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Information card for entry 1572154
Preview
Coordinates | 1572154.cif |
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Original paper (by DOI) | HTML |
Formula | C35 H34 N2 O2 |
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Calculated formula | C35 H34 N2 O2 |
Title of publication | Access to distal biaxial atropisomers by iridium catalyzed asymmetric C-H alkylation. |
Authors of publication | Hu, Xueqing; Zhao, Yunxu; He, Tong; Niu, Caoyue; Liu, Feipeng; Jia, Wei; Mu, Yi; Li, Xingwei; Rong, Zi-Qiang |
Journal of publication | Chemical science |
Year of publication | 2024 |
Journal volume | 15 |
Journal issue | 33 |
Pages of publication | 13541 - 13549 |
a | 10.8233 ± 0.0006 Å |
b | 7.0541 ± 0.0004 Å |
c | 18.1771 ± 0.001 Å |
α | 90° |
β | 94.633 ± 0.002° |
γ | 90° |
Cell volume | 1383.26 ± 0.13 Å3 |
Cell temperature | 193 K |
Ambient diffraction temperature | 193 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0321 |
Residual factor for significantly intense reflections | 0.0319 |
Weighted residual factors for significantly intense reflections | 0.0804 |
Weighted residual factors for all reflections included in the refinement | 0.0807 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.088 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
294471 (current) | 2024-09-06 | cif/ Updating files of 1572152, 1572153, 1572154, 1572155 Original log message: Adding full bibliography for 1572152--1572155.cif. |
1572154.cif |
293497 | 2024-07-23 | cif/ Adding structures of 1572152, 1572153, 1572154, 1572155 via cif-deposit CGI script. |
1572154.cif |
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Users of the data should acknowledge the original authors of the
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