#------------------------------------------------------------------------------ #$Date: 2024-07-26 01:06:42 +0300 (Fri, 26 Jul 2024) $ #$Revision: 293538 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/21/1572169.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572169 loop_ _publ_author_name 'Kundu, Sourav' 'Jana, Debgopal' 'Mandal, Nilangshu' 'Mondal, Ayan' 'Murmu, Ranjit' 'Roy, Nanda Kishore' 'Datta, Ayan' 'Bisai, Alakesh' _publ_section_title ; Biomimetic total synthesis of the reported structure of (+)-selaginedorffone B ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC04103H _journal_year 2024 _chemical_absolute_configuration syn _chemical_formula_moiety '0.5(C42 H43 O6), 0.5(C42 H46 O6)' _chemical_formula_sum 'C42 H46 O6' _chemical_formula_weight 646.79 _space_group_crystal_system triclinic _space_group_IT_number 1 _space_group_name_Hall 'P 1' _space_group_name_H-M_alt 'P 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_block_doi 10.5517/ccdc.csd.cc2ftx06 _audit_creation_date 2023-04-26 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _audit_update_record ; 2023-04-26 deposited with the CCDC. 2024-07-25 downloaded from the CCDC. ; _cell_angle_alpha 86.519(2) _cell_angle_beta 86.864(2) _cell_angle_gamma 67.266(3) _cell_formula_units_Z 2 _cell_length_a 6.2642(3) _cell_length_b 8.0505(2) _cell_length_c 36.8967(6) _cell_measurement_reflns_used 12182 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 68.1220 _cell_measurement_theta_min 2.3740 _cell_volume 1711.99(10) _computing_cell_refinement 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2016/6 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix3000 _diffrn_measured_fraction_theta_full value _diffrn_measured_fraction_theta_max 0.884 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -33.00 29.00 0.50 0.80 -- -40.33 28.00-115.00 124 2 \w -109.00 -27.00 0.50 0.80 -- -40.33 -28.00 82.00 164 3 \w -152.00 -69.00 0.50 3.33 -- -82.50 -28.00 82.00 166 4 \w 84.00 166.00 0.50 3.33 -- 96.67 28.00-115.00 164 5 \w -63.00 27.00 0.50 0.80 -- -40.33 64.00 -60.00 180 6 \w -78.00 4.00 0.50 0.80 -- -40.33 104.00-180.00 164 7 \w -24.00 35.00 0.50 0.80 -- -40.33 12.00 30.00 118 8 \w -24.00 35.00 0.50 0.80 -- -40.33 12.00 120.00 118 9 \w 27.00 110.00 0.50 0.80 -- 40.33 28.00-115.00 166 10 \w -35.00 24.00 0.50 0.80 -- 40.33 -12.00 -90.00 118 11 \w -35.00 24.00 0.50 0.80 -- 40.33 -12.00-150.00 118 12 \w -29.00 33.00 0.50 0.80 -- 40.33 -28.00 82.00 124 13 \w 41.00 99.00 0.50 0.80 -- 40.33-138.00 -90.00 116 14 \w -47.00 -15.00 0.50 3.33 -- -82.50 42.00-150.00 64 15 \w -47.00 -15.00 0.50 3.33 -- -82.50 42.00-120.00 64 16 \w -56.00 -16.00 0.50 3.33 -- -82.50 50.00 -30.00 80 17 \w -47.00 -15.00 0.50 3.33 -- -82.50 42.00-180.00 64 18 \w -149.00 -78.00 0.50 3.33 -- -82.50-117.00-150.00 142 19 \w 30.00 57.00 0.50 3.33 -- 96.67 -50.00-180.00 54 20 \w 30.00 57.00 0.50 3.33 -- 96.67 -50.00-150.00 54 21 \w 30.00 109.00 0.50 3.33 -- 96.67-117.00 -60.00 158 22 \w 44.00 127.00 0.50 3.33 -- 96.67-145.00 30.00 166 23 \w 29.00 83.00 0.50 3.33 -- 96.67 -68.00 30.00 108 24 \w 29.00 68.00 0.50 3.33 -- 96.67 -59.00 60.00 78 25 \w 82.00 167.00 0.50 3.33 -- 96.67 25.00 0.00 170 26 \w 44.00 127.00 0.50 3.33 -- 96.67-145.00-180.00 166 27 \w 29.00 68.00 0.50 3.33 -- 96.67 -59.00 -30.00 78 28 \w 30.00 57.00 0.50 3.33 -- 96.67 -50.00 -30.00 54 29 \w 29.00 68.00 0.50 3.33 -- 96.67 -59.00-180.00 78 30 \w 29.00 83.00 0.50 3.33 -- 96.67 -68.00-180.00 108 31 \w 83.00 164.00 0.50 3.33 -- 96.67 33.00 -90.00 162 32 \w 99.00 164.00 0.50 3.33 -- 96.67 117.00 -60.00 130 33 \w 105.00 170.00 0.50 3.33 -- 96.67 96.00 60.00 130 34 \w 30.00 57.00 0.50 3.33 -- 96.67 -50.00 120.00 54 35 \w 29.00 83.00 0.50 3.33 -- 96.67 -68.00 120.00 108 36 \w 29.00 83.00 0.50 3.33 -- 96.67 -68.00 -60.00 108 37 \w -109.00 -13.00 0.50 0.80 -- -40.33 -77.00 -90.00 192 38 \w -109.00 -13.00 0.50 0.80 -- -40.33 -77.00 0.00 192 39 \w -109.00 -13.00 0.50 0.80 -- -40.33 -77.00 -30.00 192 40 \w -108.00 -17.00 0.50 0.80 -- -40.33 -64.00 30.00 182 41 \w -109.00 -13.00 0.50 0.80 -- -40.33 -77.00 90.00 192 42 \w -108.00 -17.00 0.50 0.80 -- -40.33 -64.00 150.00 182 43 \w -27.00 64.00 0.50 0.80 -- 40.33 -64.00 30.00 182 44 \w 14.00 109.00 0.50 0.80 -- 40.33 77.00-180.00 190 45 \w 14.00 109.00 0.50 0.80 -- 40.33 77.00-120.00 190 46 \w 14.00 109.00 0.50 0.80 -- 40.33 77.00 -60.00 190 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix3000' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0077092000 _diffrn_orient_matrix_UB_12 0.1808219000 _diffrn_orient_matrix_UB_13 0.0128529000 _diffrn_orient_matrix_UB_21 -0.0129411000 _diffrn_orient_matrix_UB_22 -0.0660111000 _diffrn_orient_matrix_UB_23 0.0398227000 _diffrn_orient_matrix_UB_31 0.2663736000 _diffrn_orient_matrix_UB_32 -0.0779328000 _diffrn_orient_matrix_UB_33 0.0008836000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0472 _diffrn_reflns_av_unetI/netI 0.0466 _diffrn_reflns_Laue_measured_fraction_full 0.891 _diffrn_reflns_Laue_measured_fraction_max 0.884 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 44 _diffrn_reflns_limit_l_min -42 _diffrn_reflns_number 17137 _diffrn_reflns_point_group_measured_fraction_full 0.652 _diffrn_reflns_point_group_measured_fraction_max 0.646 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 68.400 _diffrn_reflns_theta_min 2.401 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.658 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.45746 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'metallic whiteish white' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier whiteish _exptl_crystal_colour_primary white _exptl_crystal_density_diffrn 1.255 _exptl_crystal_description needle _exptl_crystal_F_000 692 _exptl_crystal_size_max 0.947 _exptl_crystal_size_mid 0.129 _exptl_crystal_size_min 0.059 _refine_diff_density_max 1.163 _refine_diff_density_min -0.721 _refine_diff_density_rms 0.157 _refine_ls_abs_structure_details ; Flack x determined using 2374 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.07(14) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.828 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 880 _refine_ls_number_reflns 8151 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.828 _refine_ls_R_factor_all 0.1242 _refine_ls_R_factor_gt 0.1227 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3578 _refine_ls_wR_factor_ref 0.3615 _reflns_Friedel_coverage 0.461 _reflns_Friedel_fraction_full 0.413 _reflns_Friedel_fraction_max 0.407 _reflns_number_gt 7862 _reflns_number_total 8151 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04103h3.cif _cod_data_source_block sk-0284_auto_kp260423 _cod_database_code 1572169 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula 'C H O' _chemical_oxdiff_usercomment '100 K' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C00L(H00L), C00V(H00V), C012(H012), C019(H019), C01F(H01Y), C01W(H4), C023(H023), C02L(H02L) 2.b Secondary CH2 refined with riding coordinates: C00C(H00B,H00C), C00J(H00D,H00E), C00K(H00I,H00J), C00X(H00K,H00M), C015(H01A, H01B), C018(H01R,H01S), C01C(H01F,H01G), C01E(H01W,H01X), C01I(H01H,H01I), C01M(H1,HD), C01O(H01J,H01K), C01R(H2,HE), C02A(H02T,H02U), C02C(H02D,H02E) 2.c Aromatic/amide H refined with riding coordinates: C00A(H00A), C00O(H00O), C00R(H00R), C011(H011), C020(H020), C025(H025), C02F(H02F), C02K(H02V) 2.d Idealised Me refined as rotating group: C00P(H00F,H00G,H00H), C01A(H01C,H01D,H01E), C01D(H01T,H01U,H01V), C01K(H01Z,H, HA), C01L(H01,HB,HC), C01S(H3,HF,HG), C01T(H01L,H01M,H01N), C01X(H5,HH,HI), C01Z(H01O,H01P,H01Q), C022(H02A,H02B,H02C), C024(H02N,H02O,H02P), C028(H02Q, H02R,H02S), C02I(H02G,H02H,H02I), C02M(H02J,H02K,H02M), C4(H4A,H4B,H4C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL sk-0284_auto_kp260423_a.res in P1 sk-0284_auto_kp260423.res created by SHELXL-2016/6 at 12:29:18 on 26-Apr-2023 REM Old TITL SK-0284_auto_kp260423 in P-1 REM SHELXT solution in P1 REM R1 0.192, Rweak 0.076, Alpha 0.000, Orientation as input REM Flack x = 0.179 ( 0.109 ) from Parsons' quotients REM Formula found by SHELXT: C81 O13 CELL 1.54184 6.2642 8.0505 36.8967 86.519 86.864 67.266 ZERR 2 0.0003 0.0002 0.0006 0.002 0.002 0.003 LATT -1 SFAC C H O UNIT 84 92 12 L.S. 40 0 0 PLAN 12 CONF BOND $H list 4 MORE -1 ABIN fmap 2 53 acta REM REM REM WGHT 0.200000 FVAR 0.52986 O001 3 0.629475 1.219154 0.044349 11.00000 0.01772 0.01512 = 0.03600 0.00003 0.00066 -0.00357 O002 3 0.520735 0.032019 0.781023 11.00000 0.01943 0.03293 = 0.03565 0.01008 -0.00797 -0.01569 O003 3 0.877343 -0.221094 0.955717 11.00000 0.02546 0.01555 = 0.02710 -0.00226 -0.00787 -0.00609 O004 3 -0.100065 1.839596 0.135048 11.00000 0.04719 0.01401 = 0.03206 -0.00023 0.00380 -0.00313 O005 3 0.206544 0.508905 0.280860 11.00000 0.02743 0.02011 = 0.04369 0.00478 -0.00884 -0.01380 O006 3 0.827667 -0.841573 0.865303 11.00000 0.03863 0.01278 = 0.03311 -0.00127 -0.00578 -0.00205 O007 3 -0.110587 0.490167 0.720773 11.00000 0.02096 0.01565 = 0.04753 0.00255 -0.00047 -0.00242 O008 3 0.413784 0.965479 0.218609 11.00000 0.01835 0.04148 = 0.04005 0.00948 -0.00838 -0.01428 C009 1 0.425948 -0.061549 0.795586 11.00000 0.01421 0.01275 = 0.03320 0.00038 0.00036 -0.00126 C00A 1 0.916849 -0.617029 0.912507 11.00000 0.01252 0.00338 = 0.03528 0.00307 -0.00342 0.00325 AFIX 43 H00A 2 1.003348 -0.740505 0.913900 11.00000 -1.20000 AFIX 0 C00B 1 0.629768 -0.362820 0.880308 11.00000 0.00778 0.01858 = 0.02098 -0.00249 -0.00585 -0.00292 C00C 1 0.439702 -0.093111 0.836500 11.00000 0.01808 0.01203 = 0.03241 0.00022 -0.00207 -0.00593 AFIX 23 H00B 2 0.306099 -0.000654 0.847623 11.00000 -1.20000 H00C 2 0.576401 -0.077315 0.844022 11.00000 -1.20000 AFIX 0 C00D 1 0.721619 -0.675795 0.860946 11.00000 0.03025 0.00755 = 0.02620 -0.00123 -0.00389 -0.00276 C00E 1 0.291750 -0.142148 0.775129 11.00000 0.01419 0.02042 = 0.02852 0.00092 -0.00489 -0.00667 C00F 1 0.214765 0.643333 0.293382 11.00000 0.01704 0.00876 = 0.03442 0.00313 -0.00111 -0.00455 C00G 1 0.951632 -0.511436 0.937526 11.00000 0.01407 0.01292 = 0.02593 0.00103 0.00211 -0.00288 C00H 1 -0.136622 1.330068 0.209609 11.00000 0.02967 0.01708 = 0.02062 0.00109 -0.00429 -0.00987 C00I 1 0.237629 1.062811 0.204059 11.00000 0.02061 0.02056 = 0.03693 0.00411 -0.00809 -0.01152 C00J 1 0.365708 -0.145799 0.734536 11.00000 0.02332 0.01471 = 0.03100 0.00037 0.00041 -0.00753 AFIX 23 H00D 2 0.533061 -0.204606 0.732494 11.00000 -1.20000 H00E 2 0.301635 -0.219118 0.722507 11.00000 -1.20000 AFIX 0 C00K 1 0.048512 1.149502 0.265767 11.00000 0.04325 0.00963 = 0.03301 0.00478 -0.01182 -0.01177 AFIX 23 H00I 2 0.154249 1.209987 0.267828 11.00000 -1.20000 H00J 2 -0.097260 1.221075 0.277734 11.00000 -1.20000 AFIX 0 C00L 1 1.127863 -0.583564 0.967029 11.00000 0.01851 0.01035 = 0.02064 -0.00035 -0.00183 -0.00167 AFIX 13 H00L 2 1.082347 -0.494387 0.985865 11.00000 -1.20000 AFIX 0 C00M 1 0.827975 -0.322226 0.932191 11.00000 0.02183 0.01676 = 0.02014 -0.00231 0.00325 -0.00557 C00N 1 0.113788 0.180032 0.727445 11.00000 0.02284 0.02463 = 0.02226 -0.00286 -0.00509 -0.01009 C00O 1 0.668998 -0.252396 0.905408 11.00000 0.02352 0.01909 = 0.01875 0.00437 -0.00148 -0.00955 AFIX 43 H00O 2 0.584592 -0.128641 0.903742 11.00000 -1.20000 AFIX 0 C00P 1 0.216694 -0.261135 0.870118 11.00000 0.00796 0.00814 = 0.03389 0.00349 -0.00304 0.00125 AFIX 137 H00F 2 0.207617 -0.377476 0.873367 11.00000 -1.50000 H00G 2 0.093715 -0.183884 0.855106 11.00000 -1.50000 H00H 2 0.202317 -0.209474 0.893348 11.00000 -1.50000 AFIX 0 C00Q 1 0.398723 1.510715 0.062837 11.00000 0.01932 0.01912 = 0.02396 0.00848 -0.00687 -0.00923 C00R 1 0.239025 1.617618 0.087283 11.00000 0.02172 0.01500 = 0.02564 0.00122 -0.00274 -0.01060 AFIX 43 H00R 2 0.199726 1.741551 0.085189 11.00000 -1.20000 AFIX 0 C00S 1 0.459499 1.323407 0.067655 11.00000 0.01703 0.01724 = 0.02451 -0.00463 0.00123 -0.00567 C00T 1 0.131230 1.547281 0.115621 11.00000 0.02831 0.01343 = 0.02848 -0.00082 -0.00323 -0.00772 C00U 1 0.445013 0.759615 0.330359 11.00000 0.02215 0.02422 = 0.02862 -0.00159 0.00182 -0.01007 C00V 1 0.520976 1.583883 0.033642 11.00000 0.02696 0.02193 = 0.02095 0.00657 -0.00379 -0.01018 AFIX 13 H00V 2 0.575435 1.495219 0.014704 11.00000 -1.20000 AFIX 0 C00W 1 0.755837 -0.546550 0.884808 11.00000 0.02468 0.01080 = 0.02323 0.00083 0.00002 -0.00546 C00X 1 0.240496 1.094772 0.163406 11.00000 0.02653 0.01907 = 0.02935 -0.00004 -0.00830 -0.00949 AFIX 23 H00K 2 0.205070 1.002075 0.152541 11.00000 -1.20000 H00M 2 0.396491 1.079970 0.155300 11.00000 -1.20000 AFIX 0 C00Y 1 0.070860 1.281651 0.148596 11.00000 0.02296 0.00469 = 0.02382 0.00223 -0.00956 -0.00534 C00Z 1 0.793232 0.738576 0.431108 11.00000 0.03226 0.03417 = 0.03266 -0.00746 -0.00232 -0.00636 C010 1 0.548943 0.756142 0.366185 11.00000 0.03087 0.02334 = 0.02247 0.00178 -0.00642 -0.00683 C011 1 0.354637 1.252595 0.094988 11.00000 0.03600 0.01595 = 0.01725 0.00376 -0.00745 -0.00668 AFIX 43 H011 2 0.395474 1.128496 0.097132 11.00000 -1.20000 AFIX 0 C012 1 0.508819 -0.411571 0.819430 11.00000 0.01123 0.01022 = 0.02628 -0.00350 -0.00364 -0.00080 AFIX 13 H012 2 0.656748 -0.416065 0.808394 11.00000 -1.20000 AFIX 0 C013 1 0.007722 1.140302 0.225264 11.00000 0.02931 0.01446 = 0.01842 0.00495 -0.00178 -0.00907 C014 1 0.293579 0.035479 0.714505 11.00000 0.02629 0.01884 = 0.02377 0.00034 0.00004 0.00039 C015 1 0.544281 -0.600148 0.832607 11.00000 0.02452 0.01201 = 0.02055 -0.00200 -0.00095 -0.00549 AFIX 23 H01A 2 0.397965 -0.601216 0.842432 11.00000 -1.20000 H01B 2 0.590749 -0.677643 0.812072 11.00000 -1.20000 AFIX 0 C016 1 0.127334 0.817885 0.273328 11.00000 0.02517 0.02028 = 0.02297 0.00167 0.00038 -0.00822 C017 1 0.325338 -0.328602 0.790308 11.00000 0.01158 0.01599 = 0.02888 0.00167 -0.00963 -0.00600 C018 1 0.017375 0.822679 0.237310 11.00000 0.02489 0.02148 = 0.02870 0.00098 -0.00434 -0.01362 AFIX 23 H01R 2 0.138182 0.759424 0.219739 11.00000 -1.20000 H01S 2 -0.086118 0.758809 0.240609 11.00000 -1.20000 AFIX 0 C019 1 0.420248 0.053672 0.679025 11.00000 0.04895 0.01394 = 0.03784 -0.00099 0.00978 -0.00330 AFIX 13 H019 2 0.347035 0.022481 0.659131 11.00000 -1.20000 AFIX 0 C01A 1 1.366579 -0.601114 0.952104 11.00000 0.01921 0.01527 = 0.02928 0.00532 -0.00820 -0.00301 AFIX 137 H01C 2 1.413042 -0.683133 0.932659 11.00000 -1.50000 H01D 2 1.476059 -0.646149 0.971082 11.00000 -1.50000 H01E 2 1.361241 -0.485131 0.943156 11.00000 -1.50000 AFIX 0 O01B 3 0.676416 1.155587 0.351936 11.00000 0.06118 0.03150 = 0.10538 0.00526 -0.02736 -0.01249 C01C 1 -0.010400 0.176173 0.763582 11.00000 0.00763 0.02503 = 0.02950 0.00055 -0.00044 -0.00579 AFIX 23 H01F 2 -0.175264 0.242726 0.760854 11.00000 -1.20000 H01G 2 0.041485 0.236543 0.781062 11.00000 -1.20000 AFIX 0 C01D 1 -0.132221 1.260226 0.130414 11.00000 0.02690 0.02639 = 0.02390 0.00352 -0.00754 -0.01239 AFIX 137 H01T 2 -0.074390 1.185690 0.109895 11.00000 -1.50000 H01U 2 -0.240505 1.376623 0.122451 11.00000 -1.50000 H01V 2 -0.208267 1.205018 0.147569 11.00000 -1.50000 AFIX 0 C01E 1 -0.116975 1.011317 0.222152 11.00000 0.01770 0.01755 = 0.02535 -0.00149 -0.00345 -0.00654 AFIX 23 H01W 2 -0.266088 1.059661 0.234977 11.00000 -1.20000 H01X 2 -0.145161 1.005313 0.196768 11.00000 -1.20000 AFIX 0 C01F 1 -0.019452 1.407912 0.181128 11.00000 0.02205 0.00734 = 0.02721 0.00238 -0.00666 -0.00228 AFIX 13 H01Y 2 0.117112 1.412190 0.192134 11.00000 -1.20000 AFIX 0 C01G 1 0.449433 -0.281117 0.851895 11.00000 0.01502 0.01038 = 0.03032 -0.00320 -0.00710 -0.00283 C01H 1 0.040038 0.356558 0.707977 11.00000 0.01541 0.02452 = 0.02843 -0.00364 -0.00566 -0.00542 C01I 1 0.156728 0.370876 0.671742 11.00000 0.02549 0.02859 = 0.03060 0.00077 -0.00176 -0.00814 AFIX 23 H01H 2 0.142878 0.494326 0.666873 11.00000 -1.20000 H01I 2 0.079580 0.339630 0.652739 11.00000 -1.20000 AFIX 0 C01J 1 -0.357356 1.420692 0.221209 11.00000 0.03297 0.02927 = 0.02587 0.00146 0.00684 -0.00731 C01K 1 0.361788 1.763501 0.015369 11.00000 0.02531 0.01426 = 0.03369 0.00544 -0.00355 -0.00281 AFIX 137 H01Z 2 0.230572 1.748886 0.005937 11.00000 -1.50000 H 2 0.446100 1.798040 -0.004132 11.00000 -1.50000 HA 2 0.309645 1.855334 0.032933 11.00000 -1.50000 AFIX 0 C01L 1 0.735692 1.599194 0.048561 11.00000 0.02302 0.01167 = 0.03329 0.00326 -0.00061 -0.00280 AFIX 137 H01 2 0.691510 1.672012 0.069470 11.00000 -1.50000 HB 2 0.805125 1.654004 0.030222 11.00000 -1.50000 HC 2 0.845058 1.481164 0.055344 11.00000 -1.50000 AFIX 0 C01M 1 -0.163733 1.599298 0.167838 11.00000 0.01989 0.00925 = 0.03477 -0.00529 -0.00378 -0.00313 AFIX 23 H1 2 -0.305537 1.601197 0.158142 11.00000 -1.20000 HD 2 -0.206151 1.676741 0.188377 11.00000 -1.20000 AFIX 0 C01N 1 0.536590 0.256600 0.635320 11.00000 0.02524 0.01909 = 0.05049 0.01133 -0.00471 -0.00393 C01O 1 0.030326 -0.013942 0.778323 11.00000 0.02312 0.02107 = 0.02333 0.00021 -0.00241 -0.01265 AFIX 23 H01J 2 -0.060627 -0.061964 0.764970 11.00000 -1.20000 H01K 2 -0.021680 -0.009724 0.803626 11.00000 -1.20000 AFIX 0 C01P 1 -0.043516 1.673960 0.139454 11.00000 0.01711 0.00542 = 0.03536 -0.00047 -0.00796 0.00180 C01Q 1 0.187908 1.363227 0.119626 11.00000 0.02769 0.01127 = 0.02355 0.00038 -0.00232 -0.00912 C01R 1 0.314011 0.632200 0.330228 11.00000 0.04585 0.01041 = 0.03121 -0.00170 -0.00602 -0.01331 AFIX 23 H2 2 0.418992 0.509381 0.335873 11.00000 -1.20000 HE 2 0.190033 0.665953 0.348657 11.00000 -1.20000 AFIX 0 C01S 1 0.708252 1.031778 0.049620 11.00000 0.03306 0.01809 = 0.02897 -0.00188 -0.00105 -0.00461 AFIX 137 H3 2 0.821438 0.975356 0.030902 11.00000 -1.50000 HF 2 0.580273 0.994780 0.048661 11.00000 -1.50000 HG 2 0.777114 0.996590 0.072915 11.00000 -1.50000 AFIX 0 C01T 1 1.129579 -0.759596 0.984871 11.00000 0.03320 0.02554 = 0.02881 0.00624 -0.01128 -0.01015 AFIX 137 H01L 2 0.979079 -0.740607 0.995508 11.00000 -1.50000 H01M 2 1.242216 -0.800132 1.003442 11.00000 -1.50000 H01N 2 1.168524 -0.849058 0.966915 11.00000 -1.50000 AFIX 0 C01U 1 0.618813 0.432949 0.585991 11.00000 0.03456 0.05956 = 0.07485 0.03160 0.00492 -0.00466 C01V 1 0.412114 0.246130 0.671149 11.00000 0.02276 0.02043 = 0.02918 0.00265 0.00015 -0.00213 C01W 1 0.916593 0.726259 0.465480 11.00000 0.04060 0.02671 = 0.02570 -0.00229 -0.01190 -0.00622 AFIX 13 H4 2 0.983946 0.598165 0.473012 11.00000 -1.20000 AFIX 0 C01X 1 0.748901 0.820918 0.495923 11.00000 0.03781 0.04150 = 0.04500 0.00812 -0.00937 -0.01428 AFIX 137 H5 2 0.827759 0.792937 0.518447 11.00000 -1.50000 HH 2 0.622709 0.780896 0.497707 11.00000 -1.50000 HI 2 0.690129 0.948816 0.490877 11.00000 -1.50000 AFIX 0 C01Y 1 0.201115 -0.419901 0.778545 11.00000 0.04022 0.01556 = 0.03858 0.00007 -0.00645 -0.01508 C01Z 1 0.532081 0.301839 0.700145 11.00000 0.02003 0.09916 = 0.04007 -0.00853 0.00591 -0.03702 AFIX 137 H01O 2 0.694135 0.226659 0.699560 11.00000 -1.50000 H01P 2 0.465035 0.288588 0.723620 11.00000 -1.50000 H01Q 2 0.512730 0.425402 0.695542 11.00000 -1.50000 AFIX 0 C020 1 0.485872 0.418441 0.616548 11.00000 0.03839 0.03534 = 0.07662 0.01920 0.02264 -0.00313 AFIX 43 H020 2 0.361494 0.519560 0.624285 11.00000 -1.20000 AFIX 0 C021 1 0.800831 0.291943 0.571447 11.00000 0.04579 0.05746 = 0.05366 0.02255 -0.00070 -0.00056 C022 1 0.765132 -0.030571 0.950714 11.00000 0.03683 0.00862 = 0.02948 0.00438 -0.00706 -0.00121 AFIX 137 H02A 2 0.792454 0.005029 0.926161 11.00000 -1.50000 H02B 2 0.825629 0.027021 0.967154 11.00000 -1.50000 H02C 2 0.601655 0.004698 0.955456 11.00000 -1.50000 AFIX 0 C023 1 0.272148 0.951961 0.320696 11.00000 0.07548 0.01357 = 0.04369 0.01705 -0.04039 -0.01856 AFIX 13 H023 2 0.158365 0.996575 0.340735 11.00000 -1.20000 AFIX 0 C024 1 0.648613 0.692434 0.301914 11.00000 0.02918 0.14427 = 0.02980 -0.02707 0.01072 -0.04286 AFIX 137 H02N 2 0.744041 0.760737 0.303118 11.00000 -1.50000 H02O 2 0.588248 0.707885 0.278034 11.00000 -1.50000 H02P 2 0.739456 0.567135 0.307001 11.00000 -1.50000 AFIX 0 C025 1 0.749952 0.873974 0.405498 11.00000 0.07860 0.02457 = 0.08145 0.00404 -0.04134 -0.00851 AFIX 43 H025 2 0.812348 0.960304 0.407901 11.00000 -1.20000 AFIX 0 C026 1 0.148430 0.963146 0.285355 11.00000 0.03478 0.02959 = 0.02612 0.00463 -0.00768 -0.01481 C027 1 0.616286 0.889131 0.375818 11.00000 0.23396 0.04561 = 0.08442 0.04405 -0.12184 -0.07263 C028 1 1.112276 0.784671 0.458967 11.00000 0.02841 0.11987 = 0.04069 0.01089 -0.01027 -0.02963 AFIX 137 H02Q 2 1.053743 0.912723 0.454138 11.00000 -1.50000 H02R 2 1.205036 0.724910 0.438460 11.00000 -1.50000 H02S 2 1.205251 0.754350 0.480068 11.00000 -1.50000 AFIX 0 C029 1 0.731888 0.597658 0.421416 11.00000 0.16704 0.03363 = 0.09610 0.02479 -0.09540 -0.03309 C02A 1 0.437482 1.065694 0.316496 11.00000 0.05722 0.04987 = 0.04452 -0.00153 0.00273 -0.01469 AFIX 23 H02T 2 0.536453 1.028521 0.294891 11.00000 -1.20000 H02U 2 0.340527 1.192360 0.312786 11.00000 -1.20000 AFIX 0 O02B 3 0.742220 0.470697 0.450152 11.00000 0.21271 0.04165 = 0.09226 0.02607 -0.07518 -0.05313 C02C 1 0.687085 -0.081661 0.679601 11.00000 0.06310 0.05993 = 0.06552 0.02775 0.03215 0.02913 AFIX 23 H02D 2 0.749699 -0.072272 0.702509 11.00000 -1.20000 H02E 2 0.695107 -0.204052 0.678569 11.00000 -1.20000 AFIX 0 C02D 1 0.587168 1.045301 0.348069 11.00000 0.06404 0.03181 = 0.05137 0.00071 0.00189 -0.01733 O02E 3 0.572757 0.598176 0.568268 11.00000 0.16466 0.07318 = 0.16500 0.05700 0.10479 -0.00373 C02F 1 0.862256 0.136886 0.592451 11.00000 0.05814 0.04392 = 0.08448 0.01918 0.03939 0.00103 AFIX 43 H02F 2 0.991793 0.038238 0.585189 11.00000 -1.20000 AFIX 0 O02G 3 1.029434 -0.157010 0.642924 11.00000 0.07409 0.04797 = 0.11734 0.00733 0.03139 -0.00582 C02H 1 0.838741 -0.047873 0.648771 11.00000 0.03093 0.04006 = 0.09037 -0.00331 0.01262 0.00090 C02I 1 1.113207 0.167467 0.524123 11.00000 0.04226 0.22088 = 0.06821 0.01107 -0.00621 -0.06073 AFIX 137 H02G 2 1.222050 0.098862 0.542055 11.00000 -1.50000 H02H 2 1.193481 0.202989 0.504172 11.00000 -1.50000 H02I 2 1.037115 0.095086 0.515505 11.00000 -1.50000 AFIX 0 C02J 1 0.740837 0.117680 0.624470 11.00000 0.10038 0.04394 = 0.06604 0.00618 0.04452 -0.00270 C02K 1 0.642323 0.600403 0.387802 11.00000 0.17735 0.01556 = 0.08860 0.01384 -0.08646 -0.03364 AFIX 43 H02V 2 0.645061 0.492972 0.379400 11.00000 -1.20000 AFIX 0 C02L 1 0.945249 0.324188 0.539930 11.00000 0.10058 0.07742 = 0.05705 0.03082 0.02639 -0.01480 AFIX 13 H02L 2 0.843466 0.400379 0.521090 11.00000 -1.20000 AFIX 0 C02M 1 1.100521 0.418195 0.552722 11.00000 0.09409 0.18068 = 0.09238 0.07695 -0.03422 -0.08738 AFIX 137 H02J 2 1.008016 0.543001 0.556393 11.00000 -1.50000 H02K 2 1.219972 0.408845 0.534576 11.00000 -1.50000 H02M 2 1.169711 0.360941 0.575117 11.00000 -1.50000 AFIX 0 C4 1 0.348998 0.742991 0.572911 11.00000 0.03409 0.13544 = 0.28121 0.14080 0.01224 0.02185 AFIX 137 H4A 2 0.318875 0.768526 0.598187 11.00000 -1.50000 H4B 2 0.231314 0.707883 0.564310 11.00000 -1.50000 H4C 2 0.348155 0.848772 0.559322 11.00000 -1.50000 AFIX 0 C14 1 0.659811 0.339540 0.444030 11.00000 0.45056 0.07921 = 0.21388 0.05743 -0.22376 -0.15749 HKLF 4 REM sk-0284_auto_kp260423_a.res in P1 REM R1 = 0.1227 for 7862 Fo > 4sig(Fo) and 0.1242 for all 8151 data REM 880 parameters refined using 3 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 1.163, deepest hole -0.721, 1-sigma level 0.157 Q1 1 0.9838 0.4456 0.4213 11.00000 0.05 1.16 Q2 1 0.6027 0.9017 0.4199 11.00000 0.05 1.05 Q3 1 0.2746 1.1168 0.3402 11.00000 0.05 0.99 Q4 1 0.8349 -0.2233 0.6171 11.00000 0.05 0.96 Q5 1 0.7071 0.3576 0.5001 11.00000 0.05 0.94 Q6 1 0.5443 0.7573 0.6003 11.00000 0.05 0.93 Q7 1 -0.1180 1.3145 0.1673 11.00000 0.05 0.86 Q8 1 0.6950 -0.0933 0.6238 11.00000 0.05 0.84 Q9 1 0.6530 1.2043 0.0134 11.00000 0.05 0.78 Q10 1 0.7515 0.1003 0.5799 11.00000 0.05 0.78 Q11 1 0.3687 1.0999 0.3761 11.00000 0.05 0.77 Q12 1 0.2832 -0.2972 0.8268 11.00000 0.05 0.77 ; _shelx_res_checksum 20999 _shelx_hkl_file ; 0 0 2 609.39 31.50 0 0 -2 651.33 31.58 0 0 2 671.50 31.56 0 0 2 638.84 31.59 0 0 -3 36.08 1.43 0 0 -3 22.62 1.26 0 0 3 21.19 1.15 0 0 3 26.30 1.18 0 0 3 21.26 1.23 0 0 3 41.64 1.38 0 0 3 20.87 1.28 0 0 -3 38.44 1.42 0 0 4 75.81 2.91 0 0 -4 69.09 3.05 0 0 4 59.44 2.87 0 0 4 69.45 3.03 0 0 4 56.68 3.01 0 0 4 62.50 2.99 0 0 4 59.61 3.05 0 0 -5 1.82 0.40 0 0 -5 1.81 0.40 0 0 -5 1.82 0.36 0 0 5 1.33 0.24 0 0 5 2.00 0.26 0 0 -5 1.38 0.35 0 0 5 1.48 0.32 0 0 5 2.12 0.38 0 0 5 1.46 0.35 0 0 5 1.59 0.41 0 0 -6 100.11 4.28 0 0 -6 95.32 4.16 0 0 -6 82.38 4.04 0 0 6 101.06 3.96 0 0 6 86.37 4.08 0 0 6 82.31 4.13 0 0 6 97.75 4.14 0 0 6 81.84 4.17 0 0 -6 81.67 4.11 0 0 -6 81.08 4.11 0 0 -7 11.23 1.06 0 0 -7 13.84 1.01 0 0 -7 15.02 1.06 0 0 7 14.62 0.87 0 0 7 11.95 1.00 0 0 7 12.43 0.97 0 0 7 12.13 0.94 0 0 7 13.50 1.09 0 0 -7 13.33 1.03 0 0 -7 13.40 1.08 0 0 7 14.20 1.14 0 0 -8 231.76 10.19 0 0 -8 225.25 9.97 0 0 -8 222.02 10.04 0 0 8 270.77 9.86 0 0 8 209.18 9.98 0 0 8 216.12 9.88 0 0 8 212.90 9.98 0 0 8 253.72 10.19 0 0 8 234.52 10.21 0 0 -8 225.80 10.07 0 0 -9 25.12 1.77 0 0 -9 23.19 1.62 0 0 -9 25.34 1.58 0 0 9 24.16 1.39 0 0 9 22.39 1.63 0 0 9 22.30 1.48 0 0 9 20.67 1.50 0 0 9 23.76 1.60 0 0 9 23.33 1.74 0 0 -9 20.95 1.58 0 0 -10 181.93 7.86 0 0 10 178.93 7.36 0 0 -10 155.16 7.49 0 0 -10 167.29 7.62 0 0 10 163.97 7.69 0 0 10 168.42 7.60 0 0 10 156.66 7.41 0 0 -10 149.78 7.57 0 0 10 172.23 7.85 0 0 -10 176.88 7.77 0 0 -11 957.46 42.14 0 0 -11 959.34 41.82 0 0 11 1071.08 41.66 0 0 -11 1081.74 42.03 0 0 11 1023.92 42.10 0 0 11 920.53 41.84 0 0 11 1045.01 42.25 0 0 -11 949.14 41.93 0 0 -11 1013.04 42.08 0 0 11 1073.59 42.36 0 0 -12 963.68 43.67 0 0 12 1109.01 43.20 0 0 -12 1041.68 43.54 0 0 -12 945.47 43.32 0 0 12 914.58 43.35 0 0 12 1164.72 43.77 0 0 -12 1086.44 43.72 0 0 -12 1057.35 43.56 0 0 12 1120.38 43.92 0 0 12 1113.31 44.03 0 0 -13 1.89 0.78 0 0 -13 1.08 0.60 0 0 -13 1.78 0.69 0 0 13 1.75 0.58 0 0 13 1.17 0.64 0 0 13 2.55 0.73 0 0 13 1.66 0.80 0 0 -13 2.15 0.67 0 0 13 2.08 0.80 0 0 -14 543.69 23.48 0 0 -14 530.49 23.06 0 0 14 544.12 22.83 0 0 -14 548.90 23.24 0 0 14 536.83 23.36 0 0 14 560.44 23.64 0 0 14 475.53 23.49 0 0 -14 572.64 23.46 0 0 -15 4.33 1.02 0 0 15 6.42 0.92 0 0 -15 5.13 0.97 0 0 15 5.39 1.08 0 0 15 5.32 1.16 0 0 -15 6.35 1.07 0 0 15 6.50 1.22 0 0 -16 286.05 13.68 0 0 -16 290.55 13.47 0 0 16 285.39 13.10 0 0 16 308.37 13.68 0 0 16 292.85 13.86 0 0 -16 319.32 13.78 0 0 16 288.88 13.94 0 0 -17 31.87 2.69 0 0 -17 28.72 2.39 0 0 17 25.77 2.14 0 0 17 27.53 2.48 0 0 17 33.20 2.83 0 0 17 32.55 2.82 0 0 -17 32.54 2.58 0 0 -18 514.93 22.10 0 0 -18 477.48 20.43 0 0 18 440.30 21.20 0 0 -18 553.55 21.85 0 0 18 513.77 22.02 0 0 -18 487.03 21.90 0 0 18 519.40 22.36 0 0 18 492.68 22.32 0 0 -19 38.66 3.22 0 0 -19 37.25 2.08 0 0 -19 40.48 3.04 0 0 19 38.28 2.79 0 0 19 41.50 3.22 0 0 19 43.14 3.49 0 0 -19 39.42 3.17 0 0 19 45.47 3.57 0 0 -20 338.76 14.77 0 0 -20 356.71 16.55 0 0 -20 387.55 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3.90 0 -3 -6 60.53 3.30 0 3 7 408.62 19.07 0 3 7 440.50 18.82 0 -3 -7 450.96 19.27 0 3 7 479.46 19.68 0 -3 -7 471.41 18.99 0 3 8 12.43 1.57 0 3 8 13.03 1.46 0 -3 -8 14.45 1.79 0 3 8 13.80 1.79 0 -3 -8 11.02 1.62 0 -3 -8 11.99 1.49 0 -3 -9 109.72 6.74 0 3 9 119.68 7.03 0 -3 -9 131.45 6.59 0 3 10 79.55 4.64 0 3 10 75.19 4.23 0 -3 -10 59.76 4.35 0 3 10 78.40 4.85 0 -3 -10 62.34 4.06 0 3 11 22.42 2.23 0 -3 -11 16.48 2.04 0 3 11 23.39 2.44 0 -3 -11 19.44 1.91 0 3 12 387.32 17.11 0 -3 -12 349.92 16.94 0 3 12 352.24 17.17 0 -3 -12 368.94 16.51 0 3 13 200.42 9.92 0 -3 -13 178.36 9.77 0 3 13 184.12 9.97 0 -3 -13 190.37 9.31 0 3 14 4.79 1.29 0 -3 -14 5.22 1.34 0 3 14 3.16 1.16 0 -3 -14 4.91 1.12 0 3 15 39.36 3.33 0 -3 -15 34.64 2.01 0 -3 -15 37.47 3.32 0 3 15 38.01 3.46 0 -3 -15 36.77 2.85 0 3 16 4.50 1.39 0 -3 -16 5.63 1.44 0 -3 -16 4.92 0.72 0 3 16 5.57 1.52 0 -3 -16 5.38 1.18 0 -3 -17 229.90 9.81 0 -3 -17 221.59 11.72 0 3 17 196.55 11.67 0 3 17 230.36 11.72 0 -3 -18 117.20 7.74 0 -3 -18 135.81 6.14 0 -3 -18 132.67 6.05 0 3 18 133.48 8.28 0 3 18 151.77 8.21 0 -3 -19 40.99 3.76 0 -3 -19 40.35 2.32 0 -3 -19 40.16 2.24 0 3 19 35.67 3.75 0 3 19 45.40 3.87 0 -3 -20 74.39 3.59 0 -3 -20 60.81 5.03 0 -3 -20 68.06 3.46 0 3 20 65.53 5.39 0 3 20 65.76 5.08 0 -3 -21 4.75 1.52 0 -3 -21 8.22 0.95 0 -3 -21 7.00 0.86 0 3 21 8.47 1.88 0 3 21 6.84 1.61 0 -3 -22 159.16 9.16 0 -3 -22 141.51 6.65 0 -3 -22 145.56 6.57 0 3 22 149.68 9.29 0 -3 -23 6.20 0.90 0 -3 -23 3.60 1.45 0 -3 -23 7.03 0.89 0 -3 -23 4.73 1.47 0 3 23 6.55 1.90 0 3 23 4.20 1.37 0 -3 -24 44.49 4.23 0 3 24 43.56 4.77 0 -3 -24 52.28 4.79 0 -3 -24 47.04 2.84 0 -3 -24 52.09 2.80 0 -3 -25 15.27 2.36 0 3 25 12.96 2.52 0 -3 -25 12.27 1.25 0 3 25 11.37 1.25 0 -3 -25 11.75 1.17 0 3 26 14.38 2.77 0 -3 -26 16.44 2.58 0 -3 -26 14.79 2.67 0 -3 -26 19.35 1.58 0 3 26 18.24 1.54 0 -3 -26 14.77 1.38 0 -3 -27 9.41 2.05 0 3 27 12.45 2.60 0 3 27 10.60 1.24 0 -3 -27 12.48 1.29 0 -3 -27 8.78 2.08 0 -3 -27 10.59 1.17 0 -3 -28 19.83 3.09 0 -3 -28 21.89 1.71 0 -3 -28 17.06 2.95 0 -3 -28 23.78 1.81 0 3 28 23.14 1.83 0 -3 -29 17.41 1.55 0 -3 -29 19.47 1.65 0 3 29 20.12 1.70 0 -3 -30 18.74 1.63 0 3 30 17.04 1.63 0 -3 -31 13.37 1.38 0 3 31 12.64 1.41 0 3 32 46.04 2.88 0 3 33 2.67 0.92 0 3 34 13.24 1.41 0 3 35 16.66 1.54 0 3 35 19.08 1.63 0 3 36 -0.58 0.71 0 3 36 0.10 0.73 0 3 37 0.68 0.63 0 3 37 0.57 0.69 0 3 38 0.25 0.57 0 3 38 0.31 0.61 0 3 39 0.52 0.58 0 3 40 0.22 0.51 0 3 41 5.11 0.73 0 3 42 7.83 0.78 0 4 -38 13.96 1.12 0 4 -37 16.49 1.28 0 -4 36 0.22 0.46 0 4 -36 0.44 0.50 0 4 -36 0.46 0.55 0 -4 35 0.87 0.55 0 4 -35 0.87 0.57 0 4 -35 0.46 0.58 0 4 -34 36.13 2.20 0 -4 34 31.76 2.02 0 -4 33 1.43 0.63 0 4 -33 1.40 0.67 0 -4 32 0.65 0.63 0 4 -32 1.73 0.72 0 -4 31 2.19 0.75 0 4 -31 3.94 0.87 0 -4 31 2.47 0.80 0 -4 30 7.83 1.13 0 4 -30 8.92 1.12 0 -4 30 7.84 1.07 0 4 -29 116.81 5.63 0 -4 29 109.93 5.51 0 -4 29 109.00 5.44 0 -4 28 18.93 1.67 0 4 -28 20.29 1.73 0 -4 28 19.78 1.63 0 -4 27 0.75 0.68 0 -4 27 1.58 0.78 0 4 -27 1.18 0.74 0 -4 26 7.73 1.11 0 -4 26 10.55 1.27 0 4 -26 8.45 1.19 0 -4 25 0.20 0.71 0 -4 25 0.89 0.75 0 4 -25 1.05 0.74 0 -4 24 240.56 10.92 0 4 -24 253.38 11.10 0 -4 24 242.36 10.97 0 -4 23 91.49 4.78 0 4 -23 105.31 5.02 0 -4 23 96.46 4.86 0 4 -23 108.45 7.77 0 -4 22 4.87 0.90 0 -4 22 2.11 1.32 0 -4 22 1.97 1.37 0 -4 22 3.60 0.84 0 4 -22 3.13 0.87 0 -4 22 4.63 0.91 0 4 -22 2.47 1.45 0 -4 21 134.58 6.37 0 -4 21 135.67 8.74 0 -4 21 138.12 6.44 0 4 -21 117.13 8.73 0 4 -21 143.63 6.57 0 -4 21 130.59 6.36 0 -4 20 73.35 3.84 0 -4 20 74.71 5.90 0 -4 20 73.40 3.88 0 4 -20 78.76 4.02 0 -4 20 77.66 3.89 0 -4 19 27.24 1.84 0 -4 19 20.47 3.02 0 4 -19 22.72 3.27 0 -4 19 28.27 1.89 0 4 -19 28.10 1.95 0 -4 19 25.28 1.80 0 -4 18 10.74 1.12 0 -4 18 11.87 2.21 0 -4 18 10.58 1.12 0 4 -18 13.58 2.42 0 -4 18 10.94 1.12 0 -4 17 0.55 0.88 0 -4 17 1.48 0.59 0 -4 17 1.03 0.58 0 4 -17 1.05 1.02 0 -4 17 1.04 0.62 0 -4 16 0.70 0.55 0 4 -16 0.20 1.01 0 -4 16 0.32 0.58 0 4 -16 -0.18 0.98 0 -4 16 0.44 0.56 0 -4 16 0.70 0.98 0 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-4 6 27.40 2.50 0 4 -6 26.54 2.69 0 -4 5 101.94 4.76 0 -4 5 110.10 6.44 0 4 -5 99.81 6.53 0 4 -5 104.52 6.18 0 -4 4 231.01 9.97 0 -4 4 226.33 11.61 0 -4 4 220.56 11.09 0 4 -4 236.71 11.61 0 4 -4 244.24 12.05 0 -4 3 641.13 26.87 0 -4 3 684.27 28.82 0 -4 3 625.19 27.69 0 4 -3 600.62 28.24 0 4 -3 729.35 28.78 0 -4 2 1118.65 46.94 0 -4 2 1060.87 45.06 0 -4 2 1044.02 45.86 0 4 -2 1128.72 46.76 0 -4 1 197.50 8.56 0 -4 1 197.88 10.23 0 -4 1 181.66 8.53 0 -4 1 199.52 9.29 0 4 -1 213.17 10.00 0 -4 0 6.51 0.71 0 -4 0 6.97 1.05 0 4 0 6.29 1.25 0 4 0 7.96 1.42 0 -4 -1 10.88 0.92 0 4 1 12.17 1.67 0 4 1 11.86 1.66 0 -4 -1 10.29 1.28 0 -4 -2 138.91 6.12 0 -4 -2 135.58 7.87 0 4 2 132.28 7.33 0 -4 -2 136.30 6.75 0 -4 -3 10.84 0.90 0 -4 -3 9.03 1.66 0 4 3 6.04 1.36 0 4 3 11.21 1.58 0 -4 -3 8.42 1.16 0 4 4 113.90 7.36 0 -4 -4 127.46 7.90 0 -4 -5 10.58 0.92 0 -4 -5 7.03 1.61 0 4 5 10.07 1.64 0 4 5 8.17 1.42 0 4 5 9.94 1.77 0 4 5 9.26 1.76 0 -4 -6 51.41 2.51 0 -4 -6 40.55 3.68 0 4 6 45.00 3.58 0 4 6 44.91 3.38 0 4 6 42.77 3.81 0 -4 -7 16.94 1.22 0 -4 -7 13.40 2.08 0 4 7 21.85 2.27 0 4 7 18.99 2.01 0 4 7 18.55 2.46 0 4 7 21.09 2.48 0 -4 -8 38.18 2.18 0 -4 -8 43.74 3.66 0 4 8 38.28 3.06 0 4 8 49.35 3.64 0 4 8 41.21 3.67 0 -4 -8 43.08 3.55 0 4 8 40.99 3.68 0 -4 -9 9.59 0.91 0 -4 -9 8.22 1.66 0 4 9 12.05 1.65 0 4 9 11.15 1.75 0 4 9 8.34 1.73 0 4 9 10.92 1.91 0 -4 -9 9.69 1.72 0 -4 -10 4.95 0.67 0 4 10 4.77 1.31 0 4 10 4.44 1.11 0 4 10 4.13 1.41 0 -4 -10 4.94 1.42 0 -4 -10 4.86 1.35 0 4 11 5.12 1.36 0 4 11 4.51 1.14 0 4 11 3.40 1.27 0 -4 -11 5.09 1.43 0 -4 -11 4.71 1.34 0 4 12 46.95 3.81 0 -4 -12 36.56 3.49 0 -4 -12 37.69 2.08 0 -4 -12 34.35 3.44 0 4 12 37.21 3.64 0 -4 -13 3.45 1.05 0 4 13 3.85 1.26 0 -4 -13 2.90 1.21 0 -4 -13 4.66 0.65 0 -4 -13 3.44 1.31 0 4 13 4.71 1.51 0 -4 -14 175.41 9.23 0 -4 -14 182.89 10.05 0 -4 -14 173.50 7.81 0 -4 -14 160.68 9.78 0 4 14 186.35 10.39 0 -4 -15 23.66 2.54 0 4 15 33.57 3.38 0 -4 -15 28.53 1.73 0 -4 -15 23.29 2.95 0 4 15 29.86 3.37 0 -4 -15 28.19 3.11 0 4 16 52.57 4.57 0 -4 -16 54.34 2.87 0 -4 -16 51.67 4.49 0 4 16 65.57 5.16 0 -4 -16 50.05 4.49 0 4 17 1.86 1.20 0 -4 -17 1.99 0.55 0 -4 -17 1.27 1.13 0 4 17 3.54 1.40 0 -4 -17 2.41 1.11 0 4 18 25.41 3.22 0 -4 -18 33.43 1.93 0 4 18 29.97 3.63 0 -4 -18 24.33 3.23 0 -4 -18 25.79 3.24 0 4 19 1.39 1.13 0 4 19 1.36 1.16 0 -4 -19 0.98 1.12 0 -4 -19 1.40 0.56 0 -4 -19 2.40 1.32 0 4 20 -0.20 0.91 0 -4 -20 1.01 1.13 0 4 20 0.47 1.06 0 -4 -20 1.20 0.56 0 -4 -20 0.41 1.00 0 4 21 1.04 1.00 0 -4 -21 1.16 0.59 0 -4 -21 0.63 1.08 0 4 21 1.96 1.43 0 -4 -21 0.21 1.03 0 4 22 6.37 1.80 0 -4 -22 9.24 1.03 0 -4 -22 6.49 1.89 0 4 22 7.32 2.06 0 -4 -22 7.69 1.98 0 4 23 3.05 1.33 0 -4 -23 1.71 0.67 0 -4 -23 1.11 1.11 0 4 23 2.86 1.59 0 -4 -23 0.45 1.06 0 4 24 9.90 2.17 0 -4 -24 12.06 1.21 0 -4 -24 11.18 2.12 0 4 24 11.18 2.52 0 -4 -24 12.82 2.50 0 -4 -24 11.15 2.32 0 -4 -25 0.10 0.61 0 -4 -25 0.23 1.13 0 -4 -25 0.24 1.07 0 4 26 128.58 6.41 0 -4 -26 133.68 6.29 0 4 27 41.48 2.66 0 -4 -27 39.18 2.50 0 4 28 193.03 8.64 0 -4 -28 176.66 8.43 0 4 29 15.10 1.55 0 -4 -29 17.06 1.50 0 4 30 96.54 5.00 0 -4 -30 97.01 4.90 0 4 31 11.71 1.37 0 4 32 49.62 2.99 0 4 33 5.40 1.02 0 4 34 60.57 3.38 0 4 35 32.81 2.16 0 4 36 3.33 0.78 0 4 36 4.12 0.81 0 4 37 26.88 1.76 0 4 37 23.98 1.67 0 4 38 11.39 1.08 0 4 39 5.11 0.74 0 4 40 0.08 0.41 0 -5 34 3.99 0.63 0 -5 34 5.32 0.75 0 -5 33 0.94 0.58 0 -5 33 1.20 0.49 0 -5 32 7.91 0.88 0 5 -32 7.20 0.92 0 -5 32 7.34 1.00 0 -5 31 8.36 0.94 0 5 -31 7.12 0.96 0 -5 31 6.75 1.04 0 -5 30 10.86 1.12 0 5 -30 12.08 1.21 0 -5 30 13.15 1.33 0 -5 29 113.08 5.56 0 5 -29 114.32 5.70 0 -5 29 128.64 5.85 0 -5 28 54.01 3.06 0 5 -28 58.06 3.23 0 -5 27 14.60 1.38 0 5 -27 15.71 1.46 0 -5 26 28.20 2.01 0 5 -26 33.96 2.24 0 -5 25 44.77 2.71 0 5 -25 46.44 2.85 0 -5 24 138.88 6.56 0 5 -24 137.02 6.71 0 -5 23 238.97 10.85 0 5 -23 248.08 11.05 0 -5 22 112.97 5.67 0 5 -22 122.68 5.89 0 -5 22 115.00 5.66 0 -5 21 8.03 1.12 0 5 -21 7.08 1.15 0 -5 21 7.43 1.06 0 -5 20 297.51 13.24 0 5 -20 306.23 13.44 0 -5 20 303.04 13.26 0 -5 19 311.18 13.41 0 -5 19 302.66 13.39 0 5 -19 302.05 13.55 0 -5 18 4.81 0.94 0 -5 18 5.16 0.97 0 -5 17 7.13 1.03 0 5 -17 9.44 2.24 0 -5 17 7.36 1.04 0 -5 17 8.82 2.08 0 -5 16 9.47 1.15 0 5 -16 10.27 2.32 0 -5 16 9.36 1.12 0 5 -16 10.11 2.34 0 -5 16 12.98 2.44 0 -5 15 105.90 5.23 0 5 -15 102.03 7.75 0 -5 15 102.46 7.42 0 -5 15 112.43 5.31 0 5 -15 103.25 7.54 0 -5 14 97.78 4.95 0 5 -14 95.04 7.38 0 -5 14 107.05 5.04 0 -5 14 92.73 7.02 0 5 -14 109.50 7.44 0 -5 13 82.24 4.09 0 5 -13 69.05 6.16 0 -5 13 71.08 5.94 0 -5 13 83.36 4.15 0 5 -13 75.85 6.08 0 -5 12 80.50 4.21 0 5 -12 90.26 6.80 0 -5 12 96.03 4.37 0 5 -12 78.29 6.15 0 -5 11 85.70 4.49 0 5 -11 79.51 6.63 0 -5 11 82.70 6.38 0 5 -11 93.83 6.64 0 5 -10 4.23 1.44 0 5 -10 4.69 1.76 0 -5 10 4.51 0.86 0 -5 10 4.06 0.82 0 -5 10 3.19 0.73 0 -5 10 4.02 1.46 0 5 -9 4.09 1.48 0 -5 9 6.23 0.91 0 5 -9 6.34 1.76 0 -5 9 4.98 0.82 0 -5 9 5.45 1.59 0 -5 8 84.68 4.33 0 5 -8 81.80 6.48 0 5 -8 78.73 6.03 0 -5 8 91.64 6.41 0 -5 8 97.69 4.50 0 -5 7 40.17 2.32 0 5 -7 32.44 3.81 0 5 -7 28.79 3.44 0 -5 7 44.37 2.41 0 -5 7 37.76 3.86 0 -5 6 47.00 2.72 0 5 -6 39.94 4.27 0 5 -6 43.59 4.10 0 -5 6 53.39 4.55 0 -5 6 56.34 2.83 0 -5 5 13.04 1.20 0 5 -5 15.82 2.56 0 -5 5 14.72 1.21 0 5 -5 11.59 2.10 0 -5 5 11.28 2.12 0 5 -4 54.01 4.46 0 -5 4 44.76 4.22 0 -5 4 53.64 2.87 0 5 -4 60.01 4.99 0 5 -3 162.19 8.90 0 -5 3 146.10 6.83 0 5 -3 156.40 9.31 0 5 -2 204.75 10.37 0 -5 2 176.87 8.16 0 5 -2 188.49 10.66 0 -5 1 121.49 5.87 0 5 -1 153.14 8.11 0 -5 0 216.01 9.77 0 5 0 249.92 12.01 0 -5 -1 85.56 4.06 0 5 1 93.92 5.84 0 -5 -2 69.78 3.56 0 5 2 74.39 5.19 0 5 2 71.51 5.10 0 -5 -3 25.47 1.64 0 5 3 26.40 2.77 0 -5 -4 173.81 7.20 0 5 4 130.99 8.60 0 5 4 160.92 8.91 0 5 4 124.36 9.05 0 -5 -5 171.03 7.11 0 -5 -5 136.88 9.06 0 5 5 166.23 8.88 0 5 5 130.18 8.54 0 5 5 129.87 9.11 0 -5 -6 7.80 0.91 0 -5 -6 5.17 1.61 0 -5 -6 5.94 0.91 0 5 6 7.84 1.76 0 5 6 7.20 1.57 0 5 6 5.30 1.67 0 -5 -7 72.07 3.67 0 -5 -7 68.56 5.48 0 -5 -7 70.73 3.61 0 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1.19 1 -5 -26 6.87 1.06 1 -5 -26 7.15 1.02 1 -5 -25 20.32 1.66 1 -5 -25 21.25 1.67 1 -5 -24 9.82 1.22 1 -5 -24 10.70 1.20 1 -5 -23 26.29 1.98 1 -5 -23 27.13 1.96 1 -5 -22 1.29 0.69 1 -5 -22 1.32 0.70 1 -5 -21 96.48 4.83 1 -5 -21 91.10 4.77 1 -5 -20 119.67 5.84 1 -5 -20 116.04 5.77 1 -5 -19 61.08 3.44 1 -5 -18 44.47 2.74 1 -5 -17 59.11 3.34 1 -5 -16 9.69 1.19 1 -5 -15 57.95 5.85 1 -5 -15 66.16 3.55 1 -5 -15 59.88 5.53 1 -5 -14 18.02 1.54 1 -5 -14 17.15 2.82 1 -5 -14 18.00 3.10 -1 5 14 17.18 3.03 -1 5 14 16.67 2.75 1 -5 -13 99.15 4.89 1 -5 -13 91.52 7.06 1 -5 -13 95.83 4.90 1 -5 -13 99.99 4.89 -1 5 13 92.87 7.48 -1 5 13 96.86 6.72 -1 5 13 86.95 6.90 1 -5 -12 180.10 8.46 1 -5 -12 166.16 10.79 1 -5 -12 189.88 8.54 1 -5 -12 185.21 8.48 -1 5 12 217.71 12.21 -1 5 12 174.49 10.43 -1 5 12 202.92 11.20 1 -5 -11 100.52 4.89 1 -5 -11 89.10 6.91 1 -5 -11 94.17 4.87 1 -5 -11 94.64 4.84 -1 5 11 107.19 7.82 -1 5 11 99.45 7.07 -1 5 11 107.48 6.85 1 -5 -10 247.55 10.95 1 -5 -10 218.74 13.27 1 -5 -10 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1.54 2 -6 -12 14.83 1.34 2 -6 -12 15.49 1.52 2 -6 -12 13.91 1.38 2 -6 -11 44.55 2.76 2 -6 -11 40.94 2.50 2 -6 -11 42.45 2.65 2 -6 -10 2.25 0.93 2 -6 -10 2.42 0.79 2 -6 -10 2.28 0.80 2 -6 -9 36.96 2.48 2 -6 -9 35.41 2.24 2 -6 -9 35.27 2.36 2 -6 -8 24.00 1.79 2 -6 -8 25.64 1.92 2 -6 -7 66.71 3.65 2 -6 -7 73.76 3.92 2 -6 -7 64.14 3.55 2 -6 -6 66.28 3.58 2 -6 -6 73.03 3.83 2 -6 -5 21.86 1.64 2 -6 -5 18.20 1.63 2 -6 -5 22.67 1.77 2 -6 -5 23.86 1.94 2 -6 -4 52.39 3.01 2 -6 -4 53.06 3.10 2 -6 -4 48.75 2.99 2 -6 -3 29.68 2.04 2 -6 -3 26.66 2.04 2 -6 -2 121.94 5.99 2 -6 -2 129.81 6.13 2 -6 -2 136.57 6.38 2 -6 -2 120.34 6.02 2 -6 -1 132.41 6.48 2 -6 -1 132.34 6.54 2 -6 -1 144.08 6.63 2 -6 -1 148.24 6.87 2 -6 0 67.44 3.61 2 -6 0 70.94 3.71 2 -6 0 71.90 3.90 2 -6 0 62.63 3.61 2 -6 1 51.08 2.85 2 -6 1 46.52 3.03 2 -6 1 46.97 2.85 2 -6 1 52.15 2.94 2 -6 2 49.67 2.75 2 -6 2 44.31 2.73 2 -6 2 46.41 2.75 2 -6 2 42.40 2.84 2 -6 3 58.93 3.42 2 -6 3 56.17 3.23 2 -6 3 59.17 3.27 2 -6 4 8.19 1.13 2 -6 4 7.95 1.15 2 -6 5 9.65 1.20 2 -6 5 10.95 1.27 2 -6 6 9.68 1.30 2 -6 6 8.39 1.13 2 -6 7 4.92 1.02 2 -6 7 2.59 0.86 2 -6 8 7.71 1.15 2 -6 8 8.29 1.09 2 -6 9 12.98 1.32 2 -6 9 12.16 1.32 2 -6 10 13.84 1.37 2 -6 10 10.24 1.20 2 -6 10 14.95 1.42 2 -6 11 30.39 2.09 2 -6 11 33.00 2.15 2 -6 11 32.72 2.11 2 -6 12 16.10 1.48 2 -6 12 18.30 1.55 2 -6 12 18.49 1.49 2 -6 13 14.10 1.34 2 -6 13 14.81 1.37 2 -6 13 14.57 1.32 2 -6 14 2.50 0.72 2 -6 14 1.81 0.79 2 -6 15 4.71 0.91 2 -6 16 0.09 0.64 2 -6 17 20.29 1.54 2 -6 18 3.75 0.80 2 -6 19 11.00 1.07 2 -6 19 9.59 1.04 2 -6 20 19.35 1.45 2 -6 20 19.86 1.43 2 -6 21 2.36 0.62 2 -6 21 1.19 0.56 2 -6 22 4.75 0.72 2 -6 22 5.40 0.74 2 -6 23 1.87 0.54 2 -6 23 1.92 0.55 2 -5 -31 3.40 0.55 2 -5 -30 16.39 1.17 2 -5 -30 15.27 1.12 2 -5 -29 2.85 0.61 2 -5 -29 3.20 0.62 2 -5 -28 1.12 0.56 2 -5 -28 1.70 0.56 2 -5 -27 24.90 1.69 2 -5 -27 26.97 1.67 2 -5 -27 24.51 1.68 2 -5 -26 20.19 1.52 2 -5 -26 20.54 1.45 2 -5 -26 20.55 1.51 2 -5 -26 18.01 1.42 2 -5 -25 49.25 2.75 2 -5 -25 50.01 2.67 2 -5 -25 45.25 2.65 2 -5 -25 46.86 2.71 2 -5 -24 42.30 2.48 2 -5 -24 46.56 2.63 2 -5 -24 41.99 2.52 2 -5 -24 42.94 2.58 2 -5 -23 29.98 2.04 2 -5 -23 28.36 1.90 2 -5 -23 28.15 1.96 2 -5 -23 30.32 2.04 2 -5 -22 59.50 3.34 2 -5 -22 59.92 3.23 2 -5 -22 58.94 3.33 2 -5 -22 60.20 3.33 2 -5 -21 58.72 3.32 2 -5 -21 57.94 3.21 2 -5 -21 60.33 3.34 2 -5 -21 59.29 3.36 2 -5 -20 19.24 1.67 2 -5 -20 23.32 1.67 2 -5 -20 21.91 1.74 2 -5 -20 18.54 1.67 2 -5 -19 61.17 3.26 2 -5 -19 54.96 3.31 2 -5 -19 57.62 3.34 2 -5 -18 109.78 5.45 2 -5 -18 113.18 5.60 2 -5 -18 112.74 5.61 2 -5 -17 49.44 2.90 2 -5 -17 50.25 3.04 2 -5 -17 49.88 3.03 2 -5 -16 35.54 2.32 2 -5 -16 37.78 2.48 2 -5 -16 35.10 2.47 2 -5 -15 116.10 5.71 2 -5 -15 117.13 5.71 2 -5 -15 119.97 5.90 2 -5 -14 15.45 1.57 2 -5 -14 15.75 1.47 2 -5 -14 15.16 1.43 2 -5 -14 15.21 1.54 2 -5 -13 18.11 1.69 2 -5 -13 17.92 1.56 2 -5 -13 15.06 1.43 2 -5 -13 17.57 1.62 2 -5 -12 38.07 2.44 2 -5 -12 38.17 2.58 2 -5 -12 37.84 2.41 2 -5 -12 37.93 2.55 2 -5 -11 22.09 1.72 2 -5 -11 23.31 1.94 2 -5 -11 23.23 1.80 2 -5 -10 20.70 1.65 2 -5 -10 21.72 1.78 2 -5 -10 18.23 1.62 2 -5 -10 20.94 1.83 2 -5 -9 21.37 1.65 2 -5 -9 21.91 1.87 2 -5 -9 17.89 1.66 2 -5 -9 18.54 1.64 2 -5 -8 53.20 3.00 2 -5 -8 50.10 3.06 2 -5 -8 53.29 3.21 2 -5 -8 51.47 3.03 2 -5 -7 86.53 4.56 2 -5 -7 86.10 4.61 2 -5 -7 86.22 4.56 2 -5 -6 128.05 6.15 2 -5 -6 122.32 5.96 2 -5 -6 116.00 5.88 2 -5 -5 264.69 12.57 2 -5 -5 294.47 12.70 2 -5 -5 304.92 12.91 2 -5 -4 240.99 11.09 2 -5 -4 222.36 11.05 2 -5 -4 254.71 11.20 2 -5 -3 285.99 11.42 2 -5 -3 221.89 11.00 2 -5 -2 50.84 3.13 2 -5 -1 14.78 1.44 2 -5 -1 16.55 1.57 2 -5 -1 17.56 1.69 2 -5 -1 18.92 1.60 2 -5 0 81.05 4.32 2 -5 0 87.80 4.43 2 -5 0 85.27 4.54 2 -5 0 83.67 4.42 2 -5 1 36.54 2.31 2 -5 1 34.48 2.37 2 -5 1 36.09 2.37 2 -5 1 34.36 2.45 2 -5 2 48.14 2.87 2 -5 2 50.35 2.99 2 -5 2 51.31 2.99 2 -5 2 50.82 3.09 2 -5 3 272.12 11.97 2 -5 3 261.02 11.98 2 -5 3 276.41 12.03 2 -5 3 272.83 12.17 2 -5 4 273.43 12.18 2 -5 4 271.96 12.23 2 -5 4 281.99 12.24 2 -5 5 329.08 14.01 2 -5 5 317.50 14.02 2 -5 5 310.44 13.97 2 -5 6 174.83 8.18 2 -5 8 42.81 2.61 2 -5 8 38.49 2.65 2 -5 9 71.31 3.67 2 -5 9 58.21 3.57 2 -5 10 7.52 1.14 2 -5 10 5.12 1.12 2 -5 11 4.92 0.98 2 -5 11 6.26 1.14 2 -5 12 28.26 2.06 2 -5 12 28.52 2.12 2 -5 13 6.33 1.14 2 -5 13 7.25 1.13 2 -5 13 6.44 1.14 2 -5 14 15.44 1.53 2 -5 14 11.73 1.34 2 -5 14 13.32 1.43 2 -5 15 5.24 1.10 2 -5 15 5.21 1.02 2 -5 15 5.47 1.08 2 -5 16 12.33 1.37 2 -5 16 12.57 1.36 2 -5 16 12.34 1.44 2 -5 17 30.17 2.18 2 -5 17 31.46 2.15 2 -5 17 30.21 2.26 2 -5 18 14.69 1.48 2 -5 18 11.27 1.42 2 -5 19 25.77 1.95 2 -5 19 25.19 2.00 2 -5 20 7.70 1.20 2 -5 20 8.61 1.21 2 -5 21 6.17 1.08 2 -5 21 5.58 1.07 2 -5 22 10.77 1.24 2 -5 22 11.69 1.34 2 -5 23 20.26 1.64 2 -5 23 22.52 1.77 2 -5 24 30.76 2.06 2 -5 24 34.15 2.21 2 -5 25 25.31 1.74 2 -5 25 24.04 1.79 2 -5 26 2.83 0.72 2 -5 26 2.84 0.78 2 -5 27 0.35 0.55 2 -5 27 0.21 0.57 2 -5 28 1.94 0.59 2 -5 28 2.62 0.66 2 -5 29 19.48 1.33 2 -5 29 20.48 1.41 2 -5 30 19.29 1.30 2 -4 -35 0.29 0.36 -2 4 35 0.29 0.43 2 -4 -34 4.77 0.66 -2 4 34 5.45 0.75 2 -4 -33 2.19 0.55 2 -4 -33 2.12 0.54 2 -4 -32 3.60 0.68 2 -4 -32 4.28 0.66 2 -4 -31 16.87 1.36 2 -4 -31 18.00 1.34 2 -4 -31 17.27 1.33 2 -4 -30 17.99 1.44 2 -4 -30 18.13 1.37 2 -4 -30 15.75 1.34 2 -4 -29 19.96 1.50 2 -4 -29 19.21 1.55 2 -4 -29 18.66 1.50 2 -4 -28 42.74 2.65 2 -4 -28 47.04 2.64 2 -4 -28 45.08 2.66 2 -4 -27 63.01 3.38 2 -4 -27 61.49 3.45 2 -4 -27 62.88 3.44 2 -4 -26 40.22 2.54 2 -4 -26 40.12 2.45 2 -4 -26 39.04 2.50 2 -4 -25 7.21 1.14 2 -4 -25 8.09 1.03 2 -4 -25 6.25 0.99 2 -4 -25 7.54 1.12 2 -4 -24 48.28 2.92 2 -4 -24 47.33 2.79 2 -4 -24 46.29 2.82 2 -4 -24 47.22 2.90 2 -4 -23 98.29 4.78 2 -4 -23 94.48 4.88 2 -4 -23 89.37 4.78 2 -4 -23 92.18 4.86 2 -4 -22 12.67 1.40 2 -4 -22 14.37 1.37 2 -4 -22 12.93 1.42 2 -4 -22 10.61 1.30 2 -4 -21 12.57 1.30 2 -4 -21 12.03 1.36 2 -4 -21 11.88 1.38 2 -4 -20 34.94 2.30 2 -4 -20 34.80 2.38 2 -4 -20 35.40 2.42 2 -4 -19 25.78 1.90 2 -4 -19 25.35 2.01 2 -4 -19 24.89 1.97 2 -4 -18 4.20 0.90 2 -4 -18 5.00 1.02 2 -4 -18 3.78 0.90 2 -4 -17 12.07 1.27 2 -4 -17 14.40 1.45 2 -4 -16 42.62 2.68 2 -4 -16 41.74 2.77 2 -4 -16 47.27 2.71 2 -4 -15 10.72 1.19 -2 4 15 7.81 1.94 2 -4 -15 9.72 1.18 2 -4 -15 8.73 1.18 2 -4 -15 7.61 2.42 2 -4 -14 20.16 1.63 2 -4 -14 20.98 3.56 -2 4 14 19.00 2.84 -2 4 14 25.49 3.55 2 -4 -14 22.34 1.72 2 -4 -14 22.36 1.82 2 -4 -14 17.04 3.25 2 -4 -13 79.77 4.12 2 -4 -13 81.22 4.25 -2 4 13 84.36 6.14 -2 4 13 74.30 6.49 2 -4 -13 69.23 6.68 2 -4 -13 68.62 6.62 2 -4 -13 78.71 4.09 2 -4 -12 25.48 1.91 2 -4 -12 27.71 2.03 -2 4 12 28.06 3.80 -2 4 12 26.18 3.25 -2 4 12 27.42 3.29 2 -4 -12 22.79 3.64 2 -4 -12 26.50 1.85 2 -4 -12 22.59 3.64 2 -4 -11 11.64 1.29 2 -4 -11 12.01 1.37 2 -4 -11 13.27 1.32 -2 4 11 11.20 2.19 -2 4 11 12.13 2.18 -2 4 11 15.82 2.89 2 -4 -11 9.39 2.60 2 -4 -11 14.05 1.27 2 -4 -11 11.09 2.65 2 -4 -10 31.22 2.07 2 -4 -10 30.87 2.10 2 -4 -10 26.54 2.07 -2 4 10 30.17 3.94 -2 4 10 30.73 3.43 2 -4 -10 20.87 3.55 2 -4 -10 26.20 3.87 2 -4 -10 33.65 2.05 2 -4 -9 75.27 4.01 2 -4 -9 71.86 4.05 2 -4 -9 81.68 4.03 -2 4 9 80.29 5.84 -2 4 9 93.12 7.07 -2 4 9 74.28 5.70 2 -4 -9 70.99 6.56 2 -4 -9 77.02 3.94 2 -4 -9 66.59 6.37 2 -4 -8 66.92 3.53 2 -4 -8 66.05 3.62 2 -4 -8 63.04 3.47 -2 4 8 78.21 5.53 -2 4 8 61.96 5.84 -2 4 8 59.80 5.01 2 -4 -8 56.93 5.78 2 -4 -8 64.20 3.43 2 -4 -7 1.37 0.76 2 -4 -7 2.29 0.80 2 -4 -7 0.92 0.76 -2 4 7 1.63 1.03 -2 4 7 1.60 1.18 -2 4 7 0.76 1.14 2 -4 -7 0.26 1.23 2 -4 -7 1.68 0.66 2 -4 -6 35.18 2.27 2 -4 -6 37.43 2.40 2 -4 -6 38.02 2.34 -2 4 6 39.37 3.73 -2 4 6 36.19 3.67 2 -4 -6 33.24 4.27 2 -4 -6 36.32 2.24 2 -4 -5 86.73 4.46 2 -4 -5 89.47 4.49 2 -4 -5 91.73 4.60 -2 4 5 92.82 6.29 -2 4 5 92.02 6.32 2 -4 -5 89.93 4.41 2 -4 -5 73.68 6.59 2 -4 -4 29.70 3.79 -2 4 4 21.39 2.90 2 -4 -3 325.28 14.48 2 -4 -3 330.58 14.60 2 -4 -3 336.26 14.50 -2 4 3 364.90 16.87 -2 4 3 358.03 16.96 2 -4 -3 294.39 17.15 2 -4 -3 340.52 14.44 -2 4 1 70.23 5.24 -2 4 1 56.66 5.05 2 -4 -1 70.07 3.63 2 -4 -1 71.22 3.63 2 -4 -1 65.28 3.64 2 -4 -1 68.45 3.57 -2 4 0 63.63 4.93 -2 4 0 54.51 4.80 2 -4 0 64.30 3.37 2 -4 0 61.26 3.33 2 -4 0 57.97 3.38 2 -4 0 65.27 3.33 -2 4 -1 30.16 3.24 -2 4 -1 28.64 3.29 2 -4 1 29.24 2.03 2 -4 1 29.76 2.03 2 -4 1 31.67 2.10 2 -4 1 31.40 1.99 -2 4 -2 29.55 3.44 2 -4 2 36.59 2.36 2 -4 2 35.78 2.30 2 -4 2 38.94 2.28 -2 4 -3 89.37 5.99 -2 4 -3 82.56 6.07 2 -4 3 74.69 4.16 2 -4 3 82.86 4.20 2 -4 3 85.28 4.15 -2 4 -4 157.04 10.11 2 -4 4 177.79 8.14 2 -4 4 183.47 8.09 2 -4 5 83.90 4.21 2 -4 5 83.29 4.16 2 -4 6 113.31 5.85 2 -4 6 125.59 5.87 -2 4 -6 101.85 7.90 -2 4 -6 107.19 7.73 2 -4 7 341.43 15.06 -2 4 -7 382.45 18.29 -2 4 -7 313.83 17.28 2 -4 7 358.48 14.97 2 -4 7 346.39 14.98 2 -4 7 340.49 14.99 -2 4 -8 126.94 8.63 -2 4 -9 95.72 7.09 2 -4 9 90.61 4.66 2 -4 9 103.38 4.86 2 -4 9 99.15 4.68 2 -4 10 8.21 1.15 -2 4 -10 5.02 1.76 2 -4 10 11.20 1.30 -2 4 -10 9.01 2.20 -2 4 -11 19.67 3.00 -2 4 -11 24.44 3.36 2 -4 11 24.36 1.94 2 -4 11 26.69 1.81 2 -4 11 23.66 1.82 -2 4 -12 101.55 7.55 -2 4 -12 102.65 7.78 2 -4 12 116.14 5.58 2 -4 12 114.11 5.69 2 -4 12 115.43 5.50 -2 4 -13 182.36 11.66 -2 4 -13 190.72 11.62 2 -4 13 207.27 9.22 2 -4 13 214.57 9.40 2 -4 13 194.61 9.10 2 -4 14 233.81 10.60 2 -4 14 225.80 10.51 2 -4 14 255.95 10.84 -2 4 -14 226.07 13.23 2 -4 15 136.38 6.61 2 -4 15 130.93 6.35 2 -4 15 134.63 6.45 2 -4 16 81.69 4.37 2 -4 16 74.97 4.07 2 -4 16 79.57 4.19 2 -4 17 44.95 2.87 2 -4 17 42.90 2.65 2 -4 17 42.74 2.69 2 -4 18 19.56 1.79 2 -4 18 17.05 1.53 2 -4 18 17.98 1.64 2 -4 19 9.63 1.35 2 -4 19 8.01 1.13 2 -4 20 21.42 1.92 2 -4 20 19.29 1.62 2 -4 21 3.52 1.05 2 -4 21 3.48 0.88 2 -4 22 22.48 1.99 2 -4 22 21.50 1.71 2 -4 23 8.80 1.32 2 -4 23 7.14 1.05 2 -4 24 20.78 1.85 2 -4 24 20.23 1.64 2 -4 25 35.73 2.44 2 -4 25 32.77 2.16 2 -4 26 23.06 1.83 2 -4 26 19.81 1.57 2 -4 27 30.77 2.17 2 -4 27 28.78 1.91 2 -4 28 13.64 1.39 2 -4 28 10.68 1.12 2 -4 29 89.31 4.33 2 -4 29 77.78 4.01 2 -4 30 11.61 1.23 2 -4 30 11.49 1.07 2 -4 31 43.70 2.50 2 -4 31 41.74 2.30 2 -4 32 71.92 3.61 -2 3 38 5.29 0.66 2 -3 -38 4.38 0.58 -2 3 37 6.39 0.77 2 -3 -37 4.45 0.64 -2 3 36 38.76 2.14 2 -3 -36 33.09 2.02 -2 3 35 2.83 0.72 2 -3 -35 2.88 0.66 -2 3 34 11.79 1.20 2 -3 -34 11.51 1.08 2 -3 -33 4.15 0.78 2 -3 -32 37.78 2.32 2 -3 -31 38.39 2.41 2 -3 -30 22.50 1.73 2 -3 -30 25.61 1.85 2 -3 -29 20.08 1.66 2 -3 -29 20.63 1.71 2 -3 -28 7.45 1.09 2 -3 -28 8.97 1.17 2 -3 -27 7.37 1.08 2 -3 -27 7.48 1.17 2 -3 -26 8.95 1.24 2 -3 -26 11.54 1.36 2 -3 -25 76.76 4.13 2 -3 -25 75.31 4.15 2 -3 -24 8.34 1.12 2 -3 -24 9.05 1.22 2 -3 -24 9.44 1.27 2 -3 -23 52.78 3.15 2 -3 -23 57.29 3.27 2 -3 -23 54.95 3.25 2 -3 -22 14.23 1.45 2 -3 -22 15.84 1.54 2 -3 -22 14.92 1.51 2 -3 -21 2.11 0.82 2 -3 -21 2.05 0.81 2 -3 -21 2.49 0.86 2 -3 -21 3.89 1.73 -2 3 21 1.59 1.22 2 -3 -20 3.09 1.61 2 -3 -20 2.80 0.82 2 -3 -20 3.97 0.92 2 -3 -20 3.01 1.60 -2 3 20 3.14 1.45 -2 3 20 3.20 1.59 2 -3 -19 85.94 7.39 2 -3 -19 94.52 4.79 2 -3 -19 95.86 4.79 2 -3 -19 84.35 7.28 -2 3 19 82.87 6.83 2 -3 -18 12.15 2.70 2 -3 -18 13.37 1.38 2 -3 -18 15.33 1.44 2 -3 -18 11.38 2.55 -2 3 18 13.63 2.56 -2 3 18 12.92 2.32 2 -3 -17 2.91 1.68 -2 3 17 2.60 1.31 -2 3 17 3.18 1.55 2 -3 -17 2.38 0.77 2 -3 -17 2.94 0.84 2 -3 -17 3.40 1.90 2 -3 -16 48.32 5.10 -2 3 16 48.20 4.30 -2 3 16 50.07 4.86 2 -3 -16 54.42 2.94 2 -3 -16 49.08 2.93 2 -3 -16 41.27 4.84 2 -3 -15 20.71 3.26 -2 3 15 15.98 2.49 -2 3 15 19.85 3.01 2 -3 -15 20.38 1.58 2 -3 -15 20.81 1.63 2 -3 -15 18.07 3.13 2 -3 -14 52.11 5.39 2 -3 -14 66.59 3.43 -2 3 14 70.53 5.81 2 -3 -14 65.07 3.46 2 -3 -14 64.55 3.53 2 -3 -14 69.73 5.98 2 -3 -13 4.99 0.83 -2 3 13 4.05 1.39 -2 3 13 5.56 1.76 2 -3 -13 3.84 1.70 2 -3 -13 5.80 0.84 2 -3 -13 1.70 1.26 2 -3 -12 40.65 2.39 -2 3 12 35.44 4.03 2 -3 -12 39.35 4.41 2 -3 -12 42.00 2.37 2 -3 -12 34.97 4.17 2 -3 -11 12.80 1.19 2 -3 -11 13.95 1.24 2 -3 -11 11.99 1.21 -2 3 11 14.21 2.17 -2 3 11 12.36 2.40 -2 3 11 13.42 2.04 2 -3 -11 12.28 2.62 2 -3 -11 14.02 1.19 2 -3 -11 13.96 2.58 2 -3 -10 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2.59 0.79 3 -5 16 2.88 0.76 3 -5 17 1.63 0.68 3 -5 17 1.88 0.70 3 -5 18 4.78 0.83 3 -5 18 3.86 0.81 3 -5 19 0.85 0.59 3 -5 19 1.00 0.64 3 -5 20 0.31 0.57 3 -5 20 0.56 0.57 3 -5 21 5.90 0.84 3 -5 22 19.74 1.42 3 -5 23 4.78 0.72 3 -5 24 16.96 1.21 3 -4 -30 23.29 1.42 3 -4 -29 41.04 2.21 3 -4 -28 19.25 1.33 3 -4 -28 17.12 1.24 3 -4 -28 17.50 1.28 3 -4 -27 30.41 1.84 3 -4 -27 30.31 1.84 3 -4 -27 26.93 1.74 3 -4 -26 40.43 2.30 3 -4 -26 37.72 2.27 3 -4 -26 39.66 2.25 3 -4 -25 6.32 0.88 3 -4 -25 5.53 0.84 3 -4 -25 5.73 0.87 3 -4 -24 6.86 0.94 3 -4 -24 7.12 0.98 3 -4 -24 5.61 0.88 3 -4 -23 19.36 1.51 3 -4 -23 17.67 1.50 3 -4 -23 17.19 1.46 3 -4 -22 2.80 0.76 3 -4 -22 2.69 0.78 3 -4 -22 3.30 0.80 3 -4 -21 29.40 2.00 3 -4 -21 26.10 1.95 3 -4 -21 27.93 1.99 3 -4 -20 32.87 2.18 3 -4 -20 31.63 2.20 3 -4 -20 32.41 2.23 3 -4 -19 14.04 1.35 3 -4 -19 13.33 1.40 3 -4 -19 11.95 1.33 3 -4 -18 24.87 1.95 3 -4 -18 26.56 1.97 3 -4 -17 3.28 0.94 3 -4 -17 3.32 0.87 3 -4 -16 31.51 2.29 3 -4 -16 33.87 2.28 3 -4 -15 18.83 1.69 3 -4 -15 18.22 1.62 3 -4 -14 68.02 3.68 3 -4 -14 66.30 3.80 3 -4 -14 67.05 3.73 3 -4 -14 62.30 3.65 3 -4 -13 23.21 2.01 3 -4 -13 26.18 1.94 3 -4 -13 24.15 1.94 3 -4 -13 25.99 1.94 3 -4 -12 130.79 6.07 3 -4 -12 116.87 6.19 3 -4 -12 122.15 6.11 3 -4 -11 99.07 4.93 3 -4 -11 96.37 5.11 3 -4 -11 92.34 4.93 3 -4 -10 22.12 1.82 3 -4 -10 20.00 1.90 3 -4 -10 22.57 1.82 3 -4 -9 56.40 3.28 3 -4 -9 56.56 3.48 3 -4 -9 56.61 3.30 3 -4 -8 124.94 6.29 3 -4 -8 123.88 6.06 3 -4 -8 124.60 6.11 3 -4 -7 63.31 3.54 3 -4 -7 62.50 3.75 3 -4 -6 8.69 1.38 3 -4 -6 8.64 1.20 3 -4 -5 88.21 5.02 3 -4 -5 100.66 4.89 3 -4 -4 74.69 4.09 3 -4 -4 79.97 4.38 3 -4 -3 109.64 5.67 3 -4 -3 123.04 5.98 3 -4 -2 234.96 10.85 3 -4 -2 236.61 10.65 3 -4 -1 206.43 9.64 3 -4 -1 218.43 9.92 3 -4 0 148.49 6.77 3 -4 0 130.21 6.86 3 -4 1 90.57 4.55 3 -4 1 81.70 4.64 3 -4 2 81.31 4.18 3 -4 2 74.53 4.29 3 -4 3 31.01 2.15 3 -4 3 28.04 2.24 3 -4 4 90.73 4.59 3 -4 4 84.16 4.69 3 -4 5 161.11 7.59 3 -4 7 8.87 1.26 3 -4 8 97.17 4.97 3 -4 9 337.70 14.80 3 -4 10 63.16 3.51 3 -4 10 60.00 3.53 3 -4 11 6.88 1.18 3 -4 11 6.79 1.20 3 -4 12 77.90 4.11 3 -4 12 74.13 4.16 3 -4 13 74.80 3.98 3 -4 13 71.33 4.04 3 -4 14 18.33 1.64 3 -4 14 14.54 1.46 3 -4 14 18.71 1.75 3 -4 15 44.10 2.75 3 -4 15 44.42 2.68 3 -4 15 45.96 2.91 3 -4 16 9.13 1.23 3 -4 16 9.08 1.16 3 -4 16 10.20 1.37 3 -4 17 23.99 1.81 3 -4 17 20.82 1.68 3 -4 17 19.58 1.80 3 -4 18 20.93 1.66 3 -4 18 21.70 1.87 3 -4 19 0.96 0.67 3 -4 19 1.01 0.83 3 -4 20 2.83 0.77 3 -4 20 3.19 0.94 3 -4 21 4.31 0.85 3 -4 21 3.38 0.96 3 -4 22 6.52 0.94 3 -4 22 5.28 1.03 3 -4 23 20.84 1.55 3 -4 23 20.09 1.68 3 -4 24 0.12 0.58 3 -4 24 0.40 0.68 3 -4 25 10.40 1.04 3 -4 25 12.30 1.23 3 -4 26 9.50 0.97 3 -4 26 10.50 1.13 3 -4 27 79.26 3.86 3 -4 27 82.39 4.03 3 -4 28 55.88 2.91 3 -4 28 63.17 3.11 3 -4 29 16.66 1.25 3 -3 -33 4.80 0.62 3 -3 -32 6.22 0.74 3 -3 -31 16.15 1.27 3 -3 -31 18.62 1.31 3 -3 -30 8.97 0.95 3 -3 -30 8.35 0.95 3 -3 -29 17.73 1.40 3 -3 -29 15.33 1.30 3 -3 -29 15.67 1.34 3 -3 -28 34.40 2.15 3 -3 -28 29.60 2.00 3 -3 -28 33.02 2.13 3 -3 -28 34.54 2.07 3 -3 -27 5.17 0.92 3 -3 -27 6.38 0.91 3 -3 -27 5.53 0.94 3 -3 -27 4.49 0.80 3 -3 -26 25.27 1.86 3 -3 -26 22.66 1.76 3 -3 -26 26.94 1.89 3 -3 -25 7.00 1.04 3 -3 -25 5.97 0.97 3 -3 -25 6.52 1.06 3 -3 -24 3.14 0.85 3 -3 -24 2.00 0.76 3 -3 -24 2.95 0.88 3 -3 -23 15.13 1.50 3 -3 -23 16.98 1.54 3 -3 -23 16.08 1.56 3 -3 -22 30.09 2.21 3 -3 -22 33.33 2.27 3 -3 -22 31.23 2.25 3 -3 -21 108.45 5.49 3 -3 -21 107.89 5.50 3 -3 -21 111.45 5.56 3 -3 -20 4.27 0.95 3 -3 -20 5.65 1.06 3 -3 -20 5.76 1.06 3 -3 -19 23.72 1.90 3 -3 -19 25.85 2.00 3 -3 -19 26.00 2.01 3 -3 -18 35.27 2.38 3 -3 -18 38.14 2.51 3 -3 -18 33.43 2.37 3 -3 -17 67.29 3.85 3 -3 -17 72.45 3.97 3 -3 -17 75.15 3.99 3 -3 -16 6.69 1.06 3 -3 -16 7.12 1.16 3 -3 -16 6.54 1.07 3 -3 -15 25.84 2.09 3 -3 -15 28.94 2.12 3 -3 -15 31.86 2.15 3 -3 -14 4.71 0.98 3 -3 -14 4.38 0.94 3 -3 -14 6.85 1.08 -3 3 13 20.34 2.96 3 -3 -13 23.77 1.76 3 -3 -13 18.93 1.79 3 -3 -13 20.59 1.73 3 -3 -13 20.06 1.69 3 -3 -13 15.63 3.20 3 -3 -12 12.25 2.82 -3 3 12 13.98 2.45 -3 3 12 19.34 3.29 3 -3 -12 14.55 1.39 3 -3 -12 15.08 1.60 3 -3 -12 13.37 1.40 3 -3 -12 13.59 1.39 3 -3 -12 11.64 2.75 3 -3 -11 20.48 3.57 -3 3 11 20.33 2.94 -3 3 11 19.93 3.40 3 -3 -11 22.20 1.69 3 -3 -11 20.05 1.83 3 -3 -11 20.52 1.72 3 -3 -11 15.27 3.11 3 -3 -10 12.25 2.82 -3 3 10 13.48 2.43 -3 3 10 13.18 2.90 3 -3 -10 17.05 1.63 3 -3 -10 17.04 1.50 3 -3 -10 14.61 1.46 3 -3 -10 15.10 2.99 3 -3 -9 0.60 1.41 -3 3 9 3.56 1.50 -3 3 9 1.39 1.43 3 -3 -9 1.50 0.78 3 -3 -9 2.02 0.81 3 -3 -9 1.72 0.72 3 -3 -9 1.96 1.44 3 -3 -8 20.80 3.60 -3 3 8 24.05 3.11 -3 3 8 27.82 3.96 3 -3 -8 27.89 1.91 3 -3 -8 23.47 1.96 3 -3 -8 25.10 1.87 3 -3 -8 22.41 3.61 3 -3 -7 96.22 8.02 -3 3 7 120.04 7.40 -3 3 7 106.75 8.21 3 -3 -7 113.67 5.22 3 -3 -7 95.00 5.26 3 -3 -7 101.67 5.16 3 -3 -7 95.05 7.82 3 -3 -6 2.90 0.93 3 -3 -6 5.07 0.97 -3 3 6 5.96 1.70 -3 3 6 4.39 1.88 3 -3 -6 3.16 1.65 3 -3 -6 5.89 2.14 3 -3 -5 101.09 4.56 3 -3 -5 74.09 4.50 -3 3 5 96.06 6.40 3 -3 -5 77.78 7.05 3 -3 -5 85.83 7.16 3 -3 -4 97.98 4.59 3 -3 -4 79.11 4.60 -3 3 4 100.08 6.53 -3 3 4 95.55 6.43 3 -3 -4 72.90 6.92 3 -3 -4 87.59 7.22 3 -3 -3 64.24 3.36 -3 3 3 60.51 4.90 3 -3 -3 52.83 5.47 -3 3 2 32.80 3.68 3 -3 -2 30.06 4.19 3 -3 -1 114.24 5.13 3 -3 -1 91.75 5.10 -3 3 1 102.02 6.93 3 -3 -1 89.77 7.43 3 -3 0 78.16 4.49 -3 3 0 82.77 6.20 3 -3 0 66.25 6.42 3 -3 1 46.57 2.56 -3 3 -1 36.88 3.90 3 -3 2 57.56 3.03 3 -3 2 48.62 3.05 -3 3 -2 56.29 4.78 3 -3 3 77.58 3.82 3 -3 3 68.61 3.88 -3 3 -3 65.82 5.53 3 -3 3 61.45 5.72 3 -3 4 18.70 1.73 -3 3 -4 21.59 3.03 3 -3 4 15.69 2.81 -3 3 -5 54.43 5.19 3 -3 5 47.64 5.05 -3 3 -6 22.90 3.24 -3 3 -6 28.99 3.90 3 -3 6 23.27 3.31 -3 3 -7 156.50 10.01 -3 3 -7 155.92 10.25 3 -3 7 157.44 7.65 3 -3 7 164.23 7.48 3 -3 7 173.73 7.65 -3 3 -8 22.34 3.34 -3 3 -8 24.48 3.74 3 -3 8 23.36 1.81 -3 3 -9 33.09 3.92 -3 3 -9 30.25 4.03 3 -3 9 34.87 2.42 3 -3 9 38.13 2.29 3 -3 9 37.51 2.38 -3 3 -10 97.02 7.22 3 -3 10 85.60 4.55 3 -3 10 84.38 4.32 3 -3 10 86.34 4.25 3 -3 10 89.66 4.49 3 -3 11 299.33 13.51 3 -3 11 306.47 13.28 3 -3 11 300.67 13.15 -3 3 -11 299.92 16.35 -3 3 -11 347.78 17.08 3 -3 12 153.64 7.45 3 -3 12 162.73 7.25 3 -3 12 152.42 7.08 -3 3 -12 141.51 9.76 -3 3 -12 161.57 10.26 3 -3 13 89.07 4.53 3 -3 13 93.25 4.43 -3 3 -13 82.55 6.94 3 -3 13 86.35 4.73 3 -3 14 42.14 2.78 3 -3 14 41.18 2.45 3 -3 14 41.74 2.56 3 -3 15 3.56 1.04 3 -3 15 4.74 0.96 3 -3 15 3.55 0.82 3 -3 16 74.17 4.10 3 -3 16 71.36 3.80 3 -3 16 69.65 3.69 3 -3 17 96.24 5.05 3 -3 17 96.81 4.68 3 -3 17 92.73 4.79 3 -3 18 20.21 1.87 3 -3 18 19.84 1.56 3 -3 18 20.86 1.68 3 -3 19 36.01 2.55 3 -3 19 35.12 2.22 3 -3 19 36.27 2.34 3 -3 20 4.53 1.10 3 -3 20 5.70 1.03 3 -3 20 4.87 0.86 3 -3 21 24.85 2.07 3 -3 21 25.79 1.78 3 -3 21 26.13 1.91 3 -3 22 16.34 1.63 3 -3 22 12.87 1.26 3 -3 22 15.08 1.44 3 -3 23 2.30 0.92 3 -3 23 2.02 0.71 3 -3 23 2.11 0.78 3 -3 24 4.78 1.02 3 -3 24 4.18 0.91 3 -3 24 5.19 0.83 3 -3 25 23.79 1.95 3 -3 25 26.25 1.87 3 -3 25 25.62 1.71 3 -3 26 30.97 2.21 3 -3 26 30.89 2.05 3 -3 27 6.70 1.06 3 -3 27 5.91 0.94 3 -3 28 0.95 0.68 3 -3 28 0.37 0.60 3 -3 29 2.59 0.79 3 -3 29 2.35 0.67 3 -3 30 16.64 1.31 3 -3 31 25.98 1.65 3 -3 32 4.39 0.68 3 -3 33 9.13 0.85 3 -2 -36 1.27 0.44 3 -2 -35 -0.16 0.42 3 -2 -34 10.17 0.99 3 -2 -33 4.49 0.76 3 -2 -32 3.07 0.73 3 -2 -31 2.56 0.72 3 -2 -31 2.13 0.69 3 -2 -30 -0.32 0.60 3 -2 -30 0.10 0.61 3 -2 -29 4.44 0.86 3 -2 -29 4.87 0.89 3 -2 -29 3.91 0.89 3 -2 -28 22.71 1.71 3 -2 -28 22.69 1.75 3 -2 -28 25.28 1.84 3 -2 -28 21.53 1.74 3 -2 -27 24.31 1.79 3 -2 -27 24.06 1.87 3 -2 -27 26.67 1.93 3 -2 -27 21.97 1.81 3 -2 -26 4.15 0.89 3 -2 -26 5.58 0.98 3 -2 -26 4.34 0.96 3 -2 -25 8.34 1.11 3 -2 -25 8.62 1.22 3 -2 -25 9.17 1.22 3 -2 -24 5.56 1.00 3 -2 -24 6.17 1.05 3 -2 -24 5.68 1.05 3 -2 -23 57.29 3.31 3 -2 -23 56.80 3.34 3 -2 -23 56.37 3.34 3 -2 -22 152.77 7.49 3 -2 -22 161.45 7.55 3 -2 -22 160.65 7.55 3 -2 -21 15.98 1.56 3 -2 -21 17.43 1.61 3 -2 -21 18.01 1.64 3 -2 -20 79.02 4.29 3 -2 -20 83.24 4.36 3 -2 -20 78.89 4.28 3 -2 -19 48.40 2.97 3 -2 -19 49.00 3.00 3 -2 -19 49.97 2.99 3 -2 -18 12.56 1.38 3 -2 -18 15.13 1.45 3 -2 -18 13.64 1.39 -3 2 18 14.83 2.77 3 -2 -17 21.23 1.77 3 -2 -17 23.24 1.82 3 -2 -17 22.03 1.76 3 -2 -17 17.00 3.20 -3 2 17 22.38 3.41 3 -2 -16 71.64 6.96 3 -2 -16 91.29 4.61 3 -2 -16 93.36 4.69 3 -2 -16 89.34 4.63 3 -2 -16 73.50 6.86 -3 2 16 104.52 7.49 3 -2 -15 25.16 3.89 3 -2 -15 34.01 2.21 -3 2 15 32.93 4.12 3 -2 -15 36.09 2.30 3 -2 -15 33.03 2.24 3 -2 -15 29.45 4.13 3 -2 -14 19.71 3.45 -3 2 14 26.36 3.66 3 -2 -14 29.12 1.93 3 -2 -14 26.46 1.93 3 -2 -14 25.13 1.89 3 -2 -14 20.23 3.43 3 -2 -13 52.95 5.67 -3 2 13 69.27 5.98 3 -2 -13 74.05 3.61 3 -2 -13 63.62 3.58 3 -2 -13 64.02 3.55 3 -2 -13 57.28 5.68 3 -2 -12 126.60 9.49 -3 2 12 158.69 9.81 3 -2 -12 149.37 6.68 3 -2 -12 141.32 6.72 3 -2 -12 140.70 6.68 3 -2 -12 121.20 9.17 3 -2 -11 12.08 2.65 -3 2 11 11.17 2.48 3 -2 -11 14.85 1.31 3 -2 -11 13.91 1.41 3 -2 -11 14.03 1.31 3 -2 -11 12.85 1.25 3 -2 -11 14.83 2.86 3 -2 -10 96.42 7.74 -3 2 10 114.36 7.99 3 -2 -10 110.96 5.15 3 -2 -10 100.04 5.25 3 -2 -10 108.22 5.21 3 -2 -10 97.37 7.65 3 -2 -9 9.10 2.30 -3 2 9 13.96 2.62 3 -2 -9 13.44 1.20 3 -2 -9 10.39 1.23 3 -2 -9 13.25 1.24 3 -2 -9 12.23 2.58 3 -2 -8 23.27 3.53 -3 2 8 23.67 3.39 3 -2 -8 30.41 1.88 3 -2 -8 27.64 1.97 3 -2 -8 25.35 1.82 3 -2 -8 24.69 3.55 3 -2 -7 3.77 1.64 -3 2 7 5.99 1.57 -3 2 7 6.71 1.96 3 -2 -7 4.05 0.88 3 -2 -7 4.33 0.78 3 -2 -7 4.44 0.76 3 -2 -7 4.87 1.88 3 -2 -6 1.24 1.24 -3 2 6 7.24 1.64 -3 2 6 2.96 1.49 3 -2 -6 3.74 0.86 3 -2 -6 5.22 0.82 3 -2 -6 4.54 1.75 3 -2 -6 5.22 0.64 3 -2 -5 19.94 3.15 -3 2 5 23.24 2.76 3 -2 -5 27.16 1.78 3 -2 -5 23.21 1.83 3 -2 -5 28.66 3.55 3 -2 -5 27.59 1.50 3 -2 -4 87.80 7.03 -3 2 4 103.72 6.30 3 -2 -4 96.57 4.65 3 -2 -4 89.07 4.74 3 -2 -4 92.31 7.00 3 -2 -4 97.71 4.33 3 -2 -3 17.25 1.40 3 -2 -3 21.48 1.63 3 -2 -3 17.53 2.87 3 -2 -2 41.65 4.59 -3 2 2 48.37 4.03 3 -2 -2 49.55 2.78 3 -2 -2 46.40 2.87 3 -2 -2 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4 0 -4 23.18 1.61 4 0 -3 22.21 1.59 4 0 -3 20.24 3.04 4 0 -3 20.33 1.39 4 0 -3 23.00 1.61 4 0 -2 38.50 4.27 4 0 -2 44.65 2.24 4 0 -2 38.31 2.36 4 0 -2 39.98 2.39 4 0 -1 99.27 7.31 4 0 -1 96.74 4.53 4 0 -1 97.39 4.78 4 0 -1 102.69 4.82 4 0 -1 89.64 6.63 4 0 1 143.40 9.57 4 0 1 156.30 6.75 4 0 1 150.44 6.98 4 0 1 153.19 7.04 4 0 1 136.44 9.01 4 0 2 98.59 7.23 4 0 2 93.88 4.39 4 0 2 93.77 4.64 4 0 2 98.81 4.72 4 0 2 90.54 6.64 4 0 3 169.58 10.31 4 0 3 156.83 7.09 4 0 3 165.24 7.39 4 0 3 162.65 7.44 4 0 3 167.18 9.81 4 0 4 139.21 9.48 4 0 4 145.06 6.88 4 0 4 142.43 9.11 4 0 4 148.62 6.55 4 0 4 152.22 6.83 4 0 5 406.14 17.47 4 0 5 395.65 17.06 4 0 5 426.53 17.40 4 0 7 64.32 3.63 4 0 7 70.09 3.31 4 0 7 73.13 3.63 4 0 8 93.26 4.73 4 0 8 95.98 4.65 4 0 9 28.91 2.07 4 0 9 34.81 2.09 4 0 10 12.98 1.31 4 0 10 14.64 1.27 4 0 11 10.60 1.21 4 0 11 12.98 1.20 4 0 12 38.89 2.45 4 0 13 98.23 4.94 4 0 13 97.45 4.63 4 0 14 31.09 2.13 4 0 14 31.47 1.90 4 0 15 68.73 3.68 4 0 15 66.96 3.42 4 0 15 62.98 5.35 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-4 -1 14 36.87 2.89 -4 -1 14 36.72 4.12 4 1 -14 35.37 2.07 4 1 -14 32.04 2.22 4 1 -14 36.32 2.39 4 1 -13 38.61 4.08 -4 -1 13 36.28 4.09 4 1 -13 42.88 2.49 4 1 -13 39.84 2.57 -4 -1 13 37.34 3.02 4 1 -12 101.52 7.31 4 1 -12 115.03 5.30 4 1 -12 109.83 5.41 -4 -1 12 107.62 6.04 4 1 -11 42.95 4.23 -4 -1 11 35.96 4.02 4 1 -11 43.91 2.53 4 1 -11 45.38 2.68 -4 -1 11 41.78 3.22 4 1 -10 45.27 2.52 4 1 -10 45.16 2.66 -4 -1 10 39.60 3.18 4 1 -9 11.55 1.09 4 1 -9 10.21 1.03 4 1 -9 8.44 0.87 4 1 -9 10.34 1.13 -4 -1 9 8.94 1.46 -4 -1 8 10.70 2.10 -4 -1 8 14.16 1.83 4 1 -8 13.56 1.17 4 1 -8 14.20 1.25 4 1 -8 12.45 1.05 4 1 -8 12.72 1.27 -4 -1 7 38.84 3.94 4 1 -7 44.29 2.60 -4 -1 7 47.89 3.63 4 1 -7 44.27 2.46 4 1 -7 46.51 2.73 -4 -1 6 151.70 9.19 -4 -1 6 159.29 8.64 4 1 -6 159.06 7.33 4 1 -6 148.72 7.15 4 1 -6 163.62 7.48 -4 -1 5 27.64 3.17 -4 -1 5 34.31 3.06 4 1 -5 29.53 3.49 4 1 -5 30.56 1.97 4 1 -5 37.85 2.11 4 1 -5 32.80 1.89 4 1 -5 32.58 2.10 -4 -1 4 45.51 3.60 4 1 -4 42.72 4.25 4 1 -4 42.73 2.43 4 1 -4 48.21 2.53 4 1 -4 40.37 2.29 4 1 -4 43.59 2.54 -4 -1 3 7.55 1.61 4 1 -3 6.71 1.82 4 1 -3 8.46 0.96 4 1 -3 11.05 0.94 4 1 -3 7.81 0.95 4 1 -3 7.40 0.92 4 1 -2 66.56 5.47 4 1 -2 69.48 3.43 4 1 -2 61.67 3.19 4 1 -2 66.18 3.44 4 1 -2 67.47 3.37 4 1 -1 32.65 3.83 4 1 -1 38.13 2.37 4 1 -1 38.16 2.35 4 1 0 20.00 1.31 4 1 0 18.24 1.42 4 1 0 17.64 2.88 4 1 1 63.95 5.42 4 1 1 62.26 3.11 4 1 1 62.96 3.31 4 1 1 65.04 3.33 4 1 2 60.08 5.21 4 1 2 61.37 3.10 4 1 2 52.92 2.84 4 1 2 60.96 3.09 4 1 3 80.69 3.89 4 1 3 70.46 3.59 4 1 3 81.81 3.89 4 1 4 157.15 6.96 4 1 4 143.55 6.66 4 1 4 157.52 6.94 4 1 5 384.99 15.71 4 1 5 392.93 15.69 4 1 6 161.26 6.58 4 1 6 146.54 6.22 4 1 7 388.73 17.12 4 1 7 413.92 17.13 4 1 8 124.00 6.11 4 1 8 139.42 6.15 4 1 9 62.56 3.47 4 1 9 72.67 3.53 4 1 10 46.41 2.78 4 1 10 55.40 2.87 4 1 11 51.23 2.98 4 1 11 58.34 3.03 4 1 12 16.52 1.38 4 1 13 98.05 4.57 4 1 13 87.23 4.21 4 1 14 35.40 2.11 4 1 14 38.77 2.14 4 1 15 32.18 3.67 4 1 15 40.94 2.16 4 1 15 32.98 2.09 4 1 16 32.96 1.96 4 1 16 37.30 3.83 -4 -1 -17 138.02 8.76 4 1 17 154.69 7.02 -4 -1 -18 12.56 2.24 4 1 18 19.82 1.44 4 1 18 16.31 2.79 -4 -1 -19 5.85 1.63 4 1 19 9.78 1.05 4 1 19 7.03 1.92 -4 -1 -20 69.57 5.58 4 1 20 82.99 3.86 4 1 20 85.96 6.46 -4 -1 -21 60.58 5.43 -4 -1 -21 71.85 5.89 4 1 22 47.22 2.72 4 1 23 35.47 2.23 4 1 24 47.08 2.72 4 1 25 149.16 6.92 4 1 26 94.96 4.70 4 1 27 11.48 1.22 4 1 28 3.40 0.79 4 1 29 35.39 2.19 4 1 30 4.03 0.78 4 1 31 20.30 1.61 4 1 31 19.37 1.47 4 1 32 3.04 0.78 4 1 32 1.96 0.65 4 1 33 3.59 0.77 4 1 33 3.24 0.68 4 1 34 3.59 0.75 4 1 34 3.40 0.64 4 1 35 20.31 1.46 4 1 35 19.48 1.31 4 1 36 3.32 0.65 4 1 36 3.16 0.55 4 1 37 5.44 0.72 4 2 -36 14.44 1.08 4 2 -35 23.84 1.54 4 2 -34 4.74 0.74 4 2 -33 10.53 1.08 4 2 -32 1.93 0.68 4 2 -31 2.47 0.76 4 2 -30 47.70 2.85 4 2 -29 39.82 2.55 4 2 -28 49.52 3.02 4 2 -27 23.99 1.98 4 2 -27 29.01 1.83 4 2 -26 64.50 3.97 4 2 -26 73.24 3.99 4 2 -25 57.70 3.02 4 2 -25 56.79 3.21 4 2 -24 60.14 3.12 4 2 -24 61.34 3.36 4 2 -23 15.13 1.44 4 2 -23 11.88 1.44 4 2 -23 16.15 1.32 4 2 -23 15.44 1.50 4 2 -22 2.40 0.82 4 2 -22 2.14 0.85 4 2 -22 4.35 0.94 4 2 -22 4.11 0.78 4 2 -21 36.03 2.41 4 2 -21 40.01 2.28 4 2 -21 39.91 2.48 4 2 -20 99.68 5.01 4 2 -20 108.24 4.84 4 2 -20 100.23 5.00 -4 -2 19 132.79 6.81 4 2 -19 131.49 5.77 4 2 -19 127.02 5.95 4 2 -19 117.82 5.92 4 2 -19 114.21 8.45 -4 -2 18 1.46 1.39 -4 -2 18 2.34 0.92 4 2 -18 2.99 0.75 4 2 -18 3.33 0.73 4 2 -18 2.29 0.83 4 2 -18 2.69 1.46 4 2 -18 2.47 0.86 -4 -2 17 131.12 9.46 -4 -2 17 159.90 8.01 4 2 -17 156.35 6.97 4 2 -17 161.89 7.19 4 2 -17 146.59 7.15 4 2 -17 149.52 9.79 4 2 -17 140.31 7.17 -4 -2 16 196.42 11.50 -4 -2 16 184.86 9.40 4 2 -16 186.59 8.42 4 2 -16 199.60 8.67 4 2 -16 180.48 8.62 4 2 -16 220.12 11.93 4 2 -16 178.80 8.67 -4 -2 15 -0.23 1.31 -4 -2 15 0.52 0.87 4 2 -15 1.09 0.64 4 2 -15 1.07 0.55 4 2 -15 0.96 0.67 4 2 -15 0.91 1.27 4 2 -15 2.44 0.78 -4 -2 14 67.66 5.70 -4 -2 14 62.55 4.25 4 2 -14 66.25 3.38 4 2 -14 67.34 3.54 4 2 -14 64.67 3.56 4 2 -14 62.89 3.57 4 2 -14 65.07 5.65 4 2 -13 29.84 3.69 -4 -2 13 26.65 3.50 -4 -2 13 27.28 2.67 4 2 -13 30.63 1.90 4 2 -13 33.75 2.09 4 2 -13 27.75 2.03 4 2 -13 34.36 2.11 4 2 -13 32.23 2.15 4 2 -12 65.91 5.64 -4 -2 12 72.22 5.88 -4 -2 12 68.63 4.66 4 2 -12 71.53 3.62 4 2 -12 77.49 3.81 4 2 -12 70.20 3.81 4 2 -12 77.54 3.82 4 2 -12 70.02 3.87 4 2 -11 14.96 2.58 -4 -2 11 16.39 2.74 -4 -2 11 18.82 2.19 4 2 -11 19.31 1.37 4 2 -11 19.45 1.50 4 2 -11 18.92 1.55 4 2 -11 23.16 1.58 4 2 -11 20.53 1.62 4 2 -10 5.46 1.71 -4 -2 10 4.55 1.64 -4 -2 10 8.37 1.55 4 2 -10 7.06 0.88 4 2 -10 7.47 0.97 4 2 -10 7.79 0.94 4 2 -10 9.04 1.05 4 2 -10 7.41 0.85 -4 -2 9 40.35 3.87 -4 -2 9 34.24 3.02 4 2 -9 31.50 2.00 4 2 -9 32.86 2.13 4 2 -9 37.08 2.12 4 2 -9 30.15 1.90 4 2 -9 32.42 2.14 -4 -2 8 79.72 5.76 -4 -2 8 73.02 4.90 4 2 -8 62.08 3.56 4 2 -8 76.61 3.77 4 2 -8 80.15 3.73 4 2 -8 68.17 3.52 4 2 -8 73.04 3.77 -4 -2 7 33.47 3.46 -4 -2 7 31.16 3.01 4 2 -7 30.95 1.98 4 2 -7 32.99 2.07 4 2 -7 34.18 2.00 4 2 -7 29.50 1.87 4 2 -7 31.48 2.05 -4 -2 6 110.56 7.21 -4 -2 6 112.66 6.78 4 2 -6 107.45 5.29 4 2 -6 114.95 5.41 4 2 -6 98.65 5.15 4 2 -6 110.27 5.39 -4 -2 5 8.11 1.77 -4 -2 5 7.05 1.69 4 2 -5 10.53 1.06 4 2 -5 10.81 1.05 4 2 -5 9.72 0.96 4 2 -5 9.63 1.04 4 2 -5 8.73 1.00 4 2 -4 30.18 1.89 4 2 -4 33.93 1.95 4 2 -4 27.33 1.77 4 2 -4 30.36 1.92 4 2 -4 29.13 1.90 4 2 -3 41.24 2.37 4 2 -3 40.46 2.35 4 2 -3 37.43 2.23 4 2 -3 39.38 2.35 4 2 -2 20.45 1.51 4 2 -2 22.87 1.53 4 2 -2 22.32 1.46 4 2 -2 17.95 1.45 -4 -2 1 64.51 4.62 4 2 -1 67.16 3.33 4 2 -1 70.30 3.32 4 2 -1 55.46 3.09 4 2 -1 62.05 3.26 4 2 -1 63.81 3.29 4 2 0 74.38 3.52 4 2 0 62.37 3.28 4 2 1 88.34 4.07 4 2 1 77.79 3.99 4 2 1 87.59 4.03 4 2 1 73.48 3.83 4 2 1 81.99 4.02 -4 -2 -2 41.71 3.60 4 2 2 42.71 2.35 4 2 2 36.22 2.11 4 2 2 40.72 2.32 4 2 2 47.56 2.37 4 2 2 35.95 2.15 4 2 2 42.15 2.32 -4 -2 -3 80.89 5.43 4 2 3 85.00 3.93 4 2 3 71.52 3.66 4 2 3 86.72 3.92 4 2 3 70.88 3.69 4 2 3 81.42 3.89 -4 -2 -4 68.08 4.75 -4 -2 -4 74.03 5.08 4 2 4 75.81 3.55 4 2 4 64.44 3.29 4 2 4 73.85 3.51 4 2 4 62.76 3.31 4 2 4 69.62 3.49 4 2 6 41.14 2.31 4 2 6 49.41 2.56 -4 -2 -6 48.14 3.83 4 2 6 47.53 2.52 4 2 7 23.06 1.45 4 2 7 24.00 1.61 -4 -2 -7 21.57 2.56 4 2 7 24.66 1.62 4 2 8 16.98 1.22 -4 -2 -8 20.25 2.45 4 2 8 21.41 1.44 4 2 9 47.04 2.54 -4 -2 -9 47.18 3.97 4 2 9 56.06 2.79 4 2 10 114.45 5.51 -4 -2 -10 117.66 7.27 4 2 10 122.30 5.60 4 2 11 18.42 1.27 -4 -2 -11 17.59 2.41 4 2 11 19.31 1.34 4 2 11 22.80 1.53 4 2 12 22.21 1.44 4 2 12 22.37 1.51 4 2 13 45.35 2.38 4 2 13 43.17 2.44 4 2 14 14.38 1.16 4 2 14 13.54 1.16 4 2 14 14.96 1.09 -4 -2 -14 10.57 2.04 4 2 15 57.09 2.88 4 2 15 56.12 2.88 4 2 15 48.04 2.78 4 2 15 56.70 2.78 4 2 16 57.79 5.11 4 2 16 66.18 3.29 4 2 16 68.04 3.28 4 2 16 58.59 3.21 -4 -2 -16 50.97 4.59 -4 -2 -16 42.17 4.32 4 2 16 69.59 3.20 4 2 17 10.85 2.25 4 2 17 15.45 1.26 4 2 17 14.62 1.22 4 2 17 12.96 1.20 -4 -2 -17 13.04 2.17 -4 -2 -17 11.50 2.16 4 2 18 31.67 3.78 4 2 18 37.97 2.15 4 2 18 35.44 2.08 4 2 18 31.64 2.04 -4 -2 -18 25.62 3.22 -4 -2 -18 27.40 3.29 4 2 19 317.92 16.31 4 2 19 295.68 13.18 -4 -2 -19 284.75 15.33 4 2 20 12.85 2.50 4 2 20 16.79 1.33 4 2 20 13.96 1.30 -4 -2 -20 11.12 2.16 4 2 21 26.87 3.62 -4 -2 -21 18.75 2.85 -4 -2 -21 16.76 2.77 4 2 21 30.23 1.92 4 2 21 31.65 1.91 4 2 22 116.85 5.55 -4 -2 -22 108.03 7.52 4 2 23 107.80 5.24 4 2 24 13.32 1.31 4 2 25 1.99 0.83 4 2 26 64.17 3.45 4 2 27 10.40 1.18 4 2 28 155.36 7.18 4 2 29 2.55 0.78 4 2 30 54.14 2.98 4 2 31 61.86 3.25 4 2 32 51.50 2.81 4 2 33 19.47 1.42 4 2 34 1.17 0.55 4 2 35 4.25 0.67 4 2 36 5.27 0.69 4 3 -33 12.56 1.08 4 3 -32 0.66 0.53 4 3 -31 0.55 0.57 4 3 -30 3.66 0.83 4 3 -29 6.40 0.99 4 3 -29 8.08 0.88 4 3 -28 10.49 1.27 4 3 -28 14.81 1.20 4 3 -27 10.79 1.25 4 3 -27 11.19 1.10 4 3 -26 25.31 1.96 4 3 -26 26.12 1.77 4 3 -25 1.17 0.74 4 3 -25 1.67 0.63 4 3 -24 62.97 3.82 4 3 -24 77.25 3.75 4 3 -23 75.11 4.24 4 3 -23 81.97 4.07 4 3 -22 121.57 6.31 4 3 -22 135.37 6.15 4 3 -21 6.01 1.11 4 3 -21 7.77 0.99 4 3 -20 67.97 4.00 4 3 -20 78.70 3.89 4 3 -19 22.65 1.94 4 3 -19 29.10 1.90 4 3 -18 99.35 5.33 4 3 -18 109.94 5.19 4 3 -18 100.49 7.95 -4 -3 18 112.11 6.12 -4 -3 17 36.17 2.98 4 3 -17 38.30 2.28 4 3 -17 34.17 2.41 -4 -3 17 30.31 3.89 4 3 -17 36.19 4.42 -4 -3 16 3.40 1.09 4 3 -16 3.63 0.74 4 3 -16 3.16 0.87 -4 -3 16 2.71 1.44 4 3 -16 1.53 1.35 -4 -3 15 94.86 5.77 4 3 -15 103.18 4.88 4 3 -15 98.54 5.05 -4 -3 15 95.36 7.17 4 3 -15 96.39 7.51 -4 -3 14 104.97 6.00 4 3 -14 102.43 4.95 4 3 -14 100.10 5.14 4 3 -14 96.86 7.47 -4 -3 14 107.22 7.46 -4 -3 13 86.68 5.57 4 3 -13 97.99 4.65 4 3 -13 92.49 4.82 4 3 -13 98.24 7.36 -4 -3 13 96.73 6.94 -4 -3 12 14.71 2.51 -4 -3 12 13.83 1.89 4 3 -12 12.97 1.16 4 3 -12 13.38 1.31 4 3 -12 11.43 1.12 4 3 -12 11.43 2.45 -4 -3 11 86.05 6.25 -4 -3 11 81.89 5.17 4 3 -11 76.78 3.87 4 3 -11 76.38 4.08 4 3 -11 80.23 6.35 4 3 -11 75.52 3.85 -4 -3 10 2.74 1.44 -4 -3 10 1.65 1.00 4 3 -10 1.71 0.55 4 3 -10 2.01 0.72 4 3 -10 3.72 1.64 4 3 -10 2.07 0.66 -4 -3 9 21.15 2.40 4 3 -9 18.04 1.44 4 3 -9 21.25 1.45 4 3 -9 20.26 1.61 -4 -3 9 17.47 2.68 4 3 -9 17.76 1.42 -4 -3 8 6.64 1.55 4 3 -8 8.19 1.00 4 3 -8 11.00 1.13 -4 -3 8 9.38 1.99 4 3 -8 8.65 1.00 -4 -3 7 143.95 7.85 4 3 -7 131.30 6.17 4 3 -7 132.93 6.24 4 3 -7 124.57 6.05 -4 -3 6 2.29 1.30 4 3 -6 2.68 0.77 4 3 -6 2.14 0.68 -4 -3 6 1.20 1.22 4 3 -6 1.98 0.67 -4 -3 5 349.11 15.68 -4 -3 5 357.98 16.37 4 3 -5 330.97 14.33 4 3 -5 339.22 14.39 -4 -3 5 357.95 16.67 4 3 -5 311.95 14.21 4 3 -4 140.19 6.41 4 3 -4 137.99 6.40 -4 -3 4 143.31 7.65 4 3 -4 132.70 6.27 4 3 -3 179.48 8.62 4 3 -3 203.71 8.82 4 3 -3 210.17 8.85 -4 -3 3 225.86 10.40 4 3 -3 190.89 8.68 4 3 -2 263.81 12.14 4 3 -2 290.21 12.32 4 3 -2 308.38 12.39 -4 -3 2 297.76 13.88 4 3 -2 274.42 12.19 -4 -3 0 157.87 8.60 4 3 0 161.30 7.12 4 3 0 138.07 6.87 4 3 0 158.10 7.06 4 3 0 141.45 6.91 -4 -3 -1 81.34 5.42 4 3 1 78.05 3.95 4 3 1 68.17 3.72 4 3 1 80.75 3.91 4 3 1 72.54 3.79 4 3 2 50.50 2.81 4 3 2 59.35 3.00 4 3 2 60.38 3.07 -4 -3 -2 66.94 4.64 4 3 2 53.42 2.87 4 3 3 62.30 3.24 4 3 3 68.60 3.38 4 3 3 73.44 3.49 -4 -3 -3 68.55 4.64 -4 -3 -3 62.24 4.80 4 3 3 60.66 3.25 4 3 4 16.49 1.23 4 3 4 15.71 1.30 4 3 4 19.74 1.44 -4 -3 -4 18.40 2.31 -4 -3 -4 19.08 2.54 4 3 4 17.60 1.30 4 3 5 49.45 2.75 4 3 5 62.21 3.04 -4 -3 -5 56.85 4.28 -4 -3 -5 54.04 4.36 4 3 6 15.63 1.18 4 3 6 16.21 1.21 -4 -3 -6 16.72 2.30 -4 -3 -6 16.52 2.42 4 3 7 72.81 3.64 4 3 7 78.45 3.85 4 3 7 72.60 3.67 -4 -3 -7 88.46 5.53 -4 -3 -7 84.84 5.61 4 3 8 20.29 1.40 4 3 8 21.12 1.53 4 3 8 22.26 1.47 -4 -3 -8 21.65 2.62 -4 -3 -8 24.89 2.88 4 3 9 97.72 4.68 4 3 9 98.76 4.63 -4 -3 -9 113.80 6.68 -4 -3 -9 98.37 6.49 4 3 10 55.21 2.90 4 3 10 58.89 2.93 4 3 10 54.16 2.83 -4 -3 -10 48.73 4.29 4 3 11 32.72 1.95 4 3 11 32.87 1.94 4 3 11 30.93 1.86 -4 -3 -11 34.47 3.37 4 3 12 18.42 1.40 4 3 12 23.01 1.50 4 3 12 21.61 1.39 -4 -3 -12 20.05 2.63 -4 -3 -12 16.74 2.53 4 3 13 45.48 2.51 4 3 13 45.26 2.53 4 3 13 46.32 2.42 -4 -3 -13 38.60 3.87 4 3 14 11.68 1.07 4 3 14 10.88 1.06 4 3 14 11.61 0.99 4 3 15 230.74 9.91 4 3 15 221.68 9.92 4 3 15 230.53 9.80 4 3 16 13.86 1.20 4 3 16 15.02 1.26 4 3 16 14.51 1.15 4 3 17 54.79 2.90 4 3 17 51.75 2.92 4 3 17 64.68 5.29 -4 -3 -17 49.13 4.52 -4 -3 -17 40.11 4.08 4 3 17 54.91 2.79 4 3 18 101.08 4.84 4 3 18 98.21 4.87 4 3 18 79.12 6.84 -4 -3 -18 87.41 6.58 -4 -3 -18 88.52 6.51 4 3 18 110.08 4.77 4 3 19 57.78 2.98 4 3 19 51.85 2.86 4 3 19 46.66 4.86 -4 -3 -19 38.58 4.16 -4 -3 -19 47.98 4.48 4 3 20 104.73 4.85 4 3 20 98.00 4.74 4 3 20 86.02 7.05 -4 -3 -20 85.29 6.50 -4 -3 -20 83.32 6.47 -4 -3 -21 100.26 7.41 -4 -3 -21 101.33 7.45 4 3 21 124.10 5.71 4 3 21 121.31 5.63 4 3 22 134.40 6.39 4 3 22 135.50 6.33 4 3 23 112.24 5.39 4 3 24 9.48 1.10 4 3 26 20.44 1.66 4 3 27 15.36 1.43 4 3 28 7.79 1.10 4 3 29 2.69 0.79 4 3 30 1.05 0.68 4 3 31 15.55 1.36 4 3 32 7.36 0.95 4 3 33 8.66 0.96 4 3 34 2.76 0.65 4 3 35 8.97 0.89 4 3 36 1.29 0.51 4 3 37 1.35 0.46 4 4 -34 2.54 0.51 4 4 -33 3.04 0.61 4 4 -32 3.57 0.66 4 4 -31 5.77 0.83 4 4 -31 6.13 0.71 4 4 -30 8.62 1.06 4 4 -30 9.58 0.91 4 4 -29 4.04 0.86 4 4 -29 3.56 0.64 4 4 -28 10.41 1.23 4 4 -28 13.62 1.13 4 4 -27 11.68 1.27 4 4 -27 11.19 1.07 4 4 -26 10.33 1.28 4 4 -26 13.63 1.20 4 4 -25 11.59 1.33 4 4 -25 12.95 1.20 4 4 -24 24.10 2.00 4 4 -24 32.21 1.97 4 4 -23 9.39 1.28 4 4 -23 10.95 1.15 4 4 -22 24.14 2.01 4 4 -22 30.62 1.97 4 4 -21 20.74 1.83 4 4 -21 24.61 1.75 4 4 -20 35.55 2.55 4 4 -20 42.44 2.50 4 4 -19 10.13 1.27 4 4 -19 11.60 1.21 4 4 -18 2.83 0.91 4 4 -18 2.32 0.70 4 4 -17 21.99 1.82 4 4 -17 22.44 1.73 4 4 -16 13.48 1.41 4 4 -16 14.36 1.33 4 4 -16 13.85 2.96 -4 -4 15 51.55 3.61 4 4 -15 48.46 2.81 4 4 -15 47.19 2.92 4 4 -15 38.43 4.91 -4 -4 15 52.90 4.93 -4 -4 14 11.12 1.63 4 4 -14 9.55 1.13 4 4 -14 12.20 1.29 4 4 -14 11.56 2.65 -4 -4 14 13.02 2.49 -4 -4 13 18.02 2.82 -4 -4 13 18.06 2.12 4 4 -13 18.15 1.49 4 4 -13 16.79 1.55 4 4 -13 19.25 1.51 4 4 -13 15.61 2.95 -4 -4 12 71.88 5.82 -4 -4 12 72.73 4.70 4 4 -12 69.43 3.72 4 4 -12 72.27 3.87 4 4 -12 72.80 6.39 4 4 -12 71.60 3.72 -4 -4 11 17.67 2.74 4 4 -11 18.71 1.57 -4 -4 11 14.99 2.00 4 4 -11 15.94 2.90 4 4 -11 18.16 1.50 -4 -4 10 55.49 4.10 -4 -4 10 53.74 3.78 4 4 -10 58.40 3.27 -4 -4 10 57.42 4.95 4 4 -10 58.85 3.17 -4 -4 9 23.57 2.52 -4 -4 9 19.46 2.16 4 4 -9 21.83 1.64 -4 -4 9 21.96 3.01 4 4 -9 21.24 1.64 4 4 -9 23.10 1.75 -4 -4 8 24.65 2.64 -4 -4 8 17.64 2.07 4 4 -8 22.93 1.71 -4 -4 8 21.17 2.97 4 4 -8 22.62 1.66 -4 -4 7 19.47 2.15 -4 -4 7 19.43 2.45 4 4 -7 22.74 1.65 4 4 -7 23.14 1.70 -4 -4 7 22.36 2.91 4 4 -7 20.43 1.61 -4 -4 6 5.06 1.39 -4 -4 6 2.29 1.03 4 4 -6 4.17 0.84 4 4 -6 4.42 0.85 -4 -4 6 3.85 1.45 4 4 -6 4.15 0.84 -4 -4 5 112.70 6.55 -4 -4 5 121.62 7.21 4 4 -5 119.73 5.64 4 4 -5 118.70 5.61 -4 -4 5 130.63 7.64 4 4 -5 108.46 5.49 4 4 -4 3.43 0.83 4 4 -4 5.00 1.00 4 4 -4 4.97 0.93 4 4 -3 50.63 2.91 4 4 -3 61.03 3.07 -4 -4 3 55.97 3.96 4 4 -3 45.94 2.82 4 4 -2 239.88 10.89 4 4 -2 254.80 11.02 4 4 -2 264.96 11.13 -4 -4 2 266.46 12.50 4 4 -2 239.86 10.95 4 4 0 142.41 6.64 4 4 0 155.12 6.90 -4 -4 0 149.58 8.18 4 4 0 142.78 6.71 4 4 1 154.12 6.98 4 4 1 169.44 7.26 -4 -4 -1 149.23 8.23 -4 -4 -1 170.17 8.75 4 4 1 142.10 6.99 4 4 2 89.48 4.41 4 4 2 99.24 4.68 4 4 2 88.67 4.46 -4 -4 -2 89.57 5.60 -4 -4 -2 99.51 6.03 4 4 3 159.27 6.89 -4 -4 -3 144.07 8.01 -4 -4 -3 161.33 8.50 4 4 3 133.50 6.62 4 4 4 116.17 5.12 -4 -4 -4 102.57 6.21 -4 -4 -4 112.28 6.64 4 4 6 44.56 2.56 4 4 6 53.35 2.86 -4 -4 -6 52.43 4.02 -4 -4 -6 49.39 4.15 4 4 7 7.48 0.84 4 4 7 10.87 1.14 -4 -4 -7 6.93 1.73 -4 -4 -7 6.52 1.53 4 4 8 23.37 1.53 4 4 8 23.00 1.71 -4 -4 -8 23.10 2.66 -4 -4 -8 28.70 3.10 4 4 9 29.53 1.83 -4 -4 -9 37.86 3.37 -4 -4 -9 32.66 3.31 4 4 10 21.05 1.49 4 4 10 21.55 1.43 -4 -4 -10 18.31 2.46 -4 -4 -10 17.17 2.57 4 4 11 4.62 0.78 4 4 11 6.24 0.77 -4 -4 -11 5.36 1.62 -4 -4 -11 6.03 1.56 4 4 12 16.03 1.31 4 4 12 16.19 1.24 -4 -4 -12 17.83 2.46 -4 -4 -12 18.27 2.57 4 4 13 7.99 0.94 4 4 13 8.61 0.97 4 4 13 7.94 0.87 -4 -4 -13 7.02 1.84 -4 -4 -13 9.76 1.94 4 4 14 88.85 4.53 4 4 14 94.84 4.60 4 4 14 95.55 4.43 -4 -4 -14 85.70 6.13 -4 -4 -14 97.84 6.49 4 4 15 338.71 14.93 4 4 15 353.78 15.01 4 4 15 368.17 14.82 -4 -4 -15 304.67 16.78 -4 -4 -15 311.59 16.91 4 4 16 298.25 13.34 4 4 16 310.58 13.41 4 4 16 324.80 13.22 4 4 17 135.85 6.71 4 4 17 146.93 6.80 -4 -4 -17 131.37 8.49 4 4 17 156.56 6.62 4 4 18 124.42 5.99 4 4 18 122.39 6.04 4 4 18 119.76 8.69 -4 -4 -18 125.45 7.93 4 4 18 136.11 5.89 4 4 19 128.89 6.00 4 4 19 124.40 6.03 4 4 19 114.66 8.66 4 4 19 142.75 5.88 -4 -4 -19 99.24 7.40 -4 -4 -19 101.03 7.52 -4 -4 -20 2.07 1.34 4 4 20 4.21 0.82 4 4 20 3.10 0.79 4 4 21 107.74 5.27 4 4 21 110.91 5.37 4 4 22 43.97 2.66 4 4 22 43.50 2.58 4 4 23 3.17 0.78 4 4 23 4.54 0.92 4 4 24 41.76 2.55 4 4 24 39.96 2.43 4 4 25 19.13 1.48 4 4 26 53.68 2.95 4 4 30 1.35 0.73 4 4 31 4.06 0.81 4 4 32 20.77 1.51 4 4 33 4.23 0.76 4 4 34 2.48 0.64 4 4 35 8.35 0.84 4 4 36 3.62 0.59 4 4 37 35.82 1.88 4 5 -32 17.18 1.19 4 5 -31 10.37 0.96 4 5 -30 2.07 0.59 4 5 -29 21.02 1.53 4 5 -28 14.03 1.10 4 5 -28 13.86 1.26 4 5 -27 29.32 1.82 4 5 -27 31.57 2.04 4 5 -26 5.66 0.77 4 5 -26 4.13 0.86 4 5 -25 0.16 0.48 4 5 -25 0.56 0.68 4 5 -24 27.71 1.84 4 5 -24 26.77 1.97 4 5 -23 26.91 1.84 4 5 -23 26.72 1.99 4 5 -22 19.40 1.56 4 5 -22 19.74 1.68 4 5 -21 32.31 2.08 4 5 -21 28.96 2.17 4 5 -20 11.72 1.23 4 5 -20 10.19 1.29 4 5 -19 89.98 4.51 4 5 -19 84.62 4.59 4 5 -18 79.58 4.18 4 5 -18 79.74 4.28 4 5 -17 63.65 3.60 4 5 -17 69.73 3.77 4 5 -16 90.79 4.68 4 5 -16 92.11 4.76 4 5 -15 7.29 1.15 4 5 -15 6.81 1.03 4 5 -15 7.08 1.07 4 5 -14 1.68 0.81 4 5 -14 0.96 0.75 4 5 -13 47.04 2.84 4 5 -13 49.31 2.92 4 5 -12 14.38 1.38 4 5 -12 12.84 1.36 4 5 -12 12.67 2.84 -4 -5 12 11.87 1.61 -4 -5 11 34.44 3.75 4 5 -11 41.62 4.88 -4 -5 11 31.62 2.75 4 5 -11 35.62 2.31 -4 -5 10 6.26 1.26 4 5 -10 6.81 1.07 -4 -5 10 7.69 1.89 -4 -5 9 105.27 5.96 -4 -5 9 118.00 7.47 4 5 -9 103.22 5.21 -4 -5 8 10.34 1.64 -4 -5 8 12.17 2.23 4 5 -8 13.93 1.39 4 5 -8 14.18 1.40 -4 -5 7 13.97 1.87 -4 -5 7 16.04 2.50 4 5 -7 15.38 1.48 4 5 -7 18.94 1.58 -4 -5 6 0.86 1.09 4 5 -6 0.40 0.73 4 5 -6 -0.11 0.75 -4 -5 5 41.89 3.30 -4 -5 5 43.72 3.98 4 5 -5 38.90 2.53 4 5 -5 45.91 2.71 4 5 -4 11.46 1.28 -4 -5 4 9.14 1.53 4 5 -4 9.85 1.19 4 5 -3 99.24 5.17 4 5 -3 118.09 5.49 -4 -5 3 113.83 6.38 4 5 -3 109.35 5.31 4 5 -2 42.26 2.56 4 5 -2 51.16 2.86 4 5 -2 48.23 2.73 4 5 0 88.44 4.42 4 5 0 99.48 4.74 -4 -5 0 85.11 5.36 -4 -5 0 95.76 5.73 4 5 0 85.73 4.48 4 5 1 68.55 3.56 4 5 1 79.14 3.92 -4 -5 -1 63.89 4.51 -4 -5 -1 71.43 4.82 4 5 1 67.15 3.65 4 5 2 34.22 2.06 4 5 2 34.58 2.31 -4 -5 -2 32.49 2.98 -4 -5 -2 33.06 3.12 4 5 2 32.56 2.13 4 5 3 28.55 1.89 4 5 3 35.29 2.26 4 5 3 29.83 2.02 -4 -5 -3 32.07 2.97 -4 -5 -3 32.97 3.09 4 5 4 30.64 2.16 4 5 5 47.90 2.70 -4 -5 -5 43.48 3.75 -4 -5 -5 43.60 3.83 4 5 6 24.58 1.63 4 5 6 26.30 1.93 -4 -5 -6 21.50 2.53 -4 -5 -6 23.67 2.72 4 5 7 0.55 0.51 4 5 7 1.84 0.86 -4 -5 -7 1.00 1.04 -4 -5 -7 0.41 0.91 4 5 8 1.90 0.60 4 5 8 1.56 0.81 -4 -5 -8 0.73 0.94 -4 -5 -8 0.97 0.86 4 5 9 18.02 1.32 4 5 9 17.05 1.53 -4 -5 -9 17.37 2.29 -4 -5 -9 17.75 2.40 -4 -5 -10 16.67 2.30 4 5 10 18.14 1.32 -4 -5 -11 26.59 2.90 4 5 11 26.41 1.69 -4 -5 -12 2.67 1.17 4 5 12 0.53 0.60 -4 -5 -13 5.42 1.45 4 5 13 8.20 1.00 -4 -5 -14 16.43 2.35 4 5 14 19.97 1.54 -4 -5 -15 3.37 1.36 4 5 15 5.22 0.88 4 5 15 5.29 0.91 4 5 16 67.10 3.46 4 5 16 68.76 3.54 4 5 17 186.01 8.50 4 5 17 190.29 8.59 4 5 18 194.35 8.78 4 5 18 194.50 8.87 4 5 19 63.07 3.42 4 5 19 64.84 3.52 4 5 20 20.05 1.54 4 5 20 17.95 1.55 4 5 21 52.12 2.93 4 5 21 53.70 3.05 4 5 22 3.55 0.78 4 5 22 3.73 0.85 4 5 23 48.93 2.87 4 5 23 49.76 2.76 4 5 24 29.58 2.02 4 5 25 65.91 3.52 4 5 26 11.57 1.19 4 5 32 17.76 1.33 4 5 33 23.71 1.53 4 5 34 2.10 0.55 4 5 35 30.18 1.70 4 5 36 25.03 1.43 4 6 -29 30.98 1.73 4 6 -28 3.28 0.57 4 6 -27 2.20 0.55 4 6 -26 3.30 0.67 4 6 -25 2.50 0.64 4 6 -25 2.76 0.57 4 6 -24 14.80 1.18 4 6 -23 0.98 0.53 4 6 -22 40.58 2.38 4 6 -21 18.89 1.47 4 6 -20 27.26 1.88 4 6 -19 13.14 1.27 4 6 -18 28.16 1.97 4 6 -17 6.63 1.00 4 6 -16 63.40 3.52 4 6 -16 67.47 3.61 4 6 -15 98.87 4.96 4 6 -14 37.27 2.44 4 6 -13 61.65 3.47 4 6 -12 56.64 3.26 4 6 -11 106.29 5.32 4 6 -10 165.47 7.74 4 6 -8 18.48 1.67 4 6 -7 19.52 1.71 4 6 -6 50.36 2.96 4 6 -6 42.69 2.64 4 6 -5 49.29 3.00 4 6 -5 47.01 2.74 4 6 -4 52.44 2.99 4 6 -4 38.91 2.52 -4 -6 2 76.88 5.02 -4 -6 2 71.34 4.05 -4 -6 1 86.65 5.33 4 6 -1 86.89 4.62 -4 -6 0 40.46 3.36 -4 -6 0 40.76 3.42 4 6 0 46.47 2.84 -4 -6 -1 123.08 7.40 -4 -6 -1 141.35 7.61 4 6 1 148.37 6.85 -4 -6 -2 192.01 10.14 -4 -6 -2 197.15 10.16 4 6 2 208.42 9.35 -4 -6 -3 215.66 10.47 4 6 3 220.11 9.52 -4 -6 -4 55.27 4.09 -4 -6 -5 24.92 2.64 4 6 5 26.63 2.05 -4 -6 -6 23.99 2.71 4 6 6 37.34 2.40 -4 -6 -7 33.59 3.10 4 6 7 32.79 2.32 4 6 8 10.41 1.34 4 6 9 66.88 3.73 4 6 10 1.05 0.79 4 6 12 1.12 0.65 4 6 13 13.33 1.28 4 6 14 12.92 1.26 4 6 15 10.44 1.12 4 6 16 21.39 1.61 4 6 16 21.90 1.69 4 6 17 15.78 1.39 4 6 17 16.91 1.46 4 6 18 20.21 1.55 4 6 18 20.56 1.63 4 6 19 27.10 1.91 4 6 20 7.35 1.03 4 6 21 16.74 1.43 4 6 22 0.77 0.61 4 6 23 25.62 1.80 4 6 24 2.53 0.70 4 6 25 2.09 0.66 4 6 33 1.66 0.49 4 6 34 4.17 0.55 4 7 -25 12.42 0.90 4 7 -21 2.52 0.56 4 7 -20 3.40 0.63 4 7 -19 9.67 1.00 4 7 -18 8.05 0.94 4 7 -17 4.31 0.83 4 7 -17 2.87 0.69 4 7 -16 2.02 0.78 4 7 -16 2.44 0.67 4 7 -15 20.09 1.61 4 7 -14 42.61 2.59 4 7 -13 75.28 3.96 4 7 -12 21.14 1.76 4 7 -11 1.32 0.90 -4 -7 9 10.48 1.21 -4 -7 8 41.04 2.52 -4 -7 7 103.13 5.34 4 7 -7 118.82 5.58 -4 -7 6 64.78 3.63 4 7 -6 71.96 3.85 -4 -7 5 149.71 7.16 4 7 -5 157.89 7.37 -4 -7 4 37.15 2.63 4 7 -4 65.58 3.23 -4 -7 2 56.83 3.15 4 7 -2 54.34 3.31 -4 -7 1 258.38 11.19 4 7 -1 243.33 11.38 -4 -7 0 256.09 11.02 4 7 0 237.17 11.19 -4 -7 -1 278.44 11.61 4 7 1 242.31 11.73 -4 -7 -2 83.33 3.95 4 7 2 63.85 3.98 4 7 3 51.86 3.16 -4 -7 -4 35.43 2.15 4 7 4 28.08 2.22 -4 -7 -6 39.38 2.32 4 7 6 31.51 2.37 -4 -7 -7 15.73 1.33 4 7 7 10.52 1.38 -4 -7 -8 92.31 4.31 4 7 8 74.50 4.37 4 7 9 2.81 0.93 4 7 10 1.59 0.83 4 7 12 10.55 1.14 4 7 13 36.80 2.24 4 7 15 9.14 1.10 4 7 16 14.24 1.30 4 7 17 19.39 1.55 4 7 18 58.01 3.14 4 7 19 57.61 3.10 4 7 20 25.13 1.73 -4 -8 20 3.30 0.53 -4 -8 19 2.23 0.52 -4 -8 18 1.62 0.49 -4 -8 17 5.52 0.73 4 8 -17 5.78 0.73 -4 -8 16 2.13 0.57 4 8 -16 1.82 0.61 -4 -8 15 33.06 1.95 4 8 -15 33.97 1.98 4 8 -15 32.88 1.97 -4 -8 14 32.60 1.96 4 8 -14 34.34 2.00 4 8 -14 30.92 1.94 -4 -8 13 28.38 1.84 4 8 -13 31.28 1.92 -4 -8 12 1.50 0.60 4 8 -12 2.39 0.73 -4 -8 11 9.32 1.00 4 8 -11 8.91 1.07 -4 -8 10 3.48 0.75 4 8 -10 3.74 0.85 -4 -8 9 11.18 1.14 4 8 -9 12.76 1.25 -4 -8 8 1.51 0.67 4 8 -8 2.99 0.82 -4 -8 7 2.86 0.73 4 8 -7 3.08 0.83 -4 -8 6 20.43 1.52 4 8 -6 20.29 1.59 4 8 -6 16.90 1.55 -4 -8 5 25.86 1.82 4 8 -5 29.36 1.96 4 8 -5 26.74 1.96 -4 -8 4 16.60 1.42 4 8 -4 20.10 1.66 -4 -8 3 66.79 3.56 4 8 -3 70.13 3.74 -4 -8 2 77.84 4.01 4 8 -2 80.74 4.07 4 8 -2 79.64 4.20 -4 -8 1 96.11 4.59 4 8 -1 89.31 4.57 4 8 -1 92.35 4.75 4 8 0 113.36 5.65 -4 -8 0 124.60 5.69 4 8 0 120.89 5.88 -4 -8 -1 77.31 3.82 4 8 1 69.58 3.93 -4 -8 -2 103.39 4.79 4 8 2 89.63 4.88 -4 -8 -4 32.86 2.03 4 8 4 28.57 2.15 -4 -8 -5 15.83 1.32 4 8 5 13.58 1.42 -4 -8 -6 10.57 1.12 4 8 6 9.76 1.21 -4 -8 -7 10.39 1.06 4 8 7 8.60 1.16 -4 -8 -8 37.94 2.21 4 8 8 33.38 2.32 -4 -8 -9 8.43 0.98 4 8 9 6.78 1.04 -4 -8 -10 12.85 1.12 4 8 10 9.12 1.16 -4 -8 -11 12.12 1.11 -4 -8 -12 3.36 0.70 -4 -8 -13 10.40 1.02 -4 -8 -14 9.65 0.99 4 8 14 11.00 1.03 -4 -8 -15 5.08 0.74 -4 -9 11 2.09 0.44 4 9 -11 1.72 0.50 4 9 -10 7.74 0.79 -4 -9 10 7.44 0.72 4 9 -9 17.94 1.22 -4 -9 9 16.92 1.15 4 9 -8 7.80 0.83 -4 -9 8 8.15 0.77 4 9 -7 16.97 1.23 -4 -9 7 17.30 1.18 4 9 -6 22.88 1.45 -4 -9 6 20.83 1.37 4 9 -5 19.19 1.31 -4 -9 5 16.14 1.20 4 9 -4 50.99 2.64 -4 -9 4 50.82 2.60 4 9 -3 40.96 2.11 -4 -9 3 33.63 2.00 4 9 -2 9.45 0.94 -4 -9 2 8.81 0.86 -4 -9 1 73.23 3.53 -4 -9 0 47.31 2.33 4 9 0 37.49 2.38 -4 -9 -1 75.57 3.50 4 9 1 67.01 3.60 -4 -9 -2 16.03 1.12 4 9 2 11.15 1.17 -4 -9 -3 35.71 1.88 4 9 3 27.74 1.95 -4 -9 -4 36.66 1.89 4 9 4 26.50 1.91 -4 -9 -5 39.65 2.05 4 9 5 32.35 2.14 -4 -9 -6 27.00 1.62 -4 -9 -7 26.69 1.61 -4 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2.20 5 -1 21 33.45 2.25 5 -1 22 26.14 1.63 5 -1 22 22.93 1.72 5 -1 23 2.06 0.59 5 -1 23 2.03 0.66 5 -1 24 7.84 0.87 5 -1 25 1.52 0.54 5 -1 26 6.01 0.73 5 -1 27 2.91 0.56 5 -1 28 6.69 0.70 5 0 -29 23.22 1.42 5 0 -28 -0.03 0.43 5 0 -27 0.76 0.49 5 0 -26 2.83 0.64 5 0 -25 4.52 0.77 5 0 -24 8.17 0.97 5 0 -23 10.30 1.11 5 0 -22 41.68 2.51 5 0 -21 0.35 0.62 5 0 -21 1.45 0.69 5 0 -20 15.68 1.43 5 0 -20 14.79 1.39 5 0 -19 7.38 1.07 5 0 -19 6.48 0.99 5 0 -18 4.37 0.91 5 0 -18 3.26 0.82 5 0 -17 31.40 2.17 5 0 -17 29.66 2.06 5 0 -16 18.67 1.67 5 0 -16 20.36 1.64 5 0 -15 14.27 1.47 5 0 -15 16.37 1.43 5 0 -14 20.42 1.74 5 0 -14 19.22 1.61 5 0 -13 27.50 2.04 5 0 -13 26.44 1.91 5 0 -12 7.86 1.16 5 0 -12 8.33 1.06 5 0 -11 96.53 4.99 5 0 -10 39.53 2.60 5 0 -10 40.99 2.23 5 0 -9 28.83 1.78 5 0 -9 28.41 2.10 5 0 -8 32.70 1.95 5 0 -8 32.08 2.28 5 0 -7 9.72 1.01 5 0 -7 7.90 1.18 5 0 -7 9.34 1.16 5 0 -6 3.54 0.89 5 0 -6 2.75 0.71 5 0 -6 3.71 0.86 5 0 -5 38.94 2.23 5 0 -5 36.93 2.50 5 0 -5 43.63 2.58 5 0 -4 8.23 0.93 5 0 -4 4.97 1.07 5 0 -4 7.72 1.11 5 0 -3 18.44 1.35 5 0 -3 19.99 1.63 5 0 -2 61.77 3.07 5 0 -2 53.50 3.38 5 0 -2 61.85 3.40 5 0 -1 35.24 1.97 5 0 -1 31.50 2.21 5 0 0 8.65 1.33 5 0 1 72.40 3.33 5 0 1 64.79 3.65 5 0 2 101.57 5.42 5 0 2 113.03 5.08 5 0 2 109.94 5.50 5 0 3 83.19 4.52 5 0 3 90.58 4.16 5 0 3 82.32 4.51 5 0 4 93.57 4.69 5 0 4 89.38 4.23 5 0 4 83.15 4.62 5 0 5 54.59 3.22 5 0 5 56.02 2.84 5 0 5 52.59 3.25 5 0 6 63.50 3.53 5 0 6 63.99 3.13 5 0 6 56.52 3.48 5 0 7 43.72 2.66 5 0 7 39.40 2.16 5 0 8 1.58 0.90 5 0 9 49.62 2.85 5 0 9 41.76 2.79 5 0 10 17.45 1.54 5 0 10 14.19 1.53 5 0 11 3.17 0.92 5 0 12 72.82 4.01 5 0 13 22.37 1.84 5 0 14 82.07 4.36 5 0 15 44.49 2.78 5 0 16 71.46 3.90 5 0 17 43.61 2.48 5 0 17 43.06 2.69 5 0 18 17.67 1.40 5 0 18 18.21 1.60 5 0 19 13.11 1.20 5 0 19 12.12 1.32 5 0 20 31.13 1.98 5 0 21 3.39 0.77 5 0 22 14.01 1.23 5 0 23 34.47 2.09 5 0 24 3.80 0.75 5 0 25 8.11 0.93 5 0 26 1.28 0.59 5 0 27 2.78 0.63 5 0 28 5.52 0.75 5 0 29 5.88 0.73 5 0 30 6.02 0.71 5 0 31 2.82 0.51 5 1 -31 9.21 0.83 5 1 -30 6.73 0.76 5 1 -29 0.91 0.50 5 1 -28 2.41 0.63 5 1 -27 7.82 0.95 5 1 -26 19.08 1.50 5 1 -25 7.31 1.00 5 1 -24 9.80 1.14 5 1 -23 17.21 1.53 5 1 -22 12.55 1.32 5 1 -21 1.96 0.78 5 1 -20 13.26 1.40 5 1 -19 10.31 1.27 5 1 -18 24.15 1.93 5 1 -17 2.98 0.95 5 1 -16 13.76 1.52 5 1 -16 17.11 1.49 5 1 -15 72.34 4.25 5 1 -15 86.37 4.25 5 1 -14 161.28 7.93 5 1 -14 173.29 7.83 5 1 -13 53.71 3.35 5 1 -13 58.99 3.23 5 1 -12 25.07 2.02 5 1 -12 24.97 1.84 5 1 -11 119.45 5.58 5 1 -11 116.05 6.01 5 1 -11 127.22 5.88 5 1 -10 79.66 3.96 5 1 -10 83.51 4.42 5 1 -9 271.03 11.78 5 1 -9 275.55 12.24 5 1 -8 1.18 0.74 5 1 -8 1.44 0.86 5 1 -7 45.30 2.66 5 1 -7 47.55 3.00 5 1 -6 32.11 2.04 5 1 -6 32.86 2.36 5 1 -6 38.58 2.37 5 1 -5 5.89 0.91 5 1 -5 6.77 1.10 5 1 -5 7.42 1.07 5 1 -4 23.38 1.63 5 1 -4 22.67 1.86 5 1 -4 24.50 1.86 5 1 -3 13.94 1.28 5 1 -3 16.38 1.55 5 1 -3 19.09 1.56 5 1 -2 36.64 2.24 5 1 -2 41.06 2.59 5 1 -2 42.24 2.58 5 1 -1 170.37 7.82 5 1 -1 176.55 8.22 5 1 -1 183.30 8.19 5 1 0 66.37 3.11 5 1 0 58.82 3.31 5 1 1 180.02 8.02 5 1 2 57.88 3.03 5 1 2 53.28 3.33 5 1 2 63.81 3.39 5 1 3 109.29 5.31 5 1 3 117.15 5.71 5 1 3 120.17 5.69 5 1 4 80.88 4.09 5 1 4 88.26 4.52 5 1 4 88.93 4.50 5 1 5 44.49 2.45 5 1 6 83.23 4.08 5 1 6 93.11 4.56 5 1 6 79.21 4.39 5 1 7 89.28 4.48 5 1 7 93.26 4.85 5 1 8 156.00 7.13 5 1 8 142.53 7.05 5 1 9 8.31 1.21 5 1 9 3.85 0.95 5 1 10 2.63 0.90 5 1 10 2.35 0.84 5 1 11 28.90 2.05 5 1 11 23.53 1.91 5 1 12 17.50 1.59 5 1 12 14.85 1.50 5 1 13 16.22 1.50 5 1 14 49.43 2.93 5 1 18 9.07 1.05 5 1 19 20.32 1.55 5 1 20 8.65 1.06 5 1 21 47.60 2.71 5 1 22 8.37 1.03 5 1 23 14.03 1.26 5 1 24 14.88 1.30 5 1 25 19.05 1.47 5 1 26 8.73 0.99 5 1 27 17.03 1.33 5 1 28 51.15 2.73 5 1 29 4.24 0.73 5 1 30 4.09 0.69 5 1 31 2.86 0.60 5 1 32 0.13 0.44 5 1 33 5.01 0.61 5 2 -31 8.90 0.84 5 2 -30 13.37 1.08 5 2 -29 2.79 0.61 5 2 -28 4.31 0.75 5 2 -27 5.16 0.81 5 2 -26 9.55 1.06 5 2 -25 2.69 0.74 5 2 -24 0.76 0.66 5 2 -23 5.22 0.92 5 2 -22 0.93 0.71 5 2 -21 3.70 0.88 5 2 -20 15.67 1.51 5 2 -19 40.13 2.81 5 2 -19 56.33 2.77 5 2 -18 53.06 3.16 5 2 -17 40.37 2.68 5 2 -17 45.06 2.67 5 2 -16 69.28 4.00 5 2 -16 78.24 3.99 5 2 -15 31.64 2.29 5 2 -15 33.27 2.25 5 2 -14 89.46 4.81 5 2 -14 94.95 4.77 5 2 -13 123.85 6.42 5 2 -13 140.14 6.44 5 2 -12 33.53 2.03 5 2 -12 30.89 2.27 5 2 -12 33.31 2.26 5 2 -11 16.88 1.40 5 2 -11 17.53 1.61 5 2 -11 19.42 1.63 5 2 -10 50.60 2.79 5 2 -10 49.25 3.04 5 2 -10 51.87 3.02 -5 -2 9 1.20 0.97 5 2 -9 1.44 0.70 5 2 -9 0.93 0.73 5 2 -9 1.08 0.74 -5 -2 8 15.72 2.19 5 2 -8 19.99 1.48 5 2 -8 18.37 1.64 5 2 -8 18.33 1.63 -5 -2 7 44.99 3.84 5 2 -7 43.20 2.50 5 2 -7 43.54 2.74 5 2 -7 44.41 2.73 -5 -2 6 22.76 2.84 5 2 -6 27.59 1.84 5 2 -6 30.05 2.10 5 2 -6 28.23 2.04 -5 -2 5 45.90 4.19 5 2 -5 52.21 2.95 5 2 -5 53.10 3.18 5 2 -5 53.73 3.17 -5 -2 4 1.94 1.11 5 2 -4 3.02 0.92 5 2 -4 2.67 0.76 5 2 -4 3.77 0.91 5 2 -4 2.75 0.85 -5 -2 3 17.34 2.59 5 2 -3 24.83 1.77 5 2 -3 18.04 1.47 5 2 -3 18.81 1.63 5 2 -3 20.79 1.69 5 2 -2 53.46 3.00 5 2 -2 56.48 3.25 -5 -2 1 60.51 5.14 5 2 -1 68.95 3.63 5 2 -1 70.91 3.87 5 2 1 41.98 2.41 5 2 2 34.62 2.13 5 2 2 36.08 2.40 5 2 2 38.33 2.37 5 2 3 7.14 0.93 5 2 3 7.61 1.15 5 2 3 7.48 1.05 5 2 4 65.67 3.49 5 2 4 70.24 3.80 5 2 4 74.50 3.79 5 2 5 34.64 2.29 5 2 5 30.43 1.95 5 2 5 34.03 2.22 5 2 6 27.96 2.08 5 2 6 27.60 1.78 5 2 6 28.86 2.02 5 2 7 62.94 3.45 5 2 7 60.29 3.40 5 2 8 17.76 1.52 5 2 8 15.40 1.44 -5 -2 -9 50.31 4.86 5 2 9 85.65 4.07 5 2 10 68.05 3.56 5 2 10 81.78 3.99 -5 -2 -11 1.11 1.05 -5 -2 -11 0.78 0.95 5 2 11 1.30 0.77 5 2 11 1.23 0.56 5 2 12 61.60 3.21 5 2 12 54.29 2.79 5 2 13 36.86 2.12 5 2 14 46.69 2.54 5 2 16 67.69 3.51 5 2 19 36.42 2.23 5 2 20 14.01 1.29 5 2 21 57.99 3.18 5 2 22 64.42 3.42 5 2 23 20.65 1.59 5 2 24 45.12 2.60 5 2 25 28.60 1.92 5 2 26 30.41 1.97 5 2 27 130.53 6.07 5 2 28 32.35 1.99 5 2 29 18.70 1.40 5 2 30 8.16 0.92 5 2 31 3.82 0.69 5 2 32 1.59 0.55 5 2 33 10.19 0.88 5 2 34 0.39 0.40 5 3 -27 5.95 0.80 5 3 -26 17.60 1.36 5 3 -25 21.92 1.60 5 3 -24 86.18 4.49 5 3 -24 95.15 4.41 5 3 -23 37.80 2.47 5 3 -23 45.78 2.43 5 3 -22 36.23 2.27 5 3 -22 30.41 2.17 5 3 -22 37.09 2.13 5 3 -21 39.91 2.50 5 3 -21 35.82 2.44 5 3 -20 39.75 2.53 5 3 -20 36.28 2.46 5 3 -20 44.63 2.43 5 3 -19 43.79 2.73 5 3 -19 42.04 2.67 5 3 -19 47.04 2.59 5 3 -18 41.33 2.68 5 3 -18 40.81 2.63 5 3 -18 46.38 2.54 5 3 -17 27.29 2.05 5 3 -17 26.09 1.99 5 3 -17 31.21 1.94 5 3 -16 25.36 1.93 5 3 -16 21.50 1.79 5 3 -16 27.34 1.77 5 3 -15 17.75 1.59 5 3 -14 15.81 1.53 5 3 -13 24.61 1.72 5 3 -13 24.76 1.91 5 3 -12 5.20 0.91 5 3 -12 5.79 1.00 5 3 -11 38.47 2.33 5 3 -11 37.69 2.51 5 3 -10 65.72 3.51 5 3 -10 67.32 3.74 5 3 -9 39.96 2.45 5 3 -9 43.04 2.67 5 3 -8 1.80 0.81 -5 -3 8 2.63 1.14 5 3 -8 1.56 0.81 5 3 -7 55.82 3.12 5 3 -7 53.63 3.05 -5 -3 7 44.68 4.09 5 3 -7 48.60 2.86 5 3 -6 69.73 3.77 5 3 -6 74.93 3.82 5 3 -6 65.53 3.56 5 3 -5 20.65 1.79 5 3 -5 26.36 1.89 -5 -3 5 17.82 2.65 5 3 -5 23.17 1.70 5 3 -4 47.09 2.89 5 3 -4 53.25 2.96 5 3 -4 46.01 2.70 5 3 -3 26.70 1.85 5 3 -3 31.22 2.15 5 3 -3 34.31 2.22 -5 -3 3 25.54 3.23 5 3 -3 29.28 1.96 5 3 -2 23.35 1.82 5 3 -2 27.31 1.96 5 3 -2 25.66 1.73 5 3 -1 42.09 2.57 5 3 -1 40.85 2.36 5 3 -1 34.97 2.21 5 3 -1 36.46 2.47 5 3 0 29.26 1.95 5 3 1 74.27 3.85 5 3 1 62.97 3.48 5 3 1 78.28 3.82 5 3 1 66.31 3.58 -5 -3 -2 5.66 1.71 5 3 2 8.85 1.19 5 3 2 6.83 0.92 5 3 2 8.90 1.12 5 3 2 6.80 0.99 -5 -3 -3 32.60 3.56 5 3 3 40.08 2.47 5 3 3 34.55 2.15 5 3 3 42.29 2.40 5 3 3 33.43 2.17 5 3 4 43.33 2.47 5 3 4 47.18 2.76 -5 -3 -4 40.54 3.99 5 3 4 42.47 2.50 5 3 5 63.50 3.33 5 3 5 59.04 3.30 -5 -3 -5 66.57 5.19 5 3 6 35.72 2.33 -5 -3 -6 30.64 3.48 5 3 7 2.51 0.72 5 3 7 5.81 0.97 -5 -3 -7 2.98 1.34 5 3 8 18.38 1.38 5 3 8 21.59 1.67 -5 -3 -9 37.14 3.94 5 3 9 52.50 2.72 -5 -3 -10 64.87 5.48 5 3 10 87.52 4.09 5 3 11 8.64 1.00 -5 -3 -11 6.07 1.70 -5 -3 -11 6.02 1.64 5 3 11 8.37 0.93 5 3 12 34.84 2.04 -5 -3 -12 20.76 2.94 -5 -3 -12 16.76 2.84 5 3 12 34.17 1.95 5 3 13 25.84 1.69 5 3 13 24.54 1.73 5 3 14 63.90 3.31 5 3 14 65.01 3.43 5 3 15 10.86 1.07 5 3 15 11.18 1.17 5 3 16 145.44 6.74 5 3 16 150.70 6.88 5 3 17 137.88 6.52 5 3 17 140.10 6.52 5 3 18 54.75 3.04 5 3 19 87.50 4.15 5 3 19 73.92 4.01 5 3 20 63.45 3.23 5 3 20 52.03 3.07 5 3 21 96.11 4.38 5 3 21 76.32 4.23 5 3 22 63.52 3.41 5 3 23 19.72 1.58 5 3 24 7.11 1.00 5 3 25 3.34 0.81 5 3 26 6.23 0.93 5 3 27 -0.12 0.63 5 3 28 0.39 0.60 5 3 29 9.87 1.03 5 3 30 2.63 0.68 5 3 31 5.08 0.74 5 3 32 3.43 0.63 5 3 33 6.83 0.74 5 3 34 16.22 1.11 5 4 -30 2.97 0.51 5 4 -29 0.06 0.41 5 4 -28 0.07 0.44 5 4 -27 10.15 1.00 5 4 -27 10.51 0.92 5 4 -26 3.31 0.68 5 4 -26 3.15 0.58 5 4 -25 31.14 2.06 5 4 -25 36.98 2.02 5 4 -24 14.68 1.34 5 4 -24 17.50 1.28 5 4 -23 3.88 0.84 5 4 -23 4.52 0.73 5 4 -22 4.64 0.90 5 4 -22 6.66 0.83 5 4 -21 12.60 1.36 5 4 -21 17.53 1.35 5 4 -20 0.32 0.65 5 4 -20 0.17 0.54 5 4 -19 3.63 0.86 5 4 -19 2.75 0.74 5 4 -18 65.11 3.97 5 4 -18 88.24 4.03 5 4 -17 16.55 1.60 5 4 -17 21.88 1.59 5 4 -16 19.02 1.75 5 4 -16 24.74 1.72 5 4 -15 6.56 1.08 5 4 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49.85 4.32 5 4 0 51.74 3.03 5 4 1 83.91 4.23 5 4 1 78.01 4.25 5 4 2 103.05 4.90 5 4 2 108.93 5.18 -5 -4 -2 97.12 6.58 5 4 2 91.10 4.86 5 4 3 53.54 2.93 -5 -4 -3 45.82 4.31 5 4 3 48.97 2.92 5 4 4 184.68 8.41 5 4 4 201.64 8.75 -5 -4 -4 189.71 10.50 5 4 4 177.96 8.40 5 4 5 70.65 3.68 5 4 5 74.59 3.94 -5 -4 -5 62.80 5.26 -5 -4 -6 53.34 4.57 5 4 7 9.96 1.10 5 4 7 12.43 1.36 5 4 7 11.75 1.16 -5 -4 -7 7.54 1.96 -5 -4 -7 8.32 1.78 5 4 8 16.44 1.33 5 4 8 15.57 1.51 5 4 8 17.15 1.39 -5 -4 -8 14.31 2.47 -5 -4 -8 11.61 2.06 5 4 9 21.70 1.64 -5 -4 -9 20.08 2.66 -5 -4 -9 18.90 2.80 5 4 9 25.17 1.66 5 4 10 32.93 2.13 5 4 10 32.71 2.05 5 4 11 3.67 0.85 5 4 11 3.77 0.79 5 4 12 257.53 11.36 5 4 12 263.59 11.39 5 4 12 251.76 11.22 5 4 13 22.78 1.73 5 4 13 23.42 1.73 5 4 13 23.55 1.65 5 4 14 185.99 8.51 5 4 14 187.95 8.54 5 4 14 187.13 8.37 5 4 15 46.98 2.60 5 4 15 45.78 2.72 5 4 15 45.68 2.74 5 4 16 81.93 4.07 5 4 16 82.85 4.22 5 4 16 82.08 4.24 5 4 17 194.23 8.43 5 4 17 188.45 8.56 5 4 17 181.30 8.58 5 4 18 141.48 6.38 5 4 18 134.75 6.55 5 4 18 138.72 6.53 5 4 19 20.44 1.63 5 4 19 19.00 1.59 5 4 20 1.96 0.75 5 4 20 2.20 0.79 5 4 20 1.45 0.68 5 4 21 56.04 3.01 5 4 21 55.22 2.96 5 4 22 12.36 1.24 5 4 22 11.36 1.21 5 4 23 6.74 0.96 5 4 23 4.31 0.88 5 4 24 1.50 0.69 5 4 25 21.51 1.62 5 4 26 18.02 1.45 5 4 27 8.44 1.01 5 4 28 5.60 0.87 5 4 29 20.71 1.48 5 4 30 4.55 0.77 5 4 31 -0.28 0.49 5 4 32 -0.15 0.46 5 4 33 5.83 0.68 5 4 34 7.30 0.71 5 5 -28 4.12 0.59 5 5 -27 2.80 0.49 5 5 -27 2.71 0.57 5 5 -26 7.86 0.78 5 5 -26 9.01 0.89 5 5 -25 4.67 0.63 5 5 -25 3.07 0.57 5 5 -25 3.56 0.67 5 5 -24 1.53 0.49 5 5 -24 1.02 0.50 5 5 -24 1.69 0.60 5 5 -23 0.25 0.46 5 5 -23 0.83 0.56 5 5 -22 4.88 0.74 5 5 -22 4.17 0.82 5 5 -21 2.60 0.64 5 5 -21 2.85 0.73 5 5 -20 26.59 1.75 5 5 -20 23.89 1.79 5 5 -19 0.48 0.54 5 5 -19 0.39 0.62 5 5 -18 38.81 2.27 5 5 -18 32.73 2.25 5 5 -17 26.54 1.78 5 5 -17 21.88 1.77 5 5 -16 26.28 1.81 5 5 -16 22.44 1.82 5 5 -15 27.00 1.80 5 5 -15 23.40 1.74 5 5 -15 22.12 1.81 5 5 -14 45.61 2.66 5 5 -14 45.95 2.64 5 5 -14 41.97 2.58 5 5 -14 43.48 2.71 5 5 -13 67.59 3.55 5 5 -13 66.64 3.53 5 5 -13 59.80 3.44 5 5 -13 66.85 3.64 5 5 -12 23.98 1.74 5 5 -12 24.59 1.78 5 5 -12 19.75 1.64 5 5 -12 22.11 1.79 5 5 -11 78.39 4.00 5 5 -11 76.09 3.99 5 5 -11 72.07 3.92 5 5 -11 76.23 4.06 5 5 -10 34.88 2.25 5 5 -10 34.48 2.29 5 5 -10 33.64 2.22 5 5 -10 34.75 2.32 5 5 -9 37.27 2.47 5 5 -9 40.34 2.46 5 5 -9 34.72 2.33 5 5 -9 37.49 2.46 5 5 -8 5.48 1.03 5 5 -8 4.81 1.01 5 5 -8 3.78 0.87 5 5 -8 3.96 0.98 5 5 -7 24.98 1.91 5 5 -7 22.80 1.79 5 5 -7 20.28 1.68 5 5 -7 23.11 1.81 5 5 -6 32.39 2.21 5 5 -6 27.29 2.03 5 5 -6 26.43 1.94 5 5 -6 27.98 2.02 5 5 -5 6.49 1.13 5 5 -5 5.03 1.04 5 5 -5 7.00 1.00 5 5 -5 4.79 0.96 5 5 -4 20.91 1.81 5 5 -4 19.87 1.66 5 5 -4 17.15 1.54 5 5 -4 20.97 1.68 5 5 -3 45.71 2.85 5 5 -3 42.67 2.68 5 5 -3 44.53 2.64 5 5 -2 38.75 2.67 5 5 -2 42.03 2.57 5 5 -2 40.25 2.48 5 5 0 53.04 3.29 5 5 0 55.97 3.12 5 5 0 53.88 3.05 5 5 1 82.57 4.35 5 5 1 75.69 4.11 5 5 1 81.13 4.10 5 5 2 79.74 4.14 5 5 2 67.15 3.83 5 5 2 75.81 3.86 5 5 3 87.76 4.70 5 5 3 95.39 4.73 5 5 4 61.20 3.56 5 5 4 61.58 3.33 5 5 5 29.38 2.10 5 5 5 23.88 1.76 5 5 6 18.68 1.55 5 5 6 19.99 1.80 5 5 6 18.95 1.62 5 5 7 13.42 1.27 5 5 7 14.52 1.54 5 5 7 14.23 1.36 5 5 8 37.90 2.27 5 5 8 34.91 2.45 5 5 8 39.54 2.39 5 5 9 6.12 0.89 5 5 9 6.28 1.10 5 5 9 7.18 0.98 5 5 9 8.02 1.00 5 5 10 8.01 1.05 5 5 10 4.87 0.92 5 5 10 5.55 0.88 5 5 11 24.13 1.82 5 5 11 25.78 1.87 5 5 11 25.31 1.73 5 5 12 13.33 1.33 5 5 12 15.33 1.41 5 5 12 13.21 1.22 5 5 13 65.52 3.69 5 5 13 68.77 3.74 5 5 13 74.11 3.60 5 5 14 63.88 3.50 5 5 14 62.88 3.53 5 5 14 66.27 3.35 5 5 15 20.79 1.50 5 5 15 20.78 1.68 5 5 15 21.85 1.73 5 5 16 22.12 1.55 5 5 16 21.64 1.70 5 5 16 21.34 1.71 5 5 17 8.29 0.96 5 5 17 7.76 1.06 5 5 17 8.56 1.12 5 5 18 34.37 2.04 5 5 18 34.72 2.23 5 5 18 33.48 2.26 5 5 19 9.15 1.11 5 5 19 10.04 1.16 5 5 20 49.76 2.88 5 5 20 47.71 2.78 5 5 21 3.28 0.77 5 5 21 3.55 0.85 5 5 22 5.32 0.87 5 5 22 4.92 0.91 5 5 23 26.71 1.88 5 5 23 25.54 1.76 5 5 24 5.75 0.88 5 5 25 22.84 1.54 5 5 25 17.77 1.47 5 5 26 25.80 1.74 5 5 27 8.25 0.95 5 5 28 7.44 0.89 5 5 29 2.69 0.63 5 5 30 1.44 0.54 5 5 31 0.76 0.48 5 5 32 28.30 1.62 5 5 33 9.03 0.77 5 6 -25 13.45 0.96 5 6 -25 13.99 1.01 5 6 -24 -0.21 0.38 5 6 -24 -0.15 0.40 5 6 -23 0.37 0.41 5 6 -23 0.25 0.41 5 6 -22 7.04 0.78 5 6 -22 5.57 0.72 5 6 -22 6.53 0.78 5 6 -21 1.81 0.52 5 6 -21 2.13 0.58 5 6 -21 1.73 0.56 5 6 -20 1.40 0.53 5 6 -20 1.94 0.58 5 6 -20 1.25 0.56 5 6 -19 21.57 1.51 5 6 -19 19.28 1.45 5 6 -19 22.11 1.53 5 6 -18 30.58 1.90 5 6 -18 25.76 1.78 5 6 -18 30.51 1.89 5 6 -17 15.94 1.31 5 6 -17 14.23 1.24 5 6 -17 15.12 1.30 5 6 -16 16.05 1.34 5 6 -16 15.68 1.32 5 6 -16 13.36 1.25 5 6 -15 14.08 1.28 5 6 -15 14.69 1.33 5 6 -15 13.10 1.23 5 6 -14 34.29 2.14 5 6 -14 32.04 2.09 5 6 -14 30.60 2.02 5 6 -13 0.63 0.57 5 6 -13 0.32 0.73 5 6 -13 0.57 0.62 5 6 -12 40.97 2.46 5 6 -12 41.67 2.49 5 6 -12 37.36 2.36 5 6 -11 8.26 1.04 5 6 -11 6.41 1.07 5 6 -11 8.56 1.03 5 6 -10 16.87 1.46 5 6 -10 17.21 1.56 5 6 -10 16.98 1.44 5 6 -9 8.15 1.03 5 6 -9 8.23 1.18 5 6 -9 7.73 1.01 5 6 -8 6.07 0.92 5 6 -8 4.33 0.95 5 6 -8 2.95 0.93 5 6 -8 4.45 0.87 5 6 -7 25.03 1.97 5 6 -7 25.30 1.93 5 6 -7 25.86 1.86 5 6 -6 63.80 3.49 5 6 -6 55.93 3.30 5 6 -6 58.62 3.24 5 6 -5 10.77 1.35 5 6 -5 11.26 1.32 5 6 -5 11.32 1.21 5 6 -4 4.50 1.05 5 6 -4 4.70 1.04 5 6 -4 3.19 0.84 5 6 -3 85.15 4.36 5 6 -3 75.67 4.10 5 6 -3 76.82 4.03 5 6 -2 7.31 1.25 5 6 -2 7.64 1.18 5 6 -2 9.79 1.12 5 6 -1 70.12 4.06 5 6 -1 77.33 3.96 5 6 0 19.81 1.83 5 6 0 19.11 1.66 5 6 0 23.56 1.67 5 6 1 43.36 2.74 5 6 1 38.82 2.49 5 6 1 40.79 2.44 5 6 2 40.38 2.60 5 6 2 33.53 2.31 5 6 2 40.11 2.33 5 6 3 43.85 2.89 5 6 3 47.85 2.66 5 6 6 50.62 3.08 5 6 6 50.36 2.80 5 6 7 10.78 1.27 5 6 7 13.13 1.46 5 6 7 13.85 1.21 5 6 8 43.22 2.64 5 6 8 38.36 2.68 5 6 8 47.86 2.53 5 6 9 11.88 1.27 5 6 9 9.55 1.27 5 6 9 11.99 1.11 5 6 10 10.47 1.20 5 6 10 8.51 0.97 5 6 11 19.14 1.57 5 6 11 17.08 1.54 5 6 11 18.46 1.41 5 6 12 47.18 2.87 5 6 12 48.83 2.93 5 6 12 52.10 2.70 5 6 13 39.82 2.48 5 6 13 40.28 2.51 5 6 14 21.46 1.63 5 6 14 19.12 1.63 5 6 15 4.95 0.93 5 6 15 6.00 1.00 5 6 16 23.34 1.73 5 6 16 22.68 1.77 5 6 17 3.23 0.82 5 6 17 4.24 0.92 5 6 18 5.13 0.89 5 6 18 5.11 0.93 5 6 19 7.74 0.98 5 6 19 8.43 1.05 5 6 20 12.42 1.18 5 6 20 14.05 1.31 5 6 21 21.38 1.58 5 6 21 18.65 1.45 5 6 22 4.29 0.73 5 6 22 3.87 0.80 5 6 23 20.67 1.52 5 6 23 19.62 1.41 5 6 24 28.54 1.75 5 6 25 23.70 1.51 5 6 27 1.81 0.55 5 6 28 8.44 0.84 5 6 29 0.11 0.42 5 6 30 3.91 0.57 -5 -7 21 1.59 0.39 5 7 -21 2.49 0.45 -5 -7 20 1.23 0.40 5 7 -20 2.20 0.47 -5 -7 19 3.48 0.54 5 7 -19 5.73 0.65 -5 -7 18 0.93 0.44 5 7 -18 1.89 0.51 5 7 -17 4.57 0.65 5 7 -17 3.60 0.62 5 7 -16 8.86 0.91 5 7 -16 9.37 0.94 5 7 -16 8.20 0.85 5 7 -15 42.57 2.23 5 7 -15 43.06 2.21 5 7 -15 39.25 2.11 5 7 -14 4.34 0.75 -5 -7 14 2.70 0.57 5 7 -14 4.33 0.79 5 7 -14 5.07 0.73 5 7 -13 0.38 0.50 -5 -7 13 0.43 0.42 5 7 -13 1.14 0.64 5 7 -13 0.85 0.52 5 7 -12 61.35 3.00 5 7 -12 60.50 2.98 5 7 -12 58.54 2.85 5 7 -11 4.06 0.78 5 7 -11 5.11 0.91 5 7 -11 6.03 0.81 5 7 -10 24.85 1.79 5 7 -10 25.41 1.84 5 7 -10 28.64 1.77 5 7 -9 30.91 2.01 5 7 -9 29.68 2.04 5 7 -9 30.72 1.92 5 7 -8 37.57 2.37 5 7 -8 39.43 2.29 5 7 -7 4.65 0.93 5 7 -7 5.84 1.02 5 7 -7 5.75 0.86 5 7 -6 50.45 2.91 5 7 -6 43.95 2.74 5 7 -6 51.67 2.73 5 7 -5 15.29 1.46 5 7 -5 16.57 1.28 5 7 -4 21.40 1.81 5 7 -4 21.63 1.74 5 7 -4 26.68 1.70 5 7 -3 12.95 1.32 5 7 -3 10.23 1.22 5 7 -3 10.88 1.12 5 7 -2 18.97 1.62 5 7 -2 23.89 1.85 5 7 -1 7.17 1.06 5 7 -1 6.82 1.14 5 7 0 70.21 3.77 5 7 0 76.08 4.01 5 7 1 70.82 3.69 5 7 1 69.89 3.88 5 7 2 72.70 3.97 5 7 3 54.64 3.21 5 7 4 71.35 3.90 5 7 5 30.59 2.16 5 7 6 34.18 2.32 5 7 7 36.48 2.57 5 7 7 48.20 2.63 5 7 8 62.39 3.81 5 7 8 85.51 3.94 5 7 9 30.13 2.22 5 7 9 38.41 2.27 5 7 10 3.87 0.89 5 7 11 29.01 1.95 5 7 11 29.79 2.00 5 7 12 34.33 2.17 5 7 12 34.16 2.20 5 7 13 114.23 5.41 5 7 13 112.66 5.48 5 7 14 77.00 3.90 5 7 14 76.58 3.96 5 7 15 2.42 0.70 5 7 15 3.27 0.79 5 7 16 4.21 0.77 5 7 16 4.30 0.83 5 7 17 7.25 0.87 5 7 17 7.61 0.99 5 7 18 27.75 1.77 5 7 18 28.68 1.86 5 7 19 14.27 1.15 5 7 19 13.61 1.21 5 7 20 3.34 0.66 5 7 20 4.67 0.76 5 7 21 10.99 1.05 5 7 22 13.40 1.11 5 7 23 0.96 0.49 -5 -8 15 1.89 0.40 5 8 -15 2.04 0.48 -5 -8 14 2.00 0.41 5 8 -14 2.33 0.55 -5 -8 13 12.26 0.95 5 8 -13 17.08 1.14 -5 -8 12 1.63 0.42 5 8 -12 2.54 0.60 -5 -8 11 2.17 0.48 5 8 -11 3.60 0.67 -5 -8 10 11.65 0.92 5 8 -10 13.37 1.11 -5 -8 9 2.58 0.52 5 8 -9 4.16 0.73 5 8 -9 2.93 0.61 -5 -8 8 2.64 0.52 5 8 -8 4.04 0.74 5 8 -8 3.26 0.64 -5 -8 7 41.04 2.28 5 8 -7 50.68 2.54 -5 -8 6 5.72 0.71 5 8 -6 7.40 0.90 5 8 -6 5.43 0.84 5 8 -5 40.44 2.18 5 8 -5 38.12 2.25 5 8 -4 8.37 0.99 5 8 -4 7.79 1.01 5 8 -3 59.70 3.03 5 8 -3 54.77 3.11 5 8 -2 54.76 2.82 5 8 -2 49.13 2.89 5 8 -1 37.45 2.14 5 8 -1 32.88 2.20 5 8 0 42.43 2.28 5 8 0 34.90 2.34 5 8 1 5.81 0.91 5 8 2 17.43 1.47 5 8 3 1.81 0.68 5 8 4 15.36 1.37 5 8 5 7.21 0.98 5 8 5 8.23 0.95 5 8 6 4.07 0.83 5 8 6 3.54 0.75 5 8 7 19.02 1.57 5 8 7 23.26 1.54 5 8 8 23.87 1.81 5 8 8 31.24 1.82 5 8 9 12.75 1.26 5 8 9 16.08 1.23 5 8 10 18.90 1.39 5 8 10 21.02 1.49 5 8 11 2.00 0.59 5 8 11 1.82 0.64 5 8 12 9.20 0.90 5 8 12 7.48 0.89 5 8 13 3.46 0.63 5 8 13 3.64 0.67 5 8 14 6.48 0.77 5 8 14 6.58 0.82 5 8 15 12.54 1.08 5 8 16 7.58 0.84 5 8 17 11.37 0.97 5 8 18 7.06 0.77 5 8 19 9.61 0.84 5 8 20 0.42 0.38 -5 -9 2 1.54 0.36 5 9 -1 2.23 0.48 -5 -9 1 1.84 0.39 5 9 0 7.08 0.71 5 9 1 3.78 0.57 5 9 2 26.94 1.54 5 9 3 17.09 1.14 5 9 4 23.86 1.41 5 9 5 3.23 0.54 5 9 6 7.17 0.69 5 9 6 6.54 0.73 5 9 7 1.15 0.39 5 9 7 0.64 0.41 5 9 8 6.21 0.68 5 9 9 8.39 0.76 5 9 10 0.66 0.39 6 -2 6 44.10 2.32 6 -2 7 5.82 0.72 6 -2 8 9.33 0.86 6 -2 9 2.38 0.54 6 -2 10 62.28 3.03 6 -2 11 8.42 0.81 6 -1 0 5.09 0.89 6 -1 1 2.42 0.74 6 -1 2 15.98 1.35 6 -1 3 16.18 1.38 6 -1 4 5.28 0.88 6 -1 5 27.95 1.86 6 -1 6 15.52 1.33 6 -1 7 9.24 1.07 6 -1 8 1.85 0.69 6 -1 9 19.28 1.49 6 -1 10 1.40 0.63 6 -1 11 4.26 0.78 6 -1 12 31.93 1.97 6 -1 13 9.95 1.02 6 -1 14 32.74 1.96 6 -1 15 1.46 0.55 6 -1 16 28.38 1.74 6 -1 17 2.22 0.56 6 -1 18 7.75 0.80 6 0 -20 10.86 0.90 6 0 -19 4.71 0.65 6 0 -18 2.61 0.58 6 0 -17 10.47 0.97 6 0 -16 3.52 0.68 6 0 -15 3.33 0.68 6 0 -14 7.63 0.94 6 0 -13 3.10 0.73 6 0 -12 42.98 2.50 6 0 -11 5.45 0.89 6 0 -10 5.46 0.89 6 0 -9 15.16 1.35 6 0 -9 16.23 1.12 6 0 -8 3.72 0.85 6 0 -8 4.54 0.67 6 0 -7 9.53 1.14 6 0 -7 10.52 0.92 6 0 -6 2.39 0.78 6 0 -6 4.12 0.67 6 0 -5 28.48 2.00 6 0 -5 30.56 1.74 6 0 -4 -0.15 0.71 6 0 -4 0.95 0.58 6 0 -3 5.55 0.97 6 0 -3 5.01 0.97 6 0 -3 6.18 0.79 6 0 -2 14.90 1.41 6 0 -2 13.08 1.34 6 0 -2 15.12 1.16 6 0 -1 10.42 1.19 6 0 -1 9.39 1.14 6 0 -1 10.23 0.97 6 0 0 9.30 1.21 6 0 0 10.07 1.17 6 0 0 12.79 1.06 6 0 1 2.45 0.85 6 0 1 3.70 0.88 6 0 1 3.64 0.73 6 0 2 71.18 3.88 6 0 2 75.66 3.54 6 0 2 71.31 3.86 6 0 3 8.47 1.16 6 0 3 11.36 1.01 6 0 4 54.71 3.27 6 0 4 62.34 2.96 6 0 4 58.89 3.30 6 0 5 9.26 0.92 6 0 5 10.15 1.27 6 0 6 25.72 1.54 6 0 6 30.06 1.98 6 0 7 4.80 0.97 6 0 7 6.67 0.79 6 0 8 29.81 2.12 6 0 8 32.93 1.80 6 0 9 2.28 0.80 6 0 10 1.76 0.73 6 0 11 2.84 0.77 6 0 12 1.32 0.66 6 0 13 2.60 0.74 6 0 14 14.65 1.28 6 0 15 60.69 3.21 6 0 16 11.21 1.10 6 0 17 7.09 0.89 6 0 18 1.10 0.55 6 1 -23 12.94 0.99 6 1 -22 6.98 0.76 6 1 -21 32.92 1.90 6 1 -20 5.27 0.75 6 1 -19 7.15 0.86 6 1 -18 4.95 0.78 6 1 -17 0.04 0.53 6 1 -16 20.01 1.53 6 1 -15 10.78 1.15 6 1 -14 18.35 1.50 6 1 -13 4.89 0.89 6 1 -12 13.76 1.35 6 1 -11 31.86 2.26 6 1 -11 36.70 1.94 6 1 -10 47.81 2.95 6 1 -10 52.72 2.63 6 1 -9 63.78 3.60 6 1 -9 67.17 3.25 6 1 -8 7.85 1.18 6 1 -8 9.18 0.94 6 1 -7 57.46 3.39 6 1 -7 62.62 3.08 6 1 -6 84.50 4.56 6 1 -6 91.07 4.23 6 1 -5 19.96 1.41 6 1 -5 18.42 1.67 6 1 -4 33.75 2.04 6 1 -4 36.69 2.42 6 1 -3 58.30 3.41 6 1 -3 58.65 3.02 6 1 -2 114.70 5.88 6 1 -2 113.09 5.48 6 1 -1 57.91 3.32 6 1 -1 50.70 3.32 6 1 -1 62.05 3.03 6 1 0 42.46 2.87 6 1 0 36.99 2.84 6 1 1 82.27 4.00 6 1 2 39.14 2.49 6 1 2 34.04 2.47 6 1 2 37.94 2.16 6 1 3 65.78 3.65 6 1 3 63.47 3.68 6 1 3 67.34 3.32 6 1 4 59.19 3.32 6 1 4 59.06 3.40 6 1 4 56.67 2.95 6 1 5 43.04 2.70 6 1 5 41.21 2.34 6 1 5 49.40 2.92 6 1 6 63.38 3.75 6 1 6 68.90 3.44 6 1 7 16.68 1.25 6 1 8 104.70 5.52 6 1 8 125.47 5.76 6 1 9 24.38 1.86 6 1 10 61.80 3.41 6 1 11 52.27 3.00 6 1 12 24.04 1.80 6 1 13 6.98 1.03 6 1 14 8.71 1.07 6 1 15 4.71 0.86 6 2 -24 3.57 0.56 6 2 -23 4.10 0.62 6 2 -22 0.89 0.47 6 2 -21 1.74 0.55 6 2 -20 1.97 0.58 6 2 -19 8.73 0.96 6 2 -18 21.60 1.56 6 2 -17 3.48 0.76 6 2 -16 27.49 1.88 6 2 -15 5.22 0.91 6 2 -14 30.78 2.07 6 2 -13 9.48 1.14 6 2 -12 8.59 0.94 6 2 -12 8.14 1.09 6 2 -11 16.01 1.25 6 2 -11 13.98 1.40 6 2 -10 46.51 2.47 6 2 -10 42.02 2.70 6 2 -9 1.36 0.82 6 2 -9 1.79 0.70 6 2 -8 89.87 4.26 6 2 -8 84.34 4.52 6 2 -7 100.01 4.69 6 2 -7 95.41 4.99 6 2 -6 43.78 2.53 6 2 -6 45.41 2.80 6 2 -5 34.23 2.08 6 2 -5 30.37 2.26 6 2 -4 115.60 5.37 6 2 -4 109.89 5.64 6 2 -3 76.61 3.87 6 2 -3 76.70 4.19 6 2 -2 79.03 3.93 6 2 -2 77.92 4.26 6 2 -1 49.98 2.67 6 2 -1 43.31 2.92 6 2 0 66.37 3.43 6 2 1 52.19 2.84 6 2 2 98.26 4.81 6 2 2 91.52 4.45 6 2 2 86.22 4.79 6 2 3 33.27 2.17 6 2 3 28.47 1.88 6 2 3 27.74 2.21 6 2 4 107.70 5.37 6 2 4 115.74 5.84 6 2 5 42.91 2.65 6 2 5 41.39 2.79 6 2 5 40.73 2.35 6 2 6 119.89 5.36 6 2 6 96.89 4.89 6 2 8 21.28 1.73 6 2 8 24.05 1.97 6 2 9 18.32 1.56 6 2 9 17.22 1.66 6 2 10 10.36 1.21 6 2 27 5.09 0.61 6 3 -21 10.08 0.94 6 3 -20 11.68 1.06 6 3 -20 13.85 1.12 6 3 -19 16.33 1.32 6 3 -19 19.76 1.39 6 3 -18 1.51 0.59 6 3 -18 1.71 0.63 6 3 -17 8.68 0.98 6 3 -17 8.88 1.00 6 3 -16 12.45 1.19 6 3 -16 15.88 1.33 6 3 -15 0.72 0.59 6 3 -15 1.74 0.67 6 3 -14 18.46 1.50 6 3 -14 19.83 1.57 6 3 -13 6.56 0.84 6 3 -13 4.71 0.88 6 3 -13 5.76 0.95 6 3 -12 22.94 1.55 6 3 -12 22.37 1.69 6 3 -12 22.55 1.74 6 3 -11 28.96 1.76 6 3 -11 22.33 1.78 6 3 -10 20.33 1.49 6 3 -10 19.15 1.59 6 3 -9 10.12 1.09 6 3 -9 8.82 1.10 6 3 -8 25.54 1.72 6 3 -8 22.02 1.77 6 3 -7 39.53 2.29 6 3 -7 35.70 2.39 6 3 -6 11.67 1.18 6 3 -6 9.57 1.23 6 3 -5 26.26 1.81 6 3 -5 25.95 1.94 6 3 -4 17.59 1.44 6 3 -4 15.04 1.48 6 3 -3 30.20 2.02 6 3 -3 33.40 2.23 6 3 -2 40.34 2.42 6 3 -2 40.20 2.60 6 3 -1 56.75 3.05 6 3 -1 53.62 3.21 6 3 1 39.38 2.37 6 3 2 19.96 1.74 6 3 2 18.92 1.50 6 3 3 3.99 1.02 6 3 3 4.82 0.88 6 3 4 19.35 1.74 6 3 4 18.69 1.47 6 3 5 54.72 3.04 6 3 5 44.70 2.66 6 3 6 66.99 3.74 6 3 7 44.72 2.83 6 3 8 72.30 3.94 6 3 9 7.15 0.88 6 3 10 15.25 1.23 6 3 11 78.89 3.87 6 3 12 22.43 1.53 6 3 28 24.90 1.43 6 4 -23 8.90 0.82 6 4 -22 16.20 1.18 6 4 -21 17.23 1.25 6 4 -20 39.94 2.25 6 4 -19 0.98 0.55 6 4 -18 0.72 0.56 6 4 -17 6.19 0.86 6 4 -16 27.28 1.84 6 4 -15 2.04 0.69 6 4 -14 18.31 1.34 6 4 -14 16.74 1.46 6 4 -13 7.12 0.88 6 4 -13 5.32 0.95 6 4 -12 28.84 1.82 6 4 -12 26.85 1.93 6 4 -11 32.71 2.02 6 4 -11 31.20 2.15 6 4 -10 20.26 1.51 6 4 -10 19.66 1.64 6 4 -9 15.71 1.36 6 4 -9 15.42 1.46 6 4 -8 3.18 0.84 6 4 -8 3.22 0.91 6 4 -7 0.52 0.73 6 4 -6 11.28 1.21 6 4 -5 16.49 1.45 6 4 -5 15.11 1.30 6 4 -4 15.17 1.39 6 4 -4 13.84 1.23 6 4 -3 18.13 1.52 6 4 -3 17.44 1.39 6 4 -2 27.04 1.91 6 4 -2 28.53 1.86 6 4 -1 49.82 2.81 6 4 -1 48.21 2.73 6 4 0 143.81 6.69 6 4 0 144.35 6.65 6 4 1 34.23 2.14 6 4 1 31.05 2.04 6 4 2 96.69 4.77 6 4 2 98.41 4.75 6 4 3 25.69 1.82 6 4 3 27.93 1.84 6 4 4 78.44 4.06 6 4 4 85.79 4.13 6 4 5 64.74 3.38 6 4 6 102.77 4.94 6 4 7 20.30 1.54 6 4 8 71.03 3.63 6 4 9 24.55 1.68 6 4 10 62.19 3.25 6 4 11 134.35 6.19 6 4 12 71.65 3.61 6 4 13 1.07 0.68 6 4 13 1.55 0.67 6 4 14 53.26 2.96 6 4 14 56.41 2.92 6 4 15 13.59 1.22 6 4 16 16.32 1.35 6 4 17 20.84 1.53 6 4 18 33.90 2.06 6 5 -22 7.83 0.76 6 5 -21 19.69 1.31 6 5 -20 57.00 2.89 6 5 -19 24.17 1.56 6 5 -18 20.16 1.42 6 5 -17 25.37 1.57 6 5 -17 29.53 1.78 6 5 -16 3.19 0.58 6 5 -16 3.77 0.73 6 5 -15 21.12 1.45 6 5 -15 27.62 1.73 6 5 -14 5.61 0.82 6 5 -14 4.01 0.67 6 5 -14 6.11 0.87 6 5 -13 17.78 1.30 6 5 -13 13.12 1.13 6 5 -13 16.00 1.34 6 5 -12 11.20 1.11 6 5 -12 9.85 0.99 6 5 -12 12.95 1.22 6 5 -11 10.92 1.13 6 5 -11 8.14 0.93 6 5 -11 10.05 1.13 6 5 -10 15.77 1.36 6 5 -10 14.60 1.23 6 5 -10 16.76 1.43 6 5 -9 6.43 0.95 6 5 -9 5.48 0.83 6 5 -9 6.23 0.98 6 5 -8 12.97 1.27 6 5 -8 12.71 1.17 6 5 -8 14.64 1.34 6 5 -7 78.71 3.83 6 5 -7 69.13 3.68 6 5 -6 24.20 1.76 6 5 -6 24.36 1.70 6 5 -5 54.41 3.08 6 5 -5 50.27 2.89 6 5 -5 49.99 2.81 6 5 -4 31.87 2.17 6 5 -4 27.28 1.94 6 5 -4 27.39 1.86 6 5 -3 2.76 0.93 6 5 -3 3.42 0.88 6 5 -3 3.46 0.80 6 5 -2 73.94 3.87 6 5 -2 67.94 3.59 6 5 -2 65.39 3.53 6 5 -1 30.81 2.16 6 5 -1 28.57 1.94 6 5 -1 25.76 1.85 6 5 0 70.69 3.76 6 5 0 64.09 3.49 6 5 0 65.87 3.51 6 5 1 38.69 2.51 6 5 1 34.33 2.25 6 5 1 37.39 2.27 6 5 2 54.89 3.17 6 5 2 50.54 2.91 6 5 2 53.77 2.94 6 5 3 57.96 3.21 6 5 3 56.42 2.96 6 5 4 30.42 2.25 6 5 4 34.81 2.13 6 5 5 94.12 4.84 6 5 5 94.07 4.60 6 5 6 94.12 5.04 6 5 6 105.37 4.89 6 5 7 61.70 3.56 6 5 7 67.34 3.42 6 5 8 17.22 1.37 6 5 8 16.97 1.39 6 5 9 9.87 1.09 6 5 9 9.17 1.04 6 5 10 99.08 4.89 6 5 10 102.80 4.84 6 5 11 62.67 3.36 6 5 11 64.96 3.31 6 5 12 19.73 1.55 6 5 12 21.40 1.51 6 5 13 111.97 5.55 6 5 13 122.45 5.49 6 5 14 12.46 1.25 6 5 14 17.30 1.27 6 5 15 18.22 1.46 6 5 15 19.24 1.39 6 5 16 16.42 1.35 6 5 17 3.56 0.76 6 5 18 15.82 1.29 6 5 19 30.60 1.91 6 5 20 19.88 1.43 6 6 -19 10.31 0.79 6 6 -19 10.30 0.85 6 6 -18 18.32 1.13 6 6 -18 16.84 1.17 6 6 -17 10.31 0.85 6 6 -17 11.82 0.95 6 6 -16 17.67 1.21 6 6 -16 20.61 1.33 6 6 -15 17.69 1.18 6 6 -15 14.87 1.10 6 6 -15 16.17 1.21 6 6 -14 1.62 0.58 6 6 -14 2.36 0.54 6 6 -14 1.97 0.57 6 6 -13 7.05 0.85 6 6 -13 7.05 0.78 6 6 -13 7.25 0.85 6 6 -12 22.91 1.55 6 6 -12 22.64 1.48 6 6 -12 23.14 1.56 6 6 -11 29.00 1.84 6 6 -11 29.79 1.78 6 6 -10 18.72 1.42 6 6 -10 18.88 1.35 6 6 -9 0.34 0.63 6 6 -9 0.67 0.55 6 6 -8 6.69 0.98 6 6 -8 6.03 0.89 6 6 -8 5.95 0.82 6 6 -7 4.72 0.90 6 6 -7 5.19 0.91 6 6 -7 5.29 0.79 6 6 -6 2.33 0.74 6 6 -6 1.42 0.70 6 6 -6 1.85 0.62 6 6 -5 4.02 0.87 6 6 -5 2.30 0.78 6 6 -5 2.99 0.69 6 6 -4 10.85 1.23 6 6 -4 8.45 1.08 6 6 -4 10.92 1.06 6 6 -3 4.69 0.90 6 6 -3 5.04 0.93 6 6 -3 4.91 0.82 6 6 -2 14.66 1.45 6 6 -2 15.01 1.34 6 6 -2 14.97 1.27 6 6 -1 3.22 0.87 6 6 -1 2.70 0.80 6 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1.41 7 3 -4 19.54 1.30 7 3 -3 12.16 1.00 7 3 -3 12.29 1.09 7 3 -2 10.00 0.92 7 3 -2 11.54 1.06 7 3 -1 10.17 0.94 7 3 -1 12.23 1.08 7 3 0 4.92 0.77 7 3 0 4.51 0.71 7 3 1 14.82 1.15 7 3 1 18.39 1.34 7 3 2 26.42 1.60 7 3 2 31.21 1.85 7 3 3 45.86 2.34 7 3 4 12.78 1.00 7 4 -12 5.92 0.61 7 4 -11 5.20 0.62 7 4 -10 11.37 0.90 7 4 -9 23.22 1.39 7 4 -8 7.87 0.77 7 4 -7 10.81 0.90 7 4 -6 1.71 0.55 7 4 -5 11.12 0.96 7 4 -4 0.51 0.55 7 4 -3 0.59 0.55 7 4 -2 7.61 0.83 7 4 -1 10.91 0.97 7 4 0 2.00 0.64 7 4 1 44.79 2.34 7 4 2 12.59 1.03 7 4 3 10.86 0.95 7 5 -11 11.47 0.85 7 5 -10 5.52 0.65 7 5 -9 8.54 0.77 7 5 -8 3.61 0.60 7 5 -7 2.09 0.56 7 5 -6 14.30 1.06 7 5 -5 4.70 0.66 7 5 -4 20.85 1.33 7 5 -3 22.58 1.41 7 5 -3 22.72 1.35 7 5 -2 4.66 0.68 7 5 -2 6.14 0.66 7 5 -1 9.46 0.90 7 5 -1 9.96 0.84 7 5 0 15.83 1.13 7 5 0 15.06 1.06 7 5 1 31.93 1.83 7 5 1 35.54 1.85 7 5 2 54.41 2.84 7 5 2 64.19 2.90 7 5 3 38.05 2.02 7 5 4 140.92 6.22 7 5 5 40.27 2.11 7 5 6 34.08 1.85 7 5 7 19.54 1.26 7 5 8 42.56 2.19 7 5 9 101.79 4.60 7 6 -8 7.81 0.68 7 6 -7 32.96 1.69 7 6 -7 31.45 1.65 7 6 -6 15.00 1.01 7 6 -6 15.12 0.97 7 6 -5 15.54 1.06 7 6 -5 17.58 1.06 7 6 -4 5.60 0.63 7 6 -4 5.82 0.60 7 6 -3 3.78 0.56 7 6 -3 3.44 0.51 7 6 -2 11.31 0.89 7 6 -2 12.34 0.89 7 6 -1 5.73 0.66 7 6 -1 7.56 0.69 7 6 0 8.87 0.80 7 6 0 11.28 0.85 7 6 1 33.93 1.80 7 6 2 25.85 1.47 7 6 3 46.34 2.31 7 6 4 38.84 2.00 7 6 5 28.50 1.58 7 6 6 81.94 3.76 7 6 7 46.04 2.29 7 6 8 5.47 0.62 7 6 9 5.24 0.60 0 0 0 0.00 0.00 TITL SK-0284_auto_kp260423 in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 6.264200 8.050542 36.896734 86.5194 86.8635 67.2663 ZERR 96.00 0.000281 0.000198 0.000600 0.0017 0.0024 0.0032 LATT 1 SFAC C H O UNIT 96.00 96.00 96.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 98192 _shelx_fab_file ; -5 -9 1 0.3473 -0.5113 -5 -9 2 -0.0327 0.6365 -5 -8 6 -0.0443 0.2347 -5 -8 7 -0.1687 -0.2531 -5 -8 8 0.3361 0.0864 -5 -8 9 -0.3243 0.1633 -5 -8 10 0.1318 -0.3269 -5 -8 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-0.2355 0.2208 6 5 -10 0.0004 -0.4140 6 5 -9 0.3325 0.3655 6 5 -8 -0.5439 -0.0722 6 5 -7 0.4851 -0.2966 6 5 -6 -0.1888 0.5148 6 5 -5 -0.1509 -0.4623 6 5 -4 0.3211 0.2123 6 5 -3 -0.2495 0.0279 6 5 -2 0.0541 -0.0805 6 5 -1 0.0566 -0.0633 6 5 0 0.0443 0.2403 6 5 1 -0.2964 -0.2512 6 5 2 0.4998 0.0272 6 5 3 -0.4763 0.3105 6 5 4 0.2137 -0.5451 6 5 5 0.1258 0.5344 6 5 6 -0.3357 -0.3179 6 5 7 0.3266 0.0753 6 5 8 -0.1845 0.0250 6 5 9 0.0857 0.0423 6 5 10 -0.1442 -0.1520 6 5 11 0.3208 0.1448 6 5 12 -0.4650 0.0363 6 5 13 0.4447 -0.3039 6 5 14 -0.2507 0.5053 6 5 15 -0.0094 -0.5466 6 5 16 0.2107 0.4534 6 5 17 -0.3101 -0.3244 6 5 18 0.3595 0.2296 6 5 19 -0.4291 -0.1501 6 5 20 0.5204 0.0114 6 6 -19 0.0384 -0.2826 6 6 -18 0.1288 0.2980 6 6 -17 -0.2894 -0.1985 6 6 -16 0.3612 0.0081 6 6 -15 -0.2969 0.1928 6 6 -14 0.1191 -0.3058 6 6 -13 0.0818 0.2727 6 6 -12 -0.1946 -0.1176 6 6 -11 0.1565 -0.0583 6 6 -10 0.0007 0.1343 6 6 -9 -0.1619 -0.0494 6 6 -8 0.1986 -0.1513 6 6 -7 -0.0544 0.3370 6 6 -6 -0.2120 -0.3725 6 6 -5 0.4590 0.2049 6 6 -4 -0.5490 0.1018 6 6 -3 0.4301 -0.4087 6 6 -2 -0.1572 0.5871 6 6 -1 -0.1545 -0.5857 6 6 0 0.4031 0.4366 6 6 1 -0.5433 -0.2088 6 6 2 0.5758 -0.0423 6 6 3 -0.5080 0.2871 6 6 4 0.3345 -0.4953 6 6 5 -0.0590 0.6091 6 6 6 -0.2642 -0.5582 6 6 7 0.5200 0.3160 6 6 8 -0.5813 0.0494 6 6 9 0.3928 -0.3814 6 6 10 -0.0270 0.5116 6 6 11 -0.3363 -0.3619 6 6 12 0.5054 0.0006 6 6 13 -0.3851 0.3883 6 6 14 0.0301 -0.6062 6 6 15 0.3905 0.5449 6 6 16 -0.6869 -0.2338 6 6 17 0.7414 -0.1915 6 6 18 -0.5482 0.5663 6 6 19 0.1934 -0.7693 6 6 20 0.1983 0.7574 6 6 21 -0.5137 -0.5594 6 7 -15 -0.1135 0.0392 6 7 -14 0.0567 -0.0678 6 7 -13 -0.0108 0.0622 6 7 -12 -0.0168 -0.0447 6 7 -11 0.0371 0.0244 6 7 -10 -0.0542 0.0093 6 7 -9 0.0482 -0.0658 6 7 -8 0.0119 0.1235 6 7 -7 -0.1288 -0.1272 6 7 -6 0.2487 0.0252 6 7 -5 -0.2766 0.1761 6 7 -4 0.1389 -0.3873 6 7 -3 0.1505 0.4734 6 7 -2 -0.4721 -0.3364 6 7 -1 0.6559 -0.0102 6 7 0 -0.5790 0.4307 6 7 1 0.2425 -0.7343 6 7 2 0.2239 0.7774 6 7 3 -0.6310 -0.5365 6 7 4 0.8247 0.1100 6 7 5 -0.7495 0.3403 6 7 6 0.4524 -0.6661 6 7 7 -0.0430 0.7807 6 7 8 -0.3536 -0.6687 6 7 9 0.6282 0.3723 6 7 10 -0.7032 0.0218 6 7 11 0.5502 -0.3935 6 7 12 -0.2107 0.6141 6 7 13 -0.1968 -0.5922 6 7 14 0.5087 0.3255 6 7 15 -0.5861 0.0782 6 7 16 0.3907 -0.4380 6 7 17 -0.0146 0.5874 6 7 18 -0.3612 -0.4630 6 7 19 0.5622 0.1390 6 7 20 -0.5129 0.2174 6 8 -7 -0.1971 -0.1188 6 8 -6 0.2149 -0.0029 6 8 -5 -0.1715 0.0926 6 8 -4 0.1141 -0.1393 6 8 -3 -0.0640 0.1705 6 8 -2 0.0013 -0.2065 6 8 -1 0.1038 0.2252 6 8 0 -0.2418 -0.1735 6 8 1 0.3476 0.0194 6 8 2 -0.3385 0.2024 6 8 3 0.1779 -0.3939 6 8 4 0.0847 0.4510 6 8 5 -0.3359 -0.3322 6 8 6 0.4642 0.0872 6 8 7 -0.4247 0.1759 6 8 8 0.2540 -0.3557 6 8 9 -0.0349 0.4073 6 8 10 -0.1569 -0.3458 6 8 11 0.2819 0.2145 6 8 12 -0.3305 -0.0533 6 8 13 0.3019 -0.1082 7 1 -9 0.3194 -0.1758 7 1 -8 -0.1934 0.3800 7 1 -7 -0.0607 -0.4912 7 1 -6 0.3707 0.4279 7 1 -5 -0.6126 -0.1686 7 1 -4 0.6635 -0.2177 7 1 -3 -0.4667 0.5882 7 1 -2 0.0709 -0.7866 7 1 -1 0.3822 0.7171 7 1 0 -0.7169 -0.3933 7 1 2 -0.6082 0.4768 7 1 3 0.2229 -0.6885 7 1 4 0.1890 0.6310 7 2 -12 0.2136 -0.0922 7 2 -11 -0.1065 0.1673 7 2 -10 -0.0006 -0.1641 7 2 -9 0.0682 0.1141 7 2 -8 -0.0920 -0.0558 7 2 -7 0.0913 0.0104 7 2 -6 -0.0851 0.0255 7 2 -5 0.0744 -0.0674 7 2 -4 -0.0393 0.1206 7 2 -3 -0.0435 -0.1627 7 2 -2 0.1714 0.1466 7 2 -1 -0.2958 -0.0285 7 2 0 0.3307 -0.1882 7 2 1 -0.2004 0.4258 7 2 2 -0.0971 -0.5520 7 2 3 0.4559 0.4522 7 2 4 -0.6977 -0.1151 7 2 5 0.6706 -0.3305 7 3 -12 -0.0692 -0.1214 7 3 -11 0.1322 0.0651 7 3 -10 -0.1563 0.0197 7 3 -9 0.1327 -0.1090 7 3 -8 -0.0634 0.1806 7 3 -7 -0.0439 -0.2128 7 3 -6 0.1701 0.1810 7 3 -5 -0.2735 -0.0683 7 3 -4 0.2936 -0.1089 7 3 -3 -0.1851 0.2816 7 3 -2 -0.0331 -0.3476 7 3 -1 0.2563 0.2362 7 3 0 -0.3392 0.0209 7 3 1 0.1946 -0.2751 7 3 2 0.1196 0.3399 7 3 3 -0.4046 -0.1234 7 3 4 0.4377 -0.2789 7 4 -12 0.2274 -0.1589 7 4 -11 -0.0595 0.2342 7 4 -10 -0.0890 -0.1732 7 4 -9 0.1297 0.0473 7 4 -8 -0.0655 0.0343 7 4 -7 -0.0156 -0.0127 7 4 -6 0.0175 -0.0730 7 4 -5 0.0800 0.1196 7 4 -4 -0.1995 -0.0510 7 4 -3 0.2293 -0.1109 7 4 -2 -0.1209 0.2577 7 4 -1 -0.0648 -0.2835 7 4 0 0.2049 0.1755 7 4 1 -0.2194 -0.0261 7 4 2 0.1407 -0.0493 7 4 3 -0.0833 0.0189 7 5 -11 -0.0311 0.1162 7 5 -10 -0.0757 -0.1372 7 5 -9 0.1842 0.0474 7 5 -8 -0.1874 0.1285 7 5 -7 0.0291 -0.2742 7 5 -6 0.2289 0.2525 7 5 -5 -0.4214 -0.0141 7 5 -4 0.3834 -0.3396 7 5 -3 -0.0741 0.5987 7 5 -2 -0.3705 -0.5761 7 5 -1 0.7079 0.2398 7 5 0 -0.7412 0.2523 7 5 1 0.4466 -0.6469 7 5 2 0.0134 0.7547 7 5 3 -0.4017 -0.5622 7 5 4 0.5586 0.2191 7 5 5 -0.4852 0.0796 7 5 6 0.3064 -0.2239 7 5 7 -0.1571 0.2348 7 5 8 0.0865 -0.2069 7 5 9 -0.0516 0.2097 7 6 -8 -0.0257 -0.1736 7 6 -7 0.1158 0.1095 7 6 -6 -0.1360 0.0061 7 6 -5 0.0586 -0.1059 7 6 -4 0.0822 0.1126 7 6 -3 -0.1950 0.0056 7 6 -2 0.1830 -0.1982 7 6 -1 -0.0131 0.3476 7 6 0 -0.2456 -0.3385 7 6 1 0.4513 0.1387 7 6 2 -0.4745 0.1663 7 6 3 0.2860 -0.4173 7 6 4 0.0173 0.4794 7 6 5 -0.2695 -0.3297 7 6 6 0.3414 0.0720 7 6 7 -0.2217 0.1322 7 6 8 0.0179 -0.1696 7 6 9 0.1205 0.0444 0 0 0 0.0 0.0 ; _shelx_fab_checksum 25581 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.479 _oxdiff_exptl_absorpt_empirical_full_min 0.435 loop_ _space_group_symop_operation_xyz 'x, y, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.6295(11) 1.2192(8) 0.04435(16) 0.0239(13) Uani 1 1 d . . . . . O002 O 0.5207(11) 0.0320(9) 0.78102(17) 0.0279(14) Uani 1 1 d . . . . . O003 O 0.8773(11) -0.2211(7) 0.95572(15) 0.0229(13) Uani 1 1 d . . . . . O004 O -0.1001(13) 1.8396(8) 0.13505(16) 0.0339(17) Uani 1 1 d . . . . . O005 O 0.2065(12) 0.5089(9) 0.28086(18) 0.0290(14) Uani 1 1 d . . . . . O006 O 0.8277(13) -0.8416(8) 0.86530(16) 0.0304(15) Uani 1 1 d . . . . . O007 O -0.1106(12) 0.4902(8) 0.72077(18) 0.0296(14) Uani 1 1 d . . . . . O008 O 0.4138(12) 0.9655(10) 0.21861(18) 0.0327(15) Uani 1 1 d . . . . . C009 C 0.4259(16) -0.0615(11) 0.7956(2) 0.0214(17) Uani 1 1 d . . . . . C00A C 0.9168(14) -0.6170(10) 0.9125(2) 0.0190(17) Uani 1 1 d . . . . . H00A H 1.003348 -0.740505 0.913900 0.023 Uiso 1 1 calc R U . . . C00B C 0.6298(14) -0.3628(11) 0.8803(2) 0.0161(16) Uani 1 1 d . . . . . C00C C 0.4397(15) -0.0931(11) 0.8365(2) 0.0208(18) Uani 1 1 d . . . . . H00B H 0.306099 -0.000654 0.847623 0.025 Uiso 1 1 calc R U . . . H00C H 0.576401 -0.077315 0.844022 0.025 Uiso 1 1 calc R U . . . C00D C 0.7216(17) -0.6758(11) 0.8609(2) 0.0226(18) Uani 1 1 d . . . . . C00E C 0.2917(15) -0.1421(11) 0.7751(2) 0.0210(17) Uani 1 1 d . . . . . C00F C 0.2148(15) 0.6433(10) 0.2934(2) 0.0204(17) Uani 1 1 d . . . . . C00G C 0.9516(15) -0.5114(11) 0.9375(2) 0.0185(17) Uani 1 1 d . . . . . C00H C -0.1366(17) 1.3301(11) 0.2096(2) 0.0221(18) Uani 1 1 d . . . . . C00I C 0.2376(16) 1.0628(12) 0.2041(2) 0.0249(18) Uani 1 1 d . . . . . C00J C 0.3657(17) -0.1458(11) 0.7345(2) 0.0231(18) Uani 1 1 d . . . . . H00D H 0.533061 -0.204606 0.732494 0.028 Uiso 1 1 calc R U . . . H00E H 0.301635 -0.219118 0.722507 0.028 Uiso 1 1 calc R U . . . C00K C 0.0485(19) 1.1495(11) 0.2658(2) 0.028(2) Uani 1 1 d . . . . . H00I H 0.154249 1.209987 0.267828 0.034 Uiso 1 1 calc R U . . . H00J H -0.097260 1.221075 0.277734 0.034 Uiso 1 1 calc R U . . . C00L C 1.1279(15) -0.5836(10) 0.9670(2) 0.0176(16) Uani 1 1 d . . . . . H00L H 1.082347 -0.494387 0.985865 0.021 Uiso 1 1 calc R U . . . C00M C 0.8280(16) -0.3222(11) 0.9322(2) 0.0202(17) Uani 1 1 d . . . . . C00N C 0.1138(17) 0.1800(12) 0.7274(2) 0.0227(18) Uani 1 1 d . . . . . C00O C 0.6690(16) -0.2524(12) 0.9054(2) 0.0202(17) Uani 1 1 d . . . . . H00O H 0.584592 -0.128641 0.903742 0.024 Uiso 1 1 calc R U . . . C00P C 0.2167(14) -0.2611(10) 0.8701(2) 0.0181(16) Uani 1 1 d . . . . . H00F H 0.207617 -0.377476 0.873367 0.027 Uiso 1 1 calc R U . . . H00G H 0.093715 -0.183884 0.855106 0.027 Uiso 1 1 calc R U . . . H00H H 0.202317 -0.209474 0.893348 0.027 Uiso 1 1 calc R U . . . C00Q C 0.3987(16) 1.5107(11) 0.0628(2) 0.0204(17) Uani 1 1 d . . . . . C00R C 0.2390(16) 1.6176(11) 0.0873(2) 0.0197(17) Uani 1 1 d . . . . . H00R H 0.199726 1.741551 0.085189 0.024 Uiso 1 1 calc R U . . . C00S C 0.4595(16) 1.3234(11) 0.0677(2) 0.0198(17) Uani 1 1 d . . . . . C00T C 0.1312(17) 1.5473(11) 0.1156(2) 0.0234(18) Uani 1 1 d . . . . . C00U C 0.4450(17) 0.7596(12) 0.3304(2) 0.0247(19) Uani 1 1 d . . . . . C00V C 0.5210(16) 1.5839(12) 0.0336(2) 0.0233(19) Uani 1 1 d . . . . . H00V H 0.575435 1.495219 0.014704 0.028 Uiso 1 1 calc R U . . . C00W C 0.7558(16) -0.5466(10) 0.8848(2) 0.0201(17) Uani 1 1 d . . . . . C00X C 0.2405(17) 1.0948(11) 0.1634(2) 0.0245(19) Uani 1 1 d . . . . . H00K H 0.205070 1.002075 0.152541 0.029 Uiso 1 1 calc R U . . . H00M H 0.396491 1.079970 0.155300 0.029 Uiso 1 1 calc R U . . . C00Y C 0.0709(15) 1.2817(10) 0.1486(2) 0.0169(17) Uani 1 1 d . . . . . C00Z C 0.793(2) 0.7386(14) 0.4311(3) 0.035(2) Uani 1 1 d . . . . . C010 C 0.5489(18) 0.7561(12) 0.3662(2) 0.027(2) Uani 1 1 d . . . . . C011 C 0.3546(18) 1.2526(12) 0.0950(2) 0.0240(19) Uani 1 1 d . . . . . H011 H 0.395474 1.128496 0.097132 0.029 Uiso 1 1 calc R U . . . C012 C 0.5088(14) -0.4116(10) 0.8194(2) 0.0167(16) Uani 1 1 d . . . . . H012 H 0.656748 -0.416065 0.808394 0.020 Uiso 1 1 calc R U . . . C013 C 0.0077(16) 1.1403(11) 0.2253(2) 0.0207(18) Uani 1 1 d . . . . . C014 C 0.2936(18) 0.0355(12) 0.7145(2) 0.0258(19) Uani 1 1 d . . . . . C015 C 0.5443(16) -0.6001(10) 0.8326(2) 0.0194(17) Uani 1 1 d . . . . . H01A H 0.397965 -0.601216 0.842432 0.023 Uiso 1 1 calc R U . . . H01B H 0.590749 -0.677643 0.812072 0.023 Uiso 1 1 calc R U . . . C016 C 0.1273(17) 0.8179(12) 0.2733(2) 0.0231(18) Uani 1 1 d . . . . . C017 C 0.3253(14) -0.3286(11) 0.7903(2) 0.0184(16) Uani 1 1 d . . . . . C018 C 0.0174(16) 0.8227(12) 0.2373(2) 0.0235(18) Uani 1 1 d . . . . . H01R H 0.138182 0.759424 0.219739 0.028 Uiso 1 1 calc R U . . . H01S H -0.086118 0.758809 0.240609 0.028 Uiso 1 1 calc R U . . . C019 C 0.420(2) 0.0537(12) 0.6790(3) 0.037(3) Uani 1 1 d . . . . . H019 H 0.347035 0.022481 0.659131 0.044 Uiso 1 1 calc R U . . . C01A C 1.3666(16) -0.6011(11) 0.9521(2) 0.0223(17) Uani 1 1 d . . . . . H01C H 1.413042 -0.683133 0.932659 0.033 Uiso 1 1 calc R U . . . H01D H 1.476059 -0.646149 0.971082 0.033 Uiso 1 1 calc R U . . . H01E H 1.361241 -0.485131 0.943156 0.033 Uiso 1 1 calc R U . . . O01B O 0.676(2) 1.1556(12) 0.3519(3) 0.067(3) Uani 1 1 d . . . . . C01C C -0.0104(15) 0.1762(12) 0.7636(2) 0.0210(17) Uani 1 1 d . . . . . H01F H -0.175264 0.242726 0.760854 0.025 Uiso 1 1 calc R U . . . H01G H 0.041485 0.236543 0.781062 0.025 Uiso 1 1 calc R U . . . C01D C -0.1322(17) 1.2602(12) 0.1304(2) 0.0250(19) Uani 1 1 d . . . . . H01T H -0.074390 1.185690 0.109895 0.038 Uiso 1 1 calc R U . . . H01U H -0.240505 1.376623 0.122451 0.038 Uiso 1 1 calc R U . . . H01V H -0.208267 1.205018 0.147569 0.038 Uiso 1 1 calc R U . . . C01E C -0.1170(15) 1.0113(11) 0.2222(2) 0.0201(17) Uani 1 1 d . . . . . H01W H -0.266088 1.059661 0.234977 0.024 Uiso 1 1 calc R U . . . H01X H -0.145161 1.005313 0.196768 0.024 Uiso 1 1 calc R U . . . C01F C -0.0195(16) 1.4079(10) 0.1811(2) 0.0198(17) Uani 1 1 d . . . . . H01Y H 0.117112 1.412190 0.192134 0.024 Uiso 1 1 calc R U . . . C01G C 0.4494(15) -0.2811(10) 0.8519(2) 0.0188(17) Uani 1 1 d . . . . . C01H C 0.0400(16) 0.3566(12) 0.7080(2) 0.0232(18) Uani 1 1 d . . . . . C01I C 0.1567(18) 0.3709(13) 0.6717(2) 0.029(2) Uani 1 1 d . . . . . H01H H 0.142878 0.494326 0.666873 0.035 Uiso 1 1 calc R U . . . H01I H 0.079580 0.339630 0.652739 0.035 Uiso 1 1 calc R U . . . C01J C -0.3574(19) 1.4207(13) 0.2212(2) 0.031(2) Uani 1 1 d . . . . . C01K C 0.3618(17) 1.7635(11) 0.0154(2) 0.0261(19) Uani 1 1 d . . . . . H01Z H 0.230572 1.748886 0.005937 0.039 Uiso 1 1 calc R U . . . H H 0.446100 1.798040 -0.004132 0.039 Uiso 1 1 calc R U . . . HA H 0.309645 1.855334 0.032933 0.039 Uiso 1 1 calc R U . . . C01L C 0.7357(16) 1.5992(11) 0.0486(2) 0.0240(18) Uani 1 1 d . . . . . H01 H 0.691510 1.672012 0.069470 0.036 Uiso 1 1 calc R U . . . HB H 0.805125 1.654004 0.030222 0.036 Uiso 1 1 calc R U . . . HC H 0.845058 1.481164 0.055344 0.036 Uiso 1 1 calc R U . . . C01M C -0.1637(16) 1.5993(11) 0.1678(2) 0.0217(18) Uani 1 1 d . . . . . H1 H -0.305537 1.601197 0.158142 0.026 Uiso 1 1 calc R U . . . HD H -0.206151 1.676741 0.188377 0.026 Uiso 1 1 calc R U . . . C01N C 0.5366(18) 0.2566(13) 0.6353(3) 0.033(2) Uani 1 1 d . . . . . C01O C 0.0303(16) -0.0139(11) 0.7783(2) 0.0212(18) Uani 1 1 d . . . . . H01J H -0.060627 -0.061964 0.764970 0.025 Uiso 1 1 calc R U . . . H01K H -0.021680 -0.009724 0.803626 0.025 Uiso 1 1 calc R U . . . C01P C -0.0435(15) 1.6740(10) 0.1395(2) 0.0209(17) Uani 1 1 d . . . . . C01Q C 0.1879(16) 1.3632(11) 0.1196(2) 0.0203(18) Uani 1 1 d . . . . . C01R C 0.3140(19) 0.6322(11) 0.3302(2) 0.028(2) Uani 1 1 d . . . . . H2 H 0.418992 0.509381 0.335873 0.034 Uiso 1 1 calc R U . . . HE H 0.190033 0.665953 0.348657 0.034 Uiso 1 1 calc R U . . . C01S C 0.7083(18) 1.0318(12) 0.0496(2) 0.028(2) Uani 1 1 d . . . . . H3 H 0.821438 0.975356 0.030902 0.042 Uiso 1 1 calc R U . . . HF H 0.580273 0.994780 0.048661 0.042 Uiso 1 1 calc R U . . . HG H 0.777114 0.996590 0.072915 0.042 Uiso 1 1 calc R U . . . C01T C 1.1296(19) -0.7596(13) 0.9849(2) 0.029(2) Uani 1 1 d . . . . . H01L H 0.979079 -0.740607 0.995508 0.044 Uiso 1 1 calc R U . . . H01M H 1.242216 -0.800132 1.003442 0.044 Uiso 1 1 calc R U . . . H01N H 1.168524 -0.849058 0.966915 0.044 Uiso 1 1 calc R U . . . C01U C 0.619(2) 0.433(2) 0.5860(4) 0.062(4) Uani 1 1 d . . . . . C01V C 0.4121(17) 0.2461(12) 0.6711(2) 0.0262(19) Uani 1 1 d . . . . . C01W C 0.917(2) 0.7263(13) 0.4655(2) 0.033(2) Uani 1 1 d . . . . . H4 H 0.983946 0.598165 0.473012 0.039 Uiso 1 1 calc R U . . . C01X C 0.749(2) 0.8209(16) 0.4959(3) 0.042(3) Uani 1 1 d . . . . . H5 H 0.827759 0.792937 0.518447 0.063 Uiso 1 1 calc R U . . . HH H 0.622709 0.780896 0.497707 0.063 Uiso 1 1 calc R U . . . HI H 0.690129 0.948816 0.490877 0.063 Uiso 1 1 calc R U . . . C01Y C 0.2011(19) -0.4199(12) 0.7785(3) 0.030(2) Uani 1 1 d . . . . . C01Z C 0.532(2) 0.302(2) 0.7001(3) 0.049(3) Uani 1 1 d . . . . . H01O H 0.694135 0.226659 0.699560 0.073 Uiso 1 1 calc R U . . . H01P H 0.465035 0.288588 0.723620 0.073 Uiso 1 1 calc R U . . . H01Q H 0.512730 0.425402 0.695542 0.073 Uiso 1 1 calc R U . . . C020 C 0.486(2) 0.4184(17) 0.6165(4) 0.055(4) Uani 1 1 d . . . . . H020 H 0.361494 0.519560 0.624285 0.066 Uiso 1 1 calc R U . . . C021 C 0.801(3) 0.292(2) 0.5714(4) 0.059(4) Uani 1 1 d . . . . . C022 C 0.7651(19) -0.0306(11) 0.9507(2) 0.027(2) Uani 1 1 d . . . . . H02A H 0.792454 0.005029 0.926161 0.041 Uiso 1 1 calc R U . . . H02B H 0.825629 0.027021 0.967154 0.041 Uiso 1 1 calc R U . . . H02C H 0.601655 0.004698 0.955456 0.041 Uiso 1 1 calc R U . . . C023 C 0.272(2) 0.9520(13) 0.3207(3) 0.043(3) Uani 1 1 d . . . . . H023 H 0.158365 0.996575 0.340735 0.052 Uiso 1 1 calc R U . . . C024 C 0.649(2) 0.692(3) 0.3019(3) 0.064(5) Uani 1 1 d . . . . . H02N H 0.744041 0.760737 0.303118 0.096 Uiso 1 1 calc R U . . . H02O H 0.588248 0.707885 0.278034 0.096 Uiso 1 1 calc R U . . . H02P H 0.739456 0.567135 0.307001 0.096 Uiso 1 1 calc R U . . . C025 C 0.750(3) 0.8740(17) 0.4055(4) 0.064(4) Uani 1 1 d . . . . . H025 H 0.812348 0.960304 0.407901 0.076 Uiso 1 1 calc R U . . . C026 C 0.1484(18) 0.9631(13) 0.2854(2) 0.029(2) Uani 1 1 d . . . . . C027 C 0.616(5) 0.889(2) 0.3758(5) 0.113(10) Uani 1 1 d . . . . . C028 C 1.112(2) 0.785(3) 0.4590(3) 0.063(4) Uani 1 1 d . . . . . H02Q H 1.053743 0.912723 0.454138 0.094 Uiso 1 1 calc R U . . . H02R H 1.205036 0.724910 0.438460 0.094 Uiso 1 1 calc R U . . . H02S H 1.205251 0.754350 0.480068 0.094 Uiso 1 1 calc R U . . . C029 C 0.732(5) 0.598(2) 0.4214(5) 0.098(8) Uani 1 1 d . . . . . C02A C 0.437(3) 1.0657(19) 0.3165(3) 0.053(3) Uani 1 1 d . . . . . H02T H 0.536453 1.028521 0.294891 0.063 Uiso 1 1 calc R U . . . H02U H 0.340527 1.192360 0.312786 0.063 Uiso 1 1 calc R U . . . O02B O 0.742(4) 0.4707(15) 0.4502(4) 0.113(6) Uani 1 1 d . . . . . C02C C 0.687(3) -0.082(2) 0.6796(4) 0.082(6) Uani 1 1 d . . . . . H02D H 0.749699 -0.072272 0.702509 0.098 Uiso 1 1 calc R U . . . H02E H 0.695107 -0.204052 0.678569 0.098 Uiso 1 1 calc R U . . . C02D C 0.587(3) 1.0453(16) 0.3481(3) 0.050(3) Uani 1 1 d . . . . . O02E O 0.573(4) 0.598(2) 0.5683(5) 0.154(10) Uani 1 1 d . . . . . C02F C 0.862(3) 0.137(2) 0.5925(4) 0.071(5) Uani 1 1 d . . . . . H02F H 0.991793 0.038238 0.585189 0.085 Uiso 1 1 calc R U . . . O02G O 1.029(2) -0.1570(15) 0.6429(4) 0.087(4) Uani 1 1 d . . . . . C02H C 0.839(2) -0.0479(19) 0.6488(4) 0.059(4) Uani 1 1 d . . . . . C02I C 1.113(3) 0.167(4) 0.5241(5) 0.108(9) Uani 1 1 d . . . . . H02G H 1.222050 0.098862 0.542055 0.162 Uiso 1 1 calc R U . . . H02H H 1.193481 0.202989 0.504172 0.162 Uiso 1 1 calc R U . . . H02I H 1.037115 0.095086 0.515505 0.162 Uiso 1 1 calc R U . . . C02J C 0.741(4) 0.118(2) 0.6245(4) 0.080(6) Uani 1 1 d . . . . . C02K C 0.642(4) 0.6004(17) 0.3878(5) 0.092(8) Uani 1 1 d . . . . . H02V H 0.645061 0.492972 0.379400 0.111 Uiso 1 1 calc R U . . . C02L C 0.945(4) 0.324(3) 0.5399(4) 0.087(6) Uani 1 1 d . . . . . H02L H 0.843466 0.400379 0.521090 0.104 Uiso 1 1 calc R U . . . C02M C 1.101(4) 0.418(4) 0.5527(6) 0.114(9) Uani 1 1 d . . . . . H02J H 1.008016 0.543001 0.556393 0.171 Uiso 1 1 calc R U . . . H02K H 1.219972 0.408845 0.534576 0.171 Uiso 1 1 calc R U . . . H02M H 1.169711 0.360941 0.575117 0.171 Uiso 1 1 calc R U . . . C4 C 0.349(4) 0.743(4) 0.5729(11) 0.174(18) Uani 1 1 d . . . . . H4A H 0.318875 0.768526 0.598187 0.261 Uiso 1 1 calc R U . . . H4B H 0.231314 0.707883 0.564310 0.261 Uiso 1 1 calc R U . . . H4C H 0.348155 0.848772 0.559322 0.261 Uiso 1 1 calc R U . . . C14 C 0.660(10) 0.340(4) 0.4440(11) 0.23(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.018(3) 0.015(3) 0.036(3) 0.000(2) 0.001(2) -0.004(2) O002 0.019(4) 0.033(4) 0.036(3) 0.010(3) -0.008(2) -0.016(3) O003 0.025(4) 0.016(3) 0.027(3) -0.002(2) -0.008(2) -0.006(3) O004 0.047(5) 0.014(3) 0.032(3) 0.000(2) 0.004(3) -0.003(3) O005 0.027(4) 0.020(3) 0.044(4) 0.005(2) -0.009(3) -0.014(3) O006 0.039(4) 0.013(3) 0.033(3) -0.001(2) -0.006(3) -0.002(3) O007 0.021(4) 0.016(3) 0.048(4) 0.003(2) 0.000(3) -0.002(3) O008 0.018(4) 0.041(4) 0.040(3) 0.009(3) -0.008(3) -0.014(3) C009 0.014(4) 0.013(4) 0.033(4) 0.000(3) 0.000(3) -0.001(3) C00A 0.013(4) 0.003(3) 0.035(4) 0.003(3) -0.003(3) 0.003(3) C00B 0.008(4) 0.019(4) 0.021(4) -0.002(3) -0.006(3) -0.003(3) C00C 0.018(5) 0.012(4) 0.032(4) 0.000(3) -0.002(3) -0.006(3) C00D 0.030(5) 0.008(4) 0.026(4) -0.001(3) -0.004(3) -0.003(3) C00E 0.014(5) 0.020(4) 0.029(4) 0.001(3) -0.005(3) -0.007(4) C00F 0.017(5) 0.009(4) 0.034(4) 0.003(3) -0.001(3) -0.005(3) C00G 0.014(4) 0.013(4) 0.026(4) 0.001(3) 0.002(3) -0.003(3) C00H 0.030(5) 0.017(4) 0.021(4) 0.001(3) -0.004(3) -0.010(4) C00I 0.021(5) 0.021(4) 0.037(5) 0.004(3) -0.008(4) -0.012(4) C00J 0.023(5) 0.015(4) 0.031(4) 0.000(3) 0.000(3) -0.008(4) C00K 0.043(6) 0.010(4) 0.033(5) 0.005(3) -0.012(4) -0.012(4) C00L 0.019(4) 0.010(4) 0.021(4) 0.000(3) -0.002(3) -0.002(3) C00M 0.022(5) 0.017(4) 0.020(4) -0.002(3) 0.003(3) -0.006(3) C00N 0.023(5) 0.025(4) 0.022(4) -0.003(3) -0.005(3) -0.010(4) C00O 0.024(5) 0.019(4) 0.019(4) 0.004(3) -0.001(3) -0.010(4) C00P 0.008(4) 0.008(3) 0.034(4) 0.003(3) -0.003(3) 0.001(3) C00Q 0.019(5) 0.019(4) 0.024(4) 0.008(3) -0.007(3) -0.009(4) C00R 0.022(5) 0.015(4) 0.026(4) 0.001(3) -0.003(3) -0.011(3) C00S 0.017(4) 0.017(4) 0.025(4) -0.005(3) 0.001(3) -0.006(3) C00T 0.028(5) 0.013(4) 0.028(4) -0.001(3) -0.003(3) -0.008(4) C00U 0.022(5) 0.024(5) 0.029(4) -0.002(3) 0.002(3) -0.010(4) C00V 0.027(5) 0.022(4) 0.021(4) 0.007(3) -0.004(3) -0.010(4) C00W 0.025(5) 0.011(4) 0.023(4) 0.001(3) 0.000(3) -0.005(3) C00X 0.027(5) 0.019(4) 0.029(4) 0.000(3) -0.008(4) -0.009(4) C00Y 0.023(5) 0.005(3) 0.024(4) 0.002(3) -0.010(3) -0.005(3) C00Z 0.032(6) 0.034(5) 0.033(5) -0.007(4) -0.002(4) -0.006(5) C010 0.031(6) 0.023(5) 0.022(4) 0.002(3) -0.006(4) -0.007(4) C011 0.036(6) 0.016(4) 0.017(4) 0.004(3) -0.007(3) -0.007(4) C012 0.011(4) 0.010(4) 0.026(4) -0.004(3) -0.004(3) -0.001(3) C013 0.029(5) 0.014(4) 0.018(4) 0.005(3) -0.002(3) -0.009(4) C014 0.026(5) 0.019(4) 0.024(4) 0.000(3) 0.000(3) 0.000(4) C015 0.025(5) 0.012(4) 0.021(4) -0.002(3) -0.001(3) -0.005(3) C016 0.025(5) 0.020(4) 0.023(4) 0.002(3) 0.000(3) -0.008(4) C017 0.012(4) 0.016(4) 0.029(4) 0.002(3) -0.010(3) -0.006(3) C018 0.025(5) 0.021(4) 0.029(4) 0.001(3) -0.004(3) -0.014(4) C019 0.049(7) 0.014(4) 0.038(5) -0.001(3) 0.010(5) -0.003(4) C01A 0.019(5) 0.015(4) 0.029(4) 0.005(3) -0.008(3) -0.003(3) O01B 0.061(7) 0.032(5) 0.105(8) 0.005(4) -0.027(5) -0.012(5) C01C 0.008(4) 0.025(4) 0.030(4) 0.001(3) 0.000(3) -0.006(3) C01D 0.027(5) 0.026(4) 0.024(4) 0.004(3) -0.008(3) -0.012(4) C01E 0.018(4) 0.018(4) 0.025(4) -0.001(3) -0.003(3) -0.007(3) C01F 0.022(5) 0.007(4) 0.027(4) 0.002(3) -0.007(3) -0.002(3) C01G 0.015(4) 0.010(4) 0.030(4) -0.003(3) -0.007(3) -0.003(3) C01H 0.015(5) 0.025(4) 0.028(4) -0.004(3) -0.006(3) -0.005(4) C01I 0.025(5) 0.029(5) 0.031(4) 0.001(3) -0.002(4) -0.008(4) C01J 0.033(6) 0.029(5) 0.026(4) 0.001(3) 0.007(4) -0.007(4) C01K 0.025(5) 0.014(4) 0.034(4) 0.005(3) -0.004(3) -0.003(4) C01L 0.023(5) 0.012(4) 0.033(4) 0.003(3) -0.001(3) -0.003(3) C01M 0.020(5) 0.009(4) 0.035(4) -0.005(3) -0.004(3) -0.003(3) C01N 0.025(6) 0.019(5) 0.050(5) 0.011(4) -0.005(4) -0.004(4) C01O 0.023(5) 0.021(4) 0.023(4) 0.000(3) -0.002(3) -0.013(4) C01P 0.017(5) 0.005(4) 0.035(4) 0.000(3) -0.008(3) 0.002(3) C01Q 0.028(5) 0.011(4) 0.024(4) 0.000(3) -0.002(3) -0.009(4) C01R 0.046(6) 0.010(4) 0.031(4) -0.002(3) -0.006(4) -0.013(4) C01S 0.033(6) 0.018(4) 0.029(4) -0.002(3) -0.001(4) -0.005(4) C01T 0.033(6) 0.026(5) 0.029(4) 0.006(3) -0.011(4) -0.010(4) C01U 0.035(7) 0.060(9) 0.075(8) 0.032(7) 0.005(6) -0.005(7) C01V 0.023(5) 0.020(4) 0.029(4) 0.003(3) 0.000(3) -0.002(4) C01W 0.041(6) 0.027(5) 0.026(4) -0.002(3) -0.012(4) -0.006(4) C01X 0.038(7) 0.041(6) 0.045(6) 0.008(4) -0.009(5) -0.014(5) C01Y 0.040(6) 0.016(4) 0.039(5) 0.000(3) -0.006(4) -0.015(4) C01Z 0.020(6) 0.099(11) 0.040(5) -0.009(6) 0.006(4) -0.037(6) C020 0.038(7) 0.035(6) 0.077(8) 0.019(6) 0.023(6) -0.003(6) C021 0.046(8) 0.057(8) 0.054(7) 0.023(6) -0.001(6) -0.001(7) C022 0.037(6) 0.009(4) 0.029(4) 0.004(3) -0.007(4) -0.001(4) C023 0.075(9) 0.014(5) 0.044(6) 0.017(4) -0.040(5) -0.019(5) C024 0.029(7) 0.144(15) 0.030(5) -0.027(7) 0.011(5) -0.043(8) C025 0.079(11) 0.025(6) 0.081(9) 0.004(6) -0.041(8) -0.009(6) C026 0.035(6) 0.030(5) 0.026(4) 0.005(3) -0.008(4) -0.015(4) C027 0.23(3) 0.046(8) 0.084(11) 0.044(8) -0.122(15) -0.073(13) C028 0.028(7) 0.120(13) 0.041(6) 0.011(7) -0.010(5) -0.030(8) C029 0.17(2) 0.034(7) 0.096(12) 0.025(7) -0.095(14) -0.033(10) C02A 0.057(9) 0.050(7) 0.045(6) -0.002(5) 0.003(6) -0.015(6) O02B 0.213(19) 0.042(6) 0.092(8) 0.026(5) -0.075(10) -0.053(9) C02C 0.063(11) 0.060(9) 0.066(8) 0.028(7) 0.032(8) 0.029(8) C02D 0.064(9) 0.032(6) 0.051(6) 0.001(5) 0.002(6) -0.017(6) O02E 0.165(17) 0.073(9) 0.165(14) 0.057(9) 0.105(13) -0.004(9) C02F 0.058(10) 0.044(7) 0.084(9) 0.019(7) 0.039(8) 0.001(7) O02G 0.074(9) 0.048(6) 0.117(9) 0.007(6) 0.031(7) -0.006(6) C02H 0.031(8) 0.040(7) 0.090(10) -0.003(6) 0.013(6) 0.001(6) C02I 0.042(10) 0.22(3) 0.068(10) 0.011(13) -0.006(8) -0.061(14) C02J 0.100(14) 0.044(8) 0.066(8) 0.006(6) 0.045(9) -0.003(8) C02K 0.18(2) 0.016(5) 0.089(10) 0.014(6) -0.086(13) -0.034(9) C02L 0.101(15) 0.077(11) 0.057(8) 0.031(7) 0.026(9) -0.015(10) C02M 0.094(16) 0.18(3) 0.092(13) 0.077(15) -0.034(11) -0.087(17) C4 0.034(10) 0.14(2) 0.28(4) 0.14(3) 0.012(16) 0.022(13) C14 0.45(8) 0.079(16) 0.21(3) 0.057(18) -0.22(4) -0.16(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 0 24 0.0800 0 2 -20 0.0393 0 1 -23 0.0457 0 -1 23 0.0805 1 -2 20 0.0845 0 5 5 0.0188 0 -3 17 0.0781 -4 -1 3 0.4512 0 0 -24 0.0459 0 4 -15 0.0428 0 -5 7 0.0615 0 5 3 0.0199 0 -5 -3 0.0386 0 4 -9 0.0319 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00S O001 C01S 118.0(6) . . ? C00M O003 C022 116.9(7) . . ? O002 C009 C00C 117.9(8) . . ? O002 C009 C00E 123.0(8) . . ? C00E C009 C00C 119.1(7) . . ? C00G C00A H00A 118.6 . . ? C00G C00A C00W 122.9(7) . . ? C00W C00A H00A 118.6 . . ? C00O C00B C01G 120.4(7) . . ? C00W C00B C00O 116.3(7) . . ? C00W C00B C01G 123.3(7) . . ? C009 C00C H00B 108.2 . . ? C009 C00C H00C 108.2 . . ? C009 C00C C01G 116.3(6) . . ? H00B C00C H00C 107.4 . . ? C01G C00C H00B 108.2 . . ? C01G C00C H00C 108.2 . . ? O006 C00D C00W 121.8(8) . . ? O006 C00D C015 120.7(8) . . ? C00W C00D C015 117.4(7) . . ? C009 C00E C00J 109.3(7) . . ? C009 C00E C017 111.3(7) . . ? C009 C00E C01O 107.5(7) . . ? C00J C00E C01O 107.3(7) . . ? C017 C00E C00J 111.1(7) . . ? C017 C00E C01O 110.3(7) . . ? O005 C00F C016 121.1(8) . . ? O005 C00F C01R 120.2(7) . . ? C016 C00F C01R 118.7(7) . . ? C00A C00G C00L 123.8(7) . . ? C00A C00G C00M 115.9(7) . . ? C00M C00G C00L 120.0(7) . . ? C01F C00H C013 116.5(7) . . ? C01J C00H C013 121.4(8) . . ? C01J C00H C01F 122.1(8) . . ? O008 C00I C00X 119.3(8) . . ? O008 C00I C013 121.7(8) . . ? C00X C00I C013 118.8(8) . . ? C00E C00J H00D 108.4 . . ? C00E C00J H00E 108.4 . . ? H00D C00J H00E 107.4 . . ? C014 C00J C00E 115.7(7) . . ? C014 C00J H00D 108.4 . . ? C014 C00J H00E 108.4 . . ? H00I C00K H00J 107.8 . . ? C013 C00K H00I 109.0 . . ? C013 C00K H00J 109.0 . . ? C026 C00K H00I 109.0 . . ? C026 C00K H00J 109.0 . . ? C026 C00K C013 113.1(7) . . ? C00G C00L H00L 107.3 . . ? C00G C00L C01A 110.4(6) . . ? C00G C00L C01T 112.1(7) . . ? C01A C00L H00L 107.3 . . ? C01A C00L C01T 112.1(7) . . ? C01T C00L H00L 107.3 . . ? O003 C00M C00G 114.6(8) . . ? O003 C00M C00O 124.0(8) . . ? C00O C00M C00G 121.5(8) . . ? C014 C00N C01C 123.4(8) . . ? C014 C00N C01H 121.0(8) . . ? C01H C00N C01C 115.4(7) . . ? C00B C00O H00O 118.9 . . ? C00M C00O C00B 122.1(8) . . ? C00M C00O H00O 118.9 . . ? H00F C00P H00G 109.5 . . ? H00F C00P H00H 109.5 . . ? H00G C00P H00H 109.5 . . ? C01G C00P H00F 109.5 . . ? C01G C00P H00G 109.5 . . ? C01G C00P H00H 109.5 . . ? C00R C00Q C00S 116.9(7) . . ? C00R C00Q C00V 123.1(7) . . ? C00S C00Q C00V 119.9(8) . . ? C00Q C00R H00R 118.6 . . ? C00Q C00R C00T 122.9(7) . . ? C00T C00R H00R 118.6 . . ? O001 C00S C00Q 115.7(7) . . ? O001 C00S C011 123.3(7) . . ? C011 C00S C00Q 121.0(7) . . ? C00R C00T C01P 118.5(7) . . ? C01Q C00T C00R 119.9(8) . . ? C01Q C00T C01P 121.6(8) . . ? C010 C00U C01R 113.0(7) . . ? C010 C00U C023 109.8(7) . . ? C010 C00U C024 106.9(9) . . ? C01R C00U C024 107.2(9) . . ? C023 C00U C01R 107.7(8) . . ? C023 C00U C024 112.2(10) . . ? C00Q C00V H00V 107.0 . . ? C00Q C00V C01K 113.5(7) . . ? C00Q C00V C01L 110.5(7) . . ? C01K C00V H00V 107.0 . . ? C01L C00V H00V 107.0 . . ? C01L C00V C01K 111.5(8) . . ? C00A C00W C00D 117.9(7) . . ? C00B C00W C00A 121.2(7) . . ? C00B C00W C00D 120.9(8) . . ? C00I C00X H00K 108.2 . . ? C00I C00X H00M 108.2 . . ? C00I C00X C00Y 116.2(7) . . ? H00K C00X H00M 107.4 . . ? C00Y C00X H00K 108.2 . . ? C00Y C00X H00M 108.2 . . ? C00X C00Y C01F 108.1(6) . . ? C01D C00Y C00X 109.8(7) . . ? C01D C00Y C01F 110.5(7) . . ? C01Q C00Y C00X 111.6(7) . . ? C01Q C00Y C01D 106.6(6) . . ? C01Q C00Y C01F 110.3(6) . . ? C025 C00Z C01W 124.5(11) . . ? C025 C00Z C029 114.0(12) . . ? C029 C00Z C01W 121.2(10) . . ? C027 C010 C00U 122.8(8) . . ? C027 C010 C02K 112.4(11) . . ? C02K C010 C00U 122.6(9) . . ? C00S C011 H011 119.1 . . ? C00S C011 C01Q 121.9(8) . . ? C01Q C011 H011 119.1 . . ? C015 C012 H012 106.9 . . ? C015 C012 C017 115.2(7) . . ? C015 C012 C01G 111.4(6) . . ? C017 C012 H012 106.9 . . ? C017 C012 C01G 109.1(6) . . ? C01G C012 H012 106.9 . . ? C00H C013 C00K 109.8(7) . . ? C00I C013 C00H 109.8(6) . . ? C00I C013 C00K 110.5(8) . . ? C00I C013 C01E 107.4(7) . . ? C01E C013 C00H 111.3(8) . . ? C01E C013 C00K 108.1(6) . . ? C00J C014 C019 119.3(7) . . ? C00N C014 C00J 120.5(8) . . ? C00N C014 C019 120.2(8) . . ? C00D C015 C012 113.8(7) . . ? C00D C015 H01A 108.8 . . ? C00D C015 H01B 108.8 . . ? C012 C015 H01A 108.8 . . ? C012 C015 H01B 108.8 . . ? H01A C015 H01B 107.7 . . ? C00F C016 C018 116.2(7) . . ? C026 C016 C00F 122.0(8) . . ? C026 C016 C018 121.7(8) . . ? C00E C017 C012 116.9(7) . . ? C01Y C017 C00E 121.5(8) . . ? C01Y C017 C012 121.6(8) . . ? C016 C018 H01R 108.8 . . ? C016 C018 H01S 108.8 . . ? H01R C018 H01S 107.7 . . ? C01E C018 C016 113.6(7) . . ? C01E C018 H01R 108.8 . . ? C01E C018 H01S 108.8 . . ? C014 C019 H019 108.4 . . ? C014 C019 C01V 112.7(7) . . ? C014 C019 C02C 110.8(8) . . ? C01V C019 H019 108.4 . . ? C01V C019 C02C 108.0(11) . . ? C02C C019 H019 108.4 . . ? C00L C01A H01C 109.5 . . ? C00L C01A H01D 109.5 . . ? C00L C01A H01E 109.5 . . ? H01C C01A H01D 109.5 . . ? H01C C01A H01E 109.5 . . ? H01D C01A H01E 109.5 . . ? C00N C01C H01F 109.0 . . ? C00N C01C H01G 109.0 . . ? C00N C01C C01O 113.1(7) . . ? H01F C01C H01G 107.8 . . ? C01O C01C H01F 109.0 . . ? C01O C01C H01G 109.0 . . ? C00Y C01D H01T 109.5 . . ? C00Y C01D H01U 109.5 . . ? C00Y C01D H01V 109.5 . . ? H01T C01D H01U 109.5 . . ? H01T C01D H01V 109.5 . . ? H01U C01D H01V 109.5 . . ? C013 C01E H01W 108.9 . . ? C013 C01E H01X 108.9 . . ? C018 C01E C013 113.4(7) . . ? C018 C01E H01W 108.9 . . ? C018 C01E H01X 108.9 . . ? H01W C01E H01X 107.7 . . ? C00H C01F C00Y 110.8(6) . . ? C00H C01F H01Y 106.7 . . ? C00H C01F C01M 114.8(7) . . ? C00Y C01F H01Y 106.7 . . ? C01M C01F C00Y 110.7(6) . . ? C01M C01F H01Y 106.7 . . ? C00B C01G C00C 112.5(7) . . ? C00B C01G C00P 106.8(6) . . ? C00B C01G C012 108.9(6) . . ? C00C C01G C012 108.3(6) . . ? C00P C01G C00C 109.8(7) . . ? C00P C01G C012 110.7(7) . . ? O007 C01H C00N 121.3(8) . . ? O007 C01H C01I 120.3(8) . . ? C00N C01H C01I 118.4(8) . . ? C01H C01I H01H 109.4 . . ? C01H C01I H01I 109.4 . . ? C01H C01I C01V 111.3(8) . . ? H01H C01I H01I 108.0 . . ? C01V C01I H01H 109.4 . . ? C01V C01I H01I 109.4 . . ? C00V C01K H01Z 109.5 . . ? C00V C01K H 109.5 . . ? C00V C01K HA 109.5 . . ? H01Z C01K H 109.5 . . ? H01Z C01K HA 109.5 . . ? H C01K HA 109.5 . . ? C00V C01L H01 109.5 . . ? C00V C01L HB 109.5 . . ? C00V C01L HC 109.5 . . ? H01 C01L HB 109.5 . . ? H01 C01L HC 109.5 . . ? HB C01L HC 109.5 . . ? C01F C01M H1 108.8 . . ? C01F C01M HD 108.8 . . ? H1 C01M HD 107.7 . . ? C01P C01M C01F 113.8(7) . . ? C01P C01M H1 108.8 . . ? C01P C01M HD 108.8 . . ? C020 C01N C01V 120.3(9) . . ? C020 C01N C02J 115.8(11) . . ? C02J C01N C01V 122.0(9) . . ? C00E C01O H01J 109.2 . . ? C00E C01O H01K 109.2 . . ? C01C C01O C00E 111.9(7) . . ? C01C C01O H01J 109.2 . . ? C01C C01O H01K 109.2 . . ? H01J C01O H01K 107.9 . . ? O004 C01P C00T 121.6(8) . . ? O004 C01P C01M 120.3(7) . . ? C00T C01P C01M 118.0(7) . . ? C00T C01Q C00Y 121.9(7) . . ? C00T C01Q C011 117.5(7) . . ? C011 C01Q C00Y 120.6(7) . . ? C00F C01R C00U 109.8(7) . . ? C00F C01R H2 109.7 . . ? C00F C01R HE 109.7 . . ? C00U C01R H2 109.7 . . ? C00U C01R HE 109.7 . . ? H2 C01R HE 108.2 . . ? O001 C01S H3 109.5 . . ? O001 C01S HF 109.5 . . ? O001 C01S HG 109.5 . . ? H3 C01S HF 109.5 . . ? H3 C01S HG 109.5 . . ? HF C01S HG 109.5 . . ? C00L C01T H01L 109.5 . . ? C00L C01T H01M 109.5 . . ? C00L C01T H01N 109.5 . . ? H01L C01T H01M 109.5 . . ? H01L C01T H01N 109.5 . . ? H01M C01T H01N 109.5 . . ? C021 C01U C020 124.7(12) . . ? C021 C01U O02E 115.2(12) . . ? O02E C01U C020 120.0(13) . . ? C01I C01V C019 106.4(9) . . ? C01N C01V C019 110.2(7) . . ? C01N C01V C01I 113.1(8) . . ? C01N C01V C01Z 106.9(9) . . ? C01Z C01V C019 111.6(9) . . ? C01Z C01V C01I 108.6(8) . . ? C00Z C01W H4 106.5 . . ? C00Z C01W C01X 111.4(10) . . ? C01X C01W H4 106.5 . . ? C028 C01W C00Z 111.2(9) . . ? C028 C01W H4 106.5 . . ? C028 C01W C01X 114.2(10) . . ? C01W C01X H5 109.5 . . ? C01W C01X HH 109.5 . . ? C01W C01X HI 109.5 . . ? H5 C01X HH 109.5 . . ? H5 C01X HI 109.5 . . ? HH C01X HI 109.5 . . ? C01V C01Z H01O 109.5 . . ? C01V C01Z H01P 109.5 . . ? C01V C01Z H01Q 109.5 . . ? H01O C01Z H01P 109.5 . . ? H01O C01Z H01Q 109.5 . . ? H01P C01Z H01Q 109.5 . . ? C01N C020 C01U 120.5(12) . . ? C01N C020 H020 119.7 . . ? C01U C020 H020 119.7 . . ? C01U C021 C02L 120.6(13) . . ? C02F C021 C01U 113.5(12) . . ? C02F C021 C02L 124.5(13) . . ? O003 C022 H02A 109.5 . . ? O003 C022 H02B 109.5 . . ? O003 C022 H02C 109.5 . . ? H02A C022 H02B 109.5 . . ? H02A C022 H02C 109.5 . . ? H02B C022 H02C 109.5 . . ? C00U C023 H023 110.1 . . ? C00U C023 C02A 102.5(10) . . ? C026 C023 C00U 112.6(8) . . ? C026 C023 H023 110.1 . . ? C026 C023 C02A 111.1(9) . . ? C02A C023 H023 110.1 . . ? C00U C024 H02N 109.5 . . ? C00U C024 H02O 109.5 . . ? C00U C024 H02P 109.5 . . ? H02N C024 H02O 109.5 . . ? H02N C024 H02P 109.5 . . ? H02O C024 H02P 109.5 . . ? C00Z C025 H025 118.7 . . ? C00Z C025 C027 122.6(14) . . ? C027 C025 H025 118.7 . . ? C016 C026 C00K 123.0(8) . . ? C016 C026 C023 120.6(8) . . ? C023 C026 C00K 116.3(8) . . ? C010 C027 C025 123.7(11) . . ? C010 C027 C02D 117.6(11) . . ? C025 C027 C02D 117.4(15) . . ? C01W C028 H02Q 109.5 . . ? C01W C028 H02R 109.5 . . ? C01W C028 H02S 109.5 . . ? H02Q C028 H02R 109.5 . . ? H02Q C028 H02S 109.5 . . ? H02R C028 H02S 109.5 . . ? C00Z C029 O02B 114.0(13) . . ? C02K C029 C00Z 121.0(13) . . ? C02K C029 O02B 124.6(16) . . ? C023 C02A H02T 108.5 . . ? C023 C02A H02U 108.5 . . ? H02T C02A H02U 107.5 . . ? C02D C02A C023 115.1(10) . . ? C02D C02A H02T 108.5 . . ? C02D C02A H02U 108.5 . . ? C14 O02B C029 117.5(17) . . ? C019 C02C H02D 108.6 . . ? C019 C02C H02E 108.6 . . ? H02D C02C H02E 107.6 . . ? C02H C02C C019 114.6(10) . . ? C02H C02C H02D 108.6 . . ? C02H C02C H02E 108.6 . . ? O01B C02D C027 121.9(13) . . ? O01B C02D C02A 120.4(11) . . ? C02A C02D C027 117.7(12) . . ? C01U O02E C4 120.4(15) . . ? C021 C02F H02F 118.2 . . ? C021 C02F C02J 123.6(13) . . ? C02J C02F H02F 118.2 . . ? O02G C02H C02C 120.2(13) . . ? O02G C02H C02J 120.5(13) . . ? C02J C02H C02C 119.2(11) . . ? H02G C02I H02H 109.5 . . ? H02G C02I H02I 109.5 . . ? H02H C02I H02I 109.5 . . ? C02L C02I H02G 109.5 . . ? C02L C02I H02H 109.5 . . ? C02L C02I H02I 109.5 . . ? C01N C02J C02F 120.7(13) . . ? C01N C02J C02H 119.1(11) . . ? C02F C02J C02H 120.1(13) . . ? C010 C02K C029 122.8(11) . . ? C010 C02K H02V 118.6 . . ? C029 C02K H02V 118.6 . . ? C021 C02L H02L 109.5 . . ? C021 C02L C02M 110.2(16) . . ? C02I C02L C021 116.3(16) . . ? C02I C02L H02L 109.5 . . ? C02I C02L C02M 101(2) . . ? C02M C02L H02L 109.5 . . ? C02L C02M H02J 109.5 . . ? C02L C02M H02K 109.5 . . ? C02L C02M H02M 109.5 . . ? H02J C02M H02K 109.5 . . ? H02J C02M H02M 109.5 . . ? H02K C02M H02M 109.5 . . ? O02E C4 H4A 109.5 . . ? O02E C4 H4B 109.5 . . ? O02E C4 H4C 109.5 . . ? H4A C4 H4B 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C00S 1.369(10) . ? O001 C01S 1.399(10) . ? O002 C009 1.213(11) . ? O003 C00M 1.350(11) . ? O003 C022 1.424(10) . ? O004 C01P 1.243(10) . ? O005 C00F 1.222(11) . ? O006 C00D 1.244(10) . ? O007 C01H 1.224(11) . ? O008 C00I 1.210(12) . ? C009 C00C 1.517(12) . ? C009 C00E 1.499(13) . ? C00A H00A 0.9300 . ? C00A C00G 1.372(12) . ? C00A C00W 1.408(12) . ? C00B C00O 1.415(12) . ? C00B C00W 1.386(11) . ? C00B C01G 1.510(11) . ? C00C H00B 0.9700 . ? C00C H00C 0.9700 . ? C00C C01G 1.564(11) . ? C00D C00W 1.486(12) . ? C00D C015 1.492(12) . ? C00E C00J 1.542(11) . ? C00E C017 1.509(11) . ? C00E C01O 1.565(12) . ? C00F C016 1.465(11) . ? C00F C01R 1.509(13) . ? C00G C00L 1.517(12) . ? C00G C00M 1.424(11) . ? C00H C013 1.539(11) . ? C00H C01F 1.492(12) . ? C00H C01J 1.349(14) . ? C00I C00X 1.507(12) . ? C00I C013 1.522(12) . ? C00J H00D 0.9700 . ? C00J H00E 0.9700 . ? C00J C014 1.509(11) . ? C00K H00I 0.9700 . ? C00K H00J 0.9700 . ? C00K C013 1.541(12) . ? C00K C026 1.535(12) . ? C00L H00L 0.9800 . ? C00L C01A 1.522(12) . ? C00L C01T 1.522(12) . ? C00M C00O 1.375(12) . ? C00N C014 1.359(13) . ? C00N C01C 1.511(11) . ? C00N C01H 1.468(12) . ? C00O H00O 0.9300 . ? C00P H00F 0.9600 . ? C00P H00G 0.9600 . ? C00P H00H 0.9600 . ? C00P C01G 1.526(12) . ? C00Q C00R 1.373(12) . ? C00Q C00S 1.408(11) . ? C00Q C00V 1.508(11) . ? C00R H00R 0.9300 . ? C00R C00T 1.420(12) . ? C00S C011 1.386(12) . ? C00T C01P 1.467(12) . ? C00T C01Q 1.384(11) . ? C00U C010 1.499(13) . ? C00U C01R 1.542(13) . ? C00U C023 1.542(14) . ? C00U C024 1.552(13) . ? C00V H00V 0.9800 . ? C00V C01K 1.543(11) . ? C00V C01L 1.531(14) . ? C00X H00K 0.9700 . ? C00X H00M 0.9700 . ? C00X C00Y 1.555(11) . ? C00Y C01D 1.541(12) . ? C00Y C01F 1.557(11) . ? C00Y C01Q 1.521(11) . ? C00Z C01W 1.499(15) . ? C00Z C025 1.352(18) . ? C00Z C029 1.40(2) . ? C010 C027 1.365(18) . ? C010 C02K 1.383(15) . ? C011 H011 0.9300 . ? C011 C01Q 1.409(12) . ? C012 H012 0.9800 . ? C012 C015 1.501(10) . ? C012 C017 1.542(11) . ? C012 C01G 1.574(11) . ? C013 C01E 1.534(12) . ? C014 C019 1.522(13) . ? C015 H01A 0.9700 . ? C015 H01B 0.9700 . ? C016 C018 1.522(13) . ? C016 C026 1.331(13) . ? C017 C01Y 1.361(13) . ? C018 H01R 0.9700 . ? C018 H01S 0.9700 . ? C018 C01E 1.513(12) . ? C019 H019 0.9800 . ? C019 C01V 1.541(13) . ? C019 C02C 1.605(19) . ? C01A H01C 0.9600 . ? C01A H01D 0.9600 . ? C01A H01E 0.9600 . ? O01B C02D 1.237(17) . ? C01C H01F 0.9700 . ? C01C H01G 0.9700 . ? C01C C01O 1.522(11) . ? C01D H01T 0.9600 . ? C01D H01U 0.9600 . ? C01D H01V 0.9600 . ? C01E H01W 0.9700 . ? C01E H01X 0.9700 . ? C01F H01Y 0.9800 . ? C01F C01M 1.520(10) . ? C01H C01I 1.508(12) . ? C01I H01H 0.9700 . ? C01I H01I 0.9700 . ? C01I C01V 1.525(14) . ? C01K H01Z 0.9600 . ? C01K H 0.9600 . ? C01K HA 0.9600 . ? C01L H01 0.9600 . ? C01L HB 0.9600 . ? C01L HC 0.9600 . ? C01M H1 0.9700 . ? C01M HD 0.9700 . ? C01M C01P 1.487(12) . ? C01N C01V 1.512(13) . ? C01N C020 1.368(15) . ? C01N C02J 1.393(19) . ? C01O H01J 0.9700 . ? C01O H01K 0.9700 . ? C01R H2 0.9700 . ? C01R HE 0.9700 . ? C01S H3 0.9600 . ? C01S HF 0.9600 . ? C01S HG 0.9600 . ? C01T H01L 0.9600 . ? C01T H01M 0.9600 . ? C01T H01N 0.9600 . ? C01U C020 1.391(17) . ? C01U C021 1.37(2) . ? C01U O02E 1.378(18) . ? C01V C01Z 1.522(16) . ? C01W H4 0.9800 . ? C01W C01X 1.517(16) . ? C01W C028 1.477(19) . ? C01X H5 0.9600 . ? C01X HH 0.9600 . ? C01X HI 0.9600 . ? C01Z H01O 0.9600 . ? C01Z H01P 0.9600 . ? C01Z H01Q 0.9600 . ? C020 H020 0.9300 . ? C021 C02F 1.360(18) . ? C021 C02L 1.51(2) . ? C022 H02A 0.9600 . ? C022 H02B 0.9600 . ? C022 H02C 0.9600 . ? C023 H023 0.9800 . ? C023 C026 1.533(14) . ? C023 C02A 1.62(2) . ? C024 H02N 0.9600 . ? C024 H02O 0.9600 . ? C024 H02P 0.9600 . ? C025 H025 0.9300 . ? C025 C027 1.39(2) . ? C027 C02D 1.533(18) . ? C028 H02Q 0.9600 . ? C028 H02R 0.9600 . ? C028 H02S 0.9600 . ? C029 O02B 1.41(2) . ? C029 C02K 1.38(2) . ? C02A H02T 0.9700 . ? C02A H02U 0.9700 . ? C02A C02D 1.50(2) . ? O02B C14 1.38(3) . ? C02C H02D 0.9700 . ? C02C H02E 0.9700 . ? C02C C02H 1.52(2) . ? O02E C4 1.45(3) . ? C02F H02F 0.9300 . ? C02F C02J 1.403(18) . ? O02G C02H 1.195(17) . ? C02H C02J 1.50(2) . ? C02I H02G 0.9600 . ? C02I H02H 0.9600 . ? C02I H02I 0.9600 . ? C02I C02L 1.43(3) . ? C02K H02V 0.9300 . ? C02L H02L 0.9800 . ? C02L C02M 1.55(3) . ? C02M H02J 0.9600 . ? C02M H02K 0.9600 . ? C02M H02M 0.9600 . ? C4 H4A 0.9600 . ? C4 H4B 0.9600 . ? C4 H4C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O001 C00S C011 C01Q 176.9(8) . . . . ? O002 C009 C00C C01G -146.6(8) . . . . ? O002 C009 C00E C00J 19.9(12) . . . . ? O002 C009 C00E C017 142.9(8) . . . . ? O002 C009 C00E C01O -96.2(10) . . . . ? O003 C00M C00O C00B 177.2(7) . . . . ? O005 C00F C016 C018 2.7(12) . . . . ? O005 C00F C016 C026 -175.5(9) . . . . ? O005 C00F C01R C00U 144.5(8) . . . . ? O006 C00D C00W C00A 1.2(13) . . . . ? O006 C00D C00W C00B -177.6(8) . . . . ? O006 C00D C015 C012 -154.7(8) . . . . ? O007 C01H C01I C01V 144.0(9) . . . . ? O008 C00I C00X C00Y -149.1(9) . . . . ? O008 C00I C013 C00H 145.7(9) . . . . ? O008 C00I C013 C00K 24.5(11) . . . . ? O008 C00I C013 C01E -93.1(10) . . . . ? C009 C00C C01G C00B 135.3(7) . . . . ? C009 C00C C01G C00P -106.0(8) . . . . ? C009 C00C C01G C012 14.9(10) . . . . ? C009 C00E C00J C014 -69.3(10) . . . . ? C009 C00E C017 C012 -7.8(10) . . . . ? C009 C00E C017 C01Y 172.9(9) . . . . ? C009 C00E C01O C01C 58.0(9) . . . . ? C00A C00G C00L C01A 83.1(10) . . . . ? C00A C00G C00L C01T -42.6(11) . . . . ? C00A C00G C00M O003 -175.7(7) . . . . ? C00A C00G C00M C00O 5.4(11) . . . . ? C00C C009 C00E C00J -161.8(7) . . . . ? C00C C009 C00E C017 -38.8(10) . . . . ? C00C C009 C00E C01O 82.0(9) . . . . ? C00E C009 C00C C01G 35.1(11) . . . . ? C00E C00J C014 C00N -21.6(14) . . . . ? C00E C00J C014 C019 160.0(9) . . . . ? C00F C016 C018 C01E 166.8(7) . . . . ? C00F C016 C026 C00K -177.1(9) . . . . ? C00F C016 C026 C023 1.5(15) . . . . ? C00G C00A C00W C00B 3.0(13) . . . . ? C00G C00A C00W C00D -175.7(8) . . . . ? C00G C00M C00O C00B -4.0(12) . . . . ? C00H C013 C01E C018 -179.8(7) . . . . ? C00H C01F C01M C01P -180.0(7) . . . . ? C00I C00X C00Y C01D -107.0(8) . . . . ? C00I C00X C00Y C01F 13.6(10) . . . . ? C00I C00X C00Y C01Q 135.1(8) . . . . ? C00I C013 C01E C018 60.0(9) . . . . ? C00J C00E C017 C012 114.2(8) . . . . ? C00J C00E C017 C01Y -65.1(11) . . . . ? C00J C00E C01O C01C -59.4(9) . . . . ? C00J C014 C019 C01V -153.6(9) . . . . ? C00J C014 C019 C02C -32.5(16) . . . . ? C00K C013 C01E C018 -59.2(9) . . . . ? C00L C00G C00M O003 -1.9(10) . . . . ? C00L C00G C00M C00O 179.2(7) . . . . ? C00M C00G C00L C01A -90.2(8) . . . . ? C00M C00G C00L C01T 144.1(8) . . . . ? C00N C014 C019 C01V 28.1(16) . . . . ? C00N C014 C019 C02C 149.2(13) . . . . ? C00N C01C C01O C00E 45.6(10) . . . . ? C00N C01H C01I C01V -35.2(12) . . . . ? C00O C00B C00W C00A -1.2(11) . . . . ? C00O C00B C00W C00D 177.5(8) . . . . ? C00O C00B C01G C00C 37.5(10) . . . . ? C00O C00B C01G C00P -83.0(9) . . . . ? C00O C00B C01G C012 157.5(7) . . . . ? C00Q C00R C00T C01P -177.8(9) . . . . ? C00Q C00R C00T C01Q 0.6(14) . . . . ? C00Q C00S C011 C01Q -1.6(14) . . . . ? C00R C00Q C00S O001 -176.1(8) . . . . ? C00R C00Q C00S C011 2.6(13) . . . . ? C00R C00Q C00V C01K -40.6(12) . . . . ? C00R C00Q C00V C01L 85.5(10) . . . . ? C00R C00T C01P O004 0.9(14) . . . . ? C00R C00T C01P C01M 177.0(8) . . . . ? C00R C00T C01Q C00Y -177.6(8) . . . . ? C00R C00T C01Q C011 0.5(13) . . . . ? C00S C00Q C00R C00T -2.1(13) . . . . ? C00S C00Q C00V C01K 144.2(8) . . . . ? C00S C00Q C00V C01L -89.7(10) . . . . ? C00S C011 C01Q C00T 0.0(14) . . . . ? C00S C011 C01Q C00Y 178.1(8) . . . . ? C00U C010 C027 C025 -167.8(19) . . . . ? C00U C010 C027 C02D -1(3) . . . . ? C00U C010 C02K C029 -178(2) . . . . ? C00U C023 C026 C00K -157.3(9) . . . . ? C00U C023 C026 C016 23.9(15) . . . . ? C00U C023 C02A C02D -52.5(13) . . . . ? C00V C00Q C00R C00T -177.4(8) . . . . ? C00V C00Q C00S O001 -0.6(12) . . . . ? C00V C00Q C00S C011 178.0(8) . . . . ? C00W C00A C00G C00L -178.5(7) . . . . ? C00W C00A C00G C00M -4.9(12) . . . . ? C00W C00B C00O C00M 1.8(11) . . . . ? C00W C00B C01G C00C -146.0(8) . . . . ? C00W C00B C01G C00P 93.5(9) . . . . ? C00W C00B C01G C012 -26.0(10) . . . . ? C00W C00D C015 C012 28.7(11) . . . . ? C00X C00I C013 C00H -39.9(10) . . . . ? C00X C00I C013 C00K -161.1(7) . . . . ? C00X C00I C013 C01E 81.2(9) . . . . ? C00X C00Y C01F C00H -58.2(9) . . . . ? C00X C00Y C01F C01M 173.2(7) . . . . ? C00X C00Y C01Q C00T -146.1(8) . . . . ? C00X C00Y C01Q C011 35.9(11) . . . . ? C00Y C01F C01M C01P -53.6(10) . . . . ? C00Z C025 C027 C010 -11(4) . . . . ? C00Z C025 C027 C02D -178.0(17) . . . . ? C00Z C029 O02B C14 173(3) . . . . ? C00Z C029 C02K C010 -18(4) . . . . ? C010 C00U C01R C00F 180.0(7) . . . . ? C010 C00U C023 C026 -176.6(9) . . . . ? C010 C00U C023 C02A 63.8(10) . . . . ? C010 C027 C02D O01B -168.2(18) . . . . ? C010 C027 C02D C02A 14(3) . . . . ? C013 C00H C01F C00Y 56.8(10) . . . . ? C013 C00H C01F C01M -176.9(7) . . . . ? C013 C00I C00X C00Y 36.4(11) . . . . ? C013 C00K C026 C016 -22.0(14) . . . . ? C013 C00K C026 C023 159.3(10) . . . . ? C014 C00N C01C C01O -18.3(13) . . . . ? C014 C00N C01H O007 -174.7(10) . . . . ? C014 C00N C01H C01I 4.5(14) . . . . ? C014 C019 C01V C01I -56.0(12) . . . . ? C014 C019 C01V C01N -178.9(9) . . . . ? C014 C019 C01V C01Z 62.4(12) . . . . ? C014 C019 C02C C02H -168.4(14) . . . . ? C015 C00D C00W C00A 177.8(7) . . . . ? C015 C00D C00W C00B -1.0(12) . . . . ? C015 C012 C017 C00E -177.4(7) . . . . ? C015 C012 C017 C01Y 1.9(11) . . . . ? C015 C012 C01G C00B 51.8(9) . . . . ? C015 C012 C01G C00C 174.4(7) . . . . ? C015 C012 C01G C00P -65.3(9) . . . . ? C016 C00F C01R C00U -36.1(11) . . . . ? C016 C018 C01E C013 43.1(10) . . . . ? C017 C00E C00J C014 167.5(8) . . . . ? C017 C00E C01O C01C 179.5(7) . . . . ? C017 C012 C015 C00D -179.6(7) . . . . ? C017 C012 C01G C00B -179.9(7) . . . . ? C017 C012 C01G C00C -57.3(9) . . . . ? C017 C012 C01G C00P 63.0(8) . . . . ? C018 C016 C026 C00K 4.8(15) . . . . ? C018 C016 C026 C023 -176.5(10) . . . . ? C019 C02C C02H O02G -167.6(16) . . . . ? C019 C02C C02H C02J 9(3) . . . . ? C01C C00N C014 C00J 5.8(15) . . . . ? C01C C00N C014 C019 -175.8(9) . . . . ? C01C C00N C01H O007 0.6(13) . . . . ? C01C C00N C01H C01I 179.9(8) . . . . ? C01D C00Y C01F C00H 61.9(9) . . . . ? C01D C00Y C01F C01M -66.6(9) . . . . ? C01D C00Y C01Q C00T 94.1(9) . . . . ? C01D C00Y C01Q C011 -84.0(10) . . . . ? C01F C00H C013 C00I -7.0(10) . . . . ? C01F C00H C013 C00K 114.7(8) . . . . ? C01F C00H C013 C01E -125.7(8) . . . . ? C01F C00Y C01Q C00T -25.9(11) . . . . ? C01F C00Y C01Q C011 156.1(8) . . . . ? C01F C01M C01P O004 -155.2(8) . . . . ? C01F C01M C01P C00T 28.6(11) . . . . ? C01G C00B C00O C00M 178.5(7) . . . . ? C01G C00B C00W C00A -177.8(8) . . . . ? C01G C00B C00W C00D 0.9(12) . . . . ? C01G C012 C015 C00D -54.7(9) . . . . ? C01G C012 C017 C00E 56.5(9) . . . . ? C01G C012 C017 C01Y -124.2(9) . . . . ? C01H C00N C014 C00J -179.2(8) . . . . ? C01H C00N C014 C019 -0.9(16) . . . . ? C01H C00N C01C C01O 166.5(8) . . . . ? C01H C01I C01V C019 59.1(10) . . . . ? C01H C01I C01V C01N -179.8(8) . . . . ? C01H C01I C01V C01Z -61.2(11) . . . . ? C01J C00H C013 C00I 173.2(9) . . . . ? C01J C00H C013 C00K -65.2(11) . . . . ? C01J C00H C013 C01E 54.4(10) . . . . ? C01J C00H C01F C00Y -123.3(9) . . . . ? C01J C00H C01F C01M 3.0(12) . . . . ? C01O C00E C00J C014 46.9(11) . . . . ? C01O C00E C017 C012 -126.9(7) . . . . ? C01O C00E C017 C01Y 53.8(11) . . . . ? C01P C00T C01Q C00Y 0.7(13) . . . . ? C01P C00T C01Q C011 178.8(9) . . . . ? C01Q C00T C01P O004 -177.5(9) . . . . ? C01Q C00T C01P C01M -1.4(13) . . . . ? C01Q C00Y C01F C00H 179.5(7) . . . . ? C01Q C00Y C01F C01M 51.0(10) . . . . ? C01R C00F C016 C018 -176.7(8) . . . . ? C01R C00F C016 C026 5.1(13) . . . . ? C01R C00U C010 C027 -161.7(17) . . . . ? C01R C00U C010 C02K 36.4(18) . . . . ? C01R C00U C023 C026 -53.2(12) . . . . ? C01R C00U C023 C02A -172.7(7) . . . . ? C01S O001 C00S C00Q 175.5(8) . . . . ? C01S O001 C00S C011 -3.2(13) . . . . ? C01U C021 C02F C02J 5(3) . . . . ? C01U C021 C02L C02I -173.1(17) . . . . ? C01U C021 C02L C02M 72(2) . . . . ? C01V C019 C02C C02H -44.6(19) . . . . ? C01V C01N C020 C01U 172.0(14) . . . . ? C01V C01N C02J C02F -175.0(17) . . . . ? C01V C01N C02J C02H 1(3) . . . . ? C01W C00Z C025 C027 -173.7(18) . . . . ? C01W C00Z C029 O02B 15(3) . . . . ? C01W C00Z C029 C02K -172(2) . . . . ? C020 C01N C01V C019 156.9(12) . . . . ? C020 C01N C01V C01I 38.0(15) . . . . ? C020 C01N C01V C01Z -81.5(14) . . . . ? C020 C01N C02J C02F -10(3) . . . . ? C020 C01N C02J C02H 165.3(16) . . . . ? C020 C01U C021 C02F -8(3) . . . . ? C020 C01U C021 C02L -175.4(19) . . . . ? C020 C01U O02E C4 -20(4) . . . . ? C021 C01U C020 C01N 2(3) . . . . ? C021 C01U O02E C4 160(3) . . . . ? C021 C02F C02J C01N 4(3) . . . . ? C021 C02F C02J C02H -171.2(19) . . . . ? C022 O003 C00M C00G 177.6(7) . . . . ? C022 O003 C00M C00O -3.5(11) . . . . ? C023 C00U C010 C027 -41(2) . . . . ? C023 C00U C010 C02K 156.6(16) . . . . ? C023 C00U C01R C00F 58.5(10) . . . . ? C023 C02A C02D O01B -162.6(13) . . . . ? C023 C02A C02D C027 15(2) . . . . ? C024 C00U C010 C027 81(2) . . . . ? C024 C00U C010 C02K -81.4(18) . . . . ? C024 C00U C01R C00F -62.4(11) . . . . ? C024 C00U C023 C026 64.5(13) . . . . ? C024 C00U C023 C02A -55.0(11) . . . . ? C025 C00Z C01W C01X 89.1(15) . . . . ? C025 C00Z C01W C028 -39.6(18) . . . . ? C025 C00Z C029 O02B -170.4(19) . . . . ? C025 C00Z C029 C02K 2(3) . . . . ? C025 C027 C02D O01B -1(3) . . . . ? C025 C027 C02D C02A -178.3(18) . . . . ? C026 C00K C013 C00H 168.5(8) . . . . ? C026 C00K C013 C00I -70.2(10) . . . . ? C026 C00K C013 C01E 47.0(11) . . . . ? C026 C016 C018 C01E -15.0(13) . . . . ? C026 C023 C02A C02D -173.1(10) . . . . ? C027 C010 C02K C029 19(3) . . . . ? C029 C00Z C01W C01X -97.1(17) . . . . ? C029 C00Z C01W C028 134.2(17) . . . . ? C029 C00Z C025 C027 12(3) . . . . ? C02A C023 C026 C00K -42.9(14) . . . . ? C02A C023 C026 C016 138.3(10) . . . . ? O02B C029 C02K C010 153(2) . . . . ? C02C C019 C01V C01I -178.6(9) . . . . ? C02C C019 C01V C01N 58.4(12) . . . . ? C02C C019 C01V C01Z -60.3(11) . . . . ? C02C C02H C02J C01N 15(3) . . . . ? C02C C02H C02J C02F -169(2) . . . . ? O02E C01U C020 C01N -177.0(19) . . . . ? O02E C01U C021 C02F 171(2) . . . . ? O02E C01U C021 C02L 4(3) . . . . ? C02F C021 C02L C02I 21(3) . . . . ? C02F C021 C02L C02M -93(2) . . . . ? O02G C02H C02J C01N -168.9(18) . . . . ? O02G C02H C02J C02F 7(3) . . . . ? C02J C01N C01V C019 -39.2(18) . . . . ? C02J C01N C01V C01I -158.2(14) . . . . ? C02J C01N C01V C01Z 82.3(16) . . . . ? C02J C01N C020 C01U 7(2) . . . . ? C02K C010 C027 C025 -4(3) . . . . ? C02K C010 C027 C02D 162(2) . . . . ? C02K C029 O02B C14 1(5) . . . . ? C02L C021 C02F C02J 171(2) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -0.1435 -0.4079 23.7008 0.2320 0.9726 0.0145 -0.1052 2.4112 -20.0348 0.1793 -0.9556 -0.2336 0.2331 0.9488 -23.2399 -0.1289 -0.9911 -0.0324 0.0573 -0.9399 23.2145 0.1280 0.9858 0.1090 0.8016 -1.8341 20.4271 -0.0753 0.9242 0.3745 -0.1390 4.6861 4.7831 0.9099 -0.1171 -0.3980 -0.2330 -3.3053 17.1046 -0.3760 0.9024 0.2106 -3.9358 -0.9947 2.5926 -0.1162 0.2198 -0.9686 -0.0802 0.4039 -23.7172 -0.2312 -0.9701 -0.0738 -0.2212 3.5344 -14.8762 0.4496 -0.8229 -0.3475 -0.3905 -4.7257 6.7122 -0.7652 0.5843 0.2702 0.4021 4.9840 2.8199 0.9344 -0.2219 -0.2788 -0.1528 -4.8813 -2.6840 -0.9160 0.2173 0.3373 0.2578 4.4966 -8.9642 0.6959 -0.6571 -0.2897 loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.192 0.252 0.404 53.2 7.9 ?