 9 183.58 15.40 10 -5 9 16.00 6.10 10 -5 9 5.40 7.30 11 -5 9 10.20 8.20 11 -5 9 12.50 5.90 12 -5 9 6.30 9.90 12 -5 9 -7.50 4.90 13 -5 9 0.20 5.30 13 -5 9 6.20 8.70 14 -5 9 12.10 7.00 14 -5 9 31.10 13.90 16 4 -9 9.10 9.50 16 4 -9 6.90 7.10 -16 -4 9 3.30 5.00 15 4 -9 3.80 6.10 15 4 -9 -14.20 6.60 -15 -4 9 -2.30 4.00 14 4 -9 -8.70 4.50 14 4 -9 -6.70 6.10 -14 -4 9 -0.80 3.40 13 4 -9 4.00 8.50 13 4 -9 12.20 6.40 -13 -4 9 8.40 4.20 12 4 -9 18.90 9.60 12 4 -9 20.40 6.00 -12 -4 9 16.30 4.40 11 4 -9 20.00 6.60 11 4 -9 17.40 8.20 -11 -4 9 26.30 5.30 10 4 -9 43.30 10.20 10 4 -9 40.80 8.40 -10 -4 9 42.80 6.40 9 4 -9 18.90 7.10 9 4 -9 16.80 5.50 -9 -4 9 15.00 4.10 8 4 -9 42.90 5.20 8 4 -9 50.99 10.10 8 4 -9 61.99 9.80 -8 -4 9 59.69 6.40 7 4 -9 5.60 2.50 7 4 -9 8.40 4.70 7 4 -9 7.10 4.00 -7 -4 9 7.80 3.20 6 4 -9 -0.20 1.70 6 4 -9 2.40 3.60 6 4 -9 -3.20 2.70 -6 -4 9 3.80 3.60 -6 -4 9 0.00 2.20 5 4 -9 269.27 16.50 5 4 -9 250.87 14.60 5 4 -9 271.07 17.50 -5 -4 9 286.97 16.70 -5 -4 9 288.97 15.80 4 4 -9 11.00 3.30 4 4 -9 5.70 2.70 4 4 -9 12.70 4.20 -4 -4 9 6.80 3.20 -4 -4 9 11.80 3.30 3 4 -9 296.97 17.30 3 4 -9 291.37 15.60 3 4 -9 280.07 13.90 -3 -4 9 284.97 13.90 -3 -4 9 245.48 16.00 -3 -4 9 266.67 15.80 2 4 -9 21.70 4.20 2 4 -9 15.10 4.00 -2 -4 9 14.70 3.90 -2 -4 9 10.20 4.00 -2 -4 9 14.30 2.10 1 4 -9 71.29 7.30 1 4 -9 71.79 6.50 -1 -4 9 75.19 7.20 -1 -4 9 52.49 6.10 0 4 -9 134.69 9.80 0 4 -9 129.09 9.70 0 -4 9 115.19 6.90 0 -4 9 124.59 9.80 0 -4 9 124.89 9.20 -1 4 -9 23.20 3.60 -1 4 -9 26.90 4.90 -1 4 -9 29.50 5.30 1 -4 9 30.50 4.50 1 -4 9 29.50 5.80 1 -4 9 21.60 4.30 -2 4 -9 110.39 7.90 2 -4 9 91.69 9.00 2 -4 9 92.29 7.90 2 -4 9 106.49 8.70 -3 4 -9 7.40 3.10 3 -4 9 6.90 4.10 3 -4 9 3.00 4.20 -4 4 -9 4.20 3.00 4 -4 9 4.90 3.60 4 -4 9 4.20 2.40 5 -4 9 -5.50 3.40 5 -4 9 -2.20 3.00 5 -4 9 -2.40 1.80 6 -4 9 165.08 11.00 6 -4 9 167.88 15.60 6 -4 9 181.38 14.20 7 -4 9 1.10 4.60 7 -4 9 4.30 4.50 8 -4 9 1.40 4.10 8 -4 9 9.70 6.50 9 -4 9 86.19 12.40 9 -4 9 79.59 15.30 10 -4 9 -6.90 5.80 10 -4 9 -6.80 3.90 11 -4 9 -5.50 5.30 11 -4 9 3.40 5.10 12 -4 9 -5.90 7.30 12 -4 9 8.00 4.80 13 -4 9 8.70 6.20 13 -4 9 10.70 9.80 14 -4 9 -2.90 4.00 14 -4 9 0.00 5.50 14 -4 9 -2.20 9.80 16 3 -9 31.00 11.10 16 3 -9 -5.70 5.70 -16 -3 9 10.40 4.70 15 3 -9 5.30 7.80 15 3 -9 1.30 5.80 14 3 -9 4.40 4.90 14 3 -9 11.40 8.70 13 3 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5.90 16 2 -9 21.80 10.40 -16 -2 9 2.80 4.40 15 2 -9 -11.50 6.90 15 2 -9 18.60 7.10 -15 -2 9 -8.50 3.30 14 2 -9 15.40 9.80 14 2 -9 9.20 5.70 -14 -2 9 0.00 5.10 -14 -2 9 9.30 3.60 13 2 -9 38.30 8.90 13 2 -9 69.19 15.40 -13 -2 9 52.99 6.40 -13 -2 9 42.70 6.70 12 2 -9 22.30 9.40 12 2 -9 40.20 9.50 -12 -2 9 26.60 5.20 -12 -2 9 25.80 5.30 11 2 -9 102.69 13.60 11 2 -9 98.39 11.50 -11 -2 9 83.99 7.40 -11 -2 9 66.49 7.10 10 2 -9 93.69 12.60 10 2 -9 62.29 10.30 -10 -2 9 71.59 6.80 9 2 -9 62.69 5.40 9 2 -9 88.59 13.30 9 2 -9 71.29 10.60 -9 -2 9 74.39 6.70 8 2 -9 17.80 3.10 8 2 -9 14.40 5.70 8 2 -9 11.00 4.50 -8 -2 9 20.00 3.90 7 2 -9 5.70 4.10 7 2 -9 1.10 3.40 7 2 -9 8.80 2.40 6 2 -9 109.99 7.40 6 2 -9 118.29 10.50 6 2 -9 122.69 10.60 -6 -2 9 100.09 9.20 -6 -2 9 104.09 8.10 5 2 -9 12.60 3.00 5 2 -9 4.00 3.30 5 2 -9 12.60 4.20 -5 -2 9 15.90 4.00 -5 -2 9 5.10 2.90 4 2 -9 65.09 5.60 4 2 -9 54.89 5.50 4 2 -9 58.39 7.00 -4 -2 9 45.50 5.80 -4 -2 9 56.49 5.10 3 2 -9 500.55 25.50 3 2 -9 490.15 23.80 3 2 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35.10 4.30 10 -2 9 49.30 14.30 11 -2 9 60.59 11.00 11 -2 9 46.20 4.80 11 -2 9 55.49 4.70 11 -2 9 68.59 15.70 12 -2 9 25.90 8.20 13 -2 9 35.50 8.80 13 -2 9 34.10 13.10 14 -2 9 14.50 6.80 14 -2 9 -2.50 8.70 16 1 -9 23.40 10.70 16 1 -9 14.60 7.30 15 1 -9 -1.10 8.40 15 1 -9 5.30 6.10 -15 -1 9 2.40 3.20 -15 -1 9 13.70 4.40 14 1 -9 61.49 15.30 14 1 -9 52.29 10.60 -14 -1 9 62.59 7.30 -14 -1 9 73.79 6.60 13 1 -9 3.70 4.20 13 1 -9 1.60 7.00 -13 -1 9 7.20 3.00 12 1 -9 12.50 8.70 12 1 -9 9.20 5.50 -12 -1 9 7.40 3.40 -12 -1 9 16.00 3.90 11 1 -9 6.20 4.80 11 1 -9 9.40 6.60 -11 -1 9 -0.20 2.60 10 1 -9 8.60 5.50 10 1 -9 -1.40 3.80 -10 -1 9 6.00 2.40 -10 -1 9 3.20 2.60 9 1 -9 102.29 12.40 9 1 -9 103.29 6.60 9 1 -9 91.99 10.90 -9 -1 9 105.59 7.40 8 1 -9 75.89 9.80 8 1 -9 74.09 5.20 8 1 -9 57.79 9.20 -8 -1 9 56.79 5.60 7 1 -9 111.49 10.70 7 1 -9 115.89 11.50 7 1 -9 107.39 6.90 -7 -1 9 108.19 7.70 6 1 -9 139.29 11.30 6 1 -9 131.79 8.20 6 1 -9 132.79 11.70 -6 -1 9 117.99 10.10 -6 -1 9 140.29 9.00 5 1 -9 142.89 10.50 5 1 -9 170.08 12.40 5 1 -9 134.19 8.80 -5 -1 9 145.89 9.50 -5 -1 9 131.29 9.70 4 1 -9 31.90 4.70 4 1 -9 23.10 5.10 4 1 -9 34.50 4.40 -4 -1 9 39.70 5.50 -4 -1 9 31.60 4.10 3 1 -9 11.00 2.30 3 1 -9 8.30 2.70 3 1 -9 6.20 3.40 -3 -1 9 3.90 2.70 -3 -1 9 7.20 2.90 2 1 -9 442.56 23.00 2 1 -9 472.55 19.60 2 1 -9 428.36 22.10 -2 -1 9 424.46 22.30 -2 -1 9 439.96 22.50 1 1 -9 629.84 26.10 1 1 -9 573.34 28.50 1 1 -9 590.04 28.80 -1 -1 9 577.14 28.90 -1 -1 9 602.34 28.30 0 1 -9 40.30 5.60 0 1 -9 33.60 5.40 0 1 -9 35.50 4.10 0 -1 9 38.00 4.10 0 -1 9 37.60 6.10 0 -1 9 34.40 4.50 -1 1 -9 200.18 11.90 -1 1 -9 189.88 11.90 1 -1 9 209.48 11.80 1 -1 9 216.38 12.60 1 -1 9 194.08 13.50 -2 1 -9 92.79 8.50 -2 1 -9 97.29 7.00 2 -1 9 89.39 8.60 2 -1 9 75.39 8.90 2 -1 9 108.39 7.10 -3 1 -9 29.60 5.90 3 -1 9 25.90 3.60 3 -1 9 25.30 5.90 3 -1 9 30.30 6.40 4 -1 9 3.10 3.50 4 -1 9 1.10 1.70 4 -1 9 1.10 3.90 5 -1 9 12.40 5.10 5 -1 9 14.80 6.00 5 -1 9 11.70 2.70 6 -1 9 39.60 3.70 6 -1 9 39.50 8.00 6 -1 9 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5.80 9 10 -10 5.90 5.10 -9 -10 10 8.70 5.10 8 10 -10 166.48 17.50 8 10 -10 165.68 15.20 -8 -10 10 163.48 14.10 7 10 -10 29.50 8.10 -7 -10 10 23.40 6.60 6 10 -10 95.49 11.70 6 10 -10 102.39 11.10 -6 -10 10 97.39 10.20 5 10 -10 0.10 3.00 -5 -10 10 -4.80 2.30 -4 -10 10 -6.50 2.30 -3 -10 10 28.00 6.00 -2 -10 10 4.00 3.10 -2 -10 10 7.60 4.30 -1 -10 10 59.29 7.70 0 -10 10 390.56 23.10 1 -10 10 68.69 10.10 1 -10 10 61.29 7.50 2 -10 10 200.78 14.70 2 -10 10 195.58 14.90 3 -10 10 3.60 3.50 3 -10 10 -0.90 3.50 4 -10 10 5.00 4.10 4 -10 10 -6.00 2.90 5 -10 10 -0.90 3.80 5 -10 10 -1.30 3.70 6 -10 10 52.79 9.10 6 -10 10 52.29 10.80 7 -10 10 151.08 13.60 7 -10 10 123.19 15.30 8 -10 10 40.50 8.20 8 -10 10 31.40 10.00 9 -10 10 7.20 4.80 9 -10 10 -6.10 5.80 10 -10 10 79.49 16.10 10 -10 10 89.79 10.50 11 -10 10 10.00 9.20 12 -10 10 12.90 11.20 12 -10 10 9.90 6.10 13 -10 10 -9.50 4.70 13 -10 10 -5.60 9.20 15 9 -10 3.90 9.60 15 9 -10 8.70 6.40 -15 -9 10 8.20 5.60 14 9 -10 -1.90 5.30 14 9 -10 2.60 8.80 -14 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10 1.80 5.70 7 -9 10 10.60 5.40 8 -9 10 67.49 10.80 8 -9 10 48.00 12.10 9 -9 10 10.00 8.90 9 -9 10 10.40 5.00 10 -9 10 37.90 8.70 10 -9 10 28.10 12.00 11 -9 10 6.20 5.00 11 -9 10 1.30 9.30 12 -9 10 51.29 15.10 12 -9 10 50.89 9.40 13 -9 10 0.60 5.80 13 -9 10 -8.60 8.30 15 8 -10 12.00 11.00 15 8 -10 29.40 9.30 -15 -8 10 42.30 8.50 14 8 -10 32.40 11.90 14 8 -10 23.50 8.10 13 8 -10 39.50 12.20 13 8 -10 30.60 8.80 -13 -8 10 33.20 8.00 12 8 -10 16.30 9.60 12 8 -10 7.50 5.90 -12 -8 10 16.10 5.90 11 8 -10 10.10 5.30 11 8 -10 15.90 8.50 -11 -8 10 16.00 5.20 10 8 -10 33.00 10.50 10 8 -10 6.70 5.60 -10 -8 10 3.90 4.70 9 8 -10 2.60 5.70 9 8 -10 0.50 4.30 -9 -8 10 6.00 3.90 8 8 -10 121.99 14.00 8 8 -10 141.99 13.20 -8 -8 10 140.49 11.90 7 8 -10 320.87 20.60 7 8 -10 276.57 21.30 -7 -8 10 306.77 18.90 6 8 -10 254.77 18.20 6 8 -10 246.88 17.70 -6 -8 10 241.48 16.40 5 8 -10 290.57 19.20 5 8 -10 275.17 18.80 -5 -8 10 328.97 18.90 -5 -8 10 299.37 19.70 4 8 -10 95.39 10.50 -4 -8 10 118.09 10.30 -4 -8 10 120.29 10.30 3 8 -10 156.78 12.70 -3 -8 10 170.78 12.50 -3 -8 10 115.39 10.40 2 8 -10 10.40 4.10 -2 -8 10 6.50 3.80 -2 -8 10 15.60 4.10 -1 -8 10 167.58 12.80 0 -8 10 105.59 8.40 0 -8 10 111.89 10.40 1 -8 10 216.18 16.10 1 -8 10 271.77 15.20 2 -8 10 75.59 7.90 2 -8 10 86.59 9.20 -3 8 -10 55.69 6.90 3 -8 10 62.79 7.80 3 -8 10 82.19 8.70 4 -8 10 61.59 9.30 4 -8 10 59.49 8.30 5 -8 10 1.30 4.00 5 -8 10 1.90 4.10 6 -8 10 56.09 9.30 6 -8 10 59.99 11.20 7 -8 10 226.98 17.20 7 -8 10 230.18 20.40 8 -8 10 4.50 7.10 8 -8 10 9.50 5.40 9 -8 10 309.07 20.90 9 -8 10 272.47 25.20 10 -8 10 23.50 7.30 10 -8 10 23.10 11.30 11 -8 10 -3.00 4.00 12 -8 10 -5.90 7.30 12 -8 10 6.40 5.40 13 -8 10 11.50 5.50 13 -8 10 16.70 10.30 15 7 -10 17.20 7.30 15 7 -10 13.90 8.80 -15 -7 10 9.50 4.90 14 7 -10 12.10 5.70 14 7 -10 15.80 9.80 -14 -7 10 10.70 4.90 13 7 -10 -4.60 4.60 13 7 -10 10.50 7.80 -13 -7 10 1.30 4.20 12 7 -10 9.20 7.30 12 7 -10 -0.70 4.30 -12 -7 10 -7.80 3.30 11 7 -10 11.20 7.90 11 7 -10 10.60 5.50 -11 -7 10 2.40 3.90 10 7 -10 8.20 5.00 10 7 -10 1.20 5.70 -10 -7 10 7.80 4.20 9 7 -10 138.19 15.40 9 7 -10 137.19 13.50 -9 -7 10 138.69 11.60 8 7 -10 10.50 5.10 8 7 -10 5.50 5.00 -8 -7 10 4.90 3.70 7 7 -10 3.10 4.80 7 7 -10 7.00 5.40 -7 -7 10 7.50 3.80 6 7 -10 42.70 8.00 6 7 -10 46.00 8.20 -6 -7 10 42.10 7.20 5 7 -10 6.40 4.00 5 7 -10 9.20 4.10 -5 -7 10 12.80 4.20 -5 -7 10 4.80 3.60 4 7 -10 30.50 5.70 4 7 -10 35.80 6.90 -4 -7 10 20.20 5.00 -4 -7 10 31.90 6.10 3 7 -10 117.29 10.80 -3 -7 10 119.49 9.10 -3 -7 10 108.79 9.70 2 7 -10 92.79 9.10 -2 -7 10 90.49 7.20 -2 -7 10 70.99 8.40 1 7 -10 309.07 18.40 -1 -7 10 259.27 16.90 0 -7 10 136.49 11.10 0 -7 10 133.69 9.00 1 -7 10 1.60 2.40 1 -7 10 6.20 3.80 -2 7 -10 3.40 2.60 2 -7 10 7.00 3.30 2 -7 10 6.50 4.10 -3 7 -10 74.89 7.40 3 -7 10 65.29 9.60 3 -7 10 63.69 8.00 4 -7 10 74.19 9.20 4 -7 10 86.69 9.60 5 -7 10 199.38 16.50 5 -7 10 204.98 15.20 6 -7 10 78.39 12.50 6 -7 10 96.19 10.50 7 -7 10 36.40 10.10 7 -7 10 29.00 7.00 8 -7 10 16.20 8.40 8 -7 10 29.10 7.60 9 -7 10 4.70 7.60 9 -7 10 20.00 7.00 10 -7 10 9.10 5.10 10 -7 10 10.90 8.40 11 -7 10 5.20 5.50 11 -7 10 4.90 8.00 12 -7 10 50.79 15.00 12 -7 10 30.00 8.70 13 -7 10 11.20 8.50 13 -7 10 3.00 5.80 14 -7 10 22.20 7.60 -16 -6 10 -2.60 5.60 15 6 -10 5.30 6.60 15 6 -10 2.30 8.50 -15 -6 10 -6.70 4.70 14 6 -10 10.00 6.80 14 6 -10 12.60 10.10 -14 -6 10 9.00 5.40 13 6 -10 21.30 7.20 13 6 -10 0.40 7.10 -13 -6 10 16.70 5.50 12 6 -10 -10.30 5.50 12 6 -10 12.20 6.00 -12 -6 10 3.10 3.50 11 6 -10 8.00 6.80 -11 -6 10 3.20 3.30 10 6 -10 3.60 4.80 10 6 -10 7.20 6.50 9 6 -10 -4.70 3.90 9 6 -10 -1.70 3.80 -9 -6 10 -3.90 2.50 8 6 -10 47.20 8.30 8 6 -10 30.00 8.00 -8 -6 10 31.20 6.30 7 6 -10 240.18 17.20 7 6 -10 242.98 17.60 -7 -6 10 200.08 14.20 6 6 -10 355.16 22.40 6 6 -10 366.36 22.70 -6 -6 10 392.26 21.20 -6 -6 10 384.56 22.40 5 6 -10 23.40 5.50 5 6 -10 13.90 4.90 -5 -6 10 21.60 5.10 -5 -6 10 21.00 4.90 4 6 -10 9.20 4.20 4 6 -10 7.80 3.20 -4 -6 10 0.30 2.80 -4 -6 10 5.20 2.90 3 6 -10 544.05 28.40 -3 -6 10 490.25 27.10 -3 -6 10 567.34 25.80 2 6 -10 10.30 4.30 -2 -6 10 11.40 4.30 -2 -6 10 13.30 2.90 1 6 -10 329.87 20.50 -1 -6 10 394.26 21.40 -1 -6 10 390.56 17.50 0 6 -10 98.99 9.20 0 -6 10 77.89 8.30 0 -6 10 80.89 6.20 1 -6 10 33.50 6.90 1 -6 10 26.70 4.50 -2 6 -10 195.68 11.80 2 -6 10 190.38 14.00 2 -6 10 171.28 12.20 -3 6 -10 32.00 5.40 3 -6 10 22.50 6.30 3 -6 10 23.00 6.00 4 -6 10 3.80 3.50 4 -6 10 0.50 3.90 5 -6 10 -1.90 2.50 5 -6 10 -1.10 3.90 6 -6 10 1.50 3.20 6 -6 10 0.90 4.90 7 -6 10 68.99 13.10 7 -6 10 79.49 10.00 8 -6 10 183.68 19.30 8 -6 10 155.58 14.60 9 -6 10 20.40 6.00 9 -6 10 22.70 9.90 10 -6 10 0.40 7.20 10 -6 10 5.40 4.10 11 -6 10 3.50 5.40 11 -6 10 -4.40 7.30 12 -6 10 5.10 5.50 12 -6 10 2.10 7.40 13 -6 10 9.90 8.60 13 -6 10 5.40 5.90 14 -6 10 2.30 6.80 14 -6 10 9.20 9.10 16 5 -10 0.40 6.70 16 5 -10 -2.30 9.10 -16 -5 10 10.30 5.10 15 5 -10 8.70 9.90 15 5 -10 4.60 5.90 -15 -5 10 5.30 4.50 14 5 -10 -0.40 5.10 -14 -5 10 -1.60 3.70 13 5 -10 -6.90 4.20 13 5 -10 -10.30 6.60 -13 -5 10 10.90 4.20 12 5 -10 -11.30 4.70 12 5 -10 9.10 5.10 -12 -5 10 0.30 3.50 11 5 -10 85.39 15.30 11 5 -10 76.99 11.70 -11 -5 10 68.09 8.10 10 5 -10 91.69 11.40 10 5 -10 108.49 14.40 -10 -5 10 95.89 9.10 9 5 -10 54.39 9.50 9 5 -10 51.19 10.40 -9 -5 10 53.69 6.80 8 5 -10 253.37 17.60 8 5 -10 220.48 18.20 -8 -5 10 223.78 14.50 7 5 -10 315.17 20.80 7 5 -10 305.17 20.20 -7 -5 10 320.47 18.30 6 5 -10 19.00 5.50 6 5 -10 25.50 6.10 -6 -5 10 22.30 4.80 -6 -5 10 40.40 6.80 5 5 -10 49.50 6.30 5 5 -10 39.70 7.20 -5 -5 10 52.99 6.10 -5 -5 10 51.29 7.40 4 5 -10 992.60 41.90 4 5 -10 882.71 40.60 4 5 -10 861.21 43.40 -4 -5 10 888.81 41.90 -4 -5 10 925.81 40.80 3 5 -10 792.82 37.50 3 5 -10 746.53 35.50 -3 -5 10 767.82 36.20 -3 -5 10 744.43 33.30 2 5 -10 698.93 34.70 2 5 -10 649.93 33.50 -2 -5 10 754.92 33.90 -2 -5 10 652.13 29.20 1 5 -10 429.76 23.00 -1 -5 10 402.76 22.70 -1 -5 10 409.56 18.30 -1 -5 10 456.95 23.20 0 5 -10 33.70 6.00 0 -5 10 29.20 3.50 0 -5 10 30.90 6.00 0 -5 10 31.50 5.60 -1 5 -10 116.29 7.60 1 -5 10 123.19 8.40 1 -5 10 115.69 10.20 1 -5 10 113.39 9.20 -2 5 -10 -0.50 1.90 2 -5 10 2.00 2.30 2 -5 10 -2.80 3.20 2 -5 10 2.50 3.40 3 -5 10 16.90 5.30 3 -5 10 23.30 5.00 3 -5 10 34.40 6.60 -4 5 -10 135.49 10.90 4 -5 10 132.89 12.20 4 -5 10 125.69 9.60 4 -5 10 131.59 11.50 5 -5 10 144.59 12.60 5 -5 10 135.09 13.50 5 -5 10 138.99 10.20 6 -5 10 54.29 6.80 6 -5 10 72.19 12.00 6 -5 10 66.69 10.10 7 -5 10 263.87 18.80 7 -5 10 254.87 21.40 8 -5 10 0.50 4.20 8 -5 10 3.30 5.80 9 -5 10 23.00 7.30 9 -5 10 18.40 9.70 10 -5 10 -1.40 4.20 10 -5 10 5.80 7.10 11 -5 10 -0.30 7.60 11 -5 10 2.50 5.90 12 -5 10 21.80 12.70 12 -5 10 24.10 7.00 13 -5 10 18.50 10.50 14 -5 10 3.50 6.90 16 4 -10 -0.80 5.70 16 4 -10 19.20 10.20 -16 -4 10 10.50 5.10 15 4 -10 22.60 7.80 15 4 -10 23.50 11.30 -15 -4 10 15.50 5.40 14 4 -10 13.60 9.30 14 4 -10 14.00 7.20 -14 -4 10 15.50 4.90 13 4 -10 -8.70 3.80 13 4 -10 -0.70 7.20 -13 -4 10 -5.60 3.20 12 4 -10 2.90 4.50 12 4 -10 17.00 9.00 -12 -4 10 10.70 4.20 11 4 -10 46.60 9.70 11 4 -10 38.00 11.00 -11 -4 10 66.79 7.10 10 4 -10 1.80 4.40 10 4 -10 8.30 6.30 -10 -4 10 -3.20 2.40 9 4 -10 23.00 6.30 9 4 -10 14.60 6.70 -9 -4 10 10.90 3.80 8 4 -10 5.90 4.30 8 4 -10 3.80 3.70 8 4 -10 2.80 2.70 -8 -4 10 6.40 3.20 7 4 -10 15.50 5.90 7 4 -10 27.50 4.50 -7 -4 10 21.90 4.90 6 4 -10 52.59 8.20 6 4 -10 57.39 8.70 6 4 -10 64.99 5.80 -6 -4 10 56.99 6.50 -6 -4 10 54.99 8.00 5 4 -10 181.48 11.70 5 4 -10 171.78 13.70 5 4 -10 196.28 12.90 -5 -4 10 196.48 12.50 -5 -4 10 199.58 12.50 4 4 -10 641.64 29.70 4 4 -10 612.94 31.80 4 4 -10 618.14 28.70 -4 -4 10 604.24 28.40 -4 -4 10 641.34 30.50 3 4 -10 249.88 12.40 3 4 -10 263.17 16.50 3 4 -10 260.77 15.10 -3 -4 10 255.27 12.50 -3 -4 10 267.17 15.70 2 4 -10 79.19 8.00 2 4 -10 63.39 6.90 -2 -4 10 65.49 7.50 -2 -4 10 79.89 7.50 1 4 -10 114.79 9.70 1 4 -10 133.79 10.50 -1 -4 10 146.09 10.60 -1 -4 10 142.99 10.80 0 4 -10 44.30 5.70 0 4 -10 48.10 3.40 0 -4 10 44.30 6.40 0 -4 10 39.50 3.70 0 -4 10 37.30 6.40 -1 4 -10 291.27 16.80 -1 4 -10 291.57 14.80 1 -4 10 283.17 17.80 1 -4 10 309.97 15.60 1 -4 10 290.47 16.70 -2 4 -10 35.80 5.30 2 -4 10 33.60 6.50 2 -4 10 45.70 5.60 2 -4 10 47.10 6.70 -3 4 -10 27.40 5.10 3 -4 10 29.60 6.10 3 -4 10 28.60 6.80 3 -4 10 24.30 4.70 -4 4 -10 11.00 3.70 4 -4 10 -0.40 3.50 4 -4 10 10.00 3.40 4 -4 10 4.30 3.90 5 -4 10 6.30 4.50 5 -4 10 1.80 3.90 5 -4 10 2.70 2.70 6 -4 10 27.60 8.20 6 -4 10 28.30 5.00 6 -4 10 22.70 6.30 7 -4 10 99.69 8.30 7 -4 10 87.79 14.60 7 -4 10 98.89 11.20 8 -4 10 17.40 7.70 8 -4 10 15.10 6.40 9 -4 10 134.89 17.60 9 -4 10 109.69 9.50 9 -4 10 129.79 13.40 10 -4 10 60.69 13.70 10 -4 10 37.70 8.50 10 -4 10 47.60 6.50 11 -4 10 22.20 4.70 11 -4 10 14.90 6.10 12 -4 10 22.80 5.50 12 -4 10 -1.70 7.20 13 -4 10 -2.10 8.10 13 -4 10 9.50 6.10 16 3 -10 15.10 7.60 16 3 -10 8.70 10.10 -16 -3 10 12.60 4.90 15 3 -10 4.90 10.70 15 3 -10 13.10 7.70 14 3 -10 4.60 6.00 14 3 -10 -2.10 6.90 -14 -3 10 -0.20 3.40 13 3 -10 8.50 5.50 13 3 -10 -0.20 6.60 -13 -3 10 11.70 4.40 12 3 -10 43.10 9.80 12 3 -10 22.10 9.60 -12 -3 10 35.50 6.10 11 3 -10 39.90 10.90 11 3 -10 32.70 8.20 -11 -3 10 43.90 6.50 -11 -3 10 19.70 8.30 10 3 -10 84.19 10.60 10 3 -10 62.49 11.90 10 3 -10 59.19 6.10 -10 -3 10 62.79 7.00 9 3 -10 120.59 13.60 9 3 -10 101.09 11.10 9 3 -10 109.59 7.90 -9 -3 10 95.89 8.50 8 3 -10 28.80 7.20 8 3 -10 28.80 4.30 -8 -3 10 22.30 4.70 7 3 -10 66.29 8.60 7 3 -10 65.49 6.00 7 3 -10 71.39 9.20 -7 -3 10 79.69 8.60 -7 -3 10 75.89 7.00 6 3 -10 -2.80 3.00 6 3 -10 -2.30 2.70 6 3 -10 4.40 2.10 -6 -3 10 1.80 2.60 -6 -3 10 -3.30 2.20 5 3 -10 281.27 18.30 5 3 -10 310.77 17.00 5 3 -10 279.57 15.60 -5 -3 10 326.97 16.90 -5 -3 10 268.77 15.70 4 3 -10 3.80 2.40 4 3 -10 1.00 3.00 4 3 -10 3.30 2.50 -4 -3 10 3.10 3.10 -4 -3 10 4.50 2.30 3 3 -10 106.39 9.70 3 3 -10 100.39 6.20 3 3 -10 109.09 8.60 -3 -3 10 106.19 8.80 -3 -3 10 118.99 6.10 2 3 -10 756.72 36.20 2 3 -10 787.42 35.50 -2 -3 10 742.03 35.70 -2 -3 10 733.63 35.60 1 3 -10 666.43 32.30 1 3 -10 684.63 32.80 -1 -3 10 685.03 32.20 -1 -3 10 657.83 32.70 0 3 -10 455.75 19.40 0 3 -10 445.16 22.80 0 -3 10 432.76 19.60 0 -3 10 419.96 22.30 0 -3 10 449.26 23.90 -1 3 -10 0.20 1.90 -1 3 -10 3.50 2.70 1 -3 10 0.20 2.10 1 -3 10 1.50 2.20 1 -3 10 -1.20 2.60 -2 3 -10 327.97 18.30 -2 3 -10 353.66 18.50 2 -3 10 355.66 20.70 2 -3 10 334.57 18.10 2 -3 10 367.96 19.40 -3 3 -10 255.57 15.40 3 -3 10 240.18 16.60 3 -3 10 260.97 16.50 3 -3 10 210.98 13.50 -4 3 -10 232.98 17.30 4 -3 10 206.78 15.80 4 -3 10 208.88 12.50 4 -3 10 209.98 15.60 5 -3 10 59.49 9.20 5 -3 10 60.79 5.90 5 -3 10 63.49 10.50 6 -3 10 109.49 11.60 6 -3 10 94.49 7.60 6 -3 10 92.99 12.40 7 -3 10 98.19 8.00 7 -3 10 113.29 12.30 7 -3 10 109.89 14.10 8 -3 10 26.30 4.60 8 -3 10 32.20 10.30 8 -3 10 29.20 7.70 9 -3 10 -0.10 3.00 9 -3 10 -3.80 4.40 9 -3 10 7.60 7.30 10 -3 10 18.70 8.30 10 -3 10 5.20 5.30 10 -3 10 -2.90 3.00 11 -3 10 -4.10 4.00 11 -3 10 -8.40 7.50 12 -3 10 -5.50 5.30 12 -3 10 15.90 10.10 12 -3 10 2.50 4.00 13 -3 10 -10.90 9.50 13 -3 10 17.60 7.30 16 2 -10 -9.60 7.00 16 2 -10 2.70 7.30 -16 -2 10 -3.60 3.90 15 2 -10 9.00 10.00 15 2 -10 4.60 6.90 -15 -2 10 5.00 6.20 14 2 -10 2.10 7.80 14 2 -10 10.60 5.80 13 2 -10 76.19 11.90 13 2 -10 87.99 16.50 -13 -2 10 77.39 8.10 -13 -2 10 99.79 8.20 12 2 -10 100.29 12.60 12 2 -10 84.49 15.60 -12 -2 10 97.59 8.30 -12 -2 10 103.69 8.60 11 2 -10 46.50 9.80 11 2 -10 43.90 11.50 -11 -2 10 36.40 5.70 -11 -2 10 48.90 6.10 10 2 -10 33.90 9.30 10 2 -10 36.40 8.20 10 2 -10 34.90 4.50 -10 -2 10 48.00 5.50 9 2 -10 3.60 4.20 9 2 -10 1.70 2.00 9 2 -10 0.70 4.30 -9 -2 10 -1.50 2.40 8 2 -10 137.29 8.70 8 2 -10 140.39 13.40 8 2 -10 142.99 12.90 -8 -2 10 149.29 9.90 7 2 -10 229.08 16.50 7 2 -10 243.38 16.70 7 2 -10 212.58 12.30 -7 -2 10 222.48 15.10 -7 -2 10 225.18 13.20 6 2 -10 0.10 1.80 6 2 -10 5.60 4.00 -6 -2 10 5.10 2.80 -6 -2 10 5.30 2.70 5 2 -10 649.14 33.70 5 2 -10 689.03 30.90 5 2 -10 660.63 31.80 -5 -2 10 681.23 31.50 -5 -2 10 655.53 30.90 4 2 -10 307.97 15.80 4 2 -10 279.67 18.20 4 2 -10 328.37 16.70 -4 -2 10 311.07 15.20 -4 -2 10 290.07 16.80 3 2 -10 8.90 2.10 3 2 -10 2.80 3.10 3 2 -10 13.20 3.70 -3 -2 10 2.00 3.00 2 2 -10 27.50 5.20 2 2 -10 21.00 4.80 -2 -2 10 33.40 5.60 -2 -2 10 23.00 4.90 1 2 -10 2.80 2.50 1 2 -10 5.40 3.30 1 2 -10 5.80 1.40 -1 -2 10 3.50 2.50 -1 -2 10 -1.30 2.40 0 2 -10 282.47 13.90 0 2 -10 275.27 16.10 0 -2 10 272.47 15.70 0 -2 10 289.07 14.00 0 -2 10 294.97 17.40 -1 2 -10 -1.80 2.00 -1 2 -10 2.20 2.20 1 -2 10 6.90 2.40 1 -2 10 2.60 3.10 -2 2 -10 269.17 15.40 -2 2 -10 286.47 16.50 2 -2 10 282.77 15.50 2 -2 10 283.57 18.00 2 -2 10 308.37 17.30 -3 2 -10 41.00 7.00 3 -2 10 46.80 4.90 3 -2 10 38.10 7.00 4 -2 10 140.39 9.20 4 -2 10 147.49 13.10 4 -2 10 145.89 13.00 5 -2 10 7.20 5.30 5 -2 10 11.70 3.00 5 -2 10 8.20 4.70 6 -2 10 12.40 5.70 6 -2 10 5.00 4.60 7 -2 10 1.00 5.00 7 -2 10 4.70 2.60 8 -2 10 -4.90 4.50 8 -2 10 2.50 5.50 8 -2 10 -0.10 2.30 9 -2 10 33.00 4.20 9 -2 10 37.70 9.20 9 -2 10 33.60 11.10 10 -2 10 18.10 8.60 10 -2 10 33.30 8.50 11 -2 10 56.29 14.60 11 -2 10 53.49 10.70 12 -2 10 10.10 6.80 12 -2 10 3.40 8.60 13 -2 10 -2.00 5.60 13 -2 10 13.50 9.60 16 1 -10 -2.30 6.70 16 1 -10 22.80 11.60 15 1 -10 14.50 7.30 15 1 -10 2.90 7.10 -15 -1 10 9.20 3.80 -15 -1 10 1.10 3.00 14 1 -10 36.20 11.70 14 1 -10 25.00 8.50 -14 -1 10 27.70 4.60 -14 -1 10 24.20 4.30 13 1 -10 5.40 4.90 13 1 -10 -1.40 5.30 -13 -1 10 -0.60 2.80 12 1 -10 7.40 5.70 12 1 -10 5.40 6.60 -12 -1 10 8.60 3.40 -12 -1 10 9.20 3.60 11 1 -10 35.80 10.20 11 1 -10 20.80 6.80 -11 -1 10 27.50 4.50 -11 -1 10 32.50 4.50 10 1 -10 91.79 14.90 10 1 -10 101.79 6.50 10 1 -10 91.79 11.40 -10 -1 10 81.59 7.00 9 1 -10 291.57 13.70 9 1 -10 257.87 20.30 9 1 -10 234.58 18.60 -9 -1 10 272.37 14.60 8 1 -10 208.58 17.10 8 1 -10 252.37 18.00 8 1 -10 221.18 12.00 -8 -1 10 249.78 13.30 7 1 -10 141.89 12.20 7 1 -10 128.79 7.90 7 1 -10 116.99 11.40 -7 -1 10 107.99 8.30 -7 -1 10 117.29 11.60 6 1 -10 101.49 7.30 6 1 -10 111.99 10.50 6 1 -10 108.09 9.70 -6 -1 10 92.99 8.60 -6 -1 10 108.09 8.00 5 1 -10 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10 -14 36.50 8.60 -4 -10 14 40.90 7.20 -4 -10 14 23.60 6.50 3 10 -14 20.50 5.70 -3 -10 14 14.70 4.80 -3 -10 14 9.50 4.90 -2 -10 14 10.70 5.00 -2 -10 14 14.60 4.00 -1 -10 14 39.80 8.40 -1 -10 14 37.90 5.30 0 -10 14 1.90 4.60 1 -10 14 26.30 7.40 1 -10 14 45.20 6.90 2 -10 14 58.59 10.80 2 -10 14 60.09 7.90 3 -10 14 5.40 4.10 3 -10 14 3.30 4.50 4 -10 14 63.69 10.30 4 -10 14 40.20 8.90 5 -10 14 0.10 5.10 5 -10 14 7.90 5.50 6 -10 14 24.10 7.60 6 -10 14 35.90 9.80 7 -10 14 202.38 19.70 7 -10 14 173.78 16.90 8 -10 14 75.49 12.40 8 -10 14 83.59 15.30 9 -10 14 14.20 6.70 9 -10 14 20.10 10.60 10 -10 14 24.20 10.20 10 -10 14 38.70 10.10 11 -10 14 -5.50 4.90 11 -10 14 -9.60 6.70 12 -10 14 0.40 8.00 12 -10 14 12.60 7.00 -15 -9 14 -4.80 5.20 14 9 -14 -6.20 6.60 14 9 -14 7.40 8.20 -14 -9 14 17.10 7.10 13 9 -14 1.40 5.60 13 9 -14 3.80 5.10 -13 -9 14 16.90 6.00 12 9 -14 18.70 7.40 12 9 -14 15.70 8.80 -12 -9 14 10.50 5.50 11 9 -14 52.29 11.10 11 9 -14 46.70 9.60 -11 -9 14 28.20 7.60 10 9 -14 5.90 6.00 10 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3.30 -3 8 -14 49.50 6.80 3 -8 14 51.99 8.40 3 -8 14 45.20 8.90 4 -8 14 66.39 10.90 4 -8 14 64.39 10.20 5 -8 14 5.10 5.10 5 -8 14 6.20 5.60 6 -8 14 92.29 12.90 6 -8 14 99.39 12.50 7 -8 14 31.50 8.90 7 -8 14 23.10 8.90 8 -8 14 33.70 9.10 8 -8 14 13.80 7.00 9 -8 14 32.10 9.00 9 -8 14 44.20 11.80 10 -8 14 22.10 10.40 10 -8 14 -2.60 4.70 11 -8 14 0.20 6.30 11 -8 14 15.00 9.00 12 -8 14 23.00 11.00 15 7 -14 -10.80 6.70 15 7 -14 8.70 6.80 -15 -7 14 1.50 4.60 14 7 -14 8.70 7.30 14 7 -14 -0.90 6.60 -14 -7 14 4.80 5.40 13 7 -14 17.80 6.90 13 7 -14 0.60 6.80 -13 -7 14 1.70 4.60 12 7 -14 13.00 8.20 12 7 -14 13.00 7.60 -12 -7 14 17.10 6.70 11 7 -14 6.00 4.90 11 7 -14 1.10 4.60 -11 -7 14 5.40 4.80 10 7 -14 -1.60 5.10 10 7 -14 10.00 5.80 -10 -7 14 13.90 5.20 9 7 -14 216.38 18.40 9 7 -14 185.48 17.20 -9 -7 14 221.38 16.20 8 7 -14 78.39 11.60 8 7 -14 70.59 11.90 -8 -7 14 68.59 10.00 7 7 -14 94.39 9.70 7 7 -14 67.69 11.20 -7 -7 14 109.09 10.80 -7 -7 14 89.99 9.90 6 7 -14 138.59 13.70 6 7 -14 114.29 10.20 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9.10 3 -6 14 54.99 8.30 4 -6 14 11.60 4.90 4 -6 14 8.40 5.40 5 -6 14 4.10 4.60 5 -6 14 3.80 4.40 6 -6 14 -1.70 5.40 6 -6 14 2.20 5.10 7 -6 14 46.90 10.70 7 -6 14 74.59 12.40 8 -6 14 90.39 15.90 8 -6 14 72.69 13.30 9 -6 14 -0.40 6.20 9 -6 14 8.30 6.40 10 -6 14 24.90 9.80 10 -6 14 13.50 6.70 11 -6 14 -5.60 6.20 11 -6 14 -6.70 5.10 12 -6 14 12.80 6.20 12 -6 14 21.20 9.40 15 5 -14 -6.20 7.10 15 5 -14 0.50 7.10 -15 -5 14 9.80 4.80 14 5 -14 -7.20 6.10 14 5 -14 -0.80 4.70 -14 -5 14 -5.40 4.00 13 5 -14 7.30 6.10 13 5 -14 -5.20 5.40 -13 -5 14 5.40 4.00 12 5 -14 113.39 14.90 12 5 -14 88.39 15.00 -12 -5 14 115.69 11.00 11 5 -14 182.98 18.00 11 5 -14 189.58 18.40 -11 -5 14 169.48 13.60 10 5 -14 98.69 13.10 10 5 -14 95.09 14.40 -10 -5 14 122.19 11.00 9 5 -14 33.50 8.50 9 5 -14 36.60 8.70 -9 -5 14 46.20 7.70 8 5 -14 124.19 12.00 8 5 -14 119.79 13.10 -8 -5 14 108.39 10.60 7 5 -14 15.80 6.00 7 5 -14 15.30 4.60 -7 -5 14 12.00 4.20 -7 -5 14 5.70 4.20 6 5 -14 73.19 7.20 6 5 -14 61.99 10.10 -6 -5 14 59.19 9.10 -6 -5 14 69.19 6.90 5 5 -14 20.00 3.80 5 5 -14 16.70 5.10 -5 -5 14 13.50 3.00 -5 -5 14 23.40 6.10 4 5 -14 211.28 16.30 -4 -5 14 226.68 15.80 -4 -5 14 202.08 9.70 3 5 -14 16.60 5.40 -3 -5 14 18.60 5.30 2 5 -14 296.57 19.60 -2 -5 14 292.67 19.40 1 5 -14 44.60 7.80 -1 -5 14 33.90 7.30 0 5 -14 36.30 7.10 0 -5 14 54.19 8.90 0 -5 14 51.99 4.20 -1 5 -14 125.79 8.10 -1 5 -14 126.69 10.90 1 -5 14 122.89 8.90 1 -5 14 112.19 11.50 -2 5 -14 40.50 5.30 2 -5 14 45.40 9.10 2 -5 14 40.20 6.40 -3 5 -14 22.60 5.30 3 -5 14 38.80 7.10 3 -5 14 30.50 7.70 4 -5 14 35.30 7.60 4 -5 14 33.70 8.80 5 -5 14 195.68 16.90 5 -5 14 197.38 17.00 6 -5 14 166.08 16.90 6 -5 14 177.28 16.40 7 -5 14 15.80 7.50 7 -5 14 32.20 9.30 8 -5 14 1.50 6.40 8 -5 14 11.90 6.20 9 -5 14 31.10 10.30 10 -5 14 7.90 9.60 10 -5 14 6.80 7.20 10 -5 14 13.10 6.90 11 -5 14 13.90 9.00 11 -5 14 17.10 7.00 12 -5 14 -10.80 6.60 12 -5 14 21.30 10.00 16 4 -14 21.90 9.00 16 4 -14 -0.70 7.40 -16 -4 14 6.80 5.20 15 4 -14 12.40 8.10 15 4 -14 16.30 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7.90 6.40 3 -18 21 0.40 5.30 4 -18 21 -7.20 5.90 4 -18 21 7.20 7.90 5 -18 21 27.80 10.50 5 -18 21 38.70 12.00 -9 -17 21 58.49 13.50 -8 -17 21 11.30 7.10 -7 -17 21 0.10 5.20 -6 -17 21 1.50 6.70 -5 -17 21 29.00 9.00 -4 -17 21 44.60 11.70 -4 -17 21 45.30 8.20 -3 -17 21 86.69 15.40 -3 -17 21 56.39 9.50 -2 -17 21 -7.50 4.00 -2 -17 21 -6.60 4.20 -1 -17 21 67.39 10.40 -1 -17 21 74.09 14.00 0 -17 21 8.80 8.20 0 -17 21 5.40 4.90 1 -17 21 -10.40 4.40 1 -17 21 -2.10 4.70 2 -17 21 38.60 10.40 2 -17 21 38.30 8.80 3 -17 21 37.60 12.00 3 -17 21 47.70 10.00 4 -17 21 100.19 16.80 4 -17 21 137.99 16.00 5 -17 21 4.30 7.70 5 -17 21 10.40 7.20 6 -17 21 -0.10 7.70 6 -17 21 14.80 9.50 -10 -16 21 0.20 7.00 -9 -16 21 3.10 5.20 -8 -16 21 6.20 5.10 -7 -16 21 -1.60 5.90 -6 -16 21 12.30 7.20 -5 -16 21 17.60 8.60 -4 -16 21 -5.60 5.90 -4 -16 21 7.50 4.10 -3 -16 21 -8.40 3.20 -3 -16 21 -4.00 4.70 -2 -16 21 58.09 12.80 -2 -16 21 64.49 8.60 -1 -16 21 44.30 12.00 -1 -16 21 43.60 8.20 0 -16 21 0.50 5.70 0 -16 21 1.30 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22.80 7.30 9 14 -21 -7.40 5.10 8 14 -21 20.20 8.90 -8 -14 21 21.70 8.30 7 14 -21 20.30 8.40 -7 -14 21 14.10 7.30 6 14 -21 10.40 7.40 -6 -14 21 17.00 7.50 -5 -14 21 46.00 7.60 -5 -14 21 30.40 9.80 -4 -14 21 3.60 4.90 -4 -14 21 15.70 5.80 -4 -14 21 19.00 4.10 -3 -14 21 24.20 7.80 -3 -14 21 24.40 4.40 -3 -14 21 10.30 5.10 -2 -14 21 25.60 4.60 -2 -14 21 13.70 7.10 -2 -14 21 22.90 5.20 -1 -14 21 130.19 16.50 -1 -14 21 139.79 10.70 -1 -14 21 131.39 11.60 0 -14 21 220.88 15.80 0 -14 21 225.28 15.40 0 -14 21 255.67 21.80 1 -14 21 257.47 17.50 1 -14 21 286.27 24.10 2 -14 21 203.08 16.00 2 -14 21 228.58 22.20 3 -14 21 35.20 10.40 3 -14 21 27.70 8.00 4 -14 21 17.40 7.30 4 -14 21 20.70 8.50 5 -14 21 -4.40 6.10 5 -14 21 18.40 8.90 6 -14 21 10.40 7.90 6 -14 21 6.10 9.20 7 -14 21 -13.10 9.00 7 -14 21 -6.40 6.40 -12 -13 21 21.10 8.90 11 13 -21 31.10 10.50 -11 -13 21 49.80 11.40 10 13 -21 54.19 12.20 -10 -13 21 44.30 10.20 9 13 -21 44.50 11.30 -9 -13 21 31.50 10.60 8 13 -21 6.90 6.80 -8 -13 21 14.50 7.50 7 13 -21 -4.90 5.10 -7 -13 21 -0.50 4.80 6 13 -21 2.00 6.30 -6 -13 21 4.80 5.20 5 13 -21 -0.40 4.50 -5 -13 21 -5.70 4.30 4 13 -21 46.80 10.90 -4 -13 21 53.99 7.00 -4 -13 21 51.19 11.20 -3 -13 21 16.70 6.90 -3 -13 21 20.70 4.70 -2 -13 21 15.70 3.50 -2 -13 21 23.90 4.60 -2 -13 21 4.60 5.50 -1 -13 21 76.79 7.20 -1 -13 21 73.69 7.90 -1 -13 21 75.19 13.30 0 -13 21 1.20 5.50 0 -13 21 -2.30 3.70 0 -13 21 2.30 3.80 1 -13 21 7.00 4.70 1 -13 21 8.40 6.70 2 -13 21 91.49 15.40 2 -13 21 99.69 11.30 3 -13 21 37.40 12.40 3 -13 21 40.60 9.40 4 -13 21 79.69 13.10 4 -13 21 93.69 16.00 5 -13 21 28.10 8.70 5 -13 21 27.10 9.30 6 -13 21 72.49 13.80 6 -13 21 76.39 14.70 7 -13 21 -1.20 7.10 7 -13 21 7.50 9.00 12 12 -21 -0.60 5.70 12 12 -21 8.20 5.80 -12 -12 21 17.20 7.10 11 12 -21 -3.60 5.90 -11 -12 21 -5.00 5.30 10 12 -21 6.40 7.10 -10 -12 21 14.20 6.70 9 12 -21 57.99 12.70 -9 -12 21 52.19 10.80 8 12 -21 85.19 14.70 -8 -12 21 56.19 13.00 -7 -12 21 89.89 14.30 -7 -12 21 84.59 10.10 6 12 -21 6.80 6.00 -6 -12 21 16.00 4.60 -6 -12 21 9.70 6.30 5 12 -21 11.60 6.70 -5 -12 21 11.50 2.90 -5 -12 21 12.50 7.40 -5 -12 21 3.50 3.20 4 12 -21 54.99 12.10 -4 -12 21 48.80 10.50 3 12 -21 58.19 11.60 -3 -12 21 27.20 9.20 -2 -12 21 5.40 5.60 -1 -12 21 41.80 10.50 0 -12 21 158.78 17.50 0 -12 21 171.28 10.80 0 -12 21 172.28 11.10 1 -12 21 127.79 11.00 1 -12 21 148.69 16.60 2 -12 21 38.80 10.70 2 -12 21 33.70 7.00 3 -12 21 123.79 12.90 3 -12 21 135.99 17.30 4 -12 21 -0.80 6.70 4 -12 21 8.50 6.30 5 -12 21 -3.20 6.10 5 -12 21 11.30 8.30 6 -12 21 11.00 6.90 6 -12 21 0.10 7.20 7 -12 21 30.60 9.70 8 -12 21 12.70 10.10 8 -12 21 -5.80 7.70 12 11 -21 20.90 10.60 12 11 -21 28.30 8.30 -12 -11 21 22.10 9.00 11 11 -21 41.50 10.80 -11 -11 21 42.80 10.40 10 11 -21 36.20 10.40 -10 -11 21 16.30 7.00 9 11 -21 37.10 10.80 -9 -11 21 64.89 12.20 8 11 -21 97.29 15.90 -8 -11 21 106.29 13.40 -8 -11 21 110.99 10.70 7 11 -21 37.90 10.10 -7 -11 21 64.99 7.50 -7 -11 21 51.09 11.80 6 11 -21 2.80 4.70 -6 -11 21 -2.20 4.20 5 11 -21 2.20 6.10 -5 -11 21 16.20 7.30 4 11 -21 18.40 7.20 -4 -11 21 10.10 7.40 3 11 -21 37.90 10.00 -3 -11 21 34.50 9.60 2 11 -21 44.50 11.00 -2 -11 21 20.30 8.00 -1 -11 21 27.40 8.40 0 -11 21 113.49 16.90 1 -11 21 75.39 14.70 1 -11 21 59.79 6.70 2 -11 21 63.79 13.00 2 -11 21 52.59 8.10 3 -11 21 39.60 8.00 3 -11 21 33.20 9.50 4 -11 21 156.98 18.20 4 -11 21 154.88 15.10 5 -11 21 6.20 7.40 5 -11 21 -4.00 5.60 6 -11 21 34.10 11.40 6 -11 21 19.10 8.30 7 -11 21 9.00 8.90 7 -11 21 20.70 10.10 8 -11 21 27.90 12.10 8 -11 21 17.90 9.40 13 10 -21 23.70 7.70 13 10 -21 20.40 8.60 -13 -10 21 14.90 6.80 12 10 -21 33.60 9.10 12 10 -21 21.80 10.30 -12 -10 21 15.70 7.50 11 10 -21 -10.50 5.60 -11 -10 21 7.10 5.70 10 10 -21 -7.30 3.80 10 10 -21 5.60 6.70 -10 -10 21 0.50 6.10 9 10 -21 56.39 12.50 -9 -10 21 50.69 10.70 8 10 -21 14.90 6.80 -8 -10 21 16.30 8.00 -8 -10 21 32.60 6.30 7 10 -21 36.30 10.40 -7 -10 21 32.70 5.10 -7 -10 21 35.40 9.30 6 10 -21 24.20 8.70 -6 -10 21 24.40 8.00 5 10 -21 13.30 7.20 -5 -10 21 17.80 7.20 4 10 -21 -7.00 4.60 -4 -10 21 6.20 6.10 3 10 -21 8.50 5.80 -3 -10 21 0.10 4.90 2 10 -21 23.10 8.10 -2 -10 21 46.30 10.60 1 10 -21 4.70 5.10 -1 -10 21 8.90 7.00 0 -10 21 65.49 12.90 1 -10 21 41.50 5.60 1 -10 21 28.60 9.30 2 -10 21 73.89 14.40 2 -10 21 60.09 8.20 3 -10 21 23.80 6.60 3 -10 21 16.60 8.50 4 -10 21 22.30 7.70 4 -10 21 8.00 7.80 5 -10 21 15.30 8.10 5 -10 21 24.70 8.10 6 -10 21 8.40 7.70 6 -10 21 3.50 6.70 7 -10 21 -5.00 7.30 7 -10 21 15.60 8.20 8 -10 21 8.90 8.00 8 -10 21 18.40 10.00 13 9 -21 2.40 8.00 13 9 -21 8.80 6.10 -13 -9 21 -4.60 5.60 12 9 -21 8.40 6.00 12 9 -21 6.50 6.30 -12 -9 21 10.60 6.10 11 9 -21 24.70 9.10 11 9 -21 -0.80 5.40 -11 -9 21 0.20 5.70 10 9 -21 25.30 9.60 10 9 -21 19.80 6.00 -10 -9 21 12.40 7.30 9 9 -21 16.30 7.30 -9 -9 21 20.30 7.00 -9 -9 21 22.50 6.00 8 9 -21 6.00 7.10 -8 -9 21 -6.00 4.50 7 9 -21 -1.70 4.10 -7 -9 21 7.40 5.40 6 9 -21 7.20 6.00 -6 -9 21 6.70 6.30 5 9 -21 86.89 14.60 -5 -9 21 97.89 14.90 4 9 -21 38.20 10.20 -4 -9 21 23.70 8.10 3 9 -21 109.29 15.80 -3 -9 21 87.09 14.10 2 9 -21 131.49 15.00 -2 -9 21 96.79 13.00 1 9 -21 41.30 9.60 -1 -9 21 23.20 7.70 0 -9 21 -2.70 3.90 1 -9 21 7.00 6.20 2 -9 21 14.30 3.80 2 -9 21 0.70 5.70 -3 9 -21 17.10 4.40 3 -9 21 19.50 7.90 3 -9 21 13.00 5.50 4 -9 21 83.69 15.30 4 -9 21 110.69 12.80 5 -9 21 35.70 11.20 5 -9 21 26.60 8.30 6 -9 21 8.80 6.90 6 -9 21 13.60 7.90 7 -9 21 2.00 7.00 7 -9 21 7.20 8.70 8 -9 21 -1.40 8.10 8 -9 21 22.60 9.80 13 8 -21 18.60 8.00 13 8 -21 13.60 8.00 -13 -8 21 2.90 6.40 12 8 -21 10.60 6.70 12 8 -21 -12.90 6.00 -12 -8 21 -1.60 5.30 11 8 -21 -10.30 5.80 11 8 -21 -0.10 5.40 -11 -8 21 9.70 6.40 10 8 -21 13.60 5.60 10 8 -21 12.10 6.90 -10 -8 21 14.90 6.80 9 8 -21 35.80 10.10 9 8 -21 26.50 6.20 -9 -8 21 28.90 8.40 8 8 -21 67.29 12.70 -8 -8 21 78.49 12.80 -8 -8 21 79.69 7.20 7 8 -21 9.30 6.40 -7 -8 21 -5.00 4.40 6 8 -21 21.70 8.00 -6 -8 21 12.10 6.70 5 8 -21 42.20 11.10 -5 -8 21 62.69 11.70 4 8 -21 25.40 8.00 -4 -8 21 23.30 7.80 3 8 -21 31.00 9.00 -3 -8 21 19.80 8.40 -2 -8 21 -9.00 4.60 1 8 -21 15.50 6.60 -1 -8 21 12.90 7.00 0 8 -21 9.20 6.30 0 -8 21 17.30 7.50 1 -8 21 14.80 7.30 2 -8 21 9.20 4.10 2 -8 21 -9.10 4.40 -3 8 -21 25.10 5.10 3 -8 21 14.10 5.60 3 -8 21 18.80 8.30 4 -8 21 7.80 5.60 4 -8 21 13.70 7.30 5 -8 21 7.60 7.10 5 -8 21 -4.40 5.40 6 -8 21 31.00 9.90 6 -8 21 40.40 11.90 7 -8 21 -1.50 5.80 7 -8 21 -13.70 7.00 8 -8 21 29.20 11.30 -14 -7 21 5.80 6.90 13 7 -21 19.00 9.70 13 7 -21 17.00 8.30 -13 -7 21 17.80 7.20 12 7 -21 9.80 7.80 12 7 -21 18.10 7.60 11 7 -21 37.90 10.90 11 7 -21 63.29 10.80 -11 -7 21 74.79 11.60 10 7 -21 44.60 11.20 10 7 -21 49.30 8.50 -10 -7 21 53.09 10.50 9 7 -21 17.30 4.90 9 7 -21 14.50 7.40 -9 -7 21 12.70 5.10 -9 -7 21 1.10 5.30 8 7 -21 42.10 10.80 -8 -7 21 56.59 5.60 -8 -7 21 32.10 8.70 7 7 -21 87.79 14.70 -7 -7 21 76.59 13.10 6 7 -21 18.30 8.40 -6 -7 21 3.60 5.60 5 7 -21 11.40 7.20 -5 -7 21 6.40 5.50 4 7 -21 4.70 5.10 -4 -7 21 15.70 7.00 3 7 -21 132.69 15.10 -3 -7 21 123.69 14.20 2 7 -21 35.20 9.00 -2 -7 21 37.10 9.50 1 7 -21 10.60 6.00 -1 -7 21 9.40 6.00 0 7 -21 1.60 4.60 0 -7 21 -5.30 4.50 -1 7 -21 4.20 5.10 1 -7 21 0.40 4.80 -2 7 -21 45.20 5.60 2 -7 21 45.80 11.90 2 -7 21 61.79 7.10 -3 7 -21 69.59 7.90 3 -7 21 45.40 11.40 3 -7 21 63.49 9.40 4 -7 21 40.60 10.70 4 -7 21 46.00 9.50 5 -7 21 6.60 7.20 5 -7 21 11.20 6.60 6 -7 21 2.40 6.00 6 -7 21 5.10 6.90 7 -7 21 -5.60 9.30 7 -7 21 25.00 10.80 8 -7 21 -6.80 6.50 8 -7 21 23.00 9.80 14 6 -21 11.20 7.90 14 6 -21 8.60 8.00 -14 -6 21 -4.30 6.00 13 6 -21 25.60 8.40 13 6 -21 8.80 7.60 -13 -6 21 23.60 7.50 12 6 -21 1.60 6.50 12 6 -21 -4.30 5.40 -12 -6 21 3.40 6.10 11 6 -21 29.80 10.60 11 6 -21 20.60 6.80 -11 -6 21 32.10 8.50 10 6 -21 2.40 5.80 10 6 -21 8.20 4.70 -10 -6 21 7.70 5.60 9 6 -21 12.80 4.90 9 6 -21 0.60 4.90 -9 -6 21 10.70 4.40 -9 -6 21 20.40 7.20 8 6 -21 0.80 2.40 8 6 -21 9.60 6.50 -8 -6 21 -2.00 4.40 7 6 -21 5.60 6.40 -7 -6 21 -4.60 4.40 6 6 -21 113.99 16.80 -6 -6 21 104.69 13.50 5 6 -21 14.50 6.90 -5 -6 21 8.30 6.40 4 6 -21 20.20 8.00 -4 -6 21 11.60 6.80 3 6 -21 8.80 5.50 -3 -6 21 -2.90 5.20 2 6 -21 0.50 4.40 -2 -6 21 -3.30 4.60 1 6 -21 16.30 6.20 -1 -6 21 13.80 7.20 0 6 -21 2.50 4.20 0 -6 21 1.00 5.40 -1 6 -21 18.90 2.80 -1 6 -21 9.90 6.10 1 -6 21 15.50 8.60 -2 6 -21 36.20 5.40 2 -6 21 33.60 6.10 2 -6 21 39.50 10.10 3 -6 21 38.50 11.20 3 -6 21 29.70 7.10 4 -6 21 6.30 6.00 4 -6 21 3.90 7.10 5 -6 21 1.20 6.20 5 -6 21 1.00 6.00 6 -6 21 29.80 8.90 7 -6 21 -4.10 7.60 7 -6 21 16.20 8.80 8 -6 21 2.60 6.90 8 -6 21 7.50 8.90 14 5 -21 12.60 8.20 14 5 -21 -10.50 6.50 -14 -5 21 -11.70 5.90 13 5 -21 -9.50 7.00 13 5 -21 6.20 6.90 -13 -5 21 0.90 5.40 12 5 -21 -5.00 6.20 12 5 -21 -9.00 4.60 -12 -5 21 -10.40 4.70 11 5 -21 16.70 9.20 11 5 -21 29.70 7.80 -11 -5 21 27.30 8.00 10 5 -21 6.00 6.40 10 5 -21 0.50 4.00 -10 -5 21 10.10 5.80 9 5 -21 1.80 3.20 9 5 -21 2.40 5.40 -9 -5 21 -0.80 5.00 8 5 -21 8.50 3.30 8 5 -21 18.70 7.80 -8 -5 21 16.90 6.50 7 5 -21 17.90 7.00 -7 -5 21 -6.00 4.50 6 5 -21 1.00 6.00 -6 -5 21 15.50 6.70 5 5 -21 -1.10 5.20 -5 -5 21 11.60 6.40 4 5 -21 21.50 7.80 -4 -5 21 27.10 8.30 3 5 -21 11.60 5.70 -3 -5 21 5.80 5.20 2 5 -21 -0.80 4.70 -2 -5 21 5.00 6.10 1 5 -21 39.60 9.30 -1 -5 21 41.30 10.00 0 5 -21 4.50 4.40 0 -5 21 -2.40 4.30 -1 5 -21 5.80 5.10 -1 5 -21 10.90 2.80 1 -5 21 2.00 5.20 -2 5 -21 7.20 3.40 2 -5 21 4.80 4.90 3 -5 21 5.00 4.60 3 -5 21 0.70 5.80 4 -5 21 6.90 5.80 4 -5 21 8.40 7.80 5 -5 21 11.80 8.00 5 -5 21 27.60 8.60 6 -5 21 -1.20 6.90 6 -5 21 0.90 6.70 7 -5 21 11.90 8.70 7 -5 21 0.00 6.50 8 -5 21 2.00 9.80 8 -5 21 -12.10 5.80 14 4 -21 9.80 7.10 14 4 -21 0.80 6.20 -14 -4 21 6.50 5.40 13 4 -21 -5.80 7.00 13 4 -21 10.30 7.40 12 4 -21 31.40 10.40 12 4 -21 15.00 6.50 -12 -4 21 33.00 7.40 11 4 -21 11.60 8.10 11 4 -21 15.20 6.40 -11 -4 21 24.90 6.70 10 4 -21 5.70 4.30 10 4 -21 4.10 6.30 -10 -4 21 -0.30 5.40 9 4 -21 14.00 7.70 9 4 -21 0.40 3.40 -9 -4 21 -10.00 3.60 8 4 -21 30.30 9.50 8 4 -21 34.90 5.70 -8 -4 21 47.90 10.10 7 4 -21 84.49 14.90 -7 -4 21 87.39 12.90 6 4 -21 185.98 18.60 -6 -4 21 163.38 15.80 5 4 -21 3.10 5.10 -5 -4 21 15.80 7.20 4 4 -21 153.38 16.20 -4 -4 21 120.99 14.40 3 4 -21 -0.20 4.60 -3 -4 21 0.50 5.10 2 4 -21 -0.60 4.50 1 4 -21 23.50 7.10 -1 -4 21 24.10 8.80 0 4 -21 54.09 10.10 0 -4 21 40.60 9.60 -1 4 -21 16.80 6.20 -1 4 -21 8.10 3.50 1 -4 21 13.90 6.60 -2 4 -21 18.90 5.50 -2 4 -21 19.70 6.30 2 -4 21 28.70 9.20 3 -4 21 6.20 6.50 3 -4 21 7.70 5.10 4 -4 21 5.00 6.00 4 -4 21 1.20 6.10 5 -4 21 14.80 8.10 5 -4 21 12.40 7.80 6 -4 21 -3.20 7.30 6 -4 21 26.10 9.00 7 -4 21 14.30 9.40 7 -4 21 7.90 8.20 8 -4 21 19.30 10.90 8 -4 21 40.50 12.00 14 3 -21 3.90 6.40 14 3 -21 12.50 8.30 -14 -3 21 5.10 4.90 13 3 -21 2.30 6.80 13 3 -21 -3.20 5.50 -13 -3 21 -5.80 4.50 12 3 -21 11.90 6.20 12 3 -21 6.70 7.50 -12 -3 21 7.70 5.00 11 3 -21 -5.00 6.10 11 3 -21 14.90 6.10 -11 -3 21 -11.70 4.30 10 3 -21 38.80 10.40 10 3 -21 36.10 7.80 -10 -3 21 43.30 8.80 9 3 -21 11.90 4.60 9 3 -21 4.50 6.50 -9 -3 21 19.40 6.80 8 3 -21 47.20 11.00 8 3 -21 32.50 5.90 -8 -3 21 43.80 9.20 7 3 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25.30 8.10 -6 -2 21 17.50 6.90 5 2 -21 70.89 13.30 -5 -2 21 75.99 12.50 4 2 -21 108.09 13.80 -4 -2 21 107.69 13.10 3 2 -21 2.30 5.00 -3 -2 21 9.80 6.70 2 2 -21 11.50 5.40 -2 -2 21 6.90 6.00 1 2 -21 171.78 10.70 1 2 -21 174.58 15.90 -1 -2 21 194.78 18.80 0 2 -21 32.10 8.10 0 -2 21 32.70 9.70 -1 2 -21 86.39 12.10 -1 2 -21 83.29 9.20 1 -2 21 81.69 14.30 -2 2 -21 17.10 6.00 2 -2 21 26.20 9.50 3 -2 21 74.99 13.80 4 -2 21 17.60 8.30 4 -2 21 31.40 10.60 5 -2 21 -1.00 6.60 5 -2 21 -2.20 6.10 6 -2 21 4.40 7.80 6 -2 21 13.00 7.80 7 -2 21 10.40 10.30 7 -2 21 17.20 10.10 14 1 -21 -0.20 7.90 -14 -1 21 14.60 5.00 13 1 -21 3.30 7.80 13 1 -21 -5.70 6.00 12 1 -21 1.80 5.90 12 1 -21 3.10 5.40 -12 -1 21 3.20 4.50 11 1 -21 16.20 7.30 11 1 -21 0.80 5.00 -11 -1 21 7.30 4.60 10 1 -21 53.89 12.60 -10 -1 21 59.99 9.60 9 1 -21 86.39 15.20 9 1 -21 118.59 11.70 -9 -1 21 87.09 11.50 8 1 -21 153.68 17.50 8 1 -21 138.99 12.10 -8 -1 21 146.09 14.10 7 1 -21 98.19 15.10 7 1 -21 81.39 8.60 -7 -1 21 97.19 11.90 6 1 -21 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6.60 -11 -13 22 9.10 7.50 10 13 -22 21.50 9.50 -10 -13 22 19.30 7.80 9 13 -22 0.90 6.00 -9 -13 22 13.80 7.20 8 13 -22 4.80 6.20 -8 -13 22 10.90 5.80 7 13 -22 22.30 9.10 -7 -13 22 9.80 6.00 -7 -13 22 13.30 6.90 6 13 -22 12.30 6.80 -6 -13 22 6.00 6.00 -6 -13 22 16.70 4.90 5 13 -22 4.30 5.70 -5 -13 22 0.90 5.50 -5 -13 22 -1.30 2.50 -5 -13 22 -6.30 3.30 4 13 -22 17.30 7.30 -3 -13 22 8.20 6.60 -2 -13 22 116.69 15.00 -1 -13 22 11.50 6.60 0 -13 22 45.90 11.50 0 -13 22 25.80 5.30 0 -13 22 19.20 5.20 1 -13 22 50.69 7.40 1 -13 22 44.70 11.50 2 -13 22 151.18 18.20 2 -13 22 109.89 11.80 3 -13 22 43.70 8.70 3 -13 22 43.00 11.90 4 -13 22 5.50 7.10 4 -13 22 -2.50 5.40 5 -13 22 0.10 6.10 5 -13 22 4.30 6.00 6 -13 22 4.80 7.50 6 -13 22 -10.40 7.30 7 -13 22 61.19 14.50 7 -13 22 66.19 13.40 12 12 -22 -0.30 7.60 -12 -12 22 0.60 5.50 11 12 -22 8.70 7.10 -11 -12 22 9.40 7.00 10 12 -22 12.40 7.20 -10 -12 22 -1.80 6.20 9 12 -22 45.70 11.00 -9 -12 22 43.40 10.60 8 12 -22 2.80 6.50 -8 -12 22 14.10 6.80 -8 -12 22 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2 -10 22 18.90 4.80 2 -10 22 26.30 9.40 3 -10 22 10.10 7.90 3 -10 22 24.00 5.90 4 -10 22 19.30 8.80 4 -10 22 20.90 6.10 5 -10 22 -4.60 5.70 5 -10 22 2.60 6.30 6 -10 22 5.90 8.00 6 -10 22 26.80 10.20 7 -10 22 17.20 8.30 7 -10 22 5.10 8.20 13 9 -22 0.30 6.70 -13 -9 22 3.30 6.40 12 9 -22 -3.30 4.80 12 9 -22 -10.00 5.60 -12 -9 22 -6.40 5.60 11 9 -22 63.89 14.00 11 9 -22 43.40 8.70 -11 -9 22 51.19 11.10 10 9 -22 18.90 4.90 10 9 -22 16.80 7.90 -10 -9 22 33.10 9.00 9 9 -22 7.30 6.70 -9 -9 22 12.00 5.10 -9 -9 22 7.30 6.60 8 9 -22 1.40 5.70 -8 -9 22 5.60 6.00 -8 -9 22 4.60 3.30 7 9 -22 9.00 7.40 -7 -9 22 -2.10 3.80 6 9 -22 8.90 6.30 -6 -9 22 11.00 6.30 5 9 -22 53.29 11.20 -5 -9 22 59.69 12.20 4 9 -22 27.30 9.20 -4 -9 22 19.50 8.10 3 9 -22 17.80 7.30 -3 -9 22 10.80 6.30 2 9 -22 0.10 4.70 -2 -9 22 -10.20 4.30 1 9 -22 -8.90 4.20 -1 -9 22 7.10 6.00 0 -9 22 3.20 4.50 1 -9 22 8.40 6.30 2 -9 22 25.20 9.00 2 -9 22 11.80 4.10 3 -9 22 16.00 9.30 3 -9 22 21.30 5.30 4 -9 22 124.19 19.00 4 -9 22 136.79 13.40 5 -9 22 -7.80 5.60 5 -9 22 6.40 7.60 6 -9 22 24.20 9.90 6 -9 22 22.50 9.20 7 -9 22 -10.10 6.70 7 -9 22 13.00 10.00 13 8 -22 -3.30 6.50 13 8 -22 -10.00 5.10 -13 -8 22 3.00 6.00 12 8 -22 -8.50 6.00 12 8 -22 -7.60 4.70 -12 -8 22 -0.50 5.80 11 8 -22 -0.10 4.40 11 8 -22 -7.50 6.00 -11 -8 22 -2.00 5.00 10 8 -22 4.20 5.90 10 8 -22 6.60 4.30 -10 -8 22 6.50 6.00 9 8 -22 9.50 8.10 -9 -8 22 6.50 4.40 -9 -8 22 12.30 6.90 8 8 -22 18.10 8.00 -8 -8 22 13.40 5.90 7 8 -22 1.90 5.70 -7 -8 22 0.10 5.20 6 8 -22 8.40 6.50 -6 -8 22 22.30 7.50 5 8 -22 1.90 5.10 -5 -8 22 0.90 4.60 4 8 -22 19.50 7.70 -4 -8 22 2.60 5.90 3 8 -22 5.60 5.30 -3 -8 22 8.90 7.00 2 8 -22 2.40 4.90 -2 -8 22 9.70 6.70 1 8 -22 -1.10 5.00 -1 -8 22 -5.00 3.90 0 8 -22 0.70 5.50 0 -8 22 13.00 7.10 1 -8 22 10.40 6.10 2 -8 22 8.10 4.00 2 -8 22 13.10 8.30 -3 8 -22 13.80 4.90 3 -8 22 18.60 9.20 3 -8 22 21.60 5.50 4 -8 22 13.70 6.20 4 -8 22 27.50 10.00 5 -8 22 2.50 6.90 5 -8 22 -7.20 5.10 6 -8 22 108.09 15.50 6 -8 22 81.99 15.30 7 -8 22 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22 42.70 9.20 10 5 -22 65.49 14.40 10 5 -22 88.29 9.50 -10 -5 22 100.39 12.60 9 5 -22 74.69 14.10 9 5 -22 55.19 7.10 -9 -5 22 78.39 12.80 8 5 -22 30.50 9.20 -8 -5 22 25.40 7.50 7 5 -22 16.10 8.20 -7 -5 22 7.10 5.50 6 5 -22 47.60 11.70 -6 -5 22 44.20 10.00 5 5 -22 101.99 16.00 -5 -5 22 96.59 15.00 4 5 -22 18.40 6.90 -4 -5 22 10.30 6.70 3 5 -22 0.80 5.00 -3 -5 22 7.40 5.60 2 5 -22 13.30 6.50 -2 -5 22 2.10 5.60 1 5 -22 38.30 9.30 -1 -5 22 39.10 10.50 0 5 -22 -4.30 3.60 0 -5 22 0.50 5.90 -1 5 -22 18.00 5.80 -1 5 -22 1.40 2.70 1 -5 22 -10.00 4.10 -2 5 -22 7.60 4.10 2 -5 22 8.00 6.30 3 -5 22 18.60 8.70 4 -5 22 33.40 10.20 4 -5 22 33.40 8.70 5 -5 22 34.30 8.70 5 -5 22 28.30 10.70 6 -5 22 17.00 10.20 6 -5 22 11.60 8.00 7 -5 22 9.50 7.70 13 4 -22 -13.70 6.60 13 4 -22 20.50 6.60 -13 -4 22 2.60 5.80 12 4 -22 17.70 7.80 12 4 -22 1.20 4.90 -12 -4 22 4.50 5.70 11 4 -22 2.90 5.60 11 4 -22 16.70 9.20 -11 -4 22 28.10 7.60 10 4 -22 -1.50 4.20 10 4 -22 7.70 6.40 -10 -4 22 -1.60 4.90 9 4 -22 6.90 3.90 9 4 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7.20 -8 -3 22 79.39 12.50 7 3 -22 72.19 14.30 -7 -3 22 89.49 13.40 6 3 -22 -3.40 5.40 -6 -3 22 5.90 5.10 5 3 -22 -1.60 5.40 -5 -3 22 4.80 6.20 4 3 -22 3.00 6.40 -4 -3 22 1.80 5.10 3 3 -22 5.30 5.10 -3 -3 22 -2.40 5.70 2 3 -22 12.50 6.80 -2 -3 22 3.10 6.10 1 3 -22 12.10 6.70 -1 -3 22 24.90 9.60 0 3 -22 26.40 7.00 0 3 -22 11.10 3.40 0 -3 22 19.70 9.00 -1 3 -22 3.40 3.70 -1 3 -22 4.00 3.90 1 -3 22 -6.40 5.50 -2 3 -22 44.60 8.60 2 -3 22 37.80 10.60 3 -3 22 38.20 11.40 4 -3 22 25.20 7.70 4 -3 22 32.90 10.60 5 -3 22 12.50 8.50 5 -3 22 21.10 7.80 6 -3 22 2.90 7.20 6 -3 22 13.40 9.30 13 2 -22 -5.00 7.10 13 2 -22 4.30 5.70 -13 -2 22 -4.10 4.70 12 2 -22 -4.20 5.40 12 2 -22 3.70 7.20 -12 -2 22 13.90 5.50 11 2 -22 12.40 8.10 11 2 -22 2.70 5.40 -11 -2 22 12.80 5.60 10 2 -22 10.50 7.50 -10 -2 22 8.40 5.70 9 2 -22 22.00 8.60 -9 -2 22 14.90 6.20 8 2 -22 11.30 7.60 8 2 -22 1.30 3.00 -8 -2 22 4.50 5.30 7 2 -22 0.40 2.70 7 2 -22 9.50 5.70 -7 -2 22 4.20 4.90 6 2 -22 12.00 7.40 -6 -2 22 0.90 4.80 5 2 -22 13.50 6.60 -5 -2 22 0.30 4.80 4 2 -22 0.10 5.00 -4 -2 22 14.10 6.50 3 2 -22 43.50 10.10 -3 -2 22 58.09 12.30 2 2 -22 52.79 10.30 -2 -2 22 56.79 11.60 1 2 -22 20.30 5.60 -1 -2 22 12.60 7.30 0 2 -22 79.09 8.00 0 2 -22 78.19 11.90 0 -2 22 70.29 12.80 -1 2 -22 136.99 13.00 -1 2 -22 163.88 14.70 1 -2 22 180.48 18.10 -2 2 -22 73.89 10.80 2 -2 22 71.49 14.00 3 -2 22 51.89 12.50 4 -2 22 5.30 8.50 5 -2 22 6.10 7.20 5 -2 22 1.30 6.30 6 -2 22 14.60 8.40 6 -2 22 -2.00 9.20 13 1 -22 -2.40 7.60 13 1 -22 -12.60 5.50 -13 -1 22 -0.40 5.20 12 1 -22 14.20 7.30 12 1 -22 9.00 6.90 -12 -1 22 10.30 5.60 11 1 -22 14.60 7.90 11 1 -22 18.50 7.20 -11 -1 22 2.10 5.30 10 1 -22 64.59 10.50 10 1 -22 87.39 16.00 -10 -1 22 81.19 11.70 9 1 -22 67.49 13.80 9 1 -22 72.09 9.30 -9 -1 22 75.99 11.80 8 1 -22 17.80 9.20 8 1 -22 19.50 4.90 -8 -1 22 20.60 7.20 7 1 -22 22.40 8.70 7 1 -22 2.90 3.50 -7 -1 22 4.20 5.90 6 1 -22 39.60 5.30 6 1 -22 38.30 10.40 6 1 -22 33.90 5.30 -6 -1 22 47.60 9.80 5 1 -22 85.79 7.20 5 1 -22 109.59 7.30 5 1 -22 127.49 15.30 -5 -1 22 115.29 13.60 4 1 -22 24.20 8.30 4 1 -22 27.60 3.90 -4 -1 22 18.80 8.40 3 1 -22 19.50 3.40 3 1 -22 20.80 7.40 -3 -1 22 21.50 7.60 2 1 -22 -2.60 3.20 2 1 -22 7.00 2.50 2 1 -22 6.50 5.20 -2 -1 22 -2.60 5.60 1 1 -22 2.60 4.90 1 1 -22 6.70 3.80 -1 -1 22 3.50 5.00 0 1 -22 8.10 5.70 0 1 -22 22.30 7.50 0 -1 22 23.90 8.70 -1 1 -22 48.20 9.30 1 -1 22 29.40 10.20 -2 1 -22 22.60 7.10 2 -1 22 32.70 10.60 -3 1 -22 19.00 6.70 3 -1 22 28.20 10.10 4 -1 22 -1.30 6.70 5 -1 22 6.80 9.30 6 -1 22 0.10 8.40 6 -1 22 12.00 8.40 13 0 -22 -16.90 5.70 13 0 -22 -13.60 5.70 -13 0 22 10.30 5.30 12 0 -22 -3.10 6.50 12 0 -22 7.00 6.90 -12 0 22 4.50 5.30 11 0 -22 5.50 7.30 11 0 -22 10.10 5.30 -11 0 22 12.60 5.50 10 0 -22 5.70 4.50 10 0 -22 -3.10 6.20 -10 0 22 10.30 5.50 9 0 -22 -2.00 3.90 9 0 -22 19.80 9.10 -9 0 22 -1.30 4.90 8 0 -22 89.59 10.00 8 0 -22 85.99 14.70 -8 0 22 102.69 12.70 7 0 -22 18.00 8.30 -7 0 22 21.20 7.60 6 0 -22 59.69 7.00 6 0 -22 56.29 7.30 6 0 -22 72.69 13.70 -6 0 22 56.79 10.60 5 0 -22 52.09 7.20 5 0 -22 48.10 6.00 5 0 -22 58.79 11.50 -5 0 22 48.20 11.00 4 0 -22 5.70 2.90 4 0 -22 -4.70 3.30 -4 0 22 2.10 5.30 3 0 -22 3.80 5.60 3 0 -22 6.00 3.80 3 0 -22 8.00 3.10 -3 0 22 -0.10 6.20 2 0 -22 7.20 5.90 2 0 -22 14.10 4.30 2 0 -22 0.80 4.80 -2 0 22 4.20 6.00 1 0 -22 83.79 12.90 1 0 -22 44.60 8.50 -1 0 22 64.39 12.90 0 0 -22 81.29 12.40 0 0 22 97.59 16.10 -1 0 -22 67.19 10.80 1 0 22 68.09 13.70 -2 0 -22 30.90 7.40 2 0 22 44.50 11.20 -3 0 -22 32.70 7.50 3 0 22 22.20 9.00 4 0 22 -12.40 5.20 5 0 22 -0.20 7.80 12 -1 -22 26.50 10.50 12 -1 -22 5.70 7.10 -12 1 22 24.30 6.20 11 -1 -22 11.70 8.30 11 -1 -22 11.10 6.10 -11 1 22 24.50 6.30 10 -1 -22 20.20 9.70 10 -1 -22 19.10 6.70 -10 1 22 20.00 6.10 9 -1 -22 71.29 14.80 9 -1 -22 81.89 10.70 -9 1 22 82.29 11.70 8 -1 -22 54.79 12.60 8 -1 -22 42.20 8.30 7 -1 -22 5.40 6.90 7 -1 -22 -4.30 3.60 6 -1 -22 15.20 7.30 6 -1 -22 34.30 9.70 6 -1 -22 21.30 5.40 -6 1 22 32.00 8.50 5 -1 -22 14.60 4.70 5 -1 -22 20.50 6.20 -5 1 22 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3.30 -4 -15 23 5.90 6.30 -4 -15 23 12.50 5.70 -3 -15 23 7.70 6.70 -3 -15 23 24.70 5.80 -3 -15 23 11.50 3.90 -2 -15 23 21.90 4.90 -2 -15 23 39.60 6.70 -2 -15 23 28.10 10.30 -1 -15 23 23.00 9.20 -1 -15 23 24.80 5.20 -1 -15 23 32.70 7.10 0 -15 23 111.89 17.50 0 -15 23 80.89 9.50 0 -15 23 98.69 11.10 1 -15 23 77.59 15.20 1 -15 23 77.69 10.30 2 -15 23 21.60 9.60 2 -15 23 15.60 7.20 3 -15 23 0.60 6.50 3 -15 23 0.60 5.90 4 -15 23 41.70 11.70 5 -15 23 49.10 12.70 5 -15 23 39.00 10.80 10 14 -23 -5.40 6.50 -10 -14 23 -5.90 5.80 9 14 -23 9.60 6.50 -9 -14 23 16.30 6.70 8 14 -23 10.20 6.70 -8 -14 23 19.40 8.30 7 14 -23 5.90 5.70 -7 -14 23 6.90 7.30 -7 -14 23 -9.90 6.70 6 14 -23 12.90 7.30 -6 -14 23 26.70 9.70 -6 -14 23 16.30 5.80 -6 -14 23 20.40 4.00 -5 -14 23 6.10 6.10 -4 -14 23 -2.50 5.60 -3 -14 23 1.40 5.60 -2 -14 23 -10.80 5.30 0 -14 23 9.50 4.40 0 -14 23 -1.60 3.40 0 -14 23 3.60 6.00 1 -14 23 72.99 14.70 1 -14 23 65.49 8.70 2 -14 23 30.30 7.50 2 -14 23 42.20 11.80 3 -14 23 23.30 10.10 3 -14 23 19.50 7.10 4 -14 23 22.60 8.30 4 -14 23 23.40 9.60 5 -14 23 14.30 8.60 5 -14 23 6.10 8.30 6 -14 23 -5.50 8.40 6 -14 23 -11.50 6.80 11 13 -23 4.90 7.40 -11 -13 23 11.10 7.10 10 13 -23 17.90 8.70 -10 -13 23 15.60 7.90 9 13 -23 4.80 7.30 -9 -13 23 -12.00 5.70 8 13 -23 24.70 10.20 -8 -13 23 33.40 8.20 7 13 -23 35.30 10.20 -7 -13 23 50.49 11.80 -7 -13 23 46.70 6.90 6 13 -23 8.60 6.70 -6 -13 23 8.20 7.30 5 13 -23 14.30 7.70 -5 -13 23 6.80 7.20 4 13 -23 13.20 7.20 -4 -13 23 19.80 9.00 -3 -13 23 13.20 6.20 -2 -13 23 128.19 18.70 -1 -13 23 16.70 8.00 0 -13 23 44.60 11.90 1 -13 23 66.69 13.80 1 -13 23 77.09 8.00 2 -13 23 13.10 5.40 2 -13 23 12.80 7.80 3 -13 23 29.30 9.70 3 -13 23 20.60 6.60 4 -13 23 -5.30 5.10 4 -13 23 3.10 5.50 5 -13 23 5.90 8.50 5 -13 23 3.50 6.40 6 -13 23 27.10 9.50 6 -13 23 14.50 9.50 11 12 -23 19.00 10.60 -11 -12 23 5.20 7.10 10 12 -23 12.10 8.10 -10 -12 23 -0.90 5.80 9 12 -23 31.00 9.60 -9 -12 23 17.40 7.30 8 12 -23 57.49 12.00 -8 -12 23 44.80 11.00 -8 -12 23 42.20 6.60 7 12 -23 -3.20 5.80 -7 -12 23 -0.90 5.40 -6 -12 23 35.90 10.10 5 12 -23 44.10 11.20 -5 -12 23 51.99 11.40 4 12 -23 56.79 11.70 -4 -12 23 35.10 9.60 3 12 -23 29.60 9.30 -3 -12 23 40.80 11.20 -2 -12 23 0.50 5.70 -1 -12 23 38.50 10.80 0 -12 23 12.80 7.00 1 -12 23 44.60 11.20 2 -12 23 -2.90 4.20 2 -12 23 -2.50 5.10 3 -12 23 52.09 12.80 3 -12 23 50.69 8.60 4 -12 23 10.70 6.50 4 -12 23 2.20 6.10 5 -12 23 29.80 9.40 5 -12 23 29.60 10.20 6 -12 23 14.00 8.60 6 -12 23 11.80 8.60 12 11 -23 9.40 7.90 -12 -11 23 11.10 7.40 11 11 -23 1.90 6.80 -11 -11 23 -10.70 5.70 10 11 -23 11.10 7.00 -10 -11 23 20.40 8.60 9 11 -23 20.00 9.20 -9 -11 23 20.30 6.60 -9 -11 23 37.60 10.30 8 11 -23 109.59 17.50 -8 -11 23 83.99 7.50 -8 -11 23 121.39 15.20 7 11 -23 54.59 12.90 -7 -11 23 46.40 11.30 6 11 -23 4.40 7.90 -6 -11 23 19.80 8.30 5 11 -23 31.90 9.20 -5 -11 23 44.60 10.60 4 11 -23 1.10 6.40 -4 -11 23 -3.30 5.80 3 11 -23 4.00 5.40 -3 -11 23 10.20 6.60 2 11 -23 40.90 10.40 -2 -11 23 27.10 9.20 -1 -11 23 44.00 11.70 0 -11 23 166.78 18.20 1 -11 23 31.60 9.60 2 -11 23 7.50 4.50 2 -11 23 8.50 7.60 3 -11 23 -14.00 5.50 3 -11 23 10.00 5.00 4 -11 23 40.50 8.50 4 -11 23 10.10 8.50 5 -11 23 27.50 7.80 5 -11 23 15.30 7.60 6 -11 23 -9.60 7.00 6 -11 23 8.70 8.00 12 10 -23 6.30 7.60 -12 -10 23 14.40 7.50 11 10 -23 0.50 6.30 -11 -10 23 17.50 7.50 10 10 -23 19.50 8.60 -10 -10 23 12.90 7.00 9 10 -23 21.40 7.70 -9 -10 23 21.20 5.30 -9 -10 23 13.40 6.40 8 10 -23 3.90 6.50 -8 -10 23 19.10 7.70 7 10 -23 9.70 7.10 -7 -10 23 22.80 7.60 6 10 -23 11.00 7.50 -6 -10 23 6.60 6.40 5 10 -23 16.90 8.50 -5 -10 23 28.30 8.60 4 10 -23 50.79 12.30 -4 -10 23 81.09 14.10 3 10 -23 121.99 15.70 -3 -10 23 115.89 14.70 2 10 -23 139.49 16.40 -2 -10 23 146.89 17.10 1 10 -23 72.69 13.40 -1 -10 23 88.39 15.20 0 -10 23 1.40 6.00 1 -10 23 30.30 9.30 2 -10 23 9.20 4.20 2 -10 23 15.30 8.70 3 -10 23 26.10 11.00 3 -10 23 32.40 6.90 4 -10 23 17.40 7.00 4 -10 23 18.00 9.50 5 -10 23 76.19 12.30 5 -10 23 57.89 14.30 6 -10 23 -1.80 7.70 6 -10 23 -3.20 7.60 7 -10 23 9.20 9.50 12 9 -23 -13.20 6.40 12 9 -23 3.40 5.20 -12 -9 23 -1.60 5.10 11 9 -23 15.50 9.50 11 9 -23 20.30 5.80 -11 -9 23 38.00 9.90 10 9 -23 -6.20 6.30 -10 -9 23 -3.00 6.10 9 9 -23 8.20 7.20 -9 -9 23 8.70 4.10 -9 -9 23 7.50 7.10 8 9 -23 6.70 6.80 -8 -9 23 6.50 5.60 7 9 -23 16.50 10.00 -7 -9 23 22.70 8.30 6 9 -23 44.40 10.70 -6 -9 23 43.40 10.60 5 9 -23 40.60 11.00 -5 -9 23 29.80 9.70 4 9 -23 0.10 5.10 -4 -9 23 5.50 6.40 3 9 -23 -2.00 4.70 -3 -9 23 -2.70 4.50 2 9 -23 1.20 5.00 -2 -9 23 25.70 9.30 1 9 -23 137.09 15.70 -1 -9 23 128.69 15.90 0 -9 23 7.40 7.40 1 -9 23 15.40 7.90 2 -9 23 70.99 7.20 2 -9 23 80.09 15.40 3 -9 23 42.60 11.50 3 -9 23 53.89 8.50 4 -9 23 22.20 7.50 4 -9 23 36.40 11.60 5 -9 23 24.50 8.00 5 -9 23 22.10 9.90 6 -9 23 -10.20 6.50 6 -9 23 1.70 7.70 7 -9 23 33.10 11.80 7 -9 23 51.79 13.40 12 8 -23 18.20 9.70 12 8 -23 11.80 6.10 -12 -8 23 16.00 8.00 11 8 -23 0.40 6.10 11 8 -23 1.00 4.40 -11 -8 23 6.60 6.20 10 8 -23 34.70 10.30 10 8 -23 33.90 6.10 -10 -8 23 38.70 9.70 9 8 -23 63.79 13.30 -9 -8 23 37.10 10.50 8 8 -23 11.90 7.40 -8 -8 23 -2.30 5.50 7 8 -23 7.80 6.00 -7 -8 23 -5.60 4.80 6 8 -23 -8.40 4.80 -6 -8 23 7.00 5.60 5 8 -23 142.89 16.80 -5 -8 23 146.29 16.80 4 8 -23 355.06 28.10 -4 -8 23 424.66 29.30 3 8 -23 401.46 28.90 -3 -8 23 409.16 29.60 2 8 -23 302.87 23.70 -2 -8 23 293.17 24.00 1 8 -23 142.29 16.20 -1 -8 23 150.68 16.50 0 8 -23 8.70 5.60 0 -8 23 8.20 7.20 1 -8 23 10.50 7.40 2 -8 23 5.20 3.60 2 -8 23 9.70 7.60 3 -8 23 29.20 7.00 3 -8 23 42.00 11.60 4 -8 23 15.60 7.40 4 -8 23 26.70 11.10 5 -8 23 34.90 9.90 5 -8 23 31.30 11.00 6 -8 23 64.69 14.50 6 -8 23 84.19 14.90 7 -8 23 5.70 8.90 7 -8 23 3.20 8.60 13 7 -23 21.20 10.00 13 7 -23 37.50 8.50 -13 -7 23 31.90 9.40 12 7 -23 59.59 13.90 12 7 -23 48.00 9.50 -12 -7 23 66.79 11.90 11 7 -23 0.30 4.10 -11 -7 23 11.10 6.40 10 7 -23 2.20 7.10 10 7 -23 5.60 3.50 -10 -7 23 8.00 6.10 -10 -7 23 -5.40 4.10 9 7 -23 35.40 11.30 -9 -7 23 19.70 8.30 8 7 -23 -6.00 6.00 -8 -7 23 12.90 6.20 7 7 -23 144.39 16.80 -7 -7 23 137.29 15.40 6 7 -23 134.29 17.30 -6 -7 23 126.49 15.40 5 7 -23 240.48 21.90 -5 -7 23 266.77 22.00 4 7 -23 333.17 26.70 -4 -7 23 390.06 27.30 3 7 -23 38.90 9.80 -3 -7 23 20.90 9.10 2 7 -23 -0.60 4.10 -2 -7 23 8.10 6.00 1 7 -23 4.20 5.40 -1 -7 23 11.50 7.20 0 7 -23 74.89 12.40 1 -7 23 10.10 6.80 -2 7 -23 41.50 5.40 2 -7 23 59.19 13.00 -3 7 -23 50.29 7.50 3 -7 23 56.89 8.30 3 -7 23 45.10 12.60 4 -7 23 52.09 9.70 4 -7 23 30.40 11.40 5 -7 23 42.30 9.90 5 -7 23 55.49 13.70 6 -7 23 9.30 7.80 6 -7 23 6.90 7.90 13 6 -23 -10.10 7.30 13 6 -23 -2.80 5.20 -13 -6 23 -3.50 6.20 12 6 -23 11.60 8.80 12 6 -23 5.30 5.80 -12 -6 23 30.80 8.40 11 6 -23 20.90 6.00 11 6 -23 31.80 9.70 -11 -6 23 19.20 8.00 10 6 -23 18.30 7.80 10 6 -23 30.80 6.00 -10 -6 23 33.30 8.70 9 6 -23 20.50 8.70 -9 -6 23 17.20 7.30 8 6 -23 9.20 7.70 -8 -6 23 -0.60 5.80 7 6 -23 109.59 17.80 -7 -6 23 91.29 14.20 6 6 -23 6.20 7.50 -6 -6 23 10.30 5.90 5 6 -23 3.40 6.60 -5 -6 23 -0.50 6.40 4 6 -23 63.09 12.30 -4 -6 23 60.09 11.70 3 6 -23 191.18 18.40 -3 -6 23 180.58 18.20 2 6 -23 88.69 14.50 -2 -6 23 69.79 13.10 1 6 -23 84.19 13.20 -1 -6 23 70.69 13.60 0 6 -23 50.39 10.40 0 -6 23 50.79 11.60 -1 6 -23 -5.00 4.20 1 -6 23 5.30 6.90 2 -6 23 15.10 7.90 3 -6 23 -8.40 6.70 3 -6 23 6.00 4.80 4 -6 23 19.80 6.70 4 -6 23 -0.80 6.30 5 -6 23 18.60 9.90 5 -6 23 35.40 9.30 6 -6 23 32.80 11.50 6 -6 23 29.60 10.20 13 5 -23 48.70 14.50 13 5 -23 30.50 8.80 12 5 -23 40.10 9.20 12 5 -23 52.79 14.60 -12 -5 23 54.99 10.50 11 5 -23 6.40 4.70 11 5 -23 8.50 6.70 -11 -5 23 27.00 7.70 10 5 -23 45.90 11.80 10 5 -23 17.90 5.00 -10 -5 23 15.90 7.40 9 5 -23 15.40 3.00 9 5 -23 14.10 6.90 8 5 -23 1.30 6.30 -8 -5 23 5.40 5.70 -7 -5 23 115.29 14.00 6 5 -23 6.40 6.30 -6 -5 23 4.30 5.50 5 5 -23 263.57 23.40 -5 -5 23 299.77 23.60 -4 -5 23 79.89 14.00 3 5 -23 2.00 4.80 -3 -5 23 9.60 7.00 2 5 -23 74.59 12.90 -2 -5 23 64.09 12.60 1 5 -23 27.70 9.20 -1 -5 23 25.30 8.90 0 5 -23 43.90 9.50 0 -5 23 28.10 9.30 -1 5 -23 51.89 9.90 -1 5 -23 58.99 5.10 1 -5 23 42.70 10.80 -2 5 -23 37.70 5.90 2 -5 23 45.20 11.40 3 -5 23 15.30 8.80 4 -5 23 9.20 7.80 4 -5 23 10.30 6.10 5 -5 23 -0.20 6.80 5 -5 23 -0.20 6.70 6 -5 23 0.40 7.90 6 -5 23 -11.50 6.40 13 4 -23 5.20 5.90 -13 -4 23 14.90 6.20 12 4 -23 5.30 9.50 12 4 -23 0.40 5.80 -12 -4 23 20.40 7.40 11 4 -23 1.40 7.20 11 4 -23 -0.60 4.60 -11 -4 23 18.00 6.50 10 4 -23 13.00 8.20 10 4 -23 15.50 4.90 -10 -4 23 19.00 6.70 9 4 -23 8.50 6.80 9 4 -23 8.80 3.00 8 4 -23 31.40 10.60 -8 -4 23 41.00 9.40 7 4 -23 63.19 13.00 -7 -4 23 52.49 10.60 6 4 -23 -1.60 4.60 -6 -4 23 11.10 5.90 5 4 -23 73.39 13.90 -5 -4 23 62.59 12.80 4 4 -23 1.50 5.80 -4 -4 23 8.90 6.20 3 4 -23 218.78 20.00 -3 -4 23 231.98 20.40 2 4 -23 266.17 21.90 -2 -4 23 284.37 23.70 1 4 -23 71.69 12.10 -1 -4 23 40.60 11.30 0 4 -23 122.79 13.80 0 -4 23 126.59 16.50 -1 4 -23 12.70 6.00 -1 4 -23 10.40 3.70 1 -4 23 1.10 5.60 -2 4 -23 -0.40 5.10 -2 4 -23 -8.80 4.40 2 -4 23 12.00 6.70 3 -4 23 -4.40 4.60 4 -4 23 -10.10 5.10 4 -4 23 2.40 8.10 5 -4 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2.0483 0.0488 15 -5 5 0.7651 0.0985 15 -5 6 -3.3200 -0.0391 15 -4 0 1.9400 -0.0664 15 -4 1 -2.8800 -0.0497 15 -4 2 -1.1931 -0.0141 15 -4 3 1.9557 0.0784 15 -4 4 -1.1359 -0.0003 15 -4 5 2.1909 -0.0127 15 -4 6 -2.2658 -0.2007 15 -3 0 -0.0926 0.0033 15 -3 1 0.4938 0.0212 15 -3 2 -3.3234 -0.0265 15 -3 3 6.1096 0.0825 15 -3 4 -2.9942 -0.0529 15 -3 5 -3.5438 -0.0885 15 -3 6 5.1560 -0.0092 15 -2 0 0.3810 0.0664 15 -2 1 -1.2393 0.0728 15 -2 2 3.2728 -0.0019 15 -2 3 -2.2711 -0.0840 15 -2 4 0.1269 -0.0357 15 -2 5 2.4274 0.0008 15 -2 6 -3.3266 0.2382 15 -1 0 -0.7472 0.0373 15 -1 1 -0.8138 -0.0443 15 -1 2 0.8856 -0.0132 15 -1 3 -1.6321 -0.0265 15 -1 4 0.2846 0.0370 15 -1 5 2.4883 0.2288 15 0 0 -3.2104 -0.0450 15 0 1 0.1503 -0.0477 15 0 2 2.1665 -0.0104 15 0 3 -1.7614 0.1010 15 0 4 1.2503 0.0852 15 0 5 -1.3710 -0.0670 15 1 0 -5.1662 -0.0820 15 1 1 8.0206 0.0936 15 1 2 -4.7716 0.0604 15 1 3 -1.3014 0.0638 15 1 4 3.0172 -0.1346 15 2 0 -0.7385 0.0734 15 2 1 -0.5333 0.1294 15 2 2 1.5100 0.0317 15 2 3 -3.3427 -0.2667 15 3 0 1.9460 0.2643 15 3 1 -1.2652 -0.0696 15 3 2 -2.1549 -0.2611 15 4 0 -0.9269 -0.1283 15 4 1 1.6829 -0.1413 15 5 0 -1.1864 -0.1628 16 -7 0 6.2610 0.1210 16 -6 0 -8.4237 0.2624 16 -6 1 4.7111 -0.2065 16 -5 0 2.2088 -0.0098 16 -5 1 -1.3647 -0.0616 16 -5 2 0.8848 -0.0017 16 -4 0 -5.3509 -0.2528 16 -4 1 2.9343 0.0134 16 -4 2 0.5176 0.2327 16 -3 0 2.2413 -0.0307 16 -3 1 -1.9712 0.1094 16 -3 2 1.7507 0.0204 16 -2 0 0.8797 0.2745 16 -2 1 2.2489 -0.0029 16 -2 2 -2.6429 -0.2621 16 -1 0 -1.4200 0.0710 16 -1 1 -1.6046 -0.2749 16 0 0 2.9844 -0.2631 16 0 1 -0.0646 0.1185 16 1 0 3.1970 0.1117 0 0 0 0.0 0.0 ; _shelx_fab_checksum 76943 _olex2_submission_special_instructions 'No special instructions were received' _site XU loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.93321(4) 0.76500(3) -0.13281(2) 0.03232(18) Uani 1 1 d . . . . . O1 O 1.0667(2) 0.84901(18) -0.08242(13) 0.0402(7) Uani 1 1 d . . . . . O2 O 1.0811(3) 0.9576(2) -0.09236(16) 0.0593(9) Uani 1 1 d . . . . . O3B O 1.177(2) 0.8760(14) -0.1232(17) 0.077(5) Uani 0.71(9) 1 d D U P A 2 O4 O 0.8047(3) 0.68076(19) -0.17839(14) 0.0531(9) Uani 1 1 d . . . . . H4A H 0.758583 0.695160 -0.159650 0.080 Uiso 1 1 d R U . . . H4B H 0.817272 0.637851 -0.174296 0.080 Uiso 1 1 d R U . . . O5 O 0.6720(3) 0.9496(2) 0.26613(14) 0.0568(9) Uani 1 1 d . . . . . O6 O 0.6555(2) 0.87184(19) 0.02128(13) 0.0475(8) Uani 1 1 d . . . . . O7 O 0.9553(3) 0.9678(2) 0.42122(14) 0.0642(10) Uani 1 1 d . . . . . O8 O 0.9727(2) 0.9759(2) 0.19979(13) 0.0485(8) Uani 1 1 d . . . . . O9 O 0.4828(11) 0.7264(6) 0.2544(5) 0.120(5) Uani 0.446(5) 1 d D U P B 1 O9A O 0.6629(6) 0.7713(4) 0.3472(3) 0.084(2) Uani 0.554(5) 1 d D U P B 2 O10 O 0.6957(7) 0.5000(7) 0.2869(4) 0.087(3) Uani 0.446(5) 1 d D U P B 1 O10A O 0.5223(5) 0.4637(4) 0.1950(3) 0.0632(19) Uani 0.554(5) 1 d D U P B 2 N1 N 0.9320(3) 0.7641(2) -0.04438(15) 0.0350(8) Uani 1 1 d . . . . . N2 N 0.9380(3) 0.7650(2) 0.77916(15) 0.0351(8) Uani 1 1 d . . . . . N3 N 0.9696(3) 0.3220(2) 0.14289(15) 0.0362(8) Uani 1 1 d . . . . . N4 N 0.1489(3) 1.1386(2) 0.11761(15) 0.0361(8) Uani 1 1 d . . . . . N5 N 1.1079(3) 0.8937(2) -0.09726(16) 0.0415(9) Uani 1 1 d D . . . . C1 C 0.8471(3) 0.7614(3) -0.02819(19) 0.0384(11) Uani 1 1 d . . . . . H1 H 0.786925 0.761784 -0.055971 0.046 Uiso 1 1 calc R U . . . C2 C 0.8426(3) 0.7579(3) 0.02658(19) 0.0416(11) Uani 1 1 d . . . . . H2 H 0.780134 0.755757 0.035488 0.050 Uiso 1 1 calc R U . . . C3 C 0.9280(3) 0.7575(3) 0.06878(18) 0.0353(10) Uani 1 1 d . . . . . C4 C 1.0157(3) 0.7596(3) 0.05104(19) 0.0430(11) Uani 1 1 d . . . . . H4 H 1.076914 0.758597 0.077677 0.052 Uiso 1 1 calc R U . . . C5 C 1.0148(3) 0.7630(3) -0.00397(18) 0.0392(11) Uani 1 1 d . . . . . H5 H 1.076148 0.764675 -0.014187 0.047 Uiso 1 1 calc R U . . . C6 C 0.9248(3) 0.7552(3) 0.12882(18) 0.0387(10) Uani 1 1 d . . . . . C7 C 0.8541(3) 0.7859(3) 0.15806(18) 0.0384(10) Uani 1 1 d . . . . . H7 H 0.803442 0.807152 0.138549 0.046 Uiso 1 1 calc R U . . . C8 C 0.8552(3) 0.7866(3) 0.21486(19) 0.0410(11) Uani 1 1 d . . . . . H8 H 0.805028 0.807879 0.233706 0.049 Uiso 1 1 calc R U . . . C9 C 0.9280(4) 0.7569(3) 0.24492(19) 0.0442(11) Uani 1 1 d . . . . . C10 C 0.9993(4) 0.7237(3) 0.2159(2) 0.0537(13) Uani 1 1 d . . . . . H10 H 1.048852 0.701665 0.235496 0.064 Uiso 1 1 calc R U . . . C11 C 0.9982(4) 0.7227(3) 0.1589(2) 0.0483(13) Uani 1 1 d . . . . . H11 H 1.047145 0.699952 0.139487 0.058 Uiso 1 1 calc R U . . . C12 C 0.9323(4) 0.7605(3) 0.30831(19) 0.0439(11) Uani 1 1 d . . . . . C13 C 1.0046(4) 0.8105(3) 0.3611(2) 0.0479(12) Uani 1 1 d . . . . . C14 C 1.0037(4) 0.8063(3) 0.4171(2) 0.0481(12) Uani 1 1 d . . . . . H14 H 1.053745 0.839012 0.453458 0.058 Uiso 1 1 calc R U . . . C15 C 0.9321(4) 0.7560(3) 0.4218(2) 0.0489(12) Uani 1 1 d . . . . . C16 C 0.8569(4) 0.7094(3) 0.3692(2) 0.0497(12) Uani 1 1 d . . . . . C17 C 0.8599(4) 0.7120(3) 0.3137(2) 0.0536(13) Uani 1 1 d . . . . . H17 H 0.809983 0.678917 0.277441 0.064 Uiso 1 1 calc R U . . . C18 C 0.9348(4) 0.7572(3) 0.48415(19) 0.0477(12) Uani 1 1 d . . . . . C19 C 0.9342(4) 0.8259(3) 0.5328(2) 0.0570(14) Uani 1 1 d . . . . . H19 H 0.933606 0.872825 0.526785 0.068 Uiso 1 1 calc R U . . . C20 C 0.9345(4) 0.8274(3) 0.5903(2) 0.0542(14) Uani 1 1 d . . . . . H20 H 0.932613 0.874907 0.622851 0.065 Uiso 1 1 calc R U . . . C21 C 0.9375(4) 0.7589(3) 0.60057(19) 0.0438(11) Uani 1 1 d . . . . . C22 C 0.9405(4) 0.6907(3) 0.5519(2) 0.0540(14) Uani 1 1 d . . . . . H22 H 0.944227 0.643904 0.558086 0.065 Uiso 1 1 calc R U . . . C23 C 0.9382(4) 0.6898(3) 0.4948(2) 0.0553(14) Uani 1 1 d . . . . . H23 H 0.939043 0.642111 0.462085 0.066 Uiso 1 1 calc R U . . . C24 C 0.9391(3) 0.7605(3) 0.66252(18) 0.0402(11) Uani 1 1 d . . . . . C25 C 0.9239(4) 0.6929(3) 0.6718(2) 0.0599(15) Uani 1 1 d . . . . . H25 H 0.913525 0.643538 0.638391 0.072 Uiso 1 1 calc R U . . . C26 C 0.9241(4) 0.6979(3) 0.7298(2) 0.0525(13) Uani 1 1 d . . . . . H26 H 0.913704 0.650861 0.734964 0.063 Uiso 1 1 calc R U . . . C27 C 0.9515(3) 0.8297(3) 0.77003(19) 0.0391(10) Uani 1 1 d . . . . . H27 H 0.961997 0.878329 0.804262 0.047 Uiso 1 1 calc R U . . . C28 C 0.9511(3) 0.8298(3) 0.71359(18) 0.0423(11) Uani 1 1 d . . . . . H28 H 0.959098 0.877772 0.709481 0.051 Uiso 1 1 calc R U . . . C29 C 1.0776(4) 0.8729(3) 0.3608(2) 0.0528(13) Uani 1 1 d . . . . . H29A H 1.120847 0.902902 0.403203 0.063 Uiso 1 1 calc R U . . . H29B H 1.120704 0.847978 0.334288 0.063 Uiso 1 1 calc R U . . . C30 C 1.0238(3) 0.9278(3) 0.3370(2) 0.0456(12) Uani 1 1 d . . . . . C31 C 1.0333(3) 0.9339(3) 0.2833(2) 0.0441(11) Uani 1 1 d . . . . . H31 H 1.084894 0.912344 0.266093 0.053 Uiso 1 1 calc R U . . . C32 C 0.9697(3) 0.9705(3) 0.25459(19) 0.0423(11) Uani 1 1 d . . . . . C33 C 0.8945(4) 1.0041(3) 0.2785(2) 0.0454(12) Uani 1 1 d . . . . . C34 C 0.8901(4) 1.0029(3) 0.3359(2) 0.0485(12) Uani 1 1 d . . . . . H34 H 0.841437 1.027364 0.354675 0.058 Uiso 1 1 calc R U . . . C35 C 0.9541(4) 0.9674(3) 0.3644(2) 0.0479(12) Uani 1 1 d . . . . . C36 C 1.0562(4) 0.9535(3) 0.1777(2) 0.0559(14) Uani 1 1 d . . . . . H36A H 1.050971 0.961912 0.139858 0.084 Uiso 1 1 calc R U . . . H36B H 1.058050 0.898348 0.168850 0.084 Uiso 1 1 calc R U . . . H36C H 1.117287 0.984761 0.209099 0.084 Uiso 1 1 calc R U . . . C37 C 0.8655(5) 0.9729(5) 0.4382(3) 0.096(2) Uani 1 1 d . . . . . H37A H 0.816814 0.926532 0.410003 0.144 Uiso 1 1 calc R U . . . H37B H 0.839391 1.019309 0.435742 0.144 Uiso 1 1 calc R U . . . H37C H 0.877729 0.976514 0.480500 0.144 Uiso 1 1 calc R U . . . C38 C 0.8165(4) 1.0361(3) 0.2437(2) 0.0495(12) Uani 1 1 d . . . . . H38A H 0.849369 1.067217 0.226497 0.059 Uiso 1 1 calc R U . . . H38B H 0.783299 1.071078 0.272793 0.059 Uiso 1 1 calc R U . . . C39 C 0.7387(3) 0.9721(3) 0.1917(2) 0.0437(11) Uani 1 1 d . . . . . C40 C 0.7351(3) 0.9523(3) 0.13022(19) 0.0401(11) Uani 1 1 d . . . . . H40 H 0.780871 0.981032 0.120057 0.048 Uiso 1 1 calc R U . . . C41 C 0.6667(3) 0.8922(3) 0.08376(19) 0.0381(10) Uani 1 1 d . . . . . C42 C 0.6013(3) 0.8458(3) 0.09640(19) 0.0367(10) Uani 1 1 d . . . . . C43 C 0.6052(3) 0.8651(3) 0.1575(2) 0.0429(11) Uani 1 1 d . . . . . H43 H 0.561934 0.834208 0.167473 0.051 Uiso 1 1 calc R U . . . C44 C 0.6696(4) 0.9276(3) 0.2045(2) 0.0467(12) Uani 1 1 d . . . . . C45 C 0.5853(8) 0.9855(6) 0.2794(4) 0.095(4) Uani 0.699(10) 1 d . U P C 1 H45A H 0.593777 1.038579 0.281425 0.142 Uiso 0.699(10) 1 calc R U P C 1 H45B H 0.578816 0.987135 0.318999 0.142 Uiso 0.699(10) 1 calc R U P C 1 H45C H 0.525238 0.955018 0.246554 0.142 Uiso 0.699(10) 1 calc R U P C 1 C45A C 0.6141(16) 0.9014(13) 0.2820(9) 0.077(6) Uani 0.301(10) 1 d . U P C 3 H45D H 0.543365 0.902925 0.266105 0.116 Uiso 0.301(10) 1 calc R U P C 3 H45E H 0.631276 0.919771 0.327097 0.116 Uiso 0.301(10) 1 calc R U P C 3 H45F H 0.627302 0.847985 0.264071 0.116 Uiso 0.301(10) 1 calc R U P C 3 C46 C 0.7173(4) 0.9187(3) 0.0049(2) 0.0593(14) Uani 1 1 d . . . . . H46A H 0.704865 0.897085 -0.040049 0.089 Uiso 1 1 calc R U . . . H46B H 0.787421 0.919326 0.024235 0.089 Uiso 1 1 calc R U . . . H46C H 0.701960 0.971828 0.019362 0.089 Uiso 1 1 calc R U . . . C47 C 0.5305(3) 0.7770(3) 0.04340(19) 0.0381(10) Uani 1 1 d . . . . . H47A H 0.473991 0.796167 0.023155 0.046 Uiso 1 1 calc R U . . . H47B H 0.566020 0.750491 0.012383 0.046 Uiso 1 1 calc R U . . . C48 C 0.4911(3) 0.7196(3) 0.06512(18) 0.0371(10) Uani 1 1 d . . . . . C49 C 0.5498(3) 0.6639(3) 0.07115(19) 0.0378(10) Uani 1 1 d . . . . . H49 H 0.606154 0.659062 0.055277 0.045 Uiso 1 1 calc R U . . . C50 C 0.5300(3) 0.6151(3) 0.09917(19) 0.0395(10) Uani 1 1 d . . . . . C51 C 0.4461(3) 0.6206(3) 0.1224(2) 0.0386(10) Uani 1 1 d . . . . . C52 C 0.4266(4) 0.5760(3) 0.1596(2) 0.0501(12) Uani 1 1 d . . . . . H52A H 0.418185 0.519534 0.134116 0.060 Uiso 1 1 calc R U . . . H52B H 0.363741 0.587377 0.170930 0.060 Uiso 1 1 calc R U . . . C53 C 0.5106(4) 0.5968(3) 0.2177(2) 0.0441(11) Uani 1 1 d . . . . . C54 C 0.5599(4) 0.5403(3) 0.2302(2) 0.0514(12) Uani 1 1 d . . . . . H54 H 0.536653 0.487179 0.203484 0.062 Uiso 0.446(5) 1 calc R U P B 1 C55 C 0.6424(4) 0.5595(3) 0.2806(2) 0.0545(13) Uani 1 1 d . . . . . H55 H 0.674997 0.519571 0.288019 0.065 Uiso 0.554(5) 1 calc R U P B 2 C56 C 0.6778(4) 0.6376(4) 0.3208(2) 0.0591(14) Uani 1 1 d . . . . . C57 C 0.6273(5) 0.6941(3) 0.3096(3) 0.0668(16) Uani 1 1 d . . . . . H57 H 0.649462 0.747324 0.336539 0.080 Uiso 0.446(5) 1 calc R U P B 1 C58 C 0.5445(4) 0.6735(3) 0.2593(2) 0.0589(14) Uani 1 1 d . . . . . H58 H 0.509828 0.713108 0.253103 0.071 Uiso 0.554(5) 1 calc R U P B 2 C59 C 0.4319(19) 0.7782(13) 0.2986(10) 0.184(7) Uani 0.446(5) 1 d D U P B 1 H59A H 0.448943 0.772752 0.338030 0.276 Uiso 0.446(5) 1 d R U P B 1 H59B H 0.362763 0.754002 0.275860 0.276 Uiso 0.446(5) 1 d R U P B 1 H59C H 0.439573 0.833552 0.306330 0.276 Uiso 0.446(5) 1 d R U P B 1 C59A C 0.6224(13) 0.8245(8) 0.3207(7) 0.142(5) Uani 0.554(5) 1 d D U P B 2 H59D H 0.639827 0.814030 0.281962 0.213 Uiso 0.554(5) 1 calc R U P B 2 H59E H 0.650253 0.878182 0.349790 0.213 Uiso 0.554(5) 1 calc R U P B 2 H59F H 0.549671 0.817189 0.312546 0.213 Uiso 0.554(5) 1 calc R U P B 2 C60 C 0.6512(12) 0.4193(8) 0.2501(7) 0.094(4) Uani 0.446(5) 1 d D U P B 1 H60A H 0.653122 0.405240 0.207303 0.141 Uiso 0.446(5) 1 calc R U P B 1 H60B H 0.581891 0.412058 0.251228 0.141 Uiso 0.446(5) 1 calc R U P B 1 H60C H 0.688601 0.385958 0.266851 0.141 Uiso 0.446(5) 1 calc R U P B 1 C60A C 0.5772(10) 0.4046(6) 0.2066(6) 0.085(3) Uani 0.554(5) 1 d D U P B 2 H60D H 0.551646 0.354241 0.171670 0.127 Uiso 0.554(5) 1 calc R U P B 2 H60E H 0.568686 0.401065 0.244347 0.127 Uiso 0.554(5) 1 calc R U P B 2 H60F H 0.648105 0.418903 0.211615 0.127 Uiso 0.554(5) 1 calc R U P B 2 C61 C 0.7716(4) 0.6591(4) 0.3739(3) 0.0757(19) Uani 1 1 d . . . . . H61A H 0.794797 0.610816 0.375209 0.091 Uiso 1 1 calc R U . . . H61B H 0.755217 0.687616 0.413113 0.091 Uiso 1 1 calc R U . . . C62 C 0.3869(3) 0.6753(3) 0.1153(2) 0.0435(11) Uani 1 1 d . . . . . H62 H 0.329137 0.678519 0.129729 0.052 Uiso 1 1 calc R U . . . C63 C 0.4067(3) 0.7255(3) 0.08843(18) 0.0348(10) Uani 1 1 d . . . . . C64 C 0.3494(3) 0.7898(3) 0.0901(2) 0.0395(10) Uani 1 1 d . . . . . C65 C 0.3072(3) 0.8035(3) 0.0380(2) 0.0422(11) Uani 1 1 d . . . . . H65 H 0.306366 0.766525 -0.001728 0.051 Uiso 1 1 calc R U . . . C66 C 0.2665(3) 0.8709(3) 0.04352(19) 0.0393(11) Uani 1 1 d . . . . . H66 H 0.238272 0.879073 0.007320 0.047 Uiso 1 1 calc R U . . . C67 C 0.2660(3) 0.9270(3) 0.1010(2) 0.0392(10) Uani 1 1 d . . . . . C68 C 0.3029(3) 0.9106(3) 0.1523(2) 0.0421(11) Uani 1 1 d . . . . . H68 H 0.300231 0.946284 0.191680 0.051 Uiso 1 1 calc R U . . . C69 C 0.3434(3) 0.8438(3) 0.1474(2) 0.0437(11) Uani 1 1 d . . . . . H69 H 0.367533 0.834244 0.183394 0.052 Uiso 1 1 calc R U . . . C70 C 0.2278(3) 0.9997(3) 0.10611(18) 0.0346(10) Uani 1 1 d . . . . . C71 C 0.1500(3) 1.0035(3) 0.06025(19) 0.0360(10) Uani 1 1 d . . . . . H71 H 0.121250 0.958222 0.023648 0.043 Uiso 1 1 calc R U . . . C72 C 0.1143(3) 1.0721(3) 0.06733(18) 0.0353(10) Uani 1 1 d . . . . . H72 H 0.061759 1.072369 0.034614 0.042 Uiso 1 1 calc R U . . . C73 C 0.2268(3) 1.1362(3) 0.1620(2) 0.0410(11) Uani 1 1 d . . . . . H73 H 0.255405 1.182631 0.197644 0.049 Uiso 1 1 calc R U . . . C74 C 0.2664(3) 1.0684(3) 0.1573(2) 0.0434(11) Uani 1 1 d . . . . . H74 H 0.320580 1.069499 0.189721 0.052 Uiso 1 1 calc R U . . . C75 C 0.6030(3) 0.5624(3) 0.10661(19) 0.0386(10) Uani 1 1 d . . . . . C76 C 0.5803(4) 0.4821(3) 0.0804(2) 0.0446(11) Uani 1 1 d . . . . . H76 H 0.514237 0.457871 0.056472 0.054 Uiso 1 1 calc R U . . . C77 C 0.6524(4) 0.4367(3) 0.0885(2) 0.0458(11) Uani 1 1 d . . . . . H77 H 0.634593 0.381684 0.070545 0.055 Uiso 1 1 calc R U . . . C78 C 0.7505(3) 0.4695(3) 0.12242(19) 0.0385(10) Uani 1 1 d . . . . . C79 C 0.7743(3) 0.5506(3) 0.14844(19) 0.0380(10) Uani 1 1 d . . . . . H79 H 0.840632 0.574414 0.172124 0.046 Uiso 1 1 calc R U . . . C80 C 0.7032(3) 0.5965(3) 0.1403(2) 0.0400(10) Uani 1 1 d . . . . . H80 H 0.721407 0.651379 0.157393 0.048 Uiso 1 1 calc R U . . . C81 C 0.8262(3) 0.4198(2) 0.13119(19) 0.0370(10) Uani 1 1 d . . . . . C82 C 0.8018(3) 0.3495(3) 0.1349(2) 0.0406(11) Uani 1 1 d . . . . . H82 H 0.735214 0.332811 0.132781 0.049 Uiso 1 1 calc R U . . . C83 C 0.8747(4) 0.3039(3) 0.1417(2) 0.0424(11) Uani 1 1 d . . . . . H83 H 0.856477 0.257169 0.145701 0.051 Uiso 1 1 calc R U . . . C84 C 0.9936(3) 0.3901(3) 0.14015(19) 0.0384(10) Uani 1 1 d . . . . . H84 H 1.060716 0.404647 0.141964 0.046 Uiso 1 1 calc R U . . . C85 C 0.9269(3) 0.4409(3) 0.1348(2) 0.0411(11) Uani 1 1 d . . . . . H85 H 0.948508 0.488877 0.133666 0.049 Uiso 1 1 calc R U . . . O11 O 0.8853(4) 0.4475(4) -0.1259(3) 0.130(2) Uani 1 1 d . . . . . N7 N 0.8289(4) 0.4891(4) -0.0406(2) 0.0855(17) Uani 1 1 d . . . . . C86 C 0.7689(7) 0.5427(5) -0.0060(4) 0.129(3) Uani 1 1 d . . . . . H86A H 0.745736 0.576543 -0.026886 0.194 Uiso 1 1 calc R U . . . H86B H 0.810063 0.574506 0.036074 0.194 Uiso 1 1 calc R U . . . H86C H 0.711391 0.512349 -0.004329 0.194 Uiso 1 1 calc R U . . . C88 C 0.8404(5) 0.4916(5) -0.0929(3) 0.092(2) Uani 1 1 d . . . . . H88 H 0.812132 0.529765 -0.105266 0.110 Uiso 1 1 calc R U . . . C87 C 0.8734(6) 0.4332(5) -0.0199(4) 0.115(3) Uani 1 1 d . . . . . H87A H 0.938282 0.457774 0.010221 0.172 Uiso 1 1 calc R U . . . H87B H 0.882408 0.389358 -0.055229 0.172 Uiso 1 1 calc R U . . . H87C H 0.829747 0.414407 -0.000474 0.172 Uiso 1 1 calc R U . . . O12 O 0.3801(8) 0.3001(7) 0.1291(6) 0.129(4) Uani 0.436(3) 1 d D U P D 1 O13 O 0.2925(8) 0.3844(5) 0.1272(5) 0.083(3) Uani 0.436(3) 1 d D U P D 1 O14 O 0.3869(9) 0.3602(6) 0.0713(6) 0.124(4) Uani 0.436(3) 1 d D U P D 1 N6 N 0.3593(8) 0.3509(6) 0.1101(6) 0.090(3) Uani 0.436(3) 1 d D U P D 1 O14A O 0.5266(11) 1.0660(10) 0.1415(10) 0.182(7) Uani 0.418(3) 1 d D U P E 2 O12A O 0.545(2) 1.1522(14) 0.1113(14) 0.212(7) Uani 0.418(3) 1 d D U P E 2 O13A O 0.5048(13) 1.1878(12) 0.1942(10) 0.219(7) Uani 0.418(3) 1 d D U P E 2 N6A N 0.5283(17) 1.1349(11) 0.1522(11) 0.201(7) Uani 0.418(3) 1 d D U P E 2 O13B O 0.533(6) 1.123(4) 0.125(4) 0.187(9) Uani 0.147(3) 1 d D U P F 3 O14B O 0.617(4) 1.115(3) 0.066(3) 0.213(12) Uani 0.147(3) 1 d D U P F 3 O12B O 0.588(3) 1.227(3) 0.108(3) 0.179(11) Uani 0.147(3) 1 d D U P F 3 N6B N 0.578(6) 1.159(3) 0.103(3) 0.201(8) Uani 0.147(3) 1 d D U P F 3 O3A O 1.195(2) 0.884(4) -0.100(4) 0.090(10) Uani 0.29(9) 1 d D U P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0455(4) 0.0369(4) 0.0236(3) 0.0177(3) 0.0143(2) 0.0176(3) O1 0.0495(18) 0.045(2) 0.0315(16) 0.0212(15) 0.0104(14) 0.0168(16) O2 0.070(2) 0.054(2) 0.065(2) 0.034(2) 0.0188(19) 0.0169(19) O3B 0.097(7) 0.062(7) 0.108(13) 0.045(8) 0.074(8) 0.029(6) O4 0.074(2) 0.049(2) 0.0387(18) 0.0172(16) 0.0189(17) 0.0230(18) O5 0.067(2) 0.069(3) 0.0346(18) 0.0203(18) 0.0182(17) -0.0007(19) O6 0.058(2) 0.056(2) 0.0332(17) 0.0227(16) 0.0137(15) 0.0037(17) O7 0.087(3) 0.076(3) 0.0320(18) 0.0229(18) 0.0186(18) 0.006(2) O8 0.062(2) 0.061(2) 0.0346(17) 0.0302(16) 0.0167(15) 0.0101(17) O9 0.238(14) 0.054(6) 0.069(6) 0.030(5) 0.030(7) 0.059(7) O9A 0.126(7) 0.050(5) 0.067(5) 0.023(4) 0.015(4) 0.007(4) O10 0.081(6) 0.112(7) 0.075(6) 0.052(5) 0.005(5) 0.043(5) O10A 0.080(4) 0.046(4) 0.065(4) 0.028(3) 0.010(3) 0.024(3) N1 0.044(2) 0.042(2) 0.0276(18) 0.0189(17) 0.0136(16) 0.0154(17) N2 0.049(2) 0.037(2) 0.0273(18) 0.0185(17) 0.0141(16) 0.0179(17) N3 0.049(2) 0.041(2) 0.0309(19) 0.0203(17) 0.0216(17) 0.0175(18) N4 0.046(2) 0.042(2) 0.0284(18) 0.0191(17) 0.0142(16) 0.0198(18) N5 0.048(2) 0.040(2) 0.032(2) 0.0089(18) 0.0099(18) 0.0144(19) C1 0.042(2) 0.053(3) 0.030(2) 0.023(2) 0.014(2) 0.020(2) C2 0.051(3) 0.053(3) 0.032(2) 0.022(2) 0.022(2) 0.017(2) C3 0.048(3) 0.043(3) 0.023(2) 0.0193(19) 0.0115(19) 0.018(2) C4 0.049(3) 0.057(3) 0.032(2) 0.026(2) 0.012(2) 0.020(2) C5 0.046(3) 0.054(3) 0.027(2) 0.022(2) 0.015(2) 0.022(2) C6 0.052(3) 0.044(3) 0.026(2) 0.019(2) 0.012(2) 0.010(2) C7 0.047(3) 0.048(3) 0.027(2) 0.021(2) 0.013(2) 0.009(2) C8 0.050(3) 0.049(3) 0.028(2) 0.019(2) 0.014(2) 0.005(2) C9 0.066(3) 0.044(3) 0.026(2) 0.017(2) 0.013(2) 0.003(2) C10 0.063(3) 0.071(4) 0.038(3) 0.034(3) 0.012(2) 0.018(3) C11 0.064(3) 0.063(3) 0.035(2) 0.028(2) 0.026(2) 0.029(3) C12 0.065(3) 0.047(3) 0.028(2) 0.022(2) 0.016(2) 0.010(2) C13 0.061(3) 0.058(3) 0.031(2) 0.026(2) 0.013(2) 0.006(3) C14 0.063(3) 0.057(3) 0.026(2) 0.021(2) 0.009(2) 0.007(3) C15 0.065(3) 0.057(3) 0.031(2) 0.025(2) 0.014(2) 0.009(3) C16 0.065(3) 0.058(3) 0.028(2) 0.022(2) 0.010(2) 0.002(3) C17 0.073(3) 0.060(4) 0.028(2) 0.022(2) 0.010(2) 0.003(3) C18 0.065(3) 0.057(3) 0.024(2) 0.019(2) 0.012(2) 0.004(3) C19 0.096(4) 0.050(3) 0.031(2) 0.022(2) 0.019(3) 0.006(3) C20 0.094(4) 0.045(3) 0.023(2) 0.016(2) 0.014(2) 0.001(3) C21 0.061(3) 0.047(3) 0.029(2) 0.021(2) 0.013(2) 0.007(2) C22 0.094(4) 0.050(3) 0.034(3) 0.026(2) 0.029(3) 0.023(3) C23 0.089(4) 0.050(3) 0.033(3) 0.019(2) 0.020(3) 0.018(3) C24 0.057(3) 0.040(3) 0.024(2) 0.014(2) 0.011(2) 0.007(2) C25 0.112(5) 0.044(3) 0.032(3) 0.019(2) 0.028(3) 0.014(3) C26 0.096(4) 0.045(3) 0.033(2) 0.026(2) 0.029(3) 0.021(3) C27 0.056(3) 0.035(3) 0.026(2) 0.0114(19) 0.011(2) 0.010(2) C28 0.064(3) 0.042(3) 0.027(2) 0.021(2) 0.013(2) 0.006(2) C29 0.059(3) 0.068(4) 0.037(3) 0.030(3) 0.009(2) 0.004(3) C30 0.052(3) 0.051(3) 0.032(2) 0.020(2) 0.005(2) -0.004(2) C31 0.051(3) 0.048(3) 0.035(2) 0.021(2) 0.011(2) 0.001(2) C32 0.053(3) 0.044(3) 0.033(2) 0.019(2) 0.013(2) 0.000(2) C33 0.064(3) 0.038(3) 0.035(2) 0.018(2) 0.012(2) 0.000(2) C34 0.057(3) 0.050(3) 0.036(2) 0.015(2) 0.013(2) 0.000(2) C35 0.061(3) 0.052(3) 0.034(2) 0.021(2) 0.013(2) 0.003(3) C36 0.066(3) 0.067(4) 0.048(3) 0.033(3) 0.022(3) 0.008(3) C37 0.106(5) 0.145(7) 0.068(4) 0.060(5) 0.048(4) 0.028(5) C38 0.064(3) 0.051(3) 0.041(3) 0.023(2) 0.018(2) 0.008(3) C39 0.053(3) 0.038(3) 0.038(2) 0.014(2) 0.012(2) 0.005(2) C40 0.047(3) 0.047(3) 0.038(2) 0.027(2) 0.016(2) 0.010(2) C41 0.045(3) 0.044(3) 0.030(2) 0.021(2) 0.009(2) 0.012(2) C42 0.041(2) 0.043(3) 0.037(2) 0.024(2) 0.017(2) 0.020(2) C43 0.052(3) 0.042(3) 0.039(3) 0.017(2) 0.019(2) 0.007(2) C44 0.056(3) 0.058(3) 0.033(2) 0.021(2) 0.020(2) 0.014(3) C45 0.129(8) 0.102(8) 0.066(6) 0.028(6) 0.052(6) 0.044(7) C45A 0.099(13) 0.101(14) 0.057(10) 0.044(10) 0.047(9) 0.023(11) C46 0.077(4) 0.067(4) 0.045(3) 0.032(3) 0.022(3) 0.008(3) C47 0.042(2) 0.043(3) 0.036(2) 0.019(2) 0.016(2) 0.018(2) C48 0.041(2) 0.037(3) 0.031(2) 0.013(2) 0.0069(19) 0.012(2) C49 0.043(3) 0.036(3) 0.034(2) 0.013(2) 0.012(2) 0.015(2) C50 0.047(3) 0.036(3) 0.034(2) 0.015(2) 0.005(2) 0.014(2) C51 0.045(3) 0.030(2) 0.041(2) 0.017(2) 0.007(2) 0.011(2) C52 0.052(3) 0.045(3) 0.061(3) 0.027(3) 0.018(3) 0.006(2) C53 0.053(3) 0.043(3) 0.043(3) 0.023(2) 0.014(2) 0.009(2) C54 0.059(3) 0.048(3) 0.053(3) 0.025(3) 0.017(3) 0.009(3) C55 0.061(3) 0.065(4) 0.049(3) 0.034(3) 0.018(3) 0.012(3) C56 0.073(4) 0.069(4) 0.044(3) 0.035(3) 0.014(3) -0.007(3) C57 0.097(5) 0.050(4) 0.047(3) 0.020(3) 0.009(3) 0.000(3) C58 0.081(4) 0.041(3) 0.056(3) 0.022(3) 0.016(3) 0.011(3) C59 0.282(16) 0.103(10) 0.118(10) 0.013(9) 0.017(11) 0.048(11) C59A 0.184(10) 0.061(7) 0.130(9) 0.006(7) 0.009(8) 0.012(7) C60 0.103(7) 0.093(7) 0.081(7) 0.042(6) 0.001(6) 0.038(6) C60A 0.111(7) 0.061(5) 0.077(6) 0.032(5) 0.004(5) 0.028(5) C61 0.084(4) 0.094(5) 0.051(3) 0.047(3) 0.001(3) -0.019(4) C62 0.042(3) 0.041(3) 0.048(3) 0.017(2) 0.013(2) 0.012(2) C63 0.037(2) 0.039(3) 0.030(2) 0.015(2) 0.0094(19) 0.011(2) C64 0.044(3) 0.042(3) 0.039(2) 0.020(2) 0.014(2) 0.016(2) C65 0.046(3) 0.042(3) 0.037(2) 0.015(2) 0.008(2) 0.017(2) C66 0.043(3) 0.050(3) 0.031(2) 0.021(2) 0.009(2) 0.022(2) C67 0.040(2) 0.046(3) 0.039(2) 0.023(2) 0.014(2) 0.016(2) C68 0.053(3) 0.051(3) 0.035(2) 0.025(2) 0.017(2) 0.028(2) C69 0.054(3) 0.050(3) 0.039(2) 0.027(2) 0.014(2) 0.024(2) C70 0.038(2) 0.045(3) 0.032(2) 0.023(2) 0.0160(19) 0.017(2) C71 0.050(3) 0.037(3) 0.031(2) 0.019(2) 0.018(2) 0.020(2) C72 0.040(2) 0.047(3) 0.027(2) 0.022(2) 0.0107(19) 0.016(2) C73 0.046(3) 0.042(3) 0.033(2) 0.014(2) 0.009(2) 0.014(2) C74 0.046(3) 0.054(3) 0.033(2) 0.022(2) 0.006(2) 0.022(2) C75 0.050(3) 0.036(3) 0.031(2) 0.013(2) 0.011(2) 0.018(2) C76 0.049(3) 0.037(3) 0.040(3) 0.010(2) 0.006(2) 0.013(2) C77 0.059(3) 0.029(3) 0.045(3) 0.011(2) 0.011(2) 0.013(2) C78 0.048(3) 0.034(3) 0.036(2) 0.017(2) 0.011(2) 0.014(2) C79 0.041(2) 0.036(3) 0.034(2) 0.015(2) 0.004(2) 0.012(2) C80 0.046(3) 0.031(3) 0.043(3) 0.016(2) 0.009(2) 0.015(2) C81 0.050(3) 0.030(2) 0.036(2) 0.0140(19) 0.015(2) 0.019(2) C82 0.046(3) 0.037(3) 0.048(3) 0.021(2) 0.021(2) 0.018(2) C83 0.064(3) 0.033(3) 0.046(3) 0.026(2) 0.026(2) 0.017(2) C84 0.042(2) 0.039(3) 0.038(2) 0.021(2) 0.009(2) 0.010(2) C85 0.050(3) 0.032(3) 0.041(3) 0.017(2) 0.008(2) 0.009(2) O11 0.118(4) 0.186(7) 0.123(5) 0.079(5) 0.065(4) 0.046(4) N7 0.092(4) 0.103(5) 0.059(3) 0.036(3) 0.015(3) -0.006(3) C86 0.185(9) 0.100(7) 0.099(6) 0.024(5) 0.062(6) -0.002(6) C88 0.077(5) 0.127(7) 0.087(5) 0.056(5) 0.030(4) 0.008(5) C87 0.129(7) 0.132(8) 0.099(6) 0.076(6) 0.010(5) 0.018(6) O12 0.086(7) 0.088(8) 0.148(10) 0.009(7) -0.025(7) 0.038(6) O13 0.110(7) 0.051(6) 0.091(7) 0.026(5) 0.037(6) 0.018(5) O14 0.140(9) 0.058(7) 0.128(9) -0.029(6) 0.079(7) -0.030(6) N6 0.088(7) 0.038(6) 0.122(8) -0.005(5) 0.053(6) -0.002(5) O14A 0.085(8) 0.135(12) 0.300(14) 0.064(11) 0.043(9) 0.033(9) O12A 0.113(10) 0.213(13) 0.245(12) 0.053(10) -0.001(9) 0.012(10) O13A 0.124(10) 0.173(13) 0.277(14) 0.033(11) 0.014(10) -0.015(10) N6A 0.108(8) 0.187(11) 0.257(12) 0.055(9) 0.018(8) 0.018(9) O13B 0.094(10) 0.176(13) 0.257(14) 0.068(12) 0.024(11) 0.012(11) O14B 0.127(16) 0.211(18) 0.242(18) 0.055(16) 0.007(15) 0.020(16) O12B 0.104(15) 0.181(18) 0.215(17) 0.071(16) -0.001(15) -0.015(16) N6B 0.108(10) 0.194(13) 0.248(13) 0.057(11) 0.009(10) 0.017(11) O3A 0.072(11) 0.089(14) 0.13(2) 0.050(19) 0.048(12) 0.019(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Co1 N1 85.52(12) . . ? O1 Co1 N2 93.74(13) . 1_554 ? O1 Co1 N3 86.10(13) . 2_765 ? O1 Co1 N4 87.52(13) . 2_675 ? O4 Co1 O1 177.01(11) . . ? O4 Co1 N1 91.81(13) . . ? O4 Co1 N2 88.90(13) . 1_554 ? O4 Co1 N3 92.49(14) . 2_765 ? O4 Co1 N4 93.89(14) . 2_675 ? N2 Co1 N1 178.57(13) 1_554 . ? N2 Co1 N3 90.28(12) 1_554 2_765 ? N3 Co1 N1 88.45(12) 2_765 . ? N4 Co1 N1 91.38(12) 2_675 . ? N4 Co1 N2 89.81(12) 2_675 1_554 ? N4 Co1 N3 173.61(15) 2_675 2_765 ? N5 O1 Co1 129.6(3) . . ? Co1 O4 H4A 109.4 . . ? Co1 O4 H4B 109.2 . . ? H4A O4 H4B 104.4 . . ? C44 O5 C45 111.3(5) . . ? C44 O5 C45A 118.7(9) . . ? C41 O6 C46 117.2(4) . . ? C35 O7 C37 117.9(4) . . ? C32 O8 C36 117.2(4) . . ? C58 O9 C59 131.8(12) . . ? C57 O9A C59A 113.7(8) . . ? C55 O10 C60 119.5(9) . . ? C54 O10A C60A 119.1(7) . . ? C1 N1 Co1 121.5(3) . . ? C5 N1 Co1 122.2(3) . . ? C5 N1 C1 116.2(3) . . ? C26 N2 Co1 120.4(3) . 1_556 ? C27 N2 Co1 123.2(3) . 1_556 ? C27 N2 C26 116.3(3) . . ? C83 N3 Co1 119.8(3) . 2_765 ? C84 N3 Co1 122.9(3) . 2_765 ? C84 N3 C83 116.4(4) . . ? C72 N4 Co1 120.5(3) . 2_675 ? C72 N4 C73 115.9(4) . . ? C73 N4 Co1 122.6(3) . 2_675 ? O1 N5 O2 122.7(4) . . ? O1 N5 O3B 121.4(10) . . ? O1 N5 O3A 114(3) . . ? O2 N5 O3B 115.7(10) . . ? O2 N5 O3A 120(3) . . ? N1 C1 H1 118.3 . . ? N1 C1 C2 123.4(4) . . ? C2 C1 H1 118.3 . . ? C1 C2 H2 119.7 . . ? C1 C2 C3 120.7(4) . . ? C3 C2 H2 119.7 . . ? C2 C3 C4 115.3(4) . . ? C2 C3 C6 121.5(4) . . ? C4 C3 C6 123.2(4) . . ? C3 C4 H4 119.6 . . ? C5 C4 C3 120.9(4) . . ? C5 C4 H4 119.6 . . ? N1 C5 C4 123.5(4) . . ? N1 C5 H5 118.2 . . ? C4 C5 H5 118.2 . . ? C7 C6 C3 122.3(4) . . ? C7 C6 C11 117.6(4) . . ? C11 C6 C3 120.1(4) . . ? C6 C7 H7 119.2 . . ? C8 C7 C6 121.5(4) . . ? C8 C7 H7 119.2 . . ? C7 C8 H8 119.5 . . ? C7 C8 C9 121.0(4) . . ? C9 C8 H8 119.5 . . ? C8 C9 C10 118.9(4) . . ? C8 C9 C12 121.3(4) . . ? C10 C9 C12 119.8(4) . . ? C9 C10 H10 119.9 . . ? C11 C10 C9 120.2(4) . . ? C11 C10 H10 119.9 . . ? C6 C11 H11 119.6 . . ? C10 C11 C6 120.8(4) . . ? C10 C11 H11 119.6 . . ? C13 C12 C9 122.8(4) . . ? C13 C12 C17 119.2(4) . . ? C17 C12 C9 118.1(4) . . ? C12 C13 C14 117.7(4) . . ? C12 C13 C29 122.6(4) . . ? C14 C13 C29 119.5(4) . . ? C13 C14 H14 118.7 . . ? C15 C14 C13 122.7(5) . . ? C15 C14 H14 118.7 . . ? C14 C15 C18 119.1(4) . . ? C16 C15 C14 119.0(4) . . ? C16 C15 C18 121.7(4) . . ? C15 C16 C61 120.3(4) . . ? C17 C16 C15 118.0(5) . . ? C17 C16 C61 121.7(5) . . ? C12 C17 H17 118.4 . . ? C16 C17 C12 123.3(5) . . ? C16 C17 H17 118.4 . . ? C19 C18 C15 120.7(5) . . ? C19 C18 C23 118.1(4) . . ? C23 C18 C15 121.2(4) . . ? C18 C19 H19 119.4 . . ? C18 C19 C20 121.2(5) . . ? C20 C19 H19 119.4 . . ? C19 C20 H20 119.9 . . ? C19 C20 C21 120.3(5) . . ? C21 C20 H20 119.9 . . ? C20 C21 C24 120.4(4) . . ? C22 C21 C20 118.1(4) . . ? C22 C21 C24 121.5(4) . . ? C21 C22 H22 119.5 . . ? C23 C22 C21 121.0(5) . . ? C23 C22 H22 119.5 . . ? C18 C23 H23 119.3 . . ? C22 C23 C18 121.3(5) . . ? C22 C23 H23 119.3 . . ? C25 C24 C21 122.1(4) . . ? C28 C24 C21 121.8(4) . . ? C28 C24 C25 116.1(4) . . ? C24 C25 H25 120.2 . . ? C26 C25 C24 119.6(5) . . ? C26 C25 H25 120.2 . . ? N2 C26 C25 124.0(5) . . ? N2 C26 H26 118.0 . . ? C25 C26 H26 118.0 . . ? N2 C27 H27 118.4 . . ? N2 C27 C28 123.3(4) . . ? C28 C27 H27 118.4 . . ? C24 C28 H28 119.6 . . ? C27 C28 C24 120.7(4) . . ? C27 C28 H28 119.6 . . ? C13 C29 H29A 109.3 . . ? C13 C29 H29B 109.3 . . ? H29A C29 H29B 108.0 . . ? C30 C29 C13 111.4(4) . . ? C30 C29 H29A 109.3 . . ? C30 C29 H29B 109.3 . . ? C31 C30 C29 121.4(4) . . ? C31 C30 C35 117.4(5) . . ? C35 C30 C29 120.8(4) . . ? C30 C31 H31 119.3 . . ? C32 C31 C30 121.4(4) . . ? C32 C31 H31 119.3 . . ? O8 C32 C33 114.3(4) . . ? C31 C32 O8 124.3(4) . . ? C31 C32 C33 121.4(4) . . ? C32 C33 C34 116.8(4) . . ? C32 C33 C38 122.1(4) . . ? C34 C33 C38 121.0(4) . . ? C33 C34 H34 119.3 . . ? C35 C34 C33 121.3(5) . . ? C35 C34 H34 119.3 . . ? O7 C35 C30 115.7(4) . . ? C34 C35 O7 123.2(4) . . ? C34 C35 C30 121.2(4) . . ? O8 C36 H36A 109.5 . . ? O8 C36 H36B 109.5 . . ? O8 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? O7 C37 H37A 109.5 . . ? O7 C37 H37B 109.5 . . ? O7 C37 H37C 109.5 . . ? H37A C37 H37B 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.2 . . ? C33 C38 H38B 109.2 . . ? C33 C38 C39 112.0(4) . . ? H38A C38 H38B 107.9 . . ? C39 C38 H38A 109.2 . . ? C39 C38 H38B 109.2 . . ? C40 C39 C38 122.0(4) . . ? C40 C39 C44 117.3(4) . . ? C44 C39 C38 120.7(4) . . ? C39 C40 H40 119.4 . . ? C41 C40 C39 121.3(4) . . ? C41 C40 H40 119.4 . . ? O6 C41 C42 114.1(4) . . ? C40 C41 O6 124.3(4) . . ? C40 C41 C42 121.5(4) . . ? C41 C42 C47 119.6(4) . . ? C43 C42 C41 117.1(4) . . ? C43 C42 C47 123.2(4) . . ? C42 C43 H43 118.9 . . ? C44 C43 C42 122.1(4) . . ? C44 C43 H43 118.9 . . ? O5 C44 C39 116.5(4) . . ? C43 C44 O5 122.9(4) . . ? C43 C44 C39 120.5(4) . . ? O5 C45 H45A 109.5 . . ? O5 C45 H45B 109.5 . . ? O5 C45 H45C 109.5 . . ? H45A C45 H45B 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? O5 C45A H45D 109.5 . . ? O5 C45A H45E 109.5 . . ? O5 C45A H45F 109.5 . . ? H45D C45A H45E 109.5 . . ? H45D C45A H45F 109.5 . . ? H45E C45A H45F 109.5 . . ? O6 C46 H46A 109.5 . . ? O6 C46 H46B 109.5 . . ? O6 C46 H46C 109.5 . . ? H46A C46 H46B 109.5 . . ? H46A C46 H46C 109.5 . . ? H46B C46 H46C 109.5 . . ? C42 C47 H47A 109.2 . . ? C42 C47 H47B 109.2 . . ? H47A C47 H47B 107.9 . . ? C48 C47 C42 112.0(3) . . ? C48 C47 H47A 109.2 . . ? C48 C47 H47B 109.2 . . ? C49 C48 C47 117.4(4) . . ? C49 C48 C63 117.7(4) . . ? C63 C48 C47 124.2(4) . . ? C48 C49 H49 118.3 . . ? C50 C49 C48 123.3(4) . . ? C50 C49 H49 118.3 . . ? C49 C50 C51 119.3(4) . . ? C49 C50 C75 117.6(4) . . ? C51 C50 C75 123.0(4) . . ? C50 C51 C52 122.1(4) . . ? C62 C51 C50 117.1(4) . . ? C62 C51 C52 120.4(4) . . ? C51 C52 H52A 109.3 . . ? C51 C52 H52B 109.3 . . ? C51 C52 C53 111.7(4) . . ? H52A C52 H52B 107.9 . . ? C53 C52 H52A 109.3 . . ? C53 C52 H52B 109.3 . . ? C54 C53 C52 121.2(5) . . ? C54 C53 C58 117.2(5) . . ? C58 C53 C52 121.5(4) . . ? O10A C54 C53 119.5(5) . . ? O10A C54 C55 118.7(5) . . ? C53 C54 H54 119.2 . . ? C53 C54 C55 121.7(5) . . ? C55 C54 H54 119.2 . . ? C54 C55 O10 118.7(7) . . ? C54 C55 H55 119.9 . . ? C54 C55 C56 120.1(5) . . ? C56 C55 O10 120.8(6) . . ? C56 C55 H55 119.9 . . ? C55 C56 C61 120.3(5) . . ? C57 C56 C55 118.5(5) . . ? C57 C56 C61 121.1(6) . . ? O9A C57 C56 119.4(6) . . ? O9A C57 C58 120.3(6) . . ? C56 C57 H57 119.9 . . ? C56 C57 C58 120.2(6) . . ? C58 C57 H57 119.9 . . ? O9 C58 C53 116.4(7) . . ? O9 C58 C57 120.6(7) . . ? C53 C58 H58 118.9 . . ? C57 C58 C53 122.2(5) . . ? C57 C58 H58 118.9 . . ? O9 C59 H59A 111.4 . . ? O9 C59 H59B 98.7 . . ? O9 C59 H59C 117.7 . . ? H59A C59 H59B 109.5 . . ? H59A C59 H59C 109.5 . . ? H59B C59 H59C 109.4 . . ? O9A C59A H59D 109.5 . . ? O9A C59A H59E 109.5 . . ? O9A C59A H59F 109.5 . . ? H59D C59A H59E 109.5 . . ? H59D C59A H59F 109.5 . . ? H59E C59A H59F 109.5 . . ? O10 C60 H60A 109.5 . . ? O10 C60 H60B 109.5 . . ? O10 C60 H60C 109.5 . . ? H60A C60 H60B 109.5 . . ? H60A C60 H60C 109.5 . . ? H60B C60 H60C 109.5 . . ? O10A C60A H60D 109.5 . . ? O10A C60A H60E 109.5 . . ? O10A C60A H60F 109.5 . . ? H60D C60A H60E 109.5 . . ? H60D C60A H60F 109.5 . . ? H60E C60A H60F 109.5 . . ? C16 C61 H61A 108.8 . . ? C16 C61 H61B 108.8 . . ? C56 C61 C16 113.7(4) . . ? C56 C61 H61A 108.8 . . ? C56 C61 H61B 108.8 . . ? H61A C61 H61B 107.7 . . ? C51 C62 H62 117.9 . . ? C63 C62 C51 124.3(4) . . ? C63 C62 H62 117.9 . . ? C48 C63 C64 119.8(4) . . ? C62 C63 C48 118.2(4) . . ? C62 C63 C64 121.6(4) . . ? C65 C64 C63 123.1(4) . . ? C65 C64 C69 117.5(4) . . ? C69 C64 C63 119.1(4) . . ? C64 C65 H65 119.7 . . ? C66 C65 C64 120.6(4) . . ? C66 C65 H65 119.7 . . ? C65 C66 H66 119.1 . . ? C65 C66 C67 121.7(4) . . ? C67 C66 H66 119.1 . . ? C66 C67 C70 120.8(4) . . ? C68 C67 C66 117.2(4) . . ? C68 C67 C70 122.0(4) . . ? C67 C68 H68 119.2 . . ? C69 C68 C67 121.6(4) . . ? C69 C68 H68 119.2 . . ? C64 C69 H69 119.4 . . ? C68 C69 C64 121.2(4) . . ? C68 C69 H69 119.4 . . ? C71 C70 C67 122.2(4) . . ? C74 C70 C67 121.8(4) . . ? C74 C70 C71 116.0(4) . . ? C70 C71 H71 119.7 . . ? C72 C71 C70 120.7(4) . . ? C72 C71 H71 119.7 . . ? N4 C72 C71 124.0(4) . . ? N4 C72 H72 118.0 . . ? C71 C72 H72 118.0 . . ? N4 C73 H73 118.7 . . ? N4 C73 C74 122.7(4) . . ? C74 C73 H73 118.7 . . ? C70 C74 C73 120.7(4) . . ? C70 C74 H74 119.6 . . ? C73 C74 H74 119.6 . . ? C76 C75 C50 124.1(4) . . ? C76 C75 C80 118.0(4) . . ? C80 C75 C50 117.9(4) . . ? C75 C76 H76 119.5 . . ? C77 C76 C75 120.9(5) . . ? C77 C76 H76 119.5 . . ? C76 C77 H77 119.2 . . ? C76 C77 C78 121.6(4) . . ? C78 C77 H77 119.2 . . ? C77 C78 C79 117.8(4) . . ? C77 C78 C81 120.6(4) . . ? C79 C78 C81 121.5(4) . . ? C78 C79 H79 119.4 . . ? C80 C79 C78 121.1(4) . . ? C80 C79 H79 119.4 . . ? C75 C80 H80 119.7 . . ? C79 C80 C75 120.5(4) . . ? C79 C80 H80 119.7 . . ? C82 C81 C78 121.9(4) . . ? C82 C81 C85 116.8(4) . . ? C85 C81 C78 121.3(4) . . ? C81 C82 H82 120.0 . . ? C83 C82 C81 119.9(4) . . ? C83 C82 H82 120.0 . . ? N3 C83 C82 123.7(4) . . ? N3 C83 H83 118.1 . . ? C82 C83 H83 118.1 . . ? N3 C84 H84 117.8 . . ? N3 C84 C85 124.4(4) . . ? C85 C84 H84 117.8 . . ? C81 C85 H85 120.7 . . ? C84 C85 C81 118.7(4) . . ? C84 C85 H85 120.7 . . ? C88 N7 C86 119.5(7) . . ? C88 N7 C87 119.1(7) . . ? C87 N7 C86 121.4(6) . . ? N7 C86 H86A 109.5 . . ? N7 C86 H86B 109.5 . . ? N7 C86 H86C 109.5 . . ? H86A C86 H86B 109.5 . . ? H86A C86 H86C 109.5 . . ? H86B C86 H86C 109.5 . . ? O11 C88 N7 124.1(8) . . ? O11 C88 H88 117.9 . . ? N7 C88 H88 117.9 . . ? N7 C87 H87A 109.5 . . ? N7 C87 H87B 109.5 . . ? N7 C87 H87C 109.5 . . ? H87A C87 H87B 109.5 . . ? H87A C87 H87C 109.5 . . ? H87B C87 H87C 109.5 . . ? O13 N6 O12 114.5(11) . . ? O14 N6 O12 125.2(13) . . ? O14 N6 O13 119.3(12) . . ? O14A N6A O12A 113.8(18) . . ? O14A N6A O13A 130(2) . . ? O12A N6A O13A 115.6(18) . . ? O14B N6B O13B 110(2) . . ? O12B N6B O13B 135(3) . . ? O12B N6B O14B 115(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 O1 2.153(3) . ? Co1 O4 2.099(4) . ? Co1 N1 2.164(3) . ? Co1 N2 2.160(3) 1_554 ? Co1 N3 2.161(3) 2_765 ? Co1 N4 2.156(3) 2_675 ? O1 N5 1.205(5) . ? O2 N5 1.248(5) . ? O3B N5 1.267(8) . ? O4 H4A 0.8719 . ? O4 H4B 0.8721 . ? O5 C44 1.389(5) . ? O5 C45 1.460(9) . ? O5 C45A 1.402(19) . ? O6 C41 1.388(5) . ? O6 C46 1.425(6) . ? O7 C35 1.378(5) . ? O7 C37 1.407(7) . ? O8 C32 1.386(5) . ? O8 C36 1.415(5) . ? O9 C58 1.371(11) . ? O9 C59 1.499(15) . ? O9A C57 1.377(9) . ? O9A C59A 1.456(13) . ? O10 C55 1.412(10) . ? O10 C60 1.451(13) . ? O10A C54 1.365(8) . ? O10A C60A 1.459(10) . ? N1 C1 1.341(5) . ? N1 C5 1.338(5) . ? N2 C26 1.338(6) . ? N2 C27 1.331(5) . ? N3 C83 1.344(6) . ? N3 C84 1.338(5) . ? N4 C72 1.341(5) . ? N4 C73 1.358(5) . ? N5 O3A 1.256(17) . ? C1 H1 0.9500 . ? C1 C2 1.375(5) . ? C2 H2 0.9500 . ? C2 C3 1.382(6) . ? C3 C4 1.396(6) . ? C3 C6 1.490(5) . ? C4 H4 0.9500 . ? C4 C5 1.362(5) . ? C5 H5 0.9500 . ? C6 C7 1.376(6) . ? C6 C11 1.420(6) . ? C7 H7 0.9500 . ? C7 C8 1.375(5) . ? C8 H8 0.9500 . ? C8 C9 1.380(6) . ? C9 C10 1.394(6) . ? C9 C12 1.506(5) . ? C10 H10 0.9500 . ? C10 C11 1.378(6) . ? C11 H11 0.9500 . ? C12 C13 1.390(7) . ? C12 C17 1.391(7) . ? C13 C14 1.399(6) . ? C13 C29 1.521(7) . ? C14 H14 0.9500 . ? C14 C15 1.395(7) . ? C15 C16 1.392(7) . ? C15 C18 1.501(6) . ? C16 C17 1.378(6) . ? C16 C61 1.536(7) . ? C17 H17 0.9500 . ? C18 C19 1.385(7) . ? C18 C23 1.390(7) . ? C19 H19 0.9500 . ? C19 C20 1.389(6) . ? C20 H20 0.9500 . ? C20 C21 1.403(6) . ? C21 C22 1.389(6) . ? C21 C24 1.492(5) . ? C22 H22 0.9500 . ? C22 C23 1.376(6) . ? C23 H23 0.9500 . ? C24 C25 1.388(6) . ? C24 C28 1.387(6) . ? C25 H25 0.9500 . ? C25 C26 1.378(6) . ? C26 H26 0.9500 . ? C27 H27 0.9500 . ? C27 C28 1.373(5) . ? C28 H28 0.9500 . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C29 C30 1.516(7) . ? C30 C31 1.391(6) . ? C30 C35 1.396(7) . ? C31 H31 0.9500 . ? C31 C32 1.375(6) . ? C32 C33 1.386(6) . ? C33 C34 1.421(6) . ? C33 C38 1.514(6) . ? C34 H34 0.9500 . ? C34 C35 1.361(7) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C38 C39 1.516(7) . ? C39 C40 1.387(6) . ? C39 C44 1.409(6) . ? C40 H40 0.9500 . ? C40 C41 1.373(6) . ? C41 C42 1.396(6) . ? C42 C43 1.378(6) . ? C42 C47 1.523(6) . ? C43 H43 0.9500 . ? C43 C44 1.373(7) . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C45A H45D 0.9800 . ? C45A H45E 0.9800 . ? C45A H45F 0.9800 . ? C46 H46A 0.9800 . ? C46 H46B 0.9800 . ? C46 H46C 0.9800 . ? C47 H47A 0.9900 . ? C47 H47B 0.9900 . ? C47 C48 1.503(6) . ? C48 C49 1.393(6) . ? C48 C63 1.416(6) . ? C49 H49 0.9500 . ? C49 C50 1.387(6) . ? C50 C51 1.408(6) . ? C50 C75 1.488(6) . ? C51 C52 1.508(6) . ? C51 C62 1.389(6) . ? C52 H52A 0.9900 . ? C52 H52B 0.9900 . ? C52 C53 1.511(7) . ? C53 C54 1.386(7) . ? C53 C58 1.388(7) . ? C54 H54 0.9500 . ? C54 C55 1.387(7) . ? C55 H55 0.9500 . ? C55 C56 1.403(7) . ? C56 C57 1.384(8) . ? C56 C61 1.518(7) . ? C57 H57 0.9500 . ? C57 C58 1.384(8) . ? C58 H58 0.9500 . ? C59 H59A 0.9798 . ? C59 H59B 0.9800 . ? C59 H59C 0.9806 . ? C59A H59D 0.9800 . ? C59A H59E 0.9800 . ? C59A H59F 0.9800 . ? C60 H60A 0.9800 . ? C60 H60B 0.9800 . ? C60 H60C 0.9800 . ? C60A H60D 0.9800 . ? C60A H60E 0.9800 . ? C60A H60F 0.9800 . ? C61 H61A 0.9900 . ? C61 H61B 0.9900 . ? C62 H62 0.9500 . ? C62 C63 1.388(6) . ? C63 C64 1.477(6) . ? C64 C65 1.394(6) . ? C64 C69 1.404(6) . ? C65 H65 0.9500 . ? C65 C66 1.389(6) . ? C66 H66 0.9500 . ? C66 C67 1.398(6) . ? C67 C68 1.388(6) . ? C67 C70 1.467(6) . ? C68 H68 0.9500 . ? C68 C69 1.381(6) . ? C69 H69 0.9500 . ? C70 C71 1.391(6) . ? C70 C74 1.380(6) . ? C71 H71 0.9500 . ? C71 C72 1.371(6) . ? C72 H72 0.9500 . ? C73 H73 0.9500 . ? C73 C74 1.392(6) . ? C74 H74 0.9500 . ? C75 C76 1.383(6) . ? C75 C80 1.419(6) . ? C76 H76 0.9500 . ? C76 C77 1.382(6) . ? C77 H77 0.9500 . ? C77 C78 1.392(6) . ? C78 C79 1.398(6) . ? C78 C81 1.479(6) . ? C79 H79 0.9500 . ? C79 C80 1.378(6) . ? C80 H80 0.9500 . ? C81 C82 1.390(6) . ? C81 C85 1.416(6) . ? C82 H82 0.9500 . ? C82 C83 1.386(6) . ? C83 H83 0.9500 . ? C84 H84 0.9500 . ? C84 C85 1.388(6) . ? C85 H85 0.9500 . ? O11 C88 1.230(8) . ? N7 C86 1.484(9) . ? N7 C88 1.337(8) . ? N7 C87 1.440(9) . ? C86 H86A 0.9800 . ? C86 H86B 0.9800 . ? C86 H86C 0.9800 . ? C88 H88 0.9500 . ? C87 H87A 0.9800 . ? C87 H87B 0.9800 . ? C87 H87C 0.9800 . ? O12 N6 1.232(10) . ? O13 N6 1.220(10) . ? O14 N6 1.165(10) . ? O14A N6A 1.220(13) . ? O12A N6A 1.227(13) . ? O13A N6A 1.250(13) . ? O13B N6B 1.237(16) . ? O14B N6B 1.230(17) . ? O12B N6B 1.228(16) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 O1 N5 O2 82.1(5) . . . . ? Co1 O1 N5 O3B -93(2) . . . . ? Co1 O1 N5 O3A -119(4) . . . . ? Co1 N1 C1 C2 177.6(4) . . . . ? Co1 N1 C5 C4 -177.5(4) . . . . ? Co1 N2 C26 C25 178.6(4) 1_556 . . . ? Co1 N2 C27 C28 -177.6(3) 1_556 . . . ? Co1 N3 C83 C82 -166.1(3) 2_765 . . . ? Co1 N3 C84 C85 167.4(3) 2_765 . . . ? Co1 N4 C72 C71 -166.1(3) 2_675 . . . ? Co1 N4 C73 C74 166.1(3) 2_675 . . . ? O6 C41 C42 C43 -177.0(4) . . . . ? O6 C41 C42 C47 3.4(6) . . . . ? O8 C32 C33 C34 -177.8(4) . . . . ? O8 C32 C33 C38 6.0(7) . . . . ? O9A C57 C58 C53 175.1(6) . . . . ? O10 C55 C56 C57 174.7(6) . . . . ? O10 C55 C56 C61 -3.2(8) . . . . ? O10A C54 C55 C56 -174.6(5) . . . . ? N1 C1 C2 C3 0.3(7) . . . . ? N2 C27 C28 C24 -1.9(7) . . . . ? N3 C84 C85 C81 -0.9(7) . . . . ? N4 C73 C74 C70 0.5(7) . . . . ? C1 N1 C5 C4 -0.3(7) . . . . ? C1 C2 C3 C4 -1.0(7) . . . . ? C1 C2 C3 C6 178.9(4) . . . . ? C2 C3 C4 C5 1.0(7) . . . . ? C2 C3 C6 C7 -28.8(7) . . . . ? C2 C3 C6 C11 153.3(5) . . . . ? C3 C4 C5 N1 -0.4(7) . . . . ? C3 C6 C7 C8 -176.8(4) . . . . ? C3 C6 C11 C10 176.7(5) . . . . ? C4 C3 C6 C7 151.1(5) . . . . ? C4 C3 C6 C11 -26.8(7) . . . . ? C5 N1 C1 C2 0.3(7) . . . . ? C6 C3 C4 C5 -178.9(4) . . . . ? C6 C7 C8 C9 0.5(7) . . . . ? C7 C6 C11 C10 -1.4(7) . . . . ? C7 C8 C9 C10 -2.0(7) . . . . ? C7 C8 C9 C12 177.3(4) . . . . ? C8 C9 C10 C11 1.7(8) . . . . ? C8 C9 C12 C13 -107.5(6) . . . . ? C8 C9 C12 C17 72.0(6) . . . . ? C9 C10 C11 C6 0.0(8) . . . . ? C9 C12 C13 C14 -177.3(4) . . . . ? C9 C12 C13 C29 7.9(8) . . . . ? C9 C12 C17 C16 179.2(5) . . . . ? C10 C9 C12 C13 71.8(7) . . . . ? C10 C9 C12 C17 -108.7(6) . . . . ? C11 C6 C7 C8 1.2(7) . . . . ? C12 C9 C10 C11 -177.6(5) . . . . ? C12 C13 C14 C15 -1.8(8) . . . . ? C12 C13 C29 C30 57.1(6) . . . . ? C13 C12 C17 C16 -1.4(8) . . . . ? C13 C14 C15 C16 -1.7(8) . . . . ? C13 C14 C15 C18 -178.1(5) . . . . ? C13 C29 C30 C31 -117.0(5) . . . . ? C13 C29 C30 C35 55.6(6) . . . . ? C14 C13 C29 C30 -117.6(5) . . . . ? C14 C15 C16 C17 3.6(8) . . . . ? C14 C15 C16 C61 -174.3(5) . . . . ? C14 C15 C18 C19 54.4(7) . . . . ? C14 C15 C18 C23 -125.4(6) . . . . ? C15 C16 C17 C12 -2.1(8) . . . . ? C15 C16 C61 C56 157.2(5) . . . . ? C15 C18 C19 C20 178.6(5) . . . . ? C15 C18 C23 C22 -179.9(5) . . . . ? C16 C15 C18 C19 -121.8(6) . . . . ? C16 C15 C18 C23 58.4(7) . . . . ? C17 C12 C13 C14 3.3(7) . . . . ? C17 C12 C13 C29 -171.5(5) . . . . ? C17 C16 C61 C56 -20.6(9) . . . . ? C18 C15 C16 C17 179.9(5) . . . . ? C18 C15 C16 C61 1.9(8) . . . . ? C18 C19 C20 C21 1.3(9) . . . . ? C19 C18 C23 C22 0.3(8) . . . . ? C19 C20 C21 C22 0.2(8) . . . . ? C19 C20 C21 C24 179.2(5) . . . . ? C20 C21 C22 C23 -1.5(8) . . . . ? C20 C21 C24 C25 168.1(5) . . . . ? C20 C21 C24 C28 -8.7(7) . . . . ? C21 C22 C23 C18 1.3(9) . . . . ? C21 C24 C25 C26 -178.6(5) . . . . ? C21 C24 C28 C27 179.5(4) . . . . ? C22 C21 C24 C25 -13.0(8) . . . . ? C22 C21 C24 C28 170.2(5) . . . . ? C23 C18 C19 C20 -1.6(8) . . . . ? C24 C21 C22 C23 179.5(5) . . . . ? C24 C25 C26 N2 0.1(9) . . . . ? C25 C24 C28 C27 2.5(7) . . . . ? C26 N2 C27 C28 0.4(7) . . . . ? C27 N2 C26 C25 0.5(7) . . . . ? C28 C24 C25 C26 -1.6(8) . . . . ? C29 C13 C14 C15 173.1(5) . . . . ? C29 C30 C31 C32 166.2(5) . . . . ? C29 C30 C35 O7 14.6(7) . . . . ? C29 C30 C35 C34 -165.4(5) . . . . ? C30 C31 C32 O8 -177.3(4) . . . . ? C30 C31 C32 C33 1.2(7) . . . . ? C31 C30 C35 O7 -172.4(4) . . . . ? C31 C30 C35 C34 7.5(7) . . . . ? C31 C32 C33 C34 3.6(7) . . . . ? C31 C32 C33 C38 -172.6(4) . . . . ? C32 C33 C34 C35 -2.8(7) . . . . ? C32 C33 C38 C39 76.1(6) . . . . ? C33 C34 C35 O7 177.1(4) . . . . ? C33 C34 C35 C30 -2.9(8) . . . . ? C33 C38 C39 C40 -107.4(5) . . . . ? C33 C38 C39 C44 69.6(6) . . . . ? C34 C33 C38 C39 -100.0(5) . . . . ? C35 C30 C31 C32 -6.7(7) . . . . ? C36 O8 C32 C31 -10.8(7) . . . . ? C36 O8 C32 C33 170.7(4) . . . . ? C37 O7 C35 C30 -151.3(5) . . . . ? C37 O7 C35 C34 28.7(8) . . . . ? C38 C33 C34 C35 173.5(5) . . . . ? C38 C39 C40 C41 177.4(4) . . . . ? C38 C39 C44 O5 4.8(7) . . . . ? C38 C39 C44 C43 -174.0(4) . . . . ? C39 C40 C41 O6 176.5(4) . . . . ? C39 C40 C41 C42 -3.3(7) . . . . ? C40 C39 C44 O5 -178.0(4) . . . . ? C40 C39 C44 C43 3.1(7) . . . . ? C40 C41 C42 C43 2.8(6) . . . . ? C40 C41 C42 C47 -176.7(4) . . . . ? C41 C42 C43 C44 0.6(7) . . . . ? C41 C42 C47 C48 161.2(4) . . . . ? C42 C43 C44 O5 177.6(4) . . . . ? C42 C43 C44 C39 -3.6(7) . . . . ? C42 C47 C48 C49 -84.6(5) . . . . ? C42 C47 C48 C63 85.5(5) . . . . ? C43 C42 C47 C48 -18.3(6) . . . . ? C44 C39 C40 C41 0.3(7) . . . . ? C45 O5 C44 C39 108.2(7) . . . . ? C45 O5 C44 C43 -72.9(7) . . . . ? C45A O5 C44 C39 -171.8(11) . . . . ? C45A O5 C44 C43 7.1(12) . . . . ? C46 O6 C41 C40 -2.2(6) . . . . ? C46 O6 C41 C42 177.6(4) . . . . ? C47 C42 C43 C44 -179.8(4) . . . . ? C47 C48 C49 C50 170.1(4) . . . . ? C47 C48 C63 C62 -170.7(4) . . . . ? C47 C48 C63 C64 2.4(6) . . . . ? C48 C49 C50 C51 0.7(7) . . . . ? C48 C49 C50 C75 -175.5(4) . . . . ? C48 C63 C64 C65 56.6(6) . . . . ? C48 C63 C64 C69 -117.9(5) . . . . ? C49 C48 C63 C62 -0.6(6) . . . . ? C49 C48 C63 C64 172.5(4) . . . . ? C49 C50 C51 C52 -172.9(4) . . . . ? C49 C50 C51 C62 0.4(6) . . . . ? C49 C50 C75 C76 -119.1(5) . . . . ? C49 C50 C75 C80 57.9(5) . . . . ? C50 C51 C52 C53 59.7(6) . . . . ? C50 C51 C62 C63 -1.7(7) . . . . ? C50 C75 C76 C77 179.0(4) . . . . ? C50 C75 C80 C79 -179.6(4) . . . . ? C51 C50 C75 C76 64.8(6) . . . . ? C51 C50 C75 C80 -118.2(5) . . . . ? C51 C52 C53 C54 -124.0(5) . . . . ? C51 C52 C53 C58 53.0(6) . . . . ? C51 C62 C63 C48 1.8(7) . . . . ? C51 C62 C63 C64 -171.1(4) . . . . ? C52 C51 C62 C63 171.7(4) . . . . ? C52 C53 C54 O10A -10.7(7) . . . . ? C52 C53 C54 C55 174.5(4) . . . . ? C52 C53 C58 O9 16.9(9) . . . . ? C52 C53 C58 C57 -173.8(5) . . . . ? C53 C54 C55 O10 -173.1(6) . . . . ? C53 C54 C55 C56 0.2(7) . . . . ? C54 C53 C58 O9 -165.9(7) . . . . ? C54 C53 C58 C57 3.4(8) . . . . ? C54 C55 C56 C57 1.5(7) . . . . ? C54 C55 C56 C61 -176.4(5) . . . . ? C55 C56 C57 O9A -177.7(6) . . . . ? C55 C56 C57 C58 -0.8(8) . . . . ? C55 C56 C61 C16 116.9(6) . . . . ? C56 C57 C58 O9 167.2(8) . . . . ? C56 C57 C58 C53 -1.7(9) . . . . ? C57 C56 C61 C16 -60.9(8) . . . . ? C58 C53 C54 O10A 172.2(5) . . . . ? C58 C53 C54 C55 -2.6(7) . . . . ? C59 O9 C58 C53 118.2(18) . . . . ? C59 O9 C58 C57 -51(2) . . . . ? C59A O9A C57 C56 162.8(10) . . . . ? C59A O9A C57 C58 -14.1(13) . . . . ? C60 O10 C55 C54 -14.6(14) . . . . ? C60 O10 C55 C56 172.1(10) . . . . ? C60A O10A C54 C53 177.2(8) . . . . ? C60A O10A C54 C55 -7.9(11) . . . . ? C61 C16 C17 C12 175.8(5) . . . . ? C61 C56 C57 O9A 0.2(9) . . . . ? C61 C56 C57 C58 177.0(5) . . . . ? C62 C51 C52 C53 -113.4(5) . . . . ? C62 C63 C64 C65 -130.5(5) . . . . ? C62 C63 C64 C69 55.0(6) . . . . ? C63 C48 C49 C50 -0.6(6) . . . . ? C63 C64 C65 C66 -170.7(4) . . . . ? C63 C64 C69 C68 170.7(4) . . . . ? C64 C65 C66 C67 -0.1(7) . . . . ? C65 C64 C69 C68 -4.1(7) . . . . ? C65 C66 C67 C68 -3.6(7) . . . . ? C65 C66 C67 C70 176.5(4) . . . . ? C66 C67 C68 C69 3.4(7) . . . . ? C66 C67 C70 C71 32.9(6) . . . . ? C66 C67 C70 C74 -147.9(4) . . . . ? C67 C68 C69 C64 0.4(7) . . . . ? C67 C70 C71 C72 178.2(4) . . . . ? C67 C70 C74 C73 -177.9(4) . . . . ? C68 C67 C70 C71 -147.0(4) . . . . ? C68 C67 C70 C74 32.1(7) . . . . ? C69 C64 C65 C66 3.9(7) . . . . ? C70 C67 C68 C69 -176.7(4) . . . . ? C70 C71 C72 N4 -1.0(6) . . . . ? C71 C70 C74 C73 1.3(6) . . . . ? C72 N4 C73 C74 -2.5(6) . . . . ? C73 N4 C72 C71 2.8(6) . . . . ? C74 C70 C71 C72 -1.0(6) . . . . ? C75 C50 C51 C52 3.1(7) . . . . ? C75 C50 C51 C62 176.5(4) . . . . ? C75 C76 C77 C78 -1.0(7) . . . . ? C76 C75 C80 C79 -2.5(6) . . . . ? C76 C77 C78 C79 0.2(7) . . . . ? C76 C77 C78 C81 179.2(4) . . . . ? C77 C78 C79 C80 -0.6(6) . . . . ? C77 C78 C81 C82 -32.1(6) . . . . ? C77 C78 C81 C85 146.5(4) . . . . ? C78 C79 C80 C75 1.8(6) . . . . ? C78 C81 C82 C83 178.5(4) . . . . ? C78 C81 C85 C84 -177.0(4) . . . . ? C79 C78 C81 C82 146.9(4) . . . . ? C79 C78 C81 C85 -34.5(6) . . . . ? C80 C75 C76 C77 2.1(7) . . . . ? C81 C78 C79 C80 -179.6(4) . . . . ? C81 C82 C83 N3 -2.4(7) . . . . ? C82 C81 C85 C84 1.7(6) . . . . ? C83 N3 C84 C85 -1.5(6) . . . . ? C84 N3 C83 C82 3.2(6) . . . . ? C85 C81 C82 C83 -0.1(6) . . . . ? C86 N7 C88 O11 -176.9(8) . . . . ? C87 N7 C88 O11 1.7(11) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.850 -0.805 0.500 2201.7 345.1 '8 DMF,2 H2O' 2 0.500 0.000 1.000 42.1 2.7 ?