#------------------------------------------------------------------------------ #$Date: 2024-07-19 01:10:40 +0300 (Fri, 19 Jul 2024) $ #$Revision: 293460 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/21/1572144.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572144 loop_ _publ_author_name 'Kreimer, Lisa N.' 'Hadlington, Terrance' _publ_section_title ; Macrocyclic bis-diphosphenes demonstrating bimetallic exo- and endo-cyclic binding modes ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC03516J _journal_year 2024 _chemical_formula_moiety 'C82 H120 N8 Ni2 O2 P4' _chemical_formula_sum 'C82 H120 N8 Ni2 O2 P4' _chemical_formula_weight 1491.15 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-05-23 deposited with the CCDC. 2024-07-16 downloaded from the CCDC. ; _cell_angle_alpha 97.50(3) _cell_angle_beta 99.40(3) _cell_angle_gamma 96.00(3) _cell_formula_units_Z 1 _cell_length_a 10.760(2) _cell_length_b 12.310(3) _cell_length_c 15.630(3) _cell_measurement_reflns_used 2000 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 32.50 _cell_measurement_theta_min 1.92 _cell_volume 2008.2(8) _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 150(2) _diffrn_detector Pilatus300K _diffrn_detector_area_resol_mean 5.81 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'STOE StadiVari' _diffrn_measurement_method '\w scans' _diffrn_radiation_collimation '0.6 mm diameter' _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0411 _diffrn_reflns_av_unetI/netI 0.0883 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 20319 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.996 _diffrn_reflns_theta_min 2.395 _diffrn_source 'Genix 3D HF Mo' _diffrn_source_current 1.000 _diffrn_source_power 0.050 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.599 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.826 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'STOE X-AREA 1.76' _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.233 _exptl_crystal_description block _exptl_crystal_F_000 800 _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.31 _exptl_crystal_size_min 0.22 _refine_diff_density_max 0.352 _refine_diff_density_min -0.295 _refine_diff_density_rms 0.056 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.877 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 474 _refine_ls_number_reflns 7853 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.877 _refine_ls_R_factor_all 0.0684 _refine_ls_R_factor_gt 0.0375 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0347P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0739 _refine_ls_wR_factor_ref 0.0792 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5047 _reflns_number_total 7853 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc03516j2.cif _cod_data_source_block 2b _cod_original_cell_volume 2008.2(7) _cod_database_code 1572144 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; REM Old TITL P-1 in P-1 REM SHELXT solution in P-1: R1 0.125, Rweak 0.008, Alpha 0.050 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C41 N4 O P2 Ni REM C:\XRay\TH151_~1\full\P-1_a.res in P-1 REM wR2 = 0.0875, GooF = S = 0.871, Restrained GooF = 0.871 for all data REM R1 = 0.0392 for 5047 Fo > 4sig(Fo) and 0.0704 for all 7853 data REM 459 parameters refined using 0 restraints REM Highest difference peak 0.463, deepest hole -0.336, 1-sigma level 0.059 TITL C:\XRay\TH151_~1\full\P-1_a.res in P-1 C:\XRay\TH151_~1\full\P-1_a.res created by SHELXL-2018/3 at 17:00:53 on 16-May-2024 CELL 0.71073 10.7600 12.3100 15.6300 97.500 99.400 96.000 ZERR 1.0000 0.0022 0.0025 0.0031 0.030 0.030 0.030 LATT 1 SFAC C H N O P NI UNIT 82 120 8 2 4 2 MERG 2 OMIT -2 52 FMAP 2 GRID PLAN 20 TEMP -123 BOND L.S. 20 ACTA WGHT 0.034700 FVAR 0.51237 0.62019 NI1 6 0.349501 0.680230 0.669419 11.00000 0.02692 0.01755 = 0.02027 0.00234 0.00662 0.00468 P2 5 0.590218 0.407825 0.450602 11.00000 0.02797 0.01631 = 0.01963 0.00156 0.00400 0.00487 P1 5 0.534203 0.731065 0.625655 11.00000 0.02674 0.01630 = 0.02255 0.00176 0.00469 0.00284 O1 4 0.632302 0.496976 0.638154 11.00000 0.03795 0.01904 = 0.02031 -0.00140 -0.00227 0.01238 N1 3 0.351771 0.745016 0.858383 11.00000 0.03633 0.02594 = 0.02198 0.00221 0.00823 0.00574 N3 3 0.186136 0.466716 0.662776 11.00000 0.03073 0.02311 = 0.02976 0.00539 0.01120 0.00279 N4 3 0.076353 0.600338 0.642080 11.00000 0.02849 0.02975 = 0.03469 0.00752 0.00968 0.00524 N2 3 0.374942 0.890088 0.797868 11.00000 0.04362 0.02062 = 0.02667 0.00060 0.01149 0.00684 C1 1 0.676579 0.395077 0.629583 11.00000 0.02021 0.01586 = 0.02470 0.00431 0.00591 0.00492 C13 1 0.669756 0.569608 0.715966 11.00000 0.02588 0.02036 = 0.01797 -0.00293 0.00425 0.00232 C12 1 0.633036 0.675779 0.714588 11.00000 0.02180 0.02425 = 0.02077 0.00252 0.00680 0.00285 C2 1 0.657930 0.338153 0.542930 11.00000 0.02289 0.01953 = 0.01952 0.00129 0.00669 0.00159 C11 1 0.679754 0.752948 0.790901 11.00000 0.02419 0.02114 = 0.02668 -0.00116 0.00702 0.00342 AFIX 43 H11 2 0.658663 0.826057 0.791597 11.00000 -1.20000 AFIX 0 C6 1 0.735103 0.352597 0.701585 11.00000 0.02280 0.02359 = 0.02142 0.00395 0.00638 0.00378 C7 1 0.755475 0.417143 0.794593 11.00000 0.03247 0.02463 = 0.01787 0.00499 0.00424 0.00767 C8 1 0.737842 0.538285 0.790340 11.00000 0.02352 0.02522 = 0.02209 0.00338 0.00714 0.00437 C5 1 0.769756 0.247140 0.687170 11.00000 0.03413 0.02692 = 0.02504 0.01004 0.00677 0.01021 AFIX 43 H5 2 0.807623 0.216198 0.736092 11.00000 -1.20000 AFIX 0 C3 1 0.698502 0.233695 0.533500 11.00000 0.03148 0.02147 = 0.02437 0.00194 0.00812 0.00728 AFIX 43 H3 2 0.689604 0.193907 0.476056 11.00000 -1.20000 AFIX 0 C10 1 0.754553 0.728362 0.864848 11.00000 0.02315 0.02733 = 0.02743 -0.00266 0.00655 0.00128 C33 1 0.199464 0.578761 0.658478 11.00000 0.03430 0.02510 = 0.01716 0.00213 0.00769 0.00507 C9 1 0.780190 0.619230 0.863771 11.00000 0.02753 0.03275 = 0.01921 0.00163 0.00306 0.00618 AFIX 43 H9 2 0.828069 0.599392 0.914731 11.00000 -1.20000 AFIX 0 C24 1 0.358868 0.776607 0.778146 11.00000 0.02471 0.02292 = 0.02573 0.00556 0.00704 0.00600 C39 1 0.041775 0.713633 0.641091 11.00000 0.03344 0.03536 = 0.03486 0.00915 0.00931 0.01237 AFIX 13 H39 2 0.115403 0.761398 0.628174 11.00000 -1.20000 AFIX 0 C30 1 0.379329 0.966530 0.732841 11.00000 0.05949 0.02062 = 0.03273 0.00236 0.01679 0.00982 AFIX 13 H30 2 0.390275 0.923395 0.676354 11.00000 -1.20000 AFIX 0 C38 1 0.311416 0.321833 0.607287 11.00000 0.04258 0.02567 = 0.04863 0.00610 0.01357 0.00936 AFIX 137 H38A 2 0.236802 0.265624 0.590088 11.00000 -1.50000 H38B 2 0.387164 0.286133 0.623898 11.00000 -1.50000 H38C 2 0.322009 0.361315 0.557891 11.00000 -1.50000 AFIX 0 C4 1 0.751460 0.184972 0.604362 11.00000 0.03469 0.02114 = 0.02940 0.00506 0.00823 0.00966 C40 1 0.016393 0.760238 0.730972 11.00000 0.04421 0.03978 = 0.03693 0.00782 0.01194 0.01902 AFIX 137 H40A 2 -0.051385 0.711398 0.746784 11.00000 -1.50000 H40B 2 -0.009694 0.833948 0.729116 11.00000 -1.50000 H40C 2 0.093944 0.765323 0.774785 11.00000 -1.50000 AFIX 0 C36 1 0.293164 0.403424 0.685072 11.00000 0.03290 0.02336 = 0.03898 0.00716 0.00396 0.00530 AFIX 13 H36 2 0.372446 0.457126 0.703578 11.00000 -1.20000 AFIX 0 C20 1 0.808341 0.814377 0.946871 11.00000 0.03159 0.03214 = 0.02726 -0.00711 0.00472 -0.00034 C27 1 0.331148 0.629193 0.871966 11.00000 0.03952 0.02668 = 0.02277 0.00736 0.00380 0.00552 AFIX 13 H27 2 0.318372 0.582572 0.813067 11.00000 -1.20000 AFIX 0 C19 1 0.888235 0.406556 0.845058 11.00000 0.04522 0.03787 = 0.03344 0.00032 -0.00587 0.01508 AFIX 137 H19A 2 0.953398 0.438246 0.815120 11.00000 -1.50000 H19B 2 0.896445 0.328380 0.847236 11.00000 -1.50000 H19C 2 0.899242 0.446312 0.904893 11.00000 -1.50000 AFIX 0 C25 1 0.362570 0.834842 0.923913 11.00000 0.05484 0.03697 = 0.02128 -0.00473 0.00952 0.00710 AFIX 43 H25 2 0.360108 0.832496 0.984131 11.00000 -1.20000 AFIX 0 C26 1 0.377145 0.925521 0.885779 11.00000 0.05505 0.02909 = 0.03076 -0.00540 0.01438 0.00730 AFIX 43 H26 2 0.387095 0.999964 0.913804 11.00000 -1.20000 AFIX 0 C35 1 0.058938 0.423841 0.648916 11.00000 0.03195 0.02898 = 0.04888 0.00453 0.01174 -0.00611 AFIX 43 H35 2 0.026197 0.349057 0.648681 11.00000 -1.20000 AFIX 0 C29 1 0.447272 0.597449 0.927355 11.00000 0.03991 0.04393 = 0.04242 0.01629 0.01278 0.01041 AFIX 137 H29A 2 0.520885 0.609540 0.898612 11.00000 -1.50000 H29B 2 0.432088 0.519329 0.933921 11.00000 -1.50000 H29C 2 0.463876 0.642968 0.985321 11.00000 -1.50000 AFIX 0 C18 1 0.652641 0.368623 0.842098 11.00000 0.05576 0.03322 = 0.03096 0.00476 0.01802 0.00506 AFIX 137 H18A 2 0.662739 0.410124 0.901270 11.00000 -1.50000 H18B 2 0.661484 0.290908 0.846009 11.00000 -1.50000 H18C 2 0.568354 0.374004 0.809202 11.00000 -1.50000 AFIX 0 C37 1 0.273687 0.343586 0.762664 11.00000 0.05944 0.03136 = 0.04770 0.01209 0.00655 0.00415 AFIX 137 H37A 2 0.260546 0.396992 0.811585 11.00000 -1.50000 H37B 2 0.348940 0.308047 0.781034 11.00000 -1.50000 H37C 2 0.199099 0.287394 0.745067 11.00000 -1.50000 AFIX 0 C41 1 -0.071065 0.714442 0.570317 11.00000 0.05859 0.06034 = 0.04158 0.00485 0.00054 0.02593 AFIX 137 H41A 2 -0.055978 0.676289 0.514611 11.00000 -1.50000 H41B 2 -0.083688 0.790955 0.564255 11.00000 -1.50000 H41C 2 -0.147011 0.676609 0.585997 11.00000 -1.50000 AFIX 0 C34 1 -0.009333 0.506918 0.635932 11.00000 0.02754 0.04147 = 0.05293 0.00451 0.01560 -0.00230 AFIX 43 H34 2 -0.099335 0.502445 0.624667 11.00000 -1.20000 AFIX 0 C32 1 0.255098 1.015684 0.716680 11.00000 0.06562 0.03745 = 0.05396 0.01557 0.00051 0.01196 AFIX 137 H32A 2 0.184321 0.955999 0.697587 11.00000 -1.50000 H32B 2 0.257602 1.062982 0.671024 11.00000 -1.50000 H32C 2 0.243363 1.059729 0.771019 11.00000 -1.50000 AFIX 0 C14 1 0.793333 0.068821 0.590746 11.00000 0.07977 0.02948 = 0.03562 0.01248 0.02357 0.02791 C28 1 0.210100 0.607437 0.908785 11.00000 0.03581 0.05092 = 0.04411 0.02059 0.00409 0.00256 AFIX 137 H28A 2 0.216677 0.656241 0.964570 11.00000 -1.50000 H28B 2 0.198168 0.530255 0.918461 11.00000 -1.50000 H28C 2 0.137429 0.621790 0.867057 11.00000 -1.50000 AFIX 0 C21 1 0.755332 0.781251 1.026246 11.00000 0.07440 0.04603 = 0.02927 -0.01181 0.01048 -0.00423 AFIX 137 H21A 2 0.790161 0.836499 1.077951 11.00000 -1.50000 H21B 2 0.779385 0.708985 1.037110 11.00000 -1.50000 H21C 2 0.662529 0.777070 1.014469 11.00000 -1.50000 AFIX 0 C22 1 0.771936 0.929480 0.934752 11.00000 0.05843 0.03592 = 0.03795 -0.01359 0.00009 0.00173 AFIX 137 H22A 2 0.806045 0.953992 0.885050 11.00000 -1.50000 H22B 2 0.807329 0.981779 0.988135 11.00000 -1.50000 H22C 2 0.679205 0.926115 0.923338 11.00000 -1.50000 AFIX 0 C31 1 0.492159 1.056228 0.762439 11.00000 0.05806 0.04200 = 0.08610 0.01868 0.02522 0.00537 AFIX 137 H31A 2 0.478054 1.105472 0.813519 11.00000 -1.50000 H31B 2 0.501741 1.098830 0.714622 11.00000 -1.50000 H31C 2 0.569433 1.022218 0.778259 11.00000 -1.50000 AFIX 0 C23 1 0.953530 0.821716 0.965949 11.00000 0.04240 0.05940 = 0.04769 -0.02516 -0.00679 0.00316 AFIX 137 H23A 2 0.988165 0.847820 0.916976 11.00000 -1.50000 H23B 2 0.978019 0.748525 0.973170 11.00000 -1.50000 H23C 2 0.987244 0.873497 1.019901 11.00000 -1.50000 PART 1 AFIX 0 C15 1 0.818484 0.018159 0.672975 21.00000 0.10751 0.03415 = 0.04091 0.00994 0.00764 0.04523 AFIX 137 H15A 2 0.832770 -0.058832 0.658133 21.00000 -1.50000 H15B 2 0.745143 0.020665 0.702685 21.00000 -1.50000 H15C 2 0.893989 0.059507 0.711891 21.00000 -1.50000 AFIX 0 C17 1 0.666812 -0.012477 0.531366 21.00000 0.10430 0.02050 = 0.04858 0.00584 0.01002 0.01117 AFIX 137 H17A 2 0.642363 0.014781 0.475637 21.00000 -1.50000 H17B 2 0.596161 -0.011975 0.563770 21.00000 -1.50000 H17C 2 0.687497 -0.088054 0.519765 21.00000 -1.50000 AFIX 0 C16 1 0.892107 0.066818 0.538459 21.00000 0.08808 0.04647 = 0.07761 0.02290 0.04850 0.05200 AFIX 137 H16A 2 0.967816 0.115905 0.570054 21.00000 -1.50000 H16B 2 0.862445 0.091882 0.482556 21.00000 -1.50000 H16C 2 0.913144 -0.008693 0.527255 21.00000 -1.50000 PART 2 AFIX 0 C18A 1 0.955945 0.090034 0.627652 -21.00000 0.02892 AFIX 137 H18D 2 0.990049 0.019299 0.620356 -21.00000 -1.50000 H18E 2 0.973909 0.122160 0.689825 -21.00000 -1.50000 H18F 2 0.995917 0.140649 0.593666 -21.00000 -1.50000 AFIX 0 C17A 1 0.779700 0.016961 0.500270 -21.00000 0.03882 AFIX 137 H17D 2 0.689320 0.000398 0.474250 -21.00000 -1.50000 H17E 2 0.818412 -0.051725 0.498292 -21.00000 -1.50000 H17F 2 0.822160 0.067189 0.467167 -21.00000 -1.50000 AFIX 0 C15A 1 0.747871 0.000539 0.649989 -21.00000 0.04130 AFIX 137 H15D 2 0.654841 -0.012307 0.636957 -21.00000 -1.50000 H15E 2 0.776138 0.037755 0.710488 -21.00000 -1.50000 H15F 2 0.781657 -0.070359 0.642889 -21.00000 -1.50000 AFIX 0 HKLF 4 REM C:\XRay\TH151_~1\full\P-1_a.res in P-1 REM wR2 = 0.0792, GooF = S = 0.877, Restrained GooF = 0.877 for all data REM R1 = 0.0375 for 5047 Fo > 4sig(Fo) and 0.0684 for all 7853 data REM 474 parameters refined using 0 restraints END WGHT 0.0346 0.0000 REM Highest difference peak 0.352, deepest hole -0.295, 1-sigma level 0.056 Q1 1 0.2931 0.6151 0.6245 11.00000 0.05 0.35 Q2 1 0.4361 0.7050 0.6417 11.00000 0.05 0.35 Q3 1 0.2608 0.6543 0.6813 11.00000 0.05 0.33 Q4 1 0.4294 0.6857 0.6187 11.00000 0.05 0.32 Q5 1 0.3866 0.7465 0.7227 11.00000 0.05 0.32 Q6 1 0.5244 0.3478 0.4131 11.00000 0.05 0.29 Q7 1 0.8184 0.0393 0.4802 11.00000 0.05 0.29 Q8 1 0.2993 0.6972 0.7316 11.00000 0.05 0.28 Q9 1 0.0710 0.7594 0.5816 11.00000 0.05 0.28 Q10 1 0.2800 0.7281 0.6412 11.00000 0.05 0.26 Q11 1 0.7512 0.3880 0.7500 11.00000 0.05 0.26 Q12 1 0.5476 0.7983 0.5932 11.00000 0.05 0.26 Q13 1 0.7768 0.1213 0.5965 11.00000 0.05 0.26 Q14 1 0.7771 0.3723 0.6874 11.00000 0.05 0.26 Q15 1 0.6142 0.4849 0.4896 11.00000 0.05 0.25 Q16 1 0.6489 0.5232 0.6744 11.00000 0.05 0.24 Q17 1 0.4036 0.8944 0.9195 11.00000 0.05 0.23 Q18 1 0.7848 0.7653 0.9074 11.00000 0.05 0.23 Q19 1 0.7192 0.3869 0.8167 11.00000 0.05 0.22 Q20 1 0.6097 0.6988 0.6646 11.00000 0.05 0.22 ; _shelx_res_checksum 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5 13 80.29 21.00 3 -3 6 288.27 18.10 3 -1 10 1116.29 38.40 4 -4 6 12.90 8.60 5 -3 10 42.00 17.70 6 -6 4 95.19 12.40 7 -3 12 39.80 24.10 7 -1 14 97.69 31.00 8 -7 4 0.50 12.90 10 -8 2 89.59 18.50 10 -6 9 81.19 27.00 -2 5 -3 151.88 10.90 -1 5 7 143.19 11.10 0 2 7 30.60 7.50 0 6 10 -0.90 12.30 0 11 10 -0.60 14.00 1 8 12 90.99 20.10 1 9 12 107.99 20.60 2 3 12 75.99 18.00 3 0 11 12.00 13.60 3 1 12 -2.20 14.40 3 5 14 91.89 25.70 4 -2 10 146.09 19.40 5 -5 5 10.60 10.50 5 -4 8 -6.70 10.50 5 1 14 -7.50 22.20 6 -3 11 52.79 20.80 6 0 14 22.20 23.00 7 -6 6 33.60 14.80 7 -2 13 -8.50 20.00 -2 10 5 31.10 6.90 -1 7 8 0.50 8.40 0 1 -6 744.13 21.50 0 1 5 221.08 11.00 0 3 8 18.20 9.50 1 -1 4 -4.20 5.40 2 0 9 -3.00 12.10 2 6 13 377.06 29.80 3 -2 8 263.77 18.10 3 3 13 96.19 22.30 3 6 14 85.29 23.60 4 -3 8 -7.70 12.30 4 -1 11 -6.90 17.30 4 3 14 45.50 22.40 5 -2 11 141.69 23.20 5 0 13 111.19 25.50 6 -6 3 9.10 9.60 6 -5 7 86.59 16.20 6 -1 13 8.90 22.80 8 -6 7 348.17 26.70 8 -4 11 9.50 19.50 9 -7 5 42.90 19.40 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39.60 24.60 10 -8 -2 2.50 10.60 10 -8 -1 2.60 11.50 -1 2 -3 387.36 12.20 0 0 -2 1776.82 17.30 0 5 9 167.28 14.70 3 0 10 17.50 15.20 3 1 11 22.90 16.30 4 -2 9 4.10 12.80 4 5 14 39.80 24.10 5 -4 -10 162.08 15.20 5 1 13 29.60 21.70 6 -5 6 46.50 13.00 6 -3 10 7.10 15.20 6 0 13 -14.50 23.00 7 -2 12 -1.90 20.10 8 -7 2 54.49 12.90 8 -6 6 6.10 15.20 8 -4 10 130.99 26.30 9 -7 4 408.76 25.70 9 -6 7 7.20 19.80 10 -7 5 13.30 19.00 11 -8 1 5.50 15.60 -3 10 -2 278.87 16.50 -3 11 -2 257.47 17.60 -2 5 -5 878.91 26.60 -1 6 7 43.80 8.50 -1 12 7 197.88 16.00 0 1 -7 207.68 14.10 0 2 6 574.64 18.90 0 12 9 11.60 16.50 1 6 11 4.60 13.90 1 10 11 59.19 19.70 2 3 11 69.79 16.80 2 5 12 22.10 16.50 3 -2 7 124.99 13.10 3 5 13 5.70 18.90 4 -3 7 25.40 10.20 4 1 12 1.20 18.40 5 -2 10 51.39 18.80 5 3 14 5.30 19.50 6 -4 8 131.09 19.80 6 -2 11 -7.00 20.90 6 -1 12 106.89 26.70 7 -4 9 4.20 17.80 -3 10 -3 36.60 13.40 -3 10 -1 125.09 11.50 -3 11 -1 109.19 11.80 -2 7 4 205.38 7.00 1 -1 3 1047.40 19.00 1 7 11 610.04 29.00 2 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14.60 22.30 7 -3 10 46.80 18.80 7 -1 12 -0.60 23.10 8 -7 -5 9.60 4.90 8 -6 5 103.49 17.10 9 -6 6 38.20 19.80 9 -3 11 92.79 23.70 11 -8 -1 0.40 13.20 11 -6 7 -5.30 22.80 -3 10 0 2.30 6.80 -2 6 3 344.07 6.40 -1 2 -5 47.60 8.50 -1 7 7 0.00 6.70 1 2 8 658.43 24.50 1 5 10 170.08 17.50 2 -1 6 171.98 13.00 3 -3 -8 23.90 9.40 3 -1 8 3.90 9.30 3 2 11 91.99 19.30 4 -2 8 24.50 13.60 4 2 12 20.90 20.20 6 -6 0 727.93 18.90 6 -5 -10 345.17 17.00 6 -3 9 -2.20 14.90 7 -2 11 107.69 23.00 8 -7 0 72.09 11.50 8 -4 9 51.99 21.50 11 -8 -2 21.70 14.10 11 -7 4 18.40 20.20 -3 11 0 620.24 16.50 -2 4 -2 2134.19 27.80 0 0 -4 1939.01 26.00 0 10 9 174.08 18.80 1 0 5 13.40 7.60 3 0 9 90.39 16.20 3 1 10 880.41 34.90 4 -4 -8 8.20 7.20 4 -3 6 38.00 11.80 5 1 12 32.00 21.80 6 -4 7 71.79 15.90 6 -2 10 43.60 19.10 6 0 12 120.19 23.90 7 -6 3 -6.70 9.10 7 -4 8 145.49 22.00 9 -7 2 287.97 21.30 10 -6 6 18.10 20.30 10 -5 8 102.89 25.40 11 -8 -3 0.40 12.70 -3 8 -4 98.59 15.30 -3 8 -3 470.25 21.00 -2 4 -3 633.64 18.10 0 8 9 427.96 22.20 0 9 9 49.10 15.00 1 -1 -7 1218.58 27.30 3 -2 6 199.88 14.50 4 -4 3 109.89 10.30 4 -1 9 55.69 16.60 4 1 11 18.60 17.00 5 -2 9 9.20 13.50 5 0 11 -0.30 18.00 5 3 13 0.90 18.20 6 -1 11 32.00 18.90 6 2 13 34.70 23.20 7 1 13 29.90 24.80 8 -7 -1 297.87 15.60 8 -3 10 20.80 18.90 8 -2 11 27.90 23.10 8 -1 12 79.39 23.30 9 -4 9 115.79 26.50 10 -7 3 49.50 17.30 -3 12 0 543.25 16.20 -2 4 -4 1446.76 29.20 -2 4 -1 43.00 5.00 -1 2 -6 166.98 12.90 1 6 10 66.99 14.80 1 11 10 89.89 18.90 2 -2 3 72.09 8.40 2 3 10 430.66 25.30 4 0 10 410.76 26.30 4 3 12 43.10 19.20 4 6 13 3.20 23.80 5 -1 10 38.50 16.00 6 -6 -1 9.00 5.70 7 -6 -9 -0.80 7.80 8 -6 4 285.97 21.20 9 -6 5 8.90 15.80 11 -6 6 12.50 21.60 -3 8 -1 17.10 6.60 -2 4 -5 126.89 12.10 0 0 -5 195.48 10.40 2 0 7 510.65 21.40 3 -3 3 853.51 21.40 3 3 11 126.19 19.90 5 -4 5 181.38 14.80 5 -3 7 22.70 12.90 5 4 13 -9.00 21.50 6 -6 -4 568.04 8.50 7 -3 9 2.10 14.90 8 -7 -2 152.28 11.40 9 -7 1 184.58 17.40 9 -5 7 190.08 24.90 9 -3 10 3.20 19.60 11 -7 3 10.50 18.00 0 2 5 530.55 16.30 1 -1 2 5091.89 35.10 1 7 10 -2.90 12.10 1 10 10 18.30 16.70 2 2 9 663.63 26.70 2 6 11 73.69 16.60 3 -3 -9 3.60 10.00 5 2 12 3.90 17.10 6 -6 -2 3.90 4.90 6 -3 8 40.80 14.20 6 1 12 8.50 18.50 6 3 13 20.70 22.50 7 -6 2 743.93 25.20 7 -2 10 -6.30 20.90 7 -1 11 42.80 20.50 7 2 13 0.80 23.80 8 -7 -4 1.60 6.40 8 -7 -3 5.70 7.70 8 -4 8 -3.90 16.10 10 -7 2 86.39 17.90 10 -6 5 10.20 20.50 0 0 -6 614.54 19.40 0 4 7 268.97 14.80 0 12 8 180.78 19.40 1 -1 -8 803.22 24.30 1 1 6 397.36 17.40 1 8 10 388.96 23.70 1 9 10 32.10 17.20 2 -1 5 36.70 9.30 2 7 11 134.99 21.00 2 10 11 7.50 18.00 3 -1 7 12.80 9.30 3 2 10 503.25 28.00 3 7 12 143.29 24.00 3 8 12 59.29 22.70 4 -2 7 86.59 13.00 4 2 11 26.60 17.80 4 4 12 14.50 20.80 5 -5 -8 376.46 13.70 6 -6 -3 416.46 9.70 6 -4 6 171.68 18.20 6 0 11 44.10 21.50 7 -4 7 124.89 19.50 8 0 12 9.60 20.60 10 -5 7 66.99 23.70 11 -5 7 39.60 23.20 -3 7 -4 864.01 26.50 -3 7 -3 32.90 10.40 -2 8 4 17.00 4.80 0 3 6 1496.65 28.60 0 6 8 31.90 9.10 1 3 8 0.30 7.80 2 4 10 23.10 14.00 2 8 11 98.99 20.50 2 9 11 9.70 18.30 3 4 11 6.70 15.80 4 -4 -9 396.66 18.40 4 -3 5 920.01 27.50 5 -2 8 24.90 15.00 5 1 11 10.30 19.30 6 -2 9 10.00 14.40 6 -1 10 5.00 17.90 6 4 13 15.30 22.40 8 -6 3 39.80 13.50 8 -3 9 28.40 17.90 8 -2 10 31.90 23.10 8 -1 11 81.29 26.60 9 -6 4 6.40 13.90 11 -7 2 -4.70 16.80 11 -6 5 6.20 19.30 -3 7 -2 228.18 12.40 0 1 3 1863.71 22.00 3 -2 5 2139.49 38.30 3 0 8 415.46 22.00 3 1 9 193.08 17.30 4 -1 8 6.60 12.90 4 1 10 51.69 17.90 5 -1 9 -0.10 15.90 5 0 10 540.55 31.80 5 3 12 2.30 19.50 6 -5 -11 96.39 14.30 6 2 12 -2.50 21.40 7 1 12 50.39 22.30 9 -7 0 231.88 17.20 9 -5 6 74.89 19.80 9 -1 11 93.69 26.70 12 -7 2 15.40 18.30 -3 8 0 33.40 6.30 -2 4 0 133.99 5.40 0 0 -7 641.14 21.80 0 11 8 173.18 17.70 4 0 9 214.08 21.80 5 -4 4 0.20 9.90 7 -6 1 382.46 17.60 7 -3 8 27.30 17.20 7 0 11 -3.70 22.20 8 1 12 106.99 28.10 9 -3 9 52.89 21.00 10 -7 1 111.49 16.90 -3 10 1 311.17 8.80 -3 11 1 550.54 11.10 -2 11 4 48.10 6.70 -1 12 6 169.18 14.30 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58.79 18.50 -2 9 4 117.49 7.40 1 7 9 18.80 13.30 2 6 10 13.00 13.60 3 -1 6 346.07 17.90 3 9 11 12.80 21.30 4 -3 4 643.34 22.50 4 2 10 4.80 16.00 4 4 11 7.30 18.30 5 -2 7 46.40 14.20 6 -1 9 56.99 18.80 7 1 11 58.79 24.90 7 3 12 38.10 24.30 8 -2 9 94.49 22.90 8 -1 10 -0.10 18.80 9 -5 5 18.10 16.70 9 0 11 90.29 23.60 -2 3 -5 2519.05 40.70 1 10 9 14.30 14.70 2 -1 4 416.66 16.00 2 7 10 0.20 13.50 2 10 10 13.20 19.40 3 2 9 538.75 25.40 3 8 11 81.19 21.40 5 3 11 79.29 21.50 5 6 12 -13.30 23.70 6 4 12 29.20 20.30 7 -6 0 92.99 10.50 9 -7 -2 4.60 10.20 9 -3 8 109.49 25.00 9 -2 9 -10.00 21.60 9 -1 10 3.60 22.00 10 -6 3 9.90 14.80 11 -7 0 11.00 16.20 11 -4 7 -2.00 19.90 -3 9 1 221.88 7.30 -2 3 -3 271.57 11.80 -1 1 -5 1284.47 27.00 -1 1 -4 1.20 5.10 1 1 5 1529.75 28.60 1 3 7 50.89 10.60 1 8 9 49.99 12.80 2 4 9 246.98 19.20 2 8 10 89.79 17.30 2 9 10 -0.30 17.50 3 -2 4 1995.20 34.70 3 0 7 97.69 14.00 3 1 8 104.79 15.50 3 4 10 82.89 13.80 4 1 9 250.17 22.60 5 -4 3 17.00 8.70 5 -1 8 -3.10 12.20 6 2 11 3.90 18.70 7 -3 7 356.86 24.40 7 0 10 178.18 27.50 8 -5 4 46.00 13.80 8 1 11 133.59 28.30 10 -5 5 9.80 19.30 10 -3 8 -9.60 18.90 10 -2 9 4.50 22.60 11 -6 3 18.10 17.60 12 -7 0 13.10 17.00 12 -6 3 95.79 23.10 -3 6 -2 10.50 6.30 -3 12 1 10.30 4.90 -1 1 -6 525.95 19.20 -1 1 -3 1043.40 19.00 0 4 6 13.10 7.00 5 -3 5 219.18 17.20 6 -3 6 250.37 20.20 7 -5 3 17.20 11.00 7 -2 8 134.49 21.10 7 -1 9 1.60 17.90 7 4 12 31.20 21.10 9 -6 2 21.20 13.20 9 1 11 12.80 27.30 10 -7 -1 8.70 13.50 11 -5 5 5.40 21.00 0 6 7 -2.10 7.90 1 2 6 96.89 9.80 4 3 10 113.09 20.20 4 6 11 -1.50 19.80 5 4 11 12.70 20.50 6 -6 -7 185.58 6.90 6 -4 4 302.47 18.60 6 1 10 94.59 22.90 7 -4 5 109.99 16.30 7 2 11 15.10 22.50 8 -6 1 944.91 27.80 8 0 10 67.19 25.90 0 3 5 3531.35 39.60 0 12 7 11.60 13.40 1 -2 -5 496.95 14.60 1 -1 1 16.40 3.30 2 3 8 193.48 16.90 3 -4 -5 450.95 10.40 3 3 9 235.18 20.50 4 7 11 11.60 22.50 4 8 11 1.20 21.30 5 -5 -10 31.10 9.80 5 -5 -1 148.99 8.40 5 2 10 39.00 18.50 6 3 11 80.19 20.90 8 -3 7 110.29 18.40 8 -1 9 54.69 23.10 8 2 11 46.00 23.90 9 -7 -3 37.60 9.50 9 -5 4 60.19 16.10 9 0 10 42.00 25.70 10 -4 6 52.39 21.40 11 -7 -1 5.50 14.80 11 -4 6 -7.10 22.80 -2 3 -2 2784.32 30.60 1 -2 -6 5318.57 49.10 1 -2 -4 2551.54 26.50 1 12 8 38.40 17.20 3 -4 -6 3.20 4.90 4 -2 5 203.48 15.70 5 5 11 -0.50 20.60 6 -2 7 11.50 12.70 6 0 9 43.60 16.50 7 -6 -1 -0.60 7.30 8 -2 8 2.20 17.00 9 -3 7 11.40 18.80 10 -6 2 35.60 14.60 12 -7 -1 3.70 16.50 12 -6 2 16.20 20.10 -3 5 -5 1352.86 33.30 -3 7 0 5.80 4.50 -1 1 -2 5127.39 34.90 0 7 7 441.26 19.60 1 -2 -7 1360.66 28.60 2 -3 -3 16.40 2.50 2 0 5 121.39 10.60 3 -3 1 114.69 7.90 3 6 10 31.90 15.60 3 10 10 -4.20 20.50 4 2 9 40.30 16.40 4 4 10 46.40 17.60 5 -2 6 47.60 13.20 5 1 9 702.13 33.90 6 -5 1 66.39 9.60 6 4 11 95.59 24.00 7 1 10 21.30 19.30 7 3 11 -8.10 20.30 9 -2 8 69.49 23.90 9 -1 9 15.40 19.50 10 -7 -2 -2.30 12.20 10 -5 4 27.00 18.40 10 -2 8 32.00 22.40 10 -1 9 5.30 22.70 11 -6 2 -0.80 17.50 11 -5 4 31.60 21.00 12 -5 4 45.00 23.20 -3 5 -4 539.35 20.20 0 11 7 -2.60 12.70 1 6 8 59.59 11.80 2 -3 -8 45.10 10.40 2 1 6 1100.99 28.80 2 2 7 470.75 20.50 2 6 9 210.18 19.40 2 11 9 -0.30 18.60 3 -4 -7 13.50 5.70 3 -1 5 93.19 11.00 3 2 8 188.38 18.10 3 7 10 20.20 16.10 3 8 10 6.20 20.30 4 -3 3 23.80 7.00 5 0 8 -9.10 15.00 5 3 10 85.19 20.20 6 -6 -8 331.37 10.70 6 2 10 309.37 29.90 7 -3 6 88.69 15.80 8 -5 3 183.28 17.00 8 1 10 15.00 24.30 8 3 11 3.70 23.80 9 -6 1 64.09 14.00 -3 6 -1 1353.36 22.50 0 8 7 2.70 9.60 1 4 7 71.09 10.90 1 11 8 8.10 15.10 3 4 9 -5.90 12.70 4 -1 6 85.39 13.60 4 1 8 12.40 13.60 5 -5 -11 277.47 18.90 5 -4 2 234.58 13.50 5 -1 7 50.09 12.50 6 5 11 46.10 22.60 7 -5 2 83.69 12.10 7 -2 7 -7.90 16.60 7 -1 8 102.89 21.30 7 0 9 167.78 23.70 7 4 11 62.29 25.60 8 -6 0 101.89 12.50 9 -7 -4 9.90 8.10 9 1 10 0.80 23.40 11 -7 -2 -5.00 13.30 0 9 7 445.06 20.30 1 -2 -3 872.61 12.60 1 7 8 29.30 11.90 2 -2 1 2414.16 24.10 2 4 8 2.70 10.60 2 7 9 41.30 14.40 2 10 9 6.80 17.30 3 -4 -8 47.10 8.80 3 1 7 642.94 25.90 4 -4 0 4.90 5.00 4 0 7 107.99 16.40 5 -3 4 82.39 11.90 6 -3 5 120.29 14.10 7 2 10 159.48 26.60 8 -3 6 146.29 20.70 8 0 9 44.00 24.60 10 -6 1 355.36 24.40 12 -7 -2 4.00 14.60 12 -4 5 6.80 22.40 -4 10 -3 61.79 14.60 -4 12 -3 34.10 15.90 0 -1 -7 15.80 9.10 0 -1 -5 210.88 11.10 1 8 8 87.59 15.20 1 10 8 75.29 16.80 2 8 9 3.20 13.10 2 9 9 46.00 18.00 4 3 9 32.80 16.30 5 4 10 60.99 21.00 6 -4 3 165.38 14.30 6 1 9 221.38 23.80 7 5 11 7.20 19.40 8 -1 8 149.79 25.30 8 2 10 60.49 24.90 9 -5 3 11.30 13.60 9 0 9 19.00 22.50 10 -7 -3 38.30 11.70 10 -4 5 7.00 15.60 10 0 9 -3.70 22.60 11 -6 1 122.69 20.90 11 -4 5 6.00 19.00 12 -6 1 53.29 19.80 -1 12 5 -2.20 10.80 1 3 6 484.15 19.10 2 -1 3 3.20 5.30 5 2 9 360.36 25.60 6 -2 6 53.89 14.80 6 0 8 151.78 21.10 7 -6 -2 410.06 14.40 8 -2 7 163.98 21.00 9 -7 -5 103.69 9.90 9 -3 6 39.10 19.80 9 -1 8 0.00 20.80 9 2 10 3.70 23.60 10 -5 3 2.80 14.50 10 -1 8 8.00 22.40 11 -5 3 37.70 19.60 12 -5 3 1.90 19.40 -3 8 1 685.03 9.60 -2 2 -6 162.18 12.80 -2 2 -5 1004.10 25.90 -2 3 -1 1126.99 16.70 -2 7 3 1277.07 13.80 0 -1 -4 362.06 12.00 3 -4 -9 1.70 10.90 4 7 10 30.20 19.20 4 8 10 5.60 21.90 4 9 10 -0.50 21.90 5 5 10 1.60 19.50 6 -6 -9 1097.29 20.10 6 -1 7 104.99 19.20 7 1 9 76.39 23.60 7 3 10 72.29 24.30 9 -6 0 7.90 11.70 9 -2 7 80.49 21.10 10 -2 7 3.80 20.90 11 -7 -3 15.20 12.80 11 -2 7 21.30 18.90 12 -7 -3 114.39 18.10 -4 9 -3 3.60 11.40 1 1 4 726.93 18.10 1 2 5 477.25 17.10 2 3 7 270.07 17.80 3 3 8 590.04 25.40 4 -2 4 100.59 12.20 5 -5 -2 483.15 11.40 5 1 8 -4.00 15.50 6 -5 0 878.81 21.90 6 4 10 237.78 28.50 7 -3 5 10.90 12.70 8 -6 -1 90.09 11.60 8 -5 2 3.90 10.20 8 1 9 168.78 28.30 8 3 10 129.19 27.40 -4 11 -2 30.80 10.80 -3 4 -5 186.18 15.00 -2 2 -4 1415.86 27.80 3 -4 -10 633.84 24.60 4 2 8 43.70 12.50 4 4 9 86.09 18.70 6 2 9 460.25 31.10 7 -5 1 153.68 13.70 7 0 8 -0.50 17.30 10 -7 -4 106.99 14.10 10 -6 0 105.59 17.00 10 1 9 8.60 20.70 12 -6 0 24.90 17.80 12 -4 4 33.30 23.50 -4 10 -2 232.78 14.70 0 4 5 2792.22 35.90 0 6 6 302.67 15.10 3 7 9 23.50 15.40 3 10 9 48.20 20.80 4 -3 2 3.20 7.20 5 -1 6 3.90 9.60 5 0 7 23.90 11.20 5 3 9 -5.80 14.30 5 7 10 10.40 23.30 5 8 10 -8.90 22.20 6 5 10 55.89 21.70 7 -2 6 402.86 25.20 7 -1 7 184.88 22.40 7 4 10 16.40 19.90 8 -3 5 29.90 15.70 8 0 8 43.30 22.40 8 4 10 14.80 22.70 9 -7 -6 6.80 6.90 9 -5 2 68.49 16.30 10 -4 4 -19.00 19.20 11 -6 0 108.59 19.70 11 -4 4 31.70 21.60 12 -5 2 46.10 22.30 12 -3 5 -1.70 23.80 -4 8 -3 137.89 14.50 -3 4 -4 1439.06 31.30 -1 0 -7 178.58 13.30 -1 0 -6 4.10 6.30 0 12 6 21.10 13.00 1 12 7 39.70 17.20 2 2 6 969.90 27.40 3 -1 4 954.40 24.80 3 2 7 -3.10 8.80 3 8 9 35.20 17.00 3 9 9 -0.10 18.10 6 -6 -10 693.43 19.40 6 -3 4 31.90 10.60 7 2 9 70.69 20.40 7 5 10 68.79 24.50 9 0 8 -8.10 21.50 10 -5 2 -4.20 15.60 10 0 8 8.30 19.40 11 -7 -4 3.70 12.20 11 -5 2 20.90 20.60 11 -3 5 2.10 21.00 11 -1 7 5.40 22.10 12 -7 -4 -3.70 15.90 -4 9 -2 129.19 12.60 -1 0 -5 8.00 7.30 0 -1 -3 1861.61 21.70 2 11 8 9.70 18.20 3 4 8 377.56 22.70 4 -5 -8 368.96 13.80 4 -5 -6 99.09 6.10 4 -1 5 145.59 13.30 4 0 6 2.00 11.30 4 5 9 -7.10 14.90 5 -3 3 50.79 10.50 6 1 8 12.10 14.30 6 3 9 377.86 30.00 8 -2 6 516.45 30.20 8 -1 7 12.20 16.70 8 2 9 13.10 20.20 8 5 10 9.80 23.70 9 -3 5 108.89 20.80 9 -1 7 9.60 20.70 9 2 9 75.09 26.00 10 -1 7 16.60 23.00 -4 7 -4 759.82 26.30 -2 2 -3 70.49 7.20 -1 1 -1 15.80 2.90 0 3 4 356.86 12.50 2 1 5 69.89 9.10 2 7 8 -2.90 12.20 2 10 8 3.80 17.80 3 1 6 148.19 13.80 4 -5 -9 478.05 17.90 4 3 8 17.50 14.70 5 2 8 -4.20 15.60 5 4 9 249.58 24.20 7 -6 -3 307.47 11.60 7 6 10 -19.00 20.10 9 -7 -7 7.70 6.40 9 -6 -1 270.77 17.10 9 -2 6 28.70 17.60 10 -7 -5 54.29 11.30 10 -2 6 38.50 19.10 -3 4 -3 1512.15 29.50 0 7 6 32.10 8.70 1 11 7 83.59 17.00 2 4 7 120.59 13.80 2 8 8 23.80 13.20 2 9 8 -6.50 16.20 3 -3 0 136.29 6.90 4 10 9 6.30 20.30 6 -1 6 93.49 16.40 6 0 7 35.70 14.10 7 1 8 1.50 15.40 7 3 9 293.47 31.00 8 -5 1 193.58 16.10 10 1 8 4.10 22.60 12 -6 -1 15.60 17.60 12 -4 3 38.70 22.50 -1 0 -4 1175.68 23.40 0 11 6 38.60 12.60 1 7 7 69.99 12.20 3 5 8 54.29 14.20 4 -5 -10 57.29 12.50 4 7 9 306.97 27.20 4 8 9 21.00 20.30 4 9 9 32.70 21.50 5 5 9 82.49 22.90 6 -6 -11 4.30 10.40 6 4 9 49.50 22.80 7 -3 4 124.19 14.80 8 -6 -2 207.78 13.10 8 1 8 44.80 20.30 8 3 9 180.98 26.70 9 -4 3 7.10 13.90 9 1 8 111.49 26.00 9 3 9 -11.70 20.00 10 -6 -1 43.70 14.40 11 -7 -5 54.29 13.50 11 -6 -1 30.50 16.10 11 -4 3 34.20 21.70 12 -5 1 158.88 25.60 12 -3 4 -1.70 23.00 -4 7 -3 72.69 11.70 -3 6 0 422.36 10.40 -2 12 3 14.20 6.50 0 8 6 24.80 9.60 1 8 7 158.18 16.00 1 9 7 -4.60 11.30 1 10 7 97.59 16.80 3 -2 2 1271.97 23.90 5 -2 4 705.83 25.20 5 1 7 67.59 15.90 6 -5 -1 619.64 17.60 6 2 8 257.47 24.70 7 -5 0 522.45 19.80 7 0 7 110.19 18.90 9 -5 1 34.50 13.60 10 -4 3 9.10 16.40 11 0 7 73.19 22.80 -4 8 -2 17.40 9.10 0 9 6 2.40 9.10 3 3 7 426.16 21.20 3 11 8 117.69 23.40 4 2 7 401.86 23.30 4 4 8 54.39 16.30 5 3 8 140.39 20.80 6 5 9 196.98 26.50 7 -2 5 352.16 22.50 7 -1 6 10.40 14.00 7 4 9 -2.50 18.90 8 -3 4 220.78 20.90 8 0 7 9.30 19.50 8 4 9 116.39 26.70 9 0 7 13.80 21.10 9 4 9 22.10 22.70 10 -7 -6 21.70 9.90 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11.60 12.40 1 -4 -8 732.43 25.10 1 2 3 4.40 4.70 1 10 5 21.00 12.70 3 8 6 47.60 16.50 4 1 4 294.47 18.20 5 5 6 32.00 17.30 5 11 6 -0.80 23.80 6 -5 -3 255.87 10.50 6 -1 3 1854.81 40.90 7 -1 3 195.18 18.30 8 -6 -5 10.10 8.20 8 -1 3 18.00 15.40 8 2 5 3.80 15.30 8 5 6 78.39 21.70 10 1 4 25.40 20.40 11 -5 -3 14.50 14.10 11 0 3 19.70 19.30 11 2 4 38.90 24.50 12 1 3 72.29 26.00 13 -2 0 6.10 22.40 -5 7 -3 -0.90 12.30 -5 11 -2 88.79 11.70 -4 9 0 294.77 9.60 -4 11 0 311.67 8.40 -2 1 -2 2916.81 31.90 1 8 5 444.96 20.70 1 9 5 242.98 17.60 2 5 5 276.97 16.70 2 12 5 -3.80 18.10 4 -6 -11 344.37 20.00 4 10 6 12.80 20.20 6 5 6 252.57 24.60 7 -2 2 247.88 17.10 7 2 5 170.58 20.70 7 5 6 46.00 18.70 8 -2 2 338.17 21.20 8 6 6 42.10 22.90 8 7 6 22.80 23.10 8 8 6 34.50 25.30 9 -6 -5 18.00 9.70 9 3 5 72.59 24.50 10 -4 -1 109.89 16.20 10 4 5 143.59 28.40 11 -3 0 16.00 18.10 12 -4 -2 3.50 18.50 1 4 4 1061.69 24.00 2 0 2 8.70 5.20 4 -6 -10 56.79 10.80 4 8 6 11.00 15.20 4 9 6 60.69 18.50 5 10 6 84.69 25.70 6 10 6 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10 -8 3 35.70 24.80 11 -6 6 26.10 27.10 11 -5 7 15.10 27.40 -2 4 -5 112.09 14.70 -2 6 -3 603.64 23.80 -2 8 -3 404.26 22.00 -1 11 -1 286.37 18.90 3 -6 -4 300.77 7.50 3 0 6 139.69 15.10 4 -5 2 322.97 18.60 5 5 9 82.19 19.80 6 1 9 234.28 25.80 6 8 9 28.70 23.00 7 -9 -3 32.20 13.30 8 -6 5 91.59 22.70 8 -3 8 110.29 27.00 9 1 10 3.10 26.80 10 -6 6 17.00 26.50 10 -5 7 65.39 30.80 10 -2 9 7.10 24.40 -2 5 -4 784.82 27.10 -1 1 -3 1041.60 20.80 1 7 5 271.17 11.00 3 2 7 9.80 10.10 4 -7 -8 1225.28 13.30 4 -7 -4 6.00 5.60 4 2 8 60.29 14.60 5 -6 2 14.80 9.80 5 -4 5 190.68 18.60 5 -3 6 0.50 11.20 5 0 8 2.90 12.00 5 6 9 0.80 19.30 6 -4 6 133.19 20.10 7 3 10 104.39 25.40 7 4 10 6.40 25.10 7 5 10 67.49 26.70 8 -8 2 83.99 19.60 8 1 10 14.10 25.20 9 -10 -3 -0.60 17.30 9 -2 9 -6.20 22.90 10 -7 5 -6.40 24.60 10 -4 8 -10.70 28.70 11 -9 2 -17.50 27.30 0 10 2 498.05 12.40 3 -6 -8 298.07 10.30 3 -5 0 469.65 16.60 3 -4 2 228.78 13.60 4 -3 5 899.31 30.70 4 -2 6 55.39 14.70 4 8 8 181.88 20.20 5 -8 -5 -1.90 7.30 5 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9 58.59 28.10 9 -1 10 -19.00 27.70 10 -8 4 16.90 24.50 11 -6 7 -1.60 27.50 -1 1 -4 1.00 6.10 1 0 3 17.30 5.30 2 0 5 109.89 12.40 3 -2 5 2175.98 43.30 3 1 7 632.24 25.90 4 -1 7 12.00 11.20 5 -1 8 8.70 12.50 6 3 10 10.50 19.40 6 5 10 72.69 24.40 8 -6 6 -2.90 22.50 8 -4 8 2.90 24.20 10 -6 7 6.50 26.20 11 -9 3 1.00 26.90 11 -7 6 6.00 27.00 -1 4 0 2.40 4.00 -1 10 -1 60.39 13.60 2 9 6 212.88 13.20 3 -6 -7 3.40 4.70 4 -7 -3 80.49 8.30 4 9 8 44.20 16.10 5 -8 -4 187.78 11.30 5 1 9 689.53 32.30 5 8 9 43.40 19.60 6 -8 0 52.59 13.70 6 -1 9 76.29 20.90 6 6 10 15.40 21.50 7 0 10 181.98 29.90 8 -10 -4 20.20 14.60 8 -8 3 -0.90 18.00 8 -1 10 -10.00 25.90 8 3 11 10.60 26.70 10 -10 0 3.30 22.90 10 -7 6 4.40 25.00 10 -5 8 68.09 27.00 10 -2 10 4.80 23.60 -1 1 -7 39.60 10.20 -1 1 -6 530.45 21.20 -1 1 -5 1312.17 28.90 -1 2 -2 9.90 5.30 1 -3 -9 73.49 13.30 1 -1 2 5137.19 39.00 2 11 5 7.90 6.80 3 -1 6 326.37 18.70 3 4 8 389.86 21.60 3 5 8 61.79 13.30 4 -5 3 90.69 13.60 5 -6 3 8.10 12.70 6 -4 7 67.49 21.00 6 7 10 13.70 23.70 7 -9 -1 46.60 15.40 7 -8 2 43.50 17.00 7 -7 4 208.48 24.80 8 -9 1 59.19 20.60 8 -7 5 17.40 19.80 8 -3 9 26.80 23.20 8 2 11 25.00 27.70 9 -10 -1 7.80 20.50 9 -9 2 67.99 24.00 9 -6 7 17.20 25.50 9 -5 8 122.09 30.70 9 -2 10 115.89 29.90 10 -9 3 128.99 29.20 10 -4 9 8.30 25.60 0 12 0 454.85 20.90 1 3 5 1686.03 27.20 1 8 5 464.75 12.30 2 -4 -11 170.98 18.20 3 -5 -12 76.39 16.20 3 6 8 8.30 11.00 4 -6 1 10.60 9.10 4 0 8 193.78 19.70 4 4 9 71.79 15.20 4 5 9 -3.70 12.70 5 -4 6 324.07 23.20 5 -3 7 16.60 12.50 6 -5 6 37.10 17.00 6 -3 8 51.79 21.10 6 1 10 93.69 22.00 7 -5 7 18.80 20.80 8 -10 -3 61.19 17.60 9 -4 9 159.58 31.40 9 0 11 95.19 29.50 -1 8 0 5.70 7.20 2 1 6 1120.59 29.00 2 5 7 23.00 9.40 3 -6 -3 826.82 14.40 4 -3 6 37.20 14.20 4 6 9 40.90 13.60 5 -8 -3 -6.40 8.10 5 -5 5 3.00 14.10 5 -2 8 27.90 18.30 5 0 9 127.99 18.70 7 -6 6 26.00 20.40 7 -4 8 143.09 24.40 7 -1 10 149.88 28.60 7 3 11 10.70 25.00 7 4 11 111.79 28.30 7 5 11 -5.30 25.70 9 -7 6 32.30 22.50 10 -10 1 14.30 24.70 10 -3 10 8.00 26.80 -1 3 -1 375.66 11.00 1 -3 -8 52.99 9.00 2 -4 0 132.19 8.60 3 -5 1 26.60 8.20 3 0 7 99.59 12.70 3 7 8 -2.50 11.50 4 -4 5 635.24 27.50 4 -2 7 78.29 16.90 5 3 10 84.09 19.50 5 4 10 70.19 18.90 5 5 10 12.20 16.90 5 9 9 91.69 18.70 6 -6 5 29.10 15.60 6 -2 9 0.20 19.00 6 0 10 -6.20 19.10 7 -3 9 15.60 22.80 7 2 11 13.90 24.20 8 -6 7 362.76 34.00 8 -5 8 -0.80 23.50 8 0 11 28.00 24.60 9 -10 0 64.09 23.10 9 -3 10 -12.00 28.30 9 -1 11 89.79 29.10 10 -6 8 62.79 28.50 3 2 8 200.48 17.70 4 -7 -2 65.79 8.70 5 6 10 9.00 19.90 6 -9 -6 212.98 11.70 6 -9 -5 344.87 15.50 6 -8 1 18.80 12.00 7 -9 0 31.70 15.30 8 -10 -2 14.40 17.50 8 -9 2 326.17 29.50 8 -4 9 60.49 26.60 9 -9 3 243.18 29.10 10 -9 4 75.99 28.00 10 -7 7 26.60 26.50 10 -5 9 9.80 24.20 -1 2 -3 409.46 14.60 -1 7 0 41.20 7.50 -1 9 -1 68.29 12.60 -1 10 -2 8.20 15.00 3 10 7 50.79 12.50 4 -6 -12 9.20 12.10 5 -1 9 -2.00 17.50 6 -9 -4 0.90 9.80 7 -7 5 16.90 18.00 7 -2 10 18.10 23.50 8 -7 6 41.50 23.00 9 -6 8 187.78 32.80 10 -4 10 54.69 32.40 0 -1 -7 22.50 9.10 1 -3 -7 78.49 9.20 2 -4 -10 62.79 13.70 3 -6 -6 23.10 3.10 4 -5 4 118.19 16.40 4 -1 8 -1.70 11.10 4 1 9 244.38 21.80 5 -8 -2 52.79 10.00 5 -6 4 163.68 17.20 5 7 10 6.70 19.80 6 -1 10 4.20 19.40 6 3 11 58.89 23.60 6 4 11 102.99 26.30 6 5 11 43.60 25.10 7 0 11 4.10 23.40 8 -3 10 31.50 23.40 8 -1 11 81.19 25.50 9 -10 1 45.30 23.40 9 -7 7 110.69 29.30 9 -5 9 3.40 22.50 9 -2 11 12.50 26.80 10 -11 -2 45.00 21.90 10 -10 2 17.40 23.50 1 2 5 490.35 16.00 2 -2 4 1427.26 29.80 3 -5 -11 14.50 11.90 3 -3 5 537.45 23.90 3 -2 6 216.28 16.50 3 8 8 6.20 13.00 4 -6 2 72.49 12.00 4 8 9 10.00 15.70 5 -4 7 22.50 15.40 5 1 10 938.41 38.20 6 -9 -7 1.70 5.90 6 -9 -3 35.40 11.80 6 -7 4 120.29 16.70 6 -5 7 79.19 20.00 6 -4 8 106.89 21.20 7 -5 8 54.39 24.40 8 -10 -1 28.90 18.60 8 2 12 -3.50 27.20 9 -4 10 214.58 34.20 -1 2 -6 172.48 13.40 -1 2 -5 47.70 9.90 -1 2 -4 890.21 22.70 0 -1 -6 1101.49 25.30 2 2 7 497.85 20.90 3 -6 -2 36.50 6.20 3 -1 7 13.40 12.60 5 -5 6 876.71 36.10 5 -3 8 2.50 14.50 6 -8 2 254.77 20.40 6 -6 6 162.88 23.30 6 6 11 71.39 24.90 7 -9 1 193.78 19.90 7 -6 7 15.30 18.00 7 -4 9 27.10 20.40 8 -9 3 119.19 22.20 8 -2 11 4.40 25.00 9 -9 4 39.50 24.80 10 -11 -1 11.00 21.50 10 -9 5 -5.10 26.00 10 -6 9 95.99 30.80 0 -1 -5 223.18 10.80 0 -1 -4 360.96 11.40 1 -2 1 2.90 4.60 4 -7 -1 149.79 11.30 4 -3 7 24.60 14.70 4 0 9 232.18 22.10 5 -8 -1 134.19 13.20 5 -2 9 -8.30 18.30 5 0 10 519.55 32.60 5 8 10 9.30 20.10 6 -9 -2 7.20 11.00 7 -3 10 31.60 24.40 7 -1 11 35.40 22.50 8 -10 0 43.00 20.60 8 -6 8 130.29 26.10 8 -5 9 12.30 21.90 9 -3 11 74.19 30.70 10 -10 3 -0.10 24.30 10 -7 8 7.30 24.00 -1 8 -1 279.87 15.20 -1 9 -2 112.59 16.00 0 12 -1 264.87 20.70 3 -5 2 6.30 8.50 3 -4 4 1452.25 35.10 4 -4 6 9.90 13.30 4 -2 8 5.10 14.80 4 4 10 28.90 16.60 6 -2 10 31.50 20.80 7 -7 6 -4.30 18.40 7 2 12 -9.40 25.30 7 3 12 53.39 28.10 7 4 12 20.80 27.00 8 -7 7 -3.40 20.20 8 -4 10 127.99 28.50 8 0 12 6.90 24.90 9 -11 -3 125.79 20.60 9 -10 2 12.30 22.30 9 -6 9 125.69 30.60 10 -11 0 -2.50 22.00 2 -4 -9 33.00 11.50 2 10 6 20.70 7.90 3 4 9 -2.80 12.00 3 5 9 29.60 13.20 4 3 10 117.19 17.90 4 5 10 71.99 16.10 5 -6 5 79.99 16.70 6 -7 5 100.29 21.20 6 0 11 28.90 19.70 7 -9 2 241.98 22.90 9 -7 8 12.90 24.90 9 -5 10 175.18 32.70 1 0 4 1161.98 23.00 1 11 3 35.60 6.30 2 -4 1 50.49 7.50 4 -6 3 31.00 12.10 4 -5 5 745.53 30.20 4 6 10 7.20 16.60 4 9 9 25.80 16.00 5 3 11 80.99 19.50 5 4 11 13.80 18.00 5 5 11 1.20 21.30 6 -9 -1 210.38 17.30 6 -5 8 15.40 20.80 7 -2 11 88.79 24.40 8 -10 1 19.70 19.50 8 -9 4 15.30 21.10 8 -1 12 83.59 29.00 9 -11 -2 -6.30 17.50 9 -9 5 24.60 25.30 9 -4 11 -0.90 27.70 10 -9 6 53.59 29.10 -1 3 -6 1147.79 31.60 -1 3 -3 446.16 16.00 -1 7 -1 154.58 11.30 0 11 0 224.78 16.00 1 -1 3 1056.29 20.50 2 1 7 284.67 16.80 3 6 9 24.80 12.70 4 -7 0 5.50 8.90 4 -6 -11 285.77 16.20 4 -1 9 55.49 17.00 5 -8 0 23.00 9.30 5 -4 8 -9.50 17.80 6 -4 9 58.09 19.60 6 -1 11 40.10 24.90 7 -10 -5 3.50 10.80 7 -10 -4 93.19 14.50 7 -10 -3 514.05 23.90 7 -6 8 -10.30 22.80 7 -5 9 47.30 22.30 7 -4 10 -4.20 24.60 7 0 12 135.89 28.60 9 -10 3 79.69 26.90 9 -8 7 21.40 22.30 10 -11 1 16.20 22.50 10 -10 4 93.19 29.50 -1 3 -5 2005.00 37.80 -1 3 -4 1362.36 29.00 -1 5 -1 49.30 7.60 -1 8 -2 79.89 13.50 0 0 -8 21.70 10.10 1 -3 -4 110.99 5.30 1 -2 -9 239.28 17.00 1 1 5 1517.25 27.80 3 -5 -10 170.38 14.50 3 -3 6 316.57 20.60 3 -2 7 116.19 16.90 4 1 10 58.49 16.60 5 -5 7 306.87 27.00 5 -3 9 7.40 17.90 5 6 11 51.09 21.70 6 -6 7 61.99 17.40 6 -3 10 18.60 17.70 6 2 12 5.90 21.60 6 3 12 80.39 26.80 6 4 12 60.59 24.10 7 -7 7 16.20 19.80 8 -7 8 135.79 28.00 8 -6 9 1.50 22.00 8 -5 10 265.97 33.20 8 -2 12 173.68 32.20 9 -11 -1 114.29 23.00 0 9 2 755.72 14.90 1 3 6 502.45 17.30 2 -2 5 962.30 27.50 2 -1 6 186.28 15.20 2 4 8 0.60 9.60 2 5 8 470.65 20.60 3 7 9 -1.00 13.20 4 -7 -7 48.20 4.40 4 7 10 19.80 16.70 6 -9 0 123.29 14.70 6 5 12 84.99 26.20 7 -10 -6 88.79 10.90 7 -10 -2 63.19 15.70 7 -9 3 37.30 17.90 7 -3 11 6.60 24.40 7 -1 12 2.80 25.60 8 -10 2 85.69 24.40 8 -4 11 -1.70 25.50 9 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3 167.58 27.30 8 -1 13 10.60 26.30 9 -11 1 49.00 23.90 0 11 -1 121.99 18.70 1 2 6 94.99 10.10 2 -4 2 2115.09 33.00 3 0 9 87.69 16.40 4 3 11 1.40 15.10 4 4 11 0.20 14.80 4 8 10 0.40 15.00 5 -8 2 213.18 18.90 5 -5 8 14.70 18.80 5 -4 9 2.00 18.90 5 -1 11 233.58 26.60 6 -6 8 56.29 18.80 7 -7 8 51.49 24.80 7 -4 11 12.40 22.30 8 -7 9 53.59 27.90 8 -6 10 43.50 24.80 8 -5 11 110.89 30.90 -1 5 -4 159.88 14.30 -1 5 -3 830.62 23.90 -1 6 -3 335.47 17.50 1 -2 2 12.30 5.00 2 9 7 3.70 9.10 3 8 9 27.90 13.50 4 -1 10 543.55 30.00 4 5 11 -12.10 15.20 5 -7 5 149.19 19.70 5 -3 10 40.30 20.70 5 2 12 -5.30 21.00 5 3 12 4.20 20.90 5 4 12 10.30 20.60 6 -9 2 36.30 15.40 6 -3 11 43.20 22.20 6 -1 12 125.49 24.00 8 -4 12 11.90 26.40 8 -2 13 -3.00 26.30 9 -11 2 53.39 24.00 9 -10 5 66.79 27.30 9 -7 10 125.19 33.20 9 -6 11 4.00 29.60 -1 6 -4 602.04 24.60 2 -3 -10 124.29 15.90 2 1 8 81.09 13.30 3 -6 1 1314.07 28.80 3 -5 4 499.65 22.90 3 -3 7 16.10 11.00 3 -2 8 248.98 20.90 3 3 10 -1.20 11.60 3 4 10 77.99 15.30 3 5 10 19.70 14.30 5 -6 7 161.08 23.00 5 5 12 7.00 20.70 6 -7 7 23.70 17.90 6 3 13 18.60 23.50 7 -10 1 20.00 14.90 7 -3 12 59.19 24.50 7 -1 13 10.70 24.50 8 -11 -4 72.69 15.00 8 -11 -2 87.59 18.20 8 -8 8 18.50 23.80 9 -8 9 5.90 25.30 1 -1 4 0.00 7.20 1 0 5 9.10 6.50 3 -4 6 604.64 26.90 4 -6 5 20.60 13.90 4 -4 8 173.28 18.50 4 -3 9 39.60 18.20 4 6 11 -4.90 18.00 5 -2 11 138.49 24.50 6 -2 12 65.19 27.40 6 1 13 6.60 22.80 6 2 13 60.39 25.70 6 4 13 21.20 23.40 7 -9 5 81.09 20.00 7 -8 7 11.30 18.80 8 -11 -5 176.78 17.60 8 -11 -1 67.89 18.50 8 -10 4 231.38 28.50 0 0 -5 178.88 11.00 2 -2 6 155.98 13.90 2 -1 7 62.89 11.30 3 -5 -9 328.97 14.30 3 -1 9 490.55 26.40 3 6 10 31.30 15.30 3 10 8 7.30 12.30 4 -6 -10 51.99 10.40 4 -5 7 18.80 14.60 5 0 12 138.39 25.30 5 6 12 2.90 19.90 6 -9 3 36.90 16.40 6 -6 9 -0.10 21.20 6 -5 10 100.19 26.40 7 -6 10 13.90 22.10 8 -11 0 13.80 18.20 8 -6 11 82.79 30.50 9 -11 3 -11.10 23.60 9 -10 6 -7.40 26.30 0 10 0 131.39 13.80 1 1 6 408.96 17.20 1 12 1 158.58 15.80 2 -4 3 679.03 21.30 3 -4 -11 396.86 23.10 3 1 10 907.11 33.80 4 -7 3 63.39 12.80 4 -2 10 128.79 19.50 4 0 11 21.60 14.70 4 9 10 0.80 18.10 5 -7 6 78.59 18.80 5 -5 9 -7.20 18.90 5 -4 10 -4.80 20.00 6 -8 6 11.30 18.20 6 -4 11 34.30 22.40 7 -7 9 10.10 20.80 7 -4 12 4.50 25.10 7 -2 13 16.90 22.40 8 -7 10 20.80 22.20 8 -5 12 -7.30 26.70 0 1 -7 222.58 14.60 2 -4 -7 3.40 6.30 2 -3 5 2452.85 42.90 2 4 9 246.98 17.70 3 -6 2 4.50 8.80 4 7 11 16.10 17.30 5 -1 12 -7.00 22.00 6 -7 8 39.60 20.60 6 -3 12 59.79 25.10 8 -10 5 38.00 24.50 8 -8 9 81.79 27.90 0 0 -4 2013.10 27.20 1 4 7 64.69 8.90 1 5 7 210.68 12.40 2 5 9 0.20 10.20 3 -5 5 1232.08 35.20 3 0 10 -1.10 13.90 4 -6 6 225.28 21.00 4 -1 11 8.60 17.40 5 -6 8 313.67 26.00 5 -3 11 27.20 19.70 6 -1 13 2.60 20.00 7 -10 3 74.29 19.00 7 -8 8 33.20 22.40 7 -3 13 6.40 24.80 8 -4 13 15.10 22.70 9 -11 4 14.80 22.40 3 -3 8 30.50 12.20 3 -2 9 85.19 16.40 3 7 10 1.30 13.30 4 -4 9 45.30 18.80 4 2 12 43.80 18.10 4 3 12 3.10 16.60 4 4 12 1.50 19.80 5 2 13 -1.80 21.40 5 3 13 2.20 22.80 6 -9 4 73.29 16.80 7 -1 14 109.09 30.70 8 -11 2 29.90 21.10 9 -10 7 65.79 30.10 0 10 -1 12.00 12.50 2 -3 -9 108.69 13.40 3 -4 7 393.06 22.40 4 -7 4 747.53 29.40 4 -5 8 316.17 26.40 5 1 13 27.30 24.40 5 4 13 1.40 20.40 6 -8 7 120.09 22.50 6 -6 10 -7.50 22.90 6 -5 11 15.00 24.20 6 -2 13 26.00 24.90 6 2 14 20.30 25.80 7 -10 4 -0.40 20.70 7 -7 10 -2.90 23.80 7 -6 11 16.70 22.90 7 -5 12 13.40 26.30 8 -10 6 56.09 27.30 8 -7 11 34.00 28.30 8 -6 12 9.10 26.90 9 -12 -2 178.58 23.40 9 -12 -1 1.10 18.80 9 -11 5 48.30 29.10 0 1 -6 770.22 22.80 1 2 7 414.56 17.70 1 8 6 45.40 7.40 2 -5 -1 14.40 4.40 2 -2 7 81.89 12.40 2 1 9 439.76 23.00 3 -6 3 314.47 17.90 3 3 11 111.29 17.80 3 4 11 5.50 14.20 4 5 12 21.00 18.00 4 8 11 -2.70 16.70 5 -9 -2 250.17 14.60 5 -9 -1 251.57 15.60 5 -7 7 213.98 22.40 5 -5 10 16.90 19.90 5 5 13 6.80 20.90 6 -7 9 3.20 22.60 6 -4 12 79.29 27.10 6 1 14 15.60 27.60 7 -4 13 27.20 26.50 7 -2 14 16.70 25.70 8 -11 3 66.59 22.90 8 -8 10 83.69 30.30 0 0 -3 2994.10 28.00 0 2 -7 152.48 15.00 0 10 -2 76.89 16.40 1 -2 -6 5130.79 46.90 1 -1 5 1300.97 27.40 1 0 6 1.90 8.20 2 -5 0 1531.25 23.30 2 -3 6 315.67 19.00 2 -1 8 84.59 13.10 4 -2 11 345.47 27.20 4 0 12 237.28 25.40 5 -9 0 7.20 11.00 5 -7 -10 42.30 9.00 5 -6 -12 -0.20 13.50 5 -6 9 15.00 20.10 5 -4 11 10.70 17.60 6 -10 -2 7.20 11.70 6 -9 5 2.20 16.70 7 -8 9 30.70 22.00 9 -12 1 19.90 20.40 0 8 2 139.99 7.50 1 12 0 279.67 19.30 3 -5 6 166.38 16.40 3 5 11 21.30 12.60 4 -7 5 196.78 19.30 4 -6 7 549.35 28.50 5 -9 -3 33.80 9.10 5 -9 1 102.69 14.70 5 -3 12 53.39 25.10 5 -1 13 7.60 21.40 6 -10 0 133.29 16.30 6 -3 13 77.49 27.40 7 -10 5 -0.20 20.00 8 -11 4 66.09 25.80 8 -10 7 42.20 26.70 8 -9 9 7.50 26.50 1 -3 0 3421.46 25.50 2 0 9 -0.10 11.80 3 -6 4 350.66 19.70 3 -3 9 436.06 26.80 3 8 10 0.90 14.40 4 -8 -1 321.67 15.00 4 -8 0 541.55 19.60 4 -4 10 282.67 27.50 4 -1 12 98.59 20.90 6 -10 -3 251.07 15.00 6 -10 1 134.29 17.30 6 -8 8 274.17 28.20 6 -1 14 -0.60 20.50 7 -7 11 0.90 25.60 7 -6 12 -3.30 28.70 7 -3 14 8.00 22.30 0 0 -2 1799.02 17.60 1 -2 4 880.51 22.20 1 1 7 26.30 8.00 1 11 2 129.69 10.30 2 -5 1 549.74 16.40 3 -5 -8 29.00 7.90 3 -4 -10 586.64 23.20 3 -4 8 204.98 18.60 3 -2 10 461.15 27.70 3 0 11 0.00 14.60 3 6 11 22.60 16.80 4 -8 -2 64.09 8.50 4 -8 1 131.49 13.50 4 -3 11 3.10 18.40 5 -9 2 30.50 12.60 5 -8 6 -3.20 16.40 5 -7 8 220.88 23.10 6 -10 2 -0.40 14.40 6 -6 11 6.90 20.80 6 -5 12 150.08 27.80 7 -11 -1 -4.10 15.00 7 -5 13 34.00 27.90 8 -8 11 18.00 26.60 8 -7 12 21.90 24.00 2 -4 5 140.49 13.10 2 3 10 436.26 22.70 2 4 10 37.40 13.10 5 -5 11 3.10 23.40 5 -2 13 -4.10 19.80 5 2 14 -4.10 22.70 5 3 14 -4.80 24.10 6 -7 10 44.30 22.30 6 -4 13 5.10 26.00 6 -2 14 0.50 21.30 7 -11 -2 176.88 17.80 7 -11 0 1.80 15.00 7 -11 1 61.29 18.80 7 -10 6 22.10 23.20 7 -8 10 -1.90 21.70 8 -11 5 116.89 27.50 8 -10 8 10.20 26.30 1 -3 1 368.96 11.00 2 -5 2 680.63 19.80 2 -4 -6 27.40 5.20 2 -2 8 12.60 10.20 3 -5 7 84.69 16.50 4 -8 2 12.30 9.50 4 -7 6 93.99 17.00 4 -6 -9 157.38 10.60 4 -6 8 92.19 17.60 4 -2 12 215.78 25.80 4 2 13 -9.80 18.60 4 3 13 -0.50 19.80 4 4 13 32.30 21.80 4 7 12 7.10 18.40 5 -9 3 91.69 16.00 5 -6 10 128.39 22.30 5 -4 12 232.48 28.40 5 1 14 -1.00 22.90 5 4 14 2.70 23.10 6 -10 3 20.30 15.90 7 -4 14 23.60 22.80 8 -9 10 9.10 26.30 0 9 -2 -2.80 13.00 1 -1 6 499.45 19.90 1 4 8 19.50 8.50 2 -3 -8 50.99 8.80 2 5 10 32.50 12.10 3 -6 5 78.89 12.40 3 -1 11 28.60 15.10 4 -8 -3 266.77 10.60 5 -9 -4 -0.70 7.30 5 -8 7 578.44 32.80 6 -10 -4 218.88 13.10 6 -8 9 22.00 19.90 6 -3 14 90.09 29.60 6 0 15 33.10 27.70 7 -11 -3 77.89 14.80 7 -11 2 22.00 17.80 7 -9 9 108.69 27.80 8 -11 6 37.40 27.70 0 1 -4 6297.47 50.79 0 1 3 1853.11 20.40 1 0 7 167.78 14.00 1 2 8 627.14 23.20 1 7 7 86.09 9.00 3 -3 10 1.00 16.90 3 2 12 48.00 17.20 3 3 12 9.40 14.70 4 -5 10 42.00 20.90 4 -4 11 96.09 21.60 4 5 13 42.50 21.40 5 -9 4 56.49 14.70 5 -7 9 371.46 28.60 5 -3 13 189.88 27.00 5 -1 14 50.99 25.20 6 -10 4 6.20 15.80 6 -6 12 63.89 28.50 7 -10 7 -8.40 23.70 7 -7 12 -3.80 22.40 7 -6 13 -9.90 23.60 0 3 -6 32.30 8.50 1 -3 2 1077.39 20.30 1 -2 5 54.69 10.30 1 0 -8 1009.00 28.70 2 -5 3 147.19 12.80 2 -4 6 478.45 23.00 3 -4 9 66.99 15.30 3 4 12 -0.40 13.80 3 7 11 -4.80 13.20 4 -7 7 -3.60 15.20 4 -3 12 366.96 30.40 4 -1 13 121.99 24.80 6 -7 11 66.69 23.90 6 -5 13 63.89 24.40 7 -8 11 -4.50 22.00 7 -5 14 56.89 25.30 8 -12 -1 81.39 18.00 8 -12 0 59.79 19.00 8 -12 1 -6.30 18.70 0 2 -5 13.50 6.50 0 8 1 -0.90 6.60 1 11 1 310.17 17.10 2 6 10 1.30 11.40 2 9 8 2.90 8.50 3 -7 0 7.20 6.70 3 -6 6 409.76 24.00 3 -5 8 126.99 18.60 3 -2 11 454.85 28.50 3 0 12 33.60 17.30 3 5 12 84.89 19.50 4 -6 9 90.49 20.90 5 -6 11 72.19 26.10 5 -5 12 73.19 25.60 5 -2 14 7.50 23.80 6 -10 5 10.70 18.00 6 -8 10 135.29 28.10 6 -4 14 35.40 26.70 6 -2 15 51.69 25.50 7 -11 4 13.10 20.50 8 -12 -2 -1.70 16.00 8 -12 2 130.49 23.90 8 -11 7 5.80 26.10 0 4 -6 11.20 8.50 1 1 8 363.56 18.60 2 -5 4 778.42 25.00 2 -3 8 161.08 18.30 2 -2 9 73.09 16.00 3 -7 -1 248.78 11.40 4 6 13 -1.20 19.10 5 -8 8 16.70 15.40 5 -7 10 81.29 25.80 5 -4 13 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2.70 20.70 5 -8 9 225.28 27.20 6 -8 11 76.69 27.50 7 -11 6 -4.10 23.10 7 -9 11 10.00 24.70 8 -12 5 39.30 25.10 0 1 4 372.66 11.60 0 2 -4 74.99 8.20 0 4 -5 1457.25 32.90 0 5 -5 0.10 9.60 1 -3 4 1279.27 26.70 1 1 -8 816.22 27.10 3 2 13 4.80 15.70 3 3 13 72.99 18.80 3 8 11 74.89 16.70 4 -8 6 148.59 18.90 4 -5 -10 47.30 11.40 4 -1 14 54.29 22.90 5 -7 11 0.90 23.40 5 -5 13 122.39 25.60 6 -10 7 5.50 21.10 6 -4 15 40.10 27.40 0 2 5 548.05 14.80 1 0 -7 9.20 8.40 1 4 9 576.34 21.60 2 -3 9 132.09 15.60 2 -2 10 1115.79 38.00 2 0 11 1196.88 37.80 2 5 11 65.09 13.90 2 7 10 3.80 11.60 3 -7 -2 1230.98 18.70 3 -3 -10 0.80 12.40 3 4 13 101.59 19.30 4 -7 9 173.28 23.90 4 5 14 48.20 20.60 5 -4 14 242.88 30.70 5 -2 15 38.90 21.90 7 -11 7 17.90 24.00 8 -12 6 33.70 26.50 1 1 9 283.67 18.20 2 -5 6 91.69 14.70 2 -4 8 -0.30 12.90 3 -6 8 30.40 15.90 4 -8 7 3.30 15.80 4 -2 14 18.10 21.60 5 -8 10 123.59 25.80 6 -9 10 -4.10 19.90 6 -7 13 0.10 25.20 6 -6 14 102.29 30.30 0 3 -4 0.40 6.90 1 -3 5 1918.01 35.90 1 -2 7 133.69 14.50 1 5 9 -1.00 8.40 2 -1 11 138.99 18.80 3 -5 10 24.50 18.00 3 -4 11 19.40 15.80 3 -3 12 489.55 32.60 3 5 13 10.20 17.50 4 -4 13 190.58 26.60 5 -10 1 7.40 11.80 5 -10 2 144.49 16.00 5 -10 3 204.58 19.60 5 -3 15 -1.10 23.90 5 0 16 73.99 27.90 6 -11 1 36.50 15.60 6 -11 2 123.79 20.00 6 -5 15 31.50 27.80 7 -9 12 -1.20 25.90 0 5 -4 26.10 9.40 1 0 9 109.09 13.70 2 2 12 11.50 12.50 3 -7 6 0.90 12.70 4 -3 14 -3.60 22.60 4 0 15 83.49 24.80 4 1 15 -2.70 23.40 4 2 15 152.18 26.50 4 3 15 181.98 28.30 5 -10 0 72.59 11.60 5 -10 4 8.90 12.90 5 -7 12 55.99 27.60 5 -6 13 166.28 27.80 5 -5 14 8.70 24.30 6 -11 0 0.70 13.30 6 -11 4 12.60 19.50 7 -11 8 9.90 24.50 0 0 3 2971.70 27.80 2 -5 7 313.07 21.60 2 -3 10 80.79 17.00 3 -6 9 73.19 19.50 3 -2 13 9.30 18.20 4 -7 10 7.80 18.00 5 -4 15 170.78 29.40 6 -9 11 8.70 23.90 0 1 -2 1202.08 16.20 0 2 -3 873.21 18.20 2 -4 9 48.50 13.00 -13 2 1 34.40 30.80 -12 -1 -3 77.19 25.10 -12 5 7 26.30 30.70 -11 4 3 81.09 25.40 -11 5 6 153.48 31.40 -10 5 5 188.48 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11.00 -3 4 13 -32.30 20.70 -12 4 5 11.80 22.90 -11 2 0 172.68 25.10 -11 4 4 113.09 26.90 -11 5 8 42.30 25.60 -10 -3 -5 77.59 18.70 -10 5 7 68.09 28.20 -9 4 3 7.60 19.40 -7 5 7 25.10 20.40 -6 5 8 186.98 24.60 -6 5 13 42.40 26.00 -5 3 1 0.70 9.40 -5 4 17 -12.90 22.60 -4 4 5 19.00 10.80 -3 4 12 -5.90 14.00 -1 3 10 -0.50 7.10 0 -7 -6 35.30 14.20 2 -2 0 297.97 12.00 -13 2 2 25.30 28.20 -13 3 4 4.00 28.90 -12 2 1 61.39 27.40 -12 3 3 13.40 25.60 -11 3 2 134.59 27.20 -11 5 9 165.98 33.50 -10 5 8 -9.80 27.00 -9 -1 -4 54.39 14.70 -9 3 1 94.69 21.50 -9 5 7 131.69 25.80 -8 2 -1 1.00 13.40 -8 4 3 5.60 16.30 -8 5 7 0.10 21.20 -8 5 15 3.10 28.50 -7 4 3 41.60 14.00 -7 5 14 21.60 26.40 -6 5 9 77.19 20.90 -6 5 12 16.90 19.30 -5 4 4 635.74 27.60 -4 4 15 1.20 18.30 -3 4 8 57.69 12.90 -2 3 15 0.00 13.10 4 -3 3 19.90 12.00 4 -2 13 6.60 11.80 -12 4 6 62.89 30.60 -11 -1 -3 163.38 23.30 -11 0 -2 -8.20 21.70 -11 1 -1 3.70 19.50 -11 4 5 13.90 25.10 -11 5 10 23.80 25.30 -11 5 11 5.60 28.50 -10 4 4 84.39 27.80 -10 5 9 388.16 37.70 -9 0 -3 55.09 16.00 -9 5 8 71.39 27.80 -8 -2 -5 1.00 12.00 -8 5 8 2.30 21.60 -8 5 14 69.09 29.60 -7 2 -1 388.46 23.50 -7 5 8 66.99 19.70 -7 5 13 -0.40 23.00 -6 3 1 -4.20 12.90 -4 3 2 209.18 14.90 -3 3 17 -1.90 16.80 1 -6 -5 500.75 23.20 3 -2 2 1218.08 26.50 4 -4 1 384.56 21.90 -13 1 1 -1.20 26.30 -12 -2 -3 11.10 20.60 -12 1 0 265.37 33.30 -10 5 10 287.77 37.40 -10 5 11 -0.80 28.60 -10 5 12 -5.60 27.20 -9 5 9 154.78 29.90 -9 5 14 16.00 28.40 -8 3 1 66.19 15.80 -8 5 9 114.09 27.40 -7 3 1 22.10 14.80 -7 5 9 618.54 35.30 -7 5 10 91.99 23.10 -6 4 4 86.39 17.80 -5 4 16 -8.30 22.60 -4 4 6 183.48 18.70 -4 4 14 439.66 30.40 -2 3 5 -3.10 7.80 2 0 14 62.59 5.20 -13 3 5 -4.60 27.60 -12 -1 -2 18.20 23.00 -12 0 -1 13.00 22.10 -12 4 7 4.00 28.00 -10 3 2 179.78 25.30 -9 4 4 69.29 20.20 -9 5 10 340.77 36.50 -9 5 11 66.49 28.30 -9 5 12 10.50 27.70 -8 4 4 416.16 31.80 -8 5 10 -6.40 24.80 -7 4 4 104.49 19.40 -6 4 17 24.50 24.80 -5 1 -2 10.30 8.40 -5 4 5 352.66 23.50 -4 -2 -5 74.69 6.00 -4 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2 9 18.50 8.30 3 4 11 7.30 14.30 4 4 -15 41.70 11.30 8 3 2 51.39 14.80 9 6 6 0.90 20.00 -7 3 7 1.10 4.40 -6 2 5 681.13 14.40 1 1 6 417.16 15.40 1 6 14 7.60 18.20 2 3 10 474.45 23.50 3 1 -8 353.66 8.60 3 5 12 60.49 18.60 4 4 10 44.90 16.80 5 1 1 13.90 7.30 5 2 -10 290.97 5.80 5 4 9 256.87 23.70 6 3 6 158.48 18.90 6 4 -14 35.10 6.20 6 4 8 256.77 23.20 7 2 0 49.30 10.50 7 6 9 32.50 22.30 9 5 4 46.30 21.20 10 5 -9 49.90 12.20 10 5 1 196.08 23.90 11 6 -8 94.69 16.70 11 6 -1 45.00 19.40 0 7 15 -3.70 19.10 2 2 8 674.03 24.00 4 1 3 387.36 15.90 5 2 5 155.78 13.90 6 2 3 811.42 27.60 6 5 9 197.18 27.30 7 3 4 143.39 16.90 7 4 6 5.70 16.00 8 3 1 0.30 11.90 8 4 4 0.00 14.80 8 5 6 85.99 19.30 11 6 -2 3.00 18.80 -6 5 12 1.20 7.40 -4 7 15 41.10 15.90 -1 1 -8 867.31 23.50 0 0 -2 1765.12 13.90 0 1 6 1119.39 21.20 0 4 12 14.10 11.80 2 7 14 8.60 20.20 3 2 7 0.70 9.50 3 3 9 250.97 20.00 4 5 11 0.60 14.90 4 6 12 54.59 18.40 5 1 0 901.61 22.00 5 3 7 16.30 11.90 5 5 10 13.70 18.50 5 6 11 37.50 20.40 6 6 10 1.40 16.90 8 6 7 42.70 20.40 9 6 5 28.90 20.10 10 5 0 117.29 20.00 11 6 -7 0.60 15.70 -9 4 6 8.50 8.80 -5 1 0 1616.54 29.50 -4 5 13 -2.30 9.70 -2 4 12 108.69 12.90 -1 1 6 425.66 11.70 -1 4 12 16.10 10.40 -1 7 15 -9.10 17.60 0 5 13 430.36 24.40 0 6 14 29.40 17.40 1 3 10 206.58 16.50 2 1 5 56.19 8.10 2 4 11 151.98 17.90 3 1 4 11.70 6.40 4 2 -11 233.38 9.30 4 3 8 4.50 11.20 7 3 -10 67.19 5.70 9 5 3 152.28 22.60 10 5 -1 40.50 17.10 11 6 -6 10.90 16.00 11 6 -5 41.70 18.30 11 6 -4 57.19 19.20 11 6 -3 4.10 16.30 -8 3 5 168.98 12.30 -7 2 2 72.69 10.30 -5 1 -1 437.16 17.20 -5 1 1 15.90 5.80 -4 6 14 44.30 12.80 -3 7 15 2.70 15.60 -2 7 15 12.90 16.60 -1 6 14 9.40 16.60 1 2 8 658.53 21.90 5 1 -1 382.46 13.90 6 2 2 149.39 14.10 6 3 5 86.79 16.10 6 4 7 538.55 29.40 7 2 -4 430.26 15.30 7 2 -3 48.30 8.10 7 3 3 9.70 11.50 7 5 7 41.00 18.00 8 3 -7 538.55 16.80 8 4 -11 20.50 6.30 8 4 3 -8.90 14.40 8 5 5 4.60 17.70 9 4 -8 110.49 11.80 10 5 -8 37.00 12.10 -9 5 9 122.99 8.40 -5 1 -2 3.50 7.30 -3 5 13 625.94 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-10 -1.60 12.60 9 7 -9 43.20 14.60 -2 -1 -3 101.09 7.70 -1 -1 -7 29.50 8.20 -1 -1 -5 1544.15 26.30 -1 4 8 703.63 21.70 0 10 11 164.88 23.30 1 7 9 18.10 12.00 2 7 8 0.50 14.30 2 9 9 49.00 19.70 3 1 -2 43.00 4.80 3 2 1 3.30 5.40 3 9 8 -4.10 18.10 4 5 4 187.68 15.90 4 6 5 289.17 21.10 5 8 5 20.50 16.40 5 11 6 -7.60 22.50 6 3 -5 39.30 7.30 7 6 -1 -4.60 13.10 9 9 -4 -0.10 19.00 -8 2 6 20.40 6.70 -5 1 5 24.90 3.10 -4 -1 -2 160.58 11.10 -4 8 12 37.40 14.60 -3 -1 -2 227.38 11.10 -2 10 12 0.20 18.20 0 6 9 -1.20 8.50 3 1 -13 11.00 8.80 4 3 1 2414.56 38.30 4 10 7 167.58 24.80 5 7 4 1.60 14.90 6 5 0 179.08 16.10 6 8 3 2.70 17.30 6 10 4 68.29 21.80 7 4 -11 152.78 9.20 7 7 0 41.00 15.60 7 8 1 59.99 17.70 7 10 2 9.30 20.00 8 6 -5 124.09 14.80 8 7 -3 215.98 20.60 9 8 -6 9.80 15.50 -6 3 8 0.70 3.30 -3 9 12 6.70 16.30 -2 6 10 40.90 12.30 -1 9 11 247.58 26.10 0 3 6 1458.85 27.70 1 6 8 50.59 13.20 2 1 0 1349.47 17.80 2 3 4 -2.40 6.50 2 10 9 9.70 20.30 3 4 4 231.88 15.20 3 6 6 56.69 12.20 3 10 8 4.30 19.50 4 8 6 19.00 18.00 4 11 7 12.00 22.60 5 2 -12 289.27 6.20 5 5 2 85.39 12.10 5 6 3 136.49 17.80 5 9 5 18.40 21.30 6 4 -2 271.47 14.90 6 6 1 105.59 17.10 6 7 2 -3.90 14.50 6 11 4 47.90 21.80 7 4 -7 286.17 13.90 8 8 -2 161.58 21.50 9 8 -7 9.10 16.60 9 9 -5 6.20 18.00 9 10 -4 15.30 20.60 -8 1 4 330.47 16.60 -5 3 8 -3.80 3.80 -5 8 12 11.30 12.60 -2 8 11 133.89 18.80 -1 7 10 114.59 16.00 0 4 7 287.87 15.50 1 3 5 1716.53 30.60 1 8 9 43.90 16.40 2 6 7 159.88 16.30 2 11 9 -4.80 19.00 3 5 5 -0.50 8.50 3 8 7 172.98 22.00 3 11 8 111.79 24.10 4 1 -10 1518.45 14.80 7 4 -10 315.17 12.50 7 4 -8 26.20 7.70 7 9 1 40.30 19.90 7 11 2 32.20 19.70 8 6 -6 17.60 10.50 -7 5 10 121.09 8.60 -6 8 12 0.00 12.00 -4 -1 -1 121.19 10.20 -1 10 11 38.60 21.40 1 5 7 239.48 16.90 2 4 5 373.56 18.50 2 5 6 160.48 15.90 2 8 8 18.00 15.20 4 2 -15 11.60 8.50 4 7 5 725.53 31.90 5 10 5 24.10 20.40 6 3 -6 23.30 5.80 6 9 3 83.29 19.50 7 4 -9 44.80 8.60 7 5 -4 296.27 18.10 8 7 -4 83.69 15.80 9 8 -8 8.00 16.50 9 9 -6 15.60 18.30 -7 0 2 85.29 11.30 -7 4 9 83.19 5.50 -6 1 5 85.79 5.60 -5 -1 -1 7.80 8.40 -4 9 12 -14.10 15.10 -3 -1 -1 220.48 10.60 -3 10 12 -2.50 16.20 -2 5 9 65.69 10.80 -1 -1 -3 398.06 11.60 0 -1 -7 25.70 6.90 0 -1 -6 1096.99 21.30 2 0 -11 117.89 11.20 2 0 -4 2.00 1.00 2 2 2 28.70 6.90 4 4 2 149.79 13.80 4 9 6 75.19 19.40 5 3 -2 64.99 8.80 5 4 0 523.95 20.90 5 8 4 196.68 22.00 5 11 5 8.50 21.10 7 7 -1 73.09 16.40 7 8 0 -0.50 16.50 8 6 -13 6.00 10.60 8 6 -7 3.00 11.30 8 8 -3 -5.80 17.40 8 9 -2 213.58 24.40 9 8 -9 39.80 15.80 9 10 -5 0.90 18.60 -4 7 11 56.29 13.80 -1 11 11 112.29 24.30 1 9 9 172.68 22.30 3 7 6 4.00 14.30 3 9 7 -8.20 18.80 4 2 -2 2041.00 27.40 4 6 4 25.70 11.20 4 10 6 6.20 20.80 5 2 -6 1143.29 17.20 6 5 -1 234.98 16.00 6 8 2 50.29 18.90 9 8 -11 22.30 14.40 9 8 -10 23.40 15.00 9 9 -7 4.40 17.60 -3 6 10 25.60 10.70 -2 9 11 7.40 16.90 -1 2 5 518.45 13.30 -1 8 10 2.40 13.00 0 -1 -5 197.28 9.00 0 10 10 181.58 24.50 1 7 8 40.40 14.60 2 9 8 -1.10 15.00 3 1 -14 79.09 12.50 3 3 2 46.10 8.00 5 5 1 321.97 19.50 5 7 3 250.67 20.60 5 9 4 41.50 19.80 6 3 -7 71.59 7.30 6 6 0 69.39 13.90 6 7 1 12.50 14.70 6 11 3 68.49 23.10 7 11 1 14.80 20.80 8 7 -5 11.50 12.50 8 10 -2 14.30 20.40 -5 9 12 93.39 17.60 -4 10 12 -0.90 16.70 -3 8 11 11.10 12.60 0 11 10 17.90 20.60 1 10 9 6.50 17.60 4 3 0 1167.28 25.90 4 8 5 73.39 16.30 4 11 6 52.39 19.60 5 6 2 55.29 13.00 7 5 -5 16.00 9.20 7 9 0 14.30 15.70 8 6 -12 62.99 11.60 8 6 -9 41.40 13.40 8 8 -4 42.10 17.70 8 9 -3 318.87 27.80 9 9 -8 3.80 17.00 -7 1 5 271.67 11.10 -2 0 2 1954.50 11.00 -2 7 10 156.88 16.10 -2 10 11 8.20 17.10 1 2 3 4.70 5.50 2 10 8 14.40 15.70 3 2 0 1673.13 25.50 3 6 5 436.26 22.80 3 11 7 11.00 19.40 4 1 -11 37.80 5.20 5 10 4 27.70 21.00 6 3 -11 1.10 4.50 6 9 2 -10.40 16.30 7 8 -1 70.99 17.80 8 6 -11 2.50 10.20 8 6 -10 14.60 11.00 8 7 -6 51.29 15.10 -9 1 4 2.90 11.90 -9 2 6 6.40 8.70 -6 9 12 45.10 14.30 -5 7 11 29.40 11.90 -4 0 3 289.27 8.10 -1 5 8 2.30 8.40 -1 9 10 173.68 21.30 0 2 4 200.28 9.60 0 6 8 36.00 9.40 2 6 6 -1.60 10.90 2 11 8 17.80 17.00 3 4 3 268.07 15.40 3 5 4 372.16 19.40 4 9 5 18.30 19.00 5 8 3 71.49 18.20 5 11 4 -5.30 20.40 6 3 -8 4.70 5.10 6 10 2 22.10 19.80 7 10 0 10.10 16.70 8 10 -3 147.09 25.20 9 9 -9 21.30 16.50 -7 9 12 1.10 14.40 -5 10 12 13.90 15.70 -3 5 9 347.17 16.10 -3 9 11 15.00 16.50 -2 -1 -1 1249.38 19.20 -2 11 11 119.69 24.00 1 6 7 17.70 9.20 1 8 8 83.59 16.70 2 3 3 48.60 8.70 2 8 7 55.29 16.50 4 7 4 222.78 19.50 5 2 -7 213.58 7.50 5 3 -3 32.30 7.10 5 4 -1 399.26 18.30 6 5 -2 -4.90 7.70 6 8 1 9.90 13.00 6 11 2 6.80 20.30 7 5 -6 2.50 8.40 7 11 0 36.80 21.00 8 8 -5 203.48 20.70 8 9 -4 17.20 18.70 -10 3 7 3.60 7.60 -8 7 11 16.60 10.40 -7 0 3 118.49 11.50 -6 7 11 190.88 15.20 -4 6 10 55.79 10.60 -4 8 11 91.79 16.40 -1 -1 -2 1363.86 18.50 -1 3 6 940.41 20.60 -1 10 10 178.78 23.30 1 1 1 218.38 7.00 2 5 5 266.97 17.20 3 9 6 3.10 17.50 4 4 1 6.90 9.30 4 10 5 103.89 23.10 5 7 2 65.99 16.30 6 3 -10 5.10 5.30 6 3 -9 25.90 5.50 6 6 -1 8.40 11.60 6 7 0 59.99 15.50 7 6 -4 11.60 10.30 7 9 -1 102.89 21.20 8 7 -7 110.79 16.40 8 11 -3 113.79 25.20 -3 -1 0 6.90 4.60 -2 6 9 58.29 11.80 -2 8 10 3.30 11.70 1 5 6 12.60 9.60 2 4 4 16.30 7.70 2 9 7 6.60 16.50 3 1 -15 151.98 15.30 3 1 -3 4357.36 26.60 3 7 5 77.19 15.90 4 5 2 223.28 16.70 4 11 5 86.59 22.90 4 12 5 30.40 22.20 5 5 0 21.30 10.50 6 9 1 3.40 17.80 8 10 -4 155.38 25.50 -3 4 8 48.20 7.60 -3 7 10 36.80 11.10 -1 11 10 27.80 19.00 0 3 5 3610.74 40.50 0 4 6 5.30 7.80 1 -1 -9 365.96 15.80 1 3 4 9.90 6.00 1 4 5 1367.36 30.40 1 9 8 210.68 21.30 3 10 6 6.50 18.50 4 1 -12 26.70 6.20 4 2 -3 147.19 8.40 4 8 4 396.46 24.90 5 6 1 404.96 21.60 7 5 -7 405.66 17.70 7 10 -1 121.99 21.40 8 7 -8 7.40 13.40 8 8 -6 16.70 14.30 8 9 -5 36.40 19.20 -8 1 5 9.40 7.90 -3 11 11 16.40 17.20 0 7 8 10.90 9.30 1 7 7 79.89 15.80 1 10 8 84.69 20.70 2 7 6 54.29 13.50 2 10 7 6.70 18.60 3 11 6 16.20 19.60 3 12 6 6.60 19.60 5 2 -13 3.90 3.60 5 11 3 13.50 20.60 6 10 1 62.09 21.00 7 11 -1 18.10 17.30 8 11 -4 66.59 24.00 -8 0 3 141.39 14.40 -5 8 11 298.97 20.00 -4 9 11 38.10 15.10 -2 9 10 191.28 20.50 1 -1 -10 264.47 14.30 1 11 8 7.20 19.00 1 12 8 35.00 20.30 2 11 7 6.40 18.90 2 12 7 18.90 20.30 3 3 1 418.96 15.40 3 6 4 67.99 12.20 3 8 5 117.79 18.40 4 3 -1 19.90 7.30 4 9 4 43.90 19.80 5 8 2 64.09 15.60 5 12 3 38.80 20.50 6 4 -5 31.30 7.50 6 8 0 7.00 12.20 6 11 1 42.70 21.70 6 12 1 8.40 20.10 7 6 -5 183.08 15.00 8 7 -9 268.97 19.90 8 10 -5 4.00 21.00 2 2 1 1.90 5.60 5 4 -2 14.90 8.00 6 6 -2 108.09 14.70 6 7 -1 -11.60 13.30 7 5 -14 74.09 8.60 7 5 -8 485.35 19.00 7 7 -4 53.99 14.20 8 8 -7 57.19 14.90 8 9 -6 131.99 22.10 -4 5 9 478.65 16.70 -4 10 11 13.10 16.30 -3 8 10 56.29 14.30 -2 10 10 7.80 18.10 0 1 2 230.48 6.80 0 8 8 240.58 20.50 1 -1 -6 396.16 11.50 2 6 5 37.70 12.30 2 8 6 79.99 17.20 3 0 -9 557.64 12.10 3 4 2 445.36 18.10 3 5 3 -0.60 7.90 4 11 4 265.87 28.60 5 7 1 1.30 13.50 5 9 2 -3.80 18.80 6 9 0 44.70 18.80 8 7 -13 54.99 13.70 8 11 -5 96.29 23.90 -10 2 6 22.00 10.20 -6 8 11 169.38 16.80 -4 7 10 100.09 13.30 -4 11 11 14.80 17.80 -2 7 9 12.10 10.00 -2 11 10 0.00 19.10 0 -1 -3 1751.82 19.60 0 6 7 -4.60 9.80 1 6 6 466.95 22.30 3 0 -10 167.38 8.60 3 2 -1 610.24 15.00 3 9 5 32.80 16.20 4 4 0 1136.29 27.90 4 6 2 -6.80 10.90 4 12 4 2.40 18.70 5 5 -1 646.14 24.10 5 6 0 54.79 12.70 5 10 2 205.38 25.10 6 10 0 -2.50 18.20 7 5 -9 26.00 9.90 7 6 -6 140.59 14.70 8 7 -12 -0.40 11.40 8 7 -11 150.78 15.70 8 8 -8 138.59 19.20 8 10 -6 4.90 20.30 -9 1 5 110.59 12.40 -5 9 11 10.90 13.90 -3 -2 -3 38.90 7.00 -3 6 9 65.99 10.80 -1 -2 -7 424.76 18.30 2 9 6 204.68 22.30 3 0 -11 8.70 6.40 3 7 4 337.57 22.50 3 10 5 208.08 25.60 4 1 -13 1.10 5.60 4 5 1 169.68 14.70 4 8 3 139.39 19.60 5 11 2 1.10 19.80 5 12 2 3.00 20.20 6 4 -6 1.10 7.10 6 8 -1 12.10 14.80 6 11 0 29.60 20.40 6 12 0 15.40 20.30 8 9 -7 9.60 16.30 -9 6 10 185.28 9.60 -7 8 11 17.00 11.80 -3 9 10 1.90 15.80 -1 5 7 151.58 12.80 -1 10 9 179.18 20.30 -1 11 9 151.08 23.40 -1 12 9 -0.10 20.30 1 9 7 -0.80 14.50 2 5 4 -0.40 7.30 3 0 -8 201.48 6.40 3 11 5 6.50 17.00 3 12 5 78.09 22.30 5 8 1 21.10 15.00 7 5 -13 11.70 7.70 7 5 -10 63.69 10.70 7 7 -5 47.70 13.20 7 8 -4 31.70 14.70 8 8 -9 5.20 14.90 8 11 -6 28.90 20.40 -5 10 11 7.80 15.20 -1 -2 -6 91.39 10.00 0 10 8 3.40 17.10 1 10 7 87.09 19.30 2 3 2 606.64 17.70 2 11 6 2.80 18.50 2 12 6 -0.20 19.30 6 7 -2 6.60 12.50 8 10 -7 28.60 18.30 -7 0 4 34.30 7.20 -6 0 4 198.68 9.60 -6 9 11 32.30 13.80 -4 4 8 2.20 4.70 -3 10 10 3.80 16.50 -2 -1 0 1369.96 17.70 -2 8 9 85.19 14.20 0 5 6 184.28 13.80 1 -1 -5 70.69 5.40 1 5 5 301.37 16.20 1 11 7 85.09 20.80 1 12 7 24.80 19.90 2 7 5 84.59 13.80 3 0 -12 7.70 7.50 3 6 3 283.57 19.00 3 8 4 116.49 17.80 4 7 2 394.66 23.90 4 10 3 85.19 21.80 5 2 -9 110.49 4.80 6 9 -1 46.90 16.20 7 5 -12 60.89 9.70 7 5 -11 160.38 11.80 7 6 -7 16.70 9.30 8 8 -10 203.88 19.90 8 9 -8 49.99 17.60 -8 6 10 74.69 9.00 -7 -1 2 7.80 8.90 -5 7 10 45.10 11.40 -4 8 10 83.69 13.60 -3 11 10 7.20 17.60 -1 -2 -5 477.15 16.70 0 7 7 460.85 21.70 1 2 2 185.88 8.60 1 7 6 19.40 9.80 4 2 -4 3046.10 29.10 4 3 -2 523.75 16.40 4 11 3 402.96 29.40 4 12 3 75.29 20.40 5 7 0 101.39 15.00 6 10 -1 209.28 24.90 7 9 -4 68.89 17.50 -7 9 11 22.60 13.00 -6 10 11 80.39 17.30 -5 -1 2 4.10 5.00 -3 -2 -2 36.20 6.60 -3 -1 1 5303.37 37.50 -2 -2 -3 38.20 7.40 -2 9 9 288.67 21.40 -1 4 6 388.56 15.20 1 4 4 1062.29 25.60 2 8 5 13.90 13.60 3 3 0 2241.88 32.50 3 9 4 66.09 16.80 4 1 -14 7.60 7.20 5 2 -14 447.66 8.90 5 6 -1 52.29 11.90 5 10 1 -2.80 16.90 5 11 1 14.80 19.20 5 12 1 -2.10 19.50 6 4 -7 57.39 7.80 6 8 -2 54.59 15.40 6 11 -1 11.40 17.40 6 12 -1 3.20 17.20 7 7 -6 6.30 11.00 7 8 -5 104.39 17.00 7 10 -4 60.19 21.10 8 8 -12 15.00 13.80 8 8 -11 88.09 15.90 8 9 -9 61.39 17.50 8 10 -8 -0.80 16.50 -4 9 10 110.39 18.10 -3 0 3 5.00 1.90 -3 5 8 23.50 7.80 -2 10 9 153.68 20.90 1 3 3 580.74 16.90 2 6 4 559.94 24.00 3 0 -13 24.60 8.80 3 5 2 446.16 19.50 3 10 4 381.56 29.00 3 12 4 47.20 21.70 3 13 4 70.29 21.00 4 6 1 393.76 20.10 4 8 2 14.40 14.60 5 5 -2 642.24 23.10 6 5 -5 -3.10 7.50 7 6 -8 417.66 19.60 7 11 -4 17.70 21.10 8 8 -13 7.20 14.40 -8 2 7 24.50 4.80 -8 9 11 16.40 14.40 -2 11 9 -2.80 19.00 -2 12 9 65.09 21.60 0 8 7 8.60 9.50 1 8 6 34.80 12.80 2 9 5 274.77 22.50 3 4 1 90.49 9.70 3 7 3 69.99 15.50 3 11 4 126.79 20.70 4 4 -1 1090.49 26.30 4 5 0 20.80 9.10 5 8 0 -2.70 11.60 6 9 -2 8.60 14.70 7 9 -5 0.40 15.50 8 9 -10 32.70 16.20 8 10 -9 19.90 17.60 -7 10 11 -0.70 13.80 -4 10 10 -5.00 15.40 -1 2 4 2673.03 26.10 -1 3 5 371.36 12.90 -1 6 7 36.20 9.90 0 -2 -7 37.00 8.10 0 2 3 127.59 7.00 0 3 4 360.46 13.20 1 6 5 210.98 16.30 1 9 6 77.09 17.80 1 13 6 10.20 19.30 2 -1 -11 555.74 19.10 2 -1 -10 78.49 9.10 2 10 5 304.07 26.10 2 12 5 1.30 19.30 2 13 5 8.40 17.90 4 9 2 334.27 23.90 4 13 2 32.80 22.30 6 10 -2 114.79 22.00 7 7 -7 141.59 16.20 7 8 -6 167.28 19.70 8 9 -11 34.80 17.30 -5 8 10 82.59 13.80 -4 11 10 8.60 15.90 -3 8 9 95.69 14.10 -1 -2 -4 876.11 20.00 0 6 6 284.87 17.30 0 9 7 464.55 25.80 0 12 7 22.90 18.40 0 13 7 68.49 22.30 1 10 6 1.80 17.00 1 12 6 -4.20 18.70 2 -1 -9 1014.00 20.50 2 11 5 -1.70 15.40 3 0 -14 63.79 12.40 4 10 2 28.40 17.10 4 11 2 59.39 20.90 4 12 2 34.80 20.80 5 9 0 25.80 13.70 5 13 0 15.70 20.50 6 11 -2 141.49 23.50 6 12 -2 18.80 17.80 7 6 -9 208.98 15.90 7 10 -5 42.00 19.90 7 11 -5 64.89 21.60 8 9 -12 18.40 16.10 8 10 -10 0.40 16.70 0 10 7 274.97 22.80 0 11 7 -0.80 17.10 1 11 6 13.90 16.30 2 -1 -12 176.38 14.30 2 5 3 33.40 8.50 2 7 4 128.99 15.40 3 8 3 664.63 29.60 4 1 -15 0.80 7.30 4 7 1 79.89 12.30 5 7 -1 3.10 9.10 5 10 0 44.40 17.10 5 11 0 -1.00 18.50 5 12 0 3.90 17.30 6 4 -8 178.88 10.60 -9 2 7 350.06 11.40 -5 9 10 150.68 18.90 -4 -1 2 206.78 8.90 -3 -2 -1 4.60 5.80 -3 9 9 107.89 15.80 0 -2 -6 579.44 17.60 2 -1 -8 766.42 16.10 3 13 3 55.89 22.50 6 5 -6 86.39 10.00 7 9 -6 228.88 22.60 -8 1 6 114.49 8.40 -4 7 9 355.46 19.00 -3 10 9 -1.60 17.50 -3 12 9 89.99 22.20 -2 -2 -2 26.40 5.60 -1 7 7 -0.80 9.60 1 7 5 275.87 19.30 3 2 -2 227.38 9.00 3 9 3 13.10 12.80 3 10 3 667.33 33.50 3 12 3 28.60 20.10 4 8 1 134.69 17.90 5 3 -6 76.59 7.00 5 6 -2 438.96 20.20 5 8 -1 23.30 13.80 6 6 -5 13.70 9.30 7 6 -10 143.09 13.30 7 7 -8 5.10 9.70 7 8 -7 5.80 11.70 7 10 -6 15.50 18.90 7 11 -6 148.69 26.30 -7 -1 3 25.50 8.60 -7 1 6 166.08 7.50 -6 8 10 260.97 18.50 -5 10 10 -3.40 14.70 -5 11 10 1.70 17.60 -4 -2 0 -0.80 5.90 -3 11 9 29.80 17.30 0 7 6 29.50 12.30 2 4 2 187.38 11.90 2 8 4 8.00 11.40 2 13 4 -10.60 19.90 4 3 -3 138.99 9.70 4 6 0 284.67 17.70 4 13 1 77.49 23.10 5 13 -1 73.29 22.30 -9 1 6 35.80 9.10 -1 5 6 1266.37 28.30 0 5 5 133.59 11.80 2 3 1 44.10 6.70 2 9 4 452.95 27.00 2 12 4 77.39 21.80 3 5 1 97.89 11.90 4 9 1 60.59 15.10 4 10 1 587.14 32.70 4 11 1 222.88 25.80 4 12 1 3.90 18.90 5 9 -1 4.00 14.80 5 12 -1 34.00 21.90 6 4 -9 1.60 6.00 7 6 -11 82.49 11.70 7 9 -7 160.38 20.30 -4 5 8 387.46 14.80 -2 9 8 -2.20 12.40 -2 10 8 257.97 22.70 -2 11 8 100.79 19.80 -2 12 8 27.00 18.60 -1 -2 -3 -0.80 5.40 -1 8 7 364.46 20.90 0 -1 -2 237.68 6.50 0 8 6 30.80 13.90 0 13 6 24.60 20.60 1 -2 -10 136.19 13.00 1 -1 -4 2585.74 21.50 1 8 5 453.95 23.00 1 13 5 22.00 17.20 2 6 3 117.39 13.60 2 10 4 145.89 21.60 4 5 -1 238.28 15.10 5 7 -2 39.30 11.80 5 10 -1 22.80 15.60 5 11 -1 17.80 16.40 6 5 -7 119.69 11.40 7 6 -12 83.69 11.80 7 7 -9 172.38 16.00 7 10 -7 4.20 17.00 -6 9 10 76.49 15.50 -4 8 9 139.79 14.40 0 12 6 10.50 17.90 1 -2 -9 227.88 14.00 1 9 5 224.18 20.80 1 11 5 58.99 19.30 1 12 5 -1.60 16.20 3 3 -1 1666.63 26.90 3 4 0 6.30 7.40 3 13 2 6.70 19.90 4 4 -2 18.10 6.40 4 7 0 36.10 11.90 6 7 -5 4.70 10.30 7 6 -14 4.40 9.30 7 6 -13 47.00 11.30 7 11 -7 46.40 19.90 -6 10 10 22.50 14.80 -6 11 10 7.90 16.20 -5 -2 1 2832.12 39.70 -4 9 9 6.10 13.20 -4 12 9 -1.00 16.60 0 9 6 -4.00 12.20 0 10 6 197.68 20.60 0 11 6 35.00 18.10 1 1 0 2101.99 17.60 1 4 3 55.69 8.00 1 10 5 22.60 13.50 3 8 2 56.29 13.70 3 12 2 172.78 24.90 5 13 -2 2.80 19.40 6 6 -6 92.79 11.70 7 7 -10 100.49 14.70 7 9 -8 31.60 17.00 -4 10 9 36.30 16.20 -4 11 9 0.90 16.30 -3 7 8 112.39 13.00 -2 4 6 32.80 6.40 1 6 4 -5.50 7.50 2 7 3 682.33 26.60 3 10 2 7.10 16.00 3 11 2 187.68 25.50 4 8 0 0.70 13.20 4 13 0 43.60 19.00 5 6 -3 313.47 17.00 5 8 -2 14.50 11.20 7 8 -9 10.20 14.40 7 10 -8 6.40 16.40 7 11 -8 -2.10 19.30 -1 6 6 181.48 14.00 0 4 4 402.56 15.40 0 6 5 569.44 21.80 2 13 3 139.39 22.10 4 12 0 38.80 20.60 5 10 -2 -4.60 16.20 5 12 -2 17.30 16.50 6 8 -5 26.10 13.30 2 5 2 23.50 7.70 4 6 -1 1.80 7.40 4 9 0 16.10 12.70 4 11 0 351.26 27.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 10168 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.34950(3) 0.68023(2) 0.66942(2) 0.02122(9) Uani 1 1 d . . . . . P2 P 0.59022(6) 0.40783(5) 0.45060(4) 0.02129(15) Uani 1 1 d . . . . . P1 P 0.53420(6) 0.73106(5) 0.62565(4) 0.02193(15) Uani 1 1 d . . . . . O1 O 0.63230(15) 0.49698(12) 0.63815(9) 0.0264(4) Uani 1 1 d . . . . . N1 N 0.35177(19) 0.74502(15) 0.85838(11) 0.0277(5) Uani 1 1 d . . . . . N3 N 0.18614(19) 0.46672(15) 0.66278(12) 0.0271(5) Uani 1 1 d . . . . . N4 N 0.0764(2) 0.60034(16) 0.64208(12) 0.0302(5) Uani 1 1 d . . . . . N2 N 0.3749(2) 0.89009(15) 0.79787(12) 0.0298(5) Uani 1 1 d . . . . . C1 C 0.6766(2) 0.39508(17) 0.62958(14) 0.0197(5) Uani 1 1 d . . . . . C13 C 0.6698(2) 0.56961(17) 0.71597(13) 0.0219(5) Uani 1 1 d . . . . . C12 C 0.6330(2) 0.67578(18) 0.71459(13) 0.0220(5) Uani 1 1 d . . . . . C2 C 0.6579(2) 0.33815(17) 0.54293(13) 0.0206(5) Uani 1 1 d . . . . . C11 C 0.6798(2) 0.75295(18) 0.79090(14) 0.0241(5) Uani 1 1 d . . . . . H11 H 0.658663 0.826057 0.791597 0.029 Uiso 1 1 calc R U . . . C6 C 0.7351(2) 0.35260(18) 0.70158(13) 0.0222(5) Uani 1 1 d . . . . . C7 C 0.7555(2) 0.41714(18) 0.79459(13) 0.0246(6) Uani 1 1 d . . . . . C8 C 0.7378(2) 0.53828(18) 0.79034(14) 0.0232(5) Uani 1 1 d . . . . . C5 C 0.7698(2) 0.24714(18) 0.68717(14) 0.0275(6) Uani 1 1 d . . . . . H5 H 0.807623 0.216198 0.736092 0.033 Uiso 1 1 calc R U . . . C3 C 0.6985(2) 0.23369(18) 0.53350(14) 0.0253(6) Uani 1 1 d . . . . . H3 H 0.689604 0.193907 0.476056 0.030 Uiso 1 1 calc R U . . . C10 C 0.7546(2) 0.72836(19) 0.86485(14) 0.0265(6) Uani 1 1 d . . . . . C33 C 0.1995(2) 0.57876(18) 0.65848(13) 0.0252(6) Uani 1 1 d . . . . . C9 C 0.7802(2) 0.61923(19) 0.86377(14) 0.0267(6) Uani 1 1 d . . . . . H9 H 0.828069 0.599392 0.914731 0.032 Uiso 1 1 calc R U . . . C24 C 0.3589(2) 0.77661(18) 0.77815(14) 0.0238(5) Uani 1 1 d . . . . . C39 C 0.0418(3) 0.7136(2) 0.64109(15) 0.0333(6) Uani 1 1 d . . . . . H39 H 0.115403 0.761398 0.628174 0.040 Uiso 1 1 calc R U . . . C30 C 0.3793(3) 0.96653(19) 0.73284(16) 0.0365(7) Uani 1 1 d . . . . . H30 H 0.390275 0.923395 0.676354 0.044 Uiso 1 1 calc R U . . . C38 C 0.3114(3) 0.32183(19) 0.60729(16) 0.0379(7) Uani 1 1 d . . . . . H38A H 0.236802 0.265624 0.590088 0.057 Uiso 1 1 calc R U . . . H38B H 0.387164 0.286133 0.623898 0.057 Uiso 1 1 calc R U . . . H38C H 0.322009 0.361315 0.557891 0.057 Uiso 1 1 calc R U . . . C4 C 0.7515(2) 0.18497(18) 0.60436(15) 0.0276(6) Uani 1 1 d . . . . . C40 C 0.0164(3) 0.7602(2) 0.73097(15) 0.0386(7) Uani 1 1 d . . . . . H40A H -0.051385 0.711398 0.746784 0.058 Uiso 1 1 calc R U . . . H40B H -0.009694 0.833948 0.729116 0.058 Uiso 1 1 calc R U . . . H40C H 0.093944 0.765323 0.774785 0.058 Uiso 1 1 calc R U . . . C36 C 0.2932(2) 0.40342(19) 0.68507(15) 0.0317(6) Uani 1 1 d . . . . . H36 H 0.372446 0.457126 0.703578 0.038 Uiso 1 1 calc R U . . . C20 C 0.8083(2) 0.8144(2) 0.94687(15) 0.0318(6) Uani 1 1 d . . . . . C27 C 0.3311(2) 0.62919(19) 0.87197(15) 0.0294(6) Uani 1 1 d . . . . . H27 H 0.318372 0.582572 0.813067 0.035 Uiso 1 1 calc R U . . . C19 C 0.8882(3) 0.4066(2) 0.84506(15) 0.0401(7) Uani 1 1 d . . . . . H19A H 0.953398 0.438246 0.815120 0.060 Uiso 1 1 calc R U . . . H19B H 0.896445 0.328380 0.847236 0.060 Uiso 1 1 calc R U . . . H19C H 0.899242 0.446312 0.904893 0.060 Uiso 1 1 calc R U . . . C25 C 0.3626(3) 0.8348(2) 0.92391(15) 0.0381(7) Uani 1 1 d . . . . . H25 H 0.360108 0.832496 0.984131 0.046 Uiso 1 1 calc R U . . . C26 C 0.3771(3) 0.9255(2) 0.88578(15) 0.0383(7) Uani 1 1 d . . . . . H26 H 0.387095 0.999964 0.913804 0.046 Uiso 1 1 calc R U . . . C35 C 0.0589(3) 0.4238(2) 0.64892(16) 0.0369(7) Uani 1 1 d . . . . . H35 H 0.026197 0.349057 0.648681 0.044 Uiso 1 1 calc R U . . . C29 C 0.4473(3) 0.5974(2) 0.92736(16) 0.0402(7) Uani 1 1 d . . . . . H29A H 0.520885 0.609540 0.898612 0.060 Uiso 1 1 calc R U . . . H29B H 0.432088 0.519329 0.933921 0.060 Uiso 1 1 calc R U . . . H29C H 0.463876 0.642968 0.985321 0.060 Uiso 1 1 calc R U . . . C18 C 0.6526(3) 0.3686(2) 0.84210(15) 0.0389(7) Uani 1 1 d . . . . . H18A H 0.662739 0.410124 0.901270 0.058 Uiso 1 1 calc R U . . . H18B H 0.661484 0.290908 0.846009 0.058 Uiso 1 1 calc R U . . . H18C H 0.568354 0.374004 0.809202 0.058 Uiso 1 1 calc R U . . . C37 C 0.2737(3) 0.3436(2) 0.76266(16) 0.0461(8) Uani 1 1 d . . . . . H37A H 0.260546 0.396992 0.811585 0.069 Uiso 1 1 calc R U . . . H37B H 0.348940 0.308047 0.781034 0.069 Uiso 1 1 calc R U . . . H37C H 0.199099 0.287394 0.745067 0.069 Uiso 1 1 calc R U . . . C41 C -0.0711(3) 0.7144(2) 0.57032(17) 0.0534(9) Uani 1 1 d . . . . . H41A H -0.055978 0.676289 0.514611 0.080 Uiso 1 1 calc R U . . . H41B H -0.083688 0.790955 0.564255 0.080 Uiso 1 1 calc R U . . . H41C H -0.147011 0.676609 0.585997 0.080 Uiso 1 1 calc R U . . . C34 C -0.0093(3) 0.5069(2) 0.63593(17) 0.0404(7) Uani 1 1 d . . . . . H34 H -0.099335 0.502445 0.624667 0.048 Uiso 1 1 calc R U . . . C32 C 0.2551(3) 1.0157(2) 0.71668(18) 0.0523(8) Uani 1 1 d . . . . . H32A H 0.184321 0.955999 0.697587 0.079 Uiso 1 1 calc R U . . . H32B H 0.257602 1.062982 0.671024 0.079 Uiso 1 1 calc R U . . . H32C H 0.243363 1.059729 0.771019 0.079 Uiso 1 1 calc R U . . . C14 C 0.7933(3) 0.0688(2) 0.59075(17) 0.0446(8) Uani 1 1 d . . . . . C28 C 0.2101(3) 0.6074(2) 0.90879(17) 0.0430(7) Uani 1 1 d . . . . . H28A H 0.216677 0.656241 0.964570 0.064 Uiso 1 1 calc R U . . . H28B H 0.198168 0.530255 0.918461 0.064 Uiso 1 1 calc R U . . . H28C H 0.137429 0.621790 0.867057 0.064 Uiso 1 1 calc R U . . . C21 C 0.7553(3) 0.7813(2) 1.02625(16) 0.0522(9) Uani 1 1 d . . . . . H21A H 0.790161 0.836499 1.077951 0.078 Uiso 1 1 calc R U . . . H21B H 0.779385 0.708985 1.037110 0.078 Uiso 1 1 calc R U . . . H21C H 0.662529 0.777070 1.014469 0.078 Uiso 1 1 calc R U . . . C22 C 0.7719(3) 0.9295(2) 0.93475(16) 0.0471(8) Uani 1 1 d . . . . . H22A H 0.806045 0.953992 0.885050 0.071 Uiso 1 1 calc R U . . . H22B H 0.807329 0.981779 0.988135 0.071 Uiso 1 1 calc R U . . . H22C H 0.679205 0.926115 0.923338 0.071 Uiso 1 1 calc R U . . . C31 C 0.4922(3) 1.0562(2) 0.7624(2) 0.0599(9) Uani 1 1 d . . . . . H31A H 0.478054 1.105472 0.813519 0.090 Uiso 1 1 calc R U . . . H31B H 0.501741 1.098830 0.714622 0.090 Uiso 1 1 calc R U . . . H31C H 0.569433 1.022218 0.778259 0.090 Uiso 1 1 calc R U . . . C23 C 0.9535(3) 0.8217(2) 0.96595(18) 0.0548(9) Uani 1 1 d . . . . . H23A H 0.988165 0.847820 0.916976 0.082 Uiso 1 1 calc R U . . . H23B H 0.978019 0.748525 0.973170 0.082 Uiso 1 1 calc R U . . . H23C H 0.987244 0.873497 1.019901 0.082 Uiso 1 1 calc R U . . . C15 C 0.8185(7) 0.0182(4) 0.6730(3) 0.0585(19) Uani 0.620(4) 1 d . . P A 1 H15A H 0.832770 -0.058832 0.658133 0.088 Uiso 0.620(4) 1 calc R U P A 1 H15B H 0.745143 0.020665 0.702685 0.088 Uiso 0.620(4) 1 calc R U P A 1 H15C H 0.893989 0.059507 0.711891 0.088 Uiso 0.620(4) 1 calc R U P A 1 C17 C 0.6668(5) -0.0125(3) 0.5314(3) 0.0579(18) Uani 0.620(4) 1 d . . P A 1 H17A H 0.642363 0.014781 0.475637 0.087 Uiso 0.620(4) 1 calc R U P A 1 H17B H 0.596161 -0.011975 0.563770 0.087 Uiso 0.620(4) 1 calc R U P A 1 H17C H 0.687497 -0.088054 0.519765 0.087 Uiso 0.620(4) 1 calc R U P A 1 C16 C 0.8921(6) 0.0668(4) 0.5385(3) 0.063(2) Uani 0.620(4) 1 d . . P A 1 H16A H 0.967816 0.115905 0.570054 0.094 Uiso 0.620(4) 1 calc R U P A 1 H16B H 0.862445 0.091882 0.482556 0.094 Uiso 0.620(4) 1 calc R U P A 1 H16C H 0.913144 -0.008693 0.527255 0.094 Uiso 0.620(4) 1 calc R U P A 1 C18A C 0.9559(6) 0.0900(5) 0.6277(4) 0.0289(19) Uiso 0.380(4) 1 d . . P A 2 H18D H 0.990049 0.019299 0.620356 0.043 Uiso 0.380(4) 1 calc R U P A 2 H18E H 0.973909 0.122160 0.689825 0.043 Uiso 0.380(4) 1 calc R U P A 2 H18F H 0.995917 0.140649 0.593666 0.043 Uiso 0.380(4) 1 calc R U P A 2 C17A C 0.7797(8) 0.0170(6) 0.5003(4) 0.039(2) Uiso 0.380(4) 1 d . . P A 2 H17D H 0.689320 0.000398 0.474250 0.058 Uiso 0.380(4) 1 calc R U P A 2 H17E H 0.818412 -0.051725 0.498292 0.058 Uiso 0.380(4) 1 calc R U P A 2 H17F H 0.822160 0.067189 0.467167 0.058 Uiso 0.380(4) 1 calc R U P A 2 C15A C 0.7479(9) 0.0005(7) 0.6500(6) 0.041(3) Uiso 0.380(4) 1 d . . P A 2 H15D H 0.654841 -0.012307 0.636957 0.062 Uiso 0.380(4) 1 calc R U P A 2 H15E H 0.776138 0.037755 0.710488 0.062 Uiso 0.380(4) 1 calc R U P A 2 H15F H 0.781657 -0.070359 0.642889 0.062 Uiso 0.380(4) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0269(2) 0.01755(17) 0.02027(16) 0.00234(12) 0.00662(13) 0.00468(13) P2 0.0280(4) 0.0163(3) 0.0196(3) 0.0016(2) 0.0040(3) 0.0049(3) P1 0.0267(4) 0.0163(3) 0.0225(3) 0.0018(2) 0.0047(3) 0.0028(3) O1 0.0380(11) 0.0190(9) 0.0203(8) -0.0014(7) -0.0023(8) 0.0124(7) N1 0.0363(14) 0.0259(11) 0.0220(11) 0.0022(8) 0.0082(9) 0.0057(10) N3 0.0307(14) 0.0231(11) 0.0298(11) 0.0054(9) 0.0112(10) 0.0028(9) N4 0.0285(14) 0.0298(12) 0.0347(12) 0.0075(9) 0.0097(10) 0.0052(10) N2 0.0436(15) 0.0206(11) 0.0267(11) 0.0006(9) 0.0115(10) 0.0068(10) C1 0.0202(14) 0.0159(12) 0.0247(12) 0.0043(9) 0.0059(10) 0.0049(10) C13 0.0259(15) 0.0204(12) 0.0180(12) -0.0029(9) 0.0042(10) 0.0023(10) C12 0.0218(14) 0.0242(13) 0.0208(12) 0.0025(10) 0.0068(10) 0.0029(10) C2 0.0229(14) 0.0195(12) 0.0195(12) 0.0013(9) 0.0067(10) 0.0016(10) C11 0.0242(15) 0.0211(13) 0.0267(13) -0.0012(10) 0.0070(11) 0.0034(10) C6 0.0228(15) 0.0236(13) 0.0214(12) 0.0039(10) 0.0064(10) 0.0038(10) C7 0.0325(16) 0.0246(13) 0.0179(12) 0.0050(10) 0.0042(11) 0.0077(11) C8 0.0235(15) 0.0252(13) 0.0221(12) 0.0034(10) 0.0071(11) 0.0044(10) C5 0.0341(17) 0.0269(14) 0.0250(13) 0.0100(10) 0.0068(11) 0.0102(11) C3 0.0315(16) 0.0215(13) 0.0244(12) 0.0019(10) 0.0081(11) 0.0073(11) C10 0.0232(15) 0.0273(14) 0.0274(13) -0.0027(10) 0.0065(11) 0.0013(11) C33 0.0343(17) 0.0251(14) 0.0172(12) 0.0021(10) 0.0077(11) 0.0051(11) C9 0.0275(16) 0.0327(15) 0.0192(12) 0.0016(10) 0.0031(11) 0.0062(11) C24 0.0247(15) 0.0229(13) 0.0257(13) 0.0056(10) 0.0070(11) 0.0060(10) C39 0.0334(17) 0.0354(15) 0.0349(14) 0.0092(11) 0.0093(12) 0.0124(12) C30 0.059(2) 0.0206(14) 0.0327(14) 0.0024(11) 0.0168(14) 0.0098(13) C38 0.0426(19) 0.0257(15) 0.0486(16) 0.0061(12) 0.0136(14) 0.0094(12) C4 0.0347(16) 0.0211(13) 0.0294(13) 0.0051(10) 0.0082(12) 0.0097(11) C40 0.0442(19) 0.0398(16) 0.0369(15) 0.0078(12) 0.0119(13) 0.0190(13) C36 0.0329(17) 0.0234(14) 0.0390(15) 0.0072(11) 0.0040(12) 0.0053(11) C20 0.0316(17) 0.0321(15) 0.0273(13) -0.0071(11) 0.0047(12) -0.0003(12) C27 0.0395(17) 0.0267(14) 0.0228(13) 0.0074(10) 0.0038(12) 0.0055(12) C19 0.0452(19) 0.0379(16) 0.0334(15) 0.0003(12) -0.0059(13) 0.0151(13) C25 0.055(2) 0.0370(16) 0.0213(13) -0.0047(12) 0.0095(13) 0.0071(14) C26 0.055(2) 0.0291(15) 0.0308(14) -0.0054(12) 0.0144(13) 0.0073(13) C35 0.0320(18) 0.0290(15) 0.0489(17) 0.0045(12) 0.0117(13) -0.0061(13) C29 0.0399(19) 0.0439(17) 0.0424(16) 0.0163(13) 0.0128(14) 0.0104(13) C18 0.056(2) 0.0332(15) 0.0310(14) 0.0048(11) 0.0180(14) 0.0051(13) C37 0.059(2) 0.0314(16) 0.0477(17) 0.0121(13) 0.0066(15) 0.0042(14) C41 0.059(2) 0.060(2) 0.0416(17) 0.0048(15) 0.0005(16) 0.0259(16) C34 0.0275(17) 0.0415(17) 0.0529(17) 0.0045(13) 0.0156(14) -0.0023(13) C32 0.066(2) 0.0374(17) 0.0540(18) 0.0156(14) 0.0005(17) 0.0120(16) C14 0.080(2) 0.0295(16) 0.0356(15) 0.0125(12) 0.0236(16) 0.0279(15) C28 0.0358(19) 0.0509(18) 0.0441(16) 0.0206(13) 0.0041(14) 0.0026(14) C21 0.074(2) 0.0460(18) 0.0293(15) -0.0118(13) 0.0105(15) -0.0042(16) C22 0.058(2) 0.0359(17) 0.0380(16) -0.0136(13) 0.0001(15) 0.0017(15) C31 0.058(2) 0.0420(19) 0.086(2) 0.0187(16) 0.0252(19) 0.0054(16) C23 0.042(2) 0.059(2) 0.0477(18) -0.0252(15) -0.0068(15) 0.0032(16) C15 0.108(6) 0.034(3) 0.041(3) 0.010(2) 0.008(3) 0.045(3) C17 0.104(5) 0.020(2) 0.049(3) 0.006(2) 0.010(3) 0.011(3) C16 0.088(5) 0.046(3) 0.078(4) 0.023(3) 0.049(4) 0.052(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C33 Ni1 C24 105.31(10) . . ? C33 Ni1 P1 150.09(7) . . ? C24 Ni1 P1 103.93(8) . . ? C33 Ni1 P2 93.68(7) . 2_666 ? C24 Ni1 P2 160.13(7) . 2_666 ? P1 Ni1 P2 56.63(3) . 2_666 ? C2 P2 P1 98.25(7) . 2_666 ? C2 P2 Ni1 105.13(7) . 2_666 ? P1 P2 Ni1 61.56(3) 2_666 2_666 ? C12 P1 P2 106.14(8) . 2_666 ? C12 P1 Ni1 94.13(8) . . ? P2 P1 Ni1 61.81(3) 2_666 . ? C1 O1 C13 119.82(17) . . ? C24 N1 C25 112.2(2) . . ? C24 N1 C27 123.43(18) . . ? C25 N1 C27 124.3(2) . . ? C33 N3 C35 110.8(2) . . ? C33 N3 C36 124.3(2) . . ? C35 N3 C36 124.8(2) . . ? C33 N4 C34 112.2(2) . . ? C33 N4 C39 122.8(2) . . ? C34 N4 C39 124.7(2) . . ? C24 N2 C26 112.2(2) . . ? C24 N2 C30 124.79(18) . . ? C26 N2 C30 122.9(2) . . ? O1 C1 C6 121.85(18) . . ? O1 C1 C2 115.40(19) . . ? C6 C1 C2 122.8(2) . . ? O1 C13 C8 121.78(19) . . ? O1 C13 C12 115.52(19) . . ? C8 C13 C12 122.69(19) . . ? C13 C12 C11 115.9(2) . . ? C13 C12 P1 129.48(16) . . ? C11 C12 P1 114.60(17) . . ? C3 C2 C1 116.1(2) . . ? C3 C2 P2 124.84(16) . . ? C1 C2 P2 119.01(16) . . ? C10 C11 C12 123.8(2) . . ? C1 C6 C5 117.70(19) . . ? C1 C6 C7 121.5(2) . . ? C5 C6 C7 120.8(2) . . ? C8 C7 C6 109.91(18) . . ? C8 C7 C19 111.30(19) . . ? C6 C7 C19 110.20(19) . . ? C8 C7 C18 107.4(2) . . ? C6 C7 C18 108.25(19) . . ? C19 C7 C18 109.6(2) . . ? C13 C8 C9 117.9(2) . . ? C13 C8 C7 121.05(19) . . ? C9 C8 C7 120.9(2) . . ? C4 C5 C6 122.8(2) . . ? C4 C3 C2 123.2(2) . . ? C11 C10 C9 117.2(2) . . ? C11 C10 C20 123.3(2) . . ? C9 C10 C20 119.6(2) . . ? N4 C33 N3 102.8(2) . . ? N4 C33 Ni1 127.38(17) . . ? N3 C33 Ni1 129.76(19) . . ? C10 C9 C8 122.3(2) . . ? N1 C24 N2 102.11(18) . . ? N1 C24 Ni1 126.47(16) . . ? N2 C24 Ni1 131.42(17) . . ? N4 C39 C41 110.8(2) . . ? N4 C39 C40 109.98(19) . . ? C41 C39 C40 111.3(2) . . ? N2 C30 C31 110.6(2) . . ? N2 C30 C32 110.4(2) . . ? C31 C30 C32 111.4(2) . . ? C5 C4 C3 117.3(2) . . ? C5 C4 C14 121.3(2) . . ? C3 C4 C14 121.3(2) . . ? N3 C36 C38 112.48(19) . . ? N3 C36 C37 109.8(2) . . ? C38 C36 C37 110.6(2) . . ? C21 C20 C23 109.2(2) . . ? C21 C20 C22 107.3(2) . . ? C23 C20 C22 108.7(2) . . ? C21 C20 C10 110.2(2) . . ? C23 C20 C10 109.6(2) . . ? C22 C20 C10 111.8(2) . . ? N1 C27 C29 111.1(2) . . ? N1 C27 C28 110.3(2) . . ? C29 C27 C28 113.4(2) . . ? C26 C25 N1 106.7(2) . . ? C25 C26 N2 106.9(2) . . ? C34 C35 N3 107.5(2) . . ? C35 C34 N4 106.7(2) . . ? C15A C14 C17A 116.0(5) . . ? C16 C14 C15 115.4(4) . . ? C15A C14 C4 111.6(4) . . ? C16 C14 C4 110.8(3) . . ? C17A C14 C4 115.8(4) . . ? C15 C14 C4 114.2(3) . . ? C16 C14 C17 106.6(3) . . ? C15 C14 C17 103.4(4) . . ? C4 C14 C17 105.3(3) . . ? C15A C14 C18A 103.0(4) . . ? C17A C14 C18A 103.9(4) . . ? C4 C14 C18A 104.6(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 C33 1.905(3) . ? Ni1 C24 1.923(2) . ? Ni1 P1 2.2594(9) . ? Ni1 P2 2.2646(9) 2_666 ? P2 C2 1.860(2) . ? P2 P1 2.1458(12) 2_666 ? P1 C12 1.855(2) . ? O1 C1 1.386(2) . ? O1 C13 1.386(2) . ? N1 C24 1.372(3) . ? N1 C25 1.387(3) . ? N1 C27 1.468(3) . ? N3 C33 1.383(3) . ? N3 C35 1.386(3) . ? N3 C36 1.477(3) . ? N4 C33 1.368(3) . ? N4 C34 1.379(3) . ? N4 C39 1.482(3) . ? N2 C24 1.377(3) . ? N2 C26 1.382(3) . ? N2 C30 1.475(3) . ? C1 C6 1.388(3) . ? C1 C2 1.414(3) . ? C13 C8 1.391(3) . ? C13 C12 1.406(3) . ? C12 C11 1.409(3) . ? C2 C3 1.398(3) . ? C11 C10 1.383(3) . ? C6 C5 1.388(3) . ? C6 C7 1.533(3) . ? C7 C8 1.531(3) . ? C7 C19 1.542(3) . ? C7 C18 1.542(3) . ? C8 C9 1.398(3) . ? C5 C4 1.388(3) . ? C3 C4 1.396(3) . ? C10 C9 1.398(3) . ? C10 C20 1.541(3) . ? C39 C41 1.505(3) . ? C39 C40 1.525(3) . ? C30 C31 1.520(4) . ? C30 C32 1.522(4) . ? C38 C36 1.525(3) . ? C4 C14 1.542(3) . ? C36 C37 1.530(3) . ? C20 C21 1.531(3) . ? C20 C23 1.533(4) . ? C20 C22 1.536(3) . ? C27 C29 1.517(3) . ? C27 C28 1.520(3) . ? C25 C26 1.339(3) . ? C35 C34 1.338(4) . ? C14 C15A 1.438(9) . ? C14 C16 1.443(5) . ? C14 C17A 1.451(7) . ? C14 C15 1.498(5) . ? C14 C17 1.666(5) . ? C14 C18A 1.731(7) . ?