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Information card for entry 1572165
Preview
Coordinates | 1572165.cif |
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Original paper (by DOI) | HTML |
Formula | C48 H69 Cl2 N O Ru |
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Calculated formula | C36 H45 Cl2 N O Ru |
Title of publication | Streamlined synthetic assembly of α-chiral CAAC ligands and catalytic performance of their copper and ruthenium complexes. |
Authors of publication | Madron du Vigné, Adrien; Cramer, Nicolai |
Journal of publication | Chemical science |
Year of publication | 2024 |
Journal volume | 15 |
Journal issue | 34 |
Pages of publication | 13864 - 13871 |
a | 18.5489 ± 0.0009 Å |
b | 8.927 ± 0.0004 Å |
c | 27.5267 ± 0.0011 Å |
α | 90° |
β | 109.441 ± 0.005° |
γ | 90° |
Cell volume | 4298.2 ± 0.4 Å3 |
Cell temperature | 140 ± 0.1 K |
Ambient diffraction temperature | 140 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0966 |
Residual factor for significantly intense reflections | 0.0852 |
Weighted residual factors for significantly intense reflections | 0.2177 |
Weighted residual factors for all reflections included in the refinement | 0.2261 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.088 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
294501 (current) | 2024-09-06 | cif/ Updating files of 1572161, 1572162, 1572163, 1572164, 1572165, 1572166 Original log message: Adding full bibliography for 1572161--1572166.cif. |
1572165.cif |
293532 | 2024-07-25 | cif/ Adding structures of 1572161, 1572162, 1572163, 1572164, 1572165, 1572166 via cif-deposit CGI script. |
1572165.cif |
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Users of the data should acknowledge the original authors of the
structural data.