Crystallography Open Database

Information card for entry 1572508

Preview

Coordinates	1572508.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Ruthenium MACHO-(N-phenylformamide)
Chemical name	carbonyl-hydrido-(bis(2-(diphenylphosphino)ethyl)amine)-(N-phenylformamide)-ruthenium
Formula	C36 H36 N2 O2 P2 Ru
Calculated formula	C36 H36 N2 O2 P2 Ru
Title of publication	Exploiting decarbonylation and dehydrogenation of formamides for the synthesis of ureas, polyureas, and poly(urea-urethanes).
Authors of publication	Luk, James; Goodfellow, Alister S.; More, Nachiket Deepak; Bühl, Michael; Kumar, Amit
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	40
Pages of publication	16594 - 16604
a	9.3455 ± 0.0003 Å
b	12.358 ± 0.0003 Å
c	14.8848 ± 0.0003 Å
α	108.452 ± 0.002°
β	92.03 ± 0.002°
γ	97.599 ± 0.002°
Cell volume	1610.9 ± 0.08 Å³
Cell temperature	173.15 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.085
Residual factor for significantly intense reflections	0.0522
Weighted residual factors for significantly intense reflections	0.0942
Weighted residual factors for all reflections included in the refinement	0.1017
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
296424 (current)	2024-12-06	cif/ Updating files of 1572508, 1572509 Original log message: Adding full bibliography for 1572508--1572509.cif.	1572508.cif
294396	2024-09-06	cif/ Adding structures of 1572508, 1572509 via cif-deposit CGI script.	1572508.cif