Crystallography Open Database

Information card for entry 1572210

Preview

Coordinates	1572210.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H46 N P Si2
Calculated formula	C24 H46 N P Si2
SMILES	p1(N(C2CCCCC2)C2CCCCC2)c([Si](C)(C)C)c(c(c1[Si](C)(C)C)C)C
Title of publication	Phospha-bicyclohexene-germylenes exhibiting unexpected reactivity.
Authors of publication	Würdemann, Marie Sophie; Kühn, Steffen; Bötel, Tobias; Schmidtmann, Marc; Müller, Thomas
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	35
Pages of publication	14161 - 14170
a	9.8664 ± 0.0004 Å
b	10.8301 ± 0.0005 Å
c	13.2382 ± 0.0005 Å
α	83.1135 ± 0.0016°
β	86.3992 ± 0.0016°
γ	69.5125 ± 0.0016°
Cell volume	1315.19 ± 0.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0428
Residual factor for significantly intense reflections	0.0345
Weighted residual factors for significantly intense reflections	0.0824
Weighted residual factors for all reflections included in the refinement	0.0862
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
295192 (current)	2024-10-06	cif/ Updating files of 1572207, 1572208, 1572209, 1572210, 1572211, 1572212, 1572213 Original log message: Adding full bibliography for 1572207--1572213.cif.	1572210.cif
293598	2024-07-31	cif/ Adding structures of 1572207, 1572208, 1572209, 1572210, 1572211, 1572212, 1572213 via cif-deposit CGI script.	1572210.cif