#------------------------------------------------------------------------------ #$Date: 2024-07-09 01:18:42 +0300 (Tue, 09 Jul 2024) $ #$Revision: 293306 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/20/1572099.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572099 loop_ _publ_author_name 'Chen, Zhao-Nian' 'Zhang, Le-Ping' 'Wu, Huai-Li' 'Qi, Qiao-Yan' 'Yan, Meng' 'Tian, Jia' 'Yang, Guanyu' 'Li, Zhan-Ting' 'Yang, Bo' _publ_section_title ; Accurate Construction of Monolayer, Bilayer, Sandwich Bilayer, Four-layer, Multi-layer and Chiral Bilayer 2D Pillararene-Type Supramolecular Networks ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC03022B _journal_year 2024 _chemical_formula_moiety 'C110 H112 Cu2 N4 O18, 4.25(H2 O), 6[H2O], 3[H2O]' _chemical_formula_sum 'C110 H138.5 Cu2 N4 O31.25' _chemical_formula_weight 2143.82 _space_group_crystal_system orthorhombic _space_group_IT_number 48 _space_group_name_Hall '-P 2ab 2bc' _space_group_name_H-M_alt 'P n n n :2' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2024-06-18 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-06-25 deposited with the CCDC. 2024-07-04 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.8537(8) _cell_length_b 22.6927(15) _cell_length_c 41.561(3) _cell_measurement_reflns_used 9922 _cell_measurement_temperature 193.00 _cell_measurement_theta_max 43.21 _cell_measurement_theta_min 2.93 _cell_volume 13065.9(15) _computing_cell_refinement 'SAINT V8.40B (Bruker, 2019)' _computing_data_collection 'APEX5 V2023.9-2 (Bruker, 2023)' _computing_data_reduction 'SAINT V8.40B (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 193.00 _diffrn_detector CPAD _diffrn_detector_area_resol_mean 7.41 _diffrn_detector_type 'Bruker PHOTON II' _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE MetalJet PHOTON II' _diffrn_measurement_method '\w and \f shutterless scans' _diffrn_measurement_specimen_support 'nylon loop' _diffrn_radiation_monochromator 'Helios Multi-layer Optic' _diffrn_radiation_probe x-ray _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0836 _diffrn_reflns_av_unetI/netI 0.0677 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 46 _diffrn_reflns_limit_l_min -50 _diffrn_reflns_number 96701 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 53.898 _diffrn_reflns_theta_min 2.925 _diffrn_source MetalJet _diffrn_source_current 2.86 _diffrn_source_power 0.19937059999999998 _diffrn_source_type 'Liquid Metal source' _diffrn_source_voltage 69.71 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.111 _exptl_absorpt_correction_T_max 0.7512 _exptl_absorpt_correction_T_min 0.5696 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1391 before and 0.0656 after correction. The Ratio of minimum to maximum transmission is 0.7583. The \l/2 correction factor is Not present. ; _exptl_crystal_colour blue _exptl_crystal_colour_primary blue _exptl_crystal_density_diffrn 1.090 _exptl_crystal_description block _exptl_crystal_F_000 4538 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.11 _refine_diff_density_max 1.482 _refine_diff_density_min -1.224 _refine_diff_density_rms 0.098 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.023 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 728 _refine_ls_number_reflns 11951 _refine_ls_number_restraints 223 _refine_ls_restrained_S_all 1.049 _refine_ls_R_factor_all 0.2090 _refine_ls_R_factor_gt 0.1380 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0700P)^2^+100.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3019 _refine_ls_wR_factor_ref 0.3428 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6242 _reflns_number_total 11951 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03022b2.cif _cod_data_source_block 230917lu_lgpz145541_0m _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_radiation_probe' value 'X-ray' was changed to 'x-ray' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas ; _cod_original_cell_volume 13066.0(14) _cod_original_sg_symbol_H-M 'P n n n' _cod_original_formula_sum 'C110 H138.50 Cu2 N4 O31.25' _cod_database_code 1572099 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.801 _shelx_estimated_absorpt_t_min 0.742 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H,H) groups 2. Restrained distances O7-C55 = O8-C55 1.25 with sigma of 0.005 O5-C53 = O6-C53 1.25 with sigma of 0.01 C52-C53 1.5 with sigma of 0.01 C54-C55 1.5 with sigma of 0.01 O6-C53 = O6A-C53A = O5A-C53A = O5-C53 1.25 with sigma of 0.01 C53A-C52A = C53-C52 1.5 with sigma of 0.01 O5-O6 2.2 with sigma of 0.01 O7-O8 2.2 with sigma of 0.01 O6A-O5A = O5-O6 2.2 with sigma of 0.01 Cu1-O6 \\sim Cu1-O5 with sigma of 0.002 O8-C54 \\sim O7-C54 with sigma of 0.02 Cu1-O6 \\sim Cu1-O5 \\sim Cu1-O6A \\sim Cu1-O5A with sigma of 0.02 Cu1-O9A \\sim Cu1-O9B with sigma of 0.02 O6A-C52A \\sim O5A-C52A with sigma of 0.02 Cu1-H9AA \\sim Cu1-H9AB with sigma of 0.02 Cu1-H9BA \\sim Cu1-H9BB with sigma of 0.02 O6-C52 \\sim O5-C52 with sigma of 0.02 3. Restrained planarity O5, O6, C52, C53 with sigma of 0.1 O7, O8, C54, C55 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints O5 \\sim O6 \\sim C52 \\sim C53: within 2A with sigma of 0.002 and sigma for terminal atoms of 0.004 within 2A N1 \\sim C1 \\sim C2 \\sim C3 \\sim C4 \\sim C5: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A O8 \\sim C55 \\sim O7 \\sim C54: within 2A with sigma of 0.002 and sigma for terminal atoms of 0.004 within 2A O6 \\sim O5 \\sim C52 \\sim C53 \\sim Cu1 \\sim O7 \\sim O8 \\sim C55 \\sim C54 \\sim O9B: within 2A with sigma of 0.002 and sigma for terminal atoms of 0.004 within 2A O9A \\sim O9B: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A O5 \\sim O6 \\sim C52 \\sim C53 \\sim O6A \\sim C52A \\sim C53A \\sim O5A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A Uanis(O16) \\sim Ueq, Uanis(O18) \\sim Ueq, Uanis(O17) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O11) \\sim Ueq, Uanis(O10) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O15) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O14) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 5. Others Sof(O9B)=Sof(H9BA)=Sof(H9BB)=1-FVAR(1) Sof(O9A)=Sof(H9AA)=Sof(H9AB)=FVAR(1) Sof(O6A)=Sof(C52A)=Sof(H52D)=Sof(H52E)=Sof(H52F)=Sof(C53A)=Sof(O5A)=1-FVAR(2) Sof(O5)=Sof(O6)=Sof(C52)=Sof(H52A)=Sof(H52B)=Sof(H52C)=Sof(C53)=FVAR(2) Fixed Sof: O10(0.25) H10A(0.25) H10B(0.25) O11(0.25) H11A(0.25) H11B(0.25) O14(0.5) H14A(0.5) H14B(0.5) O15(0.25) H15A(0.25) H15B(0.25) O16(0.125) H16A(0.125) H16B(0.125) O17(0.25) H17A(0.25) H17B(0.25) O18(0.25) H18C(0.25) H18D(0.25) O12(0.25) H12A(0.25) H12B(0.25) 6.a Riding coordinates: O9B(H9BA,H9BB), C52(H52A,H52B,H52C), O10(H10A,H10B), O11(H11A,H11B), O14(H14A, H14B), O15(H15A,H15B), O16(H16A,H16B), O17(H17A,H17B), O18(H18C,H18D), O12(H12A,H12B) 6.b Free rotating group: O9A(H9AA,H9AB) 6.c Secondary CH2 refined with riding coordinates: C18(H18A,H18B), C25(H25A,H25B), C27(H27A,H27B), C29(H29A,H29B), C34(H34A, H34B), C37(H37A,H37B), C39(H39A,H39B) 6.d Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C4(H4), C5(H5), C7(H7), C8(H8), C10(H10), C11(H11), C14(H14), C17(H17), C21(H21), C24(H24), C31(H31), C35(H35), C42(H42), C43(H43), C45(H45), C46(H46), C47(H47), C48(H48), C50(H50), C51(H51) 6.e Idealised Me refined as rotating group: C26(H26A,H26B,H26C), C28(H28A,H28B,H28C), C38(H38A,H38B,H38C), C40(H40A,H40B, H40C), C54(H54A,H54B,H54C), C52A(H52D,H52E,H52F) ; _smtbx_masks_special_details ; A solvent mask was calculated and 362 electrons were found in a volume of 2594\%A^3^ in 3 voids per unit cell. This is consistent with the presence of 6[H2O], 3[H2O] per formula unit which account for 360 electrons per unit cell. ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL 230917lu_lgpz145541_0m_a.res in Pnnn 230917lu_lgpz145541_0m.res created by SHELXL-2019/3 at 22:10:20 on 18-Jun-2024 REM Old TITL 230917LU_LGPZ145541_0m in Pnnn REM SHELXT solution in Pnnn: R1 0.478, Rweak 0.076, Alpha 0.083 REM 0.578 for 1020 systematic absences, Orientation as input REM Formula found by SHELXT: C49 N7 O6 Cl CELL 1.34139 13.8537 22.6927 41.5614 90 90 90 ZERR 4 0.0008 0.0015 0.0026 0 0 0 LATT 1 SYMM 0.5-X,0.5-Y,+Z SYMM 0.5-X,+Y,0.5-Z SYMM +X,0.5-Y,0.5-Z SFAC C H Cu N O DISP C 0.0137 0.0067 57.1 DISP Cu -2.7974 3.6876 28058.5 DISP H 0 0 0.6 DISP N 0.0241 0.0134 109.9 DISP O 0.0389 0.0241 193.4 UNIT 440 554 8 16 125 DFIX 1.25 0.005 O7 C55 O8 C55 DANG 2.2 0.01 O5 O6 DFIX 1.25 0.01 O5 C53 O6 C53 FLAT O5 O6 C52 C53 ISOR 0.01 0.02 O16 O18 O17 SIMU 0.002 0.004 2 O5 O6 C52 C53 SADI 0.002 Cu1 O6 Cu1 O5 DANG 2.2 0.01 O7 O8 DFIX 1.5 0.01 C52 C53 DFIX 1.5 0.01 C54 C55 SADI O8 C54 O7 C54 FLAT O7 O8 C54 C55 SIMU 0.01 0.02 2 N1 C1 > C5 SIMU 0.002 0.004 2 O8 C55 O7 C54 ISOR 0.01 0.02 O11 O10 ISOR 0.01 0.02 O15 ISOR 0.01 0.02 O14 SIMU 0.002 0.004 2 O6 O5 C52 C53 Cu1 O7 O8 C55 C54 O9B SADI Cu1 O6 Cu1 O5 Cu1 O6A Cu1 O5A DFIX 1.25 0.01 O6 C53 O6A C53A O5A C53A O5 C53 DANG 2.2 0.01 O6A O5A O5 O6 SADI Cu1 O9A Cu1 O9B DFIX 1.5 0.01 C53A C52A C53 C52 SIMU 0.01 0.02 2 O9A O9B SIMU 0.01 0.02 2 O5 O6 C52 C53 O6A C52A C53A O5A SADI O6A C52A O5A C52A SADI Cu1 H9Aa Cu1 H9Ab SADI Cu1 H9Ba Cu1 H9Bb SADI O6 C52 O5 C52 L.S. 20 0 1124 PLAN 32 SIZE 0.11 0.12 0.15 TEMP -80.15 CONF list 4 MORE -1 BOND $H ABIN fmap 2 acta SHEL 999 0.83 OMIT 0 0 6 OMIT 0 1 1 OMIT 0 1 5 OMIT 0 1 7 OMIT 0 1 9 OMIT 0 3 7 OMIT 0 4 0 OMIT 0 6 4 OMIT 1 1 0 OMIT 1 2 5 OMIT 1 2 11 OMIT 1 3 2 OMIT 1 3 7 OMIT 1 4 1 OMIT 1 5 4 OMIT 1 6 1 OMIT 2 0 2 OMIT 2 1 4 OMIT 2 1 9 OMIT 3 2 2 OMIT 3 2 5 REM REM REM WGHT 0.070000 100.000000 FVAR 0.23327 0.71113 0.09259 CU1 3 0.485129 0.519091 0.234275 11.00000 0.31280 0.12520 = 0.06415 -0.05106 0.06996 -0.02394 O1 5 0.617063 0.534145 0.424188 11.00000 0.06006 0.06126 = 0.06841 -0.00455 0.01594 0.01929 O2 5 0.454567 0.615972 0.537064 11.00000 0.05862 0.05039 = 0.04121 -0.00103 -0.00678 0.00709 O3 5 0.709596 0.972000 0.538942 11.00000 0.04051 0.06431 = 0.06559 -0.01905 -0.00929 -0.00567 O4 5 0.504951 0.916578 0.429206 11.00000 0.05775 0.05861 = 0.04731 0.00087 -0.00216 -0.01084 PART -1 O5 5 0.582699 0.455527 0.257148 31.00000 0.46250 0.29422 = 0.16131 -0.06756 0.07674 0.11351 O6 5 0.639596 0.539098 0.238161 31.00000 0.46266 0.29447 = 0.16136 -0.06762 0.07693 0.11374 PART 0 O7 5 0.509703 0.586642 0.213229 11.00000 0.32208 0.14252 = 0.09360 -0.04423 0.06614 -0.02336 O8 5 0.357367 0.596539 0.204653 11.00000 0.33328 0.18146 = 0.13274 -0.03044 0.05935 -0.03586 PART 1 O9B 5 0.348563 0.456492 0.243265 -21.00000 0.15882 0.26880 = 0.07205 -0.03610 0.02167 0.01416 AFIX 3 H9BA 2 0.310713 0.461971 0.259655 -21.00000 -1.50000 H9BB 2 0.355953 0.418471 0.242215 -21.00000 -1.50000 AFIX 0 PART 0 N1 4 0.464069 0.564974 0.275469 11.00000 0.20675 0.12196 = 0.07198 -0.04778 0.05987 -0.03316 N2 4 0.482974 0.973437 0.694070 11.00000 0.20539 0.10819 = 0.06559 -0.04589 -0.04761 0.03192 C1 1 0.516785 0.611074 0.281532 11.00000 0.19802 0.14030 = 0.07794 -0.04198 0.06172 -0.03571 AFIX 43 H1 2 0.565513 0.622944 0.266813 11.00000 -1.20000 AFIX 0 C2 1 0.501381 0.643136 0.309862 11.00000 0.17710 0.12370 = 0.06878 -0.05057 0.05653 -0.03464 AFIX 43 H2 2 0.543730 0.674842 0.314711 11.00000 -1.20000 AFIX 0 C3 1 0.430848 0.631298 0.330066 11.00000 0.15551 0.08453 = 0.04508 -0.03330 0.03799 -0.01532 C4 1 0.385930 0.579022 0.324360 11.00000 0.18943 0.12490 = 0.07668 -0.05658 0.05198 -0.04059 AFIX 43 H4 2 0.342229 0.563905 0.339921 11.00000 -1.20000 AFIX 0 C5 1 0.402241 0.547501 0.296598 11.00000 0.20841 0.12974 = 0.09092 -0.05985 0.05916 -0.04716 AFIX 43 H5 2 0.367222 0.512141 0.292929 11.00000 -1.20000 AFIX 0 C6 1 0.413787 0.664178 0.360558 11.00000 0.07840 0.05279 = 0.03452 -0.00751 0.00413 0.00970 C7 1 0.487012 0.699929 0.372947 11.00000 0.08715 0.05610 = 0.04264 -0.00409 0.02921 0.00051 AFIX 43 H7 2 0.544538 0.706322 0.361005 11.00000 -1.20000 AFIX 0 C8 1 0.474593 0.726511 0.403461 11.00000 0.06364 0.04508 = 0.04130 -0.00989 0.01752 -0.00279 AFIX 43 H8 2 0.523959 0.751116 0.411899 11.00000 -1.20000 AFIX 0 C9 1 0.390728 0.717026 0.421306 11.00000 0.04539 0.03856 = 0.02878 -0.00714 0.00424 0.00723 C10 1 0.319005 0.684439 0.407678 11.00000 0.05201 0.04423 = 0.03403 -0.00801 -0.00040 0.00550 AFIX 43 H10 2 0.259721 0.680049 0.418913 11.00000 -1.20000 AFIX 0 C11 1 0.329708 0.657228 0.377702 11.00000 0.06107 0.05864 = 0.03612 -0.01169 -0.00089 0.00655 AFIX 43 H11 2 0.278816 0.633914 0.369177 11.00000 -1.20000 AFIX 0 C12 1 0.384902 0.743404 0.454109 11.00000 0.03051 0.03341 = 0.03473 -0.00742 0.00207 0.00052 C13 1 0.369807 0.709494 0.481660 11.00000 0.03269 0.02941 = 0.03327 -0.00281 0.00070 0.00114 C14 1 0.373335 0.737412 0.511510 11.00000 0.03500 0.03695 = 0.03069 -0.00196 0.00099 0.00129 AFIX 43 H14 2 0.366408 0.714232 0.530404 11.00000 -1.20000 AFIX 0 C15 1 0.386768 0.798646 0.514756 11.00000 0.03685 0.03446 = 0.02958 -0.00512 -0.00400 0.00277 C16 1 0.397312 0.832288 0.486853 11.00000 0.03068 0.02874 = 0.04321 -0.00485 -0.00324 0.00184 C17 1 0.396851 0.804078 0.457189 11.00000 0.03624 0.03252 = 0.03332 -0.00286 0.00234 -0.00098 AFIX 43 H17 2 0.405000 0.827058 0.438277 11.00000 -1.20000 AFIX 0 C18 1 0.409346 0.899326 0.487605 11.00000 0.03878 0.03038 = 0.04529 -0.00484 -0.00371 -0.00128 AFIX 23 H18A 2 0.373146 0.916510 0.469336 11.00000 -1.20000 H18B 2 0.380225 0.914592 0.507698 11.00000 -1.20000 AFIX 0 C19 1 0.512970 0.919973 0.485788 11.00000 0.03499 0.02823 = 0.04923 -0.00511 0.00194 -0.00104 C20 1 0.557801 0.930494 0.456360 11.00000 0.04027 0.03338 = 0.04871 -0.00210 -0.00395 -0.00176 C21 1 0.649176 0.955345 0.455085 11.00000 0.04423 0.03628 = 0.05470 -0.00146 0.00719 0.00144 AFIX 43 H21 2 0.678264 0.962782 0.434788 11.00000 -1.20000 AFIX 0 C22 1 0.698040 0.969310 0.482702 11.00000 0.03717 0.02957 = 0.06949 -0.00816 0.00097 0.00074 C23 1 0.655310 0.956662 0.512355 11.00000 0.03843 0.03304 = 0.06605 -0.01204 -0.00572 0.00513 C24 1 0.564191 0.932948 0.513674 11.00000 0.04096 0.03423 = 0.04804 -0.00767 -0.00561 -0.00140 AFIX 43 H24 2 0.535614 0.925262 0.534024 11.00000 -1.20000 AFIX 0 C25 1 0.668550 0.965563 0.569738 11.00000 0.04941 0.07034 = 0.06942 -0.01876 -0.01243 -0.00195 AFIX 23 H25A 2 0.657799 0.923436 0.574786 11.00000 -1.20000 H25B 2 0.606073 0.986601 0.571062 11.00000 -1.20000 AFIX 0 C26 1 0.740847 0.992139 0.592543 11.00000 0.06908 0.15316 = 0.08391 -0.05124 -0.01791 -0.01986 AFIX 137 H26A 2 0.760710 1.030919 0.584555 11.00000 -1.50000 H26B 2 0.797413 0.966356 0.594057 11.00000 -1.50000 H26C 2 0.711492 0.996446 0.613868 11.00000 -1.50000 AFIX 0 C27 1 0.546743 0.927439 0.398730 11.00000 0.07688 0.08676 = 0.04559 -0.00088 0.01400 -0.00509 AFIX 23 H27A 2 0.609261 0.906643 0.396681 11.00000 -1.20000 H27B 2 0.557687 0.970161 0.395571 11.00000 -1.20000 AFIX 0 C28 1 0.474801 0.904239 0.374339 11.00000 0.12034 0.14369 = 0.04389 0.00621 0.00308 -0.01629 AFIX 137 H28A 2 0.503464 0.905637 0.352795 11.00000 -1.50000 H28B 2 0.416452 0.928641 0.374787 11.00000 -1.50000 H28C 2 0.457979 0.863443 0.379666 11.00000 -1.50000 AFIX 0 C29 1 0.356274 0.642969 0.480867 11.00000 0.03444 0.03233 = 0.03717 -0.00507 0.00374 0.00013 AFIX 23 H29A 2 0.317853 0.630946 0.499849 11.00000 -1.20000 H29B 2 0.318929 0.632402 0.461395 11.00000 -1.20000 AFIX 0 C30 1 0.450301 0.608692 0.480773 11.00000 0.03575 0.03000 = 0.04350 -0.00090 0.00194 0.00472 C31 1 0.489670 0.588468 0.451912 11.00000 0.04025 0.03399 = 0.04837 -0.00171 0.00121 0.00040 AFIX 43 H31 2 0.458663 0.597215 0.432092 11.00000 -1.20000 AFIX 0 C32 1 0.574679 0.555359 0.452161 11.00000 0.04142 0.03736 = 0.06267 -0.00461 0.01309 0.00328 C33 1 0.618227 0.539813 0.480658 11.00000 0.02857 0.02714 = 0.07700 0.00381 -0.00202 0.00107 C34 1 0.704246 0.499366 0.480967 11.00000 0.03397 0.03208 = 0.08824 0.00394 -0.00254 0.00193 AFIX 23 H34A 2 0.702713 0.474849 0.461271 11.00000 -1.20000 H34B 2 0.698568 0.472549 0.499660 11.00000 -1.20000 AFIX 0 C35 1 0.580447 0.559529 0.508975 11.00000 0.04088 0.03073 = 0.06253 -0.00098 -0.00525 0.00017 AFIX 43 H35 2 0.610671 0.549187 0.528701 11.00000 -1.20000 AFIX 0 C36 1 0.497104 0.595058 0.509296 11.00000 0.04040 0.03419 = 0.04951 0.00003 -0.00233 -0.00335 C37 1 0.501059 0.603231 0.566621 11.00000 0.06137 0.08084 = 0.04479 0.00055 -0.01048 0.00559 AFIX 23 H37A 2 0.568738 0.617211 0.566152 11.00000 -1.20000 H37B 2 0.501081 0.560234 0.570654 11.00000 -1.20000 AFIX 0 C38 1 0.445737 0.634510 0.592257 11.00000 0.08807 0.12848 = 0.05093 -0.00312 -0.00818 0.01365 AFIX 137 H38A 2 0.435997 0.675694 0.585948 11.00000 -1.50000 H38B 2 0.481954 0.633005 0.612495 11.00000 -1.50000 H38C 2 0.382925 0.615373 0.595164 11.00000 -1.50000 AFIX 0 C39 1 0.576642 0.550715 0.394019 11.00000 0.09208 0.08010 = 0.06388 0.00344 0.02287 0.04001 AFIX 23 H39A 2 0.574818 0.594163 0.391955 11.00000 -1.20000 H39B 2 0.510049 0.535341 0.391966 11.00000 -1.20000 AFIX 0 C40 1 0.641599 0.524041 0.368221 11.00000 0.15449 0.12362 = 0.07464 0.00578 0.04785 0.07003 AFIX 137 H40A 2 0.619551 0.536829 0.346931 11.00000 -1.50000 H40B 2 0.638787 0.480957 0.369534 11.00000 -1.50000 H40C 2 0.708200 0.537198 0.371618 11.00000 -1.50000 AFIX 0 C41 1 0.395876 0.823949 0.547525 11.00000 0.04930 0.03282 = 0.03638 -0.00809 -0.01234 0.00538 C42 1 0.473929 0.808801 0.566595 11.00000 0.06890 0.05327 = 0.04268 -0.01381 -0.02272 0.01403 AFIX 43 H42 2 0.517811 0.779590 0.559237 11.00000 -1.20000 AFIX 0 C43 1 0.489470 0.835276 0.596154 11.00000 0.08303 0.06545 = 0.05229 -0.01352 -0.03337 0.01182 AFIX 43 H43 2 0.544177 0.824731 0.608676 11.00000 -1.20000 AFIX 0 C44 1 0.424233 0.877740 0.607594 11.00000 0.08757 0.05637 = 0.03780 -0.01771 -0.02231 0.01130 C45 1 0.346713 0.891460 0.588963 11.00000 0.07316 0.05510 = 0.04045 -0.01493 -0.00903 0.01247 AFIX 43 H45 2 0.302717 0.920544 0.596395 11.00000 -1.20000 AFIX 0 C46 1 0.329419 0.864679 0.559577 11.00000 0.05357 0.05043 = 0.03569 -0.01116 -0.01103 0.00999 AFIX 43 H46 2 0.272812 0.873929 0.547706 11.00000 -1.20000 AFIX 0 C47 1 0.558728 0.952250 0.676159 11.00000 0.16837 0.13269 = 0.07249 -0.03656 -0.04645 -0.01521 AFIX 43 H47 2 0.623154 0.960032 0.682735 11.00000 -1.20000 AFIX 0 C48 1 0.541741 0.919538 0.648509 11.00000 0.12341 0.12110 = 0.07335 -0.03428 -0.03705 0.00147 AFIX 43 H48 2 0.594120 0.903689 0.636561 11.00000 -1.20000 AFIX 0 C49 1 0.444563 0.909972 0.638220 11.00000 0.11100 0.07685 = 0.04287 -0.01515 -0.02946 0.00694 C50 1 0.376054 0.936845 0.655514 11.00000 0.11861 0.10537 = 0.05346 -0.03624 -0.01672 0.01390 AFIX 43 H50 2 0.310979 0.934394 0.648431 11.00000 -1.20000 AFIX 0 C51 1 0.395895 0.967594 0.682887 11.00000 0.13774 0.12663 = 0.07624 -0.05390 -0.02355 0.02319 AFIX 43 H51 2 0.344059 0.985455 0.694237 11.00000 -1.20000 AFIX 0 PART -1 C52 1 0.744978 0.456995 0.239513 31.00000 0.46280 0.29452 = 0.16159 -0.06748 0.07682 0.11378 AFIX 3 H52A 2 0.741528 0.415805 0.246483 31.00000 -1.50000 H52B 2 0.791178 0.478355 0.253043 31.00000 -1.50000 H52C 2 0.766098 0.458655 0.217033 31.00000 -1.50000 AFIX 0 C53 1 0.649185 0.485899 0.245347 31.00000 0.46262 0.29442 = 0.16141 -0.06756 0.07684 0.11369 PART 0 C54 1 0.456455 0.682639 0.194574 11.00000 0.33940 0.16068 = 0.12294 -0.03341 0.05727 -0.02503 AFIX 137 H54A 2 0.475707 0.706188 0.213268 11.00000 -1.50000 H54B 2 0.396598 0.698593 0.185517 11.00000 -1.50000 H54C 2 0.507532 0.684068 0.178279 11.00000 -1.50000 AFIX 0 C55 1 0.440191 0.619066 0.204912 11.00000 0.32712 0.15268 = 0.10629 -0.03868 0.06296 -0.02620 PART 1 O10 5 0.736321 0.699158 0.551279 10.25000 0.10008 0.05684 = 0.14371 0.05259 -0.05118 -0.01234 AFIX 3 H10A 2 0.775901 0.714868 0.537449 10.25000 -1.50000 H10B 2 0.769411 0.696958 0.569019 10.25000 -1.50000 AFIX 0 O11 5 0.761030 0.694565 0.417612 10.25000 0.08788 0.02361 = 0.16075 0.00547 0.00062 0.01294 AFIX 3 H11A 2 0.755360 0.732724 0.417612 10.25000 -1.50000 H11B 2 0.725530 0.682934 0.433662 10.25000 -1.50000 AFIX 0 PART 2 O14 5 0.692314 0.743556 0.444022 10.50000 0.11343 0.25599 = 0.17023 -0.00190 -0.03292 -0.01429 AFIX 3 H14A 2 0.649224 0.734506 0.458502 10.50000 -1.50000 H14B 2 0.718844 0.710956 0.437302 10.50000 -1.50000 AFIX 0 O15 5 0.696837 0.743889 0.530966 10.25000 0.03583 0.11560 = 0.09494 -0.01185 0.01426 0.00314 AFIX 3 H15A 2 0.675327 0.747769 0.511276 10.25000 -1.50000 H15B 2 0.724797 0.776748 0.535986 10.25000 -1.50000 AFIX 0 O16 5 0.250000 0.750000 0.633006 10.12500 0.11814 0.11342 = 0.17646 0.00000 0.00000 -0.01946 AFIX 3 H16A 2 0.303410 0.733680 0.626536 10.12500 -1.50000 H16B 2 0.250000 0.750000 0.653966 10.12500 -1.50000 AFIX 0 PART 3 O17 5 0.625797 0.725507 0.473690 10.25000 0.10310 0.16147 = 0.12007 -0.01741 0.00560 -0.00370 AFIX 3 H17A 2 0.646727 0.730337 0.493270 10.25000 -1.50000 H17B 2 0.675707 0.732797 0.461630 10.25000 -1.50000 AFIX 0 PART 1 O18 5 0.615313 0.745684 0.501041 10.25000 0.12584 0.18146 = 0.13484 -0.03622 -0.01054 0.02101 AFIX 3 H18C 2 0.639683 0.745234 0.481791 10.25000 -1.50000 H18D 2 0.665153 0.748774 0.513701 10.25000 -1.50000 AFIX 0 PART 0 O12 5 0.728211 0.657775 0.624645 10.25000 0.18498 0.11542 = 0.11900 0.04777 -0.08926 -0.05389 AFIX 3 H12A 2 0.735381 0.680665 0.641255 10.25000 -1.50000 H12B 2 0.716961 0.621944 0.631085 10.25000 -1.50000 AFIX 6 PART 2 O9A 5 0.313953 0.511796 0.226600 21.00000 0.13822 0.27643 = 0.10442 -0.03591 -0.01235 0.04507 H9AA 2 0.299904 0.540085 0.239930 21.00000 -1.50000 H9AB 2 0.314372 0.528607 0.207780 21.00000 -1.50000 AFIX 0 O6A 5 0.625248 0.493045 0.257193 -31.00000 0.46417 0.29833 = 0.16343 -0.06733 0.07650 0.11666 C52A 1 0.630207 0.410804 0.292507 -31.00000 0.45957 0.29755 = 0.16239 -0.04967 0.04110 0.11140 AFIX 137 H52D 2 0.694004 0.398343 0.284926 -31.00000 -1.50000 H52E 2 0.590470 0.375978 0.296864 -31.00000 -1.50000 H52F 2 0.637327 0.433926 0.312281 -31.00000 -1.50000 AFIX 0 C53A 1 0.582389 0.447863 0.267128 -31.00000 0.46253 0.29215 = 0.16133 -0.06759 0.07738 0.11225 O5A 5 0.494207 0.439716 0.261943 -31.00000 0.45681 0.28743 = 0.15665 -0.07335 0.08284 0.10936 HKLF 4 REM 230917lu_lgpz145541_0m_a.res in Pnnn REM wR2 = 0.3428, GooF = S = 1.023, Restrained GooF = 1.049 for all data REM R1 = 0.1380 for 6242 Fo > 4sig(Fo) and 0.2090 for all 11951 data REM 728 parameters refined using 223 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 1.482, deepest hole -1.224, 1-sigma level 0.098 Q1 1 0.4620 0.5200 0.2325 11.00000 0.05 1.48 Q2 1 0.5372 0.4928 0.2449 11.00000 0.05 0.73 Q3 1 0.5554 0.5490 0.2319 11.00000 0.05 0.73 Q4 1 0.7053 0.7154 0.5666 11.00000 0.05 0.67 Q5 1 0.7525 0.6885 0.5327 11.00000 0.05 0.66 Q6 1 0.6479 0.6783 0.6518 11.00000 0.05 0.64 Q7 1 0.4848 0.4553 0.2570 11.00000 0.05 0.63 Q8 1 0.5795 0.7255 0.6636 11.00000 0.05 0.62 Q9 1 0.2500 0.7500 0.6179 10.50000 0.05 0.61 Q10 1 0.3940 0.5624 0.2100 11.00000 0.05 0.60 Q11 1 0.7940 0.6988 0.4362 11.00000 0.05 0.58 Q12 1 0.7680 0.6949 0.4005 11.00000 0.05 0.56 Q13 1 0.3345 0.6123 0.3102 11.00000 0.05 0.54 Q14 1 0.7437 0.6917 0.4344 11.00000 0.05 0.54 Q15 1 0.7786 0.6561 0.6266 11.00000 0.05 0.48 Q16 1 0.3407 0.6454 0.2129 11.00000 0.05 0.47 Q17 1 0.2853 0.7250 0.6486 11.00000 0.05 0.46 Q18 1 0.7345 0.6316 0.6157 11.00000 0.05 0.45 Q19 1 0.3499 0.5824 0.2798 11.00000 0.05 0.42 Q20 1 0.6730 0.6812 0.6254 11.00000 0.05 0.42 Q21 1 0.6979 0.5358 0.2474 11.00000 0.05 0.39 Q22 1 0.5217 0.5777 0.2909 11.00000 0.05 0.38 Q23 1 0.5174 0.6075 0.3185 11.00000 0.05 0.38 Q24 1 0.3575 0.6863 0.1924 11.00000 0.05 0.37 Q25 1 0.4836 0.3946 0.2497 11.00000 0.05 0.34 Q26 1 0.8596 0.7012 0.6966 11.00000 0.05 0.33 Q27 1 0.3142 0.5902 0.1785 11.00000 0.05 0.31 Q28 1 0.3656 0.7500 0.2500 10.50000 0.05 0.30 Q29 1 0.4571 0.6344 0.2787 11.00000 0.05 0.30 Q30 1 0.4676 0.8730 0.6663 11.00000 0.05 0.29 Q31 1 0.6625 0.3986 0.2803 11.00000 0.05 0.29 Q32 1 0.2765 0.5111 0.2191 11.00000 0.05 0.28 ; _shelx_res_checksum 36814 _shelx_hkl_file ; -1 0 0 0.00 0.40 -3 0 0 0.40 1.60 -4 0 0 172.18 7.40 -4 0 0 167.98 7.10 -5 0 0 1.50 2.40 -5 0 0 0.50 2.90 -6 0 0 891.91 32.00 -6 0 0 831.12 31.50 -7 0 0 1.20 3.70 -7 0 0 -0.90 4.10 -8 0 0 449.95 19.40 -8 0 0 479.45 18.80 -9 0 0 -2.00 5.40 -9 0 0 7.50 5.40 -10 0 0 272.37 15.50 -10 0 0 302.77 15.20 -11 0 0 -6.00 7.60 -11 0 0 9.20 7.50 -12 0 0 51.79 9.10 -12 0 0 35.10 9.60 -13 0 0 -5.00 8.70 -13 0 0 0.70 10.70 -14 0 0 -8.90 11.20 -15 0 0 0.00 13.60 -16 0 0 58.89 20.00 -17 0 0 11.00 15.50 0 -1 0 2.10 0.30 0 1 0 0.00 0.30 1 1 0 260.17 9.20 -1 -1 0 261.67 9.20 1 1 0 255.87 9.20 -1 1 0 268.57 9.20 -1 1 0 238.38 9.30 -1 1 0 254.77 9.20 -1 -1 0 254.97 9.20 -2 -1 0 0.30 1.20 2 1 0 1.70 0.60 -2 1 0 1.40 0.40 -2 1 0 1.50 1.40 -2 1 0 1.20 0.50 2 1 0 1.30 0.70 -2 -1 0 1.10 1.00 4 1 0 1.00 0.60 4 1 0 0.10 0.50 -4 -1 0 -1.50 2.30 -4 -1 0 1.10 2.00 -4 1 0 0.40 2.20 -4 1 0 -0.90 2.00 -5 -1 0 406.46 16.00 -5 1 0 433.86 15.90 -5 1 0 410.06 16.20 -5 -1 0 439.46 16.50 -6 -1 0 4.60 3.20 -6 1 0 5.20 3.10 -6 -1 0 -0.90 3.70 -6 1 0 4.50 3.50 -7 1 0 64.29 5.60 -7 -1 0 64.29 6.10 -7 -1 0 58.39 5.20 -7 1 0 56.79 4.80 -8 1 0 -0.40 4.30 -8 -1 0 -9.50 4.40 -8 -1 0 5.10 5.00 -8 1 0 4.40 4.90 -9 1 0 98.09 7.50 -9 1 0 113.49 8.70 -9 -1 0 121.59 9.30 -9 -1 0 128.19 8.70 -10 -1 0 -2.00 6.20 -10 1 0 6.80 6.80 -10 -1 0 10.50 6.90 -10 1 0 -3.40 5.90 -11 1 0 202.48 14.20 -11 -1 0 224.28 14.60 -11 -1 0 188.58 15.10 -11 1 0 200.88 14.60 -12 -1 0 12.70 8.60 -12 1 0 -7.00 7.60 -12 -1 0 9.20 9.70 -12 1 0 2.80 8.90 -13 1 0 60.49 12.30 -13 -1 0 57.89 12.30 -13 1 0 83.49 10.20 -13 -1 0 108.29 11.00 -14 1 0 8.30 9.20 -14 -1 0 -18.70 11.80 -14 1 0 -9.00 11.60 -15 1 0 31.70 13.30 -15 -1 0 43.60 18.50 -16 -1 0 30.50 19.00 -16 1 0 -6.10 17.10 -17 -1 0 4.40 14.80 -17 1 0 18.80 16.10 1 2 0 -0.20 0.80 -1 2 0 0.50 0.70 -1 -2 0 0.40 0.70 1 -2 0 -0.10 0.50 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2 0 -6.60 8.80 -14 2 0 132.99 14.40 -14 -2 0 138.79 17.50 -14 2 0 115.19 11.70 -15 2 0 9.40 10.30 -15 -2 0 30.70 19.50 -15 2 0 -0.70 11.50 -16 2 0 -13.10 14.30 -16 -2 0 -13.60 17.10 -17 -2 0 -2.40 13.90 -17 2 0 -6.40 16.30 0 3 0 -0.70 1.00 0 3 0 -1.40 1.10 0 -3 0 -1.60 0.80 -1 -3 0 146.49 5.60 1 3 0 138.99 5.80 1 -3 0 145.69 5.50 1 3 0 147.59 6.00 -1 3 0 151.28 6.00 2 -3 0 1.80 1.10 -2 3 0 1.40 1.20 -2 3 0 -1.00 1.30 2 3 0 -0.10 1.40 -2 -3 0 -1.30 1.40 -2 3 0 2.00 1.90 2 3 0 0.00 1.60 3 3 0 258.37 9.60 -3 -3 0 253.37 9.50 -3 3 0 242.98 9.50 -3 3 0 249.78 9.50 3 3 0 257.47 9.70 -3 3 0 258.37 10.00 -3 -3 0 249.58 9.80 -3 -3 0 251.77 10.30 -3 3 0 257.87 9.40 -4 3 0 0.20 1.70 -4 -3 0 -4.30 2.60 -4 3 0 -2.40 1.80 -4 3 0 -0.10 1.10 -4 -3 0 -2.80 1.80 -4 -3 0 1.00 2.30 -4 3 0 -2.50 2.30 4 3 0 -0.30 1.20 4 3 0 -0.40 1.40 -4 3 0 1.40 0.90 -5 3 0 73.29 4.90 5 3 0 84.49 3.90 -5 -3 0 82.99 5.20 -5 3 0 88.39 5.40 5 3 0 82.89 4.20 -5 -3 0 83.29 6.10 6 3 0 -0.80 1.10 6 3 0 -0.30 1.40 -6 -3 0 -0.70 3.90 -6 3 0 -1.20 3.10 -6 3 0 1.20 3.40 -6 -3 0 5.50 3.70 -7 3 0 281.07 12.30 -7 -3 0 288.87 13.10 -7 -3 0 253.87 12.30 -7 3 0 287.37 12.20 -8 3 0 4.20 4.20 -8 3 0 5.10 4.50 -8 -3 0 3.50 5.70 -8 -3 0 -1.90 4.80 -9 -3 0 3.70 6.00 -9 -3 0 -1.60 6.40 -9 3 0 6.40 5.80 -9 3 0 10.30 5.40 -10 -3 0 -9.40 6.60 -10 3 0 -6.50 6.10 -10 -3 0 -9.00 6.90 -10 3 0 1.40 6.60 -11 -3 0 53.99 8.50 11 -3 0 46.40 4.30 -11 3 0 42.00 8.00 11 3 0 47.40 6.30 -11 3 0 35.20 8.70 -11 -3 0 40.40 9.30 -12 -3 0 1.50 9.20 12 3 0 -6.10 5.80 -12 3 0 3.90 8.40 -12 3 0 2.20 8.70 -13 3 0 -1.40 9.00 -13 3 0 -1.60 9.90 -13 -3 0 5.50 12.90 -14 3 0 6.30 11.60 -14 3 0 -5.00 8.90 -14 -3 0 7.30 18.70 -15 3 0 12.40 11.60 -15 3 0 -4.70 9.50 -15 -3 0 33.80 19.30 -16 -3 0 -17.40 16.30 -16 3 0 7.40 12.50 -17 -3 0 18.20 13.90 -17 3 0 1.20 16.00 0 4 0 337.87 13.20 0 -4 0 351.66 12.80 0 4 0 366.86 13.40 -1 4 0 2.20 1.60 1 4 0 1.80 2.00 1 4 0 2.50 1.70 -1 4 0 0.50 1.90 -1 -4 0 -1.00 1.50 1 -4 0 2.20 1.30 -3 4 0 0.70 1.80 -3 -4 0 -3.80 2.50 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17.50 -13 5 0 8.40 8.90 -13 5 0 8.30 9.90 -14 -5 0 30.80 19.00 -14 5 0 0.80 9.20 -14 5 0 5.40 11.00 -15 -5 0 9.20 17.50 -15 5 0 27.90 11.80 -15 5 0 -6.00 8.90 -16 -5 0 -21.60 14.60 -16 5 0 17.20 12.00 0 6 0 2098.99 72.69 0 6 0 2027.00 72.79 0 -6 0 1954.10 72.19 0 6 0 2061.29 72.69 -1 -6 0 0.40 1.90 -1 6 0 1.30 2.40 -1 6 0 -0.10 2.00 1 6 0 0.50 2.10 1 6 0 0.20 2.40 -1 6 0 -1.80 2.30 1 6 0 -1.20 2.40 1 -6 0 0.70 1.70 2 6 0 9999.00 353.26 3 6 0 1.70 2.70 -3 6 0 -1.10 2.50 3 -6 0 -4.00 1.80 -3 6 0 0.80 2.40 3 6 0 -2.70 2.40 3 6 0 -0.60 2.20 -3 6 0 -1.80 2.70 -3 -6 0 3.50 3.10 -3 6 0 -4.10 2.10 -3 6 0 -0.10 1.80 -3 -6 0 -0.80 2.20 -4 6 0 7.30 2.80 -4 6 0 2.70 3.30 4 6 0 9.80 3.20 -4 -6 0 8.00 2.70 -4 -6 0 8.60 4.00 -4 6 0 9.90 2.40 4 6 0 12.20 2.50 4 -6 0 14.20 2.30 -4 6 0 8.50 2.10 -4 6 0 10.20 2.60 4 6 0 10.50 2.80 5 6 0 1.60 3.20 5 6 0 3.80 2.70 -5 -6 0 -1.60 2.80 -5 6 0 2.40 1.80 -5 -6 0 6.40 5.00 5 6 0 -2.10 2.30 5 -6 0 -1.40 2.10 -5 6 0 -2.00 3.50 -5 6 0 2.40 2.30 -5 6 0 0.90 2.60 -5 6 0 -1.40 2.90 -6 6 0 3.40 4.10 -6 -6 0 3.60 3.30 -6 6 0 6.00 2.00 -6 6 0 1.60 3.20 -6 -6 0 1.40 5.40 -6 6 0 10.20 1.70 6 6 0 8.10 3.60 6 6 0 6.50 3.00 6 -6 0 2.30 2.40 6 6 0 5.20 2.30 -7 6 0 2.10 4.50 7 6 0 -9.50 3.70 -7 6 0 5.00 3.80 7 6 0 1.30 2.10 -7 -6 0 -0.70 5.90 7 -6 0 -0.60 2.50 7 6 0 -1.00 2.70 8 6 0 35.90 3.30 -8 -6 0 32.70 7.70 8 6 0 42.40 5.10 8 -6 0 39.10 3.60 -8 6 0 32.50 5.50 -8 6 0 36.80 5.90 -9 -6 0 0.00 8.90 9 6 0 -4.70 4.60 -9 6 0 1.30 5.70 -9 6 0 -5.40 5.20 9 -6 0 1.50 3.30 10 6 0 33.80 5.90 -10 6 0 16.90 6.80 -10 -6 0 30.20 11.80 -10 6 0 31.20 7.10 10 -6 0 22.80 4.00 11 -6 0 4.40 4.00 -11 -6 0 22.70 14.60 -11 6 0 -0.50 7.70 11 6 0 -6.00 5.80 -11 6 0 2.90 7.50 -12 6 0 0.30 8.30 -12 -6 0 25.40 17.40 -12 6 0 2.40 9.00 12 6 0 5.90 6.80 -13 6 0 6.20 10.20 -13 6 0 10.10 9.20 -13 -6 0 -26.10 16.90 -14 -6 0 48.90 18.50 -14 6 0 63.99 11.10 -14 6 0 64.89 12.50 -15 6 0 -2.80 9.60 -15 6 0 9.80 11.70 -15 -6 0 -4.90 16.60 -16 6 0 41.60 11.80 0 7 0 -1.50 2.70 0 -7 0 0.00 2.00 0 7 0 -0.50 2.30 0 7 0 3.70 2.70 1 -7 0 5232.28 186.68 -1 7 0 5175.48 187.18 1 7 0 5240.88 187.18 1 7 0 5645.74 187.48 1 7 0 5182.08 187.28 -1 7 0 5082.59 187.18 -1 7 0 5517.65 187.38 -1 -7 0 5183.08 186.68 2 7 0 -1.20 2.80 -2 7 0 0.30 2.80 -2 7 0 -1.40 2.70 2 7 0 -0.70 2.50 2 7 0 1.00 2.90 2 -7 0 3.10 2.10 -2 -7 0 0.10 2.20 -2 7 0 1.50 2.20 -3 7 0 98.39 6.00 3 -7 0 91.79 4.80 3 7 0 88.19 6.10 -3 7 0 90.19 5.70 3 7 0 86.19 6.30 -3 -7 0 97.09 6.40 3 7 0 92.79 5.50 -3 7 0 94.69 5.40 -3 7 0 96.29 6.30 -3 -7 0 94.59 5.00 -4 7 0 -2.50 2.10 -4 -7 0 1.20 3.90 -4 -7 0 -0.30 2.80 4 -7 0 -1.30 2.30 -4 7 0 0.40 2.60 -4 7 0 -1.10 3.00 -4 7 0 3.60 2.80 4 7 0 -2.00 2.60 -4 7 0 0.90 3.60 4 7 0 -3.50 3.10 4 7 0 0.70 3.30 -5 7 0 -1.40 2.70 -5 7 0 1.40 4.00 -5 7 0 -0.60 3.20 5 7 0 4.70 3.30 5 7 0 3.10 2.60 5 -7 0 2.90 2.40 5 7 0 0.50 3.50 -5 7 0 1.80 2.70 -5 7 0 1.40 2.10 -5 -7 0 3.90 3.10 6 7 0 -1.00 3.10 -6 7 0 0.70 2.00 -6 7 0 2.40 3.50 -6 7 0 3.20 3.20 -6 7 0 2.10 2.40 -6 -7 0 -7.20 6.30 -6 7 0 -4.40 4.20 6 -7 0 0.10 2.60 6 7 0 0.40 2.50 6 7 0 -3.80 3.60 -6 -7 0 3.60 3.60 -7 7 0 11.00 4.80 -7 7 0 13.70 1.60 7 7 0 4.60 3.40 -7 -7 0 3.90 7.70 -7 7 0 11.20 4.00 7 7 0 10.40 4.30 7 -7 0 5.60 2.90 -7 7 0 10.60 2.00 8 7 0 -9.10 4.30 8 -7 0 -1.60 3.10 -8 7 0 -2.80 5.40 8 7 0 -1.70 3.20 -8 7 0 5.90 4.70 -8 -7 0 5.20 9.70 -9 -7 0 9.20 11.50 -9 7 0 6.80 5.90 9 -7 0 17.00 3.70 -9 7 0 12.40 5.80 9 7 0 12.10 5.40 -10 7 0 -2.60 6.70 -10 7 0 4.30 6.60 10 7 0 -0.70 5.30 -10 -7 0 -6.10 13.00 10 -7 0 4.50 3.90 11 -7 0 87.59 6.00 11 7 0 71.49 8.10 -11 -7 0 89.19 15.80 -11 7 0 87.69 9.10 -11 7 0 69.29 10.10 12 7 0 1.00 7.00 -12 7 0 -10.70 8.30 -12 7 0 4.20 9.60 -12 -7 0 45.00 15.30 -13 -7 0 129.49 18.90 -13 7 0 131.29 13.30 -13 7 0 112.29 11.90 -14 7 0 -9.60 10.90 -14 7 0 -2.60 10.00 -14 -7 0 -11.60 15.80 -15 7 0 -16.50 11.20 -15 -7 0 11.30 16.00 -16 7 0 -16.00 11.10 0 8 0 1434.06 52.99 0 8 0 1443.46 53.19 0 -8 0 1485.75 52.39 0 8 0 1491.15 52.99 -1 -8 0 -0.60 2.40 1 8 0 -1.00 3.10 1 8 0 1.60 2.80 -1 8 0 -0.40 3.00 -1 8 0 -3.40 3.20 1 -8 0 3.90 2.40 1 8 0 -4.90 3.10 -1 8 0 2.20 2.70 -2 -8 0 804.12 29.60 -2 8 0 793.52 30.40 -2 8 0 817.92 30.20 2 8 0 819.42 30.30 2 -8 0 820.02 29.50 2 8 0 805.82 30.30 -2 8 0 817.22 30.20 2 8 0 836.62 30.70 -3 8 0 -3.90 3.20 3 -8 0 -0.50 2.50 -3 8 0 0.90 3.50 -3 8 0 6.80 2.50 -3 8 0 -1.90 3.20 -3 -8 0 -2.40 2.80 3 8 0 0.90 2.90 3 8 0 -8.90 3.10 3 8 0 1.00 3.50 -4 8 0 258.27 11.10 4 -8 0 269.47 10.70 -4 8 0 269.47 11.00 -4 -8 0 277.37 10.90 -4 8 0 259.07 11.60 4 8 0 272.07 12.20 -4 8 0 292.77 12.00 -4 8 0 261.27 11.80 -4 -8 0 267.47 12.50 4 8 0 271.87 12.00 4 8 0 244.38 11.50 5 -8 0 0.70 2.80 -5 8 0 0.50 3.70 5 8 0 3.10 3.90 -5 8 0 -2.50 4.20 -5 8 0 0.20 3.20 -5 -8 0 2.40 3.40 5 8 0 -0.80 3.50 -5 -8 0 -2.40 4.80 -5 8 0 -0.50 3.00 -5 8 0 3.90 2.50 5 8 0 -0.20 2.90 -6 8 0 314.77 13.10 -6 8 0 331.37 12.60 -6 -8 0 270.07 15.10 -6 8 0 287.37 12.70 -6 -8 0 323.57 12.70 6 8 0 292.17 12.70 6 8 0 303.97 13.50 6 8 0 318.37 13.70 6 -8 0 294.37 12.20 -6 8 0 320.57 13.70 -6 8 0 298.97 12.20 7 8 0 -4.40 3.80 7 -8 0 -3.90 3.00 7 8 0 0.90 4.50 -7 8 0 0.00 2.00 -7 8 0 -6.00 5.00 -7 8 0 4.20 4.00 -7 -8 0 3.70 7.30 8 -8 0 35.30 4.00 8 8 0 35.80 5.60 8 8 0 22.20 4.50 -8 8 0 23.70 5.30 -8 -8 0 30.70 9.60 -8 8 0 22.60 6.10 -9 -8 0 15.60 11.20 -9 8 0 8.70 7.00 9 8 0 -6.20 5.20 -9 8 0 9.40 5.90 9 -8 0 -0.10 3.80 10 -8 0 42.30 4.90 10 8 0 47.00 6.90 -10 8 0 48.00 7.70 -10 -8 0 35.10 12.80 -10 8 0 45.20 8.00 11 8 0 -8.00 6.00 -11 -8 0 -3.00 13.60 -11 8 0 2.00 8.10 -11 8 0 14.50 8.40 11 -8 0 -1.80 4.40 -12 8 0 81.29 10.50 -12 -8 0 67.09 16.40 12 8 0 77.09 11.70 -12 8 0 81.29 11.60 -13 8 0 -12.90 9.50 -13 8 0 -6.40 10.00 -13 -8 0 -21.50 14.50 -14 8 0 -0.30 9.80 -14 -8 0 12.70 15.20 -14 8 0 -6.40 11.20 -15 8 0 -24.00 10.70 -16 8 0 17.70 11.70 0 -9 0 -0.40 2.70 0 9 0 0.80 3.50 0 9 0 0.50 3.10 0 9 0 2.70 3.80 -1 -9 0 589.44 22.20 1 -9 0 596.34 22.20 -1 9 0 588.74 22.90 -1 9 0 603.94 23.40 1 9 0 619.34 23.50 1 9 0 601.24 23.10 1 9 0 577.74 23.00 -1 9 0 615.54 23.00 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48.10 7.60 -7 12 0 -2.30 6.70 -7 12 0 5.40 4.70 7 12 0 -1.70 6.10 -7 12 0 -1.30 5.50 -7 -12 0 4.90 6.00 7 -12 0 7.20 4.50 -8 12 0 60.99 6.90 -8 12 0 56.29 9.10 8 12 0 44.80 7.50 8 -12 0 64.69 6.20 9 12 0 3.40 6.70 -9 12 0 8.10 6.80 9 -12 0 -0.30 4.90 -9 12 0 -9.80 8.20 -10 12 0 133.89 10.60 10 -12 0 124.29 8.30 10 12 0 112.19 9.70 -10 12 0 118.79 11.40 -11 12 0 -4.00 9.30 -11 12 0 18.20 9.10 11 -12 0 -9.10 5.40 11 12 0 -0.50 7.30 -12 12 0 20.00 10.20 -12 12 0 8.40 10.20 -13 12 0 13.40 9.50 -13 12 0 8.30 10.80 -14 12 0 4.70 10.80 -15 12 0 0.10 11.00 0 13 0 2.80 6.10 0 13 0 0.20 4.80 0 13 0 -5.30 5.10 0 -13 0 -0.90 4.20 1 -13 0 3.20 4.40 -1 13 0 10.60 5.20 -1 13 0 11.40 5.10 1 13 0 10.30 6.40 1 13 0 10.40 5.20 -1 13 0 6.90 6.30 -1 -13 0 4.10 4.40 1 13 0 10.00 5.40 2 13 0 -3.30 5.30 2 13 0 -3.70 5.10 -2 -13 0 3.90 4.50 -2 13 0 5.80 4.70 -2 13 0 -1.70 5.20 -2 13 0 4.10 6.10 2 -13 0 -4.20 4.10 2 13 0 10.60 6.50 3 13 0 596.64 26.00 3 13 0 627.44 26.00 -3 13 0 653.73 25.80 -3 -13 0 658.23 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21.20 9.30 2 -26 3 9.40 9.20 2 26 3 2.20 8.40 -2 26 -3 14.40 9.00 -2 -26 3 9.40 9.00 2 -26 -3 0.20 8.50 -2 26 -3 11.70 6.50 -3 -26 -3 -7.70 8.40 3 26 -3 -5.00 9.50 -3 26 3 8.30 8.90 -3 26 3 -0.50 6.40 3 -26 3 6.40 8.20 -3 26 -3 -6.40 5.90 -3 26 -3 -4.00 9.00 3 -26 -3 3.20 8.20 -3 -26 3 -1.30 8.90 3 26 3 2.00 8.50 -4 -26 -3 8.60 12.70 -4 26 3 9.00 8.70 4 26 -3 -4.80 9.40 -4 26 3 2.20 6.50 -4 26 -3 10.80 8.50 -4 26 -3 3.50 6.30 4 26 3 3.00 7.50 -4 -26 3 -10.80 11.80 -5 26 3 -8.10 5.70 -5 26 3 -0.90 7.60 5 26 -3 -3.80 7.80 -5 26 -3 -5.20 5.80 5 26 3 1.60 6.90 -5 26 -3 4.40 8.40 6 26 -3 18.00 8.10 -6 26 3 6.20 6.20 6 26 3 4.20 7.30 -6 26 -3 15.40 5.50 -6 26 -3 10.00 7.20 0 27 -3 -10.30 9.00 0 27 3 4.90 6.70 0 27 3 -0.30 8.40 0 27 -3 7.10 6.50 1 27 -3 4.80 9.00 -1 27 3 7.50 6.30 -1 27 3 1.90 9.20 1 27 3 9.10 8.40 -1 27 -3 5.50 9.10 -1 27 -3 -7.00 5.80 -2 27 3 1.00 8.60 2 27 -3 -10.60 8.90 -2 27 3 -1.70 6.30 -2 27 -3 4.20 8.60 2 27 3 -6.10 7.00 -2 27 -3 2.50 5.90 -3 27 3 21.40 9.40 3 27 -3 -2.90 8.20 -3 27 3 3.00 5.70 -3 27 -3 -2.30 5.40 -3 27 -3 -0.80 9.00 3 27 3 6.90 7.30 -4 27 3 1.60 5.10 4 27 -3 -3.40 7.80 -4 27 3 6.50 8.10 -4 27 -3 2.90 5.70 -4 27 -3 9.60 8.10 4 27 3 7.50 7.50 5 27 -3 5.70 7.40 -5 27 3 17.70 6.00 -5 27 -3 13.10 5.50 5 27 3 -2.50 6.70 -5 27 -3 6.50 7.90 0 28 3 -0.90 5.70 0 28 -3 -3.50 5.80 0 28 -3 3.00 7.30 0 28 3 -2.50 8.00 -1 28 3 12.00 5.60 -1 28 3 -3.30 8.20 1 28 -3 -7.00 8.00 1 28 -3 -14.10 6.10 1 28 3 -9.30 6.30 -1 28 -3 -8.60 5.80 1 28 3 0.60 7.10 -1 28 -3 2.70 7.90 -2 28 3 -6.50 7.50 -2 28 3 12.50 6.00 2 28 -3 1.40 7.90 -2 28 -3 8.90 8.10 -2 28 -3 2.00 5.30 2 28 3 2.40 8.20 -1 0 4 -0.70 0.60 -1 0 4 -0.30 0.70 1 0 -4 0.20 0.70 1 0 4 0.60 0.60 -1 0 -4 0.40 0.40 -2 0 4 2189.58 77.99 2 0 -4 2304.77 77.99 -2 0 -4 2116.99 77.89 3 0 4 1.90 0.70 -3 0 4 2.00 2.10 -3 0 4 1.20 1.80 3 0 -4 0.90 0.90 -3 0 -4 0.90 1.00 -3 0 4 2.40 0.80 -3 0 -4 -0.10 1.40 -4 0 4 990.20 34.70 -4 0 -4 916.61 35.00 -4 0 -4 949.40 35.20 -4 0 4 959.20 35.40 4 0 4 1012.20 34.60 -4 0 -4 997.60 34.70 -4 0 4 987.30 35.20 4 0 -4 992.70 34.80 5 0 -4 0.10 0.80 -5 0 -4 1.20 2.20 -5 0 4 1.90 0.90 -5 0 -4 0.40 2.70 -5 0 4 -0.90 2.60 -5 0 4 -1.50 2.90 -6 0 -4 339.87 13.40 -6 0 4 347.17 14.20 -6 0 -4 340.97 13.90 -6 0 4 332.37 13.80 -7 0 4 -0.40 4.40 -7 0 -4 -5.50 3.80 -7 0 4 3.00 4.10 -7 0 -4 -0.70 3.50 -8 0 -4 163.38 8.70 -8 0 4 133.39 10.10 -8 0 4 153.38 9.30 -8 0 -4 145.09 9.50 -9 0 -4 14.70 5.30 -9 0 4 4.30 6.00 -9 0 -4 0.40 5.40 -9 0 4 5.20 5.50 -10 0 4 98.29 9.70 -10 0 -4 109.19 9.60 -10 0 4 128.09 9.40 -10 0 -4 122.09 8.70 -11 0 -4 0.50 6.40 -11 0 -4 -10.80 7.30 -11 0 4 -13.10 7.50 -11 0 4 2.10 7.90 -12 0 -4 193.88 12.60 -12 0 4 192.18 16.00 -13 0 -4 -10.80 10.20 -13 0 4 -6.50 10.40 -13 0 4 -9.40 9.00 -13 0 -4 8.90 8.40 -14 0 4 3.30 9.80 -14 0 4 18.20 11.90 -14 0 -4 20.30 12.60 -15 0 -4 -6.90 18.30 -15 0 4 9.10 11.70 -16 0 4 8.90 17.10 -16 0 -4 44.10 16.80 -17 0 4 9.40 16.80 0 -1 -4 0.60 0.50 0 1 4 0.40 0.40 0 1 4 2.50 0.80 0 -1 4 0.10 0.60 0 1 -4 1.30 0.60 0 -1 -4 0.40 0.80 0 -1 -4 0.80 0.50 -1 1 4 137.29 5.20 -1 1 4 143.09 5.20 1 1 -4 139.99 5.10 1 -1 4 132.69 5.10 1 -1 -4 126.19 4.80 -1 -1 4 137.79 5.10 -1 -1 4 148.59 5.20 1 -1 -4 132.99 5.30 1 1 4 132.89 5.20 1 1 4 124.69 4.80 -1 -1 4 130.99 4.90 -2 1 4 466.35 17.20 -2 -1 -4 473.15 17.10 2 -1 4 485.65 17.20 -2 1 4 478.25 17.50 -2 -1 -4 462.85 17.30 2 1 -4 496.25 17.20 -2 1 -4 475.35 17.30 -2 -1 4 466.05 17.30 -2 -1 4 487.75 17.20 2 -1 -4 480.95 16.90 2 1 4 487.35 17.30 -2 1 -4 474.15 17.20 2 -1 -4 488.85 17.30 -2 -1 4 473.65 17.00 3 1 -4 263.27 9.20 -3 1 4 250.57 9.70 -3 1 4 243.18 9.60 -3 1 4 243.48 9.10 3 -1 4 261.87 9.10 -3 -1 -4 225.78 9.30 -3 -1 -4 255.87 9.40 -3 -1 4 256.17 9.60 -3 1 -4 255.67 9.50 -3 -1 4 252.17 9.30 3 1 4 256.27 9.30 -3 1 -4 235.78 9.20 -3 -1 4 239.48 10.00 3 -1 -4 254.37 9.30 -4 1 4 30.50 2.80 -4 -1 -4 29.60 3.00 4 -1 4 30.20 1.70 4 1 -4 29.70 1.90 -4 -1 -4 30.80 2.40 -4 -1 -4 25.00 2.30 -4 1 4 35.80 3.10 -4 1 4 29.30 1.70 -4 1 -4 29.40 2.60 -4 -1 4 22.60 3.20 -4 1 -4 26.10 1.80 -4 1 -4 36.10 2.80 -4 -1 4 31.60 2.90 -4 -1 4 31.70 2.20 4 -1 -4 26.60 2.00 4 1 4 27.60 1.90 -5 1 4 183.48 6.40 -5 -1 -4 170.68 8.00 -5 1 4 168.98 7.90 -5 -1 -4 169.48 7.50 -5 1 4 164.08 7.90 5 1 -4 173.58 6.60 -5 1 -4 174.78 7.80 5 -1 -4 174.08 6.50 -5 -1 4 175.68 8.00 5 1 4 174.68 6.40 -5 -1 4 176.68 6.70 -5 1 -4 170.78 7.60 -5 -1 4 185.48 8.40 -6 1 4 136.89 7.40 -6 -1 -4 132.79 7.60 -6 1 4 128.69 7.40 -6 -1 -4 125.99 6.90 -6 1 -4 131.79 7.30 -6 1 -4 135.19 6.70 -6 -1 4 124.89 8.20 -6 -1 4 152.38 7.40 -7 -1 -4 824.32 30.10 -7 -1 -4 808.22 29.50 -7 1 4 786.72 30.10 -7 1 4 804.62 29.50 -7 -1 4 812.02 29.80 -7 1 -4 767.62 29.70 -7 -1 4 816.62 30.40 -7 1 -4 735.23 29.20 -8 1 4 714.03 26.50 -8 1 4 702.03 27.20 -8 -1 -4 711.13 27.20 -8 -1 -4 681.03 26.40 -8 1 -4 700.83 26.80 -8 -1 4 705.53 27.60 -8 1 -4 648.94 26.20 -8 -1 4 692.73 26.80 -9 -1 -4 62.79 7.20 -9 -1 -4 39.90 6.00 -9 1 4 56.19 6.40 -9 1 4 52.49 7.20 -9 -1 4 62.19 7.00 -9 1 -4 76.09 6.40 -9 1 -4 57.69 6.70 -9 -1 4 49.20 7.50 -10 1 4 -6.40 6.40 -10 -1 -4 -5.00 6.70 -10 1 4 1.00 7.00 -10 -1 -4 5.10 6.20 -10 1 -4 -5.80 6.80 -10 -1 4 6.10 6.60 -10 1 -4 -0.90 5.40 -10 -1 4 -16.00 6.70 -11 1 4 38.90 9.10 -11 -1 -4 51.39 7.70 -11 1 4 48.70 8.50 -11 -1 -4 39.60 8.40 -11 -1 4 35.90 9.40 -11 1 -4 56.49 8.00 -11 1 -4 55.89 9.00 -11 -1 4 54.29 9.10 -12 1 4 8.10 8.40 -12 -1 -4 3.40 9.20 -12 1 4 1.00 9.20 -12 -1 -4 5.80 8.10 -12 -1 4 -0.50 9.70 -12 1 -4 7.60 8.80 -12 -1 4 2.60 8.40 -12 1 -4 9.20 7.90 -13 1 4 33.20 10.00 -13 -1 -4 14.30 11.00 -13 1 4 13.90 10.60 -13 -1 4 18.40 11.30 -13 1 -4 7.20 10.60 -13 -1 4 7.90 9.00 -13 1 -4 8.50 8.80 -14 1 4 6.00 12.00 -14 -1 -4 -7.00 14.90 -14 1 4 1.00 10.00 -14 1 -4 0.90 11.40 -14 1 -4 14.10 8.90 -14 -1 4 23.90 11.60 -15 1 4 0.30 12.30 -15 -1 -4 -5.00 18.00 -15 1 -4 -7.00 15.20 -15 -1 4 33.90 15.10 -16 -1 -4 -26.80 15.30 -16 1 4 1.20 13.10 -16 1 -4 -11.90 16.40 -16 -1 4 17.90 20.20 -17 1 4 2.40 17.00 -17 -1 4 10.50 16.80 -1 2 4 4.50 1.30 1 2 -4 7.50 1.10 -1 -2 -4 7.70 1.30 -1 -2 -4 7.10 1.50 1 -2 4 8.10 1.10 -1 2 4 7.50 1.40 1 -2 -4 6.50 0.80 1 -2 -4 4.60 1.40 -1 -2 4 3.80 1.20 1 2 4 6.70 1.40 -2 2 4 1227.38 43.00 -2 2 4 1217.88 43.10 -2 -2 -4 1229.88 43.10 2 2 -4 1204.88 42.90 2 -2 4 1233.98 42.90 -2 -2 -4 1197.48 42.90 -2 2 -4 1180.68 43.00 2 -2 -4 1219.18 43.00 -2 -2 4 1261.97 43.10 -2 -2 4 1198.38 42.80 -2 2 -4 1124.69 42.80 -2 -2 4 1159.08 43.00 2 2 4 1258.37 43.10 2 -2 -4 1190.58 42.70 -3 2 -4 5856.81 207.58 3 -2 -4 5877.71 206.88 -4 -2 -4 5122.89 173.08 -4 2 4 4945.41 172.88 -4 2 -4 4831.42 172.78 -4 -2 4 4646.64 173.28 5 2 -4 50.49 2.60 -5 2 4 50.19 2.30 -5 -2 -4 54.49 3.70 -5 2 4 55.19 4.10 -5 -2 -4 55.29 4.40 -5 2 4 49.40 3.90 -5 2 -4 52.09 2.20 -5 2 -4 48.90 2.10 -5 2 -4 51.59 4.20 -5 -2 4 54.19 4.10 -5 -2 4 51.39 4.80 -5 2 -4 47.30 3.60 5 -2 -4 52.59 2.50 -6 2 4 800.62 29.60 6 2 -4 777.62 28.40 -6 -2 -4 749.73 29.20 -6 2 4 837.02 29.40 -6 -2 -4 805.12 29.80 6 2 -4 838.52 28.60 -6 -2 4 763.32 30.10 -6 2 -4 788.52 29.40 -6 2 -4 773.12 29.20 6 2 4 797.02 28.30 6 2 4 816.82 28.40 -7 2 4 43.90 4.60 -7 -2 -4 52.09 4.80 -7 -2 -4 54.19 5.50 -7 2 4 45.00 5.10 -7 -2 4 50.09 6.00 -7 2 -4 48.10 4.30 -7 2 -4 41.30 4.90 -7 -2 4 55.69 5.40 -8 2 4 371.86 16.10 -8 -2 -4 353.56 16.40 -8 2 4 369.46 15.60 -8 -2 -4 350.56 15.50 -8 -2 4 384.16 16.00 -8 -2 4 370.86 16.60 -8 2 -4 363.96 15.60 -8 2 -4 363.86 15.20 -9 -2 -4 11.50 6.00 -9 2 4 2.60 5.60 9 2 -4 -0.20 3.20 -9 -2 -4 5.70 5.30 -9 2 4 -0.30 5.50 -9 2 -4 8.50 5.40 -9 -2 4 1.50 6.40 -9 2 -4 10.10 5.00 -9 -2 4 1.10 6.20 -10 2 4 9.20 6.30 -10 -2 -4 24.60 7.70 -10 2 4 14.70 7.10 -10 -2 -4 21.80 6.40 10 -2 -4 13.50 2.80 -10 2 -4 23.70 7.10 -10 -2 4 15.70 7.70 -10 -2 4 27.70 7.40 10 2 4 23.40 4.80 -10 2 -4 15.60 6.00 -11 -2 -4 -4.50 6.60 -11 2 4 5.40 8.50 -11 2 4 -10.50 7.50 -11 -2 -4 5.20 8.40 -11 -2 4 2.70 7.90 -11 2 -4 2.50 6.70 -11 -2 4 -3.90 8.50 -11 2 -4 -5.40 7.10 -12 2 4 23.00 8.70 -12 -2 -4 16.50 9.10 -12 2 4 8.60 9.10 -12 -2 4 19.90 9.70 -12 -2 4 4.00 9.00 -12 2 -4 12.00 8.90 -12 2 -4 10.40 7.80 13 -2 4 -14.40 4.50 -13 2 4 8.20 9.70 -13 -2 -4 -7.80 13.10 -13 2 4 2.40 9.90 13 2 -4 -9.50 7.10 -13 2 -4 3.80 9.90 -13 2 -4 1.90 8.10 -13 -2 4 -7.30 11.00 -14 -2 -4 28.70 17.70 -14 2 4 4.00 11.00 -14 2 4 19.50 10.50 -14 -2 4 3.40 12.30 -14 2 -4 15.10 9.40 -14 2 -4 22.00 11.40 -15 2 4 -0.80 10.00 -15 -2 -4 18.90 17.80 -15 2 4 -5.30 12.00 -15 2 -4 -4.80 12.90 -15 -2 4 -7.70 16.80 -16 -2 -4 19.70 15.20 -16 2 4 0.00 12.30 -16 -2 4 0.80 18.60 -16 2 -4 0.40 17.20 -17 2 4 15.70 16.50 -17 -2 4 23.30 16.00 0 -3 4 0.80 1.10 0 -3 -4 3.50 1.20 0 -3 4 2.60 1.50 0 -3 -4 2.40 1.80 0 3 -4 2.40 1.40 0 3 4 5.40 1.90 1 3 -4 244.68 8.90 -1 3 4 217.98 8.90 -1 -3 -4 228.78 8.70 -1 3 4 238.08 9.10 -1 -3 -4 236.78 9.30 1 -3 4 218.18 8.90 1 -3 -4 231.88 8.50 -1 -3 4 231.58 8.60 -1 3 -4 234.48 8.80 1 -3 -4 251.47 9.20 -1 -3 4 219.78 9.00 1 3 4 233.38 9.20 -2 3 4 2062.49 71.09 2 3 -4 2099.09 70.99 -2 -3 -4 2001.00 70.89 2 -3 4 1905.81 70.99 -2 3 4 1948.21 71.09 2 -3 -4 1964.50 70.69 -2 -3 4 1958.90 70.79 2 -3 -4 2051.59 71.09 2 3 4 2003.00 71.09 -2 3 -4 2045.10 70.89 -2 -3 4 1965.20 71.09 -3 -3 -4 47.50 3.50 -3 3 4 43.10 2.80 -3 3 4 46.60 3.70 -3 3 4 45.50 2.90 3 -3 4 39.50 2.70 3 3 -4 43.50 2.70 -3 -3 -4 44.80 3.40 -3 3 4 37.10 3.00 -3 -3 -4 44.50 3.10 -3 -3 4 45.00 3.60 -3 3 -4 47.00 3.70 -3 3 -4 45.00 3.50 3 -3 -4 41.70 2.20 3 -3 -4 45.90 2.90 -3 -3 4 43.00 3.10 -3 3 -4 45.00 2.40 -3 -3 4 42.30 3.50 3 3 4 45.30 3.10 -3 -3 4 40.20 2.60 4 -3 4 347.07 13.00 -4 3 4 357.56 13.70 4 3 -4 357.66 13.00 -4 3 4 340.77 13.00 -4 3 4 359.26 13.30 -4 -3 -4 360.36 13.40 -4 -3 -4 353.66 13.30 -4 -3 -4 337.47 13.80 4 3 4 361.46 13.30 4 -3 -4 357.46 13.10 4 -3 -4 356.76 12.80 -4 3 -4 344.07 13.10 -4 -3 4 343.27 13.70 -4 -3 4 351.06 13.30 -4 -3 4 362.16 13.00 -4 -3 4 351.36 14.20 -4 3 -4 349.27 12.80 -4 3 -4 356.06 13.50 -5 3 4 197.78 7.40 -5 3 4 194.98 9.00 -5 3 4 185.18 8.40 5 3 -4 199.58 7.60 -5 -3 -4 185.88 8.40 -5 -3 -4 199.38 9.00 -5 -3 4 180.38 9.00 -5 3 -4 186.08 8.30 5 3 4 198.28 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6 27.40 13.30 11 -11 6 -8.50 5.80 11 11 -6 2.60 7.70 -11 11 6 11.30 9.70 -11 11 6 1.30 8.80 -11 11 -6 5.20 8.20 -11 -11 6 0.40 14.00 -11 11 -6 13.70 8.70 -12 11 6 -3.60 10.00 12 -11 6 -4.10 6.10 12 11 -6 -4.50 7.70 -12 11 6 5.70 9.40 -12 11 -6 17.10 9.50 -12 11 -6 -4.10 8.90 -13 11 6 -17.60 9.70 13 11 -6 -5.10 7.80 -13 11 6 20.20 10.50 -13 11 -6 -7.40 8.60 -13 11 -6 31.90 10.60 -14 11 6 -9.90 10.60 -14 11 6 -0.30 11.30 -14 11 -6 -7.00 11.10 -15 11 6 -5.20 11.00 15 -11 -6 2.70 6.50 0 12 6 18.80 5.10 0 12 -6 15.10 5.90 0 12 6 17.30 5.90 0 -12 -6 13.80 4.20 0 -12 6 13.40 4.20 0 12 -6 7.50 5.50 0 12 -6 17.70 4.60 0 12 6 11.90 4.90 1 -12 6 300.37 12.70 1 12 -6 306.37 14.50 -1 12 6 291.67 13.40 1 12 -6 305.37 15.20 1 12 -6 288.17 13.80 -1 12 6 268.87 15.00 -1 12 6 280.87 14.00 -1 -12 -6 301.87 12.70 -1 12 -6 297.17 13.50 1 12 6 281.07 13.70 1 12 6 284.97 14.20 -1 -12 6 292.07 12.80 1 12 6 298.37 15.00 1 -12 -6 295.07 12.50 -1 12 -6 311.07 14.00 -1 12 -6 289.27 15.40 2 12 -6 14.50 4.70 2 12 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3.20 3.50 4 -7 10 1.40 3.00 4 7 -10 4.40 2.70 -4 -7 -10 -2.30 2.80 4 -7 10 3.30 3.20 4 7 -10 1.20 2.70 -4 7 -10 -1.10 2.10 -4 7 -10 -1.10 4.50 -4 -7 10 2.20 3.50 -4 7 -10 1.00 2.30 -4 7 -10 0.10 3.60 4 7 10 -1.70 2.60 -4 -7 10 4.40 2.50 -4 -7 10 7.90 5.10 -4 7 -10 2.00 3.20 4 -7 -10 2.10 3.20 4 7 10 -1.10 3.30 4 -7 -10 3.00 1.90 -5 -7 -10 6.80 4.20 -5 7 10 7.50 3.40 -5 7 10 7.80 4.20 5 -7 10 4.90 2.90 5 7 -10 5.30 2.90 -5 7 10 6.50 3.20 5 -7 -10 4.80 2.00 -5 -7 10 8.30 2.90 -5 -7 10 1.60 5.80 5 7 10 9.60 3.60 -5 7 -10 10.30 3.30 -5 7 -10 6.30 2.50 -5 7 -10 7.70 2.40 5 7 10 8.90 2.80 -5 7 -10 6.70 4.00 -5 -7 10 9.20 3.90 5 -7 -10 1.80 3.20 -6 7 10 234.98 11.20 -6 7 10 203.48 9.90 6 7 -10 204.68 10.20 -6 7 -10 205.48 9.20 -6 7 -10 211.38 10.40 -6 -7 10 204.98 12.80 6 -7 -10 213.68 8.40 -6 7 -10 216.88 9.20 6 7 10 215.08 9.40 6 7 10 217.08 10.30 -6 -7 10 214.38 9.20 -6 7 -10 220.88 9.60 -7 7 10 66.19 6.00 -7 7 10 59.39 5.70 -7 7 10 52.79 6.40 7 7 -10 43.20 5.50 -7 7 -10 46.60 5.60 -7 7 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9.10 10 -5 -28 11.60 10.70 -10 -5 28 -1.10 13.20 -11 5 28 26.70 10.10 11 -5 28 3.50 6.80 11 5 -28 9.40 10.50 -11 5 28 -0.30 9.70 11 -5 -28 2.90 11.00 -11 -5 28 -10.40 15.10 -12 5 28 26.10 10.30 -12 5 28 6.60 10.60 12 5 -28 4.50 9.80 12 -5 28 3.40 6.90 12 -5 -28 -0.50 10.70 -12 -5 28 5.20 14.80 13 5 -28 2.10 9.60 13 -5 28 -2.90 6.40 -13 5 28 -15.40 9.10 -13 -5 28 5.60 14.10 -14 5 28 3.80 8.90 14 5 -28 -9.80 8.10 -14 -5 28 6.90 12.30 0 6 28 473.95 18.70 0 -6 -28 501.05 22.10 0 6 -28 514.85 23.30 0 6 -28 493.65 21.80 0 6 28 481.25 21.40 0 -6 -28 523.85 26.10 0 -6 28 509.95 19.60 1 6 -28 7.40 6.40 1 6 -28 5.30 7.70 1 -6 28 4.70 4.50 -1 6 28 4.20 3.30 1 6 -28 -1.70 6.80 -1 -6 -28 -6.70 6.80 -1 -6 28 6.10 3.90 1 -6 -28 -4.50 6.70 -1 6 -28 2.10 6.50 -1 6 -28 3.70 7.80 2 6 -28 65.59 8.40 -2 6 28 67.29 5.50 2 6 -28 83.49 9.50 -2 -6 -28 83.79 9.10 2 -6 28 75.89 6.40 -2 6 28 81.79 5.80 -2 6 -28 60.89 9.60 -2 -6 28 67.89 5.20 -2 6 -28 76.89 7.30 2 -6 -28 62.09 8.30 3 6 -28 6.80 7.50 -3 6 28 6.30 4.50 3 6 -28 5.30 7.00 3 -6 28 8.10 5.30 -3 -6 -28 3.40 7.30 -3 6 28 9.30 3.80 -3 6 -28 8.80 8.50 -3 -6 28 5.70 3.50 3 -6 -28 8.60 7.30 -4 6 28 80.09 6.70 4 6 -28 79.09 9.40 -4 -6 -28 82.59 9.60 -4 6 28 60.59 5.70 -4 -6 28 49.20 6.50 4 -6 -28 69.39 8.90 -4 6 -28 52.99 10.30 -5 6 28 9.70 5.60 -5 6 28 9.70 5.30 -5 -6 -28 24.80 8.40 5 6 -28 20.30 8.40 5 -6 -28 3.00 7.80 -5 -6 28 21.80 6.80 -5 6 -28 12.80 9.50 -6 -6 -28 75.09 9.80 -6 6 28 84.79 8.40 -6 6 28 69.69 7.50 6 6 -28 59.89 9.40 -6 6 -28 53.99 11.20 -6 -6 28 79.09 9.10 6 -6 -28 58.79 9.50 -7 -6 -28 13.30 8.80 7 6 -28 21.50 8.50 -7 6 28 12.40 7.10 -7 6 28 -1.10 7.30 -7 6 -28 18.10 10.70 7 -6 -28 14.90 8.80 -7 -6 28 15.30 9.00 -8 6 28 4.20 7.90 -8 -6 -28 3.60 8.90 -8 6 28 -4.80 7.10 8 6 -28 1.00 8.20 8 -6 -28 -5.40 8.60 -8 6 -28 -9.40 10.70 -8 -6 28 -4.20 10.10 -9 6 28 0.40 7.90 -9 6 28 16.10 8.90 -9 -6 28 -16.70 12.30 9 -6 -28 8.60 8.90 10 6 -28 10.80 10.50 10 -6 28 1.60 6.90 -10 6 28 2.00 9.10 -10 6 28 -21.70 8.90 -10 -6 28 22.20 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13.30 8.90 3 -7 -28 18.40 7.80 -3 7 -28 -2.90 5.70 -3 -7 28 11.10 3.80 -4 7 28 4.80 5.10 -4 -7 -28 5.20 7.90 4 -7 28 6.60 5.90 4 7 -28 7.60 7.90 4 7 -28 9.00 8.00 -4 7 28 6.20 4.80 -4 7 -28 -9.20 8.70 4 -7 -28 4.50 7.70 5 -7 28 13.50 6.20 -5 -7 -28 9.10 8.20 5 7 -28 14.50 8.10 5 7 -28 11.80 9.00 -5 7 28 7.80 5.30 -5 7 28 15.20 5.90 -5 -7 28 25.20 6.90 5 -7 -28 19.40 8.20 -5 7 -28 13.70 9.90 -6 -7 -28 11.30 8.70 6 7 -28 1.90 8.10 6 7 -28 5.70 9.10 -6 7 28 4.30 6.20 -6 7 28 12.20 6.90 6 -7 28 11.20 6.70 -6 -7 28 14.40 7.80 6 -7 -28 -0.10 8.40 -6 7 -28 2.50 10.00 -7 7 28 -0.70 6.60 -7 7 28 14.40 7.80 7 7 -28 -6.50 7.60 7 -7 28 -0.40 6.70 7 7 -28 -5.30 9.80 -7 -7 -28 10.60 8.90 7 -7 -28 3.70 9.00 -7 7 -28 9.20 10.70 -7 -7 28 4.20 8.50 8 7 -28 -9.20 10.50 -8 7 28 1.90 7.30 -8 7 28 1.70 8.60 8 -7 28 2.50 6.90 8 -7 -28 14.00 8.90 -8 -7 28 -10.80 9.80 -9 7 28 -1.90 9.20 -9 7 28 14.20 8.00 9 -7 28 -9.00 7.00 9 7 -28 7.80 11.00 9 -7 -28 -0.20 9.20 -9 -7 28 17.90 12.00 -10 7 28 -7.90 9.20 -10 7 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8 -28 33.40 4.70 -3 -8 28 23.90 4.60 -3 8 -28 30.80 6.20 -3 8 -28 21.70 9.50 3 -8 -28 43.30 8.40 -4 8 28 16.20 5.50 -4 -8 -28 25.30 8.40 4 -8 28 15.40 6.50 4 8 -28 17.20 8.60 -4 8 28 11.50 5.10 4 8 -28 16.40 8.90 4 -8 -28 19.20 8.20 -4 8 -28 6.70 9.40 -5 8 28 2.30 5.70 -5 8 28 9.50 5.90 5 -8 28 0.00 6.30 5 8 -28 7.10 8.40 -5 -8 -28 14.70 8.90 5 8 -28 8.90 9.50 -5 8 -28 -6.00 9.50 5 -8 -28 -1.30 8.00 -6 8 28 4.50 6.20 -6 -8 -28 -4.60 8.20 -6 8 28 17.00 6.70 6 8 -28 -8.60 9.70 6 8 -28 1.50 8.20 6 -8 28 0.60 6.90 -6 -8 28 5.40 7.50 -6 8 -28 7.40 10.40 6 -8 -28 4.80 8.60 7 -8 28 -11.00 6.90 7 8 -28 11.10 10.50 -7 8 28 3.30 7.10 -7 -8 -28 16.00 9.30 7 8 -28 10.80 8.30 -7 8 28 -3.90 6.90 -7 -8 28 0.40 8.60 -7 8 -28 -7.00 10.90 7 -8 -28 6.10 8.80 -8 8 28 6.20 7.60 8 -8 28 -2.70 7.00 -8 8 28 2.20 8.40 8 8 -28 1.70 10.70 -8 -8 28 -15.80 9.50 8 -8 -28 -20.00 8.50 9 -8 28 -8.00 7.00 -9 8 28 9.70 8.20 9 8 -28 -18.00 10.50 -9 8 28 -7.70 9.20 9 -8 -28 -5.00 8.80 -9 -8 28 -11.10 10.90 10 -8 28 11.10 7.20 -10 8 28 13.90 8.30 10 8 -28 18.60 11.70 -10 8 28 5.70 9.40 10 -8 -28 5.60 8.70 -10 -8 28 11.00 11.30 11 -8 28 0.10 6.90 11 8 -28 -12.30 10.60 -11 8 28 -26.10 10.20 -11 8 28 2.50 9.30 -11 -8 28 6.30 12.00 11 -8 -28 -5.10 10.60 -12 8 28 -14.80 9.10 12 8 -28 9.00 11.00 12 -8 28 -3.60 6.40 -12 -8 28 12.80 11.90 12 -8 -28 -0.30 10.90 13 8 -28 14.00 10.00 -13 8 28 -7.90 9.00 13 -8 -28 5.00 11.00 -13 -8 28 8.30 11.80 0 -9 -28 2.20 7.50 0 9 -28 -9.40 8.30 0 9 28 3.60 3.40 0 -9 28 -5.20 5.20 0 9 -28 -6.10 8.10 1 -9 28 5.40 5.30 1 9 -28 8.40 8.80 1 9 -28 -16.40 9.00 -1 -9 -28 17.30 8.00 -1 9 28 2.50 3.70 -1 -9 28 8.10 5.10 -1 9 -28 8.90 9.00 1 9 28 7.00 3.50 1 -9 -28 0.40 7.40 -1 9 -28 3.40 6.70 -2 -9 -28 0.20 7.50 2 9 -28 8.90 8.60 -2 9 28 3.00 3.50 -2 9 28 -0.10 3.90 2 -9 28 1.40 5.50 2 9 -28 2.50 8.50 -2 9 -28 -0.50 6.50 -2 9 -28 0.00 8.70 2 -9 -28 8.20 7.90 2 9 28 4.70 3.30 -2 -9 28 7.00 4.50 -3 9 28 -0.50 4.10 3 9 -28 3.90 9.00 3 9 -28 20.00 8.90 -3 -9 -28 -0.60 7.80 3 -9 28 7.30 6.00 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11.90 4.90 -3 10 -28 14.30 6.60 -3 10 -28 24.00 5.60 3 10 28 15.50 4.10 3 -10 -28 3.10 8.30 -3 10 -28 5.30 9.60 -4 10 28 4.30 5.40 4 10 -28 5.40 8.70 -4 -10 -28 3.90 8.40 4 -10 28 -4.50 6.90 -4 10 28 3.50 5.60 4 10 -28 -4.80 9.50 -4 10 -28 -19.80 6.00 4 -10 -28 7.50 8.50 -4 -10 28 2.80 4.70 -4 10 -28 -12.80 9.50 -5 10 28 2.10 6.50 5 -10 28 -6.40 7.00 5 10 -28 7.10 8.60 -5 10 28 -3.70 6.20 5 10 -28 -3.60 10.10 -5 -10 -28 -4.70 8.60 -5 10 -28 5.90 10.10 5 -10 -28 -5.90 8.30 -6 10 28 6.90 7.00 6 10 -28 7.70 10.90 -6 -10 -28 9.00 8.70 6 -10 28 -5.90 7.20 -6 10 28 -2.50 6.40 6 10 -28 -8.40 8.30 6 -10 -28 3.90 8.80 -6 10 -28 -4.20 11.00 -7 10 28 1.70 7.00 -7 10 28 0.50 7.60 7 10 -28 -4.20 11.00 7 -10 28 1.20 7.40 7 -10 -28 4.10 9.10 -8 10 28 -1.00 8.70 8 10 -28 -3.40 11.60 -8 10 28 -1.90 7.90 8 -10 28 0.90 7.50 8 -10 -28 2.70 9.00 9 10 -28 16.20 11.60 -9 10 28 34.80 8.60 9 -10 28 30.30 8.10 -9 10 28 38.20 9.50 9 -10 -28 28.00 9.60 10 -10 28 1.90 7.10 -10 10 28 -12.50 8.50 -10 10 28 8.70 9.70 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0.0246 14 6 13 5.0597 0.0021 14 6 14 2.4353 -0.0670 14 6 15 -5.5070 0.0023 14 6 16 0.9210 0.0539 14 6 17 2.1235 -0.0196 14 6 18 -2.8235 -0.0192 14 6 19 1.4847 -0.0058 14 6 20 1.6091 0.0268 14 6 21 -2.5738 0.0591 14 6 22 -0.2970 -0.0533 14 6 23 2.0489 -0.0812 14 6 24 0.6757 0.0538 14 7 1 -5.2342 0.1111 14 7 2 -0.0035 -0.0852 14 7 3 2.7413 -0.0484 14 7 4 1.1765 0.1127 14 7 5 -0.2074 -0.0118 14 7 6 -2.8786 -0.1186 14 7 7 -0.4019 0.0200 14 7 8 4.5048 0.1431 14 7 9 -0.2996 -0.0330 14 7 10 -5.5957 -0.1927 14 7 11 0.4418 0.1029 14 7 12 4.0786 0.1938 14 7 13 0.3408 -0.1390 14 7 14 0.6095 -0.1230 14 7 15 -0.6023 0.0634 14 7 16 -4.1402 0.0715 14 7 17 -0.3548 0.0279 14 7 18 2.7521 -0.0967 14 7 19 1.0540 -0.0256 14 7 20 0.6434 0.1261 14 7 21 -0.0371 -0.0202 14 7 22 -1.3607 -0.0858 14 7 23 -1.7347 0.0277 14 7 24 0.0009 0.0201 14 8 0 -1.9779 -0.0743 14 8 1 -0.1238 0.0234 14 8 2 3.2208 0.1392 14 8 3 0.6947 -0.1152 14 8 4 -4.7427 -0.1790 14 8 5 -1.5122 0.1491 14 8 6 3.7033 0.1926 14 8 7 2.2486 -0.1259 14 8 8 -1.4245 -0.1998 14 8 9 -3.4255 0.1243 14 8 10 0.8502 0.1738 14 8 11 4.5222 -0.1803 14 8 12 -1.3368 -0.0830 14 8 13 -3.2719 0.2277 14 8 14 0.3499 -0.0163 14 8 15 -0.2588 -0.2068 14 8 16 1.3070 0.0433 14 8 17 2.0357 0.1569 14 8 18 -0.8724 -0.0252 14 8 19 0.2583 -0.1256 14 8 20 -1.1469 0.0422 14 8 21 -3.1895 0.0774 14 8 22 1.9019 -0.0837 14 9 1 1.3383 -0.0315 14 9 2 1.8392 0.1655 14 9 3 -0.6666 0.0813 14 9 4 -1.1903 -0.1934 14 9 5 0.9290 -0.1080 14 9 6 0.4093 0.1669 14 9 7 -1.9511 0.0634 14 9 8 -1.8803 -0.0677 14 9 9 2.3068 -0.0235 14 9 10 3.5121 -0.0295 14 9 11 -2.1902 0.0670 14 9 12 -2.8651 0.0523 14 9 13 2.2667 -0.1077 14 9 14 0.7519 -0.0297 14 9 15 -1.6857 0.0468 14 9 16 1.4185 0.0315 14 9 17 0.1104 0.0364 14 9 18 -2.9910 -0.0505 14 9 19 0.9562 -0.0405 14 9 20 2.4761 0.0323 14 9 21 -0.8803 0.0288 14 10 0 0.2578 0.0011 14 10 1 -0.9886 -0.1240 14 10 2 -1.7755 0.0100 14 10 3 2.7430 0.0614 14 10 4 3.4489 0.0329 14 10 5 -2.9137 -0.0407 14 10 6 -1.4984 -0.1216 14 10 7 0.8809 0.0434 14 10 8 -2.2619 0.1548 14 10 9 0.5830 -0.0095 14 10 10 2.9110 -0.0775 14 10 11 0.7787 -0.0874 14 10 12 0.2428 -0.0187 14 10 13 -2.6122 0.1810 14 10 14 -2.8250 0.0407 14 10 15 2.1090 -0.1974 14 10 16 1.8048 -0.0367 14 10 17 -0.4640 0.1691 14 10 18 0.6607 0.0788 14 10 19 -0.4474 -0.1688 14 10 20 -1.1162 -0.1232 14 11 1 -4.9101 0.0793 14 11 2 3.2212 -0.0367 14 11 3 2.6783 -0.0821 14 11 4 -1.1998 -0.0654 14 11 5 -0.1973 0.0794 14 11 6 -3.2336 0.1357 14 11 7 -1.1520 -0.1307 14 11 8 3.7524 -0.1045 14 11 9 1.3042 0.1728 14 11 10 0.1034 0.0300 14 11 11 0.0121 -0.1173 14 11 12 -3.1744 -0.0285 14 11 13 -2.5464 0.0332 14 11 14 2.4924 0.1101 14 11 15 3.4230 -0.0218 14 11 16 -0.1893 -0.1727 14 11 17 -0.0629 0.0199 14 11 18 -0.8471 0.1566 14 12 0 -0.4155 -0.1587 14 12 1 -0.6182 -0.0125 14 12 2 1.6755 0.1309 14 12 3 -0.3131 0.0059 14 12 4 -2.6970 -0.0322 14 12 5 3.8254 -0.0007 14 12 6 0.6148 -0.1040 14 12 7 -5.0553 0.0380 14 12 8 1.6777 0.1672 14 12 9 1.7954 -0.0866 14 12 10 -0.3073 -0.1131 14 12 11 1.0933 0.1008 14 12 12 -2.9853 0.0471 14 12 13 0.8141 -0.1118 14 12 14 3.7256 -0.0507 14 12 15 -3.9638 0.1655 14 12 16 -1.2380 0.0488 14 13 1 2.2338 -0.1167 14 13 2 0.9647 -0.1605 14 13 3 -1.8276 0.2071 14 13 4 -1.6901 0.0777 14 13 5 -0.9987 -0.2595 14 13 6 0.8819 0.0124 14 13 7 4.7773 0.2007 14 13 8 1.1311 -0.0451 14 13 9 -5.1587 -0.1029 14 13 10 -1.9947 0.0523 14 13 11 1.8218 0.0789 14 13 12 1.2222 -0.1096 14 13 13 0.7753 -0.0951 14 14 0 4.1241 -0.0403 14 14 1 -0.4928 -0.2584 14 14 2 -2.8261 0.1014 14 14 3 0.7138 0.1575 14 14 4 0.6090 -0.0859 14 14 5 0.1668 -0.1113 14 14 6 0.2057 -0.0051 14 14 7 -0.8407 0.1396 14 14 8 0.5852 0.0585 14 14 9 0.6040 -0.1301 15 0 1 -9.2805 -0.1029 15 0 3 9.5838 0.1282 15 0 5 -4.9130 -0.1477 15 0 7 -1.6026 0.1503 15 0 9 1.1254 -0.1247 15 0 11 4.7592 0.0779 15 0 13 -5.9474 -0.0407 15 0 15 0.8160 0.0280 15 0 17 2.7499 -0.0160 15 0 19 -1.6266 -0.0139 15 0 21 0.2655 0.0465 15 1 0 -0.4276 0.0545 15 1 1 -1.9425 -0.0241 15 1 2 0.5460 -0.0352 15 1 3 2.7352 0.0589 15 1 4 -0.5138 0.0657 15 1 5 0.6319 -0.1114 15 1 6 0.3824 -0.0767 15 1 7 -3.3312 0.1306 15 1 8 -1.4604 0.0251 15 1 9 3.1006 -0.1096 15 1 10 3.9898 0.0317 15 1 11 -1.3239 0.1017 15 1 12 -5.3292 -0.0447 15 1 13 -1.3854 -0.1410 15 1 14 2.9554 0.0501 15 1 15 3.7849 0.1793 15 1 16 1.3289 -0.0777 15 1 17 -2.7726 -0.1566 15 1 18 -3.0137 0.0941 15 1 19 -1.3212 0.0961 15 1 20 0.9906 -0.0833 15 1 21 3.7609 -0.0589 15 2 1 3.7089 -0.0141 15 2 2 0.7340 -0.0819 15 2 3 -2.3109 -0.0234 15 2 4 -0.4230 0.0396 15 2 5 1.5399 0.0593 15 2 6 0.5614 0.0137 15 2 7 -0.9898 -0.0768 15 2 8 -1.3428 -0.0492 15 2 9 -1.1212 0.0758 15 2 10 0.8582 0.0572 15 2 11 2.9948 -0.0641 15 2 12 -0.0435 -0.0602 15 2 13 -1.2285 0.0539 15 2 14 1.4938 0.0567 15 2 15 -2.6950 -0.0519 15 2 16 -3.1750 -0.0336 15 2 17 3.6682 0.0533 15 2 18 1.0075 0.0218 15 2 19 -0.5843 -0.0485 15 2 20 3.3023 -0.0479 15 2 21 -2.4140 0.0325 15 3 0 2.6545 -0.1049 15 3 1 -0.8785 0.0422 15 3 2 -1.6324 0.0857 15 3 3 1.6521 0.0159 15 3 4 0.9660 -0.0539 15 3 5 -1.9274 -0.0356 15 3 6 -2.4142 0.0395 15 3 7 3.5902 0.0235 15 3 8 2.4946 -0.0641 15 3 9 -4.4012 -0.0229 15 3 10 0.8303 0.0876 15 3 11 0.6581 0.0753 15 3 12 -3.3422 -0.0678 15 3 13 5.2945 -0.1599 15 3 14 1.6803 0.0321 15 3 15 -6.9088 0.1960 15 3 16 1.0684 -0.0246 15 3 17 2.3682 -0.1513 15 3 18 -1.2648 0.0277 15 3 19 3.5257 0.0961 15 3 20 0.2238 -0.0015 15 3 21 -5.8295 -0.0911 15 4 1 1.3877 -0.1064 15 4 2 1.7885 0.1002 15 4 3 -0.9799 0.1223 15 4 4 -1.0899 -0.0564 15 4 5 0.8234 -0.1427 15 4 6 -0.2719 0.0363 15 4 7 -2.1944 0.1360 15 4 8 0.2300 0.0137 15 4 9 4.7855 -0.1237 15 4 10 0.3063 -0.0835 15 4 11 -5.6505 0.1423 15 4 12 -0.5947 0.1078 15 4 13 2.8947 -0.1528 15 4 14 0.9278 -0.1050 15 4 15 1.0979 0.1019 15 4 16 -0.3385 0.1488 15 4 17 -2.6926 -0.0259 15 4 18 -1.2742 -0.2121 15 4 19 1.6357 -0.0102 15 4 20 1.0328 0.2027 15 5 0 0.5657 0.1201 15 5 1 -0.2401 -0.0344 15 5 2 0.2569 -0.1359 15 5 3 -0.2633 -0.0074 15 5 4 -0.1726 0.1451 15 5 5 1.9218 0.0195 15 5 6 -2.2024 -0.1422 15 5 7 -2.1017 0.0029 15 5 8 2.3445 0.1275 15 5 9 -0.8131 -0.0083 15 5 10 1.5997 -0.1226 15 5 11 3.8764 -0.0247 15 5 12 -3.8158 0.1452 15 5 13 -3.0656 0.0551 15 5 14 0.5970 -0.1670 15 5 15 -0.5663 -0.0568 15 5 16 3.2290 0.1447 15 5 17 2.5216 0.0504 15 5 18 -2.7263 -0.0874 15 5 19 -1.7434 -0.0458 15 6 1 1.0896 0.0978 15 6 2 1.0630 -0.1710 15 6 3 -0.0354 -0.1230 15 6 4 0.4124 0.1333 15 6 5 -0.5168 0.1065 15 6 6 -2.5198 -0.1167 15 6 7 -0.7858 -0.0673 15 6 8 1.9501 0.1614 15 6 9 2.4043 0.0301 15 6 10 1.1813 -0.2068 15 6 11 -1.1587 0.0004 15 6 12 -3.9186 0.1675 15 6 13 -2.3487 -0.0052 15 6 14 3.9411 -0.0906 15 6 15 3.3385 -0.0253 15 6 16 -1.4561 0.0847 15 6 17 -0.0903 0.0559 15 6 18 -1.1061 -0.1227 15 6 19 -3.0277 -0.0622 15 7 0 6.1807 -0.0928 15 7 1 1.0907 -0.0255 15 7 2 -2.8433 0.1256 15 7 3 -1.2015 -0.0050 15 7 4 -2.3993 -0.1284 15 7 5 -0.7334 0.0392 15 7 6 2.4756 0.1284 15 7 7 0.6602 -0.0571 15 7 8 1.7786 -0.1387 15 7 9 1.5875 0.0885 15 7 10 -3.8840 0.1397 15 7 11 -2.5175 -0.1328 15 7 12 1.4420 -0.0996 15 7 13 1.4024 0.1373 15 7 14 1.7605 0.0317 15 7 15 -0.0195 -0.1011 15 7 16 -2.1890 0.0047 15 7 17 -1.0915 0.0937 15 8 1 -6.8715 -0.0664 15 8 2 3.3185 0.1882 15 8 3 6.8517 0.1203 15 8 4 -1.2666 -0.2418 15 8 5 -5.9878 -0.1295 15 8 6 -2.9237 0.2349 15 8 7 3.3003 0.0889 15 8 8 3.2315 -0.1241 15 8 9 0.2914 -0.0388 15 8 10 -0.6733 -0.0149 15 8 11 -2.1743 0.0299 15 8 12 0.4647 0.0553 15 8 13 1.8242 -0.0539 15 8 14 -2.5531 0.0012 15 8 15 -1.5579 0.0598 15 8 16 2.4810 -0.0424 15 9 0 -5.1554 -0.0351 15 9 1 0.5954 0.0098 15 9 2 4.0415 -0.0630 15 9 3 -1.2652 -0.0398 15 9 4 -2.7262 0.1467 15 9 5 0.6071 0.0675 15 9 6 3.0549 -0.1823 15 9 7 1.3476 -0.0683 15 9 8 -3.0046 0.1708 15 9 9 -3.1776 0.0627 15 9 10 1.2587 -0.1282 15 9 11 2.9916 -0.0931 15 9 12 -0.1202 0.0899 15 9 13 -0.9567 0.1357 15 9 14 0.6480 -0.0729 15 10 1 6.0839 -0.0184 15 10 2 -1.5629 -0.0400 15 10 3 -8.4567 0.0390 15 10 4 2.9393 -0.0530 15 10 5 6.0989 -0.0382 15 10 6 -3.3138 0.1432 15 10 7 1.6508 0.0203 15 10 8 1.5546 -0.1587 15 10 9 -6.6405 -0.0089 15 10 10 1.3387 0.1269 15 10 11 4.5307 0.0084 15 10 12 -1.9454 -0.1677 15 11 0 7.1467 -0.0480 15 11 1 -1.0357 -0.1078 15 11 2 -5.0187 0.0768 15 11 3 0.9726 0.0848 15 11 4 0.5292 -0.0504 15 11 5 1.9413 -0.0791 15 11 6 2.5132 -0.0186 15 11 7 -3.8244 0.1116 15 11 8 -2.3057 0.0589 16 0 0 7.8799 0.0455 16 0 2 -6.6203 -0.0619 16 0 4 4.6894 0.0605 16 0 6 -3.2366 -0.0519 16 0 8 0.0506 0.0450 16 0 10 4.3182 -0.0478 16 0 12 -5.3200 0.0482 16 0 14 2.2213 -0.0234 16 1 1 1.1276 -0.0754 16 1 2 -0.2939 0.0165 16 1 3 -0.4443 0.0415 16 1 4 -0.8151 0.0221 16 1 5 -1.7446 -0.0280 16 1 6 1.7098 -0.0610 16 1 7 3.3118 -0.0001 16 1 8 -0.3262 0.0567 16 1 9 -1.7078 0.0434 16 1 10 -1.7819 -0.0314 16 1 11 -1.1623 -0.0718 16 1 12 1.4659 0.0284 16 1 13 2.2064 0.0832 16 1 14 0.5137 -0.0511 16 2 0 2.6378 0.0845 16 2 1 0.6541 0.1133 16 2 2 -0.0625 -0.0620 16 2 3 -1.7821 -0.0797 16 2 4 -2.7803 0.0272 16 2 5 1.1591 0.0593 16 2 6 0.6031 -0.0094 16 2 7 2.4009 -0.0369 16 2 8 2.5606 0.0121 16 2 9 -5.5678 0.0161 16 2 10 -1.4190 -0.0225 16 2 11 3.7375 -0.0068 16 2 12 -1.5203 0.0269 16 2 13 1.1550 -0.0032 16 3 1 -0.7239 -0.0250 16 3 2 0.4853 0.0871 16 3 3 -0.6833 0.0407 16 3 4 0.2252 -0.0276 16 3 5 0.7518 -0.0422 16 3 6 -1.8220 -0.0126 16 3 7 -0.9856 0.0409 16 3 8 2.0727 0.0494 16 3 9 3.9562 -0.0706 16 3 10 0.9000 -0.0890 16 3 11 -5.9385 0.1285 16 3 12 -5.4811 0.1031 16 3 13 2.7188 -0.1502 16 4 0 -0.6610 0.0270 16 4 1 0.7437 -0.0445 16 4 2 2.6043 -0.0404 16 4 3 -1.3713 -0.0060 16 4 4 -4.8487 0.0288 16 4 5 0.4874 0.0352 16 4 6 2.8922 -0.0033 16 4 7 0.8481 -0.0409 16 4 8 0.8643 -0.0057 16 4 9 -1.2165 0.0436 16 4 10 -1.2555 -0.0266 16 4 11 0.0831 -0.0565 16 4 12 -0.9649 0.0792 16 5 1 1.3855 0.0369 16 5 2 -0.5498 -0.0376 16 5 3 -4.2408 0.0056 16 5 4 0.3524 0.0362 16 5 5 3.7001 -0.0135 16 5 6 0.5392 -0.0622 16 5 7 1.3025 -0.0080 16 5 8 -0.5918 0.0909 16 5 9 -4.9155 0.0128 16 5 10 -1.7644 -0.1107 16 6 0 0.5682 0.0378 16 6 1 1.0783 -0.0582 16 6 2 -1.0141 -0.0054 16 6 3 -2.6498 0.0558 16 6 4 1.0843 -0.0176 16 6 5 2.9564 -0.0574 16 6 6 -0.2228 0.0217 16 6 7 -2.0217 0.0350 16 6 8 0.5141 -0.0276 16 6 9 0.1007 0.0103 16 7 1 -2.7791 0.0277 16 7 2 -1.6680 0.0762 16 7 3 2.5889 -0.0129 16 7 4 3.9983 -0.1174 16 7 5 -2.7301 0.0310 16 7 6 -4.0490 0.1318 0 0 0 0.0 0.0 ; _shelx_fab_checksum 67979 _olex2_submission_special_instructions 'No special instructions were received' _site XU loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x+1/2, y, -z+1/2' 'x, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x-1/2, -y, z-1/2' '-x, y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.4851(2) 0.51909(10) 0.23428(4) 0.1674(12) Uani 1 1 d D U . . . O1 O 0.6171(4) 0.5341(2) 0.42419(13) 0.0632(14) Uani 1 1 d . . . . . O2 O 0.4546(3) 0.6160(2) 0.53706(11) 0.0501(12) Uani 1 1 d . . . . . O3 O 0.7096(3) 0.9720(2) 0.53894(13) 0.0568(13) Uani 1 1 d . . . . . O4 O 0.5050(4) 0.9166(2) 0.42921(11) 0.0546(13) Uani 1 1 d . . . . . O5 O 0.583(4) 0.456(3) 0.257(3) 0.306(8) Uani 0.093(14) 1 d D U P A -1 O6 O 0.6396(19) 0.539(3) 0.238(3) 0.306(8) Uani 0.093(14) 1 d D U P A -1 O7 O 0.5097(9) 0.5866(4) 0.2132(2) 0.1861(16) Uani 1 1 d D U . . . O8 O 0.3574(9) 0.5965(5) 0.2047(3) 0.216(3) Uani 1 1 d D U . . . O9B O 0.349(2) 0.4565(15) 0.2433(7) 0.167(10) Uani 0.289(15) 1 d D U P A 1 H9BA H 0.310713 0.461971 0.259655 0.250 Uiso 0.289(15) 1 d DR U P A 1 H9BB H 0.355953 0.418471 0.242215 0.250 Uiso 0.289(15) 1 d DR U P A 1 N1 N 0.4641(9) 0.5650(5) 0.2755(2) 0.134(3) Uani 1 1 d . U . . . N2 N 0.4830(11) 0.9734(4) 0.6941(2) 0.126(4) Uani 1 1 d . . . . . C1 C 0.5168(11) 0.6111(6) 0.2815(3) 0.139(4) Uani 1 1 d . U . . . H1 H 0.565513 0.622944 0.266813 0.167 Uiso 1 1 calc R U . . . C2 C 0.5014(10) 0.6431(5) 0.3099(2) 0.123(3) Uani 1 1 d . U . . . H2 H 0.543730 0.674842 0.314711 0.148 Uiso 1 1 calc R U . . . C3 C 0.4308(9) 0.6313(4) 0.3301(2) 0.095(3) Uani 1 1 d . U . . . C4 C 0.3859(11) 0.5790(6) 0.3244(3) 0.130(3) Uani 1 1 d . U . . . H4 H 0.342229 0.563905 0.339921 0.156 Uiso 1 1 calc R U . . . C5 C 0.4022(12) 0.5475(6) 0.2966(3) 0.143(4) Uani 1 1 d . U . . . H5 H 0.367222 0.512141 0.292929 0.172 Uiso 1 1 calc R U . . . C6 C 0.4138(6) 0.6642(3) 0.36056(16) 0.0552(19) Uani 1 1 d . . . . . C7 C 0.4870(6) 0.6999(3) 0.37295(17) 0.062(2) Uani 1 1 d . . . . . H7 H 0.544538 0.706322 0.361005 0.074 Uiso 1 1 calc R U . . . C8 C 0.4746(5) 0.7265(3) 0.40346(16) 0.0500(18) Uani 1 1 d . . . . . H8 H 0.523959 0.751116 0.411899 0.060 Uiso 1 1 calc R U . . . C9 C 0.3907(5) 0.7170(3) 0.42131(14) 0.0376(14) Uani 1 1 d . . . . . C10 C 0.3190(5) 0.6844(3) 0.40768(15) 0.0434(16) Uani 1 1 d . . . . . H10 H 0.259721 0.680049 0.418913 0.052 Uiso 1 1 calc R U . . . C11 C 0.3297(6) 0.6572(3) 0.37770(16) 0.0519(18) Uani 1 1 d . . . . . H11 H 0.278816 0.633914 0.369177 0.062 Uiso 1 1 calc R U . . . C12 C 0.3849(4) 0.7434(2) 0.45411(14) 0.0329(13) Uani 1 1 d . . . . . C13 C 0.3698(4) 0.7095(2) 0.48166(14) 0.0318(13) Uani 1 1 d . . . . . C14 C 0.3733(4) 0.7374(3) 0.51151(14) 0.0342(14) Uani 1 1 d . . . . . H14 H 0.366408 0.714232 0.530404 0.041 Uiso 1 1 calc R U . . . C15 C 0.3868(4) 0.7986(2) 0.51476(14) 0.0336(13) Uani 1 1 d . . . . . C16 C 0.3973(4) 0.8323(2) 0.48685(14) 0.0342(13) Uani 1 1 d . . . . . C17 C 0.3969(4) 0.8041(2) 0.45719(14) 0.0340(13) Uani 1 1 d . . . . . H17 H 0.405000 0.827058 0.438277 0.041 Uiso 1 1 calc R U . . . C18 C 0.4093(4) 0.8993(2) 0.48761(16) 0.0381(14) Uani 1 1 d . . . . . H18A H 0.373146 0.916510 0.469336 0.046 Uiso 1 1 calc R U . . . H18B H 0.380225 0.914592 0.507698 0.046 Uiso 1 1 calc R U . . . C19 C 0.5130(4) 0.9200(2) 0.48579(15) 0.0375(14) Uani 1 1 d . . . . . C20 C 0.5578(5) 0.9305(3) 0.45636(16) 0.0408(15) Uani 1 1 d . . . . . C21 C 0.6492(5) 0.9553(3) 0.45509(17) 0.0451(16) Uani 1 1 d . . . . . H21 H 0.678264 0.962782 0.434788 0.054 Uiso 1 1 calc R U . . . C22 C 0.6980(5) 0.9693(3) 0.48270(18) 0.0454(17) Uani 1 1 d . . . . . C23 C 0.6553(5) 0.9567(3) 0.51235(18) 0.0458(17) Uani 1 1 d . . . . . C24 C 0.5642(5) 0.9329(3) 0.51367(16) 0.0411(15) Uani 1 1 d . . . . . H24 H 0.535614 0.925262 0.534024 0.049 Uiso 1 1 calc R U . . . C25 C 0.6685(6) 0.9656(4) 0.56974(19) 0.063(2) Uani 1 1 d . . . . . H25A H 0.657799 0.923436 0.574786 0.076 Uiso 1 1 calc R U . . . H25B H 0.606073 0.986601 0.571062 0.076 Uiso 1 1 calc R U . . . C26 C 0.7408(7) 0.9921(5) 0.5925(2) 0.102(4) Uani 1 1 d . . . . . H26A H 0.760710 1.030919 0.584555 0.153 Uiso 1 1 calc R U . . . H26B H 0.797413 0.966356 0.594057 0.153 Uiso 1 1 calc R U . . . H26C H 0.711492 0.996446 0.613868 0.153 Uiso 1 1 calc R U . . . C27 C 0.5467(7) 0.9274(4) 0.39873(18) 0.070(2) Uani 1 1 d . . . . . H27A H 0.609261 0.906643 0.396681 0.084 Uiso 1 1 calc R U . . . H27B H 0.557687 0.970161 0.395571 0.084 Uiso 1 1 calc R U . . . C28 C 0.4748(8) 0.9042(5) 0.3743(2) 0.103(4) Uani 1 1 d . . . . . H28A H 0.503464 0.905637 0.352795 0.154 Uiso 1 1 calc R U . . . H28B H 0.416452 0.928641 0.374787 0.154 Uiso 1 1 calc R U . . . H28C H 0.457979 0.863443 0.379666 0.154 Uiso 1 1 calc R U . . . C29 C 0.3563(4) 0.6430(2) 0.48087(15) 0.0346(14) Uani 1 1 d . . . . . H29A H 0.317853 0.630946 0.499849 0.042 Uiso 1 1 calc R U . . . H29B H 0.318929 0.632402 0.461395 0.042 Uiso 1 1 calc R U . . . C30 C 0.4503(4) 0.6087(2) 0.48077(15) 0.0364(14) Uani 1 1 d . . . . . C31 C 0.4897(5) 0.5885(3) 0.45191(16) 0.0409(15) Uani 1 1 d . . . . . H31 H 0.458663 0.597215 0.432092 0.049 Uiso 1 1 calc R U . . . C32 C 0.5747(5) 0.5554(3) 0.45216(18) 0.0472(17) Uani 1 1 d . . . . . C33 C 0.6182(4) 0.5398(3) 0.48066(18) 0.0442(16) Uani 1 1 d . . . . . C34 C 0.7042(5) 0.4994(3) 0.4810(2) 0.0514(18) Uani 1 1 d . . . . . H34A H 0.702713 0.474849 0.461271 0.062 Uiso 1 1 calc R U . . . H34B H 0.698568 0.472549 0.499660 0.062 Uiso 1 1 calc R U . . . C35 C 0.5804(5) 0.5595(3) 0.50898(18) 0.0447(16) Uani 1 1 d . . . . . H35 H 0.610671 0.549187 0.528701 0.054 Uiso 1 1 calc R U . . . C36 C 0.4971(5) 0.5951(3) 0.50930(16) 0.0414(15) Uani 1 1 d . . . . . C37 C 0.5011(6) 0.6032(4) 0.56662(17) 0.062(2) Uani 1 1 d . . . . . H37A H 0.568738 0.617211 0.566152 0.075 Uiso 1 1 calc R U . . . H37B H 0.501081 0.560234 0.570654 0.075 Uiso 1 1 calc R U . . . C38 C 0.4457(7) 0.6345(5) 0.5923(2) 0.089(3) Uani 1 1 d . . . . . H38A H 0.435997 0.675694 0.585948 0.134 Uiso 1 1 calc R U . . . H38B H 0.481954 0.633005 0.612495 0.134 Uiso 1 1 calc R U . . . H38C H 0.382925 0.615373 0.595164 0.134 Uiso 1 1 calc R U . . . C39 C 0.5766(7) 0.5507(4) 0.3940(2) 0.079(3) Uani 1 1 d . . . . . H39A H 0.574818 0.594163 0.391955 0.094 Uiso 1 1 calc R U . . . H39B H 0.510049 0.535341 0.391966 0.094 Uiso 1 1 calc R U . . . C40 C 0.6416(9) 0.5240(5) 0.3682(2) 0.118(5) Uani 1 1 d . . . . . H40A H 0.619551 0.536829 0.346931 0.176 Uiso 1 1 calc R U . . . H40B H 0.638787 0.480957 0.369534 0.176 Uiso 1 1 calc R U . . . H40C H 0.708200 0.537198 0.371618 0.176 Uiso 1 1 calc R U . . . C41 C 0.3959(5) 0.8239(3) 0.54752(14) 0.0395(15) Uani 1 1 d . . . . . C42 C 0.4739(6) 0.8088(3) 0.56659(16) 0.055(2) Uani 1 1 d . . . . . H42 H 0.517811 0.779590 0.559237 0.066 Uiso 1 1 calc R U . . . C43 C 0.4895(6) 0.8353(4) 0.59615(18) 0.067(2) Uani 1 1 d . . . . . H43 H 0.544177 0.824731 0.608676 0.080 Uiso 1 1 calc R U . . . C44 C 0.4242(6) 0.8777(3) 0.60759(17) 0.061(2) Uani 1 1 d . . . . . C45 C 0.3467(6) 0.8915(3) 0.58896(16) 0.056(2) Uani 1 1 d . . . . . H45 H 0.302717 0.920544 0.596395 0.067 Uiso 1 1 calc R U . . . C46 C 0.3294(5) 0.8647(3) 0.55958(15) 0.0466(17) Uani 1 1 d . . . . . H46 H 0.272812 0.873929 0.547706 0.056 Uiso 1 1 calc R U . . . C47 C 0.5587(12) 0.9523(6) 0.6762(3) 0.125(5) Uani 1 1 d . . . . . H47 H 0.623154 0.960032 0.682735 0.149 Uiso 1 1 calc R U . . . C48 C 0.5417(9) 0.9195(5) 0.6485(2) 0.106(4) Uani 1 1 d . . . . . H48 H 0.594120 0.903689 0.636561 0.127 Uiso 1 1 calc R U . . . C49 C 0.4446(8) 0.9100(4) 0.63822(19) 0.077(3) Uani 1 1 d . . . . . C50 C 0.3761(9) 0.9368(5) 0.6555(2) 0.092(3) Uani 1 1 d . . . . . H50 H 0.310979 0.934394 0.648431 0.111 Uiso 1 1 calc R U . . . C51 C 0.3959(10) 0.9676(5) 0.6829(3) 0.114(4) Uani 1 1 d . . . . . H51 H 0.344059 0.985455 0.694237 0.136 Uiso 1 1 calc R U . . . C52 C 0.745(7) 0.457(6) 0.240(5) 0.306(8) Uani 0.093(14) 1 d D U P A -1 H52A H 0.741528 0.415805 0.246483 0.459 Uiso 0.093(14) 1 d R U P A -1 H52B H 0.791178 0.478355 0.253043 0.459 Uiso 0.093(14) 1 d R U P A -1 H52C H 0.766098 0.458655 0.217033 0.459 Uiso 0.093(14) 1 d R U P A -1 C53 C 0.649(3) 0.486(3) 0.245(2) 0.306(8) Uani 0.093(14) 1 d D U P A -1 C54 C 0.4565(13) 0.6826(6) 0.1946(4) 0.208(3) Uani 1 1 d D U . . . H54A H 0.475707 0.706188 0.213268 0.312 Uiso 1 1 calc R U . . . H54B H 0.396598 0.698593 0.185517 0.312 Uiso 1 1 calc R U . . . H54C H 0.507532 0.684068 0.178279 0.312 Uiso 1 1 calc R U . . . C55 C 0.4402(9) 0.6191(5) 0.2049(3) 0.1954(19) Uani 1 1 d D U . . . O10 O 0.736(2) 0.6992(10) 0.5513(7) 0.100(8) Uani 0.25 1 d . U P B 1 H10A H 0.775901 0.714868 0.537449 0.150 Uiso 0.25 1 d R U P B 1 H10B H 0.769411 0.696958 0.569019 0.150 Uiso 0.25 1 d R U P B 1 O11 O 0.7610(18) 0.6946(8) 0.4176(7) 0.091(7) Uani 0.25 1 d . U P C 1 H11A H 0.755360 0.732724 0.417612 0.136 Uiso 0.25 1 d R U P C 1 H11B H 0.725530 0.682934 0.433662 0.136 Uiso 0.25 1 d R U P C 1 O14 O 0.6923(13) 0.7436(12) 0.4440(5) 0.180(8) Uani 0.5 1 d . U P D 2 H14A H 0.649224 0.734506 0.458502 0.270 Uiso 0.5 1 d R U P D 2 H14B H 0.718844 0.710956 0.437302 0.270 Uiso 0.5 1 d R U P D 2 O15 O 0.6968(14) 0.7439(12) 0.5310(6) 0.082(7) Uani 0.25 1 d . U P E 2 H15A H 0.675327 0.747769 0.511276 0.123 Uiso 0.25 1 d R U P E 2 H15B H 0.724797 0.776748 0.535986 0.123 Uiso 0.25 1 d R U P E 2 O16 O 0.250000 0.750000 0.6330(13) 0.136(16) Uani 0.25 2 d S TU P F 2 H16A H 0.303410 0.733680 0.626536 0.204 Uiso 0.125 1 d R U P F 2 H16B H 0.250000 0.750000 0.653966 0.204 Uiso 0.25 2 d R U P F 2 O17 O 0.626(2) 0.7255(16) 0.4737(9) 0.128(11) Uani 0.25 1 d . U P G 3 H17A H 0.646727 0.730337 0.493270 0.192 Uiso 0.25 1 d R U P G 3 H17B H 0.675707 0.732797 0.461630 0.192 Uiso 0.25 1 d R U P G 3 O18 O 0.615(3) 0.7457(19) 0.5010(10) 0.147(13) Uani 0.25 1 d . U P H 1 H18C H 0.639683 0.745234 0.481791 0.221 Uiso 0.25 1 d R U P H 1 H18D H 0.665153 0.748774 0.513701 0.221 Uiso 0.25 1 d R U P H 1 O12 O 0.728(3) 0.6578(14) 0.6246(7) 0.140(14) Uani 0.25 1 d . . P . . H12A H 0.735381 0.680665 0.641255 0.210 Uiso 0.25 1 d R U P . . H12B H 0.716961 0.621944 0.631085 0.210 Uiso 0.25 1 d R U P . . O9A O 0.3140(12) 0.5118(9) 0.2266(4) 0.173(7) Uani 0.711(15) 1 d DG U P A 2 H9AA H 0.299904 0.540085 0.239930 0.260 Uiso 0.711(15) 1 d DG U P A 2 H9AB H 0.314372 0.528607 0.207780 0.260 Uiso 0.711(15) 1 d DG U P A 2 O6A O 0.6252(11) 0.4930(8) 0.2572(4) 0.309(8) Uani 0.907(14) 1 d D U P A 2 C52A C 0.6302(19) 0.4108(11) 0.2925(5) 0.307(10) Uani 0.907(14) 1 d D U P A 2 H52D H 0.694004 0.398343 0.284926 0.460 Uiso 0.907(14) 1 calc R U P A 2 H52E H 0.590470 0.375978 0.296864 0.460 Uiso 0.907(14) 1 calc R U P A 2 H52F H 0.637327 0.433926 0.312281 0.460 Uiso 0.907(14) 1 calc R U P A 2 C53A C 0.5824(15) 0.4479(10) 0.2671(8) 0.305(8) Uani 0.907(14) 1 d D U P A 2 O5A O 0.4942(13) 0.4397(7) 0.2619(4) 0.300(8) Uani 0.907(14) 1 d D U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.313(3) 0.1252(15) 0.0641(10) -0.0511(10) 0.0700(15) -0.0239(18) O1 0.060(3) 0.061(3) 0.068(4) -0.005(3) 0.016(3) 0.019(3) O2 0.059(3) 0.050(3) 0.041(3) -0.001(2) -0.007(2) 0.007(2) O3 0.041(3) 0.064(3) 0.066(3) -0.019(3) -0.009(2) -0.006(2) O4 0.058(3) 0.059(3) 0.047(3) 0.001(2) -0.002(2) -0.011(3) O5 0.462(19) 0.294(15) 0.161(10) -0.068(10) 0.077(13) 0.114(14) O6 0.46(2) 0.294(15) 0.161(10) -0.068(10) 0.077(13) 0.114(14) O7 0.322(4) 0.143(2) 0.094(2) -0.044(2) 0.066(2) -0.023(3) O8 0.333(6) 0.181(5) 0.133(4) -0.030(4) 0.059(5) -0.036(5) O9B 0.16(2) 0.27(3) 0.072(16) -0.036(17) 0.022(15) 0.01(2) N1 0.207(8) 0.122(6) 0.072(5) -0.048(5) 0.060(5) -0.033(6) N2 0.205(13) 0.108(7) 0.066(6) -0.046(5) -0.048(7) 0.032(8) C1 0.198(9) 0.140(7) 0.078(5) -0.042(6) 0.062(6) -0.036(7) C2 0.177(8) 0.124(6) 0.069(5) -0.051(5) 0.057(5) -0.035(6) C3 0.156(7) 0.085(5) 0.045(4) -0.033(4) 0.038(5) -0.015(5) C4 0.189(8) 0.125(7) 0.077(5) -0.057(5) 0.052(6) -0.041(6) C5 0.208(9) 0.130(7) 0.091(6) -0.060(6) 0.059(6) -0.047(7) C6 0.078(6) 0.053(4) 0.035(4) -0.008(3) 0.004(4) 0.010(4) C7 0.087(6) 0.056(4) 0.043(4) -0.004(3) 0.029(4) 0.001(4) C8 0.064(5) 0.045(4) 0.041(4) -0.010(3) 0.018(3) -0.003(3) C9 0.045(4) 0.039(3) 0.029(3) -0.007(3) 0.004(3) 0.007(3) C10 0.052(4) 0.044(4) 0.034(3) -0.008(3) 0.000(3) 0.005(3) C11 0.061(5) 0.059(4) 0.036(4) -0.012(3) -0.001(3) 0.007(4) C12 0.031(3) 0.033(3) 0.035(3) -0.007(3) 0.002(3) 0.001(3) C13 0.033(3) 0.029(3) 0.033(3) -0.003(2) 0.001(3) 0.001(2) C14 0.035(3) 0.037(3) 0.031(3) -0.002(3) 0.001(3) 0.001(3) C15 0.037(3) 0.034(3) 0.030(3) -0.005(3) -0.004(3) 0.003(3) C16 0.031(3) 0.029(3) 0.043(4) -0.005(3) -0.003(3) 0.002(2) C17 0.036(3) 0.033(3) 0.033(3) -0.003(3) 0.002(3) -0.001(3) C18 0.039(4) 0.030(3) 0.045(4) -0.005(3) -0.004(3) -0.001(3) C19 0.035(3) 0.028(3) 0.049(4) -0.005(3) 0.002(3) -0.001(3) C20 0.040(4) 0.033(3) 0.049(4) -0.002(3) -0.004(3) -0.002(3) C21 0.044(4) 0.036(3) 0.055(4) -0.001(3) 0.007(3) 0.001(3) C22 0.037(4) 0.030(3) 0.069(5) -0.008(3) 0.001(4) 0.001(3) C23 0.038(4) 0.033(3) 0.066(5) -0.012(3) -0.006(3) 0.005(3) C24 0.041(4) 0.034(3) 0.048(4) -0.008(3) -0.006(3) -0.001(3) C25 0.049(5) 0.070(5) 0.069(5) -0.019(4) -0.012(4) -0.002(4) C26 0.069(6) 0.153(10) 0.084(7) -0.051(7) -0.018(6) -0.020(7) C27 0.077(6) 0.087(6) 0.046(4) -0.001(4) 0.014(4) -0.005(5) C28 0.120(9) 0.144(10) 0.044(5) 0.006(6) 0.003(6) -0.016(8) C29 0.034(3) 0.032(3) 0.037(3) -0.005(3) 0.004(3) 0.000(3) C30 0.036(3) 0.030(3) 0.043(4) -0.001(3) 0.002(3) 0.005(3) C31 0.040(4) 0.034(3) 0.048(4) -0.002(3) 0.001(3) 0.000(3) C32 0.041(4) 0.037(3) 0.063(5) -0.005(3) 0.013(4) 0.003(3) C33 0.029(3) 0.027(3) 0.077(5) 0.004(3) -0.002(3) 0.001(3) C34 0.034(4) 0.032(3) 0.088(6) 0.004(4) -0.003(4) 0.002(3) C35 0.041(4) 0.031(3) 0.063(5) -0.001(3) -0.005(3) 0.000(3) C36 0.040(4) 0.034(3) 0.050(4) 0.000(3) -0.002(3) -0.003(3) C37 0.061(5) 0.081(6) 0.045(4) 0.001(4) -0.010(4) 0.006(4) C38 0.088(7) 0.128(9) 0.051(5) -0.003(5) -0.008(5) 0.014(6) C39 0.092(7) 0.080(6) 0.064(5) 0.003(5) 0.023(5) 0.040(5) C40 0.154(11) 0.124(9) 0.075(7) 0.006(6) 0.048(7) 0.070(8) C41 0.049(4) 0.033(3) 0.036(3) -0.008(3) -0.012(3) 0.005(3) C42 0.069(5) 0.053(4) 0.043(4) -0.014(3) -0.023(4) 0.014(4) C43 0.083(6) 0.065(5) 0.052(5) -0.014(4) -0.033(4) 0.012(4) C44 0.088(6) 0.056(4) 0.038(4) -0.018(3) -0.022(4) 0.011(4) C45 0.073(5) 0.055(4) 0.040(4) -0.015(3) -0.009(4) 0.012(4) C46 0.054(4) 0.050(4) 0.036(4) -0.011(3) -0.011(3) 0.010(3) C47 0.168(13) 0.133(10) 0.072(7) -0.037(7) -0.046(8) -0.015(10) C48 0.123(9) 0.121(9) 0.073(7) -0.034(6) -0.037(7) 0.001(7) C49 0.111(8) 0.077(6) 0.043(5) -0.015(4) -0.029(5) 0.007(6) C50 0.119(9) 0.105(8) 0.053(5) -0.036(5) -0.017(6) 0.014(7) C51 0.138(11) 0.127(10) 0.076(7) -0.054(7) -0.024(7) 0.023(8) C52 0.46(2) 0.295(16) 0.162(11) -0.067(11) 0.077(14) 0.114(15) C53 0.463(19) 0.294(15) 0.161(10) -0.068(10) 0.077(13) 0.114(14) C54 0.339(6) 0.161(5) 0.123(5) -0.033(5) 0.057(5) -0.025(5) C55 0.327(4) 0.153(3) 0.106(3) -0.039(3) 0.063(3) -0.026(3) O10 0.100(15) 0.057(12) 0.144(17) 0.053(12) -0.051(14) -0.012(11) O11 0.088(14) 0.024(9) 0.161(18) 0.005(11) 0.001(14) 0.013(10) O14 0.113(12) 0.256(18) 0.170(14) -0.002(15) -0.033(11) -0.014(14) O15 0.036(10) 0.116(15) 0.095(14) -0.012(13) 0.014(10) 0.003(11) O16 0.12(2) 0.11(2) 0.18(2) 0.000 0.000 -0.019(18) O17 0.103(17) 0.16(2) 0.120(18) -0.017(16) 0.006(16) -0.004(16) O18 0.126(19) 0.18(2) 0.135(19) -0.036(17) -0.011(17) 0.021(17) O12 0.18(3) 0.12(2) 0.12(2) 0.05(2) -0.09(2) -0.05(2) O9A 0.138(11) 0.28(2) 0.104(10) -0.036(11) -0.012(8) 0.045(13) O6A 0.46(2) 0.298(16) 0.163(10) -0.067(10) 0.077(13) 0.117(14) C52A 0.46(2) 0.298(19) 0.162(14) -0.050(14) 0.041(17) 0.111(18) C53A 0.46(2) 0.292(15) 0.161(10) -0.068(10) 0.077(13) 0.112(14) O5A 0.46(2) 0.287(15) 0.157(9) -0.073(10) 0.083(14) 0.109(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -2.7974 3.6876 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O5 Cu1 O6 60.2(6) . . ? O5 Cu1 O9B 92(2) . . ? O5 Cu1 C53 30.8(5) . . ? O6 Cu1 O9B 152(2) . . ? O6 Cu1 C53 30.8(5) . . ? O7 Cu1 O5 131(2) . . ? O7 Cu1 O6 71(2) . . ? O7 Cu1 O9B 137.0(11) . . ? O7 Cu1 N1 90.0(4) . . ? O7 Cu1 N2 89.6(4) . 8_655 ? O7 Cu1 C53 100(2) . . ? O7 Cu1 O9A 100.5(6) . . ? O7 Cu1 O6A 105.5(6) . . ? O7 Cu1 C53A 135.5(6) . . ? O7 Cu1 O5A 165.4(6) . . ? O9B Cu1 C53 122(2) . . ? N1 Cu1 O5 93(3) . . ? N1 Cu1 O6 88(3) . . ? N1 Cu1 O9B 93.4(7) . . ? N1 Cu1 C53 98(2) . . ? N1 Cu1 O9A 90.3(5) . . ? N1 Cu1 O6A 84.3(6) . . ? N1 Cu1 C53A 87.0(9) . . ? N1 Cu1 O5A 89.3(6) . . ? N2 Cu1 O5 83(3) 8_655 . ? N2 Cu1 O6 87(3) 8_655 . ? N2 Cu1 O9B 89.9(7) 8_655 . ? N2 Cu1 N1 175.6(6) 8_655 . ? N2 Cu1 C53 78(2) 8_655 . ? N2 Cu1 O9A 94.1(6) 8_655 . ? N2 Cu1 O6A 91.5(6) 8_655 . ? N2 Cu1 C53A 90.1(9) 8_655 . ? N2 Cu1 O5A 90.0(6) 8_655 . ? O9A Cu1 C53A 124.0(7) . . ? O6A Cu1 O9A 153.4(7) . . ? O6A Cu1 C53A 30.0(3) . . ? O5A Cu1 O9A 94.1(7) . . ? O5A Cu1 O6A 59.9(4) . . ? O5A Cu1 C53A 30.0(3) . . ? C32 O1 C39 118.7(6) . . ? C36 O2 C37 117.4(5) . . ? C23 O3 C25 118.8(5) . . ? C20 O4 C27 118.3(6) . . ? C53 O5 Cu1 85.5(17) . . ? C53 O6 Cu1 85.5(17) . . ? C55 O7 Cu1 119.1(8) . . ? Cu1 O9B H9BA 120.9 . . ? Cu1 O9B H9BB 119.2 . . ? H9BA O9B H9BB 104.6 . . ? C1 N1 Cu1 119.8(8) . . ? C5 N1 Cu1 120.9(9) . . ? C5 N1 C1 119.2(10) . . ? C47 N2 Cu1 117.5(10) . 8_666 ? C51 N2 Cu1 123.5(9) . 8_666 ? C51 N2 C47 118.7(9) . . ? N1 C1 H1 120.2 . . ? N1 C1 C2 119.7(12) . . ? C2 C1 H1 120.2 . . ? C1 C2 H2 118.5 . . ? C3 C2 C1 122.9(12) . . ? C3 C2 H2 118.5 . . ? C2 C3 C4 114.0(9) . . ? C2 C3 C6 123.9(10) . . ? C4 C3 C6 120.8(9) . . ? C3 C4 H4 119.2 . . ? C3 C4 C5 121.6(11) . . ? C5 C4 H4 119.2 . . ? N1 C5 C4 121.4(12) . . ? N1 C5 H5 119.3 . . ? C4 C5 H5 119.3 . . ? C7 C6 C3 119.3(8) . . ? C11 C6 C3 121.2(8) . . ? C11 C6 C7 119.4(6) . . ? C6 C7 H7 120.3 . . ? C6 C7 C8 119.3(7) . . ? C8 C7 H7 120.3 . . ? C7 C8 H8 119.6 . . ? C9 C8 C7 120.8(7) . . ? C9 C8 H8 119.6 . . ? C8 C9 C12 118.0(6) . . ? C10 C9 C8 118.1(6) . . ? C10 C9 C12 124.0(6) . . ? C9 C10 H10 118.9 . . ? C9 C10 C11 122.2(7) . . ? C11 C10 H10 118.9 . . ? C6 C11 C10 120.1(7) . . ? C6 C11 H11 120.0 . . ? C10 C11 H11 120.0 . . ? C13 C12 C9 122.5(5) . . ? C17 C12 C9 118.3(5) . . ? C17 C12 C13 119.2(5) . . ? C12 C13 C29 123.2(5) . . ? C14 C13 C12 118.3(5) . . ? C14 C13 C29 118.3(5) . . ? C13 C14 H14 118.7 . . ? C13 C14 C15 122.6(5) . . ? C15 C14 H14 118.7 . . ? C14 C15 C41 118.8(5) . . ? C16 C15 C14 118.3(5) . . ? C16 C15 C41 122.8(5) . . ? C15 C16 C18 122.5(5) . . ? C17 C16 C15 119.0(5) . . ? C17 C16 C18 118.5(5) . . ? C12 C17 H17 118.7 . . ? C16 C17 C12 122.5(6) . . ? C16 C17 H17 118.7 . . ? C16 C18 H18A 108.7 . . ? C16 C18 H18B 108.7 . . ? H18A C18 H18B 107.6 . . ? C19 C18 C16 114.2(5) . . ? C19 C18 H18A 108.7 . . ? C19 C18 H18B 108.7 . . ? C20 C19 C18 121.4(6) . . ? C24 C19 C18 120.6(6) . . ? C24 C19 C20 117.9(6) . . ? O4 C20 C19 116.2(6) . . ? O4 C20 C21 123.0(6) . . ? C21 C20 C19 120.7(6) . . ? C20 C21 H21 119.6 . . ? C22 C21 C20 120.9(7) . . ? C22 C21 H21 119.6 . . ? C21 C22 C23 118.8(6) . . ? C21 C22 C34 120.3(7) . 2_665 ? C23 C22 C34 120.8(7) . 2_665 ? O3 C23 C22 115.0(6) . . ? C24 C23 O3 124.6(7) . . ? C24 C23 C22 120.3(6) . . ? C19 C24 H24 119.4 . . ? C23 C24 C19 121.3(7) . . ? C23 C24 H24 119.4 . . ? O3 C25 H25A 110.7 . . ? O3 C25 H25B 110.7 . . ? O3 C25 C26 105.2(7) . . ? H25A C25 H25B 108.8 . . ? C26 C25 H25A 110.7 . . ? C26 C25 H25B 110.7 . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? O4 C27 H27A 110.6 . . ? O4 C27 H27B 110.6 . . ? O4 C27 C28 105.6(7) . . ? H27A C27 H27B 108.7 . . ? C28 C27 H27A 110.6 . . ? C28 C27 H27B 110.6 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28B 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C13 C29 H29A 108.8 . . ? C13 C29 H29B 108.8 . . ? H29A C29 H29B 107.7 . . ? C30 C29 C13 113.8(5) . . ? C30 C29 H29A 108.8 . . ? C30 C29 H29B 108.8 . . ? C31 C30 C29 120.4(6) . . ? C36 C30 C29 120.9(6) . . ? C36 C30 C31 118.6(6) . . ? C30 C31 H31 120.0 . . ? C30 C31 C32 120.0(6) . . ? C32 C31 H31 120.0 . . ? O1 C32 C31 122.5(7) . . ? C33 C32 O1 116.5(6) . . ? C33 C32 C31 120.9(6) . . ? C32 C33 C34 120.8(7) . . ? C35 C33 C32 119.4(6) . . ? C35 C33 C34 119.8(7) . . ? C22 C34 H34A 108.6 2_665 . ? C22 C34 H34B 108.6 2_665 . ? C33 C34 C22 114.7(5) . 2_665 ? C33 C34 H34A 108.6 . . ? C33 C34 H34B 108.6 . . ? H34A C34 H34B 107.6 . . ? C33 C35 H35 119.6 . . ? C33 C35 C36 120.7(6) . . ? C36 C35 H35 119.6 . . ? O2 C36 C30 116.0(6) . . ? O2 C36 C35 123.7(6) . . ? C30 C36 C35 120.2(6) . . ? O2 C37 H37A 110.4 . . ? O2 C37 H37B 110.4 . . ? O2 C37 C38 106.8(7) . . ? H37A C37 H37B 108.6 . . ? C38 C37 H37A 110.4 . . ? C38 C37 H37B 110.4 . . ? C37 C38 H38A 109.5 . . ? C37 C38 H38B 109.5 . . ? C37 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? O1 C39 H39A 110.4 . . ? O1 C39 H39B 110.4 . . ? O1 C39 C40 106.4(7) . . ? H39A C39 H39B 108.6 . . ? C40 C39 H39A 110.4 . . ? C40 C39 H39B 110.4 . . ? C39 C40 H40A 109.5 . . ? C39 C40 H40B 109.5 . . ? C39 C40 H40C 109.5 . . ? H40A C40 H40B 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? C42 C41 C15 119.7(6) . . ? C42 C41 C46 118.3(6) . . ? C46 C41 C15 121.9(6) . . ? C41 C42 H42 119.3 . . ? C41 C42 C43 121.5(7) . . ? C43 C42 H42 119.3 . . ? C42 C43 H43 120.1 . . ? C42 C43 C44 119.9(7) . . ? C44 C43 H43 120.1 . . ? C43 C44 C49 120.2(7) . . ? C45 C44 C43 118.2(6) . . ? C45 C44 C49 121.4(7) . . ? C44 C45 H45 118.7 . . ? C44 C45 C46 122.6(7) . . ? C46 C45 H45 118.7 . . ? C41 C46 H46 120.3 . . ? C45 C46 C41 119.5(6) . . ? C45 C46 H46 120.3 . . ? N2 C47 H47 119.8 . . ? N2 C47 C48 120.4(13) . . ? C48 C47 H47 119.8 . . ? C47 C48 H48 120.4 . . ? C47 C48 C49 119.3(12) . . ? C49 C48 H48 120.4 . . ? C48 C49 C44 120.4(9) . . ? C50 C49 C44 123.2(9) . . ? C50 C49 C48 116.0(8) . . ? C49 C50 H50 118.7 . . ? C49 C50 C51 122.6(11) . . ? C51 C50 H50 118.7 . . ? N2 C51 C50 122.6(12) . . ? N2 C51 H51 118.7 . . ? C50 C51 H51 118.7 . . ? H52A C52 H52B 109.5 . . ? H52A C52 H52C 109.5 . . ? H52B C52 H52C 109.5 . . ? C53 C52 H52A 109.0 . . ? C53 C52 H52B 105.6 . . ? C53 C52 H52C 113.7 . . ? O5 C53 Cu1 63.8(14) . . ? O5 C53 O6 123.2(12) . . ? O5 C53 C52 118.3(11) . . ? O6 C53 Cu1 63.8(14) . . ? O6 C53 C52 118.5(11) . . ? C52 C53 Cu1 158(6) . . ? H54A C54 H54B 109.5 . . ? H54A C54 H54C 109.5 . . ? H54B C54 H54C 109.5 . . ? C55 C54 H54A 109.5 . . ? C55 C54 H54B 109.5 . . ? C55 C54 H54C 109.5 . . ? O7 C55 C54 121.2(9) . . ? O8 C55 O7 117.6(9) . . ? O8 C55 C54 121.2(9) . . ? H10A O10 H10B 104.6 . . ? H11A O11 H11B 104.5 . . ? O14 O14 H14A 135.7 2_665 . ? O14 O14 H14B 74.8 2_665 . ? H14A O14 H14B 108.0 . . ? O15 O15 H15A 108.4 2_665 . ? O15 O15 H15B 53.2 2_665 . ? H15A O15 H15B 106.9 . . ? H16A O16 H16A 144.0 . 2_565 ? H16A O16 H16B 108.0 . . ? H16B O16 H16A 108.0 . 2_565 ? H17A O17 H17B 104.5 . . ? H18C O18 H18D 104.4 . . ? H12A O12 H12B 109.5 . . ? Cu1 O9A H9AA 94.9 . . ? Cu1 O9A H9AB 94.7 . . ? H9AA O9A H9AB 104.5 . . ? C53A O6A Cu1 86.9(9) . . ? H52D C52A H52E 109.5 . . ? H52D C52A H52F 109.5 . . ? H52E C52A H52F 109.5 . . ? C53A C52A H52D 109.5 . . ? C53A C52A H52E 109.5 . . ? C53A C52A H52F 109.5 . . ? O6A C53A Cu1 63.2(9) . . ? O6A C53A C52A 118.7(14) . . ? C52A C53A Cu1 168(2) . . ? O5A C53A Cu1 58.6(8) . . ? O5A C53A O6A 121.7(15) . . ? O5A C53A C52A 117.9(14) . . ? C53A O5A Cu1 91.5(9) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 O5 2.194(18) . ? Cu1 O6 2.194(18) . ? Cu1 O7 1.797(10) . ? Cu1 O9B 2.40(2) . ? Cu1 N1 2.025(8) . ? Cu1 N2 2.015(8) 8_655 ? Cu1 C53 2.44(4) . ? Cu1 O9A 2.398(17) . ? Cu1 O6A 2.242(15) . ? Cu1 C53A 2.508(18) . ? Cu1 O5A 2.141(14) . ? O1 C32 1.389(8) . ? O1 C39 1.424(10) . ? O2 C36 1.380(8) . ? O2 C37 1.417(8) . ? O3 C23 1.381(8) . ? O3 C25 1.408(9) . ? O4 C20 1.382(8) . ? O4 C27 1.414(8) . ? O5 C53 1.251(8) . ? O6 C53 1.251(8) . ? O7 C55 1.260(5) . ? O8 C55 1.256(5) . ? O9B H9BA 0.8686 . ? O9B H9BB 0.8699 . ? N1 C1 1.300(15) . ? N1 C5 1.289(14) . ? N2 C47 1.374(17) . ? N2 C51 1.300(15) . ? C1 H1 0.9500 . ? C1 C2 1.400(13) . ? C2 H2 0.9500 . ? C2 C3 1.316(14) . ? C3 C4 1.360(14) . ? C3 C6 1.490(10) . ? C4 H4 0.9500 . ? C4 C5 1.376(13) . ? C5 H5 0.9500 . ? C6 C7 1.397(11) . ? C6 C11 1.375(10) . ? C7 H7 0.9500 . ? C7 C8 1.415(9) . ? C8 H8 0.9500 . ? C8 C9 1.395(9) . ? C9 C10 1.362(9) . ? C9 C12 1.491(8) . ? C10 H10 0.9500 . ? C10 C11 1.398(9) . ? C11 H11 0.9500 . ? C12 C13 1.395(8) . ? C12 C17 1.393(8) . ? C13 C14 1.394(8) . ? C13 C29 1.522(8) . ? C14 H14 0.9500 . ? C14 C15 1.408(8) . ? C15 C16 1.396(8) . ? C15 C41 1.483(8) . ? C16 C17 1.389(8) . ? C16 C18 1.531(8) . ? C17 H17 0.9500 . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C18 C19 1.512(8) . ? C19 C20 1.392(9) . ? C19 C24 1.390(9) . ? C20 C21 1.387(9) . ? C21 H21 0.9500 . ? C21 C22 1.370(10) . ? C22 C23 1.397(10) . ? C22 C34 1.531(9) 2_665 ? C23 C24 1.373(9) . ? C24 H24 0.9500 . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C25 C26 1.505(10) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C27 C28 1.516(12) . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C29 C30 1.517(8) . ? C30 C31 1.395(9) . ? C30 C36 1.386(9) . ? C31 H31 0.9500 . ? C31 C32 1.397(9) . ? C32 C33 1.375(10) . ? C33 C34 1.504(8) . ? C33 C35 1.364(9) . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C35 H35 0.9500 . ? C35 C36 1.408(9) . ? C37 H37A 0.9900 . ? C37 H37B 0.9900 . ? C37 C38 1.492(11) . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9900 . ? C39 H39B 0.9900 . ? C39 C40 1.525(11) . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? C41 C42 1.384(9) . ? C41 C46 1.397(9) . ? C42 H42 0.9500 . ? C42 C43 1.384(9) . ? C43 H43 0.9500 . ? C43 C44 1.404(11) . ? C44 C45 1.360(10) . ? C44 C49 1.495(10) . ? C45 H45 0.9500 . ? C45 C46 1.385(9) . ? C46 H46 0.9500 . ? C47 H47 0.9500 . ? C47 C48 1.388(13) . ? C48 H48 0.9500 . ? C48 C49 1.429(14) . ? C49 C50 1.338(13) . ? C50 H50 0.9500 . ? C50 C51 1.363(12) . ? C51 H51 0.9500 . ? C52 H52A 0.9797 . ? C52 H52B 0.9802 . ? C52 H52C 0.9798 . ? C52 C53 1.500(8) . ? C54 H54A 0.9800 . ? C54 H54B 0.9800 . ? C54 H54C 0.9800 . ? C54 C55 1.522(9) . ? O10 H10A 0.8707 . ? O10 H10B 0.8696 . ? O11 H11A 0.8695 . ? O11 H11B 0.8698 . ? O14 O14 1.62(4) 2_665 ? O14 H14A 0.8722 . ? O14 H14B 0.8720 . ? O15 O15 1.50(4) 2_665 ? O15 H15A 0.8753 . ? O15 H15B 0.8658 . ? O16 H16A 0.8700 2_565 ? O16 H16A 0.8700 . ? O16 H16B 0.8711 . ? O17 H17A 0.8708 . ? O17 H17B 0.8699 . ? O18 H18C 0.8684 . ? O18 H18D 0.8709 . ? O12 H12A 0.8696 . ? O12 H12B 0.8701 . ? O9A H9AA 0.8700 . ? O9A H9AB 0.8703 . ? O6A C53A 1.255(10) . ? C52A H52D 0.9800 . ? C52A H52E 0.9800 . ? C52A H52F 0.9800 . ? C52A C53A 1.503(10) . ? C53A O5A 1.254(10) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 O5 C53 O6 24(7) . . . . ? Cu1 O5 C53 C52 -156(7) . . . . ? Cu1 O6 C53 O5 -24(7) . . . . ? Cu1 O6 C53 C52 156(7) . . . . ? Cu1 O7 C55 O8 -16.9(17) . . . . ? Cu1 O7 C55 C54 165.0(9) . . . . ? Cu1 N1 C1 C2 179.3(11) . . . . ? Cu1 N1 C5 C4 -178.6(12) . . . . ? Cu1 N2 C47 C48 178.8(9) 8_666 . . . ? Cu1 N2 C51 C50 179.5(9) 8_666 . . . ? Cu1 O6A C53A C52A -167(3) . . . . ? Cu1 O6A C53A O5A -3(4) . . . . ? O1 C32 C33 C34 -3.0(9) . . . . ? O1 C32 C33 C35 179.6(6) . . . . ? O3 C23 C24 C19 178.4(6) . . . . ? O4 C20 C21 C22 178.8(6) . . . . ? O5 Cu1 O7 C55 -173(5) . . . . ? O6 Cu1 O7 C55 -166(3) . . . . ? O9B Cu1 O7 C55 16.8(14) . . . . ? N1 Cu1 O7 C55 -78.2(10) . . . . ? N1 C1 C2 C3 -5(2) . . . . ? N2 Cu1 O7 C55 106.2(10) 8_655 . . . ? N2 C47 C48 C49 2.3(19) . . . . ? C1 N1 C5 C4 5(3) . . . . ? C1 C2 C3 C4 12(2) . . . . ? C1 C2 C3 C6 179.1(12) . . . . ? C2 C3 C4 C5 -11(2) . . . . ? C2 C3 C6 C7 -16.0(16) . . . . ? C2 C3 C6 C11 168.0(11) . . . . ? C3 C4 C5 N1 3(3) . . . . ? C3 C6 C7 C8 -173.8(8) . . . . ? C3 C6 C11 C10 174.2(8) . . . . ? C4 C3 C6 C7 150.5(12) . . . . ? C4 C3 C6 C11 -25.5(16) . . . . ? C5 N1 C1 C2 -4(2) . . . . ? C6 C3 C4 C5 -178.7(13) . . . . ? C6 C7 C8 C9 0.5(11) . . . . ? C7 C6 C11 C10 -1.8(11) . . . . ? C7 C8 C9 C10 -3.9(10) . . . . ? C7 C8 C9 C12 176.3(6) . . . . ? C8 C9 C10 C11 4.5(10) . . . . ? C8 C9 C12 C13 -121.9(7) . . . . ? C8 C9 C12 C17 56.8(8) . . . . ? C9 C10 C11 C6 -1.7(11) . . . . ? C9 C12 C13 C14 174.8(6) . . . . ? C9 C12 C13 C29 -1.0(9) . . . . ? C9 C12 C17 C16 -176.8(6) . . . . ? C10 C9 C12 C13 58.3(9) . . . . ? C10 C9 C12 C17 -122.9(7) . . . . ? C11 C6 C7 C8 2.3(11) . . . . ? C12 C9 C10 C11 -175.7(6) . . . . ? C12 C13 C14 C15 3.2(9) . . . . ? C12 C13 C29 C30 84.8(7) . . . . ? C13 C12 C17 C16 2.0(9) . . . . ? C13 C14 C15 C16 -0.3(9) . . . . ? C13 C14 C15 C41 -176.1(6) . . . . ? C13 C29 C30 C31 -96.7(7) . . . . ? C13 C29 C30 C36 85.5(7) . . . . ? C14 C13 C29 C30 -91.0(7) . . . . ? C14 C15 C16 C17 -1.8(9) . . . . ? C14 C15 C16 C18 178.2(5) . . . . ? C14 C15 C41 C42 64.7(9) . . . . ? C14 C15 C41 C46 -117.7(7) . . . . ? C15 C16 C17 C12 0.9(9) . . . . ? C15 C16 C18 C19 96.7(7) . . . . ? C15 C41 C42 C43 174.3(7) . . . . ? C15 C41 C46 C45 -173.4(7) . . . . ? C16 C15 C41 C42 -110.9(8) . . . . ? C16 C15 C41 C46 66.7(9) . . . . ? C16 C18 C19 C20 89.1(7) . . . . ? C16 C18 C19 C24 -95.4(7) . . . . ? C17 C12 C13 C14 -4.0(9) . . . . ? C17 C12 C13 C29 -179.8(5) . . . . ? C17 C16 C18 C19 -83.4(7) . . . . ? C18 C16 C17 C12 -179.0(6) . . . . ? C18 C19 C20 O4 -4.9(8) . . . . ? C18 C19 C20 C21 173.1(5) . . . . ? C18 C19 C24 C23 -174.2(5) . . . . ? C19 C20 C21 C22 1.0(9) . . . . ? C20 O4 C27 C28 176.5(7) . . . . ? C20 C19 C24 C23 1.5(9) . . . . ? C20 C21 C22 C23 1.7(9) . . . . ? C20 C21 C22 C34 -175.7(5) . . . 2_665 ? C21 C22 C23 O3 179.8(6) . . . . ? C21 C22 C23 C24 -2.7(9) . . . . ? C22 C23 C24 C19 1.2(9) . . . . ? C23 O3 C25 C26 -173.8(7) . . . . ? C24 C19 C20 O4 179.5(5) . . . . ? C24 C19 C20 C21 -2.5(9) . . . . ? C25 O3 C23 C22 174.5(6) . . . . ? C25 O3 C23 C24 -2.8(9) . . . . ? C27 O4 C20 C19 178.9(6) . . . . ? C27 O4 C20 C21 0.9(9) . . . . ? C29 C13 C14 C15 179.2(5) . . . . ? C29 C30 C31 C32 -178.0(5) . . . . ? C29 C30 C36 O2 -1.9(8) . . . . ? C29 C30 C36 C35 175.3(5) . . . . ? C30 C31 C32 O1 -180.0(6) . . . . ? C30 C31 C32 C33 3.1(10) . . . . ? C31 C30 C36 O2 -179.7(5) . . . . ? C31 C30 C36 C35 -2.5(9) . . . . ? C31 C32 C33 C34 174.1(6) . . . . ? C31 C32 C33 C35 -3.3(10) . . . . ? C32 O1 C39 C40 176.6(8) . . . . ? C32 C33 C34 C22 97.0(8) . . . 2_665 ? C32 C33 C35 C36 0.6(9) . . . . ? C33 C35 C36 O2 179.3(6) . . . . ? C33 C35 C36 C30 2.3(9) . . . . ? C34 C22 C23 O3 -2.8(8) 2_665 . . . ? C34 C22 C23 C24 174.6(5) 2_665 . . . ? C34 C33 C35 C36 -176.9(6) . . . . ? C35 C33 C34 C22 -85.6(8) . . . 2_665 ? C36 O2 C37 C38 175.5(7) . . . . ? C36 C30 C31 C32 -0.2(9) . . . . ? C37 O2 C36 C30 -179.5(6) . . . . ? C37 O2 C36 C35 3.5(9) . . . . ? C39 O1 C32 C31 5.1(10) . . . . ? C39 O1 C32 C33 -177.8(7) . . . . ? C41 C15 C16 C17 173.9(6) . . . . ? C41 C15 C16 C18 -6.2(9) . . . . ? C41 C42 C43 C44 1.2(13) . . . . ? C42 C41 C46 C45 4.3(10) . . . . ? C42 C43 C44 C45 0.2(13) . . . . ? C42 C43 C44 C49 -175.1(8) . . . . ? C43 C44 C45 C46 0.9(13) . . . . ? C43 C44 C49 C48 28.4(14) . . . . ? C43 C44 C49 C50 -159.2(10) . . . . ? C44 C45 C46 C41 -3.2(12) . . . . ? C44 C49 C50 C51 -178.0(10) . . . . ? C45 C44 C49 C48 -146.7(10) . . . . ? C45 C44 C49 C50 25.6(14) . . . . ? C46 C41 C42 C43 -3.4(11) . . . . ? C47 N2 C51 C50 6(2) . . . . ? C47 C48 C49 C44 176.7(10) . . . . ? C47 C48 C49 C50 3.7(16) . . . . ? C48 C49 C50 C51 -5.3(17) . . . . ? C49 C44 C45 C46 176.1(8) . . . . ? C49 C50 C51 N2 1(2) . . . . ? C51 N2 C47 C48 -7(2) . . . . ? C53 Cu1 O7 C55 -176(2) . . . . ? O9A Cu1 O7 C55 12.1(10) . . . . ? O6A Cu1 O7 C55 -162.3(10) . . . . ? O6A C53A O5A Cu1 3(4) . . . . ? C52A C53A O5A Cu1 167(3) . . . . ? C53A Cu1 O7 C55 -164.0(14) . . . . ? O5A Cu1 O7 C55 -165(2) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.250 0.250 0.250 714.4 118.9 '12 H2O' 2 0.250 -0.250 0.750 714.4 115.1 '12 H2O' 3 0.250 0.250 0.750 424.9 62.4 '6 H2O' 4 -0.250 0.750 0.250 424.9 62.2 '6 H2O' 5 0.250 0.750 0.250 158.2 0.0 ? 6 0.750 0.250 0.750 158.2 0.0 ?