#------------------------------------------------------------------------------ #$Date: 2024-07-17 04:33:53 +0300 (Wed, 17 Jul 2024) $ #$Revision: 293432 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/21/1572133.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572133 loop_ _publ_author_name 'Chen, Tianhong' 'Ma, Yu-Juan' 'Xiao, Guowei' 'Fang, Xiaoyu' 'Liu, Yumin' 'Li, Kangjing' 'Yan, Dongpeng' _publ_section_title ; The trade-off anionic modulation in metal--organic glasses showing color-tunable persistent luminescence ; _journal_name_full 'Materials Horizons' _journal_paper_doi 10.1039/D4MH00771A _journal_year 2024 _chemical_formula_sum 'C16 H14 Cl2 N4 Zn' _chemical_formula_weight 398.58 _chemical_name_systematic MeBIMZnCl _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-06-12 deposited with the CCDC. 2024-07-16 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 111.748(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.5588(2) _cell_length_b 9.78700(10) _cell_length_c 14.6063(2) _cell_measurement_reflns_used 18044 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 76.2100 _cell_measurement_theta_min 3.7520 _cell_volume 1667.52(5) _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.981 _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0408 _diffrn_reflns_av_unetI/netI 0.0218 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.981 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 20726 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.981 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.371 _diffrn_reflns_theta_min 3.978 _exptl_absorpt_coefficient_mu 5.016 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.59924 _exptl_absorpt_correction_type multi-scan _exptl_crystal_colour 'clear intense colourless' _exptl_crystal_density_diffrn 1.588 _exptl_crystal_description needle _exptl_crystal_F_000 808 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.150 _refine_diff_density_max 0.361 _refine_diff_density_min -0.384 _refine_diff_density_rms 0.070 _refine_ls_extinction_coef 0.00125(13) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.079 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 211 _refine_ls_number_reflns 3431 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.079 _refine_ls_R_factor_all 0.0283 _refine_ls_R_factor_gt 0.0276 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0366P)^2^+1.4775P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0737 _refine_ls_wR_factor_ref 0.0740 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3359 _reflns_number_total 3431 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4mh00771a2.cif _cod_data_source_block 20210546c _cod_original_cell_volume 1667.52(4) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1572133 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL 20210546c_a.res in P2(1)/n 20210546c.res created by SHELXL-2018/3 at 16:51:28 on 15-Jun-2022 REM Old TITL 20210546c in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.066, Rweak 0.006, Alpha 0.024, Orientation as input REM Formula found by SHELXT: C23 N22 Cl3 Zn CELL 1.54184 12.5588 9.787 14.6063 90 111.748 90 ZERR 4 0.0002 0.0001 0.0002 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl N Zn UNIT 64 56 8 16 4 L.S. 20 PLAN 2 CONF MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.036600 1.477500 EXTI 0.001249 FVAR 0.43862 ZN1 5 0.434165 0.695261 0.211956 11.00000 0.01546 0.01571 = 0.01169 0.00185 0.00443 0.00062 CL2 3 0.289629 0.812678 0.233270 11.00000 0.01780 0.02839 = 0.01454 0.00464 0.00647 0.00633 CL3 3 0.368141 0.537663 0.093296 11.00000 0.02574 0.01901 = 0.01632 -0.00215 0.00365 -0.00258 N5 4 0.533209 0.627662 0.348791 11.00000 0.01569 0.01510 = 0.01276 0.00086 0.00511 0.00000 N15 4 0.544501 0.814113 0.173843 11.00000 0.01739 0.01618 = 0.01392 0.00068 0.00653 0.00016 N12 4 0.635065 0.634746 0.509036 11.00000 0.01625 0.01830 = 0.01135 -0.00082 0.00379 0.00018 AFIX 43 H12 2 0.671359 0.667704 0.566847 11.00000 -1.20000 AFIX 0 N22 4 0.681496 0.866741 0.119431 11.00000 0.01758 0.02123 = 0.01906 -0.00055 0.00933 -0.00037 AFIX 43 H22 2 0.740336 0.857310 0.103267 11.00000 -1.20000 AFIX 0 C6 1 0.557425 0.493589 0.382985 11.00000 0.01316 0.01715 = 0.01305 0.00288 0.00525 0.00179 C16 1 0.535681 0.953255 0.149887 11.00000 0.01681 0.01651 = 0.01115 -0.00016 0.00357 -0.00248 C11 1 0.622105 0.497497 0.484513 11.00000 0.01225 0.01883 = 0.01424 0.00081 0.00579 0.00035 C4 1 0.580915 0.707792 0.426561 11.00000 0.01302 0.01731 = 0.01436 0.00098 0.00539 0.00083 C21 1 0.621760 0.987174 0.114679 11.00000 0.01757 0.01905 = 0.01394 -0.00163 0.00490 -0.00151 C14 1 0.632305 0.766838 0.153521 11.00000 0.01708 0.01850 = 0.01458 0.00013 0.00554 -0.00005 C17 1 0.456967 1.051528 0.153779 11.00000 0.01973 0.01804 = 0.01573 -0.00055 0.00695 0.00031 AFIX 43 H17 2 0.400075 1.030553 0.177988 11.00000 -1.20000 AFIX 0 C7 1 0.527170 0.369389 0.333898 11.00000 0.01680 0.02040 = 0.01569 -0.00027 0.00626 0.00027 AFIX 43 H7 2 0.482720 0.365664 0.266939 11.00000 -1.20000 AFIX 0 C10 1 0.660331 0.379057 0.540301 11.00000 0.01474 0.02368 = 0.01439 0.00378 0.00497 0.00086 AFIX 43 H10 2 0.702698 0.382467 0.607687 11.00000 -1.20000 AFIX 0 C8 1 0.565800 0.251442 0.388591 11.00000 0.02098 0.01619 = 0.02401 -0.00027 0.01099 0.00028 AFIX 43 H8 2 0.547567 0.167046 0.357403 11.00000 -1.20000 AFIX 0 C20 1 0.633014 1.118174 0.082402 11.00000 0.02409 0.02261 = 0.01857 0.00034 0.00853 -0.00593 AFIX 43 H20 2 0.690911 1.139930 0.059573 11.00000 -1.20000 AFIX 0 C9 1 0.631850 0.256146 0.490027 11.00000 0.01821 0.01960 = 0.02268 0.00709 0.00988 0.00269 AFIX 43 H9 2 0.657030 0.174874 0.524205 11.00000 -1.20000 AFIX 0 C19 1 0.553974 1.214598 0.085870 11.00000 0.03098 0.01595 = 0.01681 -0.00038 0.00571 -0.00470 AFIX 43 H19 2 0.558781 1.303334 0.064952 11.00000 -1.20000 AFIX 0 C13 1 0.579253 0.859908 0.425622 11.00000 0.02339 0.01641 = 0.02014 -0.00054 0.00615 -0.00041 AFIX 137 H13A 2 0.626432 0.893045 0.391590 11.00000 -1.50000 H13B 2 0.608229 0.893401 0.492130 11.00000 -1.50000 H13C 2 0.502026 0.891358 0.392540 11.00000 -1.50000 AFIX 0 C18 1 0.466766 1.181172 0.120301 11.00000 0.02479 0.01687 = 0.01623 -0.00200 0.00462 0.00266 AFIX 43 H18 2 0.414221 1.247961 0.120601 11.00000 -1.20000 AFIX 0 C23 1 0.671713 0.622566 0.161852 11.00000 0.02221 0.02041 = 0.02176 0.00200 0.00936 0.00576 AFIX 137 H23A 2 0.639574 0.572399 0.201922 11.00000 -1.50000 H23B 2 0.753854 0.619789 0.191625 11.00000 -1.50000 H23C 2 0.647166 0.582319 0.097391 11.00000 -1.50000 AFIX 0 HKLF 4 REM 20210546c_a.res in P2(1)/n REM wR2 = 0.0740, GooF = S = 1.079, Restrained GooF = 1.079 for all data REM R1 = 0.0276 for 3359 Fo > 4sig(Fo) and 0.0283 for all 3431 data REM 211 parameters refined using 0 restraints END WGHT 0.0366 1.4775 REM Highest difference peak 0.361, deepest hole -0.384, 1-sigma level 0.070 Q1 1 0.5816 0.7826 0.4275 11.00000 0.05 0.36 Q2 1 0.5212 1.1923 0.1172 11.00000 0.05 0.36 ; _shelx_res_checksum 85954 _shelx_hkl_file ; 0 0 -1 0.51 0.15 0 0 1 0.50 0.12 0 0 -2 433.53 8.40 0 0 -2 419.57 8.67 0 0 -3 2.13 0.41 0 0 3 0.76 0.33 0 0 -3 1.75 0.44 0 0 3 0.15 0.28 0 0 -4 1117.76 26.31 0 0 4 1179.53 26.42 0 0 4 1128.73 26.39 0 0 -5 0.30 0.29 0 0 5 0.39 0.35 0 0 -5 0.19 0.36 0 0 -6 202.16 6.83 0 0 6 219.66 6.99 0 0 -7 0.20 0.40 0 0 7 0.53 0.45 0 0 -7 0.57 0.38 0 0 8 229.48 8.22 0 0 -8 233.29 7.80 0 0 9 0.91 0.66 0 0 -9 1.87 0.64 0 0 9 -0.15 0.53 0 0 -9 0.12 0.39 0 0 -10 564.85 17.00 0 0 10 569.02 17.88 0 0 -11 0.29 0.67 0 0 11 0.37 0.63 0 0 -12 20.88 2.58 0 0 12 19.87 2.67 0 0 12 16.95 2.16 0 0 12 16.45 2.66 0 0 12 15.93 2.84 0 0 13 0.17 0.76 0 0 -13 0.15 0.56 0 0 -14 253.44 9.65 0 0 14 259.26 10.42 0 0 14 276.35 9.32 0 0 14 271.25 9.62 0 0 15 1.13 0.79 0 0 15 0.92 0.58 0 0 15 -0.08 0.36 0 0 -15 0.19 0.49 0 0 -16 374.18 10.43 0 0 16 412.44 10.68 0 -1 0 3.20 0.33 0 -1 0 3.28 0.34 0 1 1 1612.15 34.68 0 -1 1 1519.64 34.79 0 1 2 1015.90 22.24 0 1 2 1034.39 23.03 0 -1 3 171.29 4.22 0 1 3 165.42 4.96 0 -1 4 4822.33 111.54 0 1 4 5368.38 112.84 0 1 -4 5312.21 112.64 0 -1 4 5800.13 111.22 0 -1 -4 4692.50 111.15 0 -1 -4 5275.30 112.00 0 1 -4 5776.84 110.99 0 1 4 5072.92 110.90 0 1 -5 39.10 2.33 0 -1 -5 38.48 2.01 0 1 5 45.01 2.47 0 -1 5 41.44 2.58 0 1 -6 1128.80 29.00 0 -1 -6 1333.12 28.54 0 1 6 1182.07 29.06 0 -1 6 1369.44 29.91 0 -1 -6 1203.58 29.80 0 1 -7 1558.66 38.51 0 -1 -7 1496.95 39.21 0 1 7 1610.47 38.77 0 -1 -7 1649.61 37.80 0 1 8 642.94 17.98 0 -1 8 717.42 18.51 0 1 -8 634.26 18.01 0 1 -8 612.02 18.06 0 1 8 803.65 19.39 0 -1 8 811.69 19.10 0 -1 -8 646.03 18.98 0 1 8 631.45 18.71 0 1 9 25.76 2.50 0 -1 -9 29.44 2.99 0 1 -9 30.91 2.83 0 -1 -9 29.63 2.73 0 -1 9 22.61 2.21 0 1 9 31.15 3.02 0 1 -9 32.69 2.70 0 1 -10 929.54 25.72 0 -1 -10 941.57 25.71 0 -1 10 919.07 25.31 0 1 10 989.70 27.10 0 -1 10 978.22 27.32 0 1 -11 167.72 7.82 0 -1 -11 167.41 7.79 0 -1 11 172.30 7.69 0 -1 11 181.71 8.45 0 -1 11 166.35 9.38 0 1 11 178.92 8.79 0 -1 11 176.29 8.89 0 1 12 43.57 3.49 0 -1 -12 44.44 3.78 0 1 -12 40.76 3.59 0 -1 12 33.04 4.15 0 1 12 42.56 4.16 0 -1 12 39.87 4.09 0 1 12 41.55 3.76 0 -1 12 41.16 3.87 0 -1 12 37.81 3.38 0 1 13 6.23 1.40 0 1 13 5.20 1.46 0 -1 -13 5.10 1.33 0 1 -13 5.89 1.44 0 1 13 4.57 1.12 0 1 14 112.71 5.54 0 -1 -14 115.05 5.80 0 1 -14 118.44 5.88 0 1 14 110.44 6.15 0 1 14 114.59 5.07 0 1 15 1.19 0.78 0 1 15 2.65 0.83 0 -1 15 1.20 0.63 0 -1 15 0.50 0.49 0 -1 -15 0.46 0.51 0 1 -15 0.10 0.43 0 1 16 26.31 1.78 0 -1 16 29.63 1.96 0 -1 16 23.92 1.58 0 1 -16 25.37 1.81 0 1 17 173.47 5.30 0 -2 0 2274.54 54.45 0 -2 0 2191.08 54.52 0 -2 1 349.01 7.91 0 2 1 263.79 7.18 0 2 -1 273.13 6.38 0 -2 1 347.80 7.91 0 2 2 2013.60 42.87 0 -2 2 2020.23 44.61 0 2 3 208.77 5.08 0 -2 3 245.60 7.15 0 2 4 2079.34 45.45 0 -2 4 1983.73 46.12 0 2 5 0.45 0.48 0 -2 5 1.35 0.69 0 2 -5 1.11 0.34 0 2 5 1.68 0.36 0 2 -6 38.11 2.72 0 -2 6 49.25 3.27 0 2 6 41.30 2.74 0 2 6 28.91 1.25 0 -2 6 26.24 1.32 0 2 -7 31.45 2.64 0 2 7 35.38 2.78 0 -2 -7 36.09 3.08 0 -2 7 33.90 2.99 0 2 8 69.27 4.32 0 -2 8 87.32 5.02 0 -2 -8 68.71 4.63 0 -2 8 79.04 4.48 0 2 8 68.07 3.92 0 2 -8 75.69 4.45 0 -2 -8 67.04 4.02 0 2 -8 73.57 4.27 0 2 8 74.01 4.25 0 2 8 71.75 4.47 0 2 9 441.41 14.31 0 -2 9 439.97 14.05 0 -2 -9 403.89 14.33 0 -2 9 405.47 13.44 0 2 9 452.56 13.33 0 -2 9 433.65 13.71 0 2 9 379.79 13.27 0 2 -9 430.67 13.68 0 -2 -9 435.60 13.50 0 2 -9 425.79 13.61 0 2 9 427.25 13.61 0 -2 9 417.05 15.42 0 -2 9 423.83 12.73 0 2 9 432.95 12.85 0 2 10 6.56 1.57 0 -2 -10 7.66 1.76 0 -2 10 6.30 1.42 0 2 10 6.04 1.42 0 -2 10 5.79 1.44 0 2 10 8.15 1.61 0 -2 -10 7.35 1.50 0 2 -10 6.06 1.41 0 -2 10 6.46 1.30 0 -2 10 9.37 2.14 0 2 10 4.46 1.12 0 2 11 140.15 6.65 0 -2 11 142.85 7.19 0 -2 11 187.48 8.29 0 2 11 123.99 6.78 0 -2 -11 164.68 7.59 0 2 -11 164.25 7.62 0 -2 11 158.93 9.19 0 -2 11 138.56 8.01 0 2 11 155.64 8.13 0 -2 12 176.02 7.97 0 2 12 156.63 7.77 0 -2 12 176.49 8.52 0 2 12 170.70 7.46 0 -2 -12 180.24 8.09 0 2 -12 170.16 7.88 0 -2 12 148.25 9.09 0 2 12 167.67 8.71 0 -2 12 153.25 8.65 0 -2 -13 158.50 7.49 0 2 13 159.81 7.08 0 2 -13 172.13 7.69 0 2 13 144.73 7.43 0 -2 13 174.76 8.28 0 -2 13 161.47 7.39 0 -2 -14 264.67 9.94 0 2 14 295.21 10.01 0 2 -14 301.56 10.44 0 -2 14 297.12 11.06 0 2 14 308.70 10.89 0 2 -15 205.03 7.39 0 -2 -15 199.47 7.08 0 -2 15 214.14 7.43 0 2 15 192.58 7.02 0 -2 16 1.15 0.42 0 2 -16 1.61 0.61 0 2 -16 1.74 0.51 0 -2 16 1.25 0.49 0 2 16 1.38 0.66 0 3 0 0.45 0.31 0 -3 0 4.42 0.72 0 -3 1 534.49 12.55 0 -3 1 571.17 12.96 0 -3 -1 560.64 12.54 0 -3 2 7.18 1.01 0 3 2 7.93 1.00 0 -3 2 10.35 1.20 0 3 3 59.58 3.05 0 -3 3 57.42 3.21 0 3 3 58.84 1.98 0 -3 4 638.90 16.29 0 3 4 573.71 12.88 0 -3 5 969.24 25.27 0 3 5 955.15 22.77 0 3 -5 1014.86 23.36 0 3 6 791.82 18.17 0 -3 6 788.86 16.58 0 3 -6 789.29 18.92 0 -3 6 715.49 19.01 0 3 -6 703.28 15.78 0 3 6 752.07 15.63 0 -3 7 74.68 4.32 0 -3 7 62.46 3.79 0 3 -7 77.32 4.75 0 3 -7 73.20 4.12 0 -3 7 68.40 4.82 0 -3 7 87.85 5.29 0 3 7 74.45 4.44 0 3 8 9.31 1.62 0 3 8 5.96 1.35 0 -3 -8 3.92 1.27 0 -3 8 4.51 1.33 0 -3 8 4.15 1.10 0 -3 8 2.82 0.99 0 3 8 5.17 1.06 0 3 -8 3.59 1.10 0 3 8 5.45 1.21 0 -3 -8 4.82 1.12 0 3 -8 4.97 1.16 0 -3 8 3.39 1.25 0 3 8 4.73 0.99 0 3 9 45.19 3.89 0 -3 -9 48.60 4.31 0 -3 9 63.77 4.73 0 -3 9 53.76 3.96 0 -3 9 50.55 3.97 0 3 9 53.09 3.57 0 3 9 44.67 3.86 0 3 -9 50.69 4.09 0 3 -9 51.63 3.86 0 -3 -9 52.62 3.81 0 3 9 47.56 3.73 0 3 9 47.08 3.36 0 3 10 283.01 11.36 0 -3 10 261.12 10.99 0 -3 -10 269.92 11.69 0 3 10 256.76 9.75 0 -3 10 281.77 10.84 0 3 10 246.91 10.46 0 3 -10 280.48 10.92 0 -3 -10 261.74 10.24 0 3 -10 276.40 10.49 0 3 10 270.01 10.56 0 3 10 268.18 9.75 0 3 11 149.94 8.08 0 -3 11 138.30 7.36 0 -3 11 168.84 7.96 0 -3 -11 146.18 8.28 0 -3 -11 158.52 7.49 0 3 -11 142.14 7.23 0 -3 11 133.50 8.39 0 3 11 143.24 6.77 0 3 12 171.62 7.83 0 -3 12 184.69 8.56 0 -3 12 192.72 8.46 0 3 12 184.74 7.75 0 -3 -12 172.35 8.01 0 -3 12 153.27 9.15 0 3 -12 169.90 7.97 0 -3 12 166.62 9.08 0 3 12 182.10 9.14 0 -3 -13 137.99 6.78 0 3 -13 156.55 7.17 0 3 13 144.22 6.61 0 -3 13 154.40 7.50 0 -3 13 137.12 6.84 0 3 13 153.85 7.09 0 3 -14 3.18 1.01 0 -3 -14 2.50 0.91 0 3 14 3.45 0.99 0 -3 14 4.48 1.28 0 3 -15 397.80 11.32 0 3 15 411.40 11.96 0 3 -15 430.30 12.04 0 3 -16 0.99 0.49 0 -3 16 0.69 0.33 0 -3 16 0.36 0.35 0 3 16 0.32 0.38 0 4 0 45.45 2.08 0 -4 0 23.78 2.02 0 -4 1 10.68 1.25 0 4 1 10.94 1.14 0 -4 -1 13.18 1.42 0 -4 2 -0.08 0.40 0 -4 -2 0.41 0.38 0 4 3 180.90 6.34 0 -4 3 179.25 6.60 0 -4 -3 171.92 6.00 0 -4 4 16.76 1.92 0 4 4 13.35 0.83 0 4 4 18.98 1.91 0 -4 5 2.93 0.99 0 4 5 2.60 0.74 0 4 -5 2.31 0.74 0 4 5 1.88 0.81 0 4 6 182.98 6.46 0 4 -6 187.81 6.89 0 -4 6 176.77 8.07 0 4 -6 195.42 7.42 0 -4 6 187.51 7.19 0 4 7 89.33 5.25 0 -4 7 102.02 6.23 0 -4 7 95.33 5.33 0 -4 7 107.23 5.18 0 4 -7 103.85 6.13 0 4 7 92.47 5.63 0 -4 7 99.36 6.02 0 4 -7 97.68 5.18 0 4 7 99.52 4.80 0 4 8 76.08 4.99 0 -4 8 82.93 5.75 0 4 8 75.97 5.06 0 4 8 67.34 3.81 0 -4 8 67.78 4.64 0 -4 8 74.60 4.54 0 4 8 71.25 5.02 0 4 -8 64.42 4.97 0 -4 -8 69.45 4.40 0 4 -8 67.96 4.43 0 -4 8 70.23 5.31 0 4 8 68.78 4.54 0 4 8 71.75 4.20 0 4 9 133.55 7.30 0 -4 -9 142.04 8.21 0 -4 9 159.06 8.41 0 -4 9 161.39 7.28 0 -4 9 141.05 7.19 0 4 9 123.29 5.86 0 4 -9 130.96 7.46 0 -4 -9 134.32 6.68 0 4 9 135.50 6.93 0 -4 9 154.19 8.39 0 4 -9 139.21 6.87 0 4 9 132.73 6.30 0 4 10 313.46 12.50 0 -4 -10 333.73 13.62 0 -4 10 285.47 12.29 0 -4 10 305.03 11.50 0 4 10 308.92 10.61 0 -4 10 346.89 12.39 0 4 -10 311.64 12.38 0 -4 -10 299.19 11.33 0 -4 10 303.68 13.15 0 4 -10 310.46 11.56 0 4 10 312.68 11.79 0 4 10 297.61 10.81 0 4 11 631.34 20.26 0 4 11 587.57 19.35 0 -4 11 639.34 19.12 0 -4 11 656.24 19.58 0 -4 -11 650.37 21.28 0 -4 -11 635.84 18.90 0 4 -11 609.21 18.80 0 4 11 587.83 17.94 0 -4 12 17.47 2.44 0 -4 12 18.33 2.54 0 4 -12 20.79 2.62 0 -4 -12 19.54 2.44 0 4 -12 19.56 2.48 0 4 12 21.28 2.45 0 -4 13 903.21 24.60 0 -4 -13 933.36 24.62 0 4 -13 999.73 25.18 0 4 13 1011.33 25.28 0 4 13 848.68 23.90 0 4 -13 936.51 25.15 0 -4 -14 0.36 0.46 0 4 -14 1.01 0.60 0 4 14 0.18 0.45 0 4 -14 0.34 0.65 0 4 -15 69.12 3.42 0 4 15 73.74 3.76 0 4 -15 75.35 3.72 0 -5 0 0.20 0.44 0 -5 -1 27.71 2.39 0 -5 1 26.86 2.50 0 5 1 32.07 2.19 0 -5 2 357.01 12.04 0 -5 -2 388.84 11.74 0 -5 2 397.95 11.71 0 5 2 366.14 10.34 0 5 2 411.73 11.43 0 -5 -3 39.49 2.87 0 5 3 49.17 3.20 0 -5 3 42.67 3.11 0 5 3 43.61 2.17 0 5 4 637.11 18.39 0 5 4 708.69 18.83 0 -5 -4 681.64 18.41 0 -5 4 629.25 18.37 0 -5 -5 459.05 13.59 0 5 5 466.23 15.40 0 -5 -5 499.87 15.02 0 5 5 444.41 14.10 0 5 -5 402.08 13.24 0 -5 5 439.71 14.32 0 5 -5 469.24 14.40 0 5 5 430.37 13.29 0 -5 5 460.37 14.13 0 5 6 228.24 9.98 0 5 -6 235.18 8.95 0 5 6 223.34 9.14 0 5 -6 212.13 8.48 0 -5 6 224.48 9.48 0 5 6 215.98 8.12 0 5 6 204.23 7.90 0 5 6 204.28 8.06 0 5 -6 228.47 8.76 0 -5 6 232.95 9.03 0 -5 -6 223.56 8.97 0 -5 -6 252.43 9.85 0 -5 6 229.94 9.04 0 5 -7 491.83 17.27 0 -5 7 503.15 17.28 0 5 7 462.12 15.60 0 5 -7 502.24 15.35 0 5 -7 477.76 14.92 0 -5 7 496.63 16.38 0 5 7 449.22 14.29 0 5 7 449.05 14.28 0 -5 -7 527.65 15.47 0 -5 7 478.06 14.26 0 5 -8 39.36 4.16 0 -5 8 38.63 3.21 0 -5 8 39.65 4.22 0 5 -8 43.93 3.67 0 -5 8 34.64 3.78 0 5 8 34.11 3.31 0 5 -8 35.34 3.25 0 5 8 35.55 3.17 0 5 8 37.13 3.20 0 5 9 75.69 5.69 0 5 -9 68.60 5.58 0 -5 9 62.61 4.38 0 -5 9 82.83 5.47 0 -5 9 83.38 6.24 0 5 -9 89.00 5.45 0 -5 -9 73.59 5.99 0 -5 -9 74.01 4.89 0 5 9 59.47 4.65 0 5 -9 79.22 5.11 0 -5 9 72.25 5.63 0 5 9 76.83 4.78 0 5 9 71.59 4.73 0 5 -10 17.34 2.77 0 5 10 14.89 2.57 0 -5 10 18.59 2.62 0 5 -10 19.49 2.58 0 -5 -10 16.41 2.89 0 -5 10 13.32 2.56 0 -5 -10 14.88 2.23 0 5 10 14.17 2.28 0 -5 10 21.34 3.11 0 5 -10 18.89 2.49 0 5 10 17.65 2.40 0 5 10 17.56 2.31 0 5 11 6.12 1.63 0 -5 11 7.40 1.72 0 5 -11 6.22 1.60 0 5 -11 4.47 1.42 0 -5 -11 5.88 1.40 0 5 11 6.27 1.62 0 5 11 7.63 1.66 0 5 11 7.29 1.52 0 -5 12 43.78 3.71 0 5 -12 53.41 4.01 0 -5 -12 41.70 3.44 0 5 -12 49.38 3.78 0 5 12 46.58 3.72 0 5 12 38.78 3.23 0 -5 13 40.71 3.21 0 -5 -13 35.64 2.86 0 5 -13 39.70 3.12 0 5 13 42.46 3.29 0 5 -13 43.92 3.36 0 5 -14 12.59 1.54 0 5 14 10.94 1.52 0 5 -14 11.65 1.52 0 5 15 69.58 3.22 0 5 -15 87.44 3.53 0 -6 0 1349.96 32.81 0 6 0 1271.24 31.52 0 -6 -1 364.88 12.25 0 6 1 356.43 11.44 0 -6 1 355.16 11.27 0 6 2 336.33 10.95 0 6 -2 336.51 10.60 0 6 2 317.31 9.67 0 -6 -2 335.66 11.35 0 -6 2 300.10 10.46 0 6 3 70.63 4.35 0 -6 3 76.76 4.59 0 -6 -3 67.18 4.36 0 6 -3 73.12 4.65 0 6 3 68.62 4.24 0 6 3 76.82 5.33 0 -6 3 68.90 4.23 0 6 -4 118.18 6.15 0 6 4 112.34 5.57 0 -6 -4 110.25 5.80 0 -6 -4 98.77 5.99 0 6 4 118.93 5.99 0 6 4 110.15 5.89 0 -6 4 124.30 6.26 0 6 4 123.31 6.18 0 6 4 118.32 5.54 0 6 -4 124.73 6.82 0 -6 4 119.01 5.99 0 6 -5 182.85 7.37 0 6 5 148.43 7.75 0 -6 -5 155.38 6.77 0 6 5 140.21 6.01 0 -6 -5 175.65 7.65 0 -6 5 160.12 7.21 0 6 -5 148.59 6.52 0 6 -5 160.51 7.55 0 6 5 151.87 6.72 0 6 5 143.66 6.08 0 -6 5 153.48 6.85 0 6 6 102.08 6.65 0 6 6 85.35 4.74 0 -6 -6 91.19 5.40 0 6 -6 101.68 5.57 0 -6 6 90.85 5.79 0 6 6 94.25 5.32 0 6 6 93.96 5.16 0 6 -6 96.10 5.80 0 -6 -6 114.41 6.29 0 -6 6 95.52 5.72 0 -6 6 81.93 5.71 0 -6 -6 102.11 6.44 0 -6 -7 108.09 6.15 0 6 -7 129.83 8.28 0 6 7 119.70 7.40 0 6 -7 146.46 6.88 0 6 -7 116.80 6.33 0 -6 7 125.40 7.18 0 6 7 115.93 6.05 0 -6 7 124.28 6.80 0 -6 -7 141.34 7.07 0 6 -8 21.13 3.32 0 -6 -8 22.32 2.71 0 6 8 20.53 3.10 0 -6 8 25.01 2.98 0 -6 -8 22.88 2.62 0 6 -8 24.18 2.80 0 -6 8 23.75 3.51 0 -6 8 20.62 2.90 0 6 -8 24.16 2.81 0 6 8 23.66 2.90 0 6 8 26.64 2.82 0 6 -9 857.24 27.00 0 6 9 913.73 26.39 0 -6 9 906.59 27.25 0 -6 -9 931.04 28.04 0 6 -9 971.35 25.03 0 -6 -9 917.12 24.74 0 -6 9 815.37 25.60 0 6 -9 854.49 24.41 0 6 9 830.99 24.78 0 6 9 830.82 23.94 0 6 10 77.02 5.61 0 -6 10 82.91 5.45 0 6 -10 76.66 4.98 0 -6 -10 70.77 4.79 0 6 -10 76.48 5.04 0 6 10 75.56 5.21 0 6 10 64.69 4.56 0 6 11 399.91 14.19 0 -6 11 426.87 14.21 0 -6 -11 394.41 13.34 0 6 -11 418.40 13.78 0 6 11 377.36 13.63 0 6 11 423.20 13.68 0 -6 12 60.18 4.04 0 6 -12 54.23 3.74 0 -6 -12 50.77 3.52 0 6 -12 63.70 4.06 0 6 12 53.15 3.73 0 6 -13 23.63 2.17 0 6 -13 24.24 2.20 0 6 13 21.55 2.09 0 -6 13 23.24 2.18 0 6 -14 0.13 0.41 0 6 14 0.31 0.41 0 -7 0 0.48 0.70 0 7 0 0.60 0.77 0 7 0 2.16 1.14 0 -7 0 0.73 0.61 0 7 -1 125.65 6.08 0 7 1 126.04 6.20 0 7 1 122.44 6.99 0 7 -1 129.40 6.82 0 7 -1 124.36 6.78 0 -7 -1 121.73 6.61 0 7 1 114.69 5.47 0 7 1 123.90 5.99 0 -7 1 118.86 5.69 0 -7 -1 110.94 5.25 0 7 2 437.81 14.28 0 -7 -2 407.37 14.44 0 7 2 444.27 14.64 0 7 -2 505.60 15.71 0 7 2 459.24 15.84 0 7 -2 443.41 14.86 0 7 -2 475.47 16.25 0 7 2 435.79 13.94 0 7 2 456.30 15.44 0 -7 2 426.45 13.65 0 7 3 28.28 2.98 0 -7 -3 35.00 3.51 0 7 3 31.78 3.56 0 7 3 28.83 2.98 0 -7 -3 27.52 2.97 0 7 -3 32.23 3.34 0 7 -3 29.88 3.50 0 7 3 29.16 3.21 0 7 3 29.86 2.93 0 -7 3 28.75 2.82 0 7 4 68.26 4.73 0 -7 -4 60.90 4.73 0 7 -4 78.56 5.66 0 7 4 68.59 4.48 0 7 4 72.45 5.42 0 -7 -4 61.72 4.40 0 7 -4 81.91 5.27 0 -7 4 65.38 4.34 0 7 -5 211.31 9.23 0 -7 -5 196.14 8.73 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424.01 14.54 0 8 -4 418.71 14.56 0 8 4 389.92 13.51 0 8 4 401.68 15.02 0 8 -4 387.84 15.14 0 8 4 359.62 12.95 0 8 4 359.01 14.03 0 -8 -5 43.37 4.03 0 -8 5 40.84 3.62 0 -8 5 38.60 4.28 0 -8 -5 45.88 4.77 0 8 -5 40.06 3.84 0 8 5 42.65 3.66 0 8 5 40.53 3.96 0 8 -5 36.95 4.06 0 8 5 44.34 3.81 0 8 6 259.54 10.55 0 8 -6 264.66 10.44 0 8 6 264.34 9.94 0 8 -6 273.81 13.31 0 -8 6 282.61 10.62 0 -8 -6 234.53 10.44 0 8 7 15.72 2.42 0 8 7 13.92 2.57 0 -8 7 14.71 2.19 0 -8 -7 15.44 2.31 0 8 8 81.06 5.34 0 8 8 72.33 5.10 0 8 8 85.26 5.86 0 -8 8 71.66 4.81 0 8 9 0.82 0.96 0 -8 9 0.53 0.68 0 -8 -9 0.59 0.60 0 8 -9 2.53 1.00 0 -8 -9 1.38 0.83 0 8 9 0.29 0.67 0 8 9 1.21 0.95 0 8 10 20.79 2.51 0 -8 10 22.71 2.36 0 8 -10 23.94 2.33 0 8 10 17.51 2.20 0 -8 -10 18.43 2.01 0 8 10 22.79 2.58 0 8 11 2.44 0.89 0 8 -11 2.44 0.79 0 8 12 76.93 3.91 0 -8 12 79.69 3.60 0 -9 0 0.70 0.87 0 9 0 -0.16 0.86 0 -9 0 1.85 1.62 0 9 0 0.75 1.09 0 9 0 0.19 1.05 0 9 0 -0.46 0.94 0 -9 -1 200.87 11.45 0 -9 1 214.10 8.53 0 9 -1 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650.24 18.88 -7 -5 12 679.57 19.35 -7 5 12 691.84 19.81 -7 5 12 664.34 19.57 -7 5 11 9.13 1.99 -7 5 11 8.73 1.88 -7 -5 11 8.19 1.47 -7 5 11 10.74 2.00 -7 -5 11 11.30 1.87 -7 -5 11 7.00 1.48 -7 5 11 9.57 1.88 -7 -5 11 8.02 1.80 -7 5 11 9.07 1.90 -7 5 11 12.49 1.91 -7 5 11 9.37 1.92 -7 5 10 58.45 4.85 -7 5 10 73.99 5.35 -7 -5 10 63.10 3.96 -7 -5 10 64.08 4.14 -7 5 10 63.68 4.78 -7 -5 10 66.32 4.62 -7 -5 10 62.49 4.30 -7 5 10 67.88 4.92 -7 -5 10 73.40 5.06 -7 5 10 62.09 4.48 -7 5 10 68.30 5.09 -7 5 10 66.02 5.04 -7 5 9 76.46 5.09 -7 5 9 69.45 5.17 -7 5 9 79.78 5.58 -7 5 9 64.95 4.44 -7 -5 9 76.16 4.84 -7 -5 9 67.20 5.00 -7 -5 9 77.55 4.51 -7 -5 9 74.53 4.59 -7 5 9 75.45 5.21 -7 -5 9 71.91 4.90 -7 -5 9 79.18 4.82 -7 5 9 79.27 5.27 -7 5 9 75.79 5.63 -7 5 9 79.89 5.73 -7 5 8 193.40 8.68 -7 5 8 207.37 9.41 -7 5 8 209.82 9.47 -7 -5 8 194.89 8.56 -7 -5 8 195.75 8.11 -7 5 8 179.54 8.26 -7 -5 8 187.48 8.43 -7 -5 8 181.39 8.01 -7 5 8 199.87 8.69 -7 5 8 200.86 8.75 -7 5 8 195.48 9.72 -7 5 7 120.66 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49.02 3.51 -7 7 9 2.95 1.32 -7 7 9 3.11 1.34 -7 -7 9 1.51 0.81 -7 7 9 3.07 1.11 -7 7 9 2.07 0.83 -7 7 9 1.32 1.01 -7 7 8 140.35 7.03 -7 -7 8 129.97 5.90 -7 7 8 137.84 7.50 -7 7 8 150.30 7.76 -7 -7 8 144.67 7.09 -7 -7 8 144.88 6.84 -7 7 8 137.46 7.11 -7 7 8 160.71 8.76 -7 7 7 115.01 6.51 -7 -7 7 112.35 5.58 -7 7 7 119.48 6.94 -7 7 7 122.57 7.03 -7 -7 7 114.14 6.46 -7 -7 7 125.72 6.25 -7 7 7 105.81 5.58 -7 7 7 113.75 6.31 -7 7 7 132.11 8.11 -7 7 6 174.70 8.35 -7 7 6 157.88 8.33 -7 7 6 163.77 8.36 -7 -7 6 168.46 7.25 -7 -7 6 177.52 8.42 7 7 -6 167.57 7.02 -7 -7 6 160.88 7.41 -7 -7 6 151.39 9.06 -7 7 6 164.48 7.67 -7 7 6 151.70 7.77 -7 7 6 156.78 7.39 -7 7 6 178.88 9.82 -7 7 5 3.25 1.36 7 7 -5 1.49 0.87 -7 -7 5 1.74 1.19 -7 -7 5 1.87 0.90 -7 -7 5 1.68 1.14 -7 7 5 2.28 1.23 -7 7 5 3.67 1.28 -7 7 5 2.76 1.11 -7 7 4 101.99 6.36 -7 -7 4 96.28 5.46 7 7 -4 95.07 5.43 -7 -7 4 101.10 5.55 -7 -7 4 100.58 6.60 -7 7 4 98.11 6.21 -7 -7 3 931.34 29.40 7 7 -3 989.61 26.19 -7 -7 3 943.41 26.20 -7 -7 3 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162.01 7.37 7 7 5 160.51 7.83 -7 -7 -5 164.81 7.91 7 -7 6 1.81 0.76 -7 7 -6 1.99 0.95 -7 -7 -6 1.65 0.84 7 7 6 0.97 0.91 7 -7 7 8.87 1.26 -7 -7 -7 12.15 1.72 -7 7 -7 11.54 1.56 7 7 7 12.33 1.81 7 -7 8 4.51 0.75 7 7 8 5.70 1.07 -7 -7 -8 5.85 1.05 -7 -7 -8 2.43 0.68 -7 -8 13 1.56 0.44 -7 -8 13 1.31 0.40 -7 -8 13 1.75 0.49 -7 8 12 15.84 1.81 -7 -8 12 13.63 1.42 -7 8 12 16.47 1.74 -7 -8 12 16.77 1.58 -7 -8 12 17.78 1.59 -7 -8 11 185.02 6.73 -7 8 11 191.30 7.85 -7 -8 11 199.30 7.12 -7 8 11 195.28 7.48 -7 8 11 185.00 7.37 -7 -8 10 4.96 1.03 -7 8 10 5.82 1.31 -7 -8 10 5.05 1.22 -7 8 10 5.30 1.47 -7 8 9 318.21 11.37 -7 8 9 323.17 12.22 -7 -8 9 316.90 10.27 -7 8 9 311.72 10.99 7 8 -9 291.12 9.69 -7 8 8 47.51 3.66 -7 8 8 45.13 3.86 -7 -8 8 46.56 3.55 -7 -8 8 44.12 3.24 -7 8 8 45.79 3.65 -7 8 8 47.88 4.43 -7 8 7 639.11 19.28 -7 -8 7 586.58 16.42 -7 -8 7 668.23 18.93 7 8 -7 669.66 17.39 -7 -8 7 597.35 17.40 -7 8 7 616.24 18.33 -7 8 7 630.00 18.73 -7 8 6 120.74 6.82 -7 -8 6 127.39 5.64 -7 -8 6 126.09 6.79 7 8 -6 129.98 5.93 -7 -8 6 130.25 5.99 -7 8 6 116.05 5.98 -7 8 6 122.51 6.30 -7 8 6 128.16 6.86 -7 -8 5 15.75 2.38 7 8 -5 22.31 2.43 -7 8 5 23.00 2.90 -7 8 5 15.63 2.24 -7 8 5 18.78 2.64 -7 -8 5 20.45 2.20 7 8 -4 25.96 2.73 -7 8 4 24.72 2.93 -7 8 4 29.54 3.25 7 8 -3 631.11 18.63 -7 -8 3 629.48 18.69 -7 -8 3 636.97 19.90 -7 8 3 648.36 20.33 -7 8 3 609.33 19.49 -7 8 3 682.10 19.72 -7 -8 2 56.53 4.57 -7 -8 2 52.79 4.14 -7 8 2 53.48 4.52 -7 8 2 55.22 4.73 -7 -8 1 140.06 7.44 -7 -8 1 136.51 7.13 -7 8 1 121.66 7.33 -7 -8 0 6.86 1.69 -7 -8 0 5.16 1.48 7 8 0 5.43 1.24 -7 8 0 6.13 1.82 -7 8 0 6.33 1.81 -7 -8 -1 48.23 4.02 -7 -8 -1 48.58 4.16 -7 8 -1 41.73 4.20 -7 8 -1 50.70 4.34 7 8 1 41.83 3.47 -7 -8 -1 44.86 2.99 -7 -8 -2 71.79 4.69 -7 8 -2 59.28 4.89 -7 8 -2 68.82 4.82 7 8 2 59.10 4.17 -7 -8 -2 63.14 3.64 -7 -8 -3 288.74 9.83 -7 -8 -3 277.82 10.98 -7 8 -3 304.52 11.54 7 8 3 278.45 10.28 -7 -8 -3 269.00 9.02 7 8 4 1.24 0.83 -7 -8 -4 1.42 0.91 -7 -8 -4 1.35 0.91 -7 8 -4 1.61 0.92 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25.73 2.77 -8 4 -2 23.85 3.01 -8 4 -2 21.93 2.78 -8 -4 -3 1.80 1.31 8 -4 3 1.78 0.86 -8 4 -3 2.76 1.16 -8 -4 -3 3.09 1.18 -8 4 -3 4.59 1.27 -8 4 -3 2.30 1.17 -8 -4 -3 3.46 1.34 -8 -4 -3 2.85 1.17 8 4 3 4.48 1.49 -8 4 -3 1.73 1.07 -8 4 -4 17.47 2.86 8 -4 4 14.79 2.25 -8 4 -4 15.17 2.45 -8 4 -4 17.30 2.47 -8 -4 -4 13.16 2.30 8 4 4 15.27 2.57 -8 4 -4 10.65 1.81 -8 -4 -4 14.58 2.54 8 4 5 123.49 6.82 8 -4 5 126.45 6.87 -8 4 -5 127.41 7.14 -8 4 -5 140.19 6.91 8 4 5 135.54 7.68 -8 -4 -5 132.13 7.61 8 -4 6 17.70 2.46 8 4 6 21.36 2.62 -8 4 -6 20.37 2.62 8 4 6 18.63 2.80 -8 -4 -6 20.61 2.85 8 -4 7 14.03 2.15 8 4 7 16.45 2.17 -8 4 -7 17.96 2.25 8 4 7 18.13 2.61 -8 -4 -7 19.31 2.66 -8 -4 -7 15.26 2.20 8 4 8 0.76 0.70 8 -4 8 0.97 0.75 -8 -4 -8 -0.12 0.60 -8 4 -8 0.99 0.55 -8 -4 -8 0.81 0.72 8 4 8 0.43 0.70 8 4 9 93.03 4.23 8 -4 9 92.50 4.48 -8 -4 -9 99.48 4.73 -8 -4 -9 89.96 4.37 -8 -5 16 15.42 1.26 -8 5 16 13.01 1.27 -8 -5 16 15.54 1.35 -8 5 16 13.76 1.33 -8 -5 15 211.54 7.01 -8 -5 15 200.68 6.57 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154.92 7.88 8 5 1 135.11 7.23 -8 -5 -1 150.02 7.94 -8 5 -2 247.35 11.47 -8 -5 -2 254.66 11.20 8 5 2 263.30 11.02 -8 -5 -2 245.05 10.81 -8 -5 -2 278.69 10.23 -8 5 -2 276.62 11.49 -8 5 -2 252.66 11.00 -8 -5 -3 5.12 1.50 8 5 3 6.11 1.69 -8 5 -3 6.26 1.84 8 -5 3 7.58 1.62 -8 -5 -3 6.48 1.92 -8 -5 -3 6.04 1.49 -8 -5 -3 7.98 1.93 -8 5 -3 5.46 1.56 -8 5 -3 6.47 1.64 8 5 4 10.11 2.09 8 -5 4 5.73 1.45 -8 -5 -4 6.73 1.96 -8 -5 -4 4.96 1.32 -8 5 -4 8.74 1.99 -8 -5 -4 7.52 1.82 -8 5 -4 6.55 1.63 8 5 5 329.35 11.83 8 -5 5 333.67 11.94 -8 5 -5 348.90 12.02 -8 5 -5 356.47 12.94 8 5 5 319.34 12.68 -8 -5 -5 341.94 13.05 -8 -5 -5 297.82 11.32 8 5 6 17.66 2.22 8 -5 6 19.93 2.46 -8 5 -6 20.98 2.57 8 5 6 17.60 2.55 -8 -5 -6 20.55 2.69 -8 -5 -6 15.92 2.15 -8 -5 -7 15.88 2.24 8 -5 7 19.41 2.25 8 5 7 17.76 2.05 -8 5 -7 19.25 2.20 -8 5 -8 127.59 5.07 8 -5 8 132.44 5.75 8 5 8 145.05 5.65 -8 -5 -9 50.94 2.79 8 -5 9 50.66 2.72 8 5 9 52.38 3.05 -8 6 15 332.85 9.99 -8 -6 15 456.41 10.82 -8 6 15 358.97 10.28 -8 -6 15 456.11 10.76 -8 -6 14 1.93 0.70 -8 6 14 2.08 0.75 -8 6 14 2.11 0.73 -8 -6 13 589.26 16.68 -8 -6 13 643.07 16.88 -8 6 13 597.26 16.96 -8 -6 13 642.38 17.25 -8 6 13 625.28 17.62 -8 6 13 595.61 16.85 -8 -6 12 0.90 0.67 -8 -6 12 0.65 0.57 -8 6 12 0.75 0.69 -8 6 12 0.43 0.75 -8 -6 12 0.22 0.63 -8 -6 12 1.50 0.82 -8 6 12 1.02 0.74 -8 6 11 193.93 8.49 -8 6 11 204.68 9.02 -8 -6 11 182.69 6.99 -8 6 11 192.66 8.68 -8 -6 11 216.54 8.38 -8 -6 11 189.90 7.55 -8 -6 11 220.76 8.87 -8 6 11 193.36 8.31 -8 6 11 196.97 8.49 -8 -6 10 5.21 1.15 -8 6 10 6.65 1.70 -8 -6 10 4.93 1.33 -8 -6 10 5.55 1.27 -8 6 10 6.95 1.51 -8 -6 10 3.47 1.26 -8 6 10 6.95 1.64 -8 6 10 5.59 1.68 -8 6 9 24.23 2.92 -8 -6 9 24.59 2.76 -8 6 9 21.70 2.96 -8 -6 9 23.15 2.44 -8 6 9 26.48 3.11 -8 -6 9 23.49 2.62 -8 6 9 20.71 2.52 -8 6 9 21.43 3.06 -8 6 8 0.17 0.82 -8 6 8 0.95 1.04 -8 -6 8 0.95 0.78 -8 6 8 1.04 0.95 -8 -6 8 0.26 0.61 -8 6 8 0.93 0.85 -8 -6 8 0.72 0.71 -8 6 8 1.80 0.87 -8 6 8 0.42 0.86 -8 6 8 0.98 0.75 -8 6 7 2.16 1.09 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10.85 1.11 -8 -7 14 10.23 1.07 -8 -7 14 9.44 1.01 -8 -7 13 26.48 2.03 -8 7 13 26.84 2.14 -8 7 13 25.61 2.17 -8 -7 13 31.57 2.25 -8 -7 13 27.79 2.04 -8 -7 12 123.24 5.30 -8 7 12 120.98 5.73 -8 7 12 127.64 5.70 -8 -7 12 137.31 5.74 -8 -7 12 134.15 5.30 -8 7 11 457.19 14.80 -8 -7 11 497.81 14.10 -8 7 11 465.02 14.83 -8 7 11 470.28 14.63 -8 -7 11 509.09 14.44 -8 -7 11 500.34 13.75 -8 7 11 428.78 13.34 -8 7 10 42.21 3.79 -8 -7 10 43.09 3.25 -8 7 10 43.46 3.75 -8 -7 10 46.01 3.59 -8 7 10 41.04 3.13 -8 7 9 79.04 5.21 -8 7 9 76.10 5.23 -8 -7 9 72.10 3.95 -8 -7 9 81.45 4.70 -8 7 9 73.24 4.42 -8 7 9 70.71 5.33 -8 -7 8 6.26 1.46 -8 -7 8 10.80 1.60 -8 7 8 7.74 1.81 -8 7 8 6.21 1.48 -8 -7 8 12.59 1.88 -8 7 8 9.15 1.59 -8 7 8 10.01 2.06 -8 7 8 8.51 2.05 -8 7 7 101.46 6.47 -8 7 7 110.32 6.53 -8 -7 7 105.86 5.46 -8 -7 7 112.37 6.33 -8 -7 7 118.56 6.03 -8 7 7 101.02 6.99 -8 7 7 100.26 6.04 -8 7 6 429.88 15.04 -8 7 6 440.31 15.33 -8 -7 6 437.40 13.93 -8 -7 6 454.70 15.29 -8 -7 6 459.19 14.37 -8 7 6 398.20 13.79 -8 7 6 474.18 17.24 -8 -7 5 49.59 3.80 -8 7 5 50.88 4.36 -8 -7 5 46.38 4.15 -8 -7 5 44.40 3.60 -8 7 5 41.28 3.67 -8 7 5 46.83 4.24 -8 -7 4 168.36 8.65 -8 -7 4 155.06 7.07 -8 7 4 167.47 8.04 -8 7 4 146.51 7.99 -8 7 4 165.39 8.26 -8 7 3 75.38 5.53 -8 -7 3 75.95 5.60 -8 -7 3 86.45 5.84 -8 -7 3 68.01 4.64 -8 7 3 66.55 5.04 -8 7 3 66.18 5.22 -8 7 3 78.01 5.30 -8 7 2 200.57 9.49 -8 7 2 214.11 9.95 -8 -7 2 215.38 9.82 -8 -7 2 190.04 8.77 -8 -7 1 8.17 1.41 -8 7 1 10.32 2.25 -8 -7 1 9.99 2.05 -8 -7 1 11.46 2.07 -8 -7 0 159.69 6.81 -8 7 0 158.68 8.53 -8 7 0 173.72 8.76 -8 -7 0 154.44 8.07 -8 -7 -1 159.15 6.90 -8 7 -1 170.38 8.80 -8 7 -1 173.13 8.52 8 7 1 148.71 7.26 -8 -7 -1 174.30 8.60 -8 -7 -2 27.81 2.59 -8 -7 -2 32.56 3.20 -8 7 -2 32.56 3.60 8 7 2 26.16 2.88 -8 -7 -3 162.76 8.23 -8 7 -3 173.59 8.23 8 7 3 153.17 7.31 -8 -7 -3 155.22 7.63 -8 -7 -4 694.17 20.15 -8 -7 -4 679.67 19.56 -8 7 -4 673.34 19.99 -8 7 -4 657.08 19.31 8 7 4 643.90 19.01 -8 -7 -5 73.71 4.48 8 7 5 67.29 4.23 -8 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39.55 3.75 -11 -4 5 37.44 3.90 -11 4 5 32.63 2.98 -11 4 5 37.20 3.48 -11 -4 5 34.82 3.07 -11 4 5 35.29 3.62 -11 -4 5 39.64 3.48 -11 4 5 36.27 3.64 -11 4 5 35.61 3.05 -11 4 4 304.11 11.58 -11 -4 4 307.50 12.42 -11 4 4 269.91 10.99 -11 4 4 253.68 10.10 -11 4 4 279.57 9.79 -11 -4 4 281.21 10.31 -11 4 4 300.98 11.61 -11 -4 4 271.10 10.54 -11 4 4 306.97 11.79 -11 4 3 5.79 1.62 -11 -4 3 5.57 1.32 -11 4 3 7.19 1.69 -11 -4 3 7.11 1.56 -11 -4 3 6.78 1.82 -11 4 3 6.27 1.58 -11 4 3 5.78 1.45 -11 4 3 5.19 1.49 -11 4 2 874.77 24.80 -11 -4 2 900.18 24.11 -11 -4 2 855.94 23.96 -11 4 2 899.64 25.40 -11 4 2 869.04 24.39 -11 4 1 48.45 4.02 -11 4 1 49.23 4.27 -11 -4 1 49.66 3.81 -11 4 1 48.36 4.09 -11 4 1 50.06 4.01 -11 4 0 607.24 19.01 -11 4 0 642.47 19.61 -11 -4 0 634.23 18.21 -11 4 0 617.53 18.83 -11 4 0 632.09 18.52 -11 4 -1 34.28 3.44 -11 -4 -1 37.52 3.15 -11 4 -1 36.02 3.20 -11 4 -1 35.07 3.14 -11 -4 -2 259.67 9.32 -11 4 -2 269.59 10.27 -11 4 -2 268.66 10.35 -11 4 -2 252.32 9.07 -11 4 -3 205.18 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1.92 -13 -2 14 27.40 1.94 -13 2 13 152.74 6.21 -13 -2 13 154.39 5.84 -13 2 13 151.06 6.05 -13 -2 13 161.05 5.99 -13 2 12 4.14 1.09 -13 -2 12 5.57 1.11 -13 -2 12 4.14 0.95 -13 2 11 6.41 1.42 -13 -2 11 6.19 1.25 -13 2 11 8.95 1.63 -13 -2 11 7.96 1.27 -13 -2 10 11.52 1.60 -13 2 10 14.56 2.10 -13 -2 10 10.90 1.67 -13 2 10 7.61 1.71 -13 2 10 11.80 2.01 -13 -2 9 69.14 4.39 -13 2 9 75.67 4.60 -13 -2 9 74.92 4.43 -13 2 9 73.37 5.02 -13 2 9 78.85 5.28 -13 -2 9 67.02 4.10 -13 2 9 80.50 4.64 -13 -2 8 14.72 1.94 -13 -2 8 16.89 2.07 -13 2 8 14.53 1.99 -13 2 8 14.12 2.17 -13 2 8 15.17 2.18 -13 2 7 35.96 3.08 -13 -2 7 34.71 2.96 -13 -2 7 34.81 2.93 -13 2 7 35.31 3.33 -13 2 7 34.36 3.50 -13 2 6 0.15 0.90 -13 2 6 0.48 0.64 -13 -2 6 -0.12 0.59 -13 -2 6 1.12 0.67 -13 -2 5 268.70 9.40 -13 2 5 249.10 9.99 -13 2 5 236.66 9.00 -13 -2 5 237.69 9.12 -13 -2 5 245.63 8.82 -13 2 5 237.18 9.97 -13 -2 4 10.66 1.75 -13 2 4 17.64 2.34 -13 2 4 16.44 1.98 -13 -2 4 13.21 1.88 -13 2 4 14.79 2.26 -13 -2 3 644.02 18.80 -13 2 3 717.54 20.16 -13 2 3 663.16 18.35 -13 -2 3 703.35 19.06 -13 2 3 705.55 20.26 -13 -2 2 80.88 4.69 -13 2 2 90.30 5.28 -13 -2 2 86.94 5.35 -13 2 2 92.61 5.37 -13 -2 1 74.74 4.38 -13 2 1 82.78 4.90 -13 -2 1 79.90 4.37 -13 -2 1 78.08 4.72 -13 -2 0 0.10 0.57 -13 2 0 0.36 0.61 -13 -2 0 -0.10 0.50 13 2 0 -0.11 0.56 -13 -2 0 0.29 0.55 -13 -2 -1 72.59 3.95 -13 2 -1 74.75 4.22 -13 -2 -1 80.20 3.95 13 2 1 66.59 3.91 -13 -2 -2 0.48 0.53 -13 2 -2 0.54 0.52 -13 -2 -2 0.83 0.53 13 -2 2 0.34 0.42 13 2 2 0.39 0.40 -13 -2 -3 79.81 3.50 -13 2 -3 74.27 3.48 -13 -3 14 48.76 2.39 -13 3 13 23.60 2.05 -13 -3 13 23.32 1.87 -13 3 12 86.27 4.56 -13 -3 12 91.95 4.28 -13 3 11 246.54 8.37 -13 -3 11 228.12 7.20 -13 -3 11 230.38 8.15 -13 3 10 23.85 2.45 -13 3 10 22.63 2.32 -13 -3 10 18.31 1.79 -13 3 10 21.63 2.55 -13 3 9 67.29 4.44 -13 -3 9 65.58 3.68 -13 3 9 62.66 4.20 -13 -3 9 62.91 3.90 -13 3 9 64.63 3.97 -13 3 9 62.61 4.55 -13 3 9 66.71 4.77 -13 3 8 0.14 0.86 -13 3 8 0.44 0.59 -13 -3 8 1.28 0.70 -13 3 8 0.14 0.75 -13 -3 8 1.22 0.75 -13 3 8 0.15 0.78 -13 3 7 56.31 4.15 -13 -3 7 53.57 3.53 -13 -3 7 54.74 3.67 -13 3 7 53.71 3.61 -13 -3 6 43.67 3.19 -13 -3 6 40.35 3.15 -13 3 6 45.69 3.26 -13 3 5 64.15 4.48 -13 3 5 63.10 3.80 -13 -3 5 67.39 4.04 -13 -3 5 61.32 3.84 -13 3 5 66.87 4.55 -13 3 5 61.22 4.44 -13 3 4 1.78 1.09 -13 -3 4 1.30 0.65 -13 -3 4 1.31 0.69 -13 3 3 1.18 0.86 -13 -3 3 1.91 0.81 -13 3 2 46.48 3.53 -13 -3 2 45.61 3.23 -13 3 1 182.28 7.48 -13 -3 1 195.19 7.16 -13 -3 1 176.62 7.36 -13 3 0 134.24 5.76 -13 -3 0 112.41 4.91 -13 3 -1 13.33 1.61 -13 -3 -1 15.33 1.60 13 3 1 15.22 1.76 -13 3 -2 0.58 0.43 13 3 2 0.65 0.48 -13 -3 -2 0.68 0.40 -13 -4 13 34.19 1.98 -13 4 12 163.18 6.24 -13 -4 12 164.17 5.76 -13 4 11 14.72 1.86 -13 -4 11 15.14 1.61 -13 4 10 2.62 0.92 -13 -4 10 2.68 0.85 -13 -4 9 41.94 2.51 -13 4 9 46.13 3.39 -13 4 9 49.12 3.15 -13 -4 8 22.42 1.93 -13 4 8 24.95 2.56 -13 4 8 20.99 2.36 -13 -4 7 45.42 2.90 -13 4 7 40.22 3.29 -13 -4 7 40.45 3.00 -13 4 7 40.23 3.27 -13 4 7 41.05 3.32 -13 -4 6 0.81 0.60 -13 -4 6 2.23 0.82 -13 4 6 0.49 0.79 -13 -4 5 217.78 7.77 -13 -4 5 218.70 7.94 -13 4 5 217.87 8.74 -13 4 5 217.39 8.53 -13 4 4 168.73 7.20 -13 -4 4 172.05 6.66 -13 -4 4 173.70 6.70 -13 4 4 171.76 7.50 -13 4 4 172.54 7.39 -13 -4 3 16.44 1.80 -13 -4 3 15.68 1.72 -13 4 3 13.83 1.87 -13 -4 2 64.35 3.57 -13 4 2 62.39 3.77 -13 -4 1 8.93 1.27 -13 4 1 9.03 1.35 -13 -4 0 12.61 1.41 -13 4 0 8.13 1.20 -13 -4 -1 12.11 1.28 13 4 1 9.87 1.30 13 4 2 0.22 0.31 -13 -5 12 21.48 1.44 -13 5 11 65.60 3.34 -13 -5 11 71.51 3.21 -13 5 10 68.21 3.64 -13 -5 10 68.24 3.38 -13 5 9 39.09 2.85 -13 -5 9 47.16 2.84 -13 5 8 104.37 4.96 -13 -5 8 95.65 4.46 -13 5 8 94.29 4.63 -13 -5 7 54.60 2.70 -13 5 7 54.97 3.55 -13 -5 6 1.65 0.55 -13 -5 6 1.13 0.63 -13 5 6 2.14 0.88 -13 5 5 62.86 3.62 -13 -5 5 63.83 3.20 -13 -5 5 61.83 3.48 -13 5 5 62.14 3.94 -13 5 5 62.34 3.72 -13 5 4 34.59 2.59 -13 -5 4 44.12 2.59 -13 -5 4 37.75 2.60 -13 5 4 37.05 3.00 -13 5 4 38.65 2.98 -13 5 3 25.13 2.11 -13 -5 3 32.80 2.21 -13 -5 3 30.84 2.23 -13 5 3 30.51 2.63 -13 5 3 28.92 2.59 -13 5 2 0.25 0.37 -13 -5 2 0.86 0.45 -13 -5 1 6.10 0.94 -13 -5 1 6.15 0.93 13 5 0 107.80 4.46 -13 -5 0 121.12 4.25 -13 -5 -1 16.00 1.20 -13 -6 10 67.25 2.79 -13 -6 9 1.58 0.50 -13 -6 8 7.25 0.99 -13 -6 7 13.15 1.36 -13 6 7 12.35 1.48 -13 -6 5 134.38 5.05 -13 6 5 143.42 5.72 -13 -6 4 26.22 1.89 -13 6 4 30.62 2.35 -13 -6 3 29.14 1.62 -13 -6 3 39.15 2.18 -13 -6 2 10.45 0.91 -13 -7 6 32.39 1.72 -14 0 13 -0.06 0.37 -14 0 12 7.46 1.21 -14 0 12 5.98 1.07 -14 0 12 5.36 0.91 -14 0 11 -0.36 0.54 -14 0 11 0.41 0.57 -14 0 10 927.16 23.35 -14 0 9 0.19 0.67 -14 0 9 0.30 0.61 -14 0 9 0.41 0.60 -14 0 8 81.17 4.50 -14 0 8 85.01 4.52 -14 0 8 84.59 4.72 -14 0 7 0.56 0.67 -14 0 6 148.08 6.60 -14 0 6 148.81 6.91 -14 0 5 0.12 0.69 -14 0 5 0.30 0.55 -14 0 5 0.13 0.74 -14 0 4 294.46 10.17 -14 0 4 303.51 9.79 -14 0 4 292.49 10.66 -14 0 3 0.66 0.67 -14 0 3 0.27 0.51 -14 0 3 0.49 0.80 -14 0 2 28.15 2.52 -14 0 2 27.64 2.23 -14 0 2 30.03 2.65 -14 0 1 -0.16 0.53 -14 0 -1 0.57 0.48 -14 -1 13 4.20 0.75 -14 -1 13 5.96 0.88 -14 1 13 4.95 0.88 -14 1 12 43.33 2.64 -14 -1 12 38.81 2.32 -14 1 12 39.88 2.67 -14 -1 12 37.26 2.39 -14 1 11 2.09 0.90 -14 -1 11 2.03 0.67 -14 -1 11 2.06 0.69 -14 1 11 2.76 0.87 -14 1 10 152.41 6.11 -14 -1 10 150.10 5.92 -14 -1 10 144.53 5.69 -14 1 10 139.17 6.19 -14 1 9 91.47 4.72 -14 -1 9 93.00 4.52 -14 -1 9 80.70 4.08 -14 -1 9 86.68 4.51 -14 1 9 82.57 4.46 -14 1 8 214.12 8.21 -14 -1 8 223.86 7.97 -14 -1 8 216.74 8.25 -14 1 8 205.34 8.15 -14 1 7 15.75 2.05 -14 1 7 17.65 1.98 -14 -1 7 16.39 1.90 -14 -1 6 582.73 16.13 -14 1 6 567.37 16.56 -14 1 6 564.31 15.91 -14 -1 6 576.24 16.01 -14 -1 6 543.58 16.63 -14 1 6 571.09 16.89 -14 -1 5 18.12 2.08 -14 1 5 17.19 1.91 -14 -1 5 21.85 2.49 -14 1 5 20.26 2.41 -14 -1 4 251.65 8.89 -14 1 4 246.82 8.55 -14 -1 4 261.96 9.67 -14 1 4 255.39 9.60 -14 -1 3 17.57 1.96 -14 1 3 23.64 2.38 -14 1 3 22.64 2.03 -14 -1 3 21.36 2.03 -14 -1 3 19.98 2.33 -14 1 3 25.11 2.54 -14 -1 2 92.21 4.60 -14 1 2 94.94 4.88 -14 -1 2 104.18 4.62 -14 -1 2 105.76 5.08 -14 1 2 93.95 4.85 -14 -1 1 118.84 5.22 -14 1 1 134.96 5.69 -14 -1 1 125.83 5.07 -14 -1 1 129.45 5.17 -14 -1 0 91.66 4.21 -14 1 0 97.18 4.48 -14 -1 -1 2.27 0.68 -14 1 -1 1.75 0.61 -14 -2 12 77.21 3.44 -14 2 12 74.23 3.67 -14 -2 11 66.52 3.45 -14 2 11 73.46 3.96 -14 -2 11 68.53 3.18 -14 -2 10 80.90 3.96 -14 2 10 81.96 4.47 -14 2 10 79.77 4.08 -14 -2 10 84.05 3.87 -14 -2 9 130.84 5.31 -14 2 9 128.65 5.47 -14 -2 9 127.18 5.27 -14 -2 9 113.25 5.22 -14 -2 8 3.78 1.06 -14 2 8 4.79 1.06 -14 -2 8 2.13 0.80 -14 -2 8 2.44 0.78 -14 2 7 3.48 0.95 -14 -2 7 3.78 1.00 -14 -2 6 38.59 3.15 -14 2 6 39.00 3.21 -14 2 6 37.42 2.75 -14 -2 6 41.81 2.90 -14 2 6 35.59 3.03 -14 -2 5 27.80 2.72 -14 2 5 29.51 2.81 -14 2 5 30.05 2.38 -14 -2 5 31.18 2.49 -14 2 5 32.49 2.85 -14 -2 4 11.63 1.81 -14 -2 4 9.34 1.40 -14 2 4 12.58 1.79 -14 -2 3 25.50 2.49 -14 2 3 25.15 2.41 -14 -2 2 352.57 10.89 14 2 -2 339.80 10.32 -14 2 2 363.36 11.11 -14 -2 1 8.36 1.13 14 2 -1 9.74 1.24 -14 2 1 10.00 1.40 -14 -2 1 10.43 1.29 -14 2 0 222.87 7.24 -14 -2 0 204.22 6.58 -14 -3 10 50.90 2.88 -14 3 10 51.46 2.94 -14 -3 10 44.89 2.40 -14 -3 9 0.89 0.59 -14 3 9 1.78 0.82 -14 -3 9 0.78 0.49 -14 -3 9 1.54 0.64 -14 3 8 61.50 3.72 -14 -3 8 58.61 3.14 -14 3 8 54.52 3.16 -14 -3 8 52.91 3.35 -14 -3 8 58.31 3.25 -14 -3 7 15.63 1.63 -14 -3 7 14.10 1.55 -14 3 7 16.03 1.94 -14 -3 6 11.37 1.44 -14 3 6 11.07 1.65 -14 -3 5 1.51 0.80 -14 -3 5 1.46 0.65 -14 3 5 0.62 0.65 -14 -3 4 189.67 7.39 -14 -3 4 181.48 6.55 -14 3 4 188.35 7.21 -14 -3 3 126.79 5.52 -14 -3 3 118.65 4.92 -14 3 3 127.82 5.47 -14 -3 2 27.89 2.20 -14 -3 2 32.90 2.22 -14 3 2 27.28 2.27 14 3 -1 16.28 1.53 -14 3 1 12.85 1.48 -14 -3 0 16.42 1.34 -14 -4 11 138.91 4.70 -14 -4 9 95.20 4.03 -14 -4 8 1.91 0.65 -14 -4 8 1.70 0.50 -14 -4 8 2.38 0.68 -14 -4 7 112.63 4.29 -14 -4 7 115.56 4.63 -14 4 7 120.08 5.04 -14 -4 6 0.43 0.41 -14 -4 6 0.74 0.50 -14 4 6 -0.08 0.56 -14 -4 5 155.61 5.44 -14 4 5 150.54 5.88 -14 -4 4 18.02 1.85 -14 -4 4 22.09 1.73 -14 4 4 19.83 1.86 -14 -4 3 4.36 0.92 -14 4 3 3.26 0.78 -14 -4 3 4.35 0.80 -14 -4 2 0.16 0.32 -14 -4 1 21.71 1.48 -14 -5 10 146.11 4.54 -14 -5 8 2.06 0.55 -14 -5 7 28.49 1.85 -14 -5 6 15.23 1.32 -14 -5 5 72.88 2.79 -14 -5 5 82.70 3.22 -14 -5 4 23.76 1.42 -14 -5 4 21.38 1.69 -15 0 11 165.36 5.30 -15 0 10 0.36 0.43 -15 0 9 0.60 0.49 -15 0 9 1.36 0.56 -15 0 8 0.47 0.50 -15 0 7 305.84 9.22 -15 0 6 -0.07 0.54 -15 0 6 0.35 0.43 -15 0 6 -0.09 0.56 -15 0 5 11.62 1.45 -15 0 5 16.01 1.53 -15 0 5 14.76 1.71 -15 0 4 0.43 0.56 -15 0 4 -0.12 0.37 -15 0 4 0.41 0.51 -15 0 3 64.11 3.22 -15 0 2 0.18 0.40 -15 -1 11 3.42 0.63 -15 1 11 5.35 0.88 -15 -1 10 289.07 8.20 -15 -1 9 9.43 1.13 -15 -1 9 6.43 0.99 -15 1 8 6.30 1.08 -15 -1 8 5.10 0.93 -15 1 8 6.47 1.02 -15 -1 8 4.93 0.95 -15 1 7 42.44 2.70 -15 -1 7 43.03 2.58 -15 1 7 37.84 2.44 -15 1 6 3.00 0.85 -15 1 6 2.98 0.73 -15 1 6 2.62 0.84 -15 -1 6 3.09 0.89 -15 1 5 50.30 2.98 -15 -1 5 52.69 3.19 -15 -1 4 1.12 0.51 -15 -1 4 1.01 0.59 -15 -1 3 219.00 6.70 -15 -1 3 223.26 6.99 -15 1 2 29.44 2.00 -15 -2 10 2.69 0.53 -15 2 10 5.53 0.90 -15 2 9 1.90 0.66 -15 -2 9 2.27 0.58 -15 -2 9 1.71 0.52 -15 -2 8 138.46 4.85 -15 -2 8 145.30 5.21 -15 -2 7 21.65 1.69 -15 2 6 92.22 4.14 -15 -2 6 84.88 3.69 -15 -2 6 91.57 4.16 -15 2 5 173.78 6.15 -15 -2 5 168.49 5.74 -15 -2 5 179.34 6.32 -15 2 4 1.46 0.63 -15 -2 4 1.29 0.54 -15 2 3 5.23 0.90 -15 -2 2 80.20 3.03 -15 -3 8 42.20 2.07 -15 -3 8 48.06 2.49 -15 3 7 3.96 0.84 -15 -3 7 3.96 0.66 -15 3 6 71.89 3.31 -15 -3 6 64.27 2.85 -15 -3 6 75.99 3.41 -15 3 5 8.51 1.12 -15 -3 5 7.75 0.92 -15 -3 5 8.37 1.07 -15 -3 4 13.39 1.13 -15 -3 3 17.19 1.23 0 0 0 0.00 0.00 TITL 20210546c in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 12.558748 9.787033 14.606266 90.0000 111.7479 90.0000 ZERR 19.00 0.000203 0.000124 0.000237 0.0000 0.0018 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Cl Zn UNIT 19.00 19.00 19.00 19.00 19.00 19.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 27696 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.43417(2) 0.69526(2) 0.21196(2) 0.01446(10) Uani 1 1 d . . . . . Cl2 Cl 0.28963(4) 0.81268(4) 0.23327(3) 0.02011(11) Uani 1 1 d . . . . . Cl3 Cl 0.36814(4) 0.53766(4) 0.09330(3) 0.02154(12) Uani 1 1 d . . . . . N5 N 0.53321(12) 0.62766(14) 0.34879(10) 0.0146(3) Uani 1 1 d . . . . . N15 N 0.54450(13) 0.81411(15) 0.17384(11) 0.0156(3) Uani 1 1 d . . . . . N12 N 0.63507(12) 0.63475(15) 0.50904(10) 0.0157(3) Uani 1 1 d . . . . . H12 H 0.671359 0.667704 0.566847 0.019 Uiso 1 1 calc R U . . . N22 N 0.68150(13) 0.86674(16) 0.11943(11) 0.0186(3) Uani 1 1 d . . . . . H22 H 0.740336 0.857310 0.103267 0.022 Uiso 1 1 calc R U . . . C6 C 0.55743(14) 0.49359(17) 0.38298(12) 0.0143(3) Uani 1 1 d . . . . . C16 C 0.53568(14) 0.95325(17) 0.14989(12) 0.0153(3) Uani 1 1 d . . . . . C11 C 0.62210(14) 0.49750(18) 0.48451(12) 0.0149(3) Uani 1 1 d . . . . . C4 C 0.58092(14) 0.70779(17) 0.42656(13) 0.0148(3) Uani 1 1 d . . . . . C21 C 0.62176(15) 0.98717(18) 0.11468(12) 0.0171(3) Uani 1 1 d . . . . . C14 C 0.63230(15) 0.76684(18) 0.15352(12) 0.0168(3) Uani 1 1 d . . . . . C17 C 0.45697(15) 1.05153(18) 0.15378(13) 0.0177(3) Uani 1 1 d . . . . . H17 H 0.400075 1.030553 0.177988 0.021 Uiso 1 1 calc R U . . . C7 C 0.52717(15) 0.36939(18) 0.33390(13) 0.0176(3) Uani 1 1 d . . . . . H7 H 0.482720 0.365664 0.266939 0.021 Uiso 1 1 calc R U . . . C10 C 0.66033(14) 0.37906(19) 0.54030(13) 0.0177(3) Uani 1 1 d . . . . . H10 H 0.702698 0.382467 0.607687 0.021 Uiso 1 1 calc R U . . . C8 C 0.56580(15) 0.25144(18) 0.38859(14) 0.0196(4) Uani 1 1 d . . . . . H8 H 0.547567 0.167046 0.357403 0.024 Uiso 1 1 calc R U . . . C20 C 0.63301(16) 1.11817(19) 0.08240(13) 0.0216(4) Uani 1 1 d . . . . . H20 H 0.690911 1.139930 0.059573 0.026 Uiso 1 1 calc R U . . . C9 C 0.63185(15) 0.25615(19) 0.49003(14) 0.0195(4) Uani 1 1 d . . . . . H9 H 0.657030 0.174874 0.524205 0.023 Uiso 1 1 calc R U . . . C19 C 0.55397(17) 1.21460(19) 0.08587(13) 0.0221(4) Uani 1 1 d . . . . . H19 H 0.558781 1.303334 0.064952 0.027 Uiso 1 1 calc R U . . . C13 C 0.57925(16) 0.85991(18) 0.42562(14) 0.0205(4) Uani 1 1 d . . . . . H13A H 0.626432 0.893045 0.391590 0.031 Uiso 1 1 calc R U . . . H13B H 0.608229 0.893401 0.492130 0.031 Uiso 1 1 calc R U . . . H13C H 0.502026 0.891358 0.392540 0.031 Uiso 1 1 calc R U . . . C18 C 0.46677(16) 1.18117(18) 0.12030(13) 0.0202(4) Uani 1 1 d . . . . . H18 H 0.414221 1.247961 0.120601 0.024 Uiso 1 1 calc R U . . . C23 C 0.67171(16) 0.62257(19) 0.16185(14) 0.0211(4) Uani 1 1 d . . . . . H23A H 0.639574 0.572399 0.201922 0.032 Uiso 1 1 calc R U . . . H23B H 0.753854 0.619789 0.191625 0.032 Uiso 1 1 calc R U . . . H23C H 0.647166 0.582319 0.097391 0.032 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.01546(14) 0.01571(14) 0.01169(14) 0.00185(8) 0.00443(10) 0.00062(8) Cl2 0.0178(2) 0.0284(2) 0.0145(2) 0.00464(15) 0.00647(16) 0.00633(15) Cl3 0.0257(2) 0.0190(2) 0.0163(2) -0.00215(15) 0.00365(16) -0.00258(16) N5 0.0157(7) 0.0151(7) 0.0128(7) 0.0009(5) 0.0051(5) 0.0000(5) N15 0.0174(7) 0.0162(7) 0.0139(7) 0.0007(5) 0.0065(6) 0.0002(5) N12 0.0162(7) 0.0183(7) 0.0113(7) -0.0008(5) 0.0038(5) 0.0002(5) N22 0.0176(7) 0.0212(8) 0.0191(7) -0.0006(6) 0.0093(6) -0.0004(6) C6 0.0132(7) 0.0171(8) 0.0131(8) 0.0029(6) 0.0052(6) 0.0018(6) C16 0.0168(8) 0.0165(8) 0.0111(7) -0.0002(6) 0.0036(6) -0.0025(6) C11 0.0122(7) 0.0188(8) 0.0142(8) 0.0008(6) 0.0058(6) 0.0004(6) C4 0.0130(8) 0.0173(8) 0.0144(8) 0.0010(6) 0.0054(6) 0.0008(6) C21 0.0176(8) 0.0191(8) 0.0139(8) -0.0016(6) 0.0049(6) -0.0015(7) C14 0.0171(8) 0.0185(8) 0.0146(8) 0.0001(6) 0.0055(6) 0.0000(7) C17 0.0197(8) 0.0180(8) 0.0157(8) -0.0005(6) 0.0070(7) 0.0003(7) C7 0.0168(8) 0.0204(9) 0.0157(8) -0.0003(7) 0.0063(6) 0.0003(7) C10 0.0147(8) 0.0237(9) 0.0144(8) 0.0038(7) 0.0050(6) 0.0009(7) C8 0.0210(8) 0.0162(8) 0.0240(9) -0.0003(7) 0.0110(7) 0.0003(7) C20 0.0241(9) 0.0226(9) 0.0186(8) 0.0003(7) 0.0085(7) -0.0059(7) C9 0.0182(8) 0.0196(9) 0.0227(9) 0.0071(7) 0.0099(7) 0.0027(7) C19 0.0310(10) 0.0160(8) 0.0168(9) -0.0004(7) 0.0057(8) -0.0047(7) C13 0.0234(9) 0.0164(9) 0.0201(9) -0.0005(7) 0.0062(7) -0.0004(7) C18 0.0248(9) 0.0169(8) 0.0162(8) -0.0020(6) 0.0046(7) 0.0027(7) C23 0.0222(9) 0.0204(9) 0.0218(9) 0.0020(7) 0.0094(7) 0.0058(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn -1.5491 0.6778 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N5 Zn1 N15 102.94(6) . . ? N5 Zn1 Cl3 116.95(4) . . ? N15 Zn1 Cl3 106.03(4) . . ? N5 Zn1 Cl2 105.03(4) . . ? N15 Zn1 Cl2 114.11(4) . . ? Cl3 Zn1 Cl2 111.738(18) . . ? C4 N5 C6 106.24(14) . . ? C4 N5 Zn1 124.53(12) . . ? C6 N5 Zn1 129.03(11) . . ? C14 N15 C16 106.17(14) . . ? C14 N15 Zn1 124.58(12) . . ? C16 N15 Zn1 128.64(12) . . ? C4 N12 C11 108.14(14) . . ? C4 N12 H12 125.9 . . ? C11 N12 H12 125.9 . . ? C14 N22 C21 108.80(14) . . ? C14 N22 H22 125.6 . . ? C21 N22 H22 125.6 . . ? C7 C6 N5 130.92(15) . . ? C7 C6 C11 120.63(16) . . ? N5 C6 C11 108.45(15) . . ? C17 C16 C21 120.48(16) . . ? C17 C16 N15 130.68(16) . . ? C21 C16 N15 108.81(15) . . ? N12 C11 C10 132.28(16) . . ? N12 C11 C6 105.46(14) . . ? C10 C11 C6 122.26(16) . . ? N5 C4 N12 111.71(15) . . ? N5 C4 C13 125.65(16) . . ? N12 C4 C13 122.63(16) . . ? N22 C21 C20 132.85(16) . . ? N22 C21 C16 104.94(15) . . ? C20 C21 C16 122.20(17) . . ? N15 C14 N22 111.26(15) . . ? N15 C14 C23 126.30(16) . . ? N22 C14 C23 122.38(16) . . ? C18 C17 C16 117.47(16) . . ? C18 C17 H17 121.3 . . ? C16 C17 H17 121.3 . . ? C8 C7 C6 117.43(16) . . ? C8 C7 H7 121.3 . . ? C6 C7 H7 121.3 . . ? C9 C10 C11 116.50(16) . . ? C9 C10 H10 121.7 . . ? C11 C10 H10 121.7 . . ? C7 C8 C9 121.64(17) . . ? C7 C8 H8 119.2 . . ? C9 C8 H8 119.2 . . ? C19 C20 C21 116.85(17) . . ? C19 C20 H20 121.6 . . ? C21 C20 H20 121.6 . . ? C10 C9 C8 121.53(17) . . ? C10 C9 H9 119.2 . . ? C8 C9 H9 119.2 . . ? C20 C19 C18 121.33(17) . . ? C20 C19 H19 119.3 . . ? C18 C19 H19 119.3 . . ? C4 C13 H13A 109.5 . . ? C4 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C4 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C17 C18 C19 121.66(17) . . ? C17 C18 H18 119.2 . . ? C19 C18 H18 119.2 . . ? C14 C23 H23A 109.5 . . ? C14 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C14 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 N5 2.0340(14) . ? Zn1 N15 2.0383(15) . ? Zn1 Cl3 2.2373(5) . ? Zn1 Cl2 2.2652(5) . ? N5 C4 1.327(2) . ? N5 C6 1.397(2) . ? N15 C14 1.327(2) . ? N15 C16 1.400(2) . ? N12 C4 1.348(2) . ? N12 C11 1.384(2) . ? N12 H12 0.8600 . ? N22 C14 1.347(2) . ? N22 C21 1.385(2) . ? N22 H22 0.8600 . ? C6 C7 1.391(2) . ? C6 C11 1.403(2) . ? C16 C17 1.395(2) . ? C16 C21 1.398(2) . ? C11 C10 1.396(2) . ? C4 C13 1.489(2) . ? C21 C20 1.391(3) . ? C14 C23 1.486(3) . ? C17 C18 1.382(3) . ? C17 H17 0.9300 . ? C7 C8 1.385(3) . ? C7 H7 0.9300 . ? C10 C9 1.385(3) . ? C10 H10 0.9300 . ? C8 C9 1.405(3) . ? C8 H8 0.9300 . ? C20 C19 1.384(3) . ? C20 H20 0.9300 . ? C9 H9 0.9300 . ? C19 C18 1.403(3) . ? C19 H19 0.9300 . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C18 H18 0.9300 . ? C23 H23A 0.9600 . ? C23 H23B 0.9600 . ? C23 H23C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C4 N5 C6 C7 178.96(17) . . . . ? Zn1 N5 C6 C7 3.9(3) . . . . ? C4 N5 C6 C11 -0.25(18) . . . . ? Zn1 N5 C6 C11 -175.27(11) . . . . ? C14 N15 C16 C17 177.90(18) . . . . ? Zn1 N15 C16 C17 6.6(3) . . . . ? C14 N15 C16 C21 -0.12(18) . . . . ? Zn1 N15 C16 C21 -171.39(12) . . . . ? C4 N12 C11 C10 179.84(17) . . . . ? C4 N12 C11 C6 0.07(18) . . . . ? C7 C6 C11 N12 -179.19(15) . . . . ? N5 C6 C11 N12 0.11(18) . . . . ? C7 C6 C11 C10 1.0(3) . . . . ? N5 C6 C11 C10 -179.69(15) . . . . ? C6 N5 C4 N12 0.30(19) . . . . ? Zn1 N5 C4 N12 175.61(11) . . . . ? C6 N5 C4 C13 178.92(16) . . . . ? Zn1 N5 C4 C13 -5.8(2) . . . . ? C11 N12 C4 N5 -0.23(19) . . . . ? C11 N12 C4 C13 -178.91(15) . . . . ? C14 N22 C21 C20 -177.58(19) . . . . ? C14 N22 C21 C16 1.17(19) . . . . ? C17 C16 C21 N22 -178.90(15) . . . . ? N15 C16 C21 N22 -0.64(18) . . . . ? C17 C16 C21 C20 0.0(3) . . . . ? N15 C16 C21 C20 178.27(16) . . . . ? C16 N15 C14 N22 0.88(19) . . . . ? Zn1 N15 C14 N22 172.60(11) . . . . ? C16 N15 C14 C23 -176.65(16) . . . . ? Zn1 N15 C14 C23 -4.9(3) . . . . ? C21 N22 C14 N15 -1.3(2) . . . . ? C21 N22 C14 C23 176.32(16) . . . . ? C21 C16 C17 C18 1.0(2) . . . . ? N15 C16 C17 C18 -176.82(17) . . . . ? N5 C6 C7 C8 179.27(17) . . . . ? C11 C6 C7 C8 -1.6(2) . . . . ? N12 C11 C10 C9 -179.26(17) . . . . ? C6 C11 C10 C9 0.5(2) . . . . ? C6 C7 C8 C9 0.8(3) . . . . ? N22 C21 C20 C19 178.08(18) . . . . ? C16 C21 C20 C19 -0.5(3) . . . . ? C11 C10 C9 C8 -1.3(2) . . . . ? C7 C8 C9 C10 0.7(3) . . . . ? C21 C20 C19 C18 -0.1(3) . . . . ? C16 C17 C18 C19 -1.6(3) . . . . ? C20 C19 C18 C17 1.1(3) . . . . ?