#------------------------------------------------------------------------------ #$Date: 2024-07-16 01:10:39 +0300 (Tue, 16 Jul 2024) $ #$Revision: 293416 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/21/1572130.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572130 loop_ _publ_author_name 'Shaw, Thomas E.' 'Jones, Zachary R.' 'Adelman, Sara L.' 'Anderson, Nickolas H.' 'Bowes, Eric G.' 'Bauer, Eric D.' 'Dan, David' 'Klouda, Jan' 'Knope, Karah E.' 'Kozimor, Stosh A.' 'MacInnes, Molly M.' 'Mocko, Veronika' 'Rocha, Francisca R.' 'Root, Harrison D.' 'Stein, Benjamin W.' 'Thompson, Joe D.' 'Wacker, Jennifer N.' _publ_section_title ; PuCl3{CoCp[OP(OEt)2]3}: transuranic elements entering the field of heterometallic molecular chemistry ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC01767F _journal_year 2024 _chemical_formula_moiety 'C17 H35 Cl3 Co O9 P3 Pu' _chemical_formula_sum 'C17 H35 Cl3 Co O9 P3 Pu' _chemical_formula_weight 883.64 _chemical_melting_point ? _chemical_name_common Pu(Kl\"aui)Cl3 _chemical_name_systematic PuCl3{CoCp[OP(OEt)2]3} _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary other _audit_creation_method SHELXL-2016/6 _audit_update_record ; 2024-01-05 deposited with the CCDC. 2024-06-24 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 95.148(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.7630(16) _cell_length_b 15.914(2) _cell_length_c 18.230(3) _cell_measurement_reflns_used 9986 _cell_measurement_temperature 288(2) _cell_measurement_theta_max 25.39 _cell_measurement_theta_min 2.29 _cell_volume 3109.9(8) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 288(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker D8 Quest' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0643 _diffrn_reflns_av_unetI/netI 0.0241 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 93339 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.390 _diffrn_reflns_theta_min 2.118 _diffrn_source 'microfocus sealed tube' _exptl_absorpt_coefficient_mu 3.085 _exptl_absorpt_correction_T_max 0.0642 _exptl_absorpt_correction_T_min 0.0187 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_colour green _exptl_crystal_density_diffrn 1.887 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1704 _exptl_crystal_recrystallization_method 'Solvent layering' _exptl_crystal_size_max 0.116 _exptl_crystal_size_mid 0.066 _exptl_crystal_size_min 0.036 _exptl_transmission_factor_max 0.9772 _exptl_transmission_factor_min 0.7830 _refine_diff_density_max 1.006 _refine_diff_density_min -1.358 _refine_diff_density_rms 0.103 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.084 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 534 _refine_ls_number_reflns 5704 _refine_ls_number_restraints 1376 _refine_ls_restrained_S_all 1.028 _refine_ls_R_factor_all 0.0503 _refine_ls_R_factor_gt 0.0385 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0312P)^2^+11.3396P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0792 _refine_ls_wR_factor_ref 0.0837 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4805 _reflns_number_total 5704 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc01767f2.cif _cod_data_source_block PuCl3(CoCp(OP(OEt)2)3) _cod_depositor_comments ; The following automatic conversions were performed: data item '_chemical_melting_point' value 'not measured' was changed to '?' -- the value is undefined or not given. data item '_exptl_crystal_density_meas' value 'not measured' was changed to '?' -- the value is perceived as not measured. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas ; _cod_original_cell_volume 3109.8(8) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1572130 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.716 _shelx_estimated_absorpt_t_max 0.897 _shelx_res_file ; TITL 2_a.res in P2(1)/n 2_a.res created by SHELXL-2016/6 at 08:32:01 on 05-Jan-2024 REM Old TITL 2 in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.130, Rweak 0.017, Alpha 0.037, Orientation as input REM Formula found by SHELXT: C11 Cl6 Co O9 Pu CELL 0.71073 10.7630 15.9138 18.2298 90.000 95.148 90.000 ZERR 4.000 0.0016 0.0023 0.0027 0.000 0.005 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H CL CO O P PU UNIT 68 140 12 4 36 12 4 TEMP 14.850 SIZE 0.036 0.066 0.116 L.S. 10 BOND $H ACTA LIST 4 RIGU ISOR 0.01 CL1 > CL3B ISOR 0.01 C13 > C17B SIMU 0.01 0.02 CL1 CL1B CL2 CL2B CL3 CL3B SADI 0.01 PU1 CL1 PU1 CL1B PU1 CL2 PU1 CL2B PU1 CL3 PU1 CL3B SIMU 0.01 0.02 C13 > C17B SADI 0.01 CO1 C13 CO1 C13B ISOR 0.01 O4 > C2B ISOR 0.005 O5 > C4 SIMU 0.01 0.02 O6 > C6B O7 > C8B SADI 0.01 P2 O6 P2 O6B P2 O7 P2 O7B ISOR 0.01 O6 > C8B SIMU 0.01 0.02 O8 > C10B O9 > C12B SADI 0.01 P3 O8 P3 O8B P3 O9 P3 O9B ISOR 0.01 O8 > C12B BIND Co1 P1 FMAP 2 PLAN 20 WGHT 0.031200 11.339600 FVAR 0.25951 0.34890 0.60379 0.45404 0.71046 0.39950 0.20810 FVAR 0.59366 0.76628 0.63315 PU1 7 0.482663 0.721872 0.802906 11.00000 0.04475 0.04344 = 0.04919 -0.00968 0.00196 -0.00141 CO1 4 0.584198 0.505189 0.691540 11.00000 0.05300 0.04329 = 0.05062 -0.00716 -0.00465 0.00857 PART 1 21 CL1 3 0.274013 0.731512 0.860450 21.00000 0.07118 0.09159 = 0.10749 -0.00423 0.03181 -0.00703 PART 2 -21 CL1B 3 0.265356 0.753421 0.844043 -21.00000 0.06127 0.08642 = 0.10394 -0.01054 0.02345 0.01036 PART 0 PART 1 31 CL2 3 0.489679 0.859913 0.729635 31.00000 0.10057 0.05279 = 0.09005 0.00774 -0.00319 0.00315 PART 2 -31 CL2B 3 0.483809 0.869584 0.745623 -31.00000 0.08583 0.04359 = 0.10049 -0.00140 -0.00704 0.00773 PART 0 PART 1 41 CL3 3 0.614751 0.755055 0.923853 41.00000 0.10106 0.07477 = 0.07157 -0.01875 -0.02359 -0.00715 PART 2 -41 CL3B 3 0.604523 0.776412 0.920949 -41.00000 0.07982 0.06888 = 0.06015 -0.00914 -0.00627 -0.01920 PART 0 P1 6 0.435039 0.589021 0.650951 11.00000 0.05258 0.05111 = 0.05154 -0.01162 -0.01111 0.00923 P2 6 0.709864 0.608863 0.718028 11.00000 0.04676 0.05354 = 0.06240 -0.00461 0.00752 0.00192 P3 6 0.526496 0.504392 0.801993 11.00000 0.07022 0.04578 = 0.05655 0.00389 0.00407 -0.00195 O1 5 0.395694 0.657086 0.703518 11.00000 0.05759 0.05907 = 0.05170 -0.01309 -0.00667 0.00932 O2 5 0.497700 0.588515 0.837525 11.00000 0.07385 0.05171 = 0.05264 -0.00424 0.00988 -0.00470 O3 5 0.655121 0.687544 0.750425 11.00000 0.04272 0.04339 = 0.07296 -0.00597 0.01331 -0.00280 PART 1 51 O4 5 0.316617 0.545411 0.612110 51.00000 0.05911 0.07206 = 0.05341 -0.01298 -0.01436 0.00372 C1 1 0.211661 0.521188 0.655462 51.00000 0.08953 0.10978 = 0.09977 0.01792 -0.00261 -0.02196 AFIX 23 H1A 2 0.200193 0.562752 0.693186 51.00000 -1.20000 H1B 2 0.227709 0.467103 0.678963 51.00000 -1.20000 AFIX 0 C2 1 0.097533 0.516738 0.600854 51.00000 0.08025 0.18689 = 0.18240 0.01459 -0.03044 -0.03017 AFIX 137 H2A 2 0.081186 0.459232 0.587312 51.00000 -1.50000 H2B 2 0.111889 0.548672 0.557742 51.00000 -1.50000 H2C 2 0.027050 0.539485 0.622832 51.00000 -1.50000 AFIX 0 PART 2 -51 SAME 0.01 O4 > C2 O4B 5 0.313175 0.530098 0.647838 -51.00000 0.05773 0.07310 = 0.08697 -0.01429 -0.01037 -0.00138 C1B 1 0.181802 0.559295 0.634586 -51.00000 0.06229 0.07873 = 0.08365 -0.00529 -0.00668 0.00111 AFIX 23 H1BA 2 0.177250 0.612295 0.608200 -51.00000 -1.20000 H1BB 2 0.144389 0.566195 0.680676 -51.00000 -1.20000 AFIX 0 C2B 1 0.117111 0.489860 0.588388 -51.00000 0.07093 0.10484 = 0.10517 -0.01134 -0.02429 -0.01583 AFIX 137 H2BA 2 0.178483 0.456074 0.567124 -51.00000 -1.50000 H2BB 2 0.062029 0.514287 0.549841 -51.00000 -1.50000 H2BC 2 0.069959 0.455359 0.619016 -51.00000 -1.50000 AFIX 0 PART 0 O5 5 0.474423 0.635455 0.579179 11.00000 0.08934 0.07773 = 0.06158 0.00322 0.00726 0.02773 C3 1 0.393428 0.699894 0.544677 11.00000 0.09435 0.08646 = 0.08020 0.00646 0.00104 0.02499 AFIX 23 H3A 2 0.340455 0.675703 0.504254 11.00000 -1.20000 H3B 2 0.340340 0.722381 0.580224 11.00000 -1.20000 AFIX 0 C4 1 0.467868 0.766250 0.517592 11.00000 0.14414 0.11058 = 0.14755 0.02369 0.00570 0.00384 AFIX 137 H4A 2 0.527545 0.785147 0.556386 11.00000 -1.50000 H4B 2 0.414807 0.812208 0.500993 11.00000 -1.50000 H4C 2 0.510900 0.745652 0.477333 11.00000 -1.50000 AFIX 0 PART 1 61 O6 5 0.747626 0.636949 0.639426 61.00000 0.08307 0.08817 = 0.08423 -0.00012 0.02451 -0.01521 C5 1 0.763522 0.705019 0.602002 61.00000 0.08537 0.09833 = 0.08615 0.01353 0.01585 -0.00309 AFIX 23 H5A 2 0.818398 0.742139 0.632113 61.00000 -1.20000 H5B 2 0.683548 0.733077 0.593314 61.00000 -1.20000 AFIX 0 C6 1 0.812654 0.694554 0.534515 61.00000 0.11148 0.12577 = 0.08841 0.01181 0.02234 -0.00016 AFIX 137 H6A 2 0.894257 0.670018 0.542285 61.00000 -1.50000 H6B 2 0.818357 0.748203 0.510972 61.00000 -1.50000 H6C 2 0.759232 0.658225 0.503746 61.00000 -1.50000 AFIX 0 PART 2 -61 SAME 0.01 O6 > C6 O6B 5 0.799593 0.634416 0.657457 -61.00000 0.06156 0.08273 = 0.08360 0.00021 0.02022 -0.00449 C5B 1 0.810205 0.708164 0.625982 -61.00000 0.09349 0.09913 = 0.08761 0.01313 0.01845 -0.00534 AFIX 23 H5B1 2 0.844879 0.746996 0.663406 -61.00000 -1.20000 H5B2 2 0.726848 0.727785 0.609933 -61.00000 -1.20000 AFIX 0 C6B 1 0.881732 0.713811 0.566200 -61.00000 0.12276 0.13191 = 0.10474 0.02448 0.03456 -0.00774 AFIX 137 H6B1 2 0.966882 0.725371 0.583530 -61.00000 -1.50000 H6B2 2 0.850225 0.758320 0.534195 -61.00000 -1.50000 H6B3 2 0.877400 0.661635 0.539662 -61.00000 -1.50000 AFIX 0 PART 0 PART 1 71 O7 5 0.850646 0.591652 0.745207 71.00000 0.05926 0.07769 = 0.08592 -0.00691 0.00409 0.00136 C7 1 0.940539 0.639096 0.786358 71.00000 0.07036 0.08241 = 0.08965 -0.00421 -0.00259 -0.00401 AFIX 23 H7A 2 0.900935 0.667742 0.825047 71.00000 -1.20000 H7B 2 0.971411 0.681783 0.754631 71.00000 -1.20000 AFIX 0 C8 1 1.042889 0.593161 0.818788 71.00000 0.07694 0.09288 = 0.09925 -0.00636 -0.00742 -0.00153 AFIX 137 H8A 2 1.070751 0.617561 0.865553 71.00000 -1.50000 H8B 2 1.109488 0.594636 0.787133 71.00000 -1.50000 H8C 2 1.018247 0.535953 0.825800 71.00000 -1.50000 AFIX 0 PART 2 -71 SAME 0.01 O7 > C8 O7B 5 0.815189 0.575869 0.778772 -71.00000 0.05469 0.07076 = 0.08657 -0.00671 -0.01256 0.00227 C7B 1 0.905867 0.626995 0.815795 -71.00000 0.07432 0.08481 = 0.09111 -0.00363 -0.00782 -0.00709 AFIX 23 H7BA 2 0.865504 0.664063 0.848597 -71.00000 -1.20000 H7BB 2 0.943039 0.661824 0.779961 -71.00000 -1.20000 AFIX 0 C8B 1 1.001949 0.582623 0.857337 -71.00000 0.07961 0.10288 = 0.11461 -0.01737 -0.02231 -0.00063 AFIX 137 H8BA 2 1.029280 0.536706 0.828648 -71.00000 -1.50000 H8BB 2 0.970999 0.561267 0.901462 -71.00000 -1.50000 H8BC 2 1.070775 0.619783 0.870093 -71.00000 -1.50000 AFIX 0 PART 0 PART 1 81 O8 5 0.603841 0.448022 0.860835 81.00000 0.07894 0.07311 = 0.06499 0.01877 0.00396 -0.00645 C9 1 0.658520 0.480787 0.928287 81.00000 0.09471 0.10404 = 0.08769 0.01058 -0.01280 -0.00178 AFIX 23 H9A 2 0.703460 0.531323 0.917004 81.00000 -1.20000 H9B 2 0.591081 0.498022 0.956844 81.00000 -1.20000 AFIX 0 C10 1 0.734578 0.434338 0.971113 81.00000 0.13172 0.12787 = 0.11340 0.01748 -0.03167 0.00791 AFIX 137 H10A 2 0.687286 0.399912 1.001724 81.00000 -1.50000 H10B 2 0.789761 0.469898 1.001543 81.00000 -1.50000 H10C 2 0.782501 0.399116 0.941501 81.00000 -1.50000 AFIX 0 PART 2 -81 SAME 0.01 O8 > C10 O8B 5 0.648640 0.473607 0.851424 -81.00000 0.09588 0.09070 = 0.07093 0.01529 -0.00156 0.01101 C9B 1 0.704871 0.497276 0.920756 -81.00000 0.09330 0.09818 = 0.08733 0.01481 -0.00854 -0.00869 AFIX 23 H9B1 2 0.726857 0.556218 0.917842 -81.00000 -1.20000 H9B2 2 0.641840 0.493064 0.955417 -81.00000 -1.20000 AFIX 0 C10B 1 0.804069 0.457230 0.949511 -81.00000 0.10364 0.11607 = 0.10546 0.02245 -0.01147 0.00188 AFIX 137 H10D 2 0.782160 0.400330 0.960182 -81.00000 -1.50000 H10E 2 0.835899 0.484716 0.994176 -81.00000 -1.50000 H10F 2 0.866752 0.457335 0.915221 -81.00000 -1.50000 AFIX 0 PART 0 PART 1 91 O9 5 0.397931 0.452182 0.795899 91.00000 0.08090 0.06672 = 0.07590 0.00183 0.00945 -0.02462 C11 1 0.323562 0.441156 0.857724 91.00000 0.09271 0.09952 = 0.09131 0.00036 0.01382 -0.02415 AFIX 23 H11A 2 0.237111 0.456325 0.844680 91.00000 -1.20000 H11B 2 0.356101 0.474288 0.899805 91.00000 -1.20000 AFIX 0 C12 1 0.337702 0.343802 0.873854 91.00000 0.13391 0.12896 = 0.13452 0.03690 0.01295 -0.02988 AFIX 137 H12A 2 0.256853 0.317861 0.869166 91.00000 -1.50000 H12B 2 0.375922 0.335551 0.922955 91.00000 -1.50000 H12C 2 0.388914 0.318907 0.839230 91.00000 -1.50000 AFIX 0 PART 2 -91 SAME 0.01 O9 > C12 O9B 5 0.465430 0.425970 0.838451 -91.00000 0.08816 0.07589 = 0.08246 0.00702 0.00969 -0.01454 C11B 1 0.331560 0.422425 0.821966 -91.00000 0.09068 0.08667 = 0.08932 0.00037 0.00968 -0.01754 AFIX 23 H11C 2 0.308661 0.385234 0.780804 -91.00000 -1.20000 H11D 2 0.296999 0.477784 0.811034 -91.00000 -1.20000 AFIX 0 C12B 1 0.286698 0.386367 0.896165 -91.00000 0.10249 0.09466 = 0.10184 0.00481 0.02099 -0.01779 AFIX 137 H12D 2 0.256454 0.330063 0.888152 -91.00000 -1.50000 H12E 2 0.221013 0.421071 0.911752 -91.00000 -1.50000 H12F 2 0.355439 0.386113 0.933560 -91.00000 -1.50000 AFIX 0 PART 0 PART 1 101 C13 1 0.538970 0.430203 0.598948 101.00000 0.07105 0.05467 = 0.06084 -0.01565 0.00241 0.00675 AFIX 13 H13 2 0.468607 0.439221 0.561813 101.00000 -1.20000 AFIX 0 C14 1 0.535739 0.383022 0.663818 101.00000 0.07216 0.04957 = 0.06583 -0.01335 -0.00098 0.00463 AFIX 13 H14 2 0.463610 0.352287 0.679262 101.00000 -1.20000 AFIX 0 C15 1 0.657460 0.385154 0.701821 101.00000 0.06926 0.04964 = 0.06996 -0.00792 -0.00053 0.01071 AFIX 13 H15 2 0.683820 0.356292 0.748104 101.00000 -1.20000 AFIX 0 C16 1 0.733000 0.433550 0.660306 101.00000 0.06951 0.05466 = 0.06471 -0.00998 0.00356 0.01522 AFIX 13 H16 2 0.821551 0.445638 0.673200 101.00000 -1.20000 AFIX 0 C17 1 0.660648 0.463160 0.596532 101.00000 0.07089 0.05798 = 0.06202 -0.01227 0.00416 0.00888 AFIX 13 H17 2 0.690064 0.498360 0.557513 101.00000 -1.20000 AFIX 0 PART 2 -101 SAME 0.01 C13 > C17 C13B 1 0.512929 0.404043 0.628248 -101.00000 0.06934 0.05154 = 0.06354 -0.01292 0.00037 0.00547 AFIX 13 H13B 2 0.425226 0.395333 0.610469 -101.00000 -1.20000 AFIX 0 C14B 1 0.572182 0.374292 0.695125 -101.00000 0.06902 0.05071 = 0.06636 -0.00947 0.00156 0.00784 AFIX 13 H14B 2 0.533119 0.341223 0.732157 -101.00000 -1.20000 AFIX 0 C15B 1 0.700149 0.398709 0.698476 -101.00000 0.06728 0.05299 = 0.06872 -0.00794 0.00274 0.01177 AFIX 13 H15B 2 0.764363 0.385848 0.738459 -101.00000 -1.20000 AFIX 0 C16B 1 0.717316 0.444613 0.635354 -101.00000 0.06820 0.05674 = 0.06476 -0.01049 0.00389 0.01097 AFIX 13 H16B 2 0.796332 0.469018 0.622891 -101.00000 -1.20000 AFIX 0 C17B 1 0.601851 0.449103 0.591344 -101.00000 0.06901 0.05610 = 0.06211 -0.01303 0.00259 0.00696 AFIX 13 H17B 2 0.587459 0.475949 0.542946 -101.00000 -1.20000 PART 0 AFIX 0 HKLF 4 REM 2_a.res in P2(1)/n REM R1 = 0.0385 for 4805 Fo > 4sig(Fo) and 0.0503 for all 5704 data REM 534 parameters refined using 1376 restraints END WGHT 0.0312 11.3395 REM Highest difference peak 1.006, deepest hole -1.358, 1-sigma level 0.103 Q1 1 0.3968 0.7196 0.8359 11.00000 0.05 1.01 Q2 1 0.5716 0.7157 0.7756 11.00000 0.05 0.97 Q3 1 0.4574 0.7210 0.7495 11.00000 0.05 0.93 Q4 1 0.4898 0.7224 0.8566 11.00000 0.05 0.85 Q5 1 0.4036 0.5982 0.5818 11.00000 0.05 0.72 Q6 1 0.6936 0.4979 0.8575 11.00000 0.05 0.58 Q7 1 0.7248 0.4585 0.8884 11.00000 0.05 0.55 Q8 1 0.4267 0.8581 0.7955 11.00000 0.05 0.53 Q9 1 0.4800 0.8830 0.8046 11.00000 0.05 0.48 Q10 1 0.5024 0.5208 0.7243 11.00000 0.05 0.47 Q11 1 0.7064 0.6584 0.6204 11.00000 0.05 0.47 Q12 1 0.5790 0.4859 0.7502 11.00000 0.05 0.44 Q13 1 0.3026 0.5189 0.6927 11.00000 0.05 0.42 Q14 1 0.4764 0.7251 0.5683 11.00000 0.05 0.42 Q15 1 0.7920 0.6158 0.6694 11.00000 0.05 0.38 Q16 1 0.1020 0.5875 0.6068 11.00000 0.05 0.38 Q17 1 0.3779 0.3863 0.9207 11.00000 0.05 0.37 Q18 1 0.5400 0.8601 0.8000 11.00000 0.05 0.37 Q19 1 0.8222 0.5892 0.7342 11.00000 0.05 0.37 Q20 1 0.3533 0.3998 0.8624 11.00000 0.05 0.35 ; _shelx_res_checksum 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45.60 -6 -3 0 855.31 40.50 -6 -3 0 891.31 33.60 -6 -3 0 915.61 47.60 -6 3 0 861.11 40.60 -6 3 0 880.11 33.40 -6 3 0 864.71 44.00 6 3 0 896.91 41.40 -6 3 0 817.82 33.00 6 3 0 877.41 47.70 6 3 0 860.51 35.80 -6 3 0 881.21 46.40 6 3 0 803.32 45.50 -6 3 0 854.91 42.20 -6 3 0 856.81 37.30 6 3 0 850.01 37.90 7 -3 0 400.86 32.90 -7 -3 0 372.76 34.70 -7 -3 0 436.66 21.10 -7 -3 0 342.97 27.50 -7 -3 0 396.26 19.80 -7 -3 0 396.06 25.60 7 -3 0 433.46 24.70 -7 -3 0 356.16 33.10 -7 -3 0 398.56 36.80 7 -3 0 451.75 23.00 7 -3 0 399.16 36.50 -7 3 0 374.76 27.50 -7 3 0 390.06 21.20 -7 3 0 382.76 20.80 -7 3 0 391.16 29.40 7 3 0 386.86 33.90 7 3 0 382.36 27.70 -7 3 0 409.66 25.00 7 3 0 401.66 24.20 7 3 0 395.66 25.60 -7 3 0 391.86 32.70 -7 3 0 428.56 33.30 -8 -3 0 280.07 36.80 8 -3 0 225.28 20.30 8 -3 0 239.48 19.90 -8 -3 0 251.57 17.10 8 -3 0 197.98 31.30 -8 -3 0 214.08 32.80 -8 -3 0 214.78 25.50 8 -3 0 228.88 30.50 -8 -3 0 306.37 37.90 -8 -3 0 220.48 17.40 -8 -3 0 230.08 23.00 -8 3 0 236.88 26.10 -8 3 0 197.38 24.30 -8 3 0 215.08 30.00 8 3 0 229.78 24.40 8 3 0 241.38 22.30 -8 3 0 195.48 18.10 -8 3 0 223.38 17.90 8 3 0 178.78 21.60 8 3 0 240.38 31.80 -8 3 0 218.38 33.80 -8 3 0 203.48 20.70 -9 -3 0 67.79 17.80 9 -3 0 70.49 15.70 9 -3 0 50.59 23.20 -9 -3 0 58.99 13.40 -9 -3 0 56.39 30.90 -9 -3 0 75.99 13.30 9 -3 0 31.10 29.20 -9 -3 0 70.69 27.30 9 -3 0 45.90 15.00 -9 -3 0 57.79 19.90 -9 -3 0 42.90 17.90 -9 -3 0 34.20 32.40 9 3 0 53.19 25.60 -9 3 0 17.60 23.90 -9 3 0 108.29 32.50 -9 3 0 53.89 16.00 -9 3 0 42.00 12.60 -9 3 0 54.39 31.30 9 3 0 36.70 17.60 -9 3 0 66.89 17.10 9 3 0 80.89 20.30 -9 3 0 62.39 19.90 -9 3 0 59.19 13.70 -9 3 0 43.50 20.00 10 -3 0 505.55 29.60 -10 -3 0 477.75 49.10 -10 -3 0 436.76 26.50 -10 -3 0 433.96 53.59 -10 -3 0 485.65 36.40 -10 -3 0 522.35 38.00 10 -3 0 530.25 46.30 -10 -3 0 473.35 27.30 -10 3 0 475.35 29.10 -10 3 0 485.85 47.00 -10 3 0 380.46 46.10 -10 3 0 545.45 40.90 10 3 0 489.35 48.50 -10 3 0 526.35 30.00 10 3 0 520.15 36.90 -10 3 0 510.45 33.00 -10 3 0 476.75 30.00 -11 -3 0 -2.00 16.30 11 -3 0 -8.40 23.30 -11 -3 0 19.90 14.50 -11 -3 0 -15.70 30.60 11 -3 0 -10.60 17.00 -11 -3 0 -1.90 13.00 -11 -3 0 39.70 18.10 -11 3 0 2.80 27.20 11 3 0 8.70 17.30 11 3 0 86.39 30.20 -11 3 0 14.10 13.60 -11 3 0 3.00 14.90 -11 3 0 -5.70 17.70 -12 -3 0 127.49 17.20 -12 -3 0 204.78 19.10 -12 -3 0 158.08 42.60 12 -3 0 135.89 33.70 -12 -3 0 103.99 25.30 -12 -3 0 147.29 36.60 -12 3 0 111.99 18.20 -12 3 0 220.48 45.40 -12 3 0 126.59 21.30 12 3 0 168.48 27.50 12 3 0 131.79 36.90 -12 3 0 148.89 33.10 -12 3 0 198.28 20.20 -12 3 0 127.49 28.60 0 -4 0 6086.09 189.78 0 -4 0 6265.57 189.88 0 -4 0 6302.07 187.38 0 -4 0 5811.12 189.88 0 -4 0 5856.41 191.08 0 4 0 6009.60 189.88 0 4 0 6321.17 189.88 0 4 0 6238.08 187.18 0 4 0 5917.21 191.38 0 4 0 5998.70 189.98 -1 -4 0 196.48 18.70 1 -4 0 196.58 14.60 -1 -4 0 191.18 8.50 1 -4 0 248.68 16.60 1 -4 0 188.98 14.60 1 -4 0 145.89 12.20 -1 -4 0 211.08 13.00 1 -4 0 214.58 16.10 -1 -4 0 182.58 14.60 -1 -4 0 195.88 15.20 -1 -4 0 205.48 17.30 -1 4 0 172.28 11.80 1 4 0 214.08 16.50 -1 4 0 201.68 14.10 -1 4 0 200.78 13.60 -1 4 0 190.48 15.90 1 4 0 203.98 18.20 -1 4 0 186.78 13.00 1 4 0 198.48 15.00 -1 4 0 201.68 11.90 1 4 0 164.58 14.70 1 4 0 192.48 13.50 -1 4 0 205.68 14.80 -2 -4 0 1959.70 69.79 2 -4 0 1861.61 66.59 -2 -4 0 1883.01 65.29 2 -4 0 1897.51 61.99 -2 -4 0 1998.20 61.09 -2 -4 0 1937.91 67.69 2 -4 0 1947.91 69.09 -2 -4 0 1857.41 69.89 -2 -4 0 1942.11 69.39 -2 -4 0 2089.89 63.89 2 -4 0 2017.60 67.79 2 -4 0 1911.41 66.29 -2 4 0 1884.71 66.39 2 4 0 2012.70 61.19 2 4 0 1987.70 70.79 -2 4 0 1842.22 61.79 -2 4 0 1721.13 65.09 -2 4 0 1928.21 66.39 -2 4 0 1994.50 68.39 2 4 0 1998.50 65.59 -2 4 0 1897.71 66.89 2 4 0 2041.50 63.59 -2 4 0 1918.51 64.79 2 4 0 1994.90 68.19 3 -4 0 282.47 17.50 -3 -4 0 303.27 13.60 3 -4 0 286.87 11.80 -3 -4 0 256.37 18.60 3 -4 0 268.97 19.60 -3 -4 0 286.77 21.30 3 -4 0 271.67 20.70 -3 -4 0 296.07 21.80 -3 -4 0 311.67 23.30 -3 -4 0 311.67 14.50 -3 -4 0 270.37 17.20 -3 4 0 289.67 16.30 3 4 0 280.47 21.50 -3 4 0 301.37 18.90 3 4 0 296.87 19.50 3 4 0 304.27 13.60 3 4 0 280.77 14.30 -3 4 0 306.87 20.30 -3 4 0 288.87 17.50 3 4 0 283.77 17.20 -3 4 0 288.17 17.90 -3 4 0 257.57 11.70 -3 4 0 313.17 20.00 4 -4 0 338.27 19.50 -4 -4 0 337.17 17.30 4 -4 0 316.87 19.90 4 -4 0 353.66 30.10 -4 -4 0 323.87 22.40 -4 -4 0 341.17 16.00 4 -4 0 294.87 22.60 -4 -4 0 301.47 25.50 -4 -4 0 334.37 28.30 4 4 0 346.17 28.00 -4 4 0 332.07 13.70 4 4 0 341.47 17.30 4 4 0 334.47 16.30 4 4 0 336.27 26.10 4 4 0 331.67 22.10 -4 4 0 343.07 23.10 -4 4 0 316.97 29.30 -4 4 0 342.27 20.80 4 4 0 341.07 23.10 -4 4 0 335.77 24.00 -5 -4 0 210.78 13.40 -5 -4 0 219.88 28.40 5 -4 0 179.38 16.60 5 -4 0 200.98 22.60 -5 -4 0 187.98 25.20 -5 -4 0 187.08 17.60 -5 -4 0 174.88 15.70 5 -4 0 169.48 16.60 5 -4 0 200.28 25.00 -5 -4 0 172.78 19.90 -5 4 0 153.18 10.50 -5 4 0 178.18 11.70 -5 4 0 143.79 17.80 5 4 0 183.38 15.10 5 4 0 193.18 13.10 5 4 0 159.98 19.00 5 4 0 190.78 18.90 -5 4 0 174.88 17.60 5 4 0 201.88 25.20 -5 4 0 195.88 23.60 5 4 0 230.98 28.00 -5 4 0 186.68 20.10 -5 4 0 196.08 24.10 -6 -4 0 86.19 16.40 6 -4 0 63.29 20.40 6 -4 0 69.69 13.40 6 -4 0 65.49 17.70 -6 -4 0 67.29 18.80 -6 -4 0 66.99 9.50 6 -4 0 78.99 12.90 -6 -4 0 78.19 12.90 -6 -4 0 61.89 20.50 -6 4 0 65.39 8.80 6 4 0 79.39 22.10 -6 4 0 63.39 18.00 6 4 0 59.99 11.40 6 4 0 67.19 18.80 -6 4 0 55.19 13.70 -6 4 0 50.89 12.80 6 4 0 85.99 10.10 -6 4 0 66.39 8.50 -6 4 0 58.49 14.90 -6 4 0 55.09 17.60 6 4 0 88.99 14.60 6 4 0 56.79 15.20 -7 -4 0 97.29 24.50 -7 -4 0 120.89 19.50 7 -4 0 93.59 23.60 -7 -4 0 114.89 26.10 -7 -4 0 111.59 12.50 7 -4 0 122.19 16.70 7 -4 0 84.09 21.10 -7 -4 0 93.19 15.10 -7 -4 0 124.29 25.70 7 -4 0 132.29 15.90 -7 -4 0 116.19 12.00 7 4 0 87.49 22.50 -7 4 0 95.19 11.80 7 4 0 127.49 16.70 -7 4 0 103.39 23.10 -7 4 0 80.89 17.50 7 4 0 110.69 25.80 -7 4 0 116.29 18.60 -7 4 0 107.39 11.50 -7 4 0 99.69 22.10 7 4 0 121.89 19.70 -7 4 0 123.29 17.40 7 4 0 132.89 16.90 8 -4 0 324.77 33.60 -8 -4 0 320.87 19.30 -8 -4 0 341.67 25.90 8 -4 0 313.27 23.30 -8 -4 0 284.07 28.00 -8 -4 0 368.96 46.40 -8 -4 0 327.27 20.30 8 -4 0 276.37 22.90 8 -4 0 280.27 34.20 -8 -4 0 420.46 62.89 -8 -4 0 336.27 40.40 -8 4 0 334.07 25.80 -8 4 0 297.17 18.80 -8 4 0 347.57 19.50 -8 4 0 285.67 41.10 8 4 0 294.67 27.90 8 4 0 373.06 38.10 -8 4 0 288.37 33.70 8 4 0 335.07 25.40 8 4 0 316.37 25.30 -8 4 0 301.87 41.50 -8 4 0 291.87 28.90 -9 -4 0 196.28 37.00 9 -4 0 186.18 22.70 -9 -4 0 180.28 23.80 9 -4 0 180.38 20.90 -9 -4 0 191.38 27.20 9 -4 0 193.08 33.20 -9 -4 0 169.68 18.40 -9 -4 0 210.88 37.40 -9 -4 0 130.29 35.20 -9 -4 0 121.89 21.60 9 -4 0 160.68 57.89 -9 -4 0 183.68 17.40 -9 4 0 154.78 29.80 9 4 0 196.28 34.90 -9 4 0 176.18 26.60 -9 4 0 177.88 28.30 9 4 0 211.18 25.90 -9 4 0 173.88 23.20 -9 4 0 172.98 17.80 -9 4 0 153.58 37.20 9 4 0 146.89 24.80 -9 4 0 140.39 17.20 -10 -4 0 87.29 18.40 -10 -4 0 64.39 12.90 -10 -4 0 41.20 26.40 -10 -4 0 49.90 18.50 -10 -4 0 78.99 34.40 10 -4 0 89.49 27.00 10 -4 0 83.89 35.10 -10 -4 0 88.49 22.60 -10 -4 0 75.09 14.20 10 -4 0 63.69 18.00 10 -4 0 65.49 17.30 -10 4 0 55.69 12.90 10 4 0 89.39 22.10 -10 4 0 45.70 16.30 -10 4 0 65.49 18.90 10 4 0 40.90 26.10 -10 4 0 65.19 12.90 10 4 0 106.49 20.00 -10 4 0 68.69 26.40 -10 4 0 58.69 22.00 -10 4 0 41.60 32.00 -11 -4 0 189.78 38.40 11 -4 0 218.98 37.40 11 -4 0 286.37 25.50 -11 -4 0 225.78 31.50 -11 -4 0 163.28 41.20 -11 -4 0 181.68 23.50 -11 -4 0 194.38 26.90 -11 -4 0 205.78 29.00 -11 4 0 162.68 30.60 -11 4 0 214.88 26.10 -11 4 0 166.08 20.00 11 4 0 176.98 22.80 11 4 0 187.48 38.10 -11 4 0 233.78 42.60 11 4 0 203.28 37.80 -11 4 0 229.78 29.80 -11 4 0 272.17 20.00 12 -4 0 26.00 24.70 -12 -4 0 33.80 20.10 -12 -4 0 23.50 27.90 12 -4 0 63.19 17.80 -12 -4 0 28.20 33.40 12 -4 0 40.60 19.20 -12 4 0 61.09 12.10 12 4 0 43.60 19.70 -12 4 0 13.20 16.40 -12 4 0 26.50 22.20 -12 4 0 23.90 31.80 -12 4 0 83.49 16.60 -12 4 0 40.40 13.40 0 -5 0 -11.10 6.40 0 -5 0 0.10 4.60 0 -5 0 8.70 8.50 0 -5 0 2.60 7.50 0 -5 0 -0.70 9.40 0 -5 0 4.70 10.70 0 5 0 19.90 11.50 0 5 0 5.20 7.90 0 5 0 -3.00 4.40 0 5 0 -7.50 7.70 0 5 0 4.40 8.20 0 5 0 5.70 7.40 1 -5 0 4474.35 144.09 -1 -5 0 4563.64 146.19 1 -5 0 4389.86 146.09 -1 -5 0 4659.13 140.89 1 -5 0 4385.06 146.39 1 -5 0 4749.22 148.79 1 -5 0 4392.66 145.79 -1 -5 0 4739.93 145.19 -1 -5 0 4587.34 146.99 -1 -5 0 4791.52 149.09 -1 -5 0 4491.45 149.59 1 5 0 4586.34 145.99 1 5 0 4401.86 149.39 1 5 0 4526.15 147.29 -1 5 0 4415.06 145.29 1 5 0 4730.53 149.88 1 5 0 4819.62 144.99 1 5 0 4626.04 140.79 -1 5 0 4691.43 144.29 -1 5 0 4517.05 145.69 -1 5 0 4350.36 146.39 -1 5 0 4776.52 148.79 -1 5 0 4656.23 146.39 -1 5 0 4471.65 144.09 2 -5 0 0.10 10.10 2 -5 0 -6.10 7.20 2 -5 0 -2.70 8.10 -2 -5 0 -7.80 8.20 -2 -5 0 -7.30 6.80 -2 -5 0 6.80 8.90 2 -5 0 2.30 9.60 -2 -5 0 5.10 10.60 2 -5 0 4.70 5.90 -2 -5 0 -7.30 3.00 -2 -5 0 -5.20 7.80 -2 -5 0 0.60 6.10 2 5 0 2.00 8.30 -2 5 0 -2.30 4.80 2 5 0 11.60 12.60 -2 5 0 9.00 7.30 -2 5 0 8.60 7.30 -2 5 0 3.40 6.40 -2 5 0 9.60 7.90 2 5 0 2.00 6.50 2 5 0 8.10 9.10 2 5 0 0.80 8.80 -2 5 0 4.20 10.30 2 5 0 9.00 3.60 -2 5 0 0.50 6.90 -3 -5 0 1792.82 73.09 -3 -5 0 1956.10 72.99 3 -5 0 1935.41 62.39 3 -5 0 1966.20 72.49 -3 -5 0 2050.99 64.79 -3 -5 0 2058.89 73.79 -3 -5 0 1990.00 62.19 3 -5 0 1925.81 68.49 -3 -5 0 1924.11 67.09 -3 -5 0 1786.92 69.39 3 -5 0 1947.91 68.99 -3 5 0 1838.32 61.89 3 5 0 1990.00 71.09 -3 5 0 1944.41 66.29 -3 5 0 1952.70 70.89 -3 5 0 2019.70 68.99 3 5 0 1955.00 67.09 3 5 0 1991.50 64.49 3 5 0 1933.21 73.79 -3 5 0 1864.11 69.89 -3 5 0 1978.50 68.59 -3 5 0 1864.61 68.79 3 5 0 1921.81 62.39 -4 -5 0 17.40 7.90 -4 -5 0 26.20 15.30 4 -5 0 8.90 13.20 -4 -5 0 11.90 12.40 -4 -5 0 34.60 7.90 -4 -5 0 32.90 12.50 -4 -5 0 33.30 19.30 4 -5 0 12.80 11.40 4 -5 0 19.10 12.70 4 -5 0 16.50 15.70 -4 -5 0 7.20 13.80 4 5 0 12.80 11.90 -4 5 0 26.80 12.30 -4 5 0 12.00 14.40 4 5 0 24.70 12.40 -4 5 0 14.10 11.00 4 5 0 12.80 6.90 -4 5 0 11.10 13.10 -4 5 0 24.90 12.30 4 5 0 21.70 15.90 4 5 0 24.20 8.40 -5 -5 0 552.04 32.00 5 -5 0 598.14 38.40 -5 -5 0 603.74 26.00 5 -5 0 541.95 29.60 -5 -5 0 560.34 37.00 -5 -5 0 604.94 24.50 5 -5 0 552.44 33.40 -5 -5 0 532.75 27.80 5 -5 0 542.95 27.50 -5 -5 0 538.45 36.40 -5 -5 0 591.44 36.90 -5 5 0 556.94 32.60 5 5 0 568.04 32.20 -5 5 0 539.95 35.50 5 5 0 587.94 24.50 -5 5 0 536.95 30.20 5 5 0 579.44 25.70 5 5 0 592.54 28.70 -5 5 0 555.54 29.70 -5 5 0 596.94 34.30 -6 -5 0 597.14 34.50 6 -5 0 611.14 32.10 -6 -5 0 613.84 40.30 6 -5 0 576.44 38.80 6 -5 0 616.44 29.70 -6 -5 0 540.35 40.70 -6 -5 0 622.34 25.90 -6 -5 0 704.33 42.00 6 -5 0 576.74 36.00 -6 -5 0 572.14 28.80 -6 -5 0 650.63 29.30 6 5 0 594.24 34.80 6 5 0 650.43 40.80 -6 5 0 619.74 36.80 6 5 0 605.44 25.50 -6 5 0 663.83 32.60 6 5 0 639.64 40.60 6 5 0 619.34 30.60 -6 5 0 613.54 34.00 -6 5 0 606.54 39.50 6 5 0 642.34 29.40 -6 5 0 601.14 36.00 -7 -5 0 614.14 35.10 7 -5 0 643.24 39.50 -7 -5 0 679.23 45.60 -7 -5 0 643.54 27.20 7 -5 0 585.84 32.90 -7 -5 0 723.33 47.20 7 -5 0 543.65 43.50 -7 -5 0 613.04 43.20 -7 -5 0 691.93 38.30 7 -5 0 661.83 31.60 -7 5 0 620.54 42.60 -7 5 0 608.14 39.80 -7 5 0 644.04 38.70 7 5 0 610.04 42.80 -7 5 0 652.13 33.90 7 5 0 604.04 37.40 7 5 0 635.44 32.00 7 5 0 623.94 26.70 -7 5 0 599.44 35.70 7 5 0 614.14 44.90 -8 -5 0 258.17 35.40 -8 -5 0 217.38 17.80 8 -5 0 189.58 32.90 -8 -5 0 282.97 38.80 8 -5 0 190.88 28.70 8 -5 0 250.57 23.20 -8 -5 0 272.97 43.10 -8 -5 0 177.58 16.40 -8 -5 0 216.68 35.80 -8 -5 0 209.18 22.50 -8 -5 0 251.97 29.40 8 5 0 262.07 27.60 -8 5 0 208.88 28.30 8 5 0 193.88 19.70 8 5 0 222.68 33.90 -8 5 0 184.38 14.50 8 5 0 280.67 44.20 -8 5 0 212.88 13.90 8 5 0 188.18 22.90 -8 5 0 220.08 27.20 -8 5 0 172.08 28.70 -8 5 0 213.38 31.50 -8 5 0 227.98 24.50 9 -5 0 69.09 29.20 9 -5 0 113.69 18.70 -9 -5 0 69.19 36.70 9 -5 0 71.89 18.30 -9 -5 0 105.79 14.10 -9 -5 0 96.19 29.50 -9 -5 0 93.79 19.40 -9 -5 0 91.19 14.30 -9 -5 0 100.39 36.80 9 -5 0 94.59 26.70 -9 -5 0 125.79 20.20 -9 -5 0 116.59 23.80 -9 5 0 86.49 12.10 9 5 0 85.89 21.60 -9 5 0 87.29 23.70 -9 5 0 81.89 26.20 -9 5 0 81.99 19.20 9 5 0 84.09 19.40 -9 5 0 114.79 12.60 9 5 0 97.69 29.80 -10 -5 0 129.49 32.60 -10 -5 0 131.99 15.10 -10 -5 0 121.09 22.30 -10 -5 0 153.38 27.40 10 -5 0 168.28 25.00 10 -5 0 121.09 28.60 10 -5 0 92.69 35.40 -10 -5 0 168.48 23.40 10 -5 0 137.49 22.90 -10 -5 0 136.09 16.00 -10 -5 0 155.48 39.10 10 5 0 125.99 25.20 -10 5 0 115.49 13.30 -10 5 0 141.09 30.70 10 5 0 111.39 21.20 -10 5 0 128.69 27.50 -10 5 0 143.19 22.90 -11 -5 0 83.09 21.00 -11 -5 0 91.69 14.30 11 -5 0 94.59 19.90 11 -5 0 45.50 34.40 11 -5 0 103.09 30.20 -11 -5 0 92.89 34.50 -11 -5 0 54.59 29.40 -11 -5 0 103.19 13.80 -11 5 0 107.59 26.90 -11 5 0 122.29 18.10 11 5 0 136.89 27.10 -11 5 0 91.29 21.30 -12 -5 0 -15.70 29.70 -12 -5 0 68.49 31.80 -12 -5 0 11.00 11.30 -12 -5 0 10.90 18.80 12 -5 0 40.10 26.30 -12 -5 0 36.10 12.40 12 -5 0 35.20 16.20 -12 5 0 55.59 19.20 12 5 0 24.00 18.90 -12 5 0 29.60 28.80 -12 5 0 7.00 19.90 0 -6 0 1429.46 52.19 0 -6 0 1460.65 54.99 0 -6 0 1365.86 52.59 0 -6 0 1411.56 54.09 0 -6 0 1489.25 48.50 0 -6 0 1452.25 52.09 0 6 0 1462.05 48.10 0 6 0 1429.06 51.89 0 6 0 1426.66 54.39 0 6 0 1409.36 51.89 0 6 0 1357.26 52.09 0 6 0 1455.15 55.09 -1 -6 0 572.04 20.50 -1 -6 0 582.14 25.40 -1 -6 0 532.15 29.30 -1 -6 0 588.24 30.20 -1 -6 0 582.34 27.20 1 -6 0 557.44 29.30 1 -6 0 578.34 26.30 1 -6 0 535.75 24.50 -1 -6 0 570.44 27.40 1 -6 0 595.44 28.10 1 -6 0 540.15 26.60 -1 6 0 551.64 23.50 -1 6 0 538.35 24.50 -1 6 0 600.44 29.80 -1 6 0 534.65 26.90 -1 6 0 565.24 26.20 1 6 0 581.64 27.00 1 6 0 574.04 25.10 -1 6 0 539.95 24.60 1 6 0 565.74 27.20 1 6 0 592.64 30.30 1 6 0 578.24 29.70 -1 6 0 569.54 26.40 1 6 0 551.34 20.30 -2 -6 0 116.39 15.20 -2 -6 0 122.39 12.20 2 -6 0 116.09 14.30 2 -6 0 137.89 15.70 2 -6 0 153.78 18.20 -2 -6 0 196.98 22.40 -2 -6 0 131.69 18.30 2 -6 0 97.49 11.50 -2 -6 0 160.68 16.90 2 -6 0 154.38 18.60 -2 -6 0 134.19 7.30 -2 6 0 127.69 11.20 2 6 0 145.89 8.00 -2 6 0 151.18 15.50 -2 6 0 122.99 13.40 2 6 0 138.09 16.60 -2 6 0 158.28 16.90 -2 6 0 132.79 15.40 2 6 0 133.19 12.10 -2 6 0 140.69 13.30 2 6 0 156.38 21.40 -2 6 0 134.69 16.40 2 6 0 134.59 16.30 2 6 0 142.69 18.30 -3 -6 0 8.70 8.60 -3 -6 0 44.80 18.50 3 -6 0 5.40 15.00 3 -6 0 9.40 12.70 -3 -6 0 6.10 11.40 -3 -6 0 19.70 16.20 -3 -6 0 21.10 24.10 3 -6 0 14.70 12.50 3 -6 0 20.40 11.30 -3 -6 0 20.10 5.60 3 -6 0 12.90 7.40 -3 6 0 12.60 10.10 -3 6 0 2.50 15.70 3 6 0 14.60 5.00 3 6 0 14.10 12.20 -3 6 0 21.00 11.60 -3 6 0 18.40 12.80 3 6 0 10.00 8.30 3 6 0 13.60 12.70 -3 6 0 16.40 11.70 -3 6 0 21.80 7.20 4 -6 0 1392.66 55.09 -4 -6 0 1386.36 61.29 4 -6 0 1310.97 44.80 -4 -6 0 1401.16 49.00 4 -6 0 1375.56 58.79 -4 -6 0 1351.56 56.29 -4 -6 0 1313.87 51.89 4 -6 0 1359.46 53.99 -4 -6 0 1432.26 60.59 -4 -6 0 1422.66 59.89 -4 -6 0 1417.36 46.60 -4 6 0 1339.47 56.09 -4 6 0 1416.46 54.79 4 6 0 1423.86 56.89 -4 6 0 1327.77 53.99 4 6 0 1423.36 62.19 4 6 0 1426.16 47.00 -4 6 0 1303.07 51.09 4 6 0 1317.77 52.19 4 6 0 1403.96 48.80 -4 6 0 1365.16 57.19 -4 6 0 1253.97 44.50 -4 6 0 1334.17 55.39 -5 -6 0 513.05 37.20 -5 -6 0 476.55 22.70 -5 -6 0 472.85 34.90 -5 -6 0 536.25 23.00 5 -6 0 501.65 27.10 -5 -6 0 500.05 36.10 5 -6 0 457.55 27.80 5 -6 0 504.45 36.30 -5 -6 0 458.25 26.40 5 -6 0 434.86 31.30 -5 -6 0 505.45 31.00 -5 6 0 470.25 28.80 -5 6 0 494.35 32.20 5 6 0 507.85 23.20 5 6 0 530.55 31.40 -5 6 0 439.66 30.10 5 6 0 472.75 27.00 5 6 0 505.35 37.50 -5 6 0 497.85 34.20 5 6 0 499.25 22.70 -5 6 0 490.45 28.60 -6 -6 0 271.77 16.90 -6 -6 0 268.57 18.90 6 -6 0 285.57 21.90 6 -6 0 279.07 32.80 -6 -6 0 252.67 21.80 6 -6 0 265.87 22.20 -6 -6 0 295.37 25.90 -6 -6 0 286.77 29.40 6 -6 0 264.47 26.40 -6 -6 0 308.37 33.40 -6 -6 0 247.48 30.50 6 6 0 287.27 22.20 -6 6 0 282.27 27.70 6 6 0 275.27 18.20 6 6 0 300.17 27.10 6 6 0 294.37 17.60 6 6 0 304.07 30.60 -6 6 0 283.57 25.60 -6 6 0 284.07 28.70 -6 6 0 278.77 24.00 -6 6 0 286.57 23.30 -7 -6 0 345.47 22.90 -7 -6 0 333.17 19.40 7 -6 0 368.26 25.50 -7 -6 0 403.76 36.50 7 -6 0 360.96 32.40 7 -6 0 292.57 24.60 -7 -6 0 429.46 40.70 -7 -6 0 300.37 33.80 -7 -6 0 344.17 29.60 7 -6 0 328.37 37.30 -7 6 0 344.37 30.30 -7 6 0 326.57 28.40 7 6 0 354.86 22.50 -7 6 0 309.07 31.70 7 6 0 366.46 29.50 7 6 0 347.17 24.90 -7 6 0 374.86 26.80 7 6 0 350.76 19.80 -7 6 0 324.47 32.10 7 6 0 335.57 37.40 8 -6 0 105.79 24.20 -8 -6 0 126.29 30.40 8 -6 0 139.49 21.80 -8 -6 0 74.09 27.30 8 -6 0 74.69 18.10 -8 -6 0 118.99 18.80 -8 -6 0 127.69 31.70 -8 -6 0 80.79 17.00 -8 -6 0 77.89 27.10 8 -6 0 84.89 30.80 -8 -6 0 77.79 13.10 -8 6 0 85.19 26.30 -8 6 0 90.29 24.80 8 6 0 110.09 22.70 -8 6 0 109.19 20.70 -8 6 0 85.69 21.40 8 6 0 118.29 19.10 8 6 0 123.19 31.80 8 6 0 110.79 13.00 -8 6 0 118.29 23.20 -9 -6 0 277.07 33.60 9 -6 0 197.98 39.30 -9 -6 0 216.48 25.80 9 -6 0 236.48 25.50 -9 -6 0 181.98 19.30 9 -6 0 234.78 25.50 -9 -6 0 159.88 36.90 9 -6 0 235.38 33.40 -9 -6 0 189.58 23.00 -9 -6 0 204.88 18.10 -9 -6 0 198.48 36.30 9 6 0 188.28 27.40 -9 6 0 205.28 25.70 -9 6 0 169.48 30.70 9 6 0 190.18 22.90 -9 6 0 236.88 32.90 -10 -6 0 -5.20 15.40 -10 -6 0 46.90 15.20 10 -6 0 -5.10 30.10 -10 -6 0 2.10 10.60 -10 -6 0 -27.10 19.20 10 -6 0 -3.70 20.70 10 -6 0 5.50 16.20 -10 -6 0 -14.40 27.10 -10 -6 0 2.80 10.60 10 -6 0 4.50 15.40 10 6 0 -4.50 17.00 -10 6 0 -15.40 16.00 -10 6 0 1.40 22.90 -10 6 0 -9.00 14.30 10 6 0 0.60 15.30 -11 -6 0 207.38 43.90 -11 -6 0 226.88 43.10 -11 -6 0 263.07 19.90 11 -6 0 356.46 30.60 -11 -6 0 236.18 29.20 11 -6 0 296.17 39.20 11 -6 0 241.78 44.90 11 -6 0 263.67 29.50 -11 -6 0 245.28 19.10 -11 6 0 269.27 29.80 -11 6 0 272.17 37.20 -12 -6 0 22.60 10.10 -12 -6 0 -37.30 29.60 12 -6 0 21.00 25.00 -12 -6 0 -22.40 28.30 -12 -6 0 29.00 28.80 12 -6 0 14.30 53.09 12 -6 0 10.60 16.20 -12 -6 0 -2.10 9.50 -12 6 0 60.19 52.59 12 6 0 9.40 20.00 -12 6 0 -29.80 18.30 -12 6 0 28.80 18.50 0 -7 0 -5.00 12.10 0 -7 0 7.90 10.40 0 -7 0 -9.30 10.00 0 -7 0 2.80 9.50 0 -7 0 9.10 10.10 0 7 0 -15.70 8.10 0 7 0 8.00 9.80 0 7 0 0.70 9.10 0 7 0 8.50 9.70 0 7 0 2.30 5.40 0 7 0 4.70 6.20 0 7 0 6.30 11.50 1 -7 0 1943.91 72.19 1 -7 0 2011.30 75.59 -1 -7 0 2045.60 72.69 1 -7 0 1990.70 69.59 -1 -7 0 1976.40 75.59 -1 -7 0 1972.60 72.79 1 -7 0 2056.29 75.39 -1 -7 0 2033.20 64.89 1 -7 0 1944.01 72.49 -1 -7 0 2104.89 70.89 -1 -7 0 2116.89 75.79 1 7 0 2105.49 70.59 1 7 0 1931.61 75.59 1 7 0 2137.89 76.99 -1 7 0 1939.31 72.59 -1 7 0 2075.59 72.49 -1 7 0 1966.50 69.99 1 7 0 1947.21 64.49 -1 7 0 2114.39 75.69 1 7 0 2016.80 71.99 -1 7 0 1979.50 71.49 -1 7 0 1943.61 69.69 1 7 0 1992.00 72.89 -1 7 0 2003.70 68.19 2 -7 0 90.59 15.70 2 -7 0 90.79 18.50 2 -7 0 59.79 15.50 2 -7 0 100.39 17.40 -2 -7 0 74.29 18.70 2 -7 0 85.29 11.80 -2 -7 0 74.69 16.40 -2 -7 0 93.39 14.40 -2 -7 0 82.69 16.40 -2 -7 0 73.19 7.10 -2 7 0 100.89 17.30 2 7 0 74.29 18.10 -2 7 0 90.39 15.50 2 7 0 73.99 7.90 -2 7 0 77.59 15.90 -2 7 0 101.09 15.10 2 7 0 77.69 12.60 -2 7 0 84.19 13.00 2 7 0 89.59 17.10 -2 7 0 86.39 21.20 -2 7 0 70.69 12.00 2 7 0 99.99 19.40 2 7 0 129.49 34.80 -3 -7 0 2784.02 100.39 -3 -7 0 2790.32 105.99 3 -7 0 2780.62 102.19 3 -7 0 2725.13 92.19 -3 -7 0 2766.82 97.49 -3 -7 0 3063.89 105.09 3 -7 0 2899.61 99.59 3 -7 0 2726.73 97.59 -3 -7 0 2986.60 95.39 -3 -7 0 2895.41 103.99 -3 -7 0 2903.31 88.69 3 -7 0 2911.01 99.89 -3 7 0 2716.33 104.39 3 7 0 2835.72 104.99 3 7 0 2881.31 101.89 -3 7 0 2946.21 99.59 -3 7 0 2772.32 98.69 -3 7 0 2791.52 98.09 -3 7 0 2966.10 103.49 3 7 0 2945.21 94.79 -3 7 0 2896.91 97.19 3 7 0 2918.31 98.09 3 7 0 2917.91 89.29 -3 7 0 2657.13 91.89 -4 -7 0 374.26 30.00 4 -7 0 314.67 15.70 -4 -7 0 335.27 29.10 -4 -7 0 335.77 15.20 4 -7 0 324.97 26.60 -4 -7 0 306.87 23.10 -4 -7 0 337.17 28.70 -4 -7 0 337.57 19.70 4 -7 0 321.67 23.40 4 -7 0 297.67 23.20 4 -7 0 333.37 30.10 -4 -7 0 304.17 24.60 -4 7 0 315.67 23.00 -4 7 0 285.87 14.80 4 7 0 337.87 15.00 -4 7 0 286.17 23.40 4 7 0 298.37 24.70 4 7 0 298.87 31.50 4 7 0 292.67 22.90 -4 7 0 327.57 28.00 -4 7 0 324.47 25.60 -4 7 0 294.37 22.20 4 7 0 345.97 20.00 -4 7 0 299.57 22.20 5 -7 0 1818.82 71.39 -5 -7 0 1957.90 75.09 -5 -7 0 2027.60 80.59 -5 -7 0 1896.11 79.29 -5 -7 0 1906.41 65.39 -5 -7 0 1807.52 68.29 5 -7 0 1861.91 73.09 5 -7 0 1830.92 76.99 -5 -7 0 1920.01 62.99 -5 -7 0 1833.82 80.19 5 7 0 1878.91 69.19 5 7 0 1834.12 79.59 -5 7 0 1921.41 76.69 -5 7 0 1739.93 72.59 -5 7 0 1845.82 72.09 5 7 0 1997.50 65.69 5 7 0 1955.50 75.39 -5 7 0 1852.61 71.29 5 7 0 1909.61 63.59 -5 7 0 1824.02 74.79 6 -7 0 167.28 20.80 -6 -7 0 157.98 15.50 -6 -7 0 168.88 27.40 -6 -7 0 182.38 28.30 -6 -7 0 159.48 15.30 6 -7 0 179.08 28.10 6 -7 0 199.38 24.90 6 -7 0 193.38 21.30 -6 -7 0 153.08 23.10 -6 -7 0 202.58 29.00 -6 7 0 202.58 25.40 -6 7 0 150.28 24.70 6 7 0 168.68 14.30 -6 7 0 169.98 21.20 -6 7 0 219.18 26.90 6 7 0 182.08 20.70 6 7 0 179.08 28.80 6 7 0 171.58 23.70 -6 7 0 190.38 22.70 6 7 0 155.98 15.50 -7 -7 0 693.53 30.40 7 -7 0 657.83 41.50 7 -7 0 748.43 37.50 7 -7 0 647.64 37.40 -7 -7 0 716.93 32.30 -7 -7 0 709.33 42.40 -7 -7 0 692.03 48.40 -7 -7 0 700.83 50.09 7 -7 0 675.63 46.70 -7 -7 0 653.63 39.40 -7 -7 0 716.03 50.39 -7 7 0 747.13 43.60 7 7 0 734.53 36.50 -7 7 0 627.04 42.40 7 7 0 663.03 30.00 -7 7 0 696.63 38.50 -7 7 0 761.62 42.30 -7 7 0 690.13 47.30 7 7 0 696.83 32.30 7 7 0 827.32 52.99 7 7 0 699.03 42.30 8 -7 0 88.09 29.80 8 -7 0 118.09 21.70 8 -7 0 104.49 20.80 -8 -7 0 137.89 15.40 8 -7 0 122.89 26.40 -8 -7 0 137.09 25.90 -8 -7 0 154.08 35.80 -8 -7 0 125.09 19.30 -8 -7 0 117.79 17.70 -8 -7 0 145.49 34.00 -8 -7 0 115.79 28.50 8 7 0 109.09 21.00 8 7 0 162.08 34.50 -8 7 0 168.68 27.00 -8 7 0 81.39 26.30 -8 7 0 128.49 26.10 -8 7 0 103.29 21.50 -8 7 0 107.69 27.60 8 7 0 125.29 14.70 8 7 0 122.49 24.00 -9 -7 0 97.89 18.70 -9 -7 0 105.19 31.00 9 -7 0 112.19 35.30 9 -7 0 136.29 24.10 9 -7 0 174.68 30.40 -9 -7 0 108.89 31.00 -9 -7 0 160.58 20.20 -9 -7 0 133.99 34.30 -9 -7 0 153.98 16.70 9 -7 0 163.98 24.60 -9 -7 0 117.69 15.40 9 7 0 130.69 21.00 -9 7 0 126.29 23.10 -9 7 0 120.19 24.60 -9 7 0 89.69 28.80 10 -7 0 35.00 23.10 10 -7 0 37.50 17.90 -10 -7 0 32.00 27.80 -10 -7 0 -10.10 14.40 -10 -7 0 2.50 22.40 10 -7 0 -8.10 27.00 -10 -7 0 8.50 10.60 10 -7 0 13.90 17.40 -10 -7 0 24.30 11.20 -10 7 0 -15.20 16.70 -10 7 0 14.40 24.10 10 7 0 11.40 19.60 -10 7 0 6.90 16.60 10 7 0 8.50 15.70 -11 -7 0 36.60 11.00 -11 -7 0 78.79 26.90 11 -7 0 40.80 25.40 -11 -7 0 10.40 10.50 11 -7 0 5.10 29.00 -11 -7 0 -26.70 15.10 11 -7 0 -4.30 17.10 -11 -7 0 -10.40 30.50 -11 7 0 2.50 17.80 -11 7 0 -18.10 17.90 11 7 0 2.80 19.60 11 7 0 -7.00 16.00 -12 -7 0 51.89 34.40 -12 -7 0 -43.00 16.00 -12 -7 0 -2.60 8.60 -12 -7 0 4.20 9.40 -12 -7 0 2.70 33.30 12 -7 0 27.10 36.70 12 -7 0 28.40 24.50 12 -7 0 59.49 19.30 -12 7 0 -18.70 16.60 12 7 0 10.60 25.90 12 7 0 13.60 19.80 -12 7 0 -7.80 21.80 0 -8 0 1882.21 72.89 0 -8 0 2060.59 75.29 0 -8 0 2023.40 76.59 0 -8 0 1898.31 71.49 0 -8 0 1853.21 71.09 0 8 0 1882.11 72.09 0 8 0 2017.90 71.49 0 8 0 1955.00 67.49 0 8 0 2069.39 66.29 0 8 0 1959.70 74.99 0 8 0 2050.39 76.19 0 8 0 1964.80 71.99 1 -8 0 16.60 13.30 -1 -8 0 7.20 12.30 -1 -8 0 36.20 18.30 1 -8 0 -0.70 12.70 1 -8 0 -1.80 11.40 1 -8 0 22.50 11.00 -1 -8 0 26.90 15.50 -1 -8 0 6.20 14.10 -1 -8 0 11.00 6.30 1 -8 0 -12.60 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1150.18 36.90 -1 1 2 1193.08 36.90 -1 1 2 1137.69 38.40 1 1 -2 1122.79 39.70 -1 1 2 1046.40 37.50 -1 1 2 1085.59 35.90 1 1 -2 1083.09 36.30 1 1 -2 1070.09 37.20 -1 1 2 1071.99 37.40 1 1 -2 1184.38 38.40 -1 1 2 1180.58 38.10 1 1 -2 1206.98 36.30 1 1 -2 1162.28 36.90 0 -1 -2 1900.11 58.19 0 -1 -2 1870.71 59.69 0 -1 -2 1921.31 58.19 0 -1 2 1827.62 58.39 0 -1 -2 1948.01 59.29 0 -1 -2 1767.12 58.89 0 -1 2 1843.02 58.99 0 -1 2 1815.02 58.29 0 -1 2 1853.41 57.29 0 -1 -2 1751.12 58.59 0 -1 2 1873.41 60.39 0 1 2 1768.82 58.89 0 1 -2 1871.91 58.39 0 1 -2 1766.62 58.29 0 1 -2 1845.82 58.99 0 1 2 1986.60 57.99 0 1 -2 1781.12 60.29 0 1 2 1811.62 58.89 0 1 -2 1774.82 57.29 0 1 2 1829.42 58.09 0 1 2 1910.51 58.29 0 1 2 1869.91 59.49 0 1 2 1855.81 58.69 -1 -1 -2 1973.60 65.49 1 -1 2 2019.80 64.39 1 -1 2 1973.00 66.09 -1 -1 -2 2010.50 65.89 -1 -1 -2 2116.19 67.09 -1 -1 -2 1939.51 66.99 -1 -1 -2 2004.20 65.99 1 -1 2 1943.71 67.49 1 -1 2 2091.79 64.39 1 -1 2 2059.79 66.09 -1 1 -2 2046.50 66.19 1 1 2 2041.60 66.09 1 1 2 2128.69 62.79 -1 1 -2 2070.39 67.79 -1 1 -2 2055.49 64.39 -1 1 -2 2079.89 66.19 1 1 2 2031.10 65.69 1 1 2 2097.09 67.29 -1 1 -2 2081.69 64.49 1 1 2 2071.89 62.89 1 1 2 2089.89 66.29 1 1 2 2013.00 67.39 -2 -1 -2 986.60 39.90 -2 -1 -2 982.10 36.40 -2 -1 -2 1025.60 39.80 2 -1 2 1029.90 34.40 -2 -1 -2 1013.30 36.70 2 -1 2 1000.70 37.50 2 -1 2 1030.20 39.00 -2 -1 -2 983.20 36.30 2 -1 2 991.30 33.80 2 -1 2 984.60 40.00 -2 1 -2 974.20 39.40 2 1 2 998.10 36.60 2 1 2 1004.60 39.80 -2 1 -2 1006.70 37.40 2 1 2 1014.60 37.00 -2 1 -2 1010.20 34.20 2 1 2 983.10 36.80 -2 1 -2 982.10 33.50 2 1 2 981.30 39.50 -2 1 -2 1031.60 38.40 -3 -1 -2 8.90 11.10 -3 -1 -2 5.50 8.10 3 -1 2 23.50 13.10 3 -1 2 0.10 11.90 -3 -1 -2 20.10 8.20 -3 -1 -2 16.10 3.10 3 -1 2 23.50 6.40 -3 -1 -2 16.10 10.90 3 -1 2 23.40 8.70 3 1 2 10.80 12.70 -3 1 -2 10.10 12.40 -3 1 -2 20.40 6.40 -3 1 -2 14.10 8.00 3 1 2 15.70 11.50 3 1 2 17.90 10.20 -3 1 -2 14.10 6.50 3 1 2 -2.00 8.70 -3 1 -2 29.40 12.50 3 1 2 26.10 8.40 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-1.80 16.60 -8 -2 2 19.80 20.50 -8 2 2 17.20 12.90 -8 2 2 -11.90 20.60 -8 2 2 7.50 13.80 8 2 -2 12.00 17.30 8 2 -2 29.60 13.80 -8 2 2 0.50 10.60 -8 2 2 19.90 14.20 -8 2 2 16.10 12.10 -8 2 2 -1.50 16.10 -8 2 2 4.20 10.30 7 -2 -2 237.28 30.30 -7 -2 2 205.98 16.70 -7 -2 2 219.78 22.80 -7 -2 2 260.87 30.80 -7 -2 2 236.68 18.10 -7 -2 2 202.68 19.60 7 -2 -2 185.78 24.70 -7 -2 2 236.58 30.60 -7 -2 2 202.08 19.30 -7 -2 2 235.58 29.50 -7 2 2 220.58 21.50 -7 2 2 215.88 22.50 -7 2 2 205.38 18.80 -7 2 2 229.78 18.80 -7 2 2 255.87 26.60 7 2 -2 236.78 28.30 7 2 -2 182.18 20.40 -7 2 2 228.18 20.30 -7 2 2 236.68 19.00 -7 2 2 214.98 25.80 -6 -2 2 97.49 14.40 -6 -2 2 92.09 19.80 -6 -2 2 134.19 22.70 6 -2 -2 110.39 19.00 -6 -2 2 115.09 16.90 -6 -2 2 96.49 20.80 -6 -2 2 113.29 14.00 -6 -2 2 135.79 15.30 -6 -2 2 105.29 13.20 6 -2 -2 81.69 20.10 -6 2 2 114.49 14.00 -6 2 2 104.49 13.70 -6 2 2 86.69 21.30 -6 2 2 106.39 16.40 6 2 -2 97.79 19.50 6 2 -2 100.09 15.50 -6 2 2 101.39 19.40 -6 2 2 98.49 16.00 -5 -2 2 871.91 36.20 -5 -2 2 838.52 44.10 -5 -2 2 860.31 38.30 -5 -2 2 871.71 42.80 -5 -2 2 869.91 33.30 5 -2 -2 841.22 35.80 -5 -2 2 712.53 50.69 -5 -2 2 825.92 35.10 5 -2 -2 767.82 38.60 -5 2 2 896.91 40.60 -5 2 2 899.61 36.70 -5 2 2 865.01 38.10 -5 2 2 814.52 33.60 -5 2 2 816.92 34.40 -5 2 2 934.91 48.80 5 2 -2 854.21 33.20 -5 2 2 842.62 39.80 5 2 -2 863.01 37.60 -4 -2 2 1907.91 69.09 -4 -2 2 1892.91 72.79 -4 -2 2 1949.70 72.29 -4 -2 2 1903.81 70.39 4 -2 -2 1981.60 69.49 4 -2 -2 1978.50 67.99 -4 -2 2 1951.00 73.79 4 -2 -2 2014.40 72.39 -4 -2 2 2052.59 67.49 -4 -2 2 2024.00 66.49 -4 -2 2 2013.10 65.69 -4 2 2 2029.30 71.39 -4 2 2 1996.30 66.59 -4 2 2 1962.50 71.29 -4 2 2 1834.82 68.39 -4 2 2 1993.90 68.29 4 2 -2 1991.90 72.39 -4 2 2 1993.00 65.79 4 2 -2 2018.00 65.59 -4 2 2 1999.90 69.49 4 2 -2 1976.50 69.29 -3 -2 2 1065.49 41.40 -3 -2 2 1036.10 43.50 3 -2 -2 1046.80 40.10 3 -2 -2 1090.09 39.00 3 -2 -2 1078.69 40.20 -3 -2 2 1121.99 38.60 -3 -2 2 1113.39 43.40 3 -2 -2 1062.19 40.90 -3 -2 2 1092.59 44.70 3 -2 -2 1074.29 36.80 -3 -2 2 1100.19 37.70 3 -2 -2 1079.69 42.80 -3 -2 2 1152.88 38.70 -3 2 2 1140.69 41.10 3 2 -2 1103.09 43.10 3 2 -2 1049.79 40.90 -3 2 2 1086.39 40.20 3 2 -2 1134.99 38.60 -3 2 2 1110.19 43.00 -3 2 2 1034.90 39.90 -3 2 2 1124.39 39.10 -2 -2 2 2325.17 78.89 -2 -2 2 2306.77 75.79 2 -2 -2 2184.98 72.59 -2 -2 2 2273.87 75.59 -2 -2 2 2219.38 71.49 2 -2 -2 2375.76 72.79 2 -2 -2 2296.67 73.99 2 -2 -2 2160.38 75.79 2 -2 -2 2108.59 74.59 2 -2 -2 2242.48 74.69 -2 -2 2 2339.97 73.49 -2 2 2 2265.87 72.69 2 2 -2 2376.96 73.69 2 2 -2 2327.37 71.79 -2 2 2 2327.17 75.09 2 2 -2 2352.86 78.99 -2 2 2 2018.80 75.09 2 2 -2 2398.96 75.79 2 2 -2 2363.06 76.19 -2 2 2 2334.87 74.19 2 2 -2 2343.97 71.99 -2 2 2 2167.68 74.69 -2 2 2 2285.77 72.19 1 -2 -2 473.55 19.20 -1 -2 2 437.46 18.80 -1 -2 2 483.45 18.40 -1 -2 2 464.25 18.10 1 -2 -2 428.56 19.60 1 -2 -2 479.75 20.00 -1 -2 2 459.25 16.40 1 -2 -2 471.65 19.00 -1 -2 2 496.45 23.00 -1 -2 2 505.75 20.00 1 2 -2 478.55 18.10 -1 2 2 438.36 20.10 -1 2 2 477.15 20.10 1 2 -2 479.15 19.80 1 2 -2 471.35 19.00 1 2 -2 444.96 21.90 1 2 -2 456.45 16.10 -1 2 2 472.85 19.20 -1 2 2 470.15 19.50 1 2 -2 438.16 19.20 -1 2 2 447.76 18.80 0 -2 2 186.78 10.70 0 -2 -2 193.08 10.10 0 -2 -2 198.48 12.90 0 -2 2 204.58 9.70 0 -2 -2 206.68 9.90 0 -2 -2 208.68 12.10 0 -2 -2 192.68 12.50 0 -2 2 183.98 10.70 0 -2 2 197.08 10.20 0 -2 2 211.28 10.40 0 -2 -2 199.18 10.00 0 -2 2 197.28 13.20 0 2 -2 201.48 10.40 0 2 -2 198.98 13.00 0 2 2 187.68 9.80 0 2 2 188.88 9.90 0 2 2 188.48 12.60 0 2 -2 198.58 9.50 0 2 2 199.58 10.00 0 2 2 196.78 12.10 0 2 2 199.48 12.70 0 2 -2 175.68 10.20 0 2 -2 199.88 10.80 0 2 -2 199.78 11.10 1 -2 2 346.27 16.60 1 -2 2 359.86 15.60 1 -2 2 348.47 17.80 -1 -2 -2 356.16 17.30 -1 -2 -2 372.36 18.30 1 -2 2 346.17 21.20 -1 -2 -2 355.16 16.30 1 -2 2 367.96 14.10 -1 -2 -2 340.07 18.60 -1 -2 -2 374.36 19.30 -1 -2 -2 376.96 13.70 -1 2 -2 364.26 17.50 1 2 2 361.96 18.50 -1 2 -2 365.66 14.00 1 2 2 358.56 16.40 1 2 2 347.57 18.90 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86.59 -4 -2 -2 2415.86 88.19 -4 -2 -2 2433.06 81.29 4 -2 2 2359.56 84.09 4 -2 2 2318.57 75.79 -4 -2 -2 2387.36 79.29 4 -2 2 2428.46 78.89 4 2 2 2334.77 87.29 -4 2 -2 2409.06 85.89 -4 2 -2 2462.65 86.09 -4 2 -2 2325.17 75.89 -4 2 -2 2392.16 83.99 4 2 2 2431.16 81.89 4 2 2 2405.16 80.29 -4 2 -2 2499.75 79.09 4 2 2 2268.17 86.29 4 2 2 2381.66 82.29 -5 -2 -2 228.78 27.80 5 -2 2 200.18 25.30 -5 -2 -2 222.38 27.40 5 -2 2 209.48 28.30 5 -2 2 162.38 12.40 -5 -2 -2 194.88 10.70 5 -2 2 195.78 19.60 -5 -2 -2 189.08 10.20 5 -2 2 176.68 14.30 -5 -2 -2 183.98 19.00 -5 -2 -2 199.88 24.70 -5 -2 -2 185.58 18.50 -5 2 -2 185.98 24.40 5 2 2 231.58 27.00 5 2 2 186.18 18.60 5 2 2 223.48 24.90 5 2 2 254.67 22.30 5 2 2 182.88 17.70 -5 2 -2 206.58 15.80 -5 2 -2 225.28 27.70 -5 2 -2 180.08 19.90 -5 2 -2 168.88 12.80 6 -2 2 3901.31 128.39 -6 -2 -2 4011.30 133.49 -6 -2 -2 4097.89 143.49 6 -2 2 3950.20 126.39 6 -2 2 3682.73 138.09 6 -2 2 4039.10 139.79 -6 -2 -2 3969.60 123.99 6 -2 2 4107.89 137.59 -6 -2 -2 3884.11 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3 372.66 28.30 -9 -3 3 347.17 30.10 -9 -3 3 359.46 44.10 -9 -3 3 375.06 34.50 9 -3 -3 361.46 40.60 -9 3 3 337.47 28.20 -9 3 3 373.26 44.80 -9 3 3 379.96 33.90 -9 3 3 347.47 27.50 -9 3 3 378.86 35.30 9 3 -3 347.27 31.00 -9 3 3 386.06 31.20 -9 3 3 391.56 38.90 -9 3 3 407.46 31.20 8 -3 -3 126.29 29.50 -8 -3 3 138.29 22.80 -8 -3 3 105.09 24.10 8 -3 -3 95.89 22.20 -8 -3 3 104.79 26.10 -8 -3 3 129.89 18.20 -8 -3 3 118.09 17.30 -8 -3 3 137.99 17.10 -8 -3 3 117.19 27.90 -8 -3 3 175.38 30.60 -8 -3 3 109.39 17.80 -8 3 3 127.99 19.90 -8 3 3 115.29 26.30 -8 3 3 132.59 19.40 -8 3 3 136.29 18.80 -8 3 3 135.49 21.00 8 3 -3 123.69 20.40 -8 3 3 166.48 26.20 -8 3 3 103.59 21.00 -8 3 3 118.89 17.40 7 -3 -3 24.90 15.10 -7 -3 3 32.70 11.70 7 -3 -3 35.80 12.40 -7 -3 3 28.30 10.40 -7 -3 3 18.00 15.30 7 -3 -3 -5.70 18.50 -7 -3 3 45.20 14.90 -7 -3 3 16.80 18.10 -7 -3 3 10.30 10.20 -7 -3 3 37.10 19.00 -7 -3 3 39.20 20.30 -7 -3 3 17.10 10.90 -7 3 3 37.70 12.40 -7 3 3 -5.10 17.50 7 3 -3 17.00 12.10 -7 3 3 30.00 15.70 -7 3 3 30.10 12.70 -7 3 3 27.60 11.20 7 3 -3 34.70 12.30 -7 3 3 29.30 11.40 -7 3 3 26.30 13.00 -7 3 3 12.50 12.50 -6 -3 3 163.28 23.80 6 -3 -3 150.68 23.50 -6 -3 3 110.59 14.10 -6 -3 3 161.28 24.60 -6 -3 3 129.99 22.30 -6 -3 3 182.58 20.50 -6 -3 3 121.89 15.40 6 -3 -3 168.78 20.60 -6 -3 3 128.39 21.80 6 -3 -3 146.59 16.80 -6 -3 3 118.09 15.40 -6 3 3 129.09 17.70 -6 3 3 153.08 18.10 -6 3 3 146.19 22.50 6 3 -3 145.49 18.10 -6 3 3 139.39 14.90 6 3 -3 130.59 15.00 -6 3 3 148.19 20.40 -6 3 3 170.78 20.60 -6 3 3 137.29 15.80 -5 -3 3 116.49 20.00 5 -3 -3 138.89 16.90 -5 -3 3 123.19 13.60 -5 -3 3 112.39 20.00 -5 -3 3 146.29 14.90 -5 -3 3 124.49 20.60 -5 -3 3 95.69 12.90 5 -3 -3 117.39 22.10 5 -3 -3 116.39 13.50 -5 -3 3 119.89 17.10 -5 -3 3 201.58 24.70 5 -3 -3 114.69 16.60 -5 3 3 162.88 20.50 -5 3 3 123.99 17.50 -5 3 3 167.58 23.10 -5 3 3 114.79 14.00 -5 3 3 123.09 16.30 -5 3 3 109.69 16.90 -5 3 3 137.99 15.10 5 3 -3 164.18 22.00 5 3 -3 128.09 15.20 5 3 -3 138.59 17.40 4 -3 -3 1016.20 42.30 -4 -3 3 1070.99 45.10 4 -3 -3 1050.99 37.70 4 -3 -3 970.90 43.90 4 -3 -3 1009.90 40.10 -4 -3 3 1100.39 39.20 -4 -3 3 1019.50 46.20 -4 -3 3 1076.79 38.90 4 -3 -3 1030.90 39.50 4 -3 -3 1031.80 41.20 -4 -3 3 1017.70 42.90 -4 -3 3 1035.20 47.70 -4 -3 3 1017.70 37.30 -4 3 3 1094.79 42.60 -4 3 3 1065.39 42.40 -4 3 3 1043.70 40.00 4 3 -3 1063.59 39.10 -4 3 3 1027.30 40.40 -4 3 3 996.50 43.00 4 3 -3 1117.29 43.50 4 3 -3 1092.89 45.40 3 -3 -3 116.69 11.50 3 -3 -3 100.59 10.60 -3 -3 3 102.59 11.00 -3 -3 3 117.89 15.00 -3 -3 3 127.39 17.50 3 -3 -3 112.69 13.40 3 -3 -3 114.89 14.80 3 -3 -3 113.69 12.30 -3 -3 3 100.19 8.30 -3 -3 3 103.39 13.00 3 -3 -3 101.79 11.70 -3 3 3 108.29 12.00 -3 3 3 84.59 11.40 3 3 -3 114.89 9.90 -3 3 3 118.29 15.10 -3 3 3 108.39 9.60 3 3 -3 128.49 15.90 -3 3 3 122.89 13.70 -3 3 3 114.29 13.20 3 3 -3 100.19 11.50 3 3 -3 111.69 8.20 3 3 -3 124.49 16.10 3 3 -3 113.29 13.10 -2 -3 3 238.68 16.90 -2 -3 3 198.38 11.00 -2 -3 3 253.77 13.70 2 -3 -3 272.17 15.60 2 -3 -3 246.48 15.10 -2 -3 3 256.07 16.50 2 -3 -3 278.47 17.30 -2 -3 3 238.88 20.30 2 -3 -3 228.58 15.30 -2 -3 3 273.07 15.30 2 -3 -3 202.28 18.80 -2 3 3 241.78 18.10 2 3 -3 250.17 15.90 2 3 -3 275.87 17.80 -2 3 3 225.78 14.90 -2 3 3 252.37 14.50 2 3 -3 251.67 20.30 2 3 -3 243.58 16.20 2 3 -3 246.68 13.40 -2 3 3 255.77 16.60 -2 3 3 282.07 17.80 2 3 -3 212.98 10.80 1 -3 -3 543.75 23.20 -1 -3 3 613.74 20.00 -1 -3 3 460.65 22.30 -1 -3 3 547.85 22.80 -1 -3 3 478.65 26.50 -1 -3 3 510.45 21.80 -1 -3 3 517.85 23.20 1 -3 -3 489.45 22.30 1 -3 -3 622.64 26.40 1 -3 -3 498.65 25.40 -1 3 3 539.05 23.60 -1 3 3 511.35 25.00 1 3 -3 493.35 26.90 1 3 -3 547.15 23.30 -1 3 3 493.35 22.00 -1 3 3 505.55 23.20 1 3 -3 567.54 23.40 1 3 -3 545.85 24.40 1 3 -3 472.75 20.00 1 3 -3 558.84 22.10 -1 3 3 519.85 24.70 0 -3 3 1795.42 64.09 0 -3 -3 1760.22 58.49 0 -3 -3 1724.13 61.89 0 -3 3 1833.02 59.59 0 -3 3 1780.12 58.69 0 -3 3 1673.23 59.39 0 -3 3 1884.31 59.39 0 -3 -3 1839.22 59.29 0 -3 3 1832.92 59.89 0 -3 -3 1918.51 61.69 0 -3 -3 1616.64 58.79 0 -3 -3 1728.73 61.59 0 3 3 1871.71 61.49 0 3 3 1789.52 61.49 0 3 -3 1817.32 59.89 0 3 -3 1742.03 58.39 0 3 3 1774.12 58.39 0 3 3 1768.12 62.39 0 3 -3 1842.42 59.59 0 3 -3 1775.92 63.89 0 3 3 1857.51 59.49 0 3 3 1802.32 59.39 0 3 -3 1814.32 59.99 0 3 -3 1721.93 59.29 -1 -3 -3 3251.47 111.49 1 -3 3 3393.46 108.59 1 -3 3 3359.46 108.59 1 -3 3 3337.37 109.09 1 -3 3 3627.34 113.99 -1 -3 -3 3473.55 109.99 -1 -3 -3 3437.36 109.89 -1 -3 -3 3437.06 106.39 1 -3 3 3423.56 106.49 1 -3 3 3328.47 106.99 -1 -3 -3 3336.77 110.49 -1 -3 -3 3536.55 108.29 1 -3 3 3439.66 109.29 1 3 3 3489.35 110.09 1 3 3 3242.48 108.39 1 3 3 3363.66 110.09 -1 3 -3 3286.47 108.89 -1 3 -3 3551.44 109.39 1 3 3 3433.06 106.49 1 3 3 3184.58 111.59 -1 3 -3 3400.06 112.89 1 3 3 3307.77 110.39 -1 3 -3 3447.26 108.59 2 -3 3 2015.20 71.29 -2 -3 -3 1896.81 67.79 -2 -3 -3 1968.20 67.29 -2 -3 -3 1969.30 61.49 -2 -3 -3 1816.12 69.79 -2 -3 -3 1957.20 69.39 2 -3 3 1907.41 67.59 2 -3 3 1968.40 68.39 2 -3 3 1937.41 62.29 2 -3 3 1978.50 65.69 -2 -3 -3 2016.00 65.79 -2 3 -3 1909.41 65.19 -2 3 -3 1918.11 70.29 -2 3 -3 1944.81 67.59 2 3 3 2002.50 69.69 -2 3 -3 1931.81 62.09 2 3 3 1981.10 68.49 -2 3 -3 1949.30 67.79 2 3 3 1900.41 67.19 2 3 3 1987.60 61.49 2 3 3 1960.30 70.69 2 3 3 2022.60 66.19 -3 -3 -3 2051.49 67.99 3 -3 3 1998.30 71.09 -3 -3 -3 2008.60 72.79 3 -3 3 2030.60 73.49 -3 -3 -3 1910.51 70.09 3 -3 3 2082.49 67.89 -3 -3 -3 1981.10 68.69 3 -3 3 1971.20 72.09 -3 -3 -3 2085.39 74.39 3 3 3 1908.41 67.89 -3 3 -3 2042.30 67.39 -3 3 -3 1927.91 62.39 -3 3 -3 2015.00 71.69 3 3 3 2002.10 70.69 3 3 3 1964.40 73.19 3 3 3 1956.50 68.99 3 3 3 1931.11 74.09 -3 3 -3 2013.10 73.09 -3 3 -3 2010.80 70.99 -4 -3 -3 47.30 12.80 -4 -3 -3 71.79 12.30 4 -3 3 26.90 16.80 4 -3 3 49.70 17.20 4 -3 3 47.10 12.20 -4 -3 -3 67.79 28.10 4 -3 3 54.29 10.50 4 3 3 88.59 23.00 -4 3 -3 56.09 17.90 4 3 3 58.09 11.30 4 3 3 66.99 16.60 -4 3 -3 28.60 16.50 -4 3 -3 56.79 10.80 4 3 3 38.40 12.40 4 3 3 81.99 33.70 5 -3 3 2509.75 81.79 -5 -3 -3 2882.41 98.79 5 -3 3 2602.54 87.29 5 -3 3 2689.63 94.69 -5 -3 -3 2572.84 97.19 -5 -3 -3 2613.64 98.69 -5 -3 -3 2458.45 88.09 -5 -3 -3 2644.04 89.99 5 -3 3 2447.35 95.69 5 -3 3 2676.73 96.29 -5 3 -3 2574.54 95.89 -5 3 -3 2603.44 96.79 5 3 3 2508.15 97.39 -5 3 -3 2650.53 94.09 5 3 3 2531.75 89.59 -5 3 -3 2509.55 81.89 5 3 3 2637.44 90.79 5 3 3 2519.55 98.99 -5 3 -3 2666.13 87.49 6 -3 3 5.40 5.60 -6 -3 -3 9.90 11.60 -6 -3 -3 1.80 10.40 6 -3 3 1.00 15.30 6 -3 3 10.50 10.60 -6 -3 -3 -3.90 17.90 6 -3 3 -3.60 8.20 -6 -3 -3 -13.50 14.70 6 -3 3 5.60 19.30 -6 3 -3 6.30 11.20 -6 3 -3 3.10 15.10 6 3 3 14.00 17.10 6 3 3 21.30 16.90 6 3 3 13.80 11.90 -6 3 -3 4.10 6.80 -6 3 -3 8.40 16.60 6 3 3 7.00 14.30 6 3 3 6.40 10.00 -6 3 -3 8.00 9.60 -7 -3 -3 1190.98 59.39 7 -3 3 1194.58 48.00 -7 -3 -3 1145.39 61.69 -7 -3 -3 1109.69 50.09 -7 -3 -3 1098.59 57.39 7 -3 3 1130.19 53.99 7 -3 3 1135.99 59.59 7 -3 3 1106.59 40.60 -7 -3 -3 1182.28 50.49 7 -3 3 1116.59 56.89 7 3 3 1177.78 49.90 7 3 3 1183.98 51.39 -7 3 -3 1108.79 41.10 -7 3 -3 1163.68 54.09 -7 3 -3 1179.68 45.90 -7 3 -3 1103.89 55.99 7 3 3 1149.78 51.09 -7 3 -3 1069.09 57.39 -8 -3 -3 10.00 19.80 -8 -3 -3 17.30 15.10 8 -3 3 -1.30 22.20 -8 -3 -3 -4.00 13.10 8 -3 3 -3.20 18.00 8 -3 3 -0.10 13.90 8 -3 3 2.00 7.70 -8 -3 -3 -1.10 23.30 8 -3 3 2.30 10.10 -8 -3 -3 -26.70 23.50 -8 3 -3 18.50 20.20 8 3 3 3.40 12.40 -8 3 -3 -15.60 13.10 -8 3 -3 8.40 11.30 8 3 3 -11.40 17.50 8 3 3 0.40 20.90 -8 3 -3 -1.70 8.90 -8 3 -3 22.30 25.00 -8 3 -3 0.10 23.30 8 3 3 18.90 13.20 9 -3 3 239.58 37.70 -9 -3 -3 190.68 42.90 9 -3 3 171.48 20.90 -9 -3 -3 220.48 27.80 -9 -3 -3 222.18 28.50 9 -3 3 244.38 29.90 9 3 3 212.38 31.20 9 3 3 218.18 27.50 -9 3 -3 222.78 21.50 9 3 3 224.58 27.60 -9 3 -3 171.48 18.50 -9 3 -3 210.38 38.30 -9 3 -3 224.38 35.90 9 3 3 183.58 41.20 -9 3 -3 218.58 18.00 -9 3 -3 255.37 47.10 -10 -3 -3 4.80 30.80 -10 -3 -3 20.70 17.90 10 -3 3 29.30 12.80 -10 -3 -3 46.00 19.90 10 -3 3 19.50 23.50 10 -3 3 6.70 18.20 -10 3 -3 14.00 27.50 10 3 3 18.40 16.10 10 3 3 40.00 17.70 10 3 3 43.60 27.20 -10 3 -3 23.70 13.70 -10 3 -3 29.10 11.20 -10 3 -3 34.50 20.20 10 3 3 10.60 20.40 -10 3 -3 19.30 11.30 -11 -3 -3 137.29 26.00 11 -3 3 192.58 36.60 11 -3 3 94.39 24.80 -11 -3 -3 136.39 38.20 -11 3 -3 103.09 15.80 -11 3 -3 165.48 40.70 -11 3 -3 131.99 19.30 -11 3 -3 170.38 19.30 11 3 3 133.09 24.60 11 3 3 115.19 33.00 11 3 3 137.69 26.30 -11 3 -3 151.38 29.40 -11 3 -3 145.39 17.40 -12 -3 -3 17.10 20.40 -12 -3 -3 -6.60 35.60 12 -3 3 12.30 24.80 12 -3 3 -14.40 20.60 12 -3 3 -8.30 15.70 -12 3 -3 -25.70 12.60 12 3 3 10.80 20.90 12 3 3 -10.70 18.00 -12 3 -3 46.30 13.90 -12 3 -3 -13.80 20.60 -12 3 -3 -7.90 9.90 12 3 3 12.40 25.60 -12 3 -3 -13.50 31.00 -12 -4 3 12.80 15.50 12 -4 -3 -9.20 19.00 -12 -4 3 -9.30 13.90 -12 -4 3 23.30 24.10 -12 -4 3 -4.20 34.50 -12 -4 3 52.29 15.70 -12 -4 3 10.20 18.00 -12 4 3 -20.70 13.40 -12 4 3 -1.70 25.90 12 4 -3 23.00 19.10 -12 4 3 -9.40 17.00 -12 4 3 9.50 20.30 -11 -4 3 45.30 16.60 -11 -4 3 54.99 27.10 -11 -4 3 55.19 32.30 -11 -4 3 62.89 16.80 11 -4 -3 21.30 33.10 11 -4 -3 53.89 23.70 -11 -4 3 40.70 19.10 -11 4 3 37.70 16.10 -11 4 3 92.09 17.40 -11 4 3 38.30 26.90 -11 4 3 16.80 20.10 -11 4 3 39.80 19.40 -11 4 3 28.70 16.00 11 4 -3 42.90 20.30 -11 4 3 84.99 25.80 10 -4 -3 34.80 30.50 -10 -4 3 75.69 31.90 -10 -4 3 79.19 22.70 -10 -4 3 97.79 19.20 -10 -4 3 80.79 27.10 -10 -4 3 45.20 15.80 10 -4 -3 48.70 22.80 -10 -4 3 54.69 16.70 -10 -4 3 47.20 18.20 -10 4 3 20.60 15.50 -10 4 3 58.49 20.40 -10 4 3 42.60 16.20 -10 4 3 91.29 26.90 -10 4 3 65.49 18.10 10 4 -3 68.89 21.80 -10 4 3 72.29 20.50 9 -4 -3 366.16 36.10 -9 -4 3 385.26 44.90 -9 -4 3 396.86 30.00 9 -4 -3 429.86 45.60 -9 -4 3 446.06 44.10 -9 -4 3 432.96 50.89 -9 -4 3 365.76 45.20 -9 -4 3 379.66 27.10 -9 -4 3 381.66 30.90 -9 -4 3 360.16 28.00 -9 4 3 429.26 35.50 9 4 -3 353.46 33.10 -9 4 3 346.47 27.20 -9 4 3 356.46 44.70 -9 4 3 350.56 37.20 -9 4 3 305.37 27.60 -9 4 3 344.27 31.90 -9 4 3 318.67 34.00 -9 4 3 438.86 32.70 -8 -4 3 90.59 15.40 -8 -4 3 91.69 27.50 8 -4 -3 99.29 18.10 -8 -4 3 110.59 29.40 -8 -4 3 105.99 21.60 8 -4 -3 86.49 27.60 -8 -4 3 92.29 27.00 -8 -4 3 113.79 17.00 -8 -4 3 67.69 21.70 8 -4 -3 70.39 20.70 -8 -4 3 114.69 17.40 -8 -4 3 97.69 16.40 -8 4 3 107.89 16.50 -8 4 3 103.09 16.00 -8 4 3 88.09 17.50 8 4 -3 83.89 18.80 -8 4 3 100.39 22.70 -8 4 3 109.19 28.40 -8 4 3 116.89 20.40 -8 4 3 80.99 19.80 -8 4 3 81.59 30.60 7 -4 -3 782.02 38.50 -7 -4 3 747.73 38.50 -7 -4 3 843.52 49.99 -7 -4 3 823.32 35.10 7 -4 -3 776.72 47.60 -7 -4 3 830.92 46.50 7 -4 -3 790.92 41.60 -7 -4 3 800.62 47.50 -7 -4 3 792.52 47.90 7 -4 -3 886.61 34.10 -7 -4 3 806.52 36.80 -7 -4 3 780.02 42.00 -7 4 3 850.61 44.20 -7 4 3 797.92 34.50 -7 4 3 788.32 35.60 -7 4 3 809.62 40.00 -7 4 3 734.63 40.20 7 4 -3 794.72 41.00 -7 4 3 772.12 43.80 7 4 -3 739.43 34.80 -7 4 3 789.22 41.70 6 -4 -3 118.79 16.80 -6 -4 3 71.39 15.80 6 -4 -3 97.79 13.00 -6 -4 3 73.79 18.60 -6 -4 3 89.59 12.70 -6 -4 3 97.49 12.30 6 -4 -3 67.89 16.20 -6 -4 3 98.09 20.50 -6 -4 3 111.49 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289.97 37.10 9 11 -4 251.77 27.40 -9 11 4 295.87 17.40 9 11 -4 271.57 28.10 8 -11 -4 23.60 20.80 8 -11 -4 33.60 29.80 -8 -11 4 -1.60 25.90 8 -11 -4 7.20 16.70 -8 -11 4 33.80 18.20 -8 -11 4 29.30 24.50 -8 11 4 54.89 12.30 8 11 -4 27.40 20.50 8 11 -4 28.40 16.30 -8 11 4 14.70 19.20 -8 11 4 -3.80 15.00 -8 11 4 39.30 11.30 8 11 -4 20.30 17.20 -8 11 4 26.80 20.60 -7 -11 4 368.26 43.30 7 -11 -4 402.36 36.90 -7 -11 4 367.26 40.90 7 -11 -4 311.07 42.60 -7 -11 4 390.26 29.40 7 -11 -4 336.67 24.30 7 -11 -4 418.86 31.00 -7 11 4 344.07 32.10 -7 11 4 317.77 34.90 7 11 -4 390.56 30.80 7 11 -4 354.66 29.80 -7 11 4 354.66 24.90 -7 11 4 338.07 27.50 -7 11 4 411.56 36.40 7 11 -4 375.26 47.70 7 11 -4 384.56 36.80 -6 -11 4 64.69 20.10 6 -11 -4 84.99 17.00 6 -11 -4 103.79 31.60 -6 -11 4 75.89 26.30 6 -11 -4 82.89 17.40 -6 -11 4 65.79 26.60 6 11 -4 76.29 18.80 -6 11 4 66.29 23.40 6 11 -4 64.19 22.80 -6 11 4 73.69 21.10 6 11 -4 59.69 19.20 -6 11 4 67.89 16.20 6 11 -4 61.09 31.60 -6 11 4 99.69 21.90 -6 11 4 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-2.90 18.00 0 5 20 10.80 18.90 0 5 20 -5.80 18.80 0 5 20 67.19 34.70 0 5 20 57.29 22.90 0 5 -20 -1.30 19.10 1 -5 20 207.98 43.20 1 -5 20 124.99 32.30 -1 -5 -20 206.78 27.80 -1 -5 -20 162.88 33.40 -1 -5 -20 196.08 29.80 1 5 20 212.98 31.50 -1 5 -20 170.18 27.00 1 5 20 188.18 38.60 1 5 20 260.87 56.59 1 5 20 309.87 38.90 -1 5 -20 203.98 30.80 1 5 20 173.88 27.00 2 -5 20 26.10 32.30 -2 -5 -20 11.40 20.10 2 -5 20 3.00 24.70 -2 -5 -20 -3.90 20.60 2 -5 20 4.50 29.90 -2 5 -20 -9.50 15.50 2 5 20 -12.80 30.10 2 5 20 41.40 24.50 2 5 20 -5.60 42.40 2 5 20 -34.00 15.70 2 5 20 30.10 17.60 2 5 20 -5.10 29.80 -2 5 -20 53.09 24.50 3 -5 20 112.59 37.60 -3 -5 -20 98.79 26.70 3 -5 20 127.09 38.20 -3 -5 -20 90.89 27.10 3 -5 20 69.09 30.30 3 5 20 194.28 32.40 3 5 20 132.49 33.00 3 5 20 123.89 41.00 3 5 20 114.29 21.20 -3 5 -20 141.09 31.10 -3 5 -20 114.49 21.70 3 5 20 174.98 30.60 3 5 20 95.29 32.70 -4 -6 20 36.30 29.20 -4 -6 20 -12.60 32.70 4 -6 -20 60.69 31.00 -4 -6 20 20.90 26.80 4 -6 -20 91.39 20.00 4 -6 -20 55.19 34.90 4 6 -20 81.99 22.00 -4 6 20 38.00 21.40 -4 6 20 34.60 25.10 -4 6 20 62.89 26.70 3 -6 -20 24.90 28.10 3 -6 -20 71.69 25.30 3 -6 -20 75.49 19.00 -3 -6 20 25.30 28.10 -3 -6 20 25.80 32.80 -3 -6 20 36.80 29.10 -3 6 20 52.49 29.30 -3 6 20 130.99 25.90 3 6 -20 47.30 23.70 -3 6 20 58.09 20.90 -3 6 20 23.10 30.80 -3 6 20 35.40 23.80 3 6 -20 72.49 21.30 -2 -6 20 15.10 29.30 2 -6 -20 95.29 24.50 2 -6 -20 91.89 19.80 -2 -6 20 57.79 35.10 2 -6 -20 23.50 19.40 2 -6 -20 122.49 33.80 -2 -6 20 70.79 33.90 -2 6 20 38.20 20.30 2 6 -20 56.49 20.40 -2 6 20 66.59 30.20 -2 6 20 126.99 28.30 2 6 -20 29.70 22.70 -2 6 20 93.49 22.10 -2 6 20 30.60 28.90 -1 -6 20 -20.40 26.30 1 -6 -20 7.00 17.50 -1 -6 20 -6.50 31.10 1 -6 -20 5.80 41.90 1 -6 -20 -27.80 18.80 -1 -6 20 -15.40 27.70 1 -6 -20 34.30 21.60 -1 6 20 21.30 28.90 -1 6 20 13.30 21.90 -1 6 20 22.20 20.50 1 6 -20 7.10 19.40 -1 6 20 1.50 27.90 1 6 -20 37.20 19.20 0 -6 -20 -3.90 23.80 0 -6 -20 -26.00 26.70 0 -6 -20 24.00 19.10 0 -6 20 8.10 30.80 0 -6 20 -1.60 25.70 0 -6 -20 20.80 18.50 0 -6 20 10.00 30.50 0 6 20 13.80 30.60 0 6 -20 18.20 19.60 0 6 20 36.40 21.70 0 6 -20 35.30 20.90 0 6 20 23.00 23.90 0 6 20 33.50 19.10 0 6 20 65.09 31.00 1 -6 20 3.20 29.80 -1 -6 -20 -34.30 25.30 -1 -6 -20 9.40 20.40 -1 -6 -20 16.90 21.10 1 -6 20 4.80 25.70 1 -6 20 47.30 36.40 -1 -6 -20 34.50 31.80 -1 6 -20 48.90 21.70 1 6 20 12.80 29.20 -1 6 -20 -2.80 17.50 1 6 20 -1.20 17.70 1 6 20 78.39 32.00 1 6 20 60.19 38.70 1 6 20 23.00 20.80 -2 -6 -20 20.20 21.90 2 -6 20 -6.60 24.90 2 -6 20 -22.70 35.00 2 -6 20 25.20 32.90 -2 6 -20 42.00 24.20 2 6 20 40.10 36.80 2 6 20 64.69 19.50 2 6 20 1.80 23.10 2 6 20 17.20 17.90 2 6 20 51.09 33.30 2 6 20 15.30 24.40 -2 6 -20 0.30 19.70 3 -7 -20 106.19 21.20 3 -7 -20 49.40 32.80 -3 -7 20 7.90 34.20 -3 -7 20 36.90 28.60 -3 -7 20 106.29 31.60 3 -7 -20 43.10 23.60 -3 7 20 43.90 26.90 -3 7 20 17.60 23.60 3 7 -20 79.89 21.00 -3 7 20 84.69 52.39 -3 7 20 60.39 26.80 -2 -7 20 -20.40 33.30 -2 -7 20 -48.60 30.20 -2 -7 20 -20.00 24.70 2 -7 -20 4.30 30.80 2 -7 -20 5.90 17.40 -2 7 20 -9.70 22.20 2 7 -20 17.60 17.10 -2 7 20 20.70 24.80 -2 7 20 -17.80 18.90 2 7 -20 1.30 19.70 1 -7 -20 43.70 21.40 1 -7 -20 130.79 41.60 1 -7 -20 164.58 38.80 1 -7 -20 95.89 23.20 -1 -7 20 61.49 31.20 -1 -7 20 63.69 33.40 -1 -7 20 87.69 37.90 1 7 -20 138.39 23.50 -1 7 20 106.99 31.80 1 7 -20 45.70 22.90 -1 7 20 80.69 27.50 -1 7 20 86.19 25.60 -1 7 20 135.19 23.90 0 -7 -20 4.70 19.50 0 -7 -20 -52.29 19.80 0 -7 20 29.30 32.20 0 -7 20 -43.90 22.90 0 -7 20 -10.20 31.40 0 -7 -20 63.79 35.70 0 7 -20 2.40 16.80 0 7 -20 10.40 21.10 0 7 20 42.80 21.40 0 7 20 47.30 20.00 0 7 20 77.89 32.50 -1 -7 -20 81.59 24.40 1 -7 20 100.89 36.90 -1 -7 -20 96.99 33.50 -1 -7 -20 46.30 28.40 1 -7 20 101.29 38.50 1 -7 20 85.49 30.70 -1 7 -20 64.29 22.90 1 7 20 106.29 31.30 1 7 20 58.19 22.40 1 7 20 138.29 27.40 1 7 20 57.39 40.70 1 7 20 83.79 34.70 4 0 -21 20.10 27.60 -4 0 21 11.50 27.70 4 0 -21 10.50 19.60 -4 0 21 -5.40 25.60 -4 0 21 -1.40 22.50 4 0 -21 6.30 19.00 3 0 -21 96.19 25.00 3 0 -21 91.49 36.70 3 0 -21 108.79 25.40 -3 0 21 60.59 28.70 -3 0 21 109.39 27.20 -3 0 21 77.19 33.70 2 0 -21 16.60 19.80 -2 0 21 -5.20 23.70 -2 0 21 9.20 20.80 -2 0 21 -24.10 34.60 -2 0 21 -36.80 26.70 2 0 -21 4.50 18.00 1 0 -21 69.19 23.50 -1 0 21 69.49 31.80 -1 0 21 14.90 31.90 1 0 -21 54.59 22.40 -1 0 21 73.39 29.20 0 0 -21 2.80 19.30 0 0 21 49.10 27.40 0 0 21 -18.00 26.30 0 0 -21 20.80 19.20 0 0 21 19.90 30.00 1 0 21 -38.90 26.70 -1 0 -21 70.29 23.30 -1 0 -21 13.70 18.50 1 0 21 51.29 35.20 1 0 21 11.50 26.90 2 0 21 154.28 37.00 2 0 21 -4.70 25.30 -2 0 -21 58.19 17.80 -2 0 -21 3.80 17.80 2 0 21 -7.30 27.70 4 -1 -21 51.49 27.30 4 -1 -21 -1.60 18.40 -4 -1 21 36.40 28.80 -4 -1 21 11.20 27.00 -4 1 21 9.70 23.00 4 1 -21 57.89 21.50 -4 1 21 8.10 21.90 4 1 -21 23.00 21.50 -4 1 21 19.10 26.30 -3 -1 21 59.59 26.70 3 -1 -21 35.80 21.20 3 -1 -21 37.40 27.40 -3 -1 21 22.60 27.80 -3 -1 21 14.20 29.30 -3 1 21 18.80 23.00 3 1 -21 49.00 22.80 -3 1 21 65.39 26.50 3 1 -21 43.00 20.40 -3 1 21 19.20 29.30 -3 1 21 3.50 28.60 -2 -1 21 12.30 27.90 -2 -1 21 -8.40 25.40 2 -1 -21 12.90 20.90 -2 -1 21 -68.39 25.90 2 -1 -21 -17.40 25.10 2 1 -21 25.80 19.80 -2 1 21 -25.10 16.60 -2 1 21 10.20 51.79 -2 1 21 -33.30 25.60 2 1 -21 28.60 22.20 -2 1 21 8.60 22.90 -1 -1 21 95.79 32.20 -1 -1 21 39.70 30.90 -1 -1 21 48.00 29.10 1 -1 -21 84.59 23.50 1 1 -21 96.29 23.90 1 1 -21 36.70 21.60 -1 1 21 50.69 32.00 -1 1 21 56.69 32.10 -1 1 21 116.39 30.10 -1 1 21 40.10 22.90 0 -1 21 -4.10 25.20 0 -1 21 6.80 26.90 0 -1 -21 23.40 20.90 0 1 21 -30.70 27.60 0 1 -21 24.30 20.70 0 1 -21 14.40 19.50 0 1 21 18.70 23.70 0 1 21 -18.30 18.10 0 1 21 -22.30 28.30 -1 -1 -21 140.99 27.70 -1 -1 -21 155.58 17.90 1 -1 21 54.69 36.60 1 -1 21 109.29 32.40 1 -1 21 56.99 32.20 1 1 21 86.49 23.30 1 1 21 107.99 30.30 1 1 21 76.29 33.50 -1 1 -21 140.49 24.60 -1 1 -21 147.69 27.80 1 1 21 106.89 38.10 2 -1 21 -10.10 33.30 -2 -1 -21 16.70 15.30 2 -1 21 30.30 29.00 2 -1 21 -19.10 26.90 -2 1 -21 32.70 30.30 2 1 21 -34.20 31.80 -2 1 -21 -1.40 17.10 2 1 21 -57.39 25.10 2 1 21 41.40 27.40 2 1 21 12.00 19.20 -2 1 -21 -13.60 11.40 -4 -2 21 -15.50 23.20 4 -2 -21 6.50 19.00 -4 -2 21 -20.20 26.90 -4 2 21 31.90 28.10 -4 2 21 29.60 23.20 -4 2 21 30.00 21.60 4 2 -21 27.70 19.10 4 2 -21 11.50 22.10 3 -2 -21 57.59 22.40 3 -2 -21 99.79 52.19 -3 -2 21 27.10 27.50 -3 -2 21 79.89 31.60 -3 -2 21 105.49 34.40 -3 2 21 126.69 29.60 -3 2 21 84.89 29.80 -3 2 21 52.49 30.30 3 2 -21 101.09 24.70 3 2 -21 104.29 24.40 -3 2 21 102.89 26.60 -2 -2 21 14.30 28.40 2 -2 -21 7.60 26.00 -2 -2 21 -47.70 25.80 2 -2 -21 12.00 19.30 -2 -2 21 21.10 31.10 -2 2 21 -2.10 27.60 -2 2 21 33.20 53.19 2 2 -21 42.90 19.60 2 2 -21 23.30 20.90 -2 2 21 -14.50 21.30 -2 2 21 65.99 24.50 1 -2 -21 85.09 23.80 -1 -2 21 99.39 32.60 1 -2 -21 65.29 31.50 -1 -2 21 58.89 32.20 -1 2 21 88.69 34.80 -1 2 21 112.59 34.50 -1 2 21 128.89 28.30 1 2 -21 97.09 24.70 1 2 -21 90.29 23.30 -1 2 21 63.89 25.00 0 -2 -21 43.10 21.20 0 -2 21 12.20 29.90 0 -2 21 5.00 26.50 0 -2 -21 54.39 10.80 0 -2 21 -16.60 25.80 0 2 21 41.50 25.60 0 2 -21 25.80 20.60 0 2 -21 14.60 18.70 0 2 21 -4.80 29.70 0 2 21 9.90 18.90 0 2 21 60.99 33.70 1 -2 21 45.90 29.90 1 -2 21 44.60 33.70 -1 -2 -21 130.09 28.10 1 -2 21 53.69 31.30 -1 -2 -21 39.60 21.50 1 2 21 41.80 31.50 1 2 21 77.49 28.30 -1 2 -21 40.70 21.50 1 2 21 45.50 21.40 -1 2 -21 26.10 19.00 1 2 21 69.49 34.90 -2 -2 -21 33.80 22.70 -2 -2 -21 11.30 16.60 2 -2 21 63.79 39.50 2 -2 21 14.90 27.60 2 -2 21 26.50 28.30 2 2 21 -3.80 27.50 2 2 21 55.39 25.50 -2 2 -21 20.50 28.60 2 2 21 10.20 18.50 -2 2 -21 11.70 9.20 -2 2 -21 5.00 17.30 2 2 21 -4.50 30.10 -4 -3 21 -11.40 49.10 -4 -3 21 -18.30 23.30 -4 -3 21 47.70 30.60 4 -3 -21 3.90 21.60 4 -3 -21 12.90 32.30 -4 3 21 -11.60 22.30 -4 3 21 61.89 21.70 -4 3 21 -9.50 29.60 -4 3 21 14.80 25.40 4 3 -21 67.39 22.10 -3 -3 21 -49.20 26.90 3 -3 -21 26.60 20.40 -3 -3 21 -10.90 29.10 -3 -3 21 -47.10 24.50 3 -3 -21 -4.10 20.80 -3 3 21 53.09 21.90 3 3 -21 -7.30 18.50 -3 3 21 30.80 47.10 -3 3 21 -14.60 27.20 3 3 -21 56.99 21.90 -3 3 21 -38.60 20.30 -2 -3 21 56.29 30.50 2 -3 -21 39.40 21.60 -2 -3 21 23.30 30.60 -2 -3 21 -26.20 28.10 2 3 -21 7.40 20.30 -2 3 21 42.00 22.50 -2 3 21 2.40 36.30 -2 3 21 10.50 21.70 2 3 -21 24.80 19.60 -2 3 21 -36.60 24.60 -1 -3 21 51.69 31.00 -1 -3 21 19.70 29.00 -1 -3 21 -27.60 27.50 1 -3 -21 49.60 22.10 -1 3 21 -42.20 27.00 1 3 -21 3.30 19.90 -1 3 21 58.59 32.80 -1 3 21 67.29 24.70 1 3 -21 42.00 20.70 -1 3 21 23.50 20.80 0 -3 -21 34.40 29.40 0 -3 -21 66.09 15.40 0 -3 21 61.19 32.80 0 -3 -21 51.49 22.30 0 -3 21 61.39 31.10 0 -3 21 54.09 32.80 0 3 21 121.09 48.50 0 3 21 60.69 32.00 0 3 -21 71.59 22.80 0 3 21 69.39 32.30 0 3 -21 61.79 22.40 0 3 21 88.19 24.50 1 -3 21 92.39 35.70 1 -3 21 73.59 30.90 1 -3 21 94.19 37.60 -1 -3 -21 108.19 19.90 1 3 21 148.09 31.60 -1 3 -21 64.09 21.70 1 3 21 103.59 38.20 1 3 21 79.49 34.70 -1 3 -21 66.09 24.00 1 3 21 94.09 23.00 -2 -3 -21 27.80 18.20 -2 -3 -21 18.60 19.90 2 -3 21 -4.60 28.20 2 -3 21 16.10 30.30 2 -3 21 26.00 35.50 2 3 21 69.49 26.10 -2 3 -21 38.50 18.90 -2 3 -21 20.50 22.30 2 3 21 64.49 34.80 2 3 21 -3.60 28.00 -3 -4 21 57.99 31.90 3 -4 -21 60.39 25.90 -3 -4 21 24.50 32.10 -3 -4 21 80.49 31.90 3 4 -21 82.89 24.10 3 4 -21 68.79 22.30 -3 4 21 94.39 31.50 -3 4 21 106.99 23.90 -3 4 21 4.80 37.00 -3 4 21 57.79 27.50 -2 -4 21 -26.50 26.40 2 -4 -21 -17.80 24.90 -2 -4 21 -23.00 26.10 -2 -4 21 -7.60 29.80 2 -4 -21 18.70 24.60 2 4 -21 15.30 18.30 2 4 -21 24.00 21.50 -2 4 21 95.09 30.50 -2 4 21 -14.60 21.40 -2 4 21 43.10 13.70 -2 4 21 64.49 21.30 -1 -4 21 0.10 30.20 1 -4 -21 -39.00 23.60 1 -4 -21 28.00 29.00 1 -4 -21 44.20 16.10 -1 -4 21 -29.90 26.50 -1 -4 21 89.99 32.50 1 4 -21 -3.30 18.20 -1 4 21 2.70 21.00 -1 4 21 59.29 22.40 1 4 -21 21.90 20.40 -1 4 21 -23.20 30.70 -1 4 21 24.50 30.80 0 -4 21 -8.60 27.60 0 -4 21 33.80 31.90 0 -4 -21 19.40 27.90 0 -4 21 98.49 33.90 0 -4 -21 60.09 17.80 0 4 21 39.70 21.90 0 4 21 1.00 30.10 0 4 21 89.39 25.10 0 4 21 6.50 32.60 0 4 -21 39.30 21.80 0 4 -21 48.70 21.60 1 -4 21 33.80 33.40 1 -4 21 -3.20 31.40 1 -4 21 10.50 25.60 -1 -4 -21 9.10 17.10 -1 -4 -21 -6.30 19.20 -1 4 -21 6.60 19.00 1 4 21 75.09 25.70 1 4 21 -7.30 17.10 -1 4 -21 9.60 20.40 1 4 21 -8.90 38.90 1 4 21 -34.30 37.10 -2 -5 21 46.70 31.30 2 -5 -21 48.30 24.40 -2 -5 21 36.00 30.90 -2 -5 21 15.20 31.40 2 -5 -21 10.40 22.40 2 -5 -21 52.69 21.30 -2 5 21 68.39 20.20 -2 5 21 122.89 33.00 2 5 -21 29.90 22.10 -2 5 21 126.99 23.10 2 5 -21 67.69 20.70 -2 5 21 42.40 34.70 -2 5 21 15.30 22.30 1 -5 -21 48.00 23.70 -1 -5 21 20.10 32.40 1 -5 -21 -15.90 23.90 -1 -5 21 -14.00 27.50 -1 -5 21 45.10 30.20 1 -5 -21 48.50 16.70 1 5 -21 57.19 21.60 -1 5 21 72.89 19.10 -1 5 21 26.30 23.00 -1 5 21 35.80 29.00 -1 5 21 -2.90 32.00 -1 5 21 63.19 22.70 1 5 -21 35.60 21.70 0 -5 -21 35.30 18.00 0 -5 -21 44.60 21.60 0 -5 -21 -45.50 25.00 0 -5 21 10.30 31.40 0 -5 21 6.70 29.20 0 -5 21 36.50 32.00 0 5 21 47.20 18.60 0 5 21 20.10 21.10 0 5 21 122.69 39.00 0 5 21 10.40 40.80 0 5 -21 37.60 22.00 0 5 21 31.30 22.10 0 5 -21 26.90 18.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 48955 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pu1 Pu 0.48266(2) 0.72187(2) 0.80291(2) 0.04593(9) Uani 1 1 d D . . . . Co1 Co 0.58420(8) 0.50519(5) 0.69154(5) 0.0495(2) Uani 1 1 d D . . . . Cl1 Cl 0.274(2) 0.732(3) 0.860(2) 0.089(5) Uani 0.35(8) 1 d D U P A 1 Cl1B Cl 0.2654(8) 0.7534(16) 0.8440(13) 0.083(3) Uani 0.65(8) 1 d D U P A 2 Cl2 Cl 0.490(3) 0.8599(16) 0.730(2) 0.082(4) Uani 0.60(14) 1 d D U P A 1 Cl2B Cl 0.484(4) 0.8696(16) 0.746(3) 0.078(5) Uani 0.40(14) 1 d D U P A 2 Cl3 Cl 0.615(2) 0.755(3) 0.9239(9) 0.084(5) Uani 0.45(11) 1 d D U P A 1 Cl3B Cl 0.605(2) 0.776(2) 0.9209(6) 0.070(4) Uani 0.55(11) 1 d D U P A 2 P1 P 0.43504(16) 0.58902(11) 0.65095(10) 0.0527(4) Uani 1 1 d . . . . . P2 P 0.70986(16) 0.60886(11) 0.71803(10) 0.0541(4) Uani 1 1 d D . . . . P3 P 0.52650(19) 0.50439(11) 0.80199(10) 0.0576(4) Uani 1 1 d D . . . . O1 O 0.3957(4) 0.6571(3) 0.7035(2) 0.0568(11) Uani 1 1 d . . . . . O2 O 0.4977(4) 0.5885(3) 0.8375(3) 0.0591(11) Uani 1 1 d . . . . . O3 O 0.6551(4) 0.6875(3) 0.7504(3) 0.0525(11) Uani 1 1 d . . . . . O4 O 0.3166(7) 0.5454(6) 0.6121(6) 0.063(3) Uani 0.71(2) 1 d D U P B 1 C1 C 0.2117(16) 0.5212(13) 0.6555(8) 0.100(5) Uani 0.71(2) 1 d D U P B 1 H1A H 0.200193 0.562752 0.693186 0.120 Uiso 0.71(2) 1 calc R U P B 1 H1B H 0.227709 0.467103 0.678963 0.120 Uiso 0.71(2) 1 calc R U P B 1 C2 C 0.0975(16) 0.5167(19) 0.6009(17) 0.152(10) Uani 0.71(2) 1 d D U P B 1 H2A H 0.081186 0.459232 0.587312 0.229 Uiso 0.71(2) 1 calc R U P B 1 H2B H 0.111889 0.548672 0.557742 0.229 Uiso 0.71(2) 1 calc R U P B 1 H2C H 0.027050 0.539485 0.622832 0.229 Uiso 0.71(2) 1 calc R U P B 1 O4B O 0.3132(19) 0.5301(16) 0.648(2) 0.074(6) Uani 0.29(2) 1 d D U P B 2 C1B C 0.182(2) 0.559(2) 0.635(2) 0.076(8) Uani 0.29(2) 1 d D U P B 2 H1BA H 0.177250 0.612295 0.608200 0.091 Uiso 0.29(2) 1 calc R U P B 2 H1BB H 0.144389 0.566195 0.680676 0.091 Uiso 0.29(2) 1 calc R U P B 2 C2B C 0.117(3) 0.490(3) 0.588(3) 0.096(12) Uani 0.29(2) 1 d D U P B 2 H2BA H 0.178483 0.456074 0.567124 0.143 Uiso 0.29(2) 1 calc R U P B 2 H2BB H 0.062029 0.514287 0.549841 0.143 Uiso 0.29(2) 1 calc R U P B 2 H2BC H 0.069959 0.455359 0.619016 0.143 Uiso 0.29(2) 1 calc R U P B 2 O5 O 0.4744(5) 0.6355(3) 0.5792(3) 0.0762(14) Uani 1 1 d . U . . . C3 C 0.3934(9) 0.6999(6) 0.5447(5) 0.087(2) Uani 1 1 d . U . . . H3A H 0.340455 0.675703 0.504254 0.105 Uiso 1 1 calc R U . . . H3B H 0.340340 0.722381 0.580224 0.105 Uiso 1 1 calc R U . . . C4 C 0.4679(13) 0.7662(8) 0.5176(8) 0.135(4) Uani 1 1 d . U . . . H4A H 0.527545 0.785147 0.556386 0.202 Uiso 1 1 calc R U . . . H4B H 0.414807 0.812208 0.500993 0.202 Uiso 1 1 calc R U . . . H4C H 0.510900 0.745652 0.477333 0.202 Uiso 1 1 calc R U . . . O6 O 0.748(2) 0.6369(13) 0.6394(7) 0.084(3) Uani 0.40(2) 1 d D U P C 1 C5 C 0.764(3) 0.7050(13) 0.6020(13) 0.089(3) Uani 0.40(2) 1 d D U P C 1 H5A H 0.818398 0.742139 0.632113 0.107 Uiso 0.40(2) 1 calc R U P C 1 H5B H 0.683548 0.733077 0.593314 0.107 Uiso 0.40(2) 1 calc R U P C 1 C6 C 0.813(3) 0.695(2) 0.5345(13) 0.108(5) Uani 0.40(2) 1 d D U P C 1 H6A H 0.894257 0.670018 0.542285 0.162 Uiso 0.40(2) 1 calc R U P C 1 H6B H 0.818357 0.748203 0.510972 0.162 Uiso 0.40(2) 1 calc R U P C 1 H6C H 0.759232 0.658225 0.503746 0.162 Uiso 0.40(2) 1 calc R U P C 1 O6B O 0.7996(12) 0.6344(8) 0.6575(7) 0.075(2) Uani 0.60(2) 1 d D U P C 2 C5B C 0.8102(19) 0.7082(10) 0.6260(10) 0.093(3) Uani 0.60(2) 1 d D U P C 2 H5B1 H 0.844879 0.746996 0.663406 0.111 Uiso 0.60(2) 1 calc R U P C 2 H5B2 H 0.726848 0.727785 0.609933 0.111 Uiso 0.60(2) 1 calc R U P C 2 C6B C 0.882(2) 0.7138(13) 0.5662(12) 0.118(5) Uani 0.60(2) 1 d D U P C 2 H6B1 H 0.966882 0.725371 0.583530 0.178 Uiso 0.60(2) 1 calc R U P C 2 H6B2 H 0.850225 0.758320 0.534195 0.178 Uiso 0.60(2) 1 calc R U P C 2 H6B3 H 0.877400 0.661635 0.539662 0.178 Uiso 0.60(2) 1 calc R U P C 2 O7 O 0.8506(14) 0.592(2) 0.745(2) 0.074(3) Uani 0.208(18) 1 d D U P C 1 C7 C 0.941(3) 0.639(2) 0.786(3) 0.081(4) Uani 0.208(18) 1 d D U P C 1 H7A H 0.900935 0.667742 0.825047 0.098 Uiso 0.208(18) 1 calc R U P C 1 H7B H 0.971411 0.681783 0.754631 0.098 Uiso 0.208(18) 1 calc R U P C 1 C8 C 1.043(3) 0.593(3) 0.819(3) 0.091(6) Uani 0.208(18) 1 d D U P C 1 H8A H 1.070751 0.617561 0.865553 0.136 Uiso 0.208(18) 1 calc R U P C 1 H8B H 1.109488 0.594636 0.787133 0.136 Uiso 0.208(18) 1 calc R U P C 1 H8C H 1.018247 0.535953 0.825800 0.136 Uiso 0.208(18) 1 calc R U P C 1 O7B O 0.8152(8) 0.5759(5) 0.7788(5) 0.072(2) Uani 0.792(18) 1 d D U P C 2 C7B C 0.9059(11) 0.6270(7) 0.8158(7) 0.084(3) Uani 0.792(18) 1 d D U P C 2 H7BA H 0.865504 0.664063 0.848597 0.101 Uiso 0.792(18) 1 calc R U P C 2 H7BB H 0.943039 0.661824 0.779961 0.101 Uiso 0.792(18) 1 calc R U P C 2 C8B C 1.0019(12) 0.5826(9) 0.8573(9) 0.101(4) Uani 0.792(18) 1 d D U P C 2 H8BA H 1.029280 0.536706 0.828648 0.151 Uiso 0.792(18) 1 calc R U P C 2 H8BB H 0.970999 0.561267 0.901462 0.151 Uiso 0.792(18) 1 calc R U P C 2 H8BC H 1.070775 0.619783 0.870093 0.151 Uiso 0.792(18) 1 calc R U P C 2 O8 O 0.6038(12) 0.4480(7) 0.8608(5) 0.072(2) Uani 0.59(2) 1 d D U P D 1 C9 C 0.6585(19) 0.4808(11) 0.9283(8) 0.097(3) Uani 0.59(2) 1 d D U P D 1 H9A H 0.703460 0.531323 0.917004 0.116 Uiso 0.59(2) 1 calc R U P D 1 H9B H 0.591081 0.498022 0.956844 0.116 Uiso 0.59(2) 1 calc R U P D 1 C10 C 0.735(2) 0.4343(14) 0.9711(11) 0.127(6) Uani 0.59(2) 1 d D U P D 1 H10A H 0.687286 0.399912 1.001724 0.190 Uiso 0.59(2) 1 calc R U P D 1 H10B H 0.789761 0.469898 1.001543 0.190 Uiso 0.59(2) 1 calc R U P D 1 H10C H 0.782501 0.399116 0.941501 0.190 Uiso 0.59(2) 1 calc R U P D 1 O8B O 0.6486(16) 0.4736(14) 0.8514(9) 0.086(3) Uani 0.41(2) 1 d D U P D 2 C9B C 0.705(2) 0.4973(16) 0.9208(11) 0.094(3) Uani 0.41(2) 1 d D U P D 2 H9B1 H 0.726857 0.556218 0.917842 0.113 Uiso 0.41(2) 1 calc R U P D 2 H9B2 H 0.641840 0.493064 0.955417 0.113 Uiso 0.41(2) 1 calc R U P D 2 C10B C 0.804(3) 0.457(2) 0.9495(15) 0.110(6) Uani 0.41(2) 1 d D U P D 2 H10D H 0.782160 0.400330 0.960182 0.164 Uiso 0.41(2) 1 calc R U P D 2 H10E H 0.835899 0.484716 0.994176 0.164 Uiso 0.41(2) 1 calc R U P D 2 H10F H 0.866752 0.457335 0.915221 0.164 Uiso 0.41(2) 1 calc R U P D 2 O9 O 0.3979(6) 0.4522(4) 0.7959(4) 0.074(2) Uani 0.766(9) 1 d D U P D 1 C11 C 0.3236(12) 0.4412(8) 0.8577(8) 0.094(3) Uani 0.766(9) 1 d D U P D 1 H11A H 0.237111 0.456325 0.844680 0.113 Uiso 0.766(9) 1 calc R U P D 1 H11B H 0.356101 0.474288 0.899805 0.113 Uiso 0.766(9) 1 calc R U P D 1 C12 C 0.3377(17) 0.3438(10) 0.8739(10) 0.132(5) Uani 0.766(9) 1 d D U P D 1 H12A H 0.256853 0.317861 0.869166 0.199 Uiso 0.766(9) 1 calc R U P D 1 H12B H 0.375922 0.335551 0.922955 0.199 Uiso 0.766(9) 1 calc R U P D 1 H12C H 0.388914 0.318907 0.839230 0.199 Uiso 0.766(9) 1 calc R U P D 1 O9B O 0.465(2) 0.4260(11) 0.8385(13) 0.082(3) Uani 0.234(9) 1 d D U P D 2 C11B C 0.332(3) 0.422(3) 0.8220(18) 0.089(3) Uani 0.234(9) 1 d D U P D 2 H11C H 0.308661 0.385234 0.780804 0.107 Uiso 0.234(9) 1 calc R U P D 2 H11D H 0.296999 0.477784 0.811034 0.107 Uiso 0.234(9) 1 calc R U P D 2 C12B C 0.287(3) 0.386(3) 0.896(2) 0.099(6) Uani 0.234(9) 1 d D U P D 2 H12D H 0.256454 0.330063 0.888152 0.148 Uiso 0.234(9) 1 calc R U P D 2 H12E H 0.221013 0.421071 0.911752 0.148 Uiso 0.234(9) 1 calc R U P D 2 H12F H 0.355439 0.386113 0.933560 0.148 Uiso 0.234(9) 1 calc R U P D 2 C13 C 0.5390(14) 0.4302(10) 0.5989(8) 0.062(2) Uani 0.633(14) 1 d D U P E 1 H13 H 0.468607 0.439221 0.561813 0.075 Uiso 0.633(14) 1 calc R U P E 1 C14 C 0.5357(13) 0.3830(8) 0.6638(10) 0.063(2) Uani 0.633(14) 1 d D U P E 1 H14 H 0.463610 0.352287 0.679262 0.076 Uiso 0.633(14) 1 calc R U P E 1 C15 C 0.6575(15) 0.3852(9) 0.7018(7) 0.063(2) Uani 0.633(14) 1 d D U P E 1 H15 H 0.683820 0.356292 0.748104 0.076 Uiso 0.633(14) 1 calc R U P E 1 C16 C 0.7330(10) 0.4336(9) 0.6603(9) 0.063(2) Uani 0.633(14) 1 d D U P E 1 H16 H 0.821551 0.445638 0.673200 0.076 Uiso 0.633(14) 1 calc R U P E 1 C17 C 0.6606(17) 0.4632(8) 0.5965(7) 0.064(2) Uani 0.633(14) 1 d D U P E 1 H17 H 0.690064 0.498360 0.557513 0.076 Uiso 0.633(14) 1 calc R U P E 1 C13B C 0.5129(16) 0.4040(13) 0.6282(16) 0.062(2) Uani 0.367(14) 1 d D U P E 2 H13B H 0.425226 0.395333 0.610469 0.074 Uiso 0.367(14) 1 calc R U P E 2 C14B C 0.572(2) 0.3743(12) 0.6951(14) 0.062(2) Uani 0.367(14) 1 d D U P E 2 H14B H 0.533119 0.341223 0.732157 0.075 Uiso 0.367(14) 1 calc R U P E 2 C15B C 0.700(2) 0.3987(17) 0.6985(11) 0.063(3) Uani 0.367(14) 1 d D U P E 2 H15B H 0.764363 0.385848 0.738459 0.076 Uiso 0.367(14) 1 calc R U P E 2 C16B C 0.7173(18) 0.4446(16) 0.6354(15) 0.063(2) Uani 0.367(14) 1 d D U P E 2 H16B H 0.796332 0.469018 0.622891 0.076 Uiso 0.367(14) 1 calc R U P E 2 C17B C 0.602(3) 0.4491(15) 0.5913(10) 0.063(2) Uani 0.367(14) 1 d D U P E 2 H17B H 0.587459 0.475949 0.542946 0.075 Uiso 0.367(14) 1 calc R U P E 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pu1 0.04475(14) 0.04344(13) 0.04919(14) -0.00968(11) 0.00196(9) -0.00141(11) Co1 0.0530(5) 0.0433(5) 0.0506(5) -0.0072(4) -0.0046(4) 0.0086(4) Cl1 0.071(6) 0.092(11) 0.107(10) -0.004(8) 0.032(6) -0.007(5) Cl1B 0.061(3) 0.086(7) 0.104(6) -0.011(4) 0.023(3) 0.010(3) Cl2 0.101(5) 0.053(4) 0.090(8) 0.008(5) -0.003(5) 0.003(4) Cl2B 0.086(6) 0.044(4) 0.100(11) -0.001(6) -0.007(8) 0.008(4) Cl3 0.101(6) 0.075(10) 0.072(5) -0.019(4) -0.024(4) -0.007(6) Cl3B 0.080(5) 0.069(8) 0.060(3) -0.009(3) -0.006(3) -0.019(4) P1 0.0526(10) 0.0511(9) 0.0515(10) -0.0116(8) -0.0111(8) 0.0092(8) P2 0.0468(9) 0.0535(10) 0.0624(11) -0.0046(8) 0.0075(8) 0.0019(8) P3 0.0702(12) 0.0458(9) 0.0566(11) 0.0039(8) 0.0041(9) -0.0019(8) O1 0.058(3) 0.059(3) 0.052(3) -0.013(2) -0.007(2) 0.009(2) O2 0.074(3) 0.052(2) 0.053(3) -0.004(2) 0.010(2) -0.005(2) O3 0.043(2) 0.043(2) 0.073(3) -0.006(2) 0.013(2) -0.0028(18) O4 0.059(4) 0.072(5) 0.053(5) -0.013(4) -0.014(3) 0.004(3) C1 0.090(7) 0.110(9) 0.100(8) 0.018(7) -0.003(5) -0.022(7) C2 0.080(9) 0.19(2) 0.182(17) 0.015(15) -0.030(10) -0.030(12) O4B 0.058(7) 0.073(8) 0.087(11) -0.014(8) -0.010(7) -0.001(6) C1B 0.062(8) 0.079(11) 0.084(12) -0.005(9) -0.007(8) 0.001(7) C2B 0.071(16) 0.105(18) 0.105(19) -0.011(14) -0.024(14) -0.016(13) O5 0.089(3) 0.078(3) 0.062(3) 0.003(2) 0.007(2) 0.028(2) C3 0.094(4) 0.086(4) 0.080(4) 0.006(3) 0.001(3) 0.025(3) C4 0.144(8) 0.111(7) 0.148(8) 0.024(6) 0.006(7) 0.004(6) O6 0.083(6) 0.088(5) 0.084(5) 0.000(4) 0.025(5) -0.015(5) C5 0.085(6) 0.098(5) 0.086(5) 0.014(5) 0.016(5) -0.003(5) C6 0.111(11) 0.126(10) 0.088(8) 0.012(8) 0.022(8) 0.000(9) O6B 0.062(5) 0.083(4) 0.084(4) 0.000(4) 0.020(4) -0.004(4) C5B 0.093(6) 0.099(5) 0.088(5) 0.013(4) 0.018(5) -0.005(5) C6B 0.123(10) 0.132(9) 0.105(9) 0.024(8) 0.035(7) -0.008(8) O7 0.059(4) 0.078(5) 0.086(5) -0.007(5) 0.004(4) 0.001(4) C7 0.070(5) 0.082(6) 0.090(6) -0.004(5) -0.003(5) -0.004(5) C8 0.077(9) 0.093(10) 0.099(11) -0.006(10) -0.007(9) -0.002(9) O7B 0.055(3) 0.071(4) 0.087(4) -0.007(3) -0.013(3) 0.002(3) C7B 0.074(4) 0.085(5) 0.091(5) -0.004(4) -0.008(4) -0.007(4) C8B 0.080(7) 0.103(7) 0.115(8) -0.017(7) -0.022(6) -0.001(6) O8 0.079(4) 0.073(4) 0.065(4) 0.019(3) 0.004(4) -0.006(4) C9 0.095(6) 0.104(6) 0.088(5) 0.011(4) -0.013(5) -0.002(5) C10 0.132(10) 0.128(10) 0.113(9) 0.017(8) -0.032(8) 0.008(8) O8B 0.096(5) 0.091(6) 0.071(5) 0.015(5) -0.002(5) 0.011(5) C9B 0.093(6) 0.098(6) 0.087(5) 0.015(5) -0.009(5) -0.009(5) C10B 0.104(9) 0.116(10) 0.105(10) 0.022(9) -0.011(8) 0.002(8) O9 0.081(4) 0.067(4) 0.076(4) 0.002(3) 0.009(3) -0.025(3) C11 0.093(5) 0.100(5) 0.091(5) 0.000(4) 0.014(4) -0.024(4) C12 0.134(9) 0.129(7) 0.135(9) 0.037(7) 0.013(8) -0.030(7) O9B 0.088(5) 0.076(5) 0.082(5) 0.007(5) 0.010(4) -0.015(4) C11B 0.091(5) 0.087(6) 0.089(6) 0.000(5) 0.010(5) -0.018(5) C12B 0.102(10) 0.095(11) 0.102(10) 0.005(9) 0.021(9) -0.018(10) C13 0.071(4) 0.055(4) 0.061(4) -0.016(3) 0.002(4) 0.007(3) C14 0.072(4) 0.050(3) 0.066(4) -0.013(3) -0.001(4) 0.005(3) C15 0.069(4) 0.050(4) 0.070(4) -0.008(3) -0.001(4) 0.011(4) C16 0.070(4) 0.055(4) 0.065(4) -0.010(4) 0.004(3) 0.015(3) C17 0.071(4) 0.058(4) 0.062(4) -0.012(3) 0.004(4) 0.009(4) C13B 0.069(4) 0.052(4) 0.064(4) -0.013(4) 0.000(4) 0.005(4) C14B 0.069(5) 0.051(4) 0.066(4) -0.009(4) 0.002(4) 0.008(4) C15B 0.067(4) 0.053(4) 0.069(4) -0.008(4) 0.003(4) 0.012(4) C16B 0.068(4) 0.057(4) 0.065(4) -0.010(4) 0.004(4) 0.011(4) C17B 0.069(4) 0.056(4) 0.062(4) -0.013(4) 0.003(4) 0.007(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pu Pu -9.4100 4.3056 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Pu1 O1 78.59(17) . . ? O2 Pu1 O3 81.10(16) . . ? O1 Pu1 O3 80.92(16) . . ? O2 Pu1 Cl1 89.1(12) . . ? O1 Pu1 Cl1 92.4(8) . . ? O3 Pu1 Cl1 169.1(9) . . ? O2 Pu1 Cl3B 93.8(9) . . ? O1 Pu1 Cl3B 171.1(9) . . ? O3 Pu1 Cl3B 93.4(6) . . ? O2 Pu1 Cl3 86.1(11) . . ? O1 Pu1 Cl3 163.2(11) . . ? O3 Pu1 Cl3 90.0(7) . . ? Cl1 Pu1 Cl3 94.2(11) . . ? O2 Pu1 Cl1B 98.6(7) . . ? O1 Pu1 Cl1B 90.0(4) . . ? O3 Pu1 Cl1B 170.9(4) . . ? Cl3B Pu1 Cl1B 95.7(7) . . ? O2 Pu1 Cl2B 171.0(14) . . ? O1 Pu1 Cl2B 96.3(13) . . ? O3 Pu1 Cl2B 90.9(12) . . ? Cl3B Pu1 Cl2B 90.6(15) . . ? Cl1B Pu1 Cl2B 88.7(13) . . ? O2 Pu1 Cl2 163.7(11) . . ? O1 Pu1 Cl2 90.2(9) . . ? O3 Pu1 Cl2 85.5(10) . . ? Cl1 Pu1 Cl2 103.2(16) . . ? Cl3 Pu1 Cl2 103.3(14) . . ? C14 Co1 C15 40.4(4) . . ? C17B Co1 C16B 40.2(5) . . ? C17B Co1 C13B 39.9(5) . . ? C16B Co1 C13B 66.7(6) . . ? C14 Co1 C16 66.5(5) . . ? C15 Co1 C16 39.1(4) . . ? C17B Co1 C14B 66.8(7) . . ? C16B Co1 C14B 66.4(7) . . ? C13B Co1 C14B 39.4(5) . . ? C14 Co1 C13 39.5(5) . . ? C15 Co1 C13 66.7(5) . . ? C16 Co1 C13 66.2(4) . . ? C14 Co1 C17 66.8(5) . . ? C15 Co1 C17 66.7(5) . . ? C16 Co1 C17 39.7(4) . . ? C13 Co1 C17 39.6(4) . . ? C17B Co1 C15B 66.5(7) . . ? C16B Co1 C15B 38.9(5) . . ? C13B Co1 C15B 66.3(6) . . ? C14B Co1 C15B 39.8(5) . . ? C17B Co1 P3 151.9(8) . . ? C14 Co1 P3 97.8(4) . . ? C15 Co1 P3 92.8(4) . . ? C16B Co1 P3 136.7(8) . . ? C13B Co1 P3 112.9(10) . . ? C16 Co1 P3 122.9(4) . . ? C14B Co1 P3 86.6(6) . . ? C13 Co1 P3 133.2(6) . . ? C17 Co1 P3 159.5(3) . . ? C15B Co1 P3 99.1(6) . . ? C17B Co1 P2 115.1(9) . . ? C14 Co1 P2 156.0(4) . . ? C15 Co1 P2 117.3(5) . . ? C16B Co1 P2 91.1(6) . . ? C13B Co1 P2 154.8(9) . . ? C16 Co1 P2 89.9(3) . . ? C14B Co1 P2 142.6(8) . . ? C13 Co1 P2 135.5(6) . . ? C17 Co1 P2 98.3(5) . . ? C15B Co1 P2 104.2(7) . . ? P3 Co1 P2 91.30(8) . . ? O1 P1 O4 109.7(4) . . ? O1 P1 O5 107.2(3) . . ? O4 P1 O5 95.7(5) . . ? O1 P1 O4B 99.4(11) . . ? O5 P1 O4B 121.2(13) . . ? O1 P1 Co1 117.40(19) . . ? O4 P1 Co1 115.5(4) . . ? O5 P1 Co1 108.8(2) . . ? O4B P1 Co1 103.3(8) . . ? O3 P2 O7 114.5(11) . . ? O3 P2 O6B 109.9(5) . . ? O3 P2 O6 104.9(8) . . ? O7 P2 O6 90.9(18) . . ? O3 P2 O7B 106.0(4) . . ? O6B P2 O7B 97.4(7) . . ? O3 P2 Co1 117.23(18) . . ? O7 P2 Co1 120.2(12) . . ? O6B P2 Co1 116.7(5) . . ? O6 P2 Co1 102.7(8) . . ? O7B P2 Co1 107.1(3) . . ? O2 P3 O8 108.9(5) . . ? O2 P3 O9B 113.8(9) . . ? O2 P3 O8B 102.5(8) . . ? O9B P3 O8B 82.7(13) . . ? O2 P3 O9 106.0(3) . . ? O8 P3 O9 98.7(6) . . ? O2 P3 Co1 118.4(2) . . ? O8 P3 Co1 117.3(5) . . ? O9B P3 Co1 124.1(10) . . ? O8B P3 Co1 103.7(8) . . ? O9 P3 Co1 104.8(3) . . ? P1 O1 Pu1 136.1(3) . . ? P3 O2 Pu1 136.8(3) . . ? P2 O3 Pu1 137.1(3) . . ? C1 O4 P1 120.1(9) . . ? O4 C1 C2 105.9(14) . . ? O4 C1 H1A 110.6 . . ? C2 C1 H1A 110.6 . . ? O4 C1 H1B 110.6 . . ? C2 C1 H1B 110.6 . . ? H1A C1 H1B 108.7 . . ? C1 C2 H2A 109.5 . . ? C1 C2 H2B 109.5 . . ? H2A C2 H2B 109.5 . . ? C1 C2 H2C 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? C1B O4B P1 126(2) . . ? O4B C1B C2B 104.2(16) . . ? O4B C1B H1BA 110.9 . . ? C2B C1B H1BA 110.9 . . ? O4B C1B H1BB 110.9 . . ? C2B C1B H1BB 110.9 . . ? H1BA C1B H1BB 108.9 . . ? C1B C2B H2BA 109.5 . . ? C1B C2B H2BB 109.5 . . ? H2BA C2B H2BB 109.5 . . ? C1B C2B H2BC 109.5 . . ? H2BA C2B H2BC 109.5 . . ? H2BB C2B H2BC 109.5 . . ? C3 O5 P1 119.3(5) . . ? C4 C3 O5 109.6(9) . . ? C4 C3 H3A 109.7 . . ? O5 C3 H3A 109.7 . . ? C4 C3 H3B 109.7 . . ? O5 C3 H3B 109.7 . . ? H3A C3 H3B 108.2 . . ? C3 C4 H4A 109.5 . . ? C3 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C3 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C5 O6 P2 139.9(16) . . ? O6 C5 C6 116.3(15) . . ? O6 C5 H5A 108.2 . . ? C6 C5 H5A 108.2 . . ? O6 C5 H5B 108.2 . . ? C6 C5 H5B 108.2 . . ? H5A C5 H5B 107.4 . . ? C5 C6 H6A 109.5 . . ? C5 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C5 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C5B O6B P2 128.0(10) . . ? O6B C5B C6B 118.3(13) . . ? O6B C5B H5B1 107.7 . . ? C6B C5B H5B1 107.7 . . ? O6B C5B H5B2 107.7 . . ? C6B C5B H5B2 107.7 . . ? H5B1 C5B H5B2 107.1 . . ? C5B C6B H6B1 109.5 . . ? C5B C6B H6B2 109.5 . . ? H6B1 C6B H6B2 109.5 . . ? C5B C6B H6B3 109.5 . . ? H6B1 C6B H6B3 109.5 . . ? H6B2 C6B H6B3 109.5 . . ? C7 O7 P2 133(2) . . ? O7 C7 C8 115.1(18) . . ? O7 C7 H7A 108.5 . . ? C8 C7 H7A 108.5 . . ? O7 C7 H7B 108.5 . . ? C8 C7 H7B 108.5 . . ? H7A C7 H7B 107.5 . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C7B O7B P2 124.3(7) . . ? O7B C7B C8B 114.4(9) . . ? O7B C7B H7BA 108.7 . . ? C8B C7B H7BA 108.7 . . ? O7B C7B H7BB 108.7 . . ? C8B C7B H7BB 108.7 . . ? H7BA C7B H7BB 107.6 . . ? C7B C8B H8BA 109.5 . . ? C7B C8B H8BB 109.5 . . ? H8BA C8B H8BB 109.5 . . ? C7B C8B H8BC 109.5 . . ? H8BA C8B H8BC 109.5 . . ? H8BB C8B H8BC 109.5 . . ? C9 O8 P3 122.3(10) . . ? C10 C9 O8 120.0(14) . . ? C10 C9 H9A 107.3 . . ? O8 C9 H9A 107.3 . . ? C10 C9 H9B 107.3 . . ? O8 C9 H9B 107.3 . . ? H9A C9 H9B 106.9 . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C9B O8B P3 133.7(15) . . ? C10B C9B O8B 120.0(16) . . ? C10B C9B H9B1 107.3 . . ? O8B C9B H9B1 107.3 . . ? C10B C9B H9B2 107.3 . . ? O8B C9B H9B2 107.3 . . ? H9B1 C9B H9B2 106.9 . . ? C9B C10B H10D 109.5 . . ? C9B C10B H10E 109.5 . . ? H10D C10B H10E 109.5 . . ? C9B C10B H10F 109.5 . . ? H10D C10B H10F 109.5 . . ? H10E C10B H10F 109.5 . . ? C11 O9 P3 122.7(7) . . ? O9 C11 C12 102.3(11) . . ? O9 C11 H11A 111.3 . . ? C12 C11 H11A 111.3 . . ? O9 C11 H11B 111.3 . . ? C12 C11 H11B 111.3 . . ? H11A C11 H11B 109.2 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C11B O9B P3 113(2) . . ? O9B C11B C12B 102.2(16) . . ? O9B C11B H11C 111.3 . . ? C12B C11B H11C 111.3 . . ? O9B C11B H11D 111.3 . . ? C12B C11B H11D 111.3 . . ? H11C C11B H11D 109.2 . . ? C11B C12B H12D 109.5 . . ? C11B C12B H12E 109.5 . . ? H12D C12B H12E 109.5 . . ? C11B C12B H12F 109.5 . . ? H12D C12B H12F 109.5 . . ? H12E C12B H12F 109.5 . . ? C14 C13 C17 108.5(10) . . ? C14 C13 Co1 69.3(7) . . ? C17 C13 Co1 70.4(6) . . ? C14 C13 H13 125.7 . . ? C17 C13 H13 125.7 . . ? Co1 C13 H13 125.7 . . ? C13 C14 C15 107.8(11) . . ? C13 C14 Co1 71.2(7) . . ? C15 C14 Co1 70.0(7) . . ? C13 C14 H14 126.1 . . ? C15 C14 H14 126.1 . . ? Co1 C14 H14 126.1 . . ? C16 C15 C14 107.8(10) . . ? C16 C15 Co1 71.1(7) . . ? C14 C15 Co1 69.6(7) . . ? C16 C15 H15 126.1 . . ? C14 C15 H15 126.1 . . ? Co1 C15 H15 126.1 . . ? C15 C16 C17 108.9(10) . . ? C15 C16 Co1 69.7(7) . . ? C17 C16 Co1 70.4(7) . . ? C15 C16 H16 125.5 . . ? C17 C16 H16 125.5 . . ? Co1 C16 H16 125.5 . . ? C13 C17 C16 107.0(10) . . ? C13 C17 Co1 70.1(6) . . ? C16 C17 Co1 69.9(7) . . ? C13 C17 H17 126.5 . . ? C16 C17 H17 126.5 . . ? Co1 C17 H17 126.5 . . ? C14B C13B C17B 108.0(12) . . ? C14B C13B Co1 70.4(9) . . ? C17B C13B Co1 68.9(11) . . ? C14B C13B H13B 126.0 . . ? C17B C13B H13B 126.0 . . ? Co1 C13B H13B 126.0 . . ? C13B C14B C15B 107.8(12) . . ? C13B C14B Co1 70.2(9) . . ? C15B C14B Co1 70.6(11) . . ? C13B C14B H14B 126.1 . . ? C15B C14B H14B 126.1 . . ? Co1 C14B H14B 126.1 . . ? C16B C15B C14B 107.9(12) . . ? C16B C15B Co1 69.4(12) . . ? C14B C15B Co1 69.6(11) . . ? C16B C15B H15B 126.1 . . ? C14B C15B H15B 126.1 . . ? Co1 C15B H15B 126.1 . . ? C15B C16B C17B 108.7(12) . . ? C15B C16B Co1 71.7(13) . . ? C17B C16B Co1 69.3(12) . . ? C15B C16B H16B 125.7 . . ? C17B C16B H16B 125.7 . . ? Co1 C16B H16B 125.7 . . ? C13B C17B C16B 107.5(12) . . ? C13B C17B Co1 71.2(10) . . ? C16B C17B Co1 70.5(12) . . ? C13B C17B H17B 126.2 . . ? C16B C17B H17B 126.2 . . ? Co1 C17B H17B 126.2 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pu1 O2 2.216(5) . ? Pu1 O1 2.218(4) . ? Pu1 O3 2.231(4) . ? Pu1 Cl1 2.567(7) . ? Pu1 Cl3B 2.569(5) . ? Pu1 Cl3 2.569(6) . ? Pu1 Cl1B 2.569(4) . ? Pu1 Cl2B 2.573(7) . ? Pu1 Cl2 2.576(5) . ? Co1 C17B 2.06(2) . ? Co1 C14 2.064(12) . ? Co1 C15 2.069(13) . ? Co1 C16B 2.07(2) . ? Co1 C13B 2.086(11) . ? Co1 C16 2.086(13) . ? Co1 C14B 2.088(19) . ? Co1 C13 2.089(10) . ? Co1 C17 2.093(12) . ? Co1 C15B 2.10(2) . ? Co1 P3 2.160(2) . ? Co1 P2 2.160(2) . ? P1 O1 1.531(5) . ? P1 O4 1.564(8) . ? P1 O5 1.593(6) . ? P1 O4B 1.61(2) . ? P2 O3 1.525(5) . ? P2 O7 1.575(9) . ? P2 O6B 1.584(7) . ? P2 O6 1.588(8) . ? P2 O7B 1.601(6) . ? P3 O2 1.531(5) . ? P3 O8 1.577(7) . ? P3 O9B 1.584(9) . ? P3 O8B 1.602(8) . ? P3 O9 1.609(6) . ? O4 C1 1.486(13) . ? C1 C2 1.51(2) . ? C1 H1A 0.9700 . ? C1 H1B 0.9700 . ? C2 H2A 0.9600 . ? C2 H2B 0.9600 . ? C2 H2C 0.9600 . ? O4B C1B 1.487(15) . ? C1B C2B 1.52(2) . ? C1B H1BA 0.9700 . ? C1B H1BB 0.9700 . ? C2B H2BA 0.9600 . ? C2B H2BB 0.9600 . ? C2B H2BC 0.9600 . ? O5 C3 1.452(9) . ? C3 C4 1.439(14) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C4 H4A 0.9600 . ? C4 H4B 0.9600 . ? C4 H4C 0.9600 . ? O6 C5 1.300(13) . ? C5 C6 1.392(16) . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? O6B C5B 1.316(12) . ? C5B C6B 1.392(15) . ? C5B H5B1 0.9700 . ? C5B H5B2 0.9700 . ? C6B H6B1 0.9600 . ? C6B H6B2 0.9600 . ? C6B H6B3 0.9600 . ? O7 C7 1.392(14) . ? C7 C8 1.407(16) . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? O7B C7B 1.397(11) . ? C7B C8B 1.415(13) . ? C7B H7BA 0.9700 . ? C7B H7BB 0.9700 . ? C8B H8BA 0.9600 . ? C8B H8BB 0.9600 . ? C8B H8BC 0.9600 . ? O8 C9 1.414(13) . ? C9 C10 1.308(15) . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? O8B C9B 1.403(13) . ? C9B C10B 1.312(16) . ? C9B H9B1 0.9700 . ? C9B H9B2 0.9700 . ? C10B H10D 0.9600 . ? C10B H10E 0.9600 . ? C10B H10F 0.9600 . ? O9 C11 1.450(13) . ? C11 C12 1.582(17) . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? O9B C11B 1.446(16) . ? C11B C12B 1.584(19) . ? C11B H11C 0.9700 . ? C11B H11D 0.9700 . ? C12B H12D 0.9600 . ? C12B H12E 0.9600 . ? C12B H12F 0.9600 . ? C13 C14 1.404(16) . ? C13 C17 1.415(16) . ? C13 H13 0.9800 . ? C14 C15 1.426(15) . ? C14 H14 0.9800 . ? C15 C16 1.392(14) . ? C15 H15 0.9800 . ? C16 C17 1.420(14) . ? C16 H16 0.9800 . ? C17 H17 0.9800 . ? C13B C14B 1.406(17) . ? C13B C17B 1.414(17) . ? C13B H13B 0.9800 . ? C14B C15B 1.427(16) . ? C14B H14B 0.9800 . ? C15B C16B 1.389(15) . ? C15B H15B 0.9800 . ? C16B C17B 1.419(16) . ? C16B H16B 0.9800 . ? C17B H17B 0.9800 . ?