#------------------------------------------------------------------------------ #$Date: 2024-09-06 02:46:52 +0300 (Fri, 06 Sep 2024) $ #$Revision: 294471 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/21/1572153.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572153 loop_ _publ_author_name 'Hu, Xueqing' 'Zhao, Yunxu' 'He, Tong' 'Niu, Caoyue' 'Liu, Feipeng' 'Jia, Wei' 'Mu, Yi' 'Li, Xingwei' 'Rong, Zi-Qiang' _publ_section_title ; Access to distal biaxial atropisomers by iridium catalyzed asymmetric C-H alkylation. ; _journal_issue 33 _journal_name_full 'Chemical science' _journal_page_first 13541 _journal_page_last 13549 _journal_paper_doi 10.1039/d4sc01837k _journal_volume 15 _journal_year 2024 _chemical_absolute_configuration ad _chemical_formula_moiety 'C42 H35 N3 O4' _chemical_formula_sum 'C42 H35 N3 O4' _chemical_formula_weight 645.73 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-07-17 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-07-21 deposited with the CCDC. 2024-07-22 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.4007(3) _cell_length_b 12.6971(3) _cell_length_c 23.0034(6) _cell_measurement_reflns_used 9601 _cell_measurement_temperature 193.00 _cell_measurement_theta_max 68.045 _cell_measurement_theta_min 4.328 _cell_volume 3329.88(15) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 193.00 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker D8 VENTURE' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0374 _diffrn_reflns_av_unetI/netI 0.0166 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 77740 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 68.302 _diffrn_reflns_theta_min 3.843 _diffrn_source_current 1.1 _diffrn_source_power 0.05500000000000001 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.665 _exptl_absorpt_correction_T_max 0.7531 _exptl_absorpt_correction_T_min 0.6912 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0666 before and 0.0450 after correction. The Ratio of minimum to maximum transmission is 0.9178. The \l/2 correction factor is Not present. ; _exptl_crystal_density_diffrn 1.288 _exptl_crystal_description block _exptl_crystal_F_000 1360 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.172 _refine_diff_density_min -0.094 _refine_diff_density_rms 0.029 _refine_ls_abs_structure_details ; Flack x determined using 2593 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.01(3) _refine_ls_extinction_coef 0.0031(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 446 _refine_ls_number_reflns 6111 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.054 _refine_ls_R_factor_all 0.0249 _refine_ls_R_factor_gt 0.0245 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0361P)^2^+0.3594P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0645 _refine_ls_wR_factor_ref 0.0648 _reflns_Friedel_coverage 0.777 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.999 _reflns_number_gt 6000 _reflns_number_total 6111 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc01837k2.cif _cod_data_source_block cu_230715lu_xgd_rzq_hxq_0m _cod_depositor_comments ; The following automatic conversions were performed: data item '_chemical_absolute_configuration' value 'AD' was changed to 'ad' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas Adding full bibliography for 1572152--1572155.cif. ; _cod_database_code 1572153 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.937 _shelx_estimated_absorpt_t_min 0.919 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C16(H16), C17(H17), C18(H18), C20(H20), C22(H22) 2.b Secondary CH2 refined with riding coordinates: C19(H19a,H19b), C21(H21a,H21b) 2.c Aromatic/amide H refined with riding coordinates: C4(H4), C7(H7), C8(H8), C9(H9), C10(H10), C11(H11), C24(H24), C28(H28), C29(H29), C30(H30), C31(H31), C35(H35), C36(H36), C39(H39), C40(H40), C41(H41), C42(H42) 2.d Idealised Me refined as rotating group: C1(H1a,H1b,H1c), C13(H13a,H13b,H13c), C26(H26a,H26b,H26c) ; _shelx_res_file ; TITL cu_230715lu_xgd_rzq_hxq_0m_a.res in P2(1)2(1)2(1) cu_230715lu_xgd_rzq_hxq_0m.res created by SHELXL-2018/3 at 13:20:50 on 17-Jul-2023 REM Old TITL a in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1): R1 0.122, Rweak 0.034, Alpha 0.003 REM 2.019 for 29 systematic absences, Orientation as input REM Flack x = 0.055 ( 0.026 ) from 2624 Parsons' quotients REM Formula found by SHELXT: C42 N3 O4 CELL 1.54178 11.4007 12.6971 23.0034 90 90 90 ZERR 4 0.0003 0.0003 0.0006 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 168 140 12 16 L.S. 4 0 0 PLAN 5 SIZE 0.1 0.12 0.13 TEMP -80.15 CONF BOND list 4 fmap 2 53 MORE -1 BOND $H ACTA REM REM REM WGHT 0.036100 0.359400 EXTI 0.003075 FVAR 0.48271 C1 1 0.707901 0.982337 0.548334 11.00000 0.06534 0.04327 = 0.05528 0.01141 0.00815 -0.00568 AFIX 137 H1A 2 0.774876 0.966097 0.523178 11.00000 -1.50000 H1B 2 0.731587 1.034047 0.577703 11.00000 -1.50000 H1C 2 0.643919 1.011380 0.524830 11.00000 -1.50000 AFIX 0 C2 1 0.581726 0.900427 0.615800 11.00000 0.04959 0.03113 = 0.03550 -0.00007 -0.00494 0.00049 C3 1 0.536519 0.801784 0.640010 11.00000 0.04565 0.02930 = 0.03048 -0.00241 -0.00233 0.00272 C4 1 0.437518 0.800538 0.677492 11.00000 0.04736 0.03000 = 0.03138 -0.00509 -0.00135 0.00810 AFIX 43 H4 2 0.397877 0.860872 0.692001 11.00000 -1.20000 AFIX 0 C5 1 0.408778 0.698622 0.689208 11.00000 0.04205 0.03398 = 0.02675 -0.00534 0.00089 0.00611 C6 1 0.309109 0.655474 0.721752 11.00000 0.04282 0.04196 = 0.02900 -0.00924 0.00379 0.00488 C7 1 0.200552 0.703549 0.715353 11.00000 0.05541 0.07666 = 0.05141 0.00562 0.01350 0.02564 AFIX 43 H7 2 0.192862 0.762653 0.690318 11.00000 -1.20000 AFIX 0 C8 1 0.103556 0.666484 0.744950 11.00000 0.05081 0.12298 = 0.07204 0.00772 0.02090 0.02795 AFIX 43 H8 2 0.029664 0.699785 0.739795 11.00000 -1.20000 AFIX 0 C9 1 0.113259 0.581659 0.781843 11.00000 0.05206 0.10150 = 0.05395 -0.00557 0.02197 -0.00669 AFIX 43 H9 2 0.046371 0.555977 0.801984 11.00000 -1.20000 AFIX 0 C10 1 0.219748 0.534863 0.789205 11.00000 0.06173 0.05737 = 0.03924 -0.00559 0.01131 -0.01083 AFIX 43 H10 2 0.226792 0.476855 0.815054 11.00000 -1.20000 AFIX 0 C11 1 0.318097 0.570448 0.759608 11.00000 0.04624 0.04086 = 0.03590 -0.00478 0.00440 -0.00234 AFIX 43 H11 2 0.391617 0.536719 0.765202 11.00000 -1.20000 AFIX 0 C12 1 0.569246 0.699110 0.629021 11.00000 0.04132 0.02966 = 0.02897 -0.00098 0.00081 -0.00053 C13 1 0.664179 0.649966 0.594096 11.00000 0.05153 0.03243 = 0.05247 -0.00222 0.01701 0.00105 AFIX 137 H13A 2 0.715845 0.609380 0.619737 11.00000 -1.50000 H13B 2 0.709660 0.705091 0.574575 11.00000 -1.50000 H13C 2 0.629668 0.603002 0.564934 11.00000 -1.50000 AFIX 0 C14 1 0.550731 0.454180 0.678284 11.00000 0.03902 0.03193 = 0.02773 0.00185 0.00088 0.00118 C15 1 0.396611 0.489808 0.612302 11.00000 0.03064 0.03353 = 0.02869 -0.00458 0.00381 0.00587 C16 1 0.505366 0.348801 0.659460 11.00000 0.03990 0.02721 = 0.02974 0.00410 0.00113 0.00056 AFIX 13 H16 2 0.476761 0.308459 0.693999 11.00000 -1.20000 AFIX 0 C17 1 0.401684 0.371714 0.617625 11.00000 0.03127 0.03061 = 0.03097 -0.00201 0.00285 -0.00154 AFIX 13 H17 2 0.326993 0.345066 0.635035 11.00000 -1.20000 AFIX 0 C18 1 0.586221 0.278473 0.622125 11.00000 0.04302 0.02752 = 0.03844 0.00110 -0.00271 0.00788 AFIX 13 H18 2 0.644445 0.236455 0.644911 11.00000 -1.20000 AFIX 0 C19 1 0.493688 0.212476 0.590737 11.00000 0.04916 0.02443 = 0.03931 0.00040 0.00458 0.00008 AFIX 23 H19A 2 0.442260 0.173336 0.617863 11.00000 -1.20000 H19B 2 0.528153 0.163756 0.561802 11.00000 -1.20000 AFIX 0 C20 1 0.431525 0.307290 0.562406 11.00000 0.03247 0.02508 = 0.03267 -0.00292 0.00307 -0.00239 AFIX 13 H20 2 0.362231 0.288505 0.537852 11.00000 -1.20000 AFIX 0 C21 1 0.639322 0.341353 0.571430 11.00000 0.03036 0.03348 = 0.04104 -0.00519 0.00184 0.00325 AFIX 23 H21A 2 0.702176 0.300666 0.552002 11.00000 -1.20000 H21B 2 0.672166 0.409056 0.585241 11.00000 -1.20000 AFIX 0 C22 1 0.533262 0.360404 0.528981 11.00000 0.03063 0.02347 = 0.03374 -0.00248 0.00254 0.00096 AFIX 13 H22 2 0.517716 0.437745 0.526145 11.00000 -1.20000 AFIX 0 C23 1 0.554956 0.316592 0.468308 11.00000 0.03151 0.02359 = 0.03381 -0.00063 0.00312 0.00364 C24 1 0.500318 0.221641 0.449529 11.00000 0.03738 0.02849 = 0.03616 -0.00143 0.00586 -0.00160 AFIX 43 H24 2 0.446634 0.187773 0.474989 11.00000 -1.20000 AFIX 0 C25 1 0.521769 0.176994 0.396366 11.00000 0.03828 0.02686 = 0.03811 -0.00294 0.00167 0.00181 C26 1 0.460965 0.075867 0.379098 11.00000 0.06384 0.03938 = 0.04852 -0.01205 0.01078 -0.01413 AFIX 137 H26A 2 0.519744 0.020991 0.372107 11.00000 -1.50000 H26B 2 0.415405 0.087572 0.343554 11.00000 -1.50000 H26C 2 0.408344 0.053506 0.410443 11.00000 -1.50000 AFIX 0 C27 1 0.601568 0.227147 0.357515 11.00000 0.03405 0.03024 = 0.03247 -0.00058 -0.00110 0.00545 C28 1 0.631263 0.183042 0.302792 11.00000 0.04244 0.03861 = 0.03396 -0.00356 -0.00159 0.00485 AFIX 43 H28 2 0.598268 0.117445 0.291514 11.00000 -1.20000 AFIX 0 C29 1 0.706778 0.233782 0.266091 11.00000 0.05383 0.04962 = 0.02951 -0.00203 0.00441 0.00521 AFIX 43 H29 2 0.726508 0.202620 0.229841 11.00000 -1.20000 AFIX 0 C30 1 0.755239 0.331016 0.281354 11.00000 0.05132 0.05166 = 0.03533 0.00846 0.01028 0.00097 AFIX 43 H30 2 0.805891 0.366458 0.255036 11.00000 -1.20000 AFIX 0 C31 1 0.729870 0.375396 0.334212 11.00000 0.04472 0.03532 = 0.03760 0.00499 0.00551 -0.00011 AFIX 43 H31 2 0.763593 0.441383 0.344192 11.00000 -1.20000 AFIX 0 C32 1 0.654002 0.324383 0.374326 11.00000 0.03365 0.03011 = 0.03299 0.00330 0.00140 0.00576 C33 1 0.629781 0.367665 0.430533 11.00000 0.03077 0.02515 = 0.03417 0.00082 0.00146 0.00310 C34 1 0.687759 0.470450 0.445735 11.00000 0.03331 0.03055 = 0.03020 0.00068 0.00668 -0.00202 C35 1 0.807245 0.655144 0.464174 11.00000 0.04346 0.04447 = 0.04474 -0.00600 0.00868 -0.01874 AFIX 43 H35 2 0.852968 0.716796 0.470003 11.00000 -1.20000 AFIX 0 C36 1 0.852321 0.559199 0.476253 11.00000 0.03095 0.05788 = 0.04533 -0.00223 0.00339 -0.01163 AFIX 43 H36 2 0.929343 0.556296 0.491931 11.00000 -1.20000 AFIX 0 C37 1 0.629660 0.567495 0.433192 11.00000 0.03698 0.02813 = 0.03060 -0.00075 0.00513 -0.00425 C38 1 0.691514 0.662816 0.442806 11.00000 0.04545 0.03281 = 0.03479 -0.00224 0.00959 -0.00941 C39 1 0.513260 0.572226 0.412039 11.00000 0.04150 0.02800 = 0.05221 -0.00075 -0.00455 -0.00189 AFIX 43 H39 2 0.471234 0.508922 0.404910 11.00000 -1.20000 AFIX 0 C40 1 0.460837 0.667256 0.401786 11.00000 0.04976 0.03557 = 0.07365 0.00452 -0.00665 0.00374 AFIX 43 H40 2 0.382570 0.669574 0.387670 11.00000 -1.20000 AFIX 0 C41 1 0.522047 0.761579 0.412004 11.00000 0.06431 0.02840 = 0.07633 0.00640 0.00528 0.00576 AFIX 43 H41 2 0.484558 0.827205 0.405063 11.00000 -1.20000 AFIX 0 C42 1 0.634646 0.759667 0.431773 11.00000 0.06451 0.02685 = 0.05724 -0.00084 0.01287 -0.01127 AFIX 43 H42 2 0.675270 0.823950 0.438193 11.00000 -1.20000 AFIX 0 N1 3 0.492205 0.637273 0.660205 11.00000 0.04051 0.02378 = 0.03076 -0.00408 0.00466 0.00215 N2 3 0.480219 0.530074 0.651110 11.00000 0.03650 0.02432 = 0.02903 -0.00248 0.00138 0.00256 N3 3 0.794776 0.465743 0.467487 11.00000 0.03119 0.04486 = 0.04300 0.00125 0.00339 -0.00321 O1 4 0.543570 0.986004 0.628711 11.00000 0.07068 0.02669 = 0.05494 0.00149 0.00509 0.00507 O2 4 0.668604 0.887310 0.576751 11.00000 0.05929 0.03274 = 0.05324 0.00599 0.01253 0.00081 O3 4 0.630711 0.474825 0.710333 11.00000 0.05385 0.04086 = 0.04722 -0.00037 -0.01847 -0.00135 O4 4 0.335440 0.544267 0.582351 11.00000 0.05011 0.04207 = 0.04423 -0.00686 -0.01148 0.01749 HKLF 4 REM cu_230715lu_xgd_rzq_hxq_0m_a.res in P2(1)2(1)2(1) REM wR2 = 0.0648, GooF = S = 1.054, Restrained GooF = 1.054 for all data REM R1 = 0.0245 for 6000 Fo > 4sig(Fo) and 0.0249 for all 6111 data REM 446 parameters refined using 0 restraints END WGHT 0.0361 0.3598 REM Highest difference peak 0.172, deepest hole -0.094, 1-sigma level 0.029 Q1 1 0.6574 0.6168 0.4360 11.00000 0.05 0.17 Q2 1 0.5471 0.8402 0.6201 11.00000 0.05 0.17 Q3 1 0.4164 0.3439 0.5908 11.00000 0.05 0.15 Q4 1 0.4066 0.4259 0.6049 11.00000 0.05 0.15 Q5 1 0.4526 0.3586 0.6344 11.00000 0.05 0.15 ; _shelx_res_checksum 69162 _shelx_hkl_file ; 0 -1 0 0.30 0.20 0 -1 0 0.30 0.10 0 -1 0 0.10 0.10 0 1 0 0.10 0.10 0 1 0 0.20 0.10 0 -2 0 1023.30 30.80 0 -3 0 0.20 0.20 0 -3 0 0.40 0.50 0 -3 0 0.10 0.10 0 -3 0 0.40 0.10 0 -3 0 0.10 0.20 0 3 0 0.30 0.20 0 3 0 0.40 0.20 0 3 0 0.10 0.20 0 4 0 100.09 3.30 0 4 0 95.09 3.30 0 -4 0 100.99 3.50 0 -4 0 101.99 3.80 0 -4 0 97.89 3.20 0 -4 0 103.29 3.20 0 4 0 103.99 3.30 0 -4 0 105.39 3.20 0 4 0 102.49 3.20 0 -5 0 0.40 0.10 0 -5 0 0.20 0.10 0 5 0 0.10 0.20 0 5 0 0.10 0.20 0 -5 0 0.30 0.20 0 -5 0 0.00 0.30 0 -5 0 1.90 0.80 0 -6 0 2828.92 85.39 0 7 0 -0.10 0.30 0 -7 0 0.00 0.30 0 -7 0 0.20 0.40 0 -7 0 0.10 1.00 0 7 0 0.30 0.30 0 -7 0 0.30 0.20 0 7 0 0.40 0.30 0 7 0 0.00 0.30 0 7 0 0.50 0.30 0 8 0 256.17 8.20 0 -8 0 241.98 7.70 0 8 0 253.17 8.30 0 8 0 262.57 8.10 0 -8 0 253.67 9.20 0 8 0 251.67 8.20 0 -8 0 254.07 8.20 0 -8 0 262.07 8.20 0 8 0 256.07 8.10 0 -8 0 257.07 8.50 0 -8 0 230.88 7.90 0 -9 0 0.60 0.50 0 9 0 0.40 0.50 0 -9 0 0.40 0.50 0 -9 0 0.60 0.50 0 9 0 0.10 0.40 0 9 0 0.30 0.40 0 9 0 0.30 0.40 0 9 0 0.00 0.40 0 -9 0 -12.20 8.70 0 -9 0 0.20 0.40 0 9 0 -0.20 0.30 0 -10 0 99.49 15.30 0 10 0 102.89 3.90 0 -10 0 97.99 3.90 0 10 0 100.99 4.00 0 10 0 101.89 3.80 0 10 0 99.89 4.00 0 -10 0 100.59 4.00 0 -10 0 102.39 4.20 0 -10 0 100.79 3.90 0 10 0 100.69 3.80 0 10 0 108.49 4.00 0 -10 0 96.99 3.90 0 -11 0 0.40 0.50 0 11 0 0.00 0.50 0 11 0 -0.10 0.40 0 11 0 0.30 0.50 0 -11 0 -0.20 0.50 0 11 0 0.20 0.50 0 -11 0 0.80 0.50 0 -11 0 0.20 0.50 0 -11 0 8.70 13.10 0 11 0 -0.30 0.40 0 11 0 0.60 0.50 0 -11 0 0.10 0.40 0 12 0 29.80 1.70 0 12 0 28.50 1.60 0 -12 0 28.80 1.90 0 -12 0 26.30 1.60 0 12 0 30.40 2.20 0 -12 0 42.60 15.60 0 -12 0 27.50 1.60 0 -12 0 28.80 1.70 0 12 0 26.70 1.60 0 12 0 26.00 1.80 0 -13 0 -0.10 0.30 0 -13 0 -0.50 0.40 0 -13 0 0.30 0.40 0 13 0 0.60 0.50 0 13 0 -0.10 0.30 0 13 0 0.20 0.60 0 -13 0 -33.30 16.30 0 -14 0 1.40 0.50 0 -14 0 2.30 0.40 0 14 0 3.40 0.70 0 14 0 4.10 0.90 0 14 0 3.00 0.50 0 -14 0 2.50 0.50 0 15 0 0.20 0.20 0 15 0 0.00 0.40 0 15 0 0.30 0.30 1 0 0 2.40 1.60 -1 0 0 2.10 0.20 1 1 0 1.40 0.10 1 1 0 1.70 0.20 1 1 0 2.30 2.50 1 -1 0 2.90 1.70 -1 -1 0 1.00 0.40 -1 1 0 1.90 0.10 -1 1 0 1.60 0.10 -1 -1 0 1.40 0.10 -1 1 0 2.30 0.20 1 -2 0 549.54 19.10 1 2 0 547.15 20.30 -1 -2 0 558.74 17.00 1 3 0 465.45 14.50 1 3 0 473.25 20.30 -1 -3 0 488.45 14.70 -1 -3 0 490.05 15.00 1 4 0 69.19 2.40 1 4 0 69.79 2.30 1 -4 0 72.39 2.20 1 4 0 68.69 2.40 1 4 0 67.09 2.40 1 4 0 67.29 10.60 -1 -4 0 70.19 3.00 -1 -4 0 68.59 2.60 -1 4 0 70.59 2.30 -1 -4 0 70.69 2.60 -1 -4 0 70.69 2.30 -1 4 0 67.19 2.40 -1 4 0 70.79 2.30 1 -5 0 72.69 2.40 1 5 0 70.19 2.50 1 5 0 75.39 2.60 1 5 0 71.89 2.50 1 5 0 72.09 14.20 -1 -5 0 70.79 2.80 -1 -5 0 72.39 2.50 -1 5 0 72.29 2.40 -1 -5 0 74.79 2.40 -1 5 0 70.19 2.50 -1 -5 0 73.19 3.30 1 6 0 171.18 6.00 1 6 0 164.08 5.50 1 -6 0 155.58 5.40 1 -6 0 175.88 5.30 1 -6 0 171.88 5.60 1 6 0 172.48 5.50 1 6 0 170.58 5.80 1 6 0 174.68 5.60 1 -6 0 146.19 23.00 1 6 0 164.38 25.10 -1 6 0 167.48 5.50 -1 -6 0 169.78 5.80 -1 -6 0 173.88 5.30 -1 6 0 166.98 5.60 -1 6 0 168.08 5.40 -1 6 0 186.18 5.60 -1 -6 0 177.18 5.40 -1 -6 0 173.48 6.50 -1 -6 0 161.68 5.60 1 7 0 227.98 7.30 1 7 0 223.08 7.20 1 7 0 230.08 7.20 1 7 0 219.48 7.30 1 -7 0 220.58 7.30 1 7 0 227.08 7.30 1 -7 0 239.08 15.70 -1 7 0 218.18 7.20 -1 -7 0 230.08 8.40 -1 -7 0 223.58 7.30 -1 -7 0 206.68 7.40 -1 -7 0 232.58 6.90 -1 7 0 223.18 7.20 -1 -7 0 225.18 7.60 -1 7 0 229.58 7.10 -1 7 0 233.08 7.30 -1 7 0 218.38 7.40 1 -8 0 77.29 3.30 1 8 0 76.59 3.00 1 8 0 72.79 3.00 1 8 0 82.39 3.00 1 -8 0 62.19 10.30 1 -8 0 71.59 2.90 1 8 0 77.79 2.80 1 -8 0 76.29 2.90 1 8 0 76.49 2.80 -1 8 0 79.09 3.00 -1 8 0 78.39 2.80 -1 8 0 74.69 3.00 -1 8 0 74.19 2.80 -1 -8 0 75.09 3.20 -1 -8 0 76.89 3.00 -1 8 0 74.09 2.90 -1 -8 0 71.39 2.90 -1 -8 0 76.79 2.60 -1 -8 0 78.39 4.20 1 9 0 380.76 11.90 1 -9 0 353.26 12.00 1 -9 0 361.96 12.20 1 9 0 390.06 12.20 1 -9 0 372.56 12.00 1 9 0 371.16 12.10 1 -9 0 387.36 12.00 1 -9 0 415.86 24.40 1 9 0 357.36 12.00 1 9 0 389.96 12.20 1 9 0 398.26 11.90 1 -9 0 377.76 12.40 -1 9 0 395.76 12.10 -1 -9 0 353.96 12.10 -1 -9 0 370.66 12.00 -1 -9 0 383.16 12.10 -1 9 0 358.46 12.00 -1 9 0 370.16 12.00 -1 9 0 383.26 11.90 -1 -9 0 378.16 13.40 -1 9 0 385.36 11.90 -1 -9 0 368.96 12.30 -1 9 0 384.76 12.90 1 -10 0 174.88 6.60 1 10 0 168.48 6.00 1 10 0 162.38 6.00 1 -10 0 168.58 5.90 1 -10 0 168.38 5.90 1 -10 0 152.28 17.20 1 10 0 169.48 5.90 1 10 0 172.98 6.10 1 10 0 163.78 5.80 1 -10 0 161.18 6.70 1 10 0 179.38 5.80 1 -10 0 181.38 6.00 -1 10 0 165.28 5.80 -1 10 0 157.28 6.00 -1 -10 0 168.38 5.90 -1 10 0 172.98 6.00 -1 -10 0 153.48 5.80 -1 10 0 171.58 5.90 -1 -10 0 174.58 6.20 -1 -10 0 160.38 6.40 -1 10 0 170.08 5.80 -1 10 0 162.88 5.90 1 -11 0 17.20 1.60 1 11 0 15.10 1.30 1 -11 0 14.80 1.10 1 -11 0 18.70 12.00 1 11 0 14.40 1.10 1 11 0 11.90 1.10 1 11 0 13.60 1.40 1 -11 0 14.20 1.20 1 11 0 15.30 1.20 1 11 0 12.90 1.30 1 -11 0 12.70 1.10 -1 11 0 12.20 1.30 -1 -11 0 14.50 1.30 -1 11 0 14.10 1.20 -1 -11 0 6.70 14.20 -1 -11 0 15.80 1.40 -1 11 0 12.20 1.30 -1 11 0 14.40 1.20 -1 11 0 15.20 1.10 -1 -11 0 14.70 1.20 -1 11 0 15.20 1.30 -1 -11 0 15.60 1.20 -1 -11 0 13.20 1.20 1 12 0 76.09 3.80 1 12 0 67.79 4.00 1 12 0 86.29 3.60 1 12 0 82.19 3.70 1 12 0 81.09 3.20 1 -12 0 82.69 3.20 1 12 0 84.19 3.40 1 -12 0 75.89 15.80 1 -12 0 81.29 3.70 1 -12 0 82.29 3.40 -1 -12 0 70.29 18.20 -1 12 0 88.39 3.30 -1 12 0 88.29 3.60 -1 -12 0 82.39 3.30 -1 -12 0 82.39 3.40 -1 -12 0 83.19 3.40 -1 12 0 79.89 3.60 -1 12 0 84.79 3.50 -1 -12 0 83.39 3.80 -1 12 0 79.29 3.70 1 -13 0 17.20 15.50 1 13 0 3.50 0.80 1 13 0 2.80 0.70 1 -13 0 4.10 0.60 1 13 0 2.80 0.60 1 -13 0 3.50 0.80 1 -13 0 3.70 0.60 1 -13 0 2.70 0.50 1 13 0 2.90 1.20 -1 -13 0 3.20 0.70 -1 -13 0 -7.90 18.00 -1 13 0 3.40 0.60 -1 -13 0 3.80 0.80 -1 -13 0 2.80 0.60 -1 13 0 3.90 0.70 -1 -13 0 3.30 0.60 1 -14 0 0.00 0.30 1 -14 0 0.20 0.30 1 14 0 0.60 0.30 1 -14 0 0.20 0.50 1 14 0 0.30 0.40 1 14 0 1.10 0.50 -1 14 0 0.60 0.40 -1 14 0 0.90 0.50 -1 14 0 0.30 0.50 -1 -14 0 0.60 0.40 -1 -14 0 0.60 0.40 -1 -14 0 0.50 0.50 1 -15 0 0.10 0.30 1 15 0 0.20 0.40 1 15 0 0.10 0.30 1 15 0 -0.10 0.20 -1 15 0 0.10 0.30 -1 15 0 -0.10 0.20 -1 15 0 0.10 0.40 2 0 0 2793.42 86.39 2 1 0 412.16 16.20 2 -1 0 414.56 15.20 -2 -1 0 413.46 12.80 -2 -1 0 393.36 12.30 2 -2 0 1714.33 54.09 2 2 0 1704.23 55.89 -2 -2 0 1709.63 51.59 2 -3 0 178.78 12.90 2 3 0 184.28 5.80 2 3 0 189.48 5.90 2 3 0 205.88 13.60 2 -3 0 189.18 9.50 2 3 0 185.98 5.90 -2 -3 0 193.38 6.60 -2 -3 0 183.98 5.90 -2 -3 0 185.48 6.10 -2 3 0 192.58 5.80 -2 -3 0 192.88 5.90 -2 3 0 184.38 5.80 2 4 0 72.09 11.20 2 -4 0 74.99 10.50 2 4 0 91.99 3.10 2 4 0 93.69 3.10 2 4 0 93.49 3.00 2 -4 0 96.49 2.90 2 -4 0 95.39 7.60 2 4 0 92.89 3.10 -2 -4 0 97.69 3.10 -2 4 0 92.89 3.10 -2 -4 0 90.39 3.80 -2 4 0 88.69 3.00 -2 -4 0 96.29 3.10 -2 -4 0 90.69 3.30 -2 4 0 92.49 3.00 2 5 0 1.90 0.40 2 5 0 0.80 10.90 2 -5 0 3.90 11.90 2 5 0 1.10 0.30 2 -5 0 1.30 0.20 2 5 0 1.20 0.40 2 -5 0 1.20 0.20 2 5 0 1.30 0.30 2 -5 0 -0.70 4.30 -2 -5 0 0.90 0.30 -2 5 0 1.50 0.30 -2 5 0 1.50 0.30 -2 5 0 1.40 0.30 -2 -5 0 3.00 0.60 -2 -5 0 1.10 0.30 -2 -5 0 1.30 1.10 -2 5 0 1.80 0.30 2 6 0 -0.20 15.80 2 6 0 7.20 0.80 2 6 0 6.60 0.60 2 -6 0 1.50 5.10 2 6 0 5.20 0.60 2 6 0 7.50 0.70 2 -6 0 -10.70 17.40 -2 -6 0 8.10 0.90 -2 -6 0 7.00 0.50 -2 6 0 7.20 0.70 -2 -6 0 6.40 1.50 -2 6 0 7.60 0.60 -2 6 0 6.60 0.60 -2 -6 0 6.80 1.00 -2 -6 0 8.00 0.60 -2 6 0 7.40 0.60 2 -7 0 851.71 25.00 2 -7 0 855.31 33.60 2 7 0 806.22 24.90 2 7 0 691.43 52.89 -2 -7 0 837.32 25.30 -2 7 0 750.52 25.10 -2 7 0 820.72 24.80 -2 7 0 818.22 24.90 -2 -7 0 832.42 26.20 -2 -7 0 827.52 25.00 2 -8 0 95.49 11.40 2 -8 0 85.19 3.50 2 -8 0 89.99 3.70 2 8 0 93.09 3.50 2 8 0 90.69 3.50 2 8 0 93.39 3.50 2 8 0 97.69 3.70 2 -8 0 90.79 3.40 2 8 0 91.19 3.50 2 8 0 92.39 3.40 2 -8 0 100.29 3.80 2 -8 0 97.19 4.60 -2 -8 0 91.99 4.20 -2 8 0 89.29 3.30 -2 -8 0 96.19 3.90 -2 8 0 96.69 3.40 -2 -8 0 99.79 5.00 -2 -8 0 95.69 3.30 -2 8 0 88.79 3.50 -2 8 0 94.19 4.30 -2 8 0 97.69 3.50 2 -9 0 68.79 3.20 2 -9 0 63.49 2.70 2 9 0 66.69 2.80 2 -9 0 66.19 2.70 2 9 0 70.69 2.70 2 9 0 69.39 2.70 2 9 0 66.09 2.80 2 -9 0 62.69 2.80 2 9 0 65.09 2.90 2 9 0 66.49 2.80 -2 9 0 60.99 2.70 -2 9 0 68.29 2.60 -2 -9 0 68.69 2.80 -2 9 0 70.49 2.80 -2 -9 0 67.49 2.40 -2 9 0 64.89 2.80 -2 -9 0 68.29 3.30 -2 -9 0 66.19 3.00 -2 -9 0 66.09 2.80 -2 9 0 67.69 2.60 -2 9 0 70.29 3.00 -2 -9 0 65.49 4.40 2 10 0 145.39 5.00 2 10 0 145.29 5.10 2 10 0 139.79 5.30 2 10 0 143.89 5.30 2 -10 0 144.19 5.10 2 -10 0 138.39 5.60 2 10 0 142.99 5.30 2 -10 0 151.28 5.70 2 -10 0 141.89 5.50 2 10 0 145.69 5.40 2 -10 0 129.89 15.90 -2 -10 0 144.19 5.20 -2 10 0 146.39 5.20 -2 10 0 140.69 5.00 -2 10 0 151.68 5.10 -2 -10 0 143.99 6.90 -2 -10 0 138.29 5.30 -2 -10 0 153.48 5.30 -2 10 0 136.29 5.20 -2 -10 0 138.79 5.60 -2 10 0 138.09 5.10 2 -11 0 13.20 1.30 2 -11 0 12.80 1.20 2 11 0 15.40 1.20 2 11 0 10.80 1.10 2 11 0 11.80 1.20 2 -11 0 6.50 11.80 2 11 0 12.30 1.30 2 11 0 13.30 1.40 2 -11 0 10.40 1.30 2 11 0 9.60 1.00 2 -11 0 12.90 1.00 -2 11 0 12.90 1.30 -2 -11 0 12.40 1.30 -2 11 0 11.90 1.20 -2 -11 0 13.80 1.20 -2 11 0 10.00 1.10 -2 11 0 11.80 1.00 -2 -11 0 10.40 1.10 -2 11 0 10.70 1.10 2 -12 0 7.90 1.60 2 -12 0 8.90 1.20 2 12 0 7.80 1.20 2 -12 0 -7.40 12.80 2 12 0 8.10 1.00 2 12 0 7.40 0.90 2 12 0 8.00 0.90 2 12 0 7.00 1.00 2 -12 0 8.20 1.00 2 -12 0 6.50 0.90 -2 12 0 9.10 1.50 -2 12 0 5.50 1.00 -2 -12 0 8.70 18.40 -2 -12 0 8.30 1.50 -2 12 0 8.40 1.20 -2 -12 0 6.60 0.80 -2 -12 0 9.90 1.30 -2 12 0 10.10 1.30 -2 12 0 7.80 0.80 -2 -12 0 8.10 1.00 -2 12 0 8.80 1.20 2 -13 0 14.70 1.00 2 13 0 13.50 1.10 2 13 0 15.30 1.30 2 13 0 13.80 1.30 2 -13 0 14.90 1.10 2 -13 0 13.10 1.30 2 13 0 14.10 1.00 2 -13 0 13.10 0.90 -2 -13 0 12.90 1.10 -2 -13 0 15.60 1.20 -2 13 0 12.40 1.20 -2 -13 0 13.90 1.10 -2 13 0 14.00 1.10 -2 13 0 15.60 1.10 -2 -13 0 13.50 1.10 2 -14 0 73.99 2.60 2 14 0 72.69 2.70 2 -14 0 75.39 3.20 2 14 0 72.99 3.00 -2 -14 0 67.29 2.80 -2 14 0 68.69 2.90 -2 14 0 70.69 2.70 -2 -14 0 65.89 2.60 -2 14 0 73.29 2.70 2 15 0 1.40 0.40 2 -15 0 0.70 0.40 2 15 0 0.70 0.40 2 15 0 1.00 0.40 -2 -15 0 1.00 0.20 -2 15 0 0.80 0.40 -2 15 0 1.10 0.30 -2 15 0 1.10 0.30 3 0 0 0.20 0.20 3 0 0 0.70 0.20 3 0 0 2.80 4.10 -3 0 0 -0.20 0.10 -3 0 0 0.20 0.20 -3 0 0 -0.30 0.20 -3 0 0 0.10 1.10 -3 0 0 0.10 0.20 3 1 0 177.48 5.40 3 1 0 171.48 5.50 3 1 0 173.28 5.40 3 -1 0 187.28 9.90 3 -1 0 174.38 5.40 3 1 0 165.98 11.10 -3 -1 0 174.08 5.50 -3 -1 0 177.88 5.50 -3 -1 0 175.28 5.50 -3 1 0 175.18 5.40 -3 -1 0 175.58 6.50 -3 1 0 179.98 5.50 3 -2 0 700.33 24.70 3 2 0 646.64 26.50 -3 -2 0 657.63 20.90 -3 -2 0 686.63 21.10 3 3 0 448.76 21.70 3 3 0 424.26 13.30 3 -3 0 437.26 17.90 -3 3 0 424.16 13.20 -3 -3 0 449.26 14.20 -3 -3 0 439.96 13.70 3 4 0 5.00 0.40 3 4 0 3.80 0.50 3 4 0 2.80 8.30 3 -4 0 14.00 4.10 3 4 0 7.00 0.60 -3 4 0 4.70 0.50 -3 4 0 4.40 0.40 -3 4 0 4.60 0.50 -3 -4 0 5.60 0.80 -3 -4 0 4.60 0.50 -3 4 0 4.80 0.40 -3 -4 0 4.10 0.40 -3 -4 0 3.80 1.30 3 5 0 40.80 1.60 3 5 0 43.30 1.70 3 -5 0 29.90 13.70 3 5 0 32.90 11.80 3 -5 0 43.90 6.30 3 5 0 41.60 1.70 3 5 0 39.40 1.70 3 5 0 42.40 1.80 -3 -5 0 42.80 1.70 -3 -5 0 41.00 2.00 -3 5 0 42.40 1.70 -3 -5 0 41.90 1.80 -3 5 0 43.40 1.60 -3 -5 0 45.00 1.70 -3 5 0 41.60 1.60 -3 5 0 38.60 2.10 -3 -5 0 44.00 2.90 3 6 0 26.40 1.30 3 6 0 25.40 1.30 3 6 0 7.30 18.40 3 6 0 26.00 1.30 3 -6 0 28.00 6.20 3 -6 0 11.90 16.90 3 6 0 24.30 1.20 3 6 0 26.00 1.20 -3 6 0 26.90 1.20 -3 6 0 25.00 1.20 -3 -6 0 24.70 1.20 -3 6 0 26.20 1.30 -3 6 0 24.90 1.10 -3 -6 0 24.70 2.60 -3 6 0 25.30 1.20 -3 -6 0 25.40 1.30 -3 -6 0 26.20 1.30 -3 -6 0 25.00 1.20 -3 -6 0 25.80 1.60 3 -7 0 269.27 9.40 3 7 0 257.37 8.20 3 7 0 256.37 8.40 3 7 0 241.98 32.10 3 7 0 257.57 8.30 3 -7 0 263.87 16.50 3 7 0 252.67 8.10 3 7 0 252.27 8.10 -3 -7 0 263.37 8.10 -3 -7 0 253.57 9.70 -3 7 0 258.17 8.00 -3 -7 0 246.38 8.20 -3 -7 0 235.38 8.00 -3 7 0 237.58 8.20 -3 7 0 253.37 8.20 -3 7 0 244.18 8.00 -3 -7 0 262.77 8.00 -3 -7 0 251.57 8.70 -3 7 0 251.37 8.10 3 8 0 9.90 1.00 3 8 0 12.10 1.10 3 8 0 11.40 1.00 3 -8 0 12.10 1.20 3 -8 0 15.40 7.40 3 8 0 11.60 1.00 3 8 0 10.50 0.80 3 -8 0 10.80 0.80 3 -8 0 10.60 1.30 3 -8 0 10.70 1.20 -3 8 0 9.10 0.80 -3 8 0 11.90 0.90 -3 -8 0 9.80 0.80 -3 8 0 11.10 0.80 -3 -8 0 8.30 2.00 -3 -8 0 11.60 1.00 -3 -8 0 11.70 1.00 -3 8 0 10.20 0.90 -3 -8 0 11.70 0.70 -3 8 0 12.00 1.00 -3 -8 0 8.00 1.10 3 -9 0 53.29 2.30 3 -9 0 50.99 2.40 3 9 0 51.99 2.50 3 -9 0 55.39 2.80 3 9 0 55.99 2.40 3 -9 0 47.00 10.30 3 9 0 55.39 2.30 3 9 0 53.59 2.50 3 -9 0 52.89 2.50 3 9 0 56.19 2.50 3 9 0 54.99 2.30 -3 -9 0 56.59 2.50 -3 9 0 50.29 2.50 -3 -9 0 56.69 2.10 -3 9 0 53.29 2.20 -3 9 0 49.40 2.30 -3 9 0 53.09 2.40 -3 -9 0 58.49 2.90 -3 -9 0 52.59 2.40 -3 9 0 56.09 2.30 -3 -9 0 56.69 6.50 -3 -9 0 53.89 2.40 3 10 0 102.29 3.80 3 10 0 106.29 3.80 3 10 0 101.39 4.00 3 -10 0 106.49 4.40 3 10 0 100.59 3.90 3 10 0 100.19 4.10 3 -10 0 96.19 13.30 3 -10 0 106.39 3.80 3 10 0 100.99 4.00 3 -10 0 99.39 3.80 3 -10 0 99.69 4.00 -3 10 0 94.79 3.80 -3 10 0 97.59 4.00 -3 10 0 99.99 3.70 -3 10 0 100.69 4.10 -3 -10 0 104.29 3.30 -3 -10 0 98.79 4.00 -3 -10 0 102.79 4.50 -3 -10 0 96.89 4.00 -3 -10 0 99.89 3.90 -3 -10 0 97.59 6.10 -3 10 0 107.89 3.80 -3 10 0 97.49 3.90 3 11 0 52.99 2.70 3 11 0 51.99 2.60 3 -11 0 52.69 2.40 3 -11 0 51.89 2.30 3 11 0 56.89 2.50 3 11 0 55.09 2.40 3 -11 0 55.39 2.90 3 11 0 50.69 2.60 3 11 0 52.79 2.40 3 -11 0 52.79 2.50 -3 -11 0 52.79 2.50 -3 11 0 55.09 2.40 -3 -11 0 53.59 3.10 -3 11 0 51.59 2.40 -3 11 0 52.79 2.60 -3 11 0 52.49 2.40 -3 -11 0 53.89 3.00 -3 11 0 53.69 2.50 -3 -11 0 55.89 2.50 -3 11 0 51.69 2.70 3 12 0 33.20 2.00 3 12 0 36.60 2.50 3 -12 0 34.00 1.60 3 12 0 35.90 1.70 3 12 0 36.50 2.00 3 12 0 32.30 1.80 3 -12 0 33.10 1.70 3 -12 0 34.10 1.90 3 -12 0 34.90 2.20 3 -12 0 38.30 12.10 -3 -12 0 33.50 1.90 -3 12 0 35.50 1.80 -3 12 0 35.60 1.80 -3 -12 0 35.60 1.90 -3 12 0 31.50 2.10 -3 12 0 36.10 1.80 -3 -12 0 36.10 21.30 -3 -12 0 34.90 1.90 -3 12 0 37.00 2.10 3 13 0 1.00 0.40 3 13 0 1.60 0.50 3 -13 0 1.90 0.40 3 13 0 0.30 0.60 3 -13 0 1.30 0.40 3 -13 0 2.40 0.70 3 13 0 0.70 0.50 3 -13 0 0.90 0.50 -3 13 0 2.30 0.60 -3 13 0 1.70 0.50 -3 -13 0 2.60 0.60 -3 -13 0 1.50 0.50 -3 13 0 1.90 0.50 -3 -13 0 1.40 0.50 3 14 0 2.80 0.50 3 -14 0 3.20 0.60 3 -14 0 3.60 0.60 3 -14 0 3.80 0.60 3 14 0 4.20 0.70 3 14 0 4.40 0.70 -3 -14 0 3.50 0.50 -3 14 0 3.90 0.50 -3 14 0 4.10 0.70 -3 -14 0 3.90 0.60 -3 14 0 3.80 0.50 4 0 0 0.30 0.20 4 0 0 0.10 0.10 4 0 0 3.30 4.60 -4 0 0 0.40 0.20 -4 0 0 0.00 0.20 -4 0 0 -1.60 1.40 -4 0 0 0.50 0.20 -4 0 0 0.10 0.20 4 1 0 0.20 0.20 4 1 0 0.00 5.50 4 1 0 0.20 0.20 4 -1 0 4.80 4.50 4 -1 0 0.80 0.20 4 -1 0 0.20 0.10 -4 1 0 0.50 0.20 -4 -1 0 0.00 1.40 -4 1 0 0.00 0.20 -4 -1 0 1.00 0.30 -4 -1 0 0.30 0.20 -4 -1 0 0.70 0.20 -4 1 0 0.30 0.20 -4 -1 0 0.70 0.30 4 2 0 36.50 1.80 4 2 0 39.60 1.50 4 -2 0 39.30 1.30 4 2 0 39.20 1.50 4 2 0 46.30 8.00 4 -2 0 39.90 6.10 -4 -2 0 37.80 1.60 -4 2 0 40.60 1.50 -4 -2 0 40.90 2.70 -4 -2 0 37.80 1.50 -4 2 0 39.00 1.50 -4 -2 0 38.90 1.90 -4 -2 0 42.30 1.60 -4 2 0 37.90 1.50 -4 -2 0 39.80 1.50 4 -3 0 213.18 7.70 4 -3 0 206.08 12.40 4 3 0 214.18 6.80 4 3 0 206.38 15.70 4 -3 0 210.78 6.50 4 3 0 228.18 6.80 4 3 0 209.78 7.00 4 3 0 215.38 6.70 -4 -3 0 213.18 6.70 -4 -3 0 219.48 6.90 -4 -3 0 218.38 6.80 -4 3 0 199.68 6.80 -4 3 0 219.68 6.70 -4 -3 0 213.18 7.30 -4 -3 0 219.68 8.40 -4 3 0 220.68 6.80 -4 3 0 213.88 6.70 4 4 0 60.59 2.20 4 4 0 54.69 11.20 4 4 0 55.19 2.20 4 -4 0 47.60 14.10 4 4 0 60.29 2.20 4 -4 0 58.39 7.20 4 4 0 56.19 2.10 -4 4 0 58.19 2.10 -4 4 0 55.39 2.00 -4 -4 0 54.89 2.80 -4 -4 0 59.39 3.40 -4 -4 0 53.29 2.20 -4 4 0 55.29 2.50 -4 -4 0 56.59 2.10 -4 4 0 54.79 2.10 -4 -4 0 57.89 2.20 -4 -4 0 59.19 2.20 4 5 0 141.59 18.00 4 -5 0 131.69 10.70 4 5 0 133.59 4.50 4 -5 0 116.79 17.60 4 5 0 135.79 4.40 4 5 0 134.89 4.60 4 5 0 140.59 4.50 4 5 0 129.79 4.40 -4 -5 0 126.29 5.90 -4 -5 0 134.29 4.40 -4 5 0 128.09 4.50 -4 5 0 129.19 4.40 -4 -5 0 140.39 4.50 -4 5 0 128.29 4.40 -4 -5 0 128.09 4.50 -4 5 0 130.49 4.30 -4 5 0 137.69 4.40 -4 -5 0 138.99 5.00 -4 -5 0 124.19 4.30 -4 -5 0 133.79 4.50 4 6 0 111.09 3.80 4 6 0 99.79 4.40 4 6 0 112.89 4.00 4 6 0 108.29 3.80 4 6 0 96.29 20.80 4 6 0 115.19 3.90 4 -6 0 114.49 11.40 4 -6 0 113.09 20.50 -4 -6 0 111.39 4.00 -4 6 0 117.69 3.90 -4 -6 0 114.99 3.90 -4 6 0 109.49 3.90 -4 6 0 111.79 3.70 -4 6 0 110.09 3.80 -4 -6 0 112.99 6.00 -4 -6 0 113.59 4.40 -4 -6 0 111.09 3.80 -4 6 0 114.29 3.90 -4 -6 0 100.79 3.70 -4 -6 0 115.59 3.90 -4 6 0 104.39 4.00 4 7 0 19.00 1.20 4 -7 0 21.10 7.50 4 -7 0 20.30 1.10 4 7 0 17.60 1.30 4 7 0 17.60 1.80 4 -7 0 19.90 1.20 4 7 0 -8.90 25.50 4 7 0 20.10 1.10 4 -7 0 18.40 1.50 4 -7 0 22.40 1.50 -4 -7 0 20.20 1.60 -4 -7 0 20.90 1.20 -4 -7 0 20.10 1.30 -4 -7 0 19.20 1.10 -4 -7 0 21.00 1.60 -4 7 0 21.50 1.20 -4 7 0 21.00 1.10 -4 7 0 20.80 1.30 -4 -7 0 21.00 2.90 -4 7 0 19.70 1.20 -4 7 0 21.80 1.20 4 -8 0 1.30 0.60 4 -8 0 1.70 0.40 4 8 0 1.40 0.50 4 8 0 1.40 0.40 4 -8 0 1.30 0.50 4 -8 0 2.20 0.70 4 8 0 1.70 0.50 4 8 0 1.20 0.40 4 8 0 1.50 0.60 4 -8 0 2.50 0.70 4 8 0 2.70 0.60 -4 -8 0 1.30 0.60 -4 8 0 1.50 0.40 -4 8 0 1.50 0.40 -4 -8 0 -2.00 2.00 -4 -8 0 1.80 0.40 -4 -8 0 0.80 0.50 -4 8 0 1.80 0.90 -4 8 0 2.10 0.60 -4 -8 0 2.20 0.60 -4 8 0 0.50 0.40 -4 -8 0 1.40 0.40 -4 -8 0 1.20 0.50 -4 8 0 1.60 0.50 4 9 0 23.60 1.60 4 9 0 25.80 1.40 4 -9 0 25.10 1.40 4 -9 0 26.80 1.50 4 -9 0 24.70 1.50 4 9 0 23.80 1.40 4 -9 0 28.00 1.80 4 9 0 27.40 1.60 4 -9 0 18.30 2.40 4 -9 0 18.60 9.40 4 9 0 25.90 1.70 -4 9 0 27.00 1.50 -4 -9 0 23.80 1.70 -4 9 0 25.80 1.40 -4 9 0 24.40 1.60 -4 9 0 26.00 1.40 -4 -9 0 21.70 3.30 -4 -9 0 25.10 1.60 -4 -9 0 17.90 1.90 -4 9 0 26.80 1.50 -4 -9 0 25.10 1.50 -4 9 0 24.70 1.50 -4 -9 0 26.40 2.00 4 -10 0 16.60 1.50 4 10 0 12.50 1.20 4 10 0 15.10 1.90 4 -10 0 11.30 1.00 4 10 0 11.10 1.10 4 -10 0 13.40 1.10 4 10 0 10.50 1.20 4 10 0 13.10 1.30 4 -10 0 16.60 10.30 4 10 0 11.50 1.10 4 -10 0 8.80 1.10 -4 10 0 10.30 1.00 -4 10 0 12.40 1.20 -4 -10 0 13.90 3.20 -4 -10 0 13.60 0.80 -4 10 0 13.80 1.00 -4 10 0 14.50 1.50 -4 -10 0 12.50 1.20 -4 -10 0 12.00 1.20 -4 -10 0 16.10 2.10 -4 10 0 10.90 1.30 -4 10 0 13.10 1.30 4 -11 0 -5.30 10.70 4 11 0 7.90 1.00 4 11 0 9.50 1.10 4 -11 0 9.50 1.10 4 -11 0 9.40 0.80 4 11 0 9.10 1.10 4 11 0 8.60 1.20 4 11 0 8.10 0.90 4 11 0 8.10 1.00 4 -11 0 8.30 1.20 4 -11 0 6.90 0.80 -4 -11 0 2.80 3.00 -4 -11 0 9.50 1.10 -4 -11 0 7.60 1.30 -4 11 0 9.10 0.90 -4 11 0 8.00 1.10 -4 11 0 7.20 0.90 -4 -11 0 8.50 1.10 -4 11 0 8.80 1.00 -4 11 0 8.70 1.10 4 12 0 4.60 0.80 4 -12 0 5.10 0.80 4 12 0 2.90 0.70 4 -12 0 3.60 0.50 4 -12 0 4.80 0.70 4 12 0 3.00 0.60 4 -12 0 2.30 0.80 -4 12 0 2.70 0.70 -4 12 0 3.60 0.60 -4 -12 0 4.10 0.70 -4 12 0 4.80 0.70 -4 -12 0 3.90 0.70 4 -13 0 1.20 0.40 4 13 0 0.80 0.50 4 13 0 0.80 0.50 4 13 0 1.20 0.40 4 -13 0 0.80 0.50 -4 13 0 0.70 0.50 -4 -13 0 1.20 0.40 -4 -13 0 0.80 0.40 -4 13 0 0.60 0.40 -4 -13 0 1.70 0.50 4 -14 0 4.50 0.70 4 14 0 4.00 0.50 4 14 0 4.50 0.60 4 -14 0 4.40 0.50 4 14 0 4.60 0.60 4 -14 0 5.10 0.50 -4 14 0 5.10 0.70 -4 -14 0 5.80 0.70 -4 14 0 4.50 0.60 -4 -14 0 3.80 0.50 -4 -14 0 5.20 0.60 -4 14 0 5.90 0.60 5 0 0 1.20 5.80 5 0 0 0.20 0.10 5 0 0 0.30 0.20 5 0 0 0.40 0.30 -5 0 0 0.00 0.20 -5 0 0 0.30 0.20 -5 0 0 4.60 2.30 -5 0 0 0.40 0.30 -5 0 0 -0.10 0.30 5 -1 0 118.19 3.60 5 -1 0 125.49 11.30 5 -1 0 117.69 3.70 5 1 0 118.39 3.80 5 1 0 125.59 11.80 5 -1 0 113.59 3.60 5 1 0 120.09 3.70 -5 -1 0 113.69 4.30 -5 1 0 109.89 3.90 -5 -1 0 120.29 5.60 -5 1 0 117.69 3.80 -5 -1 0 113.79 4.40 -5 -1 0 119.39 4.00 -5 -1 0 114.29 3.80 -5 -1 0 117.29 4.00 -5 1 0 123.29 3.90 -5 1 0 117.29 3.90 5 2 0 896.81 36.40 5 -2 0 873.71 34.10 5 -2 0 898.01 26.40 -5 -2 0 857.11 26.60 -5 2 0 865.01 26.60 -5 -2 0 877.31 27.20 -5 -2 0 881.31 27.90 5 3 0 133.09 15.10 5 3 0 130.19 4.30 5 3 0 130.69 4.30 5 -3 0 145.19 11.50 5 3 0 127.49 4.40 -5 3 0 128.99 4.40 -5 -3 0 131.69 4.30 -5 -3 0 130.89 5.00 -5 -3 0 129.19 4.50 -5 -3 0 129.09 6.00 -5 -3 0 132.19 4.40 -5 -3 0 127.79 4.50 -5 3 0 132.89 4.20 -5 3 0 135.79 4.40 -5 -3 0 134.79 4.50 -5 -3 0 128.59 4.30 5 4 0 29.20 1.30 5 4 0 16.90 11.10 5 4 0 32.70 1.50 5 4 0 29.40 1.40 5 4 0 32.90 1.50 5 -4 0 29.10 6.90 5 -4 0 30.40 17.40 5 4 0 33.00 1.40 -5 4 0 31.80 1.40 -5 4 0 29.20 1.40 -5 -4 0 33.70 1.60 -5 -4 0 30.00 1.40 -5 -4 0 29.80 1.30 -5 -4 0 30.40 1.90 -5 -4 0 26.20 2.90 -5 4 0 28.60 1.30 -5 -4 0 31.10 1.50 -5 4 0 32.00 1.30 -5 -4 0 33.60 1.50 -5 -4 0 30.80 1.50 -5 4 0 29.50 1.30 5 -5 0 206.88 23.70 5 5 0 213.18 7.20 5 5 0 221.18 7.10 5 5 0 229.18 7.20 5 5 0 243.88 26.30 5 5 0 225.58 7.30 5 5 0 229.48 7.30 5 -5 0 234.48 15.50 -5 -5 0 211.58 7.90 -5 -5 0 226.08 7.30 -5 -5 0 225.58 7.40 -5 -5 0 237.58 7.30 -5 5 0 222.28 7.10 -5 5 0 228.88 7.20 -5 5 0 203.68 7.20 -5 -5 0 220.68 7.10 -5 -5 0 224.98 9.10 -5 -5 0 221.78 7.20 -5 5 0 217.48 7.30 -5 5 0 228.58 7.20 -5 5 0 230.48 7.10 -5 -5 0 224.68 7.30 5 6 0 30.90 20.00 5 6 0 28.80 1.50 5 -6 0 2.20 34.50 5 -6 0 18.50 7.60 5 6 0 29.70 1.40 5 -6 0 26.40 1.50 5 6 0 28.90 1.40 5 -6 0 26.00 1.60 5 6 0 26.60 1.50 5 6 0 27.40 1.50 5 6 0 27.00 2.00 5 -6 0 27.80 1.60 5 -6 0 27.60 1.40 -5 -6 0 25.90 1.30 -5 -6 0 25.90 1.20 -5 -6 0 28.80 1.50 -5 -6 0 27.80 1.50 -5 -6 0 27.60 1.60 -5 -6 0 26.60 1.90 -5 6 0 25.30 1.40 -5 -6 0 25.40 3.20 -5 6 0 29.00 1.40 -5 -6 0 25.70 1.40 -5 -6 0 25.80 1.60 -5 6 0 28.60 1.30 -5 6 0 28.00 1.40 5 7 0 271.47 8.70 5 -7 0 253.27 9.10 5 7 0 270.77 8.50 5 -7 0 266.77 8.80 5 -7 0 257.87 8.60 5 7 0 260.37 8.60 5 -7 0 284.57 18.40 5 -7 0 257.27 8.50 5 7 0 264.87 8.60 5 7 0 239.78 35.00 5 -7 0 260.07 9.00 5 7 0 256.77 8.60 5 7 0 269.47 8.50 -5 -7 0 271.27 8.70 -5 -7 0 262.37 8.80 -5 -7 0 274.27 9.90 -5 7 0 266.97 8.40 -5 7 0 257.07 8.60 -5 7 0 247.48 8.50 -5 7 0 267.77 8.40 -5 7 0 273.77 8.60 -5 -7 0 266.87 9.40 -5 7 0 244.68 8.50 -5 -7 0 270.37 8.60 -5 -7 0 246.28 10.70 -5 -7 0 264.77 8.50 -5 -7 0 252.57 8.50 5 8 0 17.40 1.30 5 8 0 17.30 1.30 5 -8 0 17.10 1.20 5 -8 0 19.50 1.50 5 8 0 19.80 1.30 5 -8 0 18.80 1.50 5 -8 0 15.30 8.70 5 -8 0 18.10 1.30 5 8 0 18.30 1.10 5 8 0 19.60 1.30 5 -8 0 19.10 1.20 5 8 0 18.10 1.30 -5 -8 0 16.00 1.30 -5 -8 0 20.00 1.20 -5 -8 0 18.20 1.80 -5 8 0 19.20 1.10 -5 8 0 18.70 1.10 -5 -8 0 18.70 1.40 -5 8 0 18.20 1.50 -5 8 0 19.60 1.20 -5 8 0 19.30 1.30 -5 -8 0 20.00 1.40 -5 8 0 18.40 1.20 -5 -8 0 22.30 5.10 5 -9 0 6.10 9.40 5 -9 0 0.90 0.40 5 9 0 0.30 0.50 5 -9 0 1.10 0.50 5 -9 0 1.60 0.70 5 9 0 1.90 0.60 5 9 0 0.10 0.40 5 -9 0 0.40 0.70 5 9 0 0.60 0.60 5 9 0 0.80 0.50 5 9 0 0.60 0.40 -5 9 0 0.90 0.60 -5 9 0 1.30 0.50 -5 -9 0 1.00 0.90 -5 -9 0 -1.90 2.80 -5 -9 0 1.10 0.30 -5 9 0 0.20 0.60 -5 -9 0 0.50 0.50 -5 9 0 0.70 0.40 -5 9 0 0.50 0.50 -5 9 0 0.80 0.50 -5 -9 0 0.90 0.40 -5 -9 0 0.90 0.60 -5 -9 0 2.90 0.80 5 -10 0 9.00 1.20 5 10 0 9.90 1.10 5 10 0 7.10 1.00 5 10 0 7.50 1.00 5 10 0 9.30 0.90 5 -10 0 8.80 0.90 5 10 0 10.10 1.10 5 10 0 9.10 1.00 5 -10 0 10.90 1.20 5 -10 0 10.50 0.90 -5 -10 0 8.20 1.30 -5 -10 0 9.30 0.70 -5 10 0 10.40 1.10 -5 10 0 9.60 1.10 -5 -10 0 10.80 1.20 -5 10 0 10.20 0.90 -5 -10 0 9.50 1.00 -5 -10 0 15.10 5.70 -5 10 0 10.20 1.20 -5 10 0 10.00 1.00 5 11 0 4.70 0.80 5 -11 0 5.80 0.80 5 11 0 5.80 0.90 5 11 0 4.70 0.80 5 -11 0 5.60 1.00 5 -11 0 7.00 1.00 5 11 0 5.30 0.90 5 -11 0 7.10 0.70 5 11 0 5.70 0.70 -5 11 0 7.20 0.90 -5 11 0 7.70 0.80 -5 -11 0 5.60 0.90 -5 11 0 7.00 1.00 -5 -11 0 3.50 0.90 -5 -11 0 7.50 1.00 -5 11 0 5.90 0.90 -5 11 0 6.00 0.80 -5 -11 0 2.80 3.70 5 12 0 20.90 1.80 5 12 0 26.20 1.70 5 -12 0 26.90 1.80 5 -12 0 24.10 1.40 5 12 0 25.50 1.30 5 12 0 26.20 1.50 5 -12 0 27.90 1.60 -5 12 0 26.30 1.60 -5 -12 0 26.00 1.60 -5 12 0 26.50 1.40 -5 -12 0 28.50 1.60 -5 12 0 25.30 1.40 5 13 0 13.30 0.80 5 13 0 13.80 1.00 5 -13 0 13.10 1.00 5 -13 0 14.00 0.90 5 -13 0 14.70 1.20 -5 -13 0 13.60 1.00 -5 -13 0 13.10 1.00 -5 -13 0 14.30 1.00 -5 13 0 13.40 1.60 -5 13 0 13.30 0.90 -5 13 0 14.60 0.90 5 14 0 11.40 0.80 5 -14 0 10.40 0.70 5 -14 0 10.40 0.90 -5 14 0 11.10 0.70 -5 -14 0 11.80 0.80 -5 -14 0 11.20 0.80 -5 14 0 11.40 0.70 -5 -14 0 10.60 0.70 6 0 0 1063.89 33.30 6 0 0 1123.59 43.80 -6 0 0 1134.49 36.30 -6 0 0 1131.79 33.70 6 1 0 3.00 0.40 6 1 0 2.90 0.30 6 -1 0 2.40 0.30 6 -1 0 0.90 6.50 -6 1 0 3.50 0.50 -6 -1 0 2.40 0.40 -6 -1 0 2.90 0.50 -6 1 0 2.60 0.50 -6 -1 0 5.70 2.90 -6 -1 0 2.80 0.50 -6 1 0 2.20 0.40 -6 1 0 3.20 0.50 -6 -1 0 2.80 0.40 -6 -1 0 3.10 0.50 -6 1 0 2.50 0.40 6 2 0 90.09 2.90 6 2 0 86.29 3.10 6 -2 0 73.09 10.10 6 -2 0 91.39 2.70 6 -2 0 81.39 2.70 -6 -2 0 83.69 3.20 -6 -2 0 84.39 3.80 -6 -2 0 83.19 3.00 -6 -2 0 85.59 5.60 -6 -2 0 84.99 3.10 -6 2 0 86.89 3.00 -6 2 0 85.89 3.20 -6 2 0 83.19 3.00 -6 -2 0 84.39 3.20 -6 2 0 90.69 3.30 -6 2 0 85.49 3.10 -6 -2 0 90.79 3.10 -6 -2 0 84.69 3.20 6 3 0 79.59 18.70 6 3 0 49.70 1.80 6 3 0 49.40 1.90 6 -3 0 39.90 8.50 -6 -3 0 51.59 3.30 -6 -3 0 47.80 2.00 -6 -3 0 47.00 2.10 -6 3 0 44.40 2.00 -6 3 0 47.00 1.80 -6 -3 0 46.70 1.90 -6 3 0 47.60 2.00 -6 -3 0 46.30 1.90 -6 -3 0 51.79 4.70 -6 3 0 50.09 1.90 -6 -3 0 49.80 2.10 -6 -3 0 45.90 2.00 6 4 0 82.59 3.10 6 4 0 84.59 3.00 6 4 0 77.99 15.60 6 4 0 76.99 2.80 6 -4 0 87.29 3.70 6 -4 0 80.29 10.90 6 4 0 78.79 2.90 -6 -4 0 76.99 2.90 -6 -4 0 81.29 3.10 -6 -4 0 80.39 3.10 -6 4 0 79.49 2.80 -6 4 0 81.69 3.00 -6 -4 0 79.89 3.10 -6 -4 0 78.39 3.70 -6 -4 0 75.19 5.30 -6 4 0 77.49 2.80 -6 4 0 80.19 3.00 -6 -4 0 75.69 2.90 -6 -4 0 83.29 3.10 6 -5 0 121.89 4.30 6 -5 0 125.49 4.60 6 -5 0 124.69 4.40 6 -5 0 128.19 13.90 6 5 0 126.09 4.30 6 5 0 123.09 4.20 6 5 0 115.09 20.50 6 5 0 125.89 4.40 6 5 0 126.79 4.50 6 5 0 121.29 4.30 -6 -5 0 124.99 4.40 -6 5 0 114.59 4.50 -6 -5 0 118.59 4.60 -6 -5 0 124.59 4.20 -6 -5 0 119.09 4.30 -6 5 0 125.59 4.20 -6 -5 0 119.59 5.10 -6 5 0 143.09 5.30 -6 5 0 126.79 4.20 -6 5 0 120.89 4.60 -6 -5 0 125.09 4.50 -6 5 0 123.89 4.40 -6 -5 0 121.09 4.60 -6 -5 0 120.29 9.70 -6 -5 0 124.59 4.40 6 -6 0 9.90 1.10 6 6 0 5.90 0.80 6 6 0 7.70 0.80 6 -6 0 9.50 0.90 6 -6 0 9.10 1.10 6 6 0 8.80 0.90 6 -6 0 7.60 0.80 6 6 0 7.10 0.80 6 6 0 9.00 0.70 6 -6 0 -0.10 7.60 6 -6 0 9.90 1.10 6 6 0 18.90 21.50 6 6 0 8.40 0.80 6 6 0 8.70 0.90 -6 -6 0 7.80 0.90 -6 -6 0 8.20 1.20 -6 6 0 7.80 0.70 -6 6 0 8.90 0.90 -6 6 0 8.30 0.90 -6 -6 0 8.60 2.90 -6 -6 0 8.50 1.00 -6 -6 0 8.10 0.80 -6 -6 0 8.10 0.80 -6 6 0 8.40 0.70 -6 -6 0 8.30 0.90 -6 6 0 10.70 0.90 -6 -6 0 8.40 0.70 -6 -6 0 7.20 0.90 -6 6 0 9.20 0.90 6 -7 0 64.49 2.90 6 -7 0 63.29 2.60 6 7 0 63.69 2.60 6 7 0 64.89 2.70 6 7 0 61.19 2.70 6 7 0 63.99 2.70 6 7 0 64.79 2.80 6 -7 0 67.49 3.00 6 -7 0 60.09 11.00 6 7 0 64.59 2.50 6 7 0 42.20 29.60 6 7 0 58.69 2.60 6 -7 0 61.29 2.90 6 -7 0 62.19 2.70 -6 7 0 64.09 2.70 -6 7 0 60.39 3.10 -6 7 0 63.79 2.50 -6 -7 0 71.69 2.70 -6 -7 0 63.49 2.80 -6 7 0 60.09 2.60 -6 -7 0 68.19 2.60 -6 -7 0 53.99 6.00 -6 -7 0 69.39 2.70 -6 7 0 65.89 2.50 -6 7 0 57.99 2.60 -6 -7 0 64.29 2.80 -6 -7 0 64.49 3.50 -6 -7 0 64.99 2.90 6 8 0 0.20 0.40 6 -8 0 0.30 0.60 6 8 0 0.70 0.40 6 8 0 0.20 0.50 6 8 0 0.00 0.50 6 -8 0 0.60 0.60 6 -8 0 0.70 0.60 6 8 0 0.70 0.40 6 -8 0 0.10 0.30 6 -8 0 0.00 0.40 6 8 0 0.40 0.50 6 -8 0 -12.40 9.20 -6 -8 0 0.00 0.50 -6 8 0 1.10 0.50 -6 8 0 0.80 0.40 -6 -8 0 -0.90 3.50 -6 -8 0 0.20 0.50 -6 8 0 0.00 0.40 -6 8 0 0.10 0.40 -6 -8 0 0.70 0.90 -6 8 0 0.50 0.50 -6 -8 0 0.20 0.50 -6 8 0 0.00 0.50 -6 -8 0 0.40 0.40 6 9 0 19.70 1.50 6 -9 0 20.90 1.60 6 -9 0 22.10 1.70 6 -9 0 18.50 1.20 6 -9 0 11.20 10.20 6 9 0 19.60 1.20 6 9 0 21.80 1.40 6 9 0 21.90 1.50 6 9 0 23.60 1.60 6 9 0 21.00 1.50 6 -9 0 19.90 1.50 6 -9 0 18.90 1.40 -6 -9 0 20.70 1.60 -6 -9 0 23.30 2.80 -6 -9 0 21.40 1.50 -6 9 0 21.50 1.40 -6 9 0 20.40 1.40 -6 -9 0 20.40 1.00 -6 9 0 22.30 1.30 -6 -9 0 19.30 4.40 -6 9 0 21.60 1.30 -6 -9 0 21.10 1.60 -6 9 0 23.30 1.50 -6 -9 0 22.00 1.30 6 10 0 354.26 11.30 6 -10 0 340.17 12.20 6 -10 0 344.17 11.20 6 10 0 345.17 11.00 6 10 0 345.57 11.50 6 10 0 345.17 11.50 6 -10 0 351.36 11.30 6 -10 0 352.66 11.50 6 -10 0 349.67 11.70 -6 10 0 358.16 11.10 -6 10 0 327.17 11.50 -6 -10 0 350.36 11.50 -6 10 0 341.07 11.20 -6 -10 0 352.86 11.10 -6 10 0 353.16 12.30 -6 -10 0 354.16 12.60 -6 -10 0 320.57 14.80 -6 -10 0 353.36 11.40 -6 10 0 353.66 11.40 6 -11 0 61.59 2.10 6 -11 0 61.49 2.80 6 -11 0 58.99 3.00 6 11 0 64.19 2.70 6 11 0 60.99 2.80 6 11 0 60.19 2.40 6 -11 0 62.39 2.60 -6 -11 0 57.29 6.40 -6 -11 0 64.09 2.80 -6 -11 0 63.49 2.80 -6 11 0 63.69 2.50 -6 11 0 64.49 2.60 -6 11 0 66.49 2.80 6 12 0 11.60 1.00 6 -12 0 12.30 1.10 6 12 0 11.30 1.30 6 12 0 12.30 1.50 6 -12 0 12.00 1.00 6 -12 0 9.60 1.10 -6 12 0 11.80 0.90 -6 12 0 11.40 0.90 -6 -12 0 9.20 0.90 -6 -12 0 9.50 0.90 6 -13 0 0.90 0.40 6 -13 0 0.10 0.30 6 13 0 0.50 0.40 6 -13 0 0.40 0.40 -6 13 0 0.90 0.30 -6 -13 0 1.10 0.50 -6 -13 0 0.70 0.40 -6 -13 0 1.30 0.40 7 0 0 0.00 8.90 7 0 0 0.70 0.40 7 0 0 0.10 0.20 7 0 0 1.20 0.60 7 0 0 0.10 0.40 -7 0 0 0.50 0.40 -7 0 0 -0.10 0.30 -7 0 0 0.00 0.30 -7 0 0 -0.20 0.20 -7 0 0 0.40 0.30 7 1 0 2.00 0.60 7 1 0 -5.90 8.60 7 -1 0 2.20 0.60 7 1 0 1.50 0.30 7 -1 0 1.80 0.20 7 -1 0 1.60 0.50 7 1 0 2.80 0.40 7 1 0 1.60 0.50 7 1 0 1.40 0.50 7 -1 0 1.50 0.50 7 -1 0 2.20 0.70 7 -1 0 1.40 7.90 -7 1 0 2.10 0.40 -7 -1 0 2.50 0.50 -7 -1 0 2.00 0.50 -7 1 0 1.40 0.50 -7 1 0 1.90 0.50 -7 -1 0 2.20 0.50 -7 1 0 2.10 0.40 -7 -1 0 1.70 0.40 -7 -1 0 1.80 0.40 -7 -1 0 2.40 0.60 7 -2 0 70.89 2.90 7 -2 0 72.29 3.00 7 2 0 70.79 2.90 7 -2 0 68.49 3.00 7 2 0 64.69 13.50 7 2 0 72.69 2.60 7 2 0 70.79 2.90 7 -2 0 63.49 10.90 7 -2 0 70.29 2.90 7 2 0 73.39 2.40 7 -2 0 67.69 2.80 7 2 0 70.09 2.90 -7 -2 0 71.29 2.70 -7 -2 0 74.49 2.90 -7 -2 0 70.49 2.80 -7 -2 0 71.89 2.70 -7 2 0 70.59 2.60 -7 -2 0 66.79 2.90 -7 2 0 68.99 2.90 -7 2 0 73.39 2.80 -7 -2 0 69.49 2.80 -7 2 0 69.49 2.80 -7 -2 0 70.79 2.90 -7 2 0 70.29 2.60 7 -3 0 35.10 1.70 7 3 0 32.80 1.60 7 -3 0 31.60 1.70 7 -3 0 40.90 2.50 7 -3 0 36.80 1.90 7 3 0 34.80 1.50 7 3 0 44.40 14.00 7 -3 0 30.60 9.30 7 3 0 41.10 2.40 7 3 0 32.80 1.70 -7 -3 0 33.80 1.90 -7 3 0 31.60 1.60 -7 -3 0 34.10 4.90 -7 -3 0 35.50 1.60 -7 -3 0 34.40 1.80 -7 -3 0 34.50 1.70 -7 -3 0 34.40 1.80 -7 3 0 35.60 1.50 -7 3 0 33.60 1.80 -7 3 0 33.40 1.50 7 -4 0 3.90 0.70 7 -4 0 17.60 8.70 7 4 0 4.00 0.80 7 -4 0 3.20 0.70 7 -4 0 4.10 0.60 7 4 0 3.00 0.50 7 4 0 3.20 0.60 7 4 0 6.90 16.20 7 -4 0 3.40 0.60 7 4 0 2.90 0.50 7 -4 0 4.60 0.70 7 4 0 3.30 0.60 7 4 0 2.50 0.70 -7 4 0 2.70 0.50 -7 -4 0 1.00 4.10 -7 4 0 2.00 0.60 -7 -4 0 2.90 0.60 -7 4 0 3.00 0.50 -7 -4 0 3.50 0.70 -7 -4 0 3.40 0.70 -7 -4 0 2.70 0.70 -7 4 0 3.00 0.60 -7 -4 0 4.60 0.70 -7 4 0 2.50 0.50 -7 -4 0 3.30 0.50 -7 -4 0 4.10 0.60 -7 4 0 3.00 0.60 7 -5 0 7.60 0.90 7 5 0 6.30 0.80 7 -5 0 6.20 0.80 7 -5 0 7.00 0.80 7 5 0 5.00 19.20 7 5 0 5.40 0.70 7 -5 0 7.00 0.80 7 -5 0 6.20 0.90 7 -5 0 7.50 1.00 7 5 0 6.40 0.70 7 5 0 6.70 0.80 7 5 0 6.60 0.60 -7 5 0 5.70 0.70 -7 -5 0 9.60 4.20 -7 -5 0 5.40 0.80 -7 5 0 6.10 0.80 -7 5 0 6.20 0.70 -7 -5 0 6.60 0.80 -7 -5 0 5.50 0.70 -7 -5 0 7.60 1.00 -7 5 0 7.30 0.80 -7 -5 0 5.80 0.60 -7 -5 0 5.90 0.90 -7 -5 0 5.20 0.70 -7 5 0 7.50 0.70 7 6 0 109.89 3.90 7 6 0 102.29 4.00 7 -6 0 102.69 3.80 7 6 0 98.59 3.80 7 -6 0 105.29 4.20 7 6 0 76.99 28.10 7 -6 0 102.99 4.10 7 -6 0 104.59 4.00 7 6 0 102.29 3.90 7 -6 0 96.79 13.20 7 6 0 100.39 3.60 7 6 0 92.89 4.30 7 -6 0 107.59 4.10 7 6 0 101.69 3.70 -7 6 0 98.19 3.80 -7 -6 0 103.69 4.00 -7 6 0 105.29 3.70 -7 6 0 98.59 3.90 -7 6 0 106.29 3.70 -7 -6 0 101.89 4.00 -7 -6 0 111.79 8.30 -7 6 0 106.29 3.90 -7 -6 0 104.19 4.10 -7 -6 0 100.59 3.90 -7 -6 0 103.89 4.20 -7 -6 0 103.39 3.60 -7 -6 0 105.49 4.00 7 7 0 1.90 0.60 7 7 0 1.60 0.60 7 -7 0 1.90 0.70 7 -7 0 1.80 0.60 7 7 0 1.50 0.40 7 7 0 1.80 0.50 7 -7 0 1.90 0.50 7 -7 0 2.50 0.60 7 -7 0 -6.40 9.40 7 7 0 1.30 0.50 7 -7 0 1.50 0.60 7 7 0 41.70 35.10 7 7 0 0.90 0.50 -7 7 0 0.80 0.50 -7 -7 0 1.10 0.60 -7 7 0 1.50 0.50 -7 -7 0 2.70 0.70 -7 -7 0 0.90 1.10 -7 -7 0 0.40 0.30 -7 -7 0 2.60 0.70 -7 -7 0 -0.10 4.60 -7 7 0 1.00 0.60 -7 -7 0 1.20 0.50 -7 7 0 1.70 0.50 7 -8 0 22.10 1.60 7 8 0 22.20 1.60 7 8 0 25.70 1.50 7 8 0 20.00 1.20 7 -8 0 23.40 1.50 7 -8 0 22.50 1.30 7 -8 0 23.50 1.70 7 -8 0 20.50 10.80 7 8 0 22.80 1.40 7 -8 0 24.10 1.70 7 8 0 21.60 1.40 -7 -8 0 22.80 1.40 -7 -8 0 21.40 1.50 -7 -8 0 23.40 1.30 -7 8 0 23.30 1.40 -7 -8 0 22.30 5.60 -7 -8 0 21.10 1.60 -7 -8 0 22.30 1.70 -7 8 0 22.50 1.40 -7 8 0 21.40 1.40 -7 8 0 20.60 1.30 7 9 0 4.30 0.60 7 -9 0 5.10 0.80 7 -9 0 4.00 0.90 7 9 0 5.90 0.90 7 9 0 5.40 0.90 7 -9 0 5.80 0.60 7 9 0 4.60 0.70 7 -9 0 4.80 0.90 7 -9 0 4.30 0.80 7 9 0 5.10 0.70 -7 -9 0 2.80 0.70 -7 9 0 6.10 0.80 -7 9 0 4.20 0.70 -7 9 0 5.20 0.70 -7 -9 0 6.70 1.40 -7 -9 0 3.70 0.60 -7 -9 0 6.30 1.00 -7 9 0 4.80 0.80 -7 -9 0 4.80 0.90 -7 -9 0 11.60 5.30 7 -10 0 3.80 0.70 7 10 0 5.40 0.80 7 -10 0 4.10 0.80 7 -10 0 5.20 0.80 7 -10 0 5.00 0.50 7 10 0 3.90 0.70 7 -10 0 4.90 0.90 -7 -10 0 4.20 6.10 -7 10 0 4.40 0.70 -7 -10 0 2.90 0.70 -7 -10 0 4.40 0.80 -7 10 0 3.90 0.60 7 11 0 0.90 0.60 7 -11 0 0.50 0.40 7 -11 0 -0.10 0.50 7 11 0 0.30 0.40 7 -11 0 1.00 0.60 -7 -11 0 0.00 0.40 -7 11 0 0.00 0.30 -7 11 0 0.60 0.50 -7 -11 0 0.30 0.40 7 12 0 13.60 1.40 7 -12 0 11.30 0.80 7 -12 0 11.60 1.00 7 -12 0 9.70 1.00 -7 12 0 11.90 0.80 -7 12 0 11.00 0.80 -7 -12 0 8.00 0.80 -7 -12 0 10.40 1.10 7 13 0 8.20 0.70 -7 -13 0 8.70 0.70 -7 13 0 7.60 0.60 -7 -13 0 8.20 0.60 -7 -13 0 6.90 0.70 8 0 0 0.80 0.50 8 0 0 -0.10 0.50 8 0 0 -3.70 10.20 8 0 0 0.20 0.40 8 0 0 -0.10 0.40 8 0 0 -0.30 0.40 8 0 0 0.10 0.20 -8 0 0 0.30 0.30 -8 0 0 0.20 0.40 -8 0 0 0.00 0.40 -8 0 0 1.00 0.50 -8 0 0 -0.10 0.40 8 -1 0 26.50 1.60 8 -1 0 30.00 11.40 8 1 0 28.70 1.70 8 -1 0 24.70 1.70 8 -1 0 26.70 1.50 8 1 0 32.20 13.00 8 1 0 24.30 1.50 8 1 0 26.00 1.30 8 1 0 26.20 1.60 8 -1 0 26.70 1.60 8 -1 0 27.70 1.60 8 1 0 25.10 1.60 8 1 0 27.30 1.10 -8 -1 0 25.40 1.40 -8 1 0 25.00 1.30 -8 1 0 24.20 2.10 -8 1 0 26.30 1.60 -8 -1 0 24.80 1.60 -8 1 0 23.00 1.50 -8 -1 0 26.70 1.60 -8 1 0 26.20 1.40 -8 -1 0 23.30 1.50 -8 -1 0 25.80 1.40 -8 1 0 25.80 1.50 -8 -1 0 25.40 1.50 8 -2 0 0.70 0.50 8 2 0 0.70 0.30 8 -2 0 1.50 0.50 8 2 0 1.10 0.40 8 2 0 9.20 13.70 8 2 0 1.00 0.50 8 -2 0 -5.10 9.20 8 -2 0 0.70 0.50 8 2 0 0.70 0.50 8 -2 0 0.60 0.50 8 2 0 0.60 0.50 8 2 0 0.70 0.50 8 -2 0 2.10 0.60 -8 -2 0 1.20 0.70 -8 -2 0 1.80 0.50 -8 2 0 1.30 0.50 -8 -2 0 1.40 0.50 -8 -2 0 1.10 0.50 -8 -2 0 1.20 0.40 -8 2 0 1.60 0.60 -8 -2 0 0.40 0.40 -8 2 0 1.00 0.40 -8 -2 0 0.20 0.40 -8 -2 0 0.70 0.40 -8 2 0 1.10 0.40 8 -3 0 434.96 14.00 8 3 0 444.66 13.40 8 -3 0 460.45 14.00 8 3 0 445.96 13.60 8 -3 0 461.95 26.80 8 3 0 436.56 14.10 8 3 0 436.06 14.00 8 3 0 437.56 14.20 8 -3 0 438.26 14.10 8 3 0 435.36 13.80 8 3 0 419.96 14.10 8 3 0 410.56 34.70 8 -3 0 441.76 14.30 8 -3 0 447.06 14.00 -8 -3 0 420.96 14.20 -8 -3 0 442.36 13.80 -8 3 0 430.66 14.10 -8 3 0 439.06 14.00 -8 3 0 435.66 14.00 -8 3 0 450.25 14.00 -8 -3 0 437.56 14.00 -8 -3 0 424.16 14.00 -8 -3 0 446.16 13.90 -8 -3 0 443.36 14.00 -8 -3 0 455.85 14.10 -8 3 0 449.46 13.70 -8 -3 0 433.66 14.10 -8 3 0 452.85 13.80 8 4 0 8.90 1.00 8 -4 0 7.90 0.90 8 4 0 7.00 0.70 8 4 0 7.50 0.60 8 4 0 8.50 0.90 8 -4 0 6.20 9.90 8 -4 0 8.00 1.00 8 -4 0 7.40 1.00 8 -4 0 7.50 0.90 8 -4 0 8.90 0.90 8 4 0 7.00 0.90 -8 -4 0 9.40 1.00 -8 -4 0 6.50 0.90 -8 -4 0 9.20 1.10 -8 4 0 8.50 0.90 -8 4 0 6.50 1.10 -8 4 0 7.50 0.70 -8 -4 0 8.80 0.80 -8 4 0 8.10 0.80 -8 4 0 9.60 1.00 -8 -4 0 7.30 0.80 -8 4 0 8.60 1.00 -8 -4 0 6.00 0.90 -8 -4 0 6.90 0.90 8 5 0 67.19 22.90 8 5 0 31.80 2.30 8 -5 0 34.30 2.10 8 -5 0 34.00 1.70 8 -5 0 36.40 2.30 8 -5 0 34.30 1.90 8 5 0 34.10 1.50 8 -5 0 25.70 10.70 8 -5 0 34.90 2.10 8 5 0 35.50 1.70 8 -5 0 33.80 2.10 8 5 0 37.00 2.60 -8 5 0 35.30 1.70 -8 5 0 33.40 1.90 -8 -5 0 32.70 1.90 -8 -5 0 31.10 1.60 -8 -5 0 34.00 2.00 -8 -5 0 34.70 1.80 -8 5 0 35.50 1.90 -8 5 0 33.50 1.80 -8 5 0 36.00 1.70 -8 -5 0 34.00 2.10 -8 -5 0 34.60 1.90 8 -6 0 29.30 11.30 8 -6 0 29.90 1.80 8 6 0 10.00 30.80 8 -6 0 31.30 2.00 8 6 0 31.90 1.60 8 6 0 33.20 1.70 8 6 0 32.50 1.80 8 -6 0 32.00 1.90 8 -6 0 34.30 2.10 8 6 0 31.50 1.70 8 -6 0 32.70 1.70 -8 -6 0 30.00 2.30 -8 6 0 30.00 1.90 -8 6 0 32.10 1.80 -8 6 0 31.40 1.80 -8 -6 0 32.80 1.90 -8 6 0 33.70 1.80 -8 -6 0 31.70 1.50 -8 -6 0 33.10 2.00 -8 -6 0 22.50 2.10 8 7 0 381.06 12.10 8 -7 0 384.56 12.70 8 7 0 377.86 52.49 8 -7 0 388.66 24.60 8 -7 0 383.56 12.40 8 7 0 374.46 12.20 8 7 0 388.16 12.30 8 7 0 381.46 12.30 8 -7 0 379.76 12.60 8 -7 0 396.66 12.60 8 -7 0 387.06 12.20 -8 7 0 395.96 12.20 -8 7 0 381.06 12.40 -8 -7 0 372.76 12.30 -8 -7 0 391.46 12.50 -8 7 0 370.76 12.30 -8 -7 0 376.66 12.70 -8 -7 0 393.76 12.70 -8 7 0 383.76 12.20 -8 -7 0 394.46 12.50 8 -8 0 51.39 14.20 8 8 0 62.19 2.70 8 -8 0 62.29 3.00 8 8 0 61.69 2.60 8 -8 0 67.89 3.00 8 -8 0 61.39 3.00 8 -8 0 65.69 2.80 8 8 0 65.89 2.70 8 -8 0 65.79 2.50 8 -8 0 45.70 9.60 -8 -8 0 64.89 3.00 -8 -8 0 61.39 2.70 -8 8 0 66.19 2.90 -8 8 0 60.19 2.80 -8 -8 0 62.39 2.90 -8 8 0 66.89 2.60 -8 -8 0 66.99 3.30 -8 8 0 63.59 2.70 -8 -8 0 61.69 2.70 8 -9 0 45.70 2.40 8 -9 0 43.60 2.10 8 -9 0 45.30 2.30 8 -9 0 44.30 2.30 8 -9 0 44.90 1.70 8 9 0 44.60 2.10 8 9 0 48.70 2.20 -8 -9 0 46.50 2.10 -8 9 0 42.10 2.10 -8 -9 0 48.90 2.40 -8 -9 0 48.70 2.30 -8 9 0 44.90 2.00 8 10 0 42.30 2.00 8 -10 0 41.80 2.10 8 -10 0 43.70 2.10 8 10 0 43.80 2.00 8 -10 0 42.70 2.20 8 -10 0 41.30 1.90 -8 -10 0 44.00 2.10 -8 10 0 44.30 1.90 -8 -10 0 41.60 2.20 -8 -10 0 39.10 1.70 -8 10 0 43.70 2.00 8 -11 0 -0.10 0.40 8 -11 0 -0.10 0.30 8 11 0 0.40 0.50 -8 -11 0 0.10 0.40 -8 -11 0 0.00 0.30 -8 11 0 0.30 0.30 -8 11 0 0.20 0.30 8 -12 0 0.40 0.40 8 12 0 0.60 0.30 8 12 0 0.50 0.40 8 -12 0 0.70 0.30 -8 12 0 0.70 0.30 -8 12 0 1.10 0.30 -8 -12 0 0.40 0.30 -8 -12 0 0.40 0.30 9 0 0 -0.20 0.80 9 0 0 -23.80 12.50 9 0 0 0.80 0.60 9 0 0 0.10 0.60 -9 0 0 -0.20 0.50 -9 0 0 -0.30 0.40 -9 0 0 -0.50 0.40 -9 0 0 0.60 0.50 -9 0 0 0.40 0.50 -9 0 0 0.30 0.50 -9 0 0 -0.20 0.30 9 1 0 111.09 3.50 9 1 0 102.29 4.50 9 -1 0 112.39 4.30 9 1 0 115.49 4.60 9 1 0 110.09 4.40 9 -1 0 69.79 15.30 9 -1 0 112.19 5.30 9 1 0 103.69 3.80 9 1 0 121.99 19.20 -9 1 0 110.29 4.20 -9 -1 0 104.69 4.20 -9 -1 0 112.29 4.00 -9 -1 0 104.89 4.20 -9 1 0 102.29 4.20 -9 1 0 107.69 4.20 -9 -1 0 109.89 4.00 -9 -1 0 114.99 4.90 -9 1 0 115.59 4.00 -9 -1 0 105.89 4.20 -9 -1 0 108.19 4.20 -9 1 0 109.99 4.00 9 2 0 35.40 16.70 9 -2 0 19.30 1.40 9 2 0 21.40 1.50 9 2 0 18.40 1.80 9 2 0 20.90 1.40 9 -2 0 23.50 2.20 9 -2 0 19.50 12.10 9 -2 0 21.30 1.50 9 2 0 20.40 1.00 9 2 0 20.70 1.20 9 -2 0 21.60 1.60 9 2 0 19.50 1.50 9 -2 0 20.60 1.40 -9 -2 0 20.10 1.50 -9 2 0 18.70 1.30 -9 -2 0 20.70 1.30 -9 -2 0 20.20 1.30 -9 -2 0 21.60 1.50 -9 2 0 23.00 2.10 -9 -2 0 17.90 1.50 -9 2 0 18.70 1.40 -9 -2 0 21.30 1.60 -9 -2 0 20.40 1.50 -9 2 0 18.30 1.40 -9 2 0 16.90 1.30 -9 -2 0 20.00 1.50 -9 2 0 20.40 1.30 9 -3 0 32.50 2.00 9 3 0 33.00 1.90 9 3 0 33.90 2.00 9 3 0 35.00 1.90 9 -3 0 34.80 2.00 9 3 0 36.60 2.00 9 3 0 29.30 18.90 9 3 0 35.10 2.00 9 -3 0 33.70 1.80 9 -3 0 35.40 2.10 9 -3 0 21.70 12.40 9 -3 0 33.30 1.80 9 3 0 34.70 1.50 -9 3 0 33.00 1.90 -9 -3 0 32.70 1.70 -9 -3 0 31.70 1.90 -9 -3 0 34.10 2.10 -9 -3 0 31.30 1.80 -9 3 0 34.10 1.90 -9 3 0 33.70 1.80 -9 -3 0 34.90 2.00 -9 3 0 32.00 1.80 -9 3 0 34.30 1.70 -9 3 0 34.00 1.70 -9 -3 0 33.90 1.90 -9 -3 0 33.30 1.90 9 -4 0 48.00 2.20 9 4 0 54.89 22.50 9 4 0 46.60 2.50 9 4 0 44.90 2.30 9 4 0 44.70 1.90 9 4 0 42.70 2.00 9 -4 0 45.10 2.50 9 -4 0 47.70 2.20 9 -4 0 47.80 2.40 9 -4 0 47.90 2.50 9 -4 0 40.60 12.90 -9 -4 0 43.50 2.30 -9 -4 0 45.80 2.40 -9 -4 0 48.40 2.60 -9 -4 0 46.60 2.20 -9 -4 0 44.10 2.50 -9 4 0 43.90 2.10 -9 4 0 47.50 2.30 -9 4 0 47.80 2.50 -9 4 0 44.50 2.30 -9 -4 0 44.30 2.50 -9 4 0 42.00 2.20 9 -5 0 124.39 16.10 9 -5 0 128.39 4.60 9 -5 0 130.69 5.10 9 5 0 60.69 29.00 9 -5 0 129.79 5.00 9 -5 0 130.09 4.80 9 -5 0 123.49 4.60 9 5 0 124.59 4.50 9 5 0 119.09 4.10 9 5 0 127.79 4.40 9 5 0 130.39 4.70 -9 5 0 123.59 4.70 -9 -5 0 133.69 4.90 -9 -5 0 123.99 4.40 -9 -5 0 125.89 4.80 -9 5 0 123.89 4.70 -9 5 0 131.99 4.60 -9 -5 0 128.29 4.90 -9 5 0 119.69 4.80 -9 -5 0 132.09 5.10 -9 5 0 131.99 4.50 -9 -5 0 129.49 5.00 -9 -5 0 127.39 4.80 9 -6 0 103.19 14.70 9 6 0 106.49 4.00 9 6 0 105.89 37.20 9 -6 0 115.09 4.40 9 -6 0 105.99 4.20 9 6 0 106.59 4.10 9 -6 0 113.49 4.00 9 -6 0 107.89 4.50 9 6 0 108.99 3.90 9 6 0 102.39 3.60 -9 6 0 104.39 4.80 -9 -6 0 115.79 4.50 -9 -6 0 108.69 4.30 -9 6 0 112.99 4.00 -9 6 0 106.79 4.20 -9 6 0 114.19 4.10 -9 -6 0 106.79 4.40 -9 6 0 106.29 4.20 -9 -6 0 113.99 4.30 -9 -6 0 107.29 4.20 -9 -6 0 103.69 3.80 9 -7 0 -0.10 0.30 9 7 0 0.50 0.30 9 7 0 0.50 0.40 9 -7 0 3.90 13.60 9 7 0 0.50 0.40 9 -7 0 -1.30 9.50 9 -7 0 0.80 0.70 9 7 0 65.39 52.89 9 -7 0 1.10 0.90 -9 -7 0 0.10 0.40 -9 -7 0 0.10 0.50 -9 -7 0 1.00 0.60 -9 7 0 -0.10 0.50 -9 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26.90 1.70 10 1 0 17.40 18.00 10 -1 0 26.50 1.90 10 -1 0 26.40 1.70 10 1 0 24.90 1.70 10 1 0 29.90 1.90 10 1 0 26.10 1.70 -10 1 0 29.20 1.60 -10 1 0 27.00 1.80 -10 -1 0 26.60 1.60 -10 -1 0 26.80 1.80 -10 -1 0 25.30 1.70 -10 -1 0 24.90 1.70 -10 1 0 29.10 1.60 -10 1 0 24.20 1.70 -10 -1 0 26.90 1.70 -10 1 0 26.90 1.80 -10 1 0 25.70 1.60 -10 1 0 29.10 1.80 -10 -1 0 27.80 1.80 -10 -1 0 26.20 1.50 10 -2 0 6.90 0.90 10 2 0 5.30 0.90 10 2 0 -11.10 19.50 10 -2 0 5.90 1.00 10 -2 0 6.30 0.90 10 2 0 6.70 1.00 10 2 0 8.30 1.10 10 -2 0 7.20 0.90 10 2 0 5.50 0.80 10 -2 0 6.40 1.00 10 -2 0 11.30 14.50 -10 -2 0 5.50 0.90 -10 2 0 6.30 0.90 -10 -2 0 7.10 1.10 -10 -2 0 6.50 1.00 -10 2 0 6.50 0.80 -10 2 0 6.30 0.90 -10 2 0 7.10 1.00 -10 -2 0 6.20 0.90 -10 2 0 5.30 0.70 -10 -2 0 6.90 0.80 -10 2 0 6.20 1.00 -10 -2 0 4.90 0.80 -10 -2 0 6.40 0.90 -10 -2 0 6.40 0.90 10 3 0 6.70 0.70 10 -3 0 4.80 0.90 10 -3 0 7.10 0.90 10 3 0 8.60 1.10 10 -3 0 4.70 0.90 10 -3 0 4.90 0.80 10 -3 0 5.00 0.80 10 3 0 5.60 0.90 -10 3 0 5.70 0.80 -10 -3 0 6.00 0.90 -10 -3 0 5.20 0.70 -10 3 0 5.80 0.80 -10 3 0 7.20 1.00 -10 3 0 5.40 0.80 -10 -3 0 3.20 0.80 -10 -3 0 7.50 0.90 -10 -3 0 6.80 1.00 -10 -3 0 6.10 1.00 -10 3 0 5.70 0.90 -10 -3 0 5.40 0.90 10 -4 0 28.10 13.80 10 -4 0 19.00 1.60 10 -4 0 19.60 1.60 10 -4 0 22.50 1.40 10 4 0 23.50 1.50 10 -4 0 22.50 1.60 10 4 0 19.70 0.90 10 4 0 19.80 1.20 10 4 0 -2.10 26.40 10 -4 0 21.40 1.40 -10 4 0 20.00 1.40 -10 -4 0 19.40 1.60 -10 -4 0 19.40 1.50 -10 -4 0 19.80 1.30 -10 -4 0 21.00 1.50 -10 4 0 21.10 1.50 -10 4 0 19.80 1.60 -10 -4 0 21.30 1.60 -10 -4 0 22.30 1.60 -10 4 0 19.90 1.30 -10 4 0 20.20 1.50 -10 -4 0 20.30 1.50 10 5 0 352.56 11.00 10 5 0 350.86 44.00 10 -5 0 317.27 26.70 10 5 0 374.06 12.30 10 5 0 356.76 11.20 10 -5 0 369.96 11.50 10 -5 0 358.76 11.40 -10 5 0 356.56 12.00 -10 -5 0 348.17 11.80 -10 -5 0 351.66 11.20 -10 5 0 370.26 12.30 -10 5 0 332.97 12.10 -10 5 0 354.56 11.80 -10 5 0 371.56 11.40 -10 -5 0 368.36 11.70 -10 -5 0 346.27 11.60 -10 -5 0 333.47 11.80 10 -6 0 5.70 0.60 10 6 0 4.90 0.70 10 -6 0 4.40 0.90 10 -6 0 4.70 0.80 10 6 0 3.50 0.60 10 6 0 -2.80 49.60 10 6 0 4.30 0.50 10 -6 0 4.90 0.90 -10 -6 0 4.50 0.80 -10 -6 0 3.10 0.70 -10 6 0 3.10 0.60 -10 -6 0 2.60 0.70 -10 6 0 4.60 0.80 10 -7 0 0.10 0.50 10 -7 0 0.10 0.20 10 7 0 0.10 0.30 10 7 0 0.20 0.40 10 -7 0 -0.20 0.40 10 7 0 0.30 0.30 10 -7 0 -0.30 0.50 -10 -7 0 0.30 0.40 -10 7 0 0.20 0.40 -10 7 0 0.40 0.40 -10 -7 0 0.10 0.40 -10 -7 0 -0.50 0.40 10 8 0 73.49 2.80 10 -8 0 78.09 3.20 10 -8 0 77.89 3.10 10 8 0 80.49 3.10 10 -8 0 80.09 3.20 -10 8 0 76.49 3.20 -10 -8 0 78.19 3.30 -10 8 0 82.39 3.00 -10 -8 0 79.69 3.20 10 9 0 14.80 0.90 10 -9 0 13.20 1.00 10 -9 0 14.10 1.00 -10 -9 0 13.20 1.00 -10 -9 0 14.70 1.10 -10 9 0 15.60 1.00 -10 9 0 14.20 0.90 10 -10 0 0.30 0.30 10 -10 0 -0.40 0.20 10 -10 0 0.50 0.40 10 10 0 0.40 0.30 -10 -10 0 0.00 0.30 -10 10 0 0.20 0.20 -10 -10 0 0.00 0.30 -10 10 0 -0.10 0.30 11 0 0 -0.60 0.40 11 0 0 -0.80 0.60 11 0 0 0.40 0.70 11 0 0 -0.20 0.50 11 0 0 -9.30 19.10 -11 0 0 0.30 0.40 -11 0 0 -0.10 0.50 -11 0 0 0.10 0.60 -11 0 0 0.20 0.50 -11 0 0 -0.60 0.40 -11 0 0 0.30 0.50 11 -1 0 16.20 1.60 11 1 0 20.20 20.80 11 1 0 19.40 1.90 11 1 0 20.30 1.80 11 -1 0 12.30 1.50 11 1 0 17.80 1.50 11 1 0 17.10 1.40 11 -1 0 12.80 1.30 11 -1 0 15.40 1.30 11 -1 0 -1.90 18.10 -11 1 0 17.80 1.40 -11 -1 0 16.80 1.40 -11 1 0 15.40 1.20 -11 1 0 17.20 1.40 -11 -1 0 17.70 1.50 -11 1 0 16.70 1.40 -11 1 0 17.50 1.40 -11 -1 0 18.70 1.20 -11 -1 0 17.40 1.40 -11 1 0 19.20 1.90 -11 1 0 16.30 1.20 -11 -1 0 16.10 1.60 -11 -1 0 15.90 2.00 -11 -1 0 17.30 1.40 11 2 0 56.89 2.60 11 -2 0 55.19 2.40 11 -2 0 55.39 2.60 11 -2 0 52.69 2.70 11 2 0 53.79 2.60 11 2 0 64.99 24.50 11 -2 0 39.90 18.30 11 -2 0 57.39 2.50 -11 2 0 56.29 2.70 -11 -2 0 52.39 2.30 -11 2 0 51.29 2.40 -11 2 0 54.69 2.60 -11 -2 0 50.59 2.60 -11 2 0 52.69 2.60 -11 2 0 52.39 2.50 -11 -2 0 48.60 2.60 -11 2 0 52.29 2.30 11 -3 0 65.49 2.70 11 -3 0 66.19 2.90 11 -3 0 62.99 3.00 11 -3 0 56.09 17.50 11 3 0 69.99 2.90 11 -3 0 60.89 2.70 11 3 0 48.80 28.20 -11 3 0 66.99 2.90 -11 -3 0 63.99 2.60 -11 3 0 67.29 3.00 -11 3 0 66.79 2.70 -11 -3 0 66.99 3.00 -11 -3 0 62.89 3.00 11 -4 0 11.60 0.90 11 4 0 11.00 1.00 11 -4 0 9.50 1.10 11 -4 0 10.50 1.00 11 4 0 26.40 32.50 11 -4 0 12.70 1.00 11 -4 0 8.90 1.10 -11 -4 0 15.30 1.40 -11 -4 0 11.40 0.90 -11 -4 0 14.30 1.30 -11 4 0 11.70 1.20 -11 4 0 9.00 0.90 11 5 0 122.99 4.50 11 -5 0 122.09 4.30 11 -5 0 120.69 4.70 11 -5 0 126.99 4.60 11 -5 0 124.89 4.20 -11 5 0 127.09 4.40 -11 -5 0 127.89 4.70 -11 -5 0 130.69 4.80 -11 5 0 126.49 4.60 -11 -5 0 117.19 4.20 11 -6 0 57.79 2.60 11 6 0 53.99 2.30 11 6 0 48.90 2.30 11 -6 0 52.99 2.50 11 -6 0 53.19 2.40 -11 -6 0 56.39 2.50 -11 -6 0 46.90 2.60 -11 6 0 58.79 2.30 -11 -6 0 53.49 2.40 -11 6 0 58.99 2.40 11 -7 0 1.50 0.50 11 7 0 1.10 0.40 11 -7 0 1.60 0.60 11 -7 0 1.10 0.50 -11 7 0 0.70 0.40 -11 -7 0 1.60 0.50 -11 -7 0 0.80 0.50 -11 7 0 1.10 0.50 11 -8 0 5.00 0.70 11 -8 0 3.20 0.50 11 -8 0 4.20 0.70 -11 -8 0 4.00 0.70 -11 -8 0 4.10 0.70 -11 8 0 3.00 0.50 -11 8 0 4.50 0.80 11 -9 0 1.70 0.50 11 -9 0 1.80 0.40 11 -9 0 2.50 0.30 -11 9 0 2.00 0.50 -11 -9 0 2.10 0.40 -11 9 0 2.10 0.40 -11 -9 0 1.70 0.40 12 0 0 7.90 1.00 12 0 0 6.40 0.80 12 0 0 6.40 0.90 -12 0 0 6.70 0.90 -12 0 0 6.10 0.70 12 -1 0 1.10 0.60 12 -1 0 1.60 0.50 12 -1 0 1.30 0.60 12 -1 0 0.90 0.50 12 1 0 0.90 0.50 -12 -1 0 1.60 0.50 -12 -1 0 1.70 0.60 -12 1 0 2.30 0.70 -12 -1 0 0.60 0.60 -12 1 0 1.30 0.50 -12 1 0 1.70 0.60 12 -2 0 29.60 1.70 12 2 0 29.80 1.70 12 -2 0 27.40 1.80 12 -2 0 30.70 1.50 12 -2 0 31.70 1.60 -12 -2 0 30.20 1.50 -12 2 0 32.70 1.80 -12 -2 0 32.00 2.30 -12 2 0 30.40 1.60 -12 -2 0 30.60 1.70 -12 2 0 29.70 1.70 12 -3 0 9.30 0.90 12 -3 0 9.30 0.90 12 -3 0 10.40 0.80 12 -3 0 10.20 1.20 12 3 0 9.40 0.90 -12 -3 0 11.20 1.10 -12 3 0 10.30 1.10 -12 -3 0 9.80 0.80 -12 3 0 10.40 1.10 -12 3 0 8.60 0.80 12 -4 0 15.30 1.00 12 -4 0 13.90 1.20 12 -4 0 14.10 1.10 12 4 0 13.90 1.10 -12 -4 0 13.30 0.90 -12 4 0 15.00 1.20 -12 4 0 13.90 1.00 -12 -4 0 13.40 1.10 -12 -4 0 14.50 1.20 12 -5 0 1.40 0.50 12 -5 0 0.60 0.60 12 -5 0 0.30 0.40 12 5 0 1.10 0.40 -12 -5 0 0.70 0.50 -12 5 0 1.00 0.50 -12 5 0 0.80 0.40 -12 -5 0 1.00 0.50 -12 5 0 1.00 0.40 12 6 0 9.90 0.80 12 -6 0 9.10 0.80 12 -6 0 11.30 1.00 -12 6 0 10.30 0.80 -12 6 0 12.20 1.20 -12 6 0 11.00 1.00 -12 -6 0 11.50 0.90 -12 -6 0 10.40 1.00 12 -7 0 -0.20 0.30 12 7 0 0.20 0.30 12 -7 0 0.40 0.40 -12 -7 0 -0.20 0.30 -12 7 0 -0.10 0.30 -12 7 0 0.10 0.40 -12 -7 0 0.50 0.40 -12 7 0 0.20 0.30 13 0 0 0.10 0.30 -13 0 0 0.20 0.40 -13 0 0 0.00 0.30 13 -1 0 105.09 3.80 13 1 0 110.09 3.90 -13 1 0 109.19 4.00 -13 -1 0 105.39 3.70 -13 1 0 108.39 4.00 -13 -1 0 108.19 3.90 13 2 0 0.30 0.40 13 -2 0 0.60 0.40 13 -2 0 1.00 0.50 -13 -2 0 0.40 0.30 -13 2 0 0.20 0.40 -13 -2 0 0.40 0.50 -13 2 0 0.50 0.30 13 -3 0 0.20 0.40 13 -3 0 0.10 0.30 13 3 0 0.40 0.30 -13 3 0 0.20 0.30 -13 3 0 0.50 0.40 -13 -3 0 0.00 0.30 13 -4 0 0.00 0.20 13 -4 0 -0.10 0.30 13 4 0 -0.10 0.30 13 -4 0 0.60 0.40 -13 4 0 0.50 0.30 -13 4 0 -0.30 0.30 -13 -4 0 0.20 0.30 0 15 -1 1.10 0.40 0 15 -1 0.70 0.30 0 15 -1 1.10 0.50 0 -14 1 24.50 1.20 0 14 -1 27.60 1.50 0 -14 1 24.80 1.50 0 14 -1 26.20 1.60 0 14 -1 26.50 1.30 0 -14 1 27.70 1.50 0 -13 1 44.30 18.40 0 -13 1 27.40 1.70 0 13 -1 28.60 1.90 0 13 -1 24.70 1.80 0 13 -1 29.40 1.60 0 -13 1 27.00 1.50 0 -13 1 29.10 1.50 0 13 -1 26.90 1.60 0 -12 1 12.80 1.10 0 -12 1 15.80 1.20 0 12 -1 12.00 1.20 0 -12 1 12.60 1.30 0 12 -1 11.90 1.60 0 12 -1 13.20 1.30 0 -12 1 -9.70 15.20 0 12 -1 15.60 1.10 0 12 -1 16.10 1.60 0 -12 1 13.10 1.10 0 11 -1 46.20 2.50 0 -11 1 52.19 2.70 0 -11 1 51.29 2.40 0 -11 1 48.10 2.30 0 -11 1 51.49 15.80 0 11 -1 48.20 2.40 0 11 -1 47.30 2.30 0 -11 1 50.19 2.30 0 -11 1 46.80 2.30 0 11 -1 50.29 2.20 0 11 -1 47.80 2.30 0 11 -1 50.59 2.50 0 10 -1 3.50 0.70 0 10 -1 5.20 0.90 0 10 -1 3.80 0.70 0 -10 1 2.60 0.90 0 -10 1 4.20 0.80 0 10 -1 3.50 0.70 0 10 -1 3.50 0.60 0 -10 1 8.80 12.10 0 -10 1 4.90 0.90 0 10 -1 3.90 0.60 0 -10 1 3.80 0.70 0 -10 1 4.40 0.80 0 9 -1 -0.20 0.30 0 9 -1 0.10 0.40 0 9 -1 0.40 0.50 0 9 -1 0.60 0.50 0 9 -1 0.00 0.40 0 -9 1 0.40 0.50 0 -9 1 0.80 0.50 0 -9 1 0.30 0.40 0 -9 1 1.00 10.00 0 -9 1 0.00 0.50 0 9 -1 -0.30 0.30 0 8 -1 103.99 3.60 0 8 -1 106.09 3.60 0 -8 1 102.29 3.40 0 8 -1 99.59 3.70 0 8 -1 99.89 3.70 0 -8 1 100.99 3.70 0 -8 1 98.19 3.70 0 8 -1 107.69 3.80 0 -7 1 75.69 2.90 0 7 -1 77.59 2.90 0 -7 1 77.19 3.80 0 7 -1 74.89 2.90 0 -7 1 78.99 2.70 0 7 -1 74.39 2.70 0 -7 1 76.39 3.10 0 7 -1 78.49 2.80 0 7 -1 76.19 2.70 0 -6 1 72.49 3.40 0 6 -1 74.39 2.50 0 6 -1 69.89 2.60 0 6 -1 71.19 2.60 0 6 -1 65.89 2.50 0 -6 1 71.19 2.40 0 -6 1 68.29 2.60 0 6 -1 67.89 20.80 0 -6 1 70.39 2.30 0 -6 1 72.79 2.80 0 6 -1 69.19 2.50 0 5 -1 205.98 22.20 0 -5 1 249.28 7.50 0 -5 1 252.17 7.80 0 -5 1 248.48 8.30 0 5 -1 231.98 7.60 0 5 -1 239.78 7.60 0 5 -1 237.78 7.60 0 4 -1 4.20 8.00 0 -4 1 4.30 0.30 0 4 -1 4.00 0.40 0 4 -1 4.80 0.40 0 -4 1 4.20 0.50 0 -4 1 5.10 0.90 0 4 -1 3.40 0.30 0 4 -1 5.00 0.40 0 -4 1 4.10 0.40 0 -3 1 473.75 14.40 0 3 -1 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5 72.39 3.70 0 3 -5 1864.71 63.19 0 -3 5 1936.21 57.59 0 -2 5 26.60 1.00 0 -2 5 26.60 1.00 0 2 -5 27.50 1.00 0 2 -5 27.80 1.10 0 2 -5 27.50 1.00 0 2 -5 27.10 1.00 0 1 -5 153.08 4.70 0 1 -5 154.48 5.10 0 1 -5 155.48 4.70 0 1 -5 148.69 4.60 0 1 -5 146.19 4.70 0 -1 5 152.48 4.70 0 1 -5 154.28 4.90 0 0 -5 0.20 0.20 0 0 -5 0.40 0.10 0 0 -5 -0.20 0.40 0 0 -5 0.30 0.20 0 0 5 0.10 0.10 0 0 -5 1.20 0.60 0 -1 -5 145.89 7.30 0 -1 -5 156.68 4.70 0 -1 -5 153.58 4.80 0 -1 -5 139.09 4.50 0 1 5 156.58 4.60 0 -2 -5 28.80 1.00 0 2 5 26.90 0.90 0 -2 -5 32.70 3.70 0 2 5 27.90 0.90 0 -2 -5 26.80 1.20 0 2 5 28.80 1.00 0 -3 -5 2018.90 60.09 0 -3 -5 1996.90 62.79 0 -4 -5 74.49 2.70 0 -4 -5 77.49 7.60 0 4 5 75.09 2.40 0 4 5 67.39 2.30 0 -4 -5 68.89 2.40 0 4 5 72.69 2.30 0 -5 -5 601.14 25.20 0 5 5 629.34 18.70 0 6 5 378.16 11.70 0 -6 -5 390.66 11.80 0 -6 -5 343.27 12.30 0 -6 -5 394.26 12.20 0 7 5 20.10 1.00 0 -7 -5 30.80 13.90 0 7 5 19.30 1.10 0 -7 -5 18.10 1.10 0 -7 -5 19.70 1.70 0 -7 -5 19.60 1.10 0 7 5 20.10 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0 -8 21 2.90 0.60 0 -8 21 2.20 0.60 0 7 -21 86.49 3.50 0 -7 21 96.39 3.80 0 -7 21 94.79 4.90 0 7 -21 85.39 3.50 0 -7 21 88.19 3.50 0 -7 21 92.29 3.30 0 6 -21 24.80 1.60 0 6 -21 23.00 1.40 0 -6 21 23.00 1.90 0 -6 21 21.80 1.70 0 -6 21 23.70 1.50 0 6 -21 14.30 3.60 0 -6 21 21.40 1.60 0 5 -21 131.09 7.10 0 5 -21 130.09 4.90 0 5 -21 133.49 4.70 0 -5 21 130.89 4.60 0 -5 21 127.89 4.80 0 -5 21 119.19 5.00 0 5 -21 130.79 5.70 0 -5 21 132.69 5.00 0 4 -21 139.29 5.00 0 -4 21 132.89 4.60 0 -4 21 136.39 5.10 0 -4 21 120.19 5.00 0 4 -21 128.79 4.90 0 4 -21 125.29 6.70 0 -4 21 113.49 5.00 0 -4 21 141.39 6.20 0 -3 21 50.19 2.40 0 3 -21 50.99 2.50 0 3 -21 47.20 2.50 0 -3 21 49.40 3.70 0 3 -21 49.80 2.20 0 -3 21 50.99 2.20 0 3 -21 57.29 4.30 0 -2 21 21.10 1.40 0 2 -21 21.90 1.60 0 -2 21 21.00 1.80 0 2 -21 20.50 1.40 0 2 -21 21.00 1.20 0 2 -21 21.20 2.40 0 -2 21 20.30 1.30 0 1 -21 25.00 1.70 0 -1 21 26.90 1.60 0 -1 21 25.70 1.40 0 1 -21 25.80 1.20 0 1 -21 26.40 1.30 0 0 21 0.40 0.40 0 0 21 0.30 0.50 0 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18.10 1.10 -3 -9 21 20.60 1.10 3 -8 21 -0.10 0.40 3 -8 21 0.00 0.40 3 -8 21 -0.60 0.40 3 8 -21 0.00 0.30 3 -8 21 -0.10 0.30 -3 -8 21 0.20 0.40 -3 -8 21 0.00 0.30 -3 8 -21 -0.10 0.40 -3 -8 21 -0.20 0.40 -3 8 -21 0.30 0.40 3 -7 21 0.40 0.40 3 7 -21 0.30 0.30 3 -7 21 0.10 0.40 3 -7 21 0.10 0.40 -3 -7 21 0.50 0.30 -3 -7 21 0.40 0.40 -3 7 -21 0.20 0.40 -3 7 -21 0.20 0.50 3 -6 21 2.30 0.60 3 6 -21 3.70 0.60 3 -6 21 3.20 0.50 3 -6 21 2.40 0.70 3 -6 21 2.60 0.60 3 -6 21 2.50 0.70 -3 -6 21 2.70 0.50 -3 -6 21 3.40 0.70 -3 6 -21 3.50 0.80 -3 6 -21 2.20 0.60 3 5 -21 11.90 0.90 3 -5 21 13.20 1.20 3 5 -21 12.70 2.60 3 -5 21 11.70 0.90 3 -5 21 14.00 1.30 3 -5 21 13.20 1.30 -3 -5 21 10.60 1.00 -3 5 -21 3.60 4.30 -3 -5 21 13.20 1.10 -3 5 -21 9.10 1.80 -3 5 -21 12.50 1.10 3 -4 21 36.90 1.80 3 4 -21 39.20 1.70 3 -4 21 39.70 2.00 3 -4 21 35.50 2.10 3 -4 21 38.10 2.10 -3 -4 21 38.20 1.90 -3 -4 21 39.30 1.80 -3 4 -21 39.10 2.20 -3 4 -21 41.10 5.40 -3 4 -21 37.80 2.00 3 -3 21 48.10 2.30 3 -3 21 47.10 2.10 3 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39.30 2.00 0 -5 22 40.20 2.10 0 5 -22 37.40 4.30 0 5 -22 38.40 1.90 0 -5 22 38.70 2.20 0 -4 22 159.78 5.80 0 4 -22 161.18 5.60 0 -4 22 164.58 6.00 0 -4 22 172.78 5.70 0 3 -22 44.40 2.20 0 3 -22 38.50 3.80 0 -3 22 42.50 2.30 0 -3 22 41.30 2.00 0 3 -22 40.90 2.10 0 3 -22 44.00 1.90 0 -3 22 43.00 2.10 0 -2 22 87.59 3.70 0 2 -22 79.69 4.00 0 -2 22 92.79 3.50 0 2 -22 88.39 3.20 0 2 -22 85.89 3.40 0 2 -22 93.59 3.70 0 -2 22 92.39 3.40 0 -1 22 8.50 1.00 0 1 -22 6.80 0.60 0 1 -22 8.40 1.10 0 -1 22 7.30 1.00 0 -1 22 7.60 0.80 0 0 22 56.59 2.60 0 0 22 60.89 2.40 0 0 22 54.39 2.50 0 0 -22 55.59 3.40 0 0 -22 57.79 2.70 0 -1 -22 7.60 1.00 0 1 22 8.00 0.80 0 -1 -22 3.80 1.10 0 2 22 90.49 3.30 0 -2 -22 88.29 4.00 0 -3 -22 43.70 2.50 0 -3 -22 44.10 2.10 0 3 22 43.80 1.90 0 -4 -22 164.28 6.20 0 -4 -22 168.58 5.80 0 4 22 157.18 5.60 0 -5 -22 41.10 2.10 0 -5 -22 43.80 2.50 0 5 22 42.00 1.80 0 6 22 3.40 0.50 0 -6 -22 3.40 0.70 0 -6 -22 3.20 0.70 0 7 22 0.00 0.30 0 -7 -22 -0.20 0.40 0 -7 -22 -0.80 0.40 0 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0.30 -1 -6 25 -0.20 0.20 -1 -6 25 0.10 0.30 1 -5 25 28.70 1.50 1 -5 25 30.00 1.50 1 -5 25 30.10 1.30 -1 -5 25 31.30 1.40 -1 5 -25 29.80 1.50 -1 -5 25 32.20 1.50 -1 -5 25 31.00 1.60 -1 5 -25 28.40 1.20 -1 5 -25 28.40 1.50 1 -4 25 12.20 1.00 1 -4 25 12.10 0.80 1 -4 25 14.00 1.00 -1 4 -25 12.00 1.10 -1 -4 25 12.30 0.90 -1 -4 25 12.40 0.90 -1 4 -25 11.40 1.00 -1 -4 25 12.30 1.00 -1 4 -25 12.10 0.60 1 -3 25 24.90 1.40 1 -3 25 26.00 1.30 1 -3 25 25.30 1.40 1 3 -25 24.90 1.40 -1 -3 25 29.10 1.50 -1 3 -25 25.50 1.60 -1 -3 25 27.90 1.40 -1 -3 25 26.30 1.30 -1 3 -25 24.60 1.90 1 2 -25 7.00 0.90 1 -2 25 8.80 0.80 1 -2 25 9.70 0.90 1 -2 25 9.40 0.80 -1 2 -25 9.20 0.90 -1 -2 25 7.00 0.80 -1 2 -25 10.40 1.30 -1 -2 25 8.20 0.80 -1 -2 25 7.60 0.80 1 -1 25 0.80 0.40 1 -1 25 1.10 0.50 1 1 -25 0.80 0.50 -1 1 -25 0.80 0.50 -1 -1 25 1.30 0.50 -1 -1 25 1.40 0.50 -1 -1 25 0.70 0.30 -1 1 -25 0.60 0.50 1 0 25 9.30 0.90 1 0 -25 10.20 1.30 1 0 25 7.70 0.70 -1 0 25 7.60 0.70 -1 0 -25 7.50 1.00 1 1 25 0.90 0.40 1 -1 -25 1.60 0.70 1 1 25 1.20 0.50 -1 1 25 0.70 0.30 -1 -1 -25 0.80 0.50 1 -2 -25 8.00 1.10 1 2 25 9.00 0.70 -1 -2 -25 8.80 1.10 -1 2 25 8.90 0.70 1 3 25 26.30 1.30 1 3 25 26.30 1.30 1 -3 -25 26.40 1.60 -1 -3 -25 25.40 1.70 -1 3 25 24.10 1.20 1 4 25 12.60 0.80 1 -4 -25 9.80 1.00 -1 -4 -25 12.20 1.20 -1 4 25 12.90 0.80 1 -5 -25 28.10 1.60 1 5 25 27.20 1.30 -1 -5 -25 27.90 1.60 1 -6 -25 0.10 0.40 1 6 25 0.00 0.20 -1 -6 -25 0.10 0.30 2 -6 25 15.20 0.90 2 -6 25 14.70 1.00 2 -6 25 13.30 0.90 -2 6 -25 16.50 1.10 -2 -6 25 15.80 0.80 -2 -6 25 13.60 1.00 -2 6 -25 14.90 1.00 -2 6 -25 14.70 0.90 2 -5 25 1.50 0.40 2 -5 25 1.20 0.40 2 -5 25 0.80 0.30 -2 5 -25 1.30 0.40 -2 5 -25 1.50 0.30 -2 -5 25 1.70 0.40 -2 -5 25 1.40 0.50 -2 -5 25 1.00 0.40 2 -4 25 7.30 0.80 2 -4 25 9.10 0.90 -2 4 -25 9.20 0.90 -2 4 -25 7.90 0.60 -2 -4 25 8.50 0.80 -2 -4 25 6.80 0.80 -2 -4 25 9.00 0.70 2 -3 25 5.60 0.70 2 -3 25 5.90 0.60 2 -3 25 6.00 0.80 -2 3 -25 5.70 0.90 -2 -3 25 5.10 0.70 -2 -3 25 6.00 0.70 -2 -3 25 5.10 0.60 -2 3 -25 5.80 0.50 -2 3 -25 6.00 0.90 2 -2 25 23.70 1.30 2 -2 25 22.80 1.20 2 -2 25 23.20 1.30 -2 2 -25 23.20 1.70 -2 2 -25 22.90 1.40 -2 -2 25 23.80 1.20 -2 -2 25 23.00 1.30 -2 -2 25 22.80 1.20 2 -1 25 23.90 1.30 2 1 -25 18.20 1.20 2 -1 25 20.00 1.20 -2 1 -25 22.10 1.50 -2 1 -25 22.70 1.40 -2 -1 25 20.50 1.20 -2 -1 25 20.50 1.10 2 0 25 3.70 0.50 2 0 25 5.30 0.70 2 0 -25 5.60 0.70 -2 0 -25 5.30 0.80 -2 0 25 4.00 0.50 -2 0 -25 4.00 0.80 2 -1 -25 19.60 1.30 2 1 25 19.50 1.20 2 1 25 19.10 1.10 -2 1 25 20.70 1.10 -2 -1 -25 20.00 1.50 2 2 25 21.10 1.30 2 2 25 24.20 1.30 2 2 25 23.30 1.20 2 -2 -25 24.50 1.40 -2 -2 -25 24.10 1.60 -2 2 25 22.90 1.20 2 3 25 6.50 0.70 2 3 25 6.10 0.60 2 -3 -25 5.40 0.70 -2 3 25 6.00 0.60 -2 -3 -25 3.70 0.80 2 -4 -25 8.00 0.80 2 4 25 7.80 0.70 -2 -4 -25 8.30 0.70 -2 4 25 6.20 0.60 -2 -4 -25 7.90 1.00 2 -5 -25 1.00 0.50 2 5 25 1.50 0.40 -2 -5 -25 1.80 0.40 -2 -5 -25 2.60 0.60 2 -6 -25 13.70 1.00 2 6 25 14.10 0.90 -2 -6 -25 14.60 1.10 3 -5 25 6.40 0.70 3 -5 25 7.70 0.90 3 -5 25 6.50 0.70 -3 -5 25 6.70 0.60 -3 -5 25 6.00 0.70 -3 -5 25 7.30 0.60 -3 5 -25 7.80 0.80 -3 5 -25 6.70 0.60 3 -4 25 15.40 1.00 3 -4 25 16.20 1.00 3 -4 25 13.90 1.00 3 -4 25 15.70 0.90 -3 -4 25 17.20 1.10 -3 -4 25 14.40 0.90 -3 4 -25 15.60 0.80 -3 -4 25 13.50 1.00 -3 4 -25 13.60 1.10 3 -3 25 59.19 2.40 3 -3 25 61.89 2.40 3 -3 25 58.89 2.60 -3 -3 25 56.19 2.30 -3 3 -25 59.29 2.10 -3 -3 25 62.19 2.50 -3 -3 25 60.89 2.30 3 -2 25 13.80 0.90 3 -2 25 13.60 1.00 -3 2 -25 14.00 0.70 -3 2 -25 14.30 1.10 -3 2 -25 15.40 1.40 -3 -2 25 14.90 0.90 -3 -2 25 13.00 1.00 3 -1 25 21.90 1.30 3 -1 25 23.00 1.20 -3 -1 25 21.60 1.20 -3 1 -25 23.60 1.50 -3 1 -25 25.00 1.90 -3 -1 25 24.30 1.20 3 0 25 1.40 0.60 3 0 25 0.50 0.40 3 0 25 0.80 0.40 -3 0 25 0.60 0.30 -3 0 -25 0.90 0.50 -3 0 -25 0.70 0.50 3 1 25 22.70 1.20 3 1 25 22.80 1.30 3 1 25 23.50 1.20 -3 -1 -25 24.60 1.70 -3 1 25 22.00 1.10 3 2 25 13.70 0.90 3 2 25 13.50 0.90 3 2 25 13.00 0.90 3 -2 -25 13.90 1.10 -3 2 25 13.30 0.80 -3 -2 -25 13.70 1.40 3 3 25 59.29 2.20 3 3 25 57.89 2.30 3 -3 -25 57.49 2.50 3 3 25 59.89 2.20 -3 3 25 53.59 2.10 -3 -3 -25 63.59 2.70 -3 -3 -25 50.79 2.30 3 4 25 14.40 0.90 3 -4 -25 14.10 0.90 -3 -4 -25 16.30 1.20 -3 -4 -25 15.00 0.90 3 5 25 6.70 0.60 3 -5 -25 6.40 0.60 -3 -5 -25 6.00 0.60 -3 -5 -25 7.20 0.80 4 -4 25 10.10 0.80 4 -4 25 10.10 0.70 4 -4 25 9.80 0.80 -4 4 -25 9.70 0.60 -4 -4 25 10.70 0.90 -4 -4 25 10.10 0.70 -4 4 -25 8.60 0.90 -4 -4 25 10.10 0.80 4 -3 25 3.80 0.60 4 -3 25 3.70 0.50 4 -3 25 4.30 0.60 4 -3 25 3.50 0.70 -4 -3 25 4.80 0.50 -4 3 -25 3.40 0.60 -4 3 -25 4.90 0.50 -4 -3 25 4.70 0.60 4 -2 25 11.40 0.90 4 -2 25 11.70 0.80 4 -2 25 10.80 0.90 -4 2 -25 6.70 1.20 -4 -2 25 10.60 0.70 -4 2 -25 11.50 0.60 -4 2 -25 10.60 1.10 4 -1 25 30.40 1.50 4 -1 25 29.00 1.50 4 -1 25 27.60 1.40 -4 1 -25 32.60 1.80 -4 1 -25 29.10 1.70 -4 -1 25 32.00 1.50 -4 -1 25 27.70 1.30 4 0 25 0.80 0.40 4 0 25 0.40 0.40 4 0 25 0.40 0.30 -4 0 25 0.70 0.30 -4 0 -25 2.00 0.60 -4 0 -25 0.40 0.40 4 1 25 30.70 1.40 4 1 25 28.30 1.50 4 1 25 30.80 1.40 -4 1 25 28.00 1.30 -4 -1 -25 29.10 1.70 4 2 25 11.10 0.80 4 2 25 9.50 0.80 -4 2 25 10.90 0.70 -4 -2 -25 9.80 1.00 4 3 25 4.40 0.50 4 3 25 4.60 0.60 4 3 25 4.60 0.50 -4 -3 -25 3.70 0.70 -4 -3 -25 4.70 0.50 4 4 25 10.20 0.70 -4 -4 -25 11.40 0.70 -4 -4 -25 9.30 0.90 5 -3 25 4.00 0.50 5 -3 25 3.00 0.50 -5 -3 25 3.50 0.40 -5 3 -25 4.70 0.50 -5 3 -25 3.00 0.60 -5 3 -25 4.20 0.60 5 -2 25 1.90 0.40 5 -2 25 1.80 0.40 5 -2 25 2.20 0.50 -5 2 -25 1.80 0.50 -5 -2 25 1.90 0.40 -5 2 -25 2.00 0.40 -5 2 -25 2.40 0.60 5 -1 25 3.70 0.50 5 -1 25 3.90 0.50 5 -1 25 3.40 0.60 -5 1 -25 2.70 0.60 -5 1 -25 3.50 0.60 -5 -1 25 3.10 0.40 5 0 25 27.00 1.30 5 0 25 28.00 1.30 5 0 25 24.40 1.20 -5 0 -25 26.00 1.50 -5 0 25 25.20 1.10 5 1 25 4.40 0.60 5 1 25 2.90 0.50 5 1 25 3.30 0.50 -5 -1 -25 4.20 0.70 5 2 25 3.10 0.50 5 2 25 2.20 0.40 -5 -2 -25 1.60 0.50 5 3 25 3.50 0.50 5 3 25 3.70 0.40 -5 -3 -25 3.90 0.60 0 -5 26 1.40 0.50 0 -5 26 1.40 0.30 0 -5 26 1.70 0.60 0 -4 26 21.60 1.10 0 -4 26 21.50 1.00 0 4 -26 18.90 1.00 0 -4 26 18.20 1.10 0 -3 26 21.50 1.10 0 -3 26 22.40 1.20 0 3 -26 20.00 1.20 0 -3 26 21.50 1.30 0 -2 26 1.10 0.30 0 -2 26 0.60 0.40 0 2 -26 0.50 0.40 0 -2 26 0.80 0.40 0 1 -26 -0.20 0.40 0 -1 26 0.50 0.30 0 0 26 0.10 0.30 0 0 -26 0.20 0.40 0 -1 -26 0.30 0.50 0 1 26 0.50 0.30 0 2 26 1.00 0.30 0 -2 -26 0.60 0.50 0 3 26 19.10 1.00 0 3 26 21.50 1.30 0 -3 -26 23.00 1.40 0 -4 -26 22.00 1.30 0 4 26 18.50 1.00 0 -5 -26 1.40 0.50 1 -5 26 0.60 0.30 1 -5 26 0.60 0.30 1 -5 26 0.30 0.30 -1 -5 26 0.50 0.30 -1 5 -26 0.60 0.40 -1 -5 26 0.30 0.30 1 -4 26 17.10 1.00 1 -4 26 15.60 1.10 1 -4 26 16.80 0.90 -1 -4 26 16.00 1.00 -1 4 -26 16.90 1.20 -1 -4 26 15.60 0.90 1 -3 26 10.80 0.80 1 -3 26 9.30 0.80 1 -3 26 9.90 0.80 -1 -3 26 9.50 0.80 -1 3 -26 11.80 1.40 -1 3 -26 9.80 0.90 -1 -3 26 9.60 1.00 1 2 -26 0.20 0.50 1 -2 26 0.80 0.40 1 -2 26 0.10 0.30 -1 2 -26 0.60 0.50 -1 -2 26 0.80 0.40 -1 -2 26 0.50 0.40 -1 2 -26 0.70 0.40 -1 -2 26 0.40 0.30 1 1 -26 29.40 1.50 1 -1 26 28.80 1.40 1 -1 26 30.20 1.40 -1 -1 26 28.70 1.40 -1 1 -26 29.30 1.70 1 0 -26 38.00 1.80 1 0 26 35.40 2.00 1 0 26 36.30 1.60 -1 0 -26 35.80 1.90 -1 0 26 35.10 1.60 1 1 26 29.40 1.40 1 -1 -26 29.90 1.60 -1 -1 -26 30.50 1.70 -1 1 26 27.30 1.40 1 -2 -26 0.50 0.40 1 2 26 0.00 0.30 1 2 26 -0.10 0.30 -1 2 26 0.60 0.30 -1 -2 -26 0.40 0.50 1 3 26 9.70 0.70 1 3 26 9.90 0.70 1 -3 -26 11.10 0.90 -1 -3 -26 8.70 0.90 -1 3 26 10.10 0.70 1 -4 -26 16.60 1.10 -1 -4 -26 17.30 1.20 1 -5 -26 0.60 0.40 1 5 26 0.50 0.30 -1 -5 -26 0.40 0.40 2 -4 26 9.10 0.70 2 -4 26 10.00 0.80 2 -4 26 8.00 0.60 -2 4 -26 9.60 1.00 -2 4 -26 8.70 0.80 -2 -4 26 8.30 0.70 -2 -4 26 8.40 0.70 -2 -4 26 9.50 0.80 2 -3 26 52.29 2.10 2 -3 26 50.39 2.00 2 -3 26 52.49 2.00 -2 3 -26 49.80 2.10 -2 -3 26 50.79 2.10 -2 -3 26 53.39 2.00 -2 3 -26 51.29 2.30 -2 -3 26 51.89 2.00 2 -2 26 33.60 1.60 2 -2 26 35.70 1.70 -2 -2 26 34.70 1.60 -2 2 -26 33.20 1.80 -2 -2 26 33.70 1.80 -2 2 -26 30.70 1.60 2 -1 26 20.50 1.10 2 -1 26 21.30 1.20 -2 -1 26 21.20 1.20 -2 1 -26 19.60 1.40 -2 1 -26 21.20 1.30 2 0 26 2.60 0.50 2 0 -26 2.60 0.50 2 0 26 2.40 0.40 -2 0 26 2.80 0.40 -2 0 -26 2.80 0.60 2 1 26 22.00 1.10 2 1 26 22.60 1.10 2 1 26 20.90 1.20 2 -1 -26 18.90 1.30 -2 -1 -26 20.70 1.40 -2 1 26 22.50 1.10 2 2 26 33.70 1.50 2 2 26 30.20 1.50 2 -2 -26 33.50 1.80 -2 2 26 34.30 1.40 -2 -2 -26 32.90 1.80 2 3 26 51.39 2.00 2 3 26 53.09 2.10 2 -3 -26 54.69 2.40 -2 3 26 48.40 2.00 -2 -3 -26 55.49 2.40 2 -4 -26 9.10 0.70 2 4 26 8.30 0.70 -2 -4 -26 9.10 0.90 3 -4 26 14.90 0.90 3 -4 26 14.60 0.90 -3 4 -26 13.10 1.00 -3 -4 26 13.50 0.80 -3 4 -26 14.80 1.20 -3 -4 26 11.50 0.90 -3 -4 26 13.70 0.90 3 -3 26 17.60 0.90 3 -3 26 17.70 1.10 3 -3 26 19.00 1.00 -3 -3 26 17.50 1.10 -3 3 -26 16.20 1.20 -3 3 -26 18.10 1.10 -3 -3 26 17.70 0.90 3 -2 26 13.50 1.00 3 -2 26 12.90 0.80 3 -2 26 14.00 0.90 -3 -2 26 14.80 0.80 -3 -2 26 12.70 0.90 -3 2 -26 12.90 1.00 -3 2 -26 14.20 1.10 3 -1 26 26.30 1.30 3 -1 26 29.40 1.40 3 -1 26 29.60 1.40 -3 1 -26 27.20 1.60 -3 -1 26 25.70 1.20 -3 1 -26 28.30 1.50 3 0 26 14.70 0.90 3 0 26 12.50 0.90 3 0 26 13.90 0.90 -3 0 -26 12.80 1.10 -3 0 26 12.50 0.80 3 1 26 29.00 1.30 3 1 26 28.20 1.40 3 1 26 27.50 1.30 -3 -1 -26 27.90 1.60 -3 1 26 28.50 1.20 3 2 26 13.50 0.80 3 2 26 14.40 0.80 3 2 26 11.40 1.00 -3 -2 -26 13.30 1.10 -3 2 26 12.80 0.80 3 3 26 18.80 1.00 -3 -3 -26 17.70 1.20 3 4 26 13.90 0.80 -3 -4 -26 14.20 1.00 4 -2 26 4.10 0.50 4 -2 26 4.90 0.60 -4 -2 26 4.10 0.50 -4 2 -26 4.40 0.60 -4 2 -26 4.90 0.70 -4 -2 26 4.80 0.50 4 -1 26 19.50 1.00 4 -1 26 17.50 1.10 4 -1 26 20.10 1.10 -4 1 -26 19.50 1.20 -4 1 -26 17.50 1.10 -4 -1 26 17.90 0.90 4 0 26 8.70 0.70 4 0 26 10.80 1.10 -4 0 26 9.00 0.70 -4 0 -26 6.90 0.80 4 1 26 20.70 1.00 4 1 26 18.10 1.00 -4 -1 -26 20.40 1.30 4 2 26 4.20 0.50 4 2 26 5.70 0.60 4 2 26 4.90 0.50 -4 -2 -26 4.80 0.70 0 -3 27 0.30 0.30 0 -3 27 0.10 0.20 0 -2 27 2.20 0.40 0 2 -27 1.00 0.40 0 -2 27 2.10 0.40 0 1 -27 5.40 0.80 0 -1 27 5.80 0.60 0 0 27 -0.20 0.20 0 0 -27 0.40 0.40 0 -1 -27 5.60 0.70 0 1 27 7.50 0.60 0 2 27 2.00 0.30 0 -2 -27 1.50 0.50 0 2 27 1.70 0.30 0 -3 -27 0.20 0.40 0 3 27 0.10 0.20 1 -3 27 16.60 0.90 1 -3 27 13.90 0.80 -1 -3 27 15.50 0.80 -1 -3 27 16.10 1.20 -1 3 -27 14.40 0.90 1 -2 27 21.10 1.00 1 -2 27 22.70 1.10 -1 -2 27 21.30 1.10 1 1 -27 15.00 1.10 1 -1 27 17.10 0.90 1 -1 27 17.40 0.90 -1 -1 27 16.40 0.90 -1 1 -27 16.50 1.10 1 0 -27 7.90 0.70 1 0 27 7.60 0.60 -1 0 27 7.60 0.60 -1 0 -27 9.30 0.90 1 1 27 15.80 0.90 1 -1 -27 16.30 1.00 1 1 27 16.00 1.00 -1 -1 -27 16.90 1.10 -1 1 27 17.30 0.90 1 -2 -27 22.10 1.20 1 2 27 22.10 1.00 1 2 27 21.10 1.00 -1 2 27 19.60 1.30 -1 -2 -27 21.70 1.30 1 -3 -27 14.10 0.90 1 3 27 15.50 1.00 -1 -3 -27 14.40 1.00 2 -2 27 14.20 0.90 2 -2 27 13.40 0.90 2 -2 27 14.70 0.80 -2 -2 27 14.00 0.80 -2 2 -27 14.00 1.00 2 -1 27 42.10 1.70 2 -1 27 42.90 1.80 2 -1 27 40.70 1.70 -2 1 -27 44.10 2.00 -2 -1 27 42.80 1.70 2 0 27 46.80 1.80 2 0 27 49.50 2.00 2 0 27 45.90 1.90 -2 0 -27 48.60 2.10 -2 0 27 45.30 1.80 2 1 27 40.50 1.80 2 1 27 42.80 1.70 -2 1 27 41.90 1.90 -2 -1 -27 40.00 1.90 2 2 27 15.10 0.80 2 2 27 14.80 0.80 -2 -2 -27 14.20 1.10 3 0 27 2.20 0.50 3 0 27 2.50 0.40 3 0 27 3.10 0.40 -3 0 27 2.00 0.30 -3 0 -27 2.60 0.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 1641 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.7079(2) 0.98234(16) 0.54833(9) 0.0546(5) Uani 1 1 d . . . . . H1A H 0.774876 0.966097 0.523178 0.082 Uiso 1 1 calc R U . . . H1B H 0.731587 1.034047 0.577703 0.082 Uiso 1 1 calc R U . . . H1C H 0.643919 1.011380 0.524830 0.082 Uiso 1 1 calc R U . . . C2 C 0.58173(16) 0.90043(13) 0.61580(7) 0.0387(4) Uani 1 1 d . . . . . C3 C 0.53652(15) 0.80178(12) 0.64001(7) 0.0351(3) Uani 1 1 d . . . . . C4 C 0.43752(15) 0.80054(12) 0.67749(7) 0.0362(3) Uani 1 1 d . . . . . H4 H 0.397877 0.860872 0.692001 0.043 Uiso 1 1 calc R U . . . C5 C 0.40878(14) 0.69862(13) 0.68921(6) 0.0343(3) Uani 1 1 d . . . . . C6 C 0.30911(15) 0.65547(14) 0.72175(7) 0.0379(4) Uani 1 1 d . . . . . C7 C 0.20055(19) 0.7035(2) 0.71535(10) 0.0612(6) Uani 1 1 d . . . . . H7 H 0.192862 0.762653 0.690318 0.073 Uiso 1 1 calc R U . . . C8 C 0.1036(2) 0.6665(3) 0.74495(12) 0.0819(8) Uani 1 1 d . . . . . H8 H 0.029664 0.699785 0.739795 0.098 Uiso 1 1 calc R U . . . C9 C 0.1133(2) 0.5817(2) 0.78184(10) 0.0692(7) Uani 1 1 d . . . . . H9 H 0.046371 0.555977 0.801984 0.083 Uiso 1 1 calc R U . . . C10 C 0.21975(19) 0.53486(17) 0.78921(8) 0.0528(5) Uani 1 1 d . . . . . H10 H 0.226792 0.476855 0.815054 0.063 Uiso 1 1 calc R U . . . C11 C 0.31810(16) 0.57045(14) 0.75961(7) 0.0410(4) Uani 1 1 d . . . . . H11 H 0.391617 0.536719 0.765202 0.049 Uiso 1 1 calc R U . . . C12 C 0.56925(14) 0.69911(12) 0.62902(6) 0.0333(3) Uani 1 1 d . . . . . C13 C 0.66418(17) 0.64997(14) 0.59410(8) 0.0455(4) Uani 1 1 d . . . . . H13A H 0.715845 0.609380 0.619737 0.068 Uiso 1 1 calc R U . . . H13B H 0.709660 0.705091 0.574575 0.068 Uiso 1 1 calc R U . . . H13C H 0.629668 0.603002 0.564934 0.068 Uiso 1 1 calc R U . . . C14 C 0.55073(14) 0.45418(12) 0.67828(6) 0.0329(3) Uani 1 1 d . . . . . C15 C 0.39661(13) 0.48981(12) 0.61230(6) 0.0310(3) Uani 1 1 d . . . . . C16 C 0.50537(14) 0.34880(12) 0.65946(6) 0.0323(3) Uani 1 1 d . . . . . H16 H 0.476761 0.308459 0.693999 0.039 Uiso 1 1 calc R U . . . C17 C 0.40168(13) 0.37171(12) 0.61762(6) 0.0309(3) Uani 1 1 d . . . . . H17 H 0.326993 0.345066 0.635035 0.037 Uiso 1 1 calc R U . . . C18 C 0.58622(15) 0.27847(12) 0.62212(7) 0.0363(4) Uani 1 1 d . . . . . H18 H 0.644445 0.236455 0.644911 0.044 Uiso 1 1 calc R U . . . C19 C 0.49369(16) 0.21248(12) 0.59074(7) 0.0376(4) Uani 1 1 d . . . . . H19A H 0.442260 0.173336 0.617863 0.045 Uiso 1 1 calc R U . . . H19B H 0.528153 0.163756 0.561802 0.045 Uiso 1 1 calc R U . . . C20 C 0.43152(13) 0.30729(11) 0.56241(7) 0.0301(3) Uani 1 1 d . . . . . H20 H 0.362231 0.288505 0.537852 0.036 Uiso 1 1 calc R U . . . C21 C 0.63932(14) 0.34135(13) 0.57143(7) 0.0350(3) Uani 1 1 d . . . . . H21A H 0.702176 0.300666 0.552002 0.042 Uiso 1 1 calc R U . . . H21B H 0.672166 0.409056 0.585241 0.042 Uiso 1 1 calc R U . . . C22 C 0.53326(13) 0.36040(11) 0.52898(6) 0.0293(3) Uani 1 1 d . . . . . H22 H 0.517716 0.437745 0.526145 0.035 Uiso 1 1 calc R U . . . C23 C 0.55496(13) 0.31659(11) 0.46831(7) 0.0296(3) Uani 1 1 d . . . . . C24 C 0.50032(14) 0.22164(12) 0.44953(7) 0.0340(3) Uani 1 1 d . . . . . H24 H 0.446634 0.187773 0.474989 0.041 Uiso 1 1 calc R U . . . C25 C 0.52177(14) 0.17699(12) 0.39637(7) 0.0344(3) Uani 1 1 d . . . . . C26 C 0.46097(19) 0.07587(15) 0.37910(9) 0.0506(5) Uani 1 1 d . . . . . H26A H 0.519744 0.020991 0.372107 0.076 Uiso 1 1 calc R U . . . H26B H 0.415405 0.087572 0.343554 0.076 Uiso 1 1 calc R U . . . H26C H 0.408344 0.053506 0.410443 0.076 Uiso 1 1 calc R U . . . C27 C 0.60157(14) 0.22715(12) 0.35752(7) 0.0323(3) Uani 1 1 d . . . . . C28 C 0.63126(15) 0.18304(13) 0.30279(7) 0.0383(4) Uani 1 1 d . . . . . H28 H 0.598268 0.117445 0.291514 0.046 Uiso 1 1 calc R U . . . C29 C 0.70678(17) 0.23378(15) 0.26609(7) 0.0443(4) Uani 1 1 d . . . . . H29 H 0.726508 0.202620 0.229841 0.053 Uiso 1 1 calc R U . . . C30 C 0.75524(17) 0.33102(15) 0.28135(8) 0.0461(4) Uani 1 1 d . . . . . H30 H 0.805891 0.366458 0.255036 0.055 Uiso 1 1 calc R U . . . C31 C 0.72987(15) 0.37540(14) 0.33421(7) 0.0392(4) Uani 1 1 d . . . . . H31 H 0.763593 0.441383 0.344192 0.047 Uiso 1 1 calc R U . . . C32 C 0.65400(14) 0.32438(12) 0.37433(7) 0.0323(3) Uani 1 1 d . . . . . C33 C 0.62978(13) 0.36767(11) 0.43053(7) 0.0300(3) Uani 1 1 d . . . . . C34 C 0.68776(14) 0.47045(12) 0.44573(6) 0.0314(3) Uani 1 1 d . . . . . C35 C 0.80724(16) 0.65514(15) 0.46417(8) 0.0442(4) Uani 1 1 d . . . . . H35 H 0.852968 0.716796 0.470003 0.053 Uiso 1 1 calc R U . . . C36 C 0.85232(15) 0.55920(16) 0.47625(8) 0.0447(4) Uani 1 1 d . . . . . H36 H 0.929343 0.556296 0.491931 0.054 Uiso 1 1 calc R U . . . C37 C 0.62966(14) 0.56750(12) 0.43319(6) 0.0319(3) Uani 1 1 d . . . . . C38 C 0.69151(15) 0.66282(13) 0.44281(7) 0.0377(4) Uani 1 1 d . . . . . C39 C 0.51326(15) 0.57223(13) 0.41204(8) 0.0406(4) Uani 1 1 d . . . . . H39 H 0.471234 0.508922 0.404910 0.049 Uiso 1 1 calc R U . . . C40 C 0.46084(18) 0.66726(15) 0.40179(10) 0.0530(5) Uani 1 1 d . . . . . H40 H 0.382570 0.669574 0.387670 0.064 Uiso 1 1 calc R U . . . C41 C 0.5220(2) 0.76158(15) 0.41200(10) 0.0563(5) Uani 1 1 d . . . . . H41 H 0.484558 0.827205 0.405063 0.068 Uiso 1 1 calc R U . . . C42 C 0.63465(19) 0.75967(14) 0.43177(9) 0.0495(5) Uani 1 1 d . . . . . H42 H 0.675270 0.823950 0.438193 0.059 Uiso 1 1 calc R U . . . N1 N 0.49221(12) 0.63727(9) 0.66020(5) 0.0317(3) Uani 1 1 d . . . . . N2 N 0.48022(11) 0.53007(9) 0.65111(5) 0.0300(3) Uani 1 1 d . . . . . N3 N 0.79478(12) 0.46574(12) 0.46749(6) 0.0397(3) Uani 1 1 d . . . . . O1 O 0.54357(13) 0.98600(9) 0.62871(6) 0.0508(3) Uani 1 1 d . . . . . O2 O 0.66860(12) 0.88731(9) 0.57675(6) 0.0484(3) Uani 1 1 d . . . . . O3 O 0.63071(12) 0.47483(10) 0.71033(5) 0.0473(3) Uani 1 1 d . . . . . O4 O 0.33544(11) 0.54427(10) 0.58235(5) 0.0455(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0653(12) 0.0433(10) 0.0553(11) 0.0114(9) 0.0081(10) -0.0057(9) C2 0.0496(10) 0.0311(8) 0.0355(8) -0.0001(6) -0.0049(7) 0.0005(7) C3 0.0456(9) 0.0293(7) 0.0305(7) -0.0024(6) -0.0023(7) 0.0027(7) C4 0.0474(9) 0.0300(7) 0.0314(7) -0.0051(6) -0.0014(7) 0.0081(7) C5 0.0421(8) 0.0340(8) 0.0268(7) -0.0053(6) 0.0009(6) 0.0061(7) C6 0.0428(9) 0.0420(9) 0.0290(7) -0.0092(7) 0.0038(7) 0.0049(7) C7 0.0554(11) 0.0767(14) 0.0514(11) 0.0056(11) 0.0135(10) 0.0256(11) C8 0.0508(12) 0.123(2) 0.0720(16) 0.0077(16) 0.0209(12) 0.0280(15) C9 0.0521(12) 0.1015(19) 0.0540(12) -0.0056(13) 0.0220(10) -0.0067(13) C10 0.0617(12) 0.0574(12) 0.0392(9) -0.0056(8) 0.0113(9) -0.0108(10) C11 0.0462(9) 0.0409(9) 0.0359(8) -0.0048(7) 0.0044(7) -0.0023(8) C12 0.0413(8) 0.0297(7) 0.0290(7) -0.0010(6) 0.0008(6) -0.0005(7) C13 0.0515(10) 0.0324(8) 0.0525(10) -0.0022(7) 0.0170(8) 0.0010(7) C14 0.0390(8) 0.0319(8) 0.0277(7) 0.0019(6) 0.0009(6) 0.0012(6) C15 0.0306(7) 0.0335(8) 0.0287(7) -0.0046(6) 0.0038(6) 0.0059(6) C16 0.0399(8) 0.0272(7) 0.0297(7) 0.0041(6) 0.0011(6) 0.0006(6) C17 0.0313(7) 0.0306(7) 0.0310(7) -0.0020(6) 0.0028(6) -0.0015(6) C18 0.0430(9) 0.0275(7) 0.0384(8) 0.0011(6) -0.0027(7) 0.0079(6) C19 0.0492(9) 0.0244(7) 0.0393(8) 0.0004(6) 0.0046(7) 0.0001(7) C20 0.0325(7) 0.0251(7) 0.0327(7) -0.0029(6) 0.0031(6) -0.0024(6) C21 0.0304(7) 0.0335(8) 0.0410(9) -0.0052(7) 0.0018(6) 0.0032(6) C22 0.0306(7) 0.0235(7) 0.0337(7) -0.0025(6) 0.0025(6) 0.0010(5) C23 0.0315(7) 0.0236(7) 0.0338(7) -0.0006(6) 0.0031(6) 0.0036(6) C24 0.0374(8) 0.0285(7) 0.0362(8) -0.0014(6) 0.0059(7) -0.0016(6) C25 0.0383(8) 0.0269(7) 0.0381(8) -0.0029(6) 0.0017(6) 0.0018(6) C26 0.0638(12) 0.0394(9) 0.0485(10) -0.0120(8) 0.0108(9) -0.0141(9) C27 0.0340(8) 0.0302(7) 0.0325(7) -0.0006(6) -0.0011(6) 0.0054(6) C28 0.0424(9) 0.0386(9) 0.0340(8) -0.0036(7) -0.0016(7) 0.0049(7) C29 0.0538(10) 0.0496(10) 0.0295(8) -0.0020(7) 0.0044(7) 0.0052(8) C30 0.0513(10) 0.0517(10) 0.0353(9) 0.0085(8) 0.0103(8) 0.0010(9) C31 0.0447(9) 0.0353(8) 0.0376(8) 0.0050(7) 0.0055(7) -0.0001(7) C32 0.0337(7) 0.0301(7) 0.0330(8) 0.0033(6) 0.0014(6) 0.0058(6) C33 0.0308(7) 0.0252(7) 0.0342(8) 0.0008(6) 0.0015(6) 0.0031(6) C34 0.0333(8) 0.0306(7) 0.0302(7) 0.0007(6) 0.0067(6) -0.0020(6) C35 0.0435(9) 0.0445(9) 0.0447(9) -0.0060(8) 0.0087(8) -0.0187(8) C36 0.0309(8) 0.0579(11) 0.0453(9) -0.0022(8) 0.0034(7) -0.0116(8) C37 0.0370(8) 0.0281(7) 0.0306(7) -0.0008(6) 0.0051(6) -0.0042(6) C38 0.0454(9) 0.0328(8) 0.0348(8) -0.0022(6) 0.0096(7) -0.0094(7) C39 0.0415(9) 0.0280(7) 0.0522(9) -0.0007(7) -0.0046(8) -0.0019(7) C40 0.0498(10) 0.0356(9) 0.0736(13) 0.0045(9) -0.0066(10) 0.0037(8) C41 0.0643(13) 0.0284(8) 0.0763(14) 0.0064(9) 0.0053(11) 0.0058(8) C42 0.0645(12) 0.0268(8) 0.0572(12) -0.0008(8) 0.0129(9) -0.0113(8) N1 0.0405(7) 0.0238(6) 0.0308(6) -0.0041(5) 0.0047(5) 0.0021(5) N2 0.0365(6) 0.0243(6) 0.0290(6) -0.0025(5) 0.0014(5) 0.0026(5) N3 0.0312(7) 0.0449(8) 0.0430(7) 0.0012(6) 0.0034(6) -0.0032(6) O1 0.0707(9) 0.0267(6) 0.0549(7) 0.0015(5) 0.0051(7) 0.0051(6) O2 0.0593(8) 0.0327(6) 0.0532(8) 0.0060(5) 0.0125(6) 0.0008(6) O3 0.0538(7) 0.0409(6) 0.0472(7) -0.0004(6) -0.0185(6) -0.0013(6) O4 0.0501(7) 0.0421(6) 0.0442(6) -0.0069(5) -0.0115(6) 0.0175(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? O2 C1 H1A 109.5 . . ? O2 C1 H1B 109.5 . . ? O2 C1 H1C 109.5 . . ? O1 C2 C3 123.32(16) . . ? O1 C2 O2 122.68(16) . . ? O2 C2 C3 113.99(14) . . ? C4 C3 C2 121.34(14) . . ? C12 C3 C2 130.05(15) . . ? C12 C3 C4 108.40(14) . . ? C3 C4 H4 125.6 . . ? C5 C4 C3 108.78(14) . . ? C5 C4 H4 125.6 . . ? C4 C5 C6 129.96(15) . . ? C4 C5 N1 105.73(14) . . ? N1 C5 C6 124.21(14) . . ? C7 C6 C5 118.19(17) . . ? C7 C6 C11 118.26(18) . . ? C11 C6 C5 123.53(16) . . ? C6 C7 H7 119.6 . . ? C8 C7 C6 120.8(2) . . ? C8 C7 H7 119.6 . . ? C7 C8 H8 119.8 . . ? C9 C8 C7 120.4(2) . . ? C9 C8 H8 119.8 . . ? C8 C9 H9 120.3 . . ? C10 C9 C8 119.3(2) . . ? C10 C9 H9 120.3 . . ? C9 C10 H10 119.4 . . ? C9 C10 C11 121.1(2) . . ? C11 C10 H10 119.4 . . ? C6 C11 H11 120.0 . . ? C10 C11 C6 120.03(18) . . ? C10 C11 H11 120.0 . . ? C3 C12 C13 133.89(15) . . ? C3 C12 N1 105.69(14) . . ? N1 C12 C13 120.41(14) . . ? C12 C13 H13A 109.5 . . ? C12 C13 H13B 109.5 . . ? C12 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? N2 C14 C16 106.68(12) . . ? O3 C14 C16 129.35(15) . . ? O3 C14 N2 123.97(14) . . ? N2 C15 C17 106.57(12) . . ? O4 C15 C17 130.02(15) . . ? O4 C15 N2 123.40(14) . . ? C14 C16 H16 109.9 . . ? C14 C16 C17 105.95(12) . . ? C14 C16 C18 118.10(13) . . ? C17 C16 H16 109.9 . . ? C18 C16 H16 109.9 . . ? C18 C16 C17 102.60(12) . . ? C15 C17 C16 105.45(12) . . ? C15 C17 H17 109.7 . . ? C15 C17 C20 117.89(13) . . ? C16 C17 H17 109.7 . . ? C20 C17 C16 104.02(12) . . ? C20 C17 H17 109.7 . . ? C16 C18 H18 114.4 . . ? C19 C18 C16 99.66(13) . . ? C19 C18 H18 114.4 . . ? C19 C18 C21 101.43(13) . . ? C21 C18 C16 110.89(12) . . ? C21 C18 H18 114.4 . . ? C18 C19 H19A 112.7 . . ? C18 C19 H19B 112.7 . . ? C18 C19 C20 95.10(12) . . ? H19A C19 H19B 110.2 . . ? C20 C19 H19A 112.7 . . ? C20 C19 H19B 112.7 . . ? C17 C20 H20 114.6 . . ? C19 C20 C17 99.60(12) . . ? C19 C20 H20 114.6 . . ? C19 C20 C22 101.89(12) . . ? C22 C20 C17 110.01(12) . . ? C22 C20 H20 114.6 . . ? C18 C21 H21A 110.9 . . ? C18 C21 H21B 110.9 . . ? C18 C21 C22 104.36(12) . . ? H21A C21 H21B 108.9 . . ? C22 C21 H21A 110.9 . . ? C22 C21 H21B 110.9 . . ? C20 C22 C21 101.59(11) . . ? C20 C22 H22 109.1 . . ? C21 C22 H22 109.1 . . ? C23 C22 C20 114.72(12) . . ? C23 C22 C21 112.83(12) . . ? C23 C22 H22 109.1 . . ? C24 C23 C22 121.08(13) . . ? C33 C23 C22 120.40(13) . . ? C33 C23 C24 118.51(14) . . ? C23 C24 H24 118.6 . . ? C25 C24 C23 122.89(14) . . ? C25 C24 H24 118.6 . . ? C24 C25 C26 120.26(15) . . ? C24 C25 C27 119.26(14) . . ? C27 C25 C26 120.48(14) . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C28 C27 C25 122.16(15) . . ? C28 C27 C32 118.86(15) . . ? C32 C27 C25 118.99(14) . . ? C27 C28 H28 119.6 . . ? C29 C28 C27 120.81(16) . . ? C29 C28 H28 119.6 . . ? C28 C29 H29 119.7 . . ? C28 C29 C30 120.68(16) . . ? C30 C29 H29 119.7 . . ? C29 C30 H30 119.9 . . ? C31 C30 C29 120.17(16) . . ? C31 C30 H30 119.9 . . ? C30 C31 H31 119.4 . . ? C30 C31 C32 121.13(16) . . ? C32 C31 H31 119.4 . . ? C27 C32 C33 119.78(14) . . ? C31 C32 C27 118.29(15) . . ? C31 C32 C33 121.93(15) . . ? C23 C33 C32 120.51(14) . . ? C23 C33 C34 122.22(13) . . ? C32 C33 C34 117.27(13) . . ? C37 C34 C33 119.85(13) . . ? N3 C34 C33 117.07(14) . . ? N3 C34 C37 122.97(14) . . ? C36 C35 H35 120.3 . . ? C36 C35 C38 119.30(16) . . ? C38 C35 H35 120.3 . . ? C35 C36 H36 117.7 . . ? C35 C36 N3 124.63(16) . . ? N3 C36 H36 117.7 . . ? C38 C37 C34 118.30(14) . . ? C39 C37 C34 122.76(14) . . ? C39 C37 C38 118.94(15) . . ? C35 C38 C37 117.40(16) . . ? C35 C38 C42 123.47(16) . . ? C42 C38 C37 119.11(16) . . ? C37 C39 H39 119.8 . . ? C40 C39 C37 120.46(16) . . ? C40 C39 H39 119.8 . . ? C39 C40 H40 119.8 . . ? C39 C40 C41 120.40(18) . . ? C41 C40 H40 119.8 . . ? C40 C41 H41 119.7 . . ? C42 C41 C40 120.56(18) . . ? C42 C41 H41 119.7 . . ? C38 C42 H42 119.7 . . ? C41 C42 C38 120.52(17) . . ? C41 C42 H42 119.7 . . ? C12 N1 C5 111.35(12) . . ? C12 N1 N2 122.97(12) . . ? N2 N1 C5 123.55(13) . . ? C14 N2 C15 115.02(12) . . ? N1 N2 C14 123.51(13) . . ? N1 N2 C15 121.46(12) . . ? C34 N3 C36 117.32(15) . . ? C2 O2 C1 115.26(14) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? C1 O2 1.444(2) . ? C2 C3 1.464(2) . ? C2 O1 1.208(2) . ? C2 O2 1.347(2) . ? C3 C4 1.420(2) . ? C3 C12 1.379(2) . ? C4 H4 0.9500 . ? C4 C5 1.362(2) . ? C5 C6 1.467(2) . ? C5 N1 1.3988(19) . ? C6 C7 1.388(3) . ? C6 C11 1.391(2) . ? C7 H7 0.9500 . ? C7 C8 1.381(3) . ? C8 H8 0.9500 . ? C8 C9 1.376(4) . ? C9 H9 0.9500 . ? C9 C10 1.362(3) . ? C10 H10 0.9500 . ? C10 C11 1.387(3) . ? C11 H11 0.9500 . ? C12 C13 1.485(2) . ? C12 N1 1.379(2) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 C16 1.498(2) . ? C14 N2 1.402(2) . ? C14 O3 1.202(2) . ? C15 C17 1.506(2) . ? C15 N2 1.402(2) . ? C15 O4 1.1996(19) . ? C16 H16 1.0000 . ? C16 C17 1.552(2) . ? C16 C18 1.544(2) . ? C17 H17 1.0000 . ? C17 C20 1.549(2) . ? C18 H18 1.0000 . ? C18 C19 1.529(2) . ? C18 C21 1.537(2) . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C19 C20 1.542(2) . ? C20 H20 1.0000 . ? C20 C22 1.546(2) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 C22 1.573(2) . ? C22 H22 1.0000 . ? C22 C23 1.523(2) . ? C23 C24 1.424(2) . ? C23 C33 1.380(2) . ? C24 H24 0.9500 . ? C24 C25 1.370(2) . ? C25 C26 1.512(2) . ? C25 C27 1.425(2) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 C28 1.419(2) . ? C27 C32 1.425(2) . ? C28 H28 0.9500 . ? C28 C29 1.367(3) . ? C29 H29 0.9500 . ? C29 C30 1.397(3) . ? C30 H30 0.9500 . ? C30 C31 1.371(3) . ? C31 H31 0.9500 . ? C31 C32 1.421(2) . ? C32 C33 1.432(2) . ? C33 C34 1.504(2) . ? C34 C37 1.428(2) . ? C34 N3 1.320(2) . ? C35 H35 0.9500 . ? C35 C36 1.351(3) . ? C35 C38 1.411(3) . ? C36 H36 0.9500 . ? C36 N3 1.371(2) . ? C37 C38 1.418(2) . ? C37 C39 1.415(2) . ? C38 C42 1.413(3) . ? C39 H39 0.9500 . ? C39 C40 1.367(2) . ? C40 H40 0.9500 . ? C40 C41 1.406(3) . ? C41 H41 0.9500 . ? C41 C42 1.362(3) . ? C42 H42 0.9500 . ? N1 N2 1.3839(17) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 C3 C4 C5 174.73(15) . . . . ? C2 C3 C12 C13 5.7(3) . . . . ? C2 C3 C12 N1 -175.55(16) . . . . ? C3 C2 O2 C1 174.77(16) . . . . ? C3 C4 C5 C6 -174.84(15) . . . . ? C3 C4 C5 N1 1.61(18) . . . . ? C3 C12 N1 C5 2.00(17) . . . . ? C3 C12 N1 N2 165.91(14) . . . . ? C4 C3 C12 C13 -179.67(18) . . . . ? C4 C3 C12 N1 -0.94(18) . . . . ? C4 C5 C6 C7 38.6(3) . . . . ? C4 C5 C6 C11 -139.94(19) . . . . ? C4 C5 N1 C12 -2.28(17) . . . . ? C4 C5 N1 N2 -166.07(14) . . . . ? C5 C6 C7 C8 -179.9(2) . . . . ? C5 C6 C11 C10 179.43(16) . . . . ? C5 N1 N2 C14 -111.52(17) . . . . ? C5 N1 N2 C15 69.93(18) . . . . ? C6 C5 N1 C12 174.43(15) . . . . ? C6 C5 N1 N2 10.6(2) . . . . ? C6 C7 C8 C9 0.7(4) . . . . ? C7 C6 C11 C10 0.9(3) . . . . ? C7 C8 C9 C10 0.4(4) . . . . ? C8 C9 C10 C11 -0.8(4) . . . . ? C9 C10 C11 C6 0.2(3) . . . . ? C11 C6 C7 C8 -1.3(3) . . . . ? C12 C3 C4 C5 -0.44(19) . . . . ? C12 N1 N2 C14 86.53(18) . . . . ? C12 N1 N2 C15 -92.03(18) . . . . ? C13 C12 N1 C5 -179.05(15) . . . . ? C13 C12 N1 N2 -15.1(2) . . . . ? C14 C16 C17 C15 2.68(15) . . . . ? C14 C16 C17 C20 127.38(12) . . . . ? C14 C16 C18 C19 -154.55(13) . . . . ? C14 C16 C18 C21 -48.29(18) . . . . ? C15 C17 C20 C19 149.62(14) . . . . ? C15 C17 C20 C22 43.13(18) . . . . ? C16 C14 N2 C15 -4.43(16) . . . . ? C16 C14 N2 N1 176.93(13) . . . . ? C16 C17 C20 C19 33.34(14) . . . . ? C16 C17 C20 C22 -73.16(14) . . . . ? C16 C18 C19 C20 58.99(13) . . . . ? C16 C18 C21 C22 -71.24(16) . . . . ? C17 C15 N2 C14 6.19(17) . . . . ? C17 C15 N2 N1 -175.14(12) . . . . ? C17 C16 C18 C19 -38.54(14) . . . . ? C17 C16 C18 C21 67.72(15) . . . . ? C17 C20 C22 C21 69.14(14) . . . . ? C17 C20 C22 C23 -168.83(12) . . . . ? C18 C16 C17 C15 -121.79(13) . . . . ? C18 C16 C17 C20 2.91(14) . . . . ? C18 C19 C20 C17 -56.63(13) . . . . ? C18 C19 C20 C22 56.34(13) . . . . ? C18 C21 C22 C20 1.33(14) . . . . ? C18 C21 C22 C23 -122.01(13) . . . . ? C19 C18 C21 C22 33.84(14) . . . . ? C19 C20 C22 C21 -35.82(14) . . . . ? C19 C20 C22 C23 86.22(14) . . . . ? C20 C22 C23 C24 -11.47(19) . . . . ? C20 C22 C23 C33 169.49(13) . . . . ? C21 C18 C19 C20 -54.80(13) . . . . ? C21 C22 C23 C24 104.23(16) . . . . ? C21 C22 C23 C33 -74.81(17) . . . . ? C22 C23 C24 C25 -176.84(14) . . . . ? C22 C23 C33 C32 177.47(13) . . . . ? C22 C23 C33 C34 -3.3(2) . . . . ? C23 C24 C25 C26 179.89(16) . . . . ? C23 C24 C25 C27 -0.4(2) . . . . ? C23 C33 C34 C37 -88.49(18) . . . . ? C23 C33 C34 N3 95.25(17) . . . . ? C24 C23 C33 C32 -1.6(2) . . . . ? C24 C23 C33 C34 177.62(13) . . . . ? C24 C25 C27 C28 177.46(15) . . . . ? C24 C25 C27 C32 -2.0(2) . . . . ? C25 C27 C28 C29 179.03(16) . . . . ? C25 C27 C32 C31 -177.64(15) . . . . ? C25 C27 C32 C33 2.6(2) . . . . ? C26 C25 C27 C28 -2.8(2) . . . . ? C26 C25 C27 C32 177.70(15) . . . . ? C27 C28 C29 C30 -0.9(3) . . . . ? C27 C32 C33 C23 -0.8(2) . . . . ? C27 C32 C33 C34 179.98(13) . . . . ? C28 C27 C32 C31 2.8(2) . . . . ? C28 C27 C32 C33 -176.92(14) . . . . ? C28 C29 C30 C31 1.8(3) . . . . ? C29 C30 C31 C32 -0.3(3) . . . . ? C30 C31 C32 C27 -2.0(2) . . . . ? C30 C31 C32 C33 177.74(16) . . . . ? C31 C32 C33 C23 179.48(15) . . . . ? C31 C32 C33 C34 0.2(2) . . . . ? C32 C27 C28 C29 -1.5(2) . . . . ? C32 C33 C34 C37 90.75(17) . . . . ? C32 C33 C34 N3 -85.52(17) . . . . ? C33 C23 C24 C25 2.2(2) . . . . ? C33 C34 C37 C38 -173.89(14) . . . . ? C33 C34 C37 C39 6.5(2) . . . . ? C33 C34 N3 C36 173.95(14) . . . . ? C34 C37 C38 C35 0.1(2) . . . . ? C34 C37 C38 C42 -178.72(15) . . . . ? C34 C37 C39 C40 178.72(17) . . . . ? C35 C36 N3 C34 -0.1(3) . . . . ? C35 C38 C42 C41 -178.96(18) . . . . ? C36 C35 C38 C37 -2.2(2) . . . . ? C36 C35 C38 C42 176.62(17) . . . . ? C37 C34 N3 C36 -2.2(2) . . . . ? C37 C38 C42 C41 -0.2(3) . . . . ? C37 C39 C40 C41 0.2(3) . . . . ? C38 C35 C36 N3 2.3(3) . . . . ? C38 C37 C39 C40 -0.9(3) . . . . ? C39 C37 C38 C35 179.72(15) . . . . ? C39 C37 C38 C42 0.9(2) . . . . ? C39 C40 C41 C42 0.6(3) . . . . ? C40 C41 C42 C38 -0.5(3) . . . . ? N1 C5 C6 C7 -137.24(19) . . . . ? N1 C5 C6 C11 44.2(2) . . . . ? N2 C14 C16 C17 0.76(15) . . . . ? N2 C14 C16 C18 114.96(14) . . . . ? N2 C15 C17 C16 -5.14(15) . . . . ? N2 C15 C17 C20 -120.66(14) . . . . ? N3 C34 C37 C38 2.1(2) . . . . ? N3 C34 C37 C39 -177.43(15) . . . . ? O1 C2 C3 C4 4.9(3) . . . . ? O1 C2 C3 C12 178.86(18) . . . . ? O1 C2 O2 C1 -4.0(3) . . . . ? O2 C2 C3 C4 -173.90(15) . . . . ? O2 C2 C3 C12 0.1(3) . . . . ? O3 C14 C16 C17 -179.57(16) . . . . ? O3 C14 C16 C18 -65.4(2) . . . . ? O3 C14 N2 C15 175.88(15) . . . . ? O3 C14 N2 N1 -2.8(2) . . . . ? O4 C15 C17 C16 175.38(16) . . . . ? O4 C15 C17 C20 59.9(2) . . . . ? O4 C15 N2 C14 -174.29(15) . . . . ? O4 C15 N2 N1 4.4(2) . . . . ?