#------------------------------------------------------------------------------ #$Date: 2024-09-06 11:49:32 +0300 (Fri, 06 Sep 2024) $ #$Revision: 294648 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/25/1572510.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572510 loop_ _publ_author_name 'Bojarska, Joanna' '\/Lyczko, Krzysztof' 'Breza, Martin' 'Mieczkowski, Adam' _publ_section_title ; Recurrent Supramolecular Patterns in a Series of Salts of Heterocyclic Polyamines and Heterocyclic Dicarboxylic Acids: Synthesis, Single-Crystal X-ray Structure, Hirshfeld Surface Analysis, Energy Framework, and Quantum Chemical Calculations ; _journal_issue 8 _journal_name_full Crystals _journal_page_first 733 _journal_paper_doi 10.3390/cryst14080733 _journal_volume 14 _journal_year 2024 _chemical_formula_moiety 'C6 H3 N2 O4, C4 H7 N4, H2 O' _chemical_formula_sum 'C10 H12 N6 O5' _chemical_formula_weight 296.26 _chemical_name_systematic ' 2,4-diaminopyrimidin-1-ium 3-carboxypyrazine-2-carboxylate monohydrate' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_date 2024-06-12 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _cell_angle_alpha 90 _cell_angle_beta 92.4078(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.54619(5) _cell_length_b 12.52881(9) _cell_length_c 15.12082(15) _cell_measurement_reflns_used 22894 _cell_measurement_temperature 100.0(1) _cell_measurement_theta_max 69.6720 _cell_measurement_theta_min 4.5550 _cell_volume 1239.054(18) _computing_cell_refinement 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2017/1 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.0(1) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.0131 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -32.00 42.00 1.00 1.00 -- 0.00 77.00-150.00 74 2 \w -21.00 32.00 1.00 1.00 -- 0.00 -77.00 0.00 53 3 \w -22.00 69.00 1.00 1.00 -- 0.00 57.00 -30.00 91 4 \w -21.00 32.00 1.00 1.00 -- 0.00 -77.00-120.00 53 5 \w 30.00 122.00 1.00 1.75 -- 54.00 62.00 -48.31 92 6 \w 25.00 124.00 1.00 1.75 -- 54.00 72.00 74.76 99 7 \w 26.00 124.00 1.00 1.75 -- 54.00 70.00 179.45 98 8 \w 32.00 123.00 1.00 1.75 -- 54.00 57.00-180.00 91 9 \w 32.00 123.00 1.00 1.75 -- 54.00 57.00 -60.00 91 10 \w 6.00 98.00 1.00 1.75 -- 54.00 -99.00 120.00 92 11 \w 25.00 124.00 1.00 1.75 -- 54.00 72.00 116.94 99 12 \w 32.00 123.00 1.00 1.75 -- 54.00 57.00 -90.00 91 13 \w -19.00 81.00 1.00 1.75 -- 54.00 -37.00 120.00 100 14 \w 32.00 123.00 1.00 1.75 -- 54.00 57.00-120.00 91 15 \w 26.00 124.00 1.00 1.75 -- 54.00 70.00 -26.63 98 16 \w -17.00 86.00 1.00 1.75 -- 54.00 -77.00 -60.00 103 17 \w 32.00 123.00 1.00 1.75 -- 54.00 57.00 30.00 91 18 \w -19.00 81.00 1.00 1.75 -- 54.00 -37.00 -30.00 100 19 \w 26.00 124.00 1.00 1.75 -- 54.00 70.00 36.40 98 20 \w -17.00 86.00 1.00 1.75 -- 54.00 -77.00 -90.00 103 21 \w 35.00 109.00 1.00 2.50 -- 108.00-111.00 -60.00 74 22 \w 80.00 178.00 1.00 2.50 -- 108.00 71.00 10.79 98 23 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00 0.00 93 24 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00-180.00 91 25 \w 86.00 177.00 1.00 2.50 -- 108.00 59.00 -77.96 91 26 \w 35.00 106.00 1.00 2.50 -- 108.00 -91.00 150.00 71 27 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00-120.00 93 28 \w 83.00 176.00 1.00 2.50 -- 108.00 65.00-145.59 93 29 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 90.00 91 30 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 -90.00 91 31 \w 81.00 178.00 1.00 2.50 -- 108.00 69.00-115.45 97 32 \w 35.00 135.00 1.00 2.50 -- 108.00 -37.00 -90.00 100 33 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00-180.00 93 34 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00 90.00 93 35 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 0.00 91 36 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00 -30.00 93 37 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00-120.00 91 38 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 -30.00 91 39 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00-150.00 93 40 \w 41.00 132.00 1.00 2.50 -- 108.00 -63.00-180.00 91 41 \w 77.00 178.00 1.00 2.50 -- 108.00 33.00 -59.45 101 42 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 60.00 91 43 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00 120.00 93 44 \w 35.00 109.00 1.00 2.50 -- 108.00-111.00 60.00 74 45 \w 35.00 109.00 1.00 2.50 -- 108.00-111.00-150.00 74 46 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 30.00 91 47 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 150.00 91 48 \w 84.00 178.00 1.00 2.50 -- 108.00 46.00 149.00 94 49 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00-150.00 91 50 \w 35.00 106.00 1.00 2.50 -- 108.00 -91.00 -30.00 71 51 \w 35.00 106.00 1.00 2.50 -- 108.00 -91.00 90.00 71 52 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00 60.00 93 53 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 -60.00 91 54 \w 85.00 178.00 1.00 2.50 -- 108.00 50.00 -60.00 93 55 \w 81.00 178.00 1.00 2.50 -- 108.00 37.00-180.00 97 56 \w 84.00 175.00 1.00 2.50 -- 108.00 63.00 120.00 91 57 \w -74.00 74.00 1.00 1.00 -- 0.00 0.00-180.00 148 58 \w -73.00 27.00 1.00 1.00 -- 0.00 -37.00 150.00 100 59 \w -74.00 74.00 1.00 1.00 -- 0.00 0.00-120.00 148 60 \w -74.00 74.00 1.00 1.00 -- 0.00 0.00-150.00 148 61 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 -90.00 148 62 \w 28.00 123.00 1.00 1.75 -- 54.00 66.00 116.97 95 63 \w 32.00 124.00 1.00 1.75 -- 54.00 54.00 -89.77 92 64 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00-150.00 148 65 \w 32.00 123.00 1.00 1.75 -- 54.00 57.00 -30.00 91 66 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00-120.00 148 67 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00-180.00 148 68 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 -60.00 148 69 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 -30.00 148 70 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 0.00 148 71 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 60.00 148 72 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 30.00 148 73 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 90.00 148 74 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 120.00 148 75 \w -20.00 128.00 1.00 1.75 -- 54.00 0.00 150.00 148 76 \w -20.00 112.00 1.00 1.75 -- 54.00 0.00-180.00 132 77 \w 27.00 112.00 1.00 1.75 -- 54.00-125.00-120.00 85 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.2078514000 _diffrn_orient_matrix_UB_12 0.0562211000 _diffrn_orient_matrix_UB_13 -0.0150766000 _diffrn_orient_matrix_UB_21 -0.0786710000 _diffrn_orient_matrix_UB_22 -0.0952871000 _diffrn_orient_matrix_UB_23 -0.0561354000 _diffrn_orient_matrix_UB_31 -0.0780383000 _diffrn_orient_matrix_UB_32 -0.0536677000 _diffrn_orient_matrix_UB_33 0.0837825000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0281 _diffrn_reflns_av_unetI/netI 0.0101 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 38635 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 69.591 _diffrn_reflns_theta_min 4.585 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.119 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.72297 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.84a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.588 _exptl_crystal_description block _exptl_crystal_F_000 616 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.04 _refine_diff_density_max 0.248 _refine_diff_density_min -0.231 _refine_diff_density_rms 0.042 _refine_ls_extinction_coef 0.0017(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2017/1 (Sheldrick 2017)' _refine_ls_goodness_of_fit_ref 1.101 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 215 _refine_ls_number_reflns 2315 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.102 _refine_ls_R_factor_all 0.0311 _refine_ls_R_factor_gt 0.0295 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0330P)^2^+0.7476P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0761 _refine_ls_wR_factor_ref 0.0773 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2182 _reflns_number_total 2315 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file structures_1-7.cif _cod_data_source_block k7a2 _cod_database_code 1572510 _shelx_shelxl_version_number 2017/1 _chemical_oxdiff_formula 'C10 H10 N6 O4' _chemical_oxdiff_usercomment 'colourless block, Cu, 100K, 0.20x0.14x0.07' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All O(H,H,H,H,H) groups At 1.5 times of: All O(H,H,H) groups 2. Restrained distances O4-H4 0.9 with sigma of 0.02 3.a Aromatic/amide H refined with riding coordinates: C3(H3), C9(H9), C4(H4A), C10(H10) ; _shelx_res_file ; TITL K-K7A2 in P21/n #14 k7a2.res created by SHELXL-2017/1 at 14:15:41 on 12-Jun-2024 REM reset to P21/n #14 CELL 1.54184 6.54619 12.52881 15.12082 90 92.4078 90 ZERR 4 0.00005 0.00009 0.00015 0 0.0008 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O UNIT 40 48 24 20 EQIV $1 1-X,2-Y,1-Z EQIV $2 1-X,1-Y,1-Z EQIV $3 1.5-X,0.5+Y,0.5-Z EQIV $4 0.5+X,1.5-Y,0.5+Z EQIV $5 0.5+X,1.5-Y,-0.5+Z EQIV $6 0.5-X,0.5+Y,0.5-Z EQIV $7 -X,1-Y,1-Z DFIX 0.9 O4 H4 L.S. 20 PLAN 1 TEMP -173 CONF HTAB C9 O4_$1 HTAB C9 N2_$1 HTAB N5 N1_$2 HTAB N6 O2_$3 HTAB N5 O3_$4 HTAB N6 O5_$2 HTAB N4 O5_$5 HTAB O4 O1_$6 HTAB O5 O2_$2 HTAB O5 O1_$7 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.033000 0.747600 EXTI 0.001750 FVAR 6.02856 O1 4 0.132335 0.496140 0.284483 11.00000 0.01666 0.01408 = 0.01593 -0.00345 0.00157 -0.00096 O3 4 0.287433 0.732163 0.255502 11.00000 0.03124 0.01381 = 0.01151 -0.00063 0.00338 -0.00102 O2 4 0.473165 0.509503 0.300575 11.00000 0.01594 0.01519 = 0.01948 -0.00286 0.00538 0.00145 O4 4 0.324427 0.874176 0.345437 11.00000 0.02208 0.00992 = 0.01340 0.00021 0.00181 -0.00116 N1 3 0.238834 0.534955 0.477029 11.00000 0.01400 0.01376 = 0.01395 0.00133 0.00207 -0.00054 N2 3 0.249627 0.757864 0.487248 11.00000 0.01312 0.01416 = 0.01287 -0.00150 0.00100 0.00008 N6 3 0.820208 0.837993 0.292222 11.00000 0.02162 0.01154 = 0.01390 0.00006 0.00485 -0.00225 N4 3 0.780060 0.954081 0.408707 11.00000 0.01624 0.01057 = 0.01475 0.00126 0.00200 -0.00053 C5 1 0.296600 0.530722 0.321792 11.00000 0.01730 0.00713 = 0.01346 0.00317 0.00355 0.00055 C1 1 0.268898 0.595397 0.405248 11.00000 0.00890 0.01314 = 0.01341 0.00042 0.00126 -0.00034 N3 3 0.767987 0.767540 0.429934 11.00000 0.01367 0.01199 = 0.01376 -0.00022 0.00191 -0.00014 C8 1 0.789634 0.852129 0.378095 11.00000 0.00939 0.01278 = 0.01576 -0.00044 0.00067 -0.00024 C2 1 0.272531 0.706417 0.410445 11.00000 0.00988 0.01289 = 0.01303 -0.00070 0.00119 0.00042 C6 1 0.296616 0.772818 0.328949 11.00000 0.01170 0.01167 = 0.01432 -0.00024 0.00132 0.00086 N5 3 0.729569 0.700418 0.568903 11.00000 0.02181 0.01244 = 0.01272 0.00037 0.00280 0.00064 C3 1 0.219553 0.697315 0.557918 11.00000 0.01527 0.01808 = 0.01097 -0.00145 0.00173 0.00018 AFIX 43 H3 2 0.202217 0.730816 0.613464 11.00000 -1.20000 AFIX 0 C9 1 0.754019 0.972873 0.496512 11.00000 0.01352 0.01327 = 0.01783 -0.00334 0.00135 -0.00044 AFIX 43 H9 2 0.746114 1.044079 0.517690 11.00000 -1.20000 AFIX 0 C4 1 0.212760 0.586562 0.552859 11.00000 0.01495 0.01749 = 0.01231 0.00202 0.00193 -0.00061 AFIX 43 H4A 2 0.188909 0.546584 0.604805 11.00000 -1.20000 AFIX 0 C7 1 0.745124 0.785107 0.516909 11.00000 0.00887 0.01523 = 0.01500 0.00013 0.00156 0.00022 C10 1 0.739548 0.890360 0.553071 11.00000 0.01643 0.01631 = 0.01384 -0.00254 0.00235 0.00011 AFIX 43 H10 2 0.726143 0.901751 0.614671 11.00000 -1.20000 AFIX 0 O5 4 0.208373 0.385073 0.773157 11.00000 0.01718 0.01656 = 0.01732 0.00034 0.00386 0.00061 H5A 2 0.739574 0.634483 0.545905 11.00000 -1.20000 H6A 2 0.873527 0.889935 0.263630 11.00000 -1.20000 H5B 2 0.734001 0.710872 0.626489 11.00000 -1.20000 H6B 2 0.826916 0.770357 0.272709 11.00000 -1.20000 H4B 2 0.774963 1.008145 0.370867 11.00000 -1.20000 H4 2 0.334374 0.915921 0.293581 11.00000 -1.50000 H5C 2 0.308358 0.404361 0.738364 11.00000 -1.50000 H5D 2 0.102471 0.415482 0.748348 11.00000 -1.50000 HKLF 4 REM K-K7A2 in P21/n #14 REM R1 = 0.0295 for 2182 Fo > 4sig(Fo) and 0.0311 for all 2315 data REM 215 parameters refined using 1 restraints END WGHT 0.0330 0.7476 REM Highest difference peak 0.248, deepest hole -0.231, 1-sigma level 0.042 Q1 1 0.2661 0.6521 0.4015 11.00000 0.05 0.25 ; _shelx_res_checksum 91114 _shelx_hkl_file ; 0 0 1 20.0847 21.4817 1 0 0 -1 7.24136 22.7155 4 0 0 -1-2.17173 19.3056 58 0 0 1-2.83866 15.1471 57 0 0 -1 18.6097 14.7544 57 0 0 -1 8.78988 14.0854 60 0 0 1-5.44040 14.3292 60 0 0 1-7.79668 15.2718 59 0 0 2 25768.2 585.957 1 0 0 2 26959.6 525.890 2 0 0 -2 27411.6 590.136 1 0 0 -2 25497.1 601.219 4 0 0 -2 26441.9 523.394 2 0 0 -2 26359.2 542.907 60 0 0 -2 26601.3 543.601 57 0 0 2 26510.8 546.100 59 0 0 2 26329.1 542.968 60 0 0 2 25904.4 542.559 57 0 0 -2 25905.1 583.703 58 0 0 -3-19.4044 50.2453 1 0 0 -3 41.3797 37.0300 2 0 0 3 52.7239 62.1826 1 0 0 -3 8.51731 60.9436 4 0 0 -3 69.0507 44.2419 60 0 0 3 22.2413 41.0540 57 0 0 3-2.32773 38.1194 60 0 0 -3 48.8356 42.8243 57 0 0 -3 6.55099 54.6568 58 0 0 3 19.6629 40.3955 59 0 0 4 196477. 3760.04 1 0 0 4 199869. 3687.93 10 0 0 -4 207651. 3755.02 1 0 0 4 204283. 3652.95 20 0 0 -4 210997. 3797.26 3 0 0 -4 206706. 3814.35 4 0 0 4 222317. 3647.51 77 0 0 -4 202617. 3640.33 57 0 0 -4 207065. 3644.39 60 0 0 -4 198197. 3742.54 58 0 0 4 194461. 3646.52 60 0 0 4 195229. 3653.21 57 0 0 4 198193. 3653.66 59 0 0 5 44.4842 67.5279 1 0 0 5-48.2335 55.6073 16 0 0 -5-47.7145 80.5053 4 0 0 5-6.70425 70.5757 10 0 0 -5 1.73791 47.6116 14 0 0 5 18.1667 55.4830 20 0 0 5 14.1047 48.0921 13 0 0 -5-17.7835 58.9296 3 0 0 5 16.3276 77.3575 4 0 0 -5-24.5857 52.0456 1 0 0 5 15.3682 56.0760 77 0 0 -5 11.0650 74.2019 58 0 0 -5 34.0819 46.6747 57 0 0 5 27.2562 51.5364 59 0 0 -5 8.09869 43.6022 60 0 0 5-3.30525 44.5232 57 0 0 5 13.9272 47.2582 60 0 0 6 57031.0 1292.99 20 0 0 6 59304.0 1255.66 16 0 0 6 56860.3 1248.94 13 0 0 -6 54238.9 1382.57 1 0 0 6 57875.0 1350.47 10 0 0 6 58343.8 1453.95 1 0 0 -6 55770.1 1220.55 14 0 0 6 64200.7 1298.71 77 0 0 -6 60627.4 1258.21 63 0 0 6 59209.6 1294.82 59 0 0 6 59019.6 1264.11 59 0 0 -6 57639.1 1409.41 58 0 0 -6 57006.0 1250.32 57 0 0 6 59684.2 1297.99 57 0 0 6 59306.0 1289.54 60 0 0 7-17.8598 79.1555 10 0 0 7 73.8650 52.7172 13 0 0 -7 23.3716 62.3040 12 0 0 7-10.1973 68.8169 20 0 0 7-1.16914 59.9227 16 0 0 -7-4.54807 60.4834 14 0 0 7-38.4804 67.6858 77 0 0 -7 171.909 75.0848 63 0 0 -8 14152.4 490.541 14 0 0 -8 14080.9 524.234 12 0 0 8 14353.6 520.695 16 0 0 8 13522.5 512.658 13 0 0 8 14192.2 606.647 10 0 0 8 14289.8 563.527 20 0 0 8 15981.7 558.124 77 0 0 -8 14698.8 522.022 63 0 0 9-14.7246 77.3422 20 0 0 -9-6.92115 69.3672 12 0 0 -9 7.64647 55.1810 14 0 0 9-19.7259 60.7866 77 0 0 -9-30.1300 67.3270 63 0 0 -10 10181.1 490.826 12 0 0 10 10213.4 530.656 20 0 0 10 10518.4 498.000 77 0 0 -10 10069.4 478.072 63 0 0 -11 93.0478 92.4169 12 0 0 11-21.0659 80.0442 20 0 0 11 164.807 89.3654 77 0 0 -11 67.4265 71.0947 63 0 0 -12 12495.0 628.697 9 0 0 12 10904.5 532.079 21 0 0 12 12737.5 659.257 20 0 0 12 10931.9 556.604 22 0 0 -12 11863.4 588.711 12 0 0 12 10739.0 575.022 26 0 0 12 11653.5 556.963 40 0 0 -12 11113.9 562.741 63 0 0 -13 16.8530 94.6575 9 0 0 13-11.7258 104.885 20 0 0 13-316.812 117.738 22 0 0 13-39.2243 78.2734 21 0 0 13-36.5562 79.4132 40 0 0 13-55.0685 124.591 26 0 0 14 12587.1 592.669 21 0 0 14 12596.3 618.271 22 0 0 14 11711.7 633.333 26 0 0 14 12149.7 592.774 40 0 0 15 39.8842 92.7752 21 0 0 15-59.2360 91.4870 40 0 0 16 173.637 96.4910 21 0 0 16 105.779 86.7807 40 0 0 17-129.695 76.2316 21 0 0 17-56.5390 78.3391 40 0 0 18 4790.79 253.052 21 0 0 18 5038.45 265.456 40 0 1 0 17.4700 17.7420 3 0 -1 0 12.4216 16.7458 3 0 -1 0-7.07635 25.9788 60 0 -1 0-6.77260 26.7053 57 0 -1 0-3.53471 25.9866 59 0 1 -1 305.193 34.9900 4 0 1 1 347.125 44.5912 4 0 -1 -1 272.512 42.9109 3 0 -1 1 306.132 34.6676 4 0 -1 -1 263.337 39.6967 4 0 1 1 337.373 49.3181 3 0 -1 1 318.846 55.0667 1 0 1 -1 288.607 32.0909 60 0 -1 1 305.365 41.2815 58 0 -1 -1 252.352 49.7421 60 0 -1 1 261.696 32.3674 60 0 -1 -1 307.093 53.0207 57 0 -1 -1 303.671 53.7770 59 0 1 -1 295.440 31.3597 59 0 1 -1 259.015 31.1295 57 0 1 -1 434.494 44.1130 58 0 -1 1 277.817 34.7642 57 0 -1 1 274.031 33.3809 59 0 -1 -2 158520. 2823.41 3 0 1 -2 157348. 2785.15 4 0 -1 2 153413. 2786.78 4 0 1 2 160246. 2824.12 3 0 -1 -2 151354. 2809.47 4 0 1 2 158819. 2820.11 4 0 -1 2 154031. 2846.47 1 0 1 2 151369. 2814.13 57 0 1 -2 149922. 2762.63 58 0 -1 -2 154907. 2807.75 57 0 1 2 150948. 2810.74 59 0 1 2 153523. 2810.82 60 0 -1 2 154350. 2686.70 59 0 -1 2 157364. 2775.52 58 0 -1 2 153311. 2693.10 57 0 -1 -2 154379. 2804.94 60 0 -1 2 155426. 2688.46 60 0 1 -2 158692. 2688.61 59 0 -1 -2 152072. 2806.46 59 0 1 3 2538.86 177.086 3 0 1 3 2706.91 163.719 1 0 -1 3 2356.78 176.919 1 0 1 -3 2256.62 168.021 1 0 1 -3 2448.80 146.389 2 0 -1 -3 2395.40 171.076 4 0 -1 3 2634.30 170.207 4 0 1 -3 2353.88 161.243 4 0 1 3 2496.38 172.810 4 0 -1 3 2362.52 101.449 59 0 -1 -3 2441.27 158.075 59 0 -1 3 2425.52 106.080 57 0 -1 -3 2441.25 155.349 60 0 1 3 2449.39 159.297 60 0 -1 3 2475.24 154.272 58 0 -1 3 2466.46 106.835 60 0 -1 3 2650.35 107.776 60 0 1 -3 2555.56 155.522 58 0 1 3 2425.54 158.057 59 0 -1 -3 2443.27 154.808 57 0 1 3 2488.21 164.667 57 0 1 4 110680. 2114.10 1 0 1 4 102506. 2015.09 6 0 -1 4 106089. 1985.98 20 0 -1 4 108880. 2156.97 4 0 1 4 110954. 1952.98 2 0 -1 4 104616. 2168.49 1 0 1 -4 105225. 2135.65 4 0 -1 -4 103553. 2160.10 4 0 -1 -4 104771. 1997.63 12 0 1 -4 108358. 2157.32 1 0 1 4 105040. 2020.39 16 0 1 -4 102445. 2021.40 2 0 1 -4 110797. 2133.28 3 0 -1 -4 106901. 1972.07 14 0 1 4 97003.1 1991.49 13 0 -1 4 112688. 2025.46 77 0 -1 4 107686. 1948.56 59 0 1 -4 106075. 2085.05 58 0 1 4 106229. 2091.71 60 0 -1 -4 103977. 2075.65 60 0 -1 -4 110975. 1999.37 63 0 1 4 104909. 2092.78 59 0 -1 4 106216. 1942.59 60 0 -1 -4 105576. 2080.86 57 0 -1 4 105349. 1933.74 59 0 -1 4 106813. 1943.33 57 0 1 4 106079. 2097.11 57 0 1 5 30234.1 892.627 4 0 1 5 28821.2 628.588 2 0 1 5 28614.4 732.876 20 0 1 -5 28397.5 832.943 1 0 -1 5 27886.3 742.375 10 0 -1 -5 27175.0 849.621 4 0 1 -5 27759.6 705.283 2 0 -1 5 29332.7 862.384 4 0 1 -5 29354.1 831.047 3 0 -1 -5 27354.3 837.644 3 0 -1 5 28089.2 857.408 1 0 -1 5 27822.9 655.486 16 0 -1 -5 28153.9 700.433 12 0 1 5 28736.0 718.314 6 0 1 -5 29375.8 850.147 4 0 1 5 29677.8 728.458 16 0 -1 -5 28905.1 676.843 14 0 -1 5 28033.2 696.947 20 0 -1 5 28890.7 686.709 13 0 1 -5 28654.2 669.610 7 0 1 5 29514.3 813.753 1 0 1 5 27872.8 674.239 75 0 -1 -5 28075.7 646.563 68 0 1 5 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348.241 18 1 3 2 9343.74 334.383 11 1 -3 2 9851.26 351.424 5 -1 -3 -2 9936.90 350.417 3 1 3 2 10197.1 354.248 19 1 -3 2 10172.0 331.255 10 -1 3 -2 9637.26 361.974 7 1 3 2 9604.79 358.240 6 -1 -3 -2 9470.11 346.567 14 1 -3 2 9391.90 434.723 1 -1 3 -2 9449.99 429.387 1 1 3 2 9752.62 379.225 4 -1 3 -2 9936.52 366.488 8 1 -3 2 9518.64 337.584 13 -1 -3 -2 9907.09 307.429 9 1 -3 2 9541.83 337.345 15 -1 3 -2 9381.59 333.514 11 -1 -3 -2 9835.13 335.618 12 1 3 2 9393.12 341.305 17 1 3 2 9285.27 357.161 71 -1 3 -2 9744.36 313.621 66 1 -3 2 10288.7 320.970 72 1 3 2 9155.22 353.834 73 1 -3 2 10264.4 319.214 71 -1 3 -2 9506.86 312.865 64 -1 3 -2 9822.50 317.406 67 -1 -3 -2 9965.55 337.712 68 1 -3 2 10031.8 314.878 73 1 -3 2 10084.7 320.058 70 1 3 2 9725.73 352.670 67 1 3 2 9518.18 350.304 76 1 3 2 9714.20 355.953 74 -1 3 -2 10039.7 327.705 75 1 -3 2 9549.35 337.574 65 -1 -3 -2 9952.78 336.900 69 -1 3 -2 9723.22 316.722 76 -1 -3 -2 10490.9 342.126 63 -1 -3 -2 10051.7 339.934 70 1 3 2 9318.58 347.184 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66 -1 -3 -3-50.7059 64.2467 70 1 3 3 37.2021 66.5072 71 1 -3 3-5.81187 45.3667 72 1 -3 3-21.3849 46.8338 71 1 3 3-22.4192 62.1367 74 -1 -3 -3 82.8925 58.0566 68 1 -3 3 38.0067 44.5580 73 -1 -3 -3 82.7102 64.6106 69 1 3 3-14.1850 63.7341 67 1 3 3-22.2998 61.7557 73 -1 3 -3 37.9411 47.3030 64 1 3 3 22.8291 61.3610 76 1 -3 3 8.97602 44.3533 74 -1 3 -3 0.77252 40.1880 68 1 -3 3 16.5577 53.2308 65 -1 3 -3 90.4112 51.8126 67 -1 3 -3-14.1548 43.3425 66 -1 3 -3 12.6388 45.0154 76 1 -3 3 25.5610 47.4997 70 1 3 3 33.2760 67.3647 75 -1 -3 -3 44.6383 70.3226 60 -1 3 -3-44.5814 80.0244 58 1 -3 3-9.36137 57.0028 60 1 3 3 44.0841 61.7048 60 -1 -3 -3 14.9378 69.8670 57 -1 -3 -3 46.0051 62.4919 63 1 -3 3 32.0847 69.1190 58 -1 3 -3 12.9406 41.2403 62 1 3 3 21.5083 73.4763 59 1 3 3-51.6750 80.5557 57 1 3 3 243.860 68.8503 62 -1 3 -3 12.0898 51.3959 59 1 -3 3-47.5963 61.0984 57 -1 -3 -3-39.9669 60.6214 61 -1 3 -3-15.5777 43.8298 61 1 -3 3 25.9199 61.6648 59 1 3 4 20.1125 67.3345 19 -1 -3 -4 95.4976 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63.7094 60 -1 -3 -4 78.7197 61.2292 61 -1 3 -4 60.8906 48.1448 61 1 -3 5 2579.22 201.983 13 -1 -3 -5 2961.97 214.603 14 1 -3 5 2760.16 220.260 10 1 -3 5 2457.89 228.770 4 1 3 5 2515.19 218.648 19 -1 3 -5 2464.88 196.521 8 -1 -3 -5 2355.88 195.371 12 1 3 5 2406.09 203.749 6 -1 -3 -5 2630.26 194.222 9 -1 -3 -5 2660.96 178.728 18 -1 3 -5 2230.90 194.710 7 -1 -3 -5 2454.38 190.074 69 -1 3 -5 2541.58 151.869 68 -1 -3 -5 2465.01 187.270 72 -1 -3 -5 2344.32 187.302 68 1 3 5 2548.71 215.435 74 -1 3 -5 2519.34 155.546 64 1 3 5 2540.57 205.349 67 1 3 5 2644.15 213.316 75 -1 3 -5 2324.70 147.186 66 1 3 5 2374.98 198.371 64 -1 -3 -5 2571.26 193.786 70 1 -3 5 2696.40 206.445 77 1 3 5 2541.86 215.042 73 1 3 5 2493.87 205.146 76 -1 -3 -5 2594.90 195.410 61 -1 -3 -5 2660.90 201.068 63 -1 3 -5 2511.04 151.286 61 1 3 6 307.191 110.646 20 -1 -3 -6 327.207 100.195 14 -1 -3 -6 331.124 107.350 12 -1 3 -6 307.830 95.1007 8 1 -3 6 258.433 100.982 10 1 3 6 357.381 103.103 6 -1 -3 -6 393.766 94.8887 9 1 3 6 203.857 99.6418 19 -1 3 -6 300.151 104.852 7 1 -3 6 348.263 110.838 13 -1 -3 -6 473.298 101.963 72 1 3 6 348.216 102.360 76 1 3 6 286.337 99.3810 75 1 -3 6 343.950 108.104 77 -1 -3 -6 208.208 75.5539 70 -1 -3 -6 293.531 87.7582 68 1 3 6 401.869 96.6294 64 1 3 6 263.333 95.3046 74 -1 -3 -6 288.179 88.0849 69 1 3 6 327.661 96.9159 67 1 3 6 223.543 85.7833 73 -1 -3 -6 332.664 98.1658 63 -1 -3 -6 282.672 89.7698 61 -1 3 -7 940.236 132.800 8 1 3 7 891.010 151.994 19 1 -3 7 823.595 134.716 13 -1 3 -7 1115.78 156.358 7 -1 -3 -7 923.880 147.401 14 -1 -3 -7 1051.72 155.780 9 1 -3 7 1190.67 178.792 10 1 3 7 1091.66 166.531 20 1 3 7 1004.22 155.231 6 -1 -3 -7 1085.70 160.398 12 -1 -3 -7 918.777 137.289 69 1 3 7 896.126 152.824 74 1 3 7 788.621 147.041 73 -1 -3 -7 795.578 124.284 70 1 3 7 756.909 140.958 67 1 3 7 971.375 154.330 76 1 3 7 1073.65 158.952 64 1 -3 7 1467.59 187.748 77 -1 -3 -7 1291.52 157.242 68 1 3 7 708.420 138.960 75 -1 -3 -7 1115.45 143.138 72 -1 -3 -7 947.754 145.112 63 -1 -3 -7 1045.04 140.663 61 1 3 8 126903. 2719.10 16 -1 -3 -8 127030. 2700.78 12 -1 3 -8 125698. 2643.76 7 1 3 8 129447. 2712.44 6 -1 -3 -8 124888. 2681.56 9 -1 -3 -8 127248. 2673.86 14 1 -3 8 132751. 2826.19 10 1 -3 8 129080. 2709.53 13 1 3 8 126446. 2759.12 20 -1 -3 -8 126910. 2613.81 72 1 3 8 125409. 2696.19 64 -1 -3 -8 126688. 2617.79 69 1 3 8 128203. 2708.67 76 1 3 8 123646. 2735.04 73 1 3 8 124955. 2698.10 67 1 3 8 124420. 2719.57 74 1 3 8 127064. 2712.32 75 -1 -3 -8 125070. 2612.91 70 -1 -3 -8 127423. 2618.31 68 -1 -3 -8 131615. 2701.42 63 -1 -3 -8 124125. 2609.27 61 1 -3 9 13508.6 674.184 10 -1 -3 -9 13328.6 602.727 9 -1 -3 -9 13206.3 603.327 12 1 3 9 14165.2 628.264 16 -1 3 -9 13300.6 583.776 14 -1 -3 -9 13607.3 592.765 14 1 3 9 13822.6 653.487 20 1 -3 9 13928.3 621.492 13 -1 -3 -9 13798.8 561.136 69 1 3 9 12695.3 614.666 73 -1 -3 -9 13598.5 557.084 72 1 3 9 13329.2 603.657 67 1 3 9 12530.3 594.452 75 1 -3 9 15146.6 663.590 77 1 3 9 13821.0 612.177 64 -1 -3 -9 13824.6 562.171 70 -1 -3 -9 13864.4 564.500 68 1 3 9 13465.2 606.950 76 1 3 9 13331.7 619.958 74 -1 -3 -9 13602.2 605.147 63 -1 -3 -9 13756.0 561.431 61 -1 -3 -10 5.31461 83.5746 9 -1 -3 -10-3.54019 72.6824 12 1 -3 10 92.5083 107.411 10 1 -3 10 109.756 91.9838 13 -1 -3 -10 55.7540 81.0180 14 1 3 10-95.7225 84.8836 16 1 3 10-77.2598 92.1093 20 -1 3 -10 85.5342 70.2056 14 1 -3 10-18.5886 85.7650 77 -1 -3 -10 30.8217 76.6358 63 1 -3 11 5767.89 382.170 40 1 3 11 5998.90 410.946 35 1 -3 11 5795.97 400.744 26 1 -3 11 5137.30 368.238 38 1 3 11 5346.20 358.643 40 1 3 11 6025.41 464.221 20 -1 -3 -11 5120.15 380.146 14 -1 3 -11 5548.85 387.191 14 1 3 11 5221.68 384.762 22 -1 -3 -11 5263.83 407.071 12 -1 -3 -11 5138.10 402.727 9 1 -3 11 5710.72 442.869 77 1 -3 11 6592.70 469.430 51 -1 -3 -11 5153.60 398.429 63 1 3 11 5530.48 403.499 46 1 -3 11 5706.40 360.875 45 1 -3 12 2015.68 254.538 26 1 -3 12 1950.49 236.853 40 1 3 12 1928.47 232.395 40 1 3 12 2233.59 258.883 35 -1 -3 -12 1988.90 266.426 12 1 3 12 1884.59 275.818 20 -1 -3 -12 1668.05 247.479 9 1 3 12 2147.90 266.017 22 -1 -3 -12 1416.97 226.108 5 -1 3 -12 2103.14 254.214 12 -1 3 -12 1842.34 227.494 14 1 -3 12 2432.81 295.584 77 1 3 12 2151.01 272.419 46 1 -3 12 1900.94 219.283 45 -1 -3 -12 2042.26 260.419 63 -1 3 -12 2212.23 252.355 63 1 3 13 116.452 99.6758 22 -1 -3 -13 155.533 89.9844 37 1 -3 13 135.037 104.389 26 1 -3 13 65.1049 91.3295 40 1 3 13 245.342 121.370 40 1 3 13 182.318 124.750 46 1 -3 13 239.891 104.478 45 1 3 14 8545.87 509.615 22 1 3 14 7887.68 462.456 21 1 3 14 7714.01 463.240 40 1 -3 14 8128.04 497.225 26 1 -3 14 7857.52 464.781 40 1 -3 14 7943.52 439.827 45 1 3 14 7786.14 497.455 46 1 3 15 201.568 117.417 22 1 3 15 159.438 102.357 21 1 -3 15 193.408 83.8480 40 1 -3 15 301.002 128.390 26 1 3 15 250.953 117.627 40 -1 -3 -15 269.657 99.3921 31 1 3 15 157.649 108.701 46 1 -3 15 271.380 91.0402 45 1 3 16 989.947 151.272 21 1 -3 16 904.564 137.065 40 -1 -3 -16 1020.94 139.722 31 1 3 16 1283.31 177.263 40 1 -3 16 1071.66 171.780 26 1 -3 16 999.344 134.030 45 1 3 17 1967.33 175.903 21 1 -3 17 1848.69 168.755 40 1 3 17 2010.92 184.674 40 -1 4 17 5955.24 300.899 21 -1 4 17 5294.19 295.354 40 -1 -4 17 5632.29 297.208 45 -1 4 16 61.3246 66.8257 21 -1 -4 16 1.57913 60.1399 21 -1 -4 16 1.13108 81.5467 26 -1 4 16-56.5064 72.6064 40 -1 -4 16 35.2816 73.9388 45 -1 -4 15 2352.96 227.167 21 -1 4 15 2015.07 216.952 21 -1 4 15 2158.72 234.679 40 -1 -4 15 2074.48 246.619 26 -1 -4 15 2519.86 245.786 45 -1 4 15 2349.53 247.203 42 -1 -4 14 2927.78 266.180 21 -1 4 14 3220.88 284.397 21 -1 4 14 2773.62 273.015 40 -1 -4 14 2567.54 288.380 26 -1 -4 14 3123.52 286.284 45 -1 4 14 3274.37 300.004 52 -1 4 14 2953.27 289.671 42 -1 4 13 131.742 98.4161 21 -1 -4 13 108.571 96.3237 21 -1 4 13 54.3336 96.3174 40 -1 -4 13 225.346 107.232 26 -1 4 13 119.690 93.4602 42 -1 4 13 175.043 110.734 52 -1 -4 13 211.680 119.869 45 -1 4 12 6071.04 404.476 40 -1 -4 12 6435.49 441.152 26 1 -4 -12 7036.75 474.293 15 1 -4 -12 5600.84 449.034 5 -1 4 12 6573.92 502.384 20 1 -4 -12 5719.28 445.742 9 -1 -4 12 6122.13 511.738 10 -1 4 12 6320.34 484.814 16 -1 -4 12 5685.76 373.078 21 -1 4 12 5582.37 375.081 21 -1 -4 12 6934.60 495.790 77 1 -4 -12 6034.70 445.867 65 -1 4 12 6051.88 424.167 52 -1 -4 12 5916.95 396.107 45 -1 -4 12 5464.28 397.728 51 -1 4 12 6183.11 428.924 42 -1 4 12 6447.20 445.086 46 -1 -4 12 7631.96 493.380 44 -1 -4 11 55785.7 1543.75 26 -1 4 11 56638.5 1493.47 40 -1 4 11 59544.8 1694.58 16 -1 4 11 58505.2 1695.93 20 1 -4 -11 61445.3 1628.20 15 -1 4 11 55818.6 1451.68 21 1 -4 -11 58354.0 1655.38 5 1 -4 -11 58641.8 1637.55 9 -1 -4 11 58012.9 1768.56 10 -1 -4 11 55364.2 1443.82 21 1 -4 -11 57130.8 1599.60 65 -1 -4 11 62483.3 1684.52 77 -1 4 11 56513.1 1546.85 42 -1 -4 11 53283.1 1519.73 51 -1 -4 11 54492.3 1530.70 44 -1 -4 11 55429.7 1462.58 45 -1 4 11 57350.8 1567.63 52 -1 4 11 58470.8 1575.78 46 -1 -4 10 3094.02 342.632 10 1 -4 -10 3164.35 298.868 15 1 -4 -10 3725.40 331.221 9 -1 4 10 3356.02 328.297 20 1 -4 -10 3243.44 321.488 5 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160.705 63 -2 3 4 2090.13 184.092 75 2 -3 -4 2435.20 183.282 69 -2 3 4 2264.70 177.415 61 -2 3 4 2108.77 209.781 62 -2 3 3 10595.3 385.161 20 -2 -3 3 10204.7 399.639 20 2 3 -3 10294.8 384.377 19 -2 -3 3 10793.5 410.627 18 2 3 -3 12905.0 397.246 17 -2 3 3 10424.9 459.338 11 -2 -3 3 10107.6 419.535 16 -2 -3 3 10710.3 414.833 10 2 -3 -3 10660.7 413.067 5 -2 3 3 10508.1 401.974 16 2 -3 -3 10142.4 361.075 12 2 -3 -3 10338.6 399.499 15 2 -3 -3 10668.6 400.079 9 -2 3 3 10076.0 366.521 8 -2 -3 3 10683.2 391.933 77 -2 3 3 10355.5 404.009 76 -2 3 3 10271.7 393.334 66 2 -3 -3 10852.5 399.114 72 2 -3 -3 11042.7 395.292 73 2 -3 -3 10436.8 361.211 63 -2 3 3 9808.62 395.766 67 -2 3 3 11019.1 409.204 64 2 -3 -3 11183.0 410.002 65 2 -3 -3 11362.4 403.011 71 2 -3 -3 10513.1 396.073 70 -2 3 3 10333.1 411.006 75 2 -3 -3 10656.6 397.611 69 -2 3 3 10667.8 393.032 61 -2 3 3 10750.2 463.850 62 -2 3 2 2043.93 190.572 11 -2 3 2 1963.49 148.730 7 -2 -3 2 1858.64 161.651 18 2 -3 -2 1943.00 153.762 13 2 3 -2 2002.02 151.810 17 -2 3 2 1942.52 141.754 20 2 -3 -2 1816.34 160.855 5 -2 -3 2 1815.32 165.890 16 -2 -3 2 1747.59 160.087 10 -2 3 2 1805.07 148.125 16 2 -3 -2 1749.96 152.693 9 2 -3 -2 1718.37 152.410 15 -2 3 2 2018.52 160.795 8 2 3 -2 1933.33 156.492 19 -2 -3 2 1651.52 116.513 69 2 3 -2 1806.18 129.945 74 2 3 -2 1677.86 127.906 73 -2 -3 2 1816.35 147.578 77 -2 3 2 1742.88 152.439 66 2 -3 -2 1978.80 159.436 73 -2 3 2 1993.45 171.017 75 -2 -3 2 1866.76 123.975 68 2 -3 -2 1851.52 153.570 72 2 -3 -2 1839.39 156.053 70 2 3 -2 1588.90 126.128 71 2 -3 -2 1792.41 151.766 71 -2 3 2 1880.09 161.239 67 -2 3 2 1880.84 158.697 64 2 -3 -2 1762.91 153.769 65 2 3 -2 1663.63 123.341 67 -2 3 2 1642.20 152.379 76 2 3 -2 1727.28 126.123 75 -2 -3 2 1748.00 120.840 70 2 -3 -2 1997.18 162.529 69 2 3 -2 1718.06 125.689 76 -2 -3 2 1820.34 122.539 66 2 3 -2 1775.57 161.118 57 -2 -3 2 2027.82 168.938 57 2 3 -2 1653.79 156.943 59 -2 3 2 1865.34 184.509 62 -2 3 2 1814.32 152.738 61 2 3 -2 1538.54 149.506 60 -2 -3 2 1986.83 125.536 61 2 3 -2 1731.29 153.249 59 -2 3 1 4586.50 204.648 20 -2 3 1 4316.97 269.654 11 -2 3 1 4366.86 235.953 7 -2 -3 1 4426.93 255.961 18 2 -3 -1 4437.33 248.693 5 -2 -3 1 5082.05 269.013 16 2 3 -1 4337.26 228.033 17 -2 3 1 4515.53 209.807 16 2 3 -1 4387.33 338.516 2 2 -3 -1 4601.34 235.614 13 2 -3 -1 4492.90 239.476 9 2 -3 -1 4765.41 247.084 15 -2 -3 1 4073.52 213.348 14 -2 3 1 4637.47 252.580 8 2 3 -1 4407.98 240.602 19 2 3 -1 4461.24 260.259 6 -2 -3 1 4383.82 208.993 69 2 3 -1 4071.50 215.082 74 -2 3 1 4294.71 247.551 75 2 -3 -1 4650.24 245.644 72 2 3 -1 4127.30 217.409 73 -2 3 1 4350.45 238.469 66 -2 -3 1 4576.23 213.248 68 -2 -3 1 4342.35 209.591 66 -2 3 1 4669.93 249.910 76 2 3 -1 4166.80 220.825 71 -2 3 1 4733.74 248.548 64 2 -3 -1 4672.62 245.530 71 -2 3 1 3947.88 232.736 67 2 -3 -1 4377.06 236.668 73 2 -3 -1 4275.78 238.190 70 2 -3 -1 4516.24 239.094 65 2 3 -1 4273.53 216.437 67 2 3 -1 4549.35 222.374 76 -2 -3 1 4672.00 215.521 70 2 -3 -1 4393.84 238.963 69 2 3 -1 4230.88 214.070 75 -2 -3 1 4572.02 279.034 57 2 3 -1 4499.01 279.090 59 2 3 -1 4674.75 273.882 59 -2 3 1 4213.05 265.153 62 2 3 -1 4090.61 266.239 57 2 3 -1 4239.30 268.210 60 -2 -3 1 4368.57 208.479 61 -2 3 1 4242.11 230.983 61 -2 3 0 9554.58 387.628 1 2 -3 0 9700.01 334.202 17 -2 3 0 9065.87 384.270 11 2 3 0 9343.08 370.529 19 -2 -3 0 9165.93 375.837 18 2 -3 0 8865.59 360.153 5 2 3 0 9530.23 389.916 6 -2 3 0 9496.31 372.829 7 2 3 0 9752.89 366.601 17 2 3 0 9333.94 481.907 2 2 -3 0 8455.62 371.729 1 2 -3 0 9001.40 356.837 15 -2 -3 0 8468.28 338.312 14 2 -3 0 8990.42 355.409 9 2 -3 0 8780.48 346.321 13 -2 3 0 9053.86 380.489 8 2 -3 0 8864.89 295.345 19 -2 -3 0 9051.01 334.361 69 2 3 0 8402.83 339.760 74 2 3 0 8926.74 348.273 67 -2 3 0 9142.15 352.436 66 2 -3 0 9967.19 364.683 73 -2 -3 0 9399.12 338.671 68 2 -3 0 9695.38 363.333 72 2 3 0 8046.24 344.772 71 2 3 0 8519.53 346.579 73 -2 3 0 9404.75 358.393 64 2 -3 0 9668.88 361.095 71 -2 3 0 9377.92 361.251 67 -2 -3 0 9247.73 336.588 70 2 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79.9999 74 -2 -3 -1 192.442 69.2287 69 -2 3 -1 184.094 72.7443 76 2 -3 1 161.503 66.6005 74 2 3 1 106.924 72.8378 73 2 -3 1 156.258 64.9528 73 -2 -3 -1 153.596 65.7620 66 -2 -3 -1 149.917 69.1104 68 2 -3 1 182.712 73.5741 72 -2 3 -1 172.243 63.4421 66 -2 3 -1 204.727 71.6206 68 2 3 1 132.178 72.6250 71 2 -3 1 192.573 72.8380 71 -2 3 -1 167.489 70.9573 64 2 3 1 92.7888 67.9109 75 -2 3 -1 198.235 72.2780 67 2 -3 1 219.800 76.3123 70 2 3 1 126.633 71.3651 67 2 3 1 172.403 82.3890 59 -2 -3 -1 246.103 77.4064 61 -2 -3 -1 192.671 67.5613 58 -2 -3 -1 59.2490 75.5636 57 -2 3 -1 110.837 60.0547 62 -2 -3 -1 103.947 45.5437 63 -2 3 -1 165.400 70.1573 61 -2 -3 -2 7226.64 296.267 12 2 -3 2 7050.04 414.926 1 -2 3 -2 7053.65 345.119 7 -2 3 -2 7119.02 319.471 11 2 -3 2 7182.75 337.461 5 2 -3 2 7820.47 340.597 13 -2 -3 -2 7195.57 334.369 18 -2 -3 -2 7252.82 350.768 7 2 3 2 7497.31 350.242 17 2 -3 2 7015.44 291.056 17 2 3 2 7056.84 343.576 19 2 3 2 7385.90 391.901 2 2 -3 2 6737.99 326.020 15 2 3 2 7761.58 353.631 6 -2 -3 -2 7153.15 330.898 14 -2 3 -2 7787.94 364.914 8 2 3 2 7353.84 341.757 67 -2 -3 -2 7262.56 322.689 69 2 3 2 6791.09 333.304 74 2 -3 2 7540.65 324.579 74 -2 3 -2 7744.22 322.932 66 2 3 2 6645.85 332.810 73 2 -3 2 7367.61 319.910 73 -2 -3 -2 7083.87 319.195 68 2 -3 2 7045.18 319.983 72 -2 3 -2 7011.79 306.177 68 -2 3 -2 7275.06 318.149 64 2 3 2 6888.07 332.559 76 2 3 2 6746.26 341.241 71 -2 3 -2 7609.09 325.967 67 2 -3 2 7695.57 328.938 71 2 -3 2 6985.18 328.820 65 2 -3 2 7117.97 322.159 70 -2 3 -2 7549.49 327.821 76 -2 -3 -2 7428.23 325.048 70 2 3 2 6935.76 331.985 75 -2 -3 -2 7293.60 322.909 66 -2 -3 -2 7609.47 375.393 58 -2 3 -2 7502.04 316.569 61 -2 -3 -2 7640.09 327.155 61 -2 -3 -2 6909.27 291.117 63 -2 3 -2 7372.77 317.426 62 -2 -3 -3 4833.13 282.473 7 2 3 3 4607.48 284.705 19 -2 3 -3 4990.75 251.872 11 -2 -3 -3 4734.40 268.991 18 -2 3 -3 4650.47 283.727 7 2 -3 3 4783.24 275.730 13 2 3 3 4662.44 286.488 17 2 -3 3 4325.33 234.624 17 2 -3 3 4697.68 241.135 10 -2 -3 -3 4736.36 252.137 12 2 -3 3 4892.68 286.295 15 -2 -3 -3 4857.01 276.955 14 -2 -3 -3 4573.60 224.432 9 2 3 3 4273.29 265.214 6 -2 3 -3 4572.82 287.520 8 -2 -3 -3 4288.16 275.442 3 -2 -3 -3 4737.88 263.876 69 -2 -3 -3 4572.89 260.468 68 -2 3 -3 4497.72 248.481 66 2 3 3 4765.61 281.170 76 2 -3 3 4669.93 258.067 73 -2 3 -3 4947.16 260.981 64 -2 3 -3 4715.95 251.151 68 2 3 3 4567.30 287.158 71 -2 3 -3 4887.79 262.316 67 2 -3 3 4659.07 259.579 71 2 -3 3 4540.36 272.246 65 2 3 3 4430.25 276.026 74 2 -3 3 4546.64 259.001 70 2 3 3 4825.49 285.339 67 -2 -3 -3 4841.14 267.430 70 2 3 3 4395.53 278.203 73 2 -3 3 4929.05 268.343 72 2 3 3 4831.98 282.331 75 -2 -3 -3 4864.43 269.274 66 2 -3 3 4340.38 248.980 74 -2 -3 -3 4664.84 261.902 61 -2 -3 -3 4575.49 247.926 63 -2 3 -3 4742.53 239.492 62 -2 3 -3 4647.99 250.165 61 -2 -3 -4 7245.75 353.103 7 2 3 4 7104.33 377.798 19 2 3 4 7010.97 375.443 17 -2 -3 -4 7046.37 335.989 18 -2 3 -4 6942.24 367.629 7 2 -3 4 7112.86 336.263 10 2 -3 4 7281.93 371.331 15 -2 -3 -4 7355.24 361.821 14 2 3 4 6871.08 352.081 6 2 -3 4 7179.88 358.942 13 -2 -3 -4 7173.05 337.218 12 -2 3 -4 7479.90 380.780 8 -2 3 -4 7738.93 337.300 64 -2 3 -4 6987.06 320.740 66 2 -3 4 7209.84 334.182 73 -2 -3 -4 7160.40 344.772 68 2 3 4 6588.48 364.683 73 2 -3 4 7104.22 341.427 72 -2 3 -4 7294.83 322.669 68 -2 -3 -4 7253.33 349.473 69 2 3 4 6665.28 370.702 71 -2 3 -4 7673.42 338.134 67 2 3 4 7069.29 368.523 76 2 -3 4 7513.56 345.861 71 2 3 4 6639.50 360.165 74 2 -3 4 7478.98 337.468 74 2 -3 4 6490.19 324.830 70 -2 -3 -4 7222.46 349.254 70 2 3 4 7078.99 367.325 67 2 3 4 6708.88 357.544 75 -2 -3 -4 7239.60 348.892 66 -2 3 -4 7414.38 323.916 61 -2 -3 -4 7463.18 350.679 61 -2 -3 -4 6859.35 332.439 63 -2 3 -5 1140.00 162.919 8 -2 -3 -5 1107.28 147.504 12 2 3 5 1140.18 168.636 19 -2 -3 -5 1253.57 147.047 18 -2 -3 -5 1076.81 143.710 7 2 3 5 1049.02 169.777 17 2 -3 5 1243.94 159.106 10 -2 3 -5 1362.56 177.790 7 -2 -3 -5 1086.68 158.467 14 2 -3 5 1349.40 169.633 13 2 3 5 1321.28 164.789 6 -2 -3 -5 1390.18 162.900 69 2 -3 5 1425.53 149.817 74 -2 3 -5 1117.68 130.456 69 2 3 5 931.058 156.317 73 -2 -3 -5 1197.36 154.339 70 2 -3 5 1253.23 156.734 72 2 -3 5 1370.33 152.340 73 -2 -3 -5 1174.85 153.819 66 -2 -3 -5 1144.84 147.794 68 2 -3 5 1300.90 151.228 71 2 3 5 1142.88 170.566 71 -2 3 -5 1334.97 137.723 66 2 3 5 1043.64 155.005 74 -2 3 -5 1270.48 138.914 68 2 3 5 1255.62 169.596 76 2 3 5 984.250 152.286 67 2 3 5 978.768 150.992 75 -2 3 -5 1384.91 145.150 64 2 -3 5 1254.65 147.432 75 -2 -3 -5 1115.51 145.770 61 -2 -3 -5 1277.04 157.706 63 -2 3 -5 1380.67 145.601 61 -2 -3 -6 51106.8 1301.88 12 -2 3 -6 52057.7 1349.06 7 2 3 6 48489.4 1370.48 17 2 3 6 53451.3 1411.99 19 2 -3 6 57003.6 1376.59 10 2 3 6 53906.3 1346.96 6 -2 -3 -6 52121.5 1331.08 14 2 -3 6 51944.1 1347.04 13 -2 3 -6 52833.2 1340.38 8 -2 -3 -6 51988.5 1296.69 69 -2 3 -6 52569.8 1216.00 69 2 -3 6 52272.1 1260.41 74 2 -3 6 52508.4 1271.94 73 -2 3 -6 51306.6 1216.36 64 2 3 6 51244.8 1355.46 76 -2 -3 -6 53174.8 1302.95 68 2 -3 6 51618.7 1288.04 72 -2 3 -6 51369.4 1205.88 68 2 3 6 49364.9 1349.94 74 2 3 6 48761.3 1362.77 71 2 -3 6 52417.9 1287.04 71 -2 3 -6 52948.3 1221.28 66 2 3 6 50112.5 1371.05 73 2 3 6 52425.8 1365.82 67 -2 -3 -6 51606.4 1297.25 70 2 3 6 51035.9 1351.40 75 -2 -3 -6 53298.0 1306.28 66 2 -3 6 54049.8 1275.87 75 -2 3 -6 52194.2 1210.24 61 -2 -3 -6 53054.8 1303.78 61 -2 -3 -6 51579.5 1303.01 63 -2 -3 -7 71943.6 1742.96 12 2 3 7 74152.9 1863.11 19 -2 3 -7 76169.4 1785.27 7 2 -3 7 78015.3 1840.60 10 -2 -3 -7 75751.3 1779.07 14 -2 3 -7 75260.7 1757.95 14 2 -3 7 76551.5 1812.25 13 -2 3 -7 72497.5 1737.06 8 -2 -3 -7 73267.2 1721.98 69 2 3 7 69330.9 1792.64 74 2 3 7 70004.1 1783.01 76 2 3 7 69948.0 1811.47 73 -2 -3 -7 75619.9 1732.16 68 2 3 7 66441.0 1796.52 71 2 3 7 71011.5 1793.52 67 2 -3 7 84441.4 1850.80 77 -2 -3 -7 75066.9 1734.19 70 -2 -3 -7 74831.0 1731.10 66 2 3 7 69975.3 1786.18 75 -2 -3 -7 74659.6 1727.65 61 -2 -3 -7 73627.2 1743.91 63 -2 3 -8 347.176 105.323 8 -2 -3 -8 431.792 130.049 12 2 3 8 506.249 156.115 19 2 -3 8 683.123 168.978 10 -2 3 -8 385.764 115.793 7 2 3 8 562.164 152.189 20 2 -3 8 280.340 103.118 13 -2 3 -8 430.299 122.251 14 -2 -3 -8 429.994 121.898 14 -2 -3 -8 416.904 112.655 9 2 3 8 430.809 134.594 74 -2 -3 -8 328.024 104.817 69 2 3 8 529.426 155.277 73 2 3 8 481.428 134.881 76 -2 -3 -8 503.732 117.114 70 2 3 8 443.365 128.529 64 -2 -3 -8 448.995 116.429 68 2 3 8 364.758 121.477 67 -2 -3 -8 508.062 122.240 72 2 3 8 537.531 144.607 75 2 -3 8 517.665 145.873 77 -2 -3 -8 459.695 119.244 63 -2 -3 -8 410.451 114.369 61 -2 -3 -9 51.1780 79.1746 12 2 3 9 127.362 109.619 20 -2 3 -9-9.25891 87.1348 14 2 3 9-36.1257 106.780 19 -2 3 -9 294.263 121.436 7 -2 -3 -9 70.5446 81.9761 9 2 -3 9 125.216 87.4421 13 -2 -3 -9 121.296 113.020 14 2 3 9 185.655 95.5109 67 -2 -3 -9 219.645 103.705 69 -2 -3 -9 62.6313 73.5332 70 2 3 9 31.7063 85.6762 73 2 3 9 199.960 95.8293 64 -2 -3 -9 163.374 83.8666 68 -2 -3 -9 110.330 66.1893 72 2 -3 9 129.342 100.380 77 2 3 9 122.546 107.670 74 2 3 9 42.7524 77.8836 76 2 3 9 129.915 94.7929 75 -2 -3 -9 95.5661 86.7560 63 -2 -3 -9 79.1469 72.1094 61 -2 -3 -10 1757.49 234.102 12 2 3 10 1907.97 267.660 20 2 -3 10 1961.14 267.419 13 -2 -3 -10 1901.13 243.174 14 -2 3 -10 1819.38 229.495 14 -2 -3 -10 1963.68 241.488 9 2 3 10 1995.88 264.117 74 -2 -3 -10 1938.69 223.944 70 2 3 10 2122.32 279.973 73 2 3 10 2000.75 259.292 64 2 3 10 2258.37 272.825 75 -2 -3 -10 1899.22 223.057 72 -2 -3 -10 1789.52 215.509 68 2 -3 10 2559.34 294.147 77 2 3 10 1963.81 256.906 67 -2 -3 -10 1798.78 222.463 69 2 3 10 1808.64 242.012 76 -2 -3 -10 1610.10 208.152 61 -2 -3 -10 1673.45 229.501 63 2 -3 11 9882.57 546.301 36 2 3 11 10504.1 525.885 40 -2 -3 -11 12034.1 565.993 27 2 -3 11 11013.8 552.834 26 2 -3 11 10274.5 562.882 38 2 3 11 11033.9 592.040 35 -2 -3 -11 11201.4 616.268 12 2 3 11 10885.8 664.602 20 -2 -3 -11 10517.9 594.261 9 -2 -3 -11 10338.2 588.608 14 -2 3 -11 11520.0 598.844 14 2 -3 11 11714.8 658.971 13 2 3 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9096.85 554.270 73 2 4 8 9429.40 545.466 67 2 -4 8 10627.1 568.999 77 -2 -4 -8 8976.75 487.635 70 2 4 8 9237.43 540.320 76 2 4 8 8951.18 536.804 75 -2 -4 -8 9140.81 490.474 61 -2 -4 -8 8999.87 503.822 63 -2 -4 -9-16.6153 79.8100 12 2 4 9 280.082 127.030 20 -2 4 -9 138.061 87.2215 7 2 -4 9 105.797 102.847 10 2 4 9-5.94492 72.9057 16 -2 -4 -9 145.291 88.3310 9 -2 4 -9 259.977 102.845 14 -2 -4 -9 207.227 96.5917 14 2 -4 9 169.838 93.5678 13 2 4 9 60.5370 83.9704 74 -2 -4 -9 320.620 117.852 69 2 4 9 244.728 121.753 73 2 4 9 141.868 101.851 64 -2 -4 -9 111.821 81.0033 72 2 -4 9 301.333 128.451 77 -2 -4 -9 240.282 103.589 68 2 4 9 258.418 104.285 67 2 4 9 290.220 118.599 76 -2 -4 -9 197.264 92.1847 70 2 4 9 27.4514 85.3280 75 -2 -4 -9 173.824 88.4564 61 -2 -4 -9 309.683 111.609 63 2 -4 10 1280.11 199.891 26 2 4 10 1366.85 211.636 35 2 -4 10 1317.79 206.608 38 2 4 10 1464.94 214.557 42 -2 -4 -10 1074.85 168.775 27 2 -4 10 1171.50 187.790 36 -2 -4 -10 1308.19 185.088 37 2 4 10 1205.52 220.222 20 -2 -4 -10 908.782 186.509 12 -2 -4 -10 1155.54 187.796 5 2 4 10 1165.08 200.603 22 -2 -4 -10 1244.16 206.049 14 -2 4 -10 1381.45 208.303 14 -2 -4 -10 1260.19 202.026 9 2 -4 10 1040.48 197.434 13 2 4 10 1219.27 203.299 23 2 4 10 1185.22 216.875 64 2 4 10 1210.06 245.109 73 2 4 10 1319.02 223.944 75 -2 -4 -10 1021.37 178.791 68 -2 -4 -10 1067.45 178.418 72 2 4 10 1293.35 224.559 74 2 4 10 1050.09 201.452 76 -2 -4 -10 1314.02 193.512 69 2 4 10 1137.83 207.976 67 2 -4 10 1769.49 261.979 77 -2 -4 -10 1314.20 195.185 70 -2 -4 -10 1215.35 210.121 63 -2 -4 -10 1311.53 199.283 61 2 4 10 1292.73 204.340 46 2 -4 10 1183.20 171.268 45 2 4 10 986.655 175.042 52 2 4 11 1169.32 198.731 35 2 -4 11 1043.93 184.412 36 2 -4 11 1391.36 213.707 38 -2 -4 -11 1371.43 201.408 37 -2 -4 -11 1163.97 189.396 27 2 -4 11 1201.08 193.813 26 -2 -4 -11 878.523 184.629 12 2 4 11 996.692 227.494 20 -2 -4 -11 1234.05 210.174 5 2 4 11 1426.54 217.911 22 -2 4 -11 1193.79 200.950 14 -2 -4 -11 902.657 185.568 14 -2 -4 -11 768.020 166.851 9 2 4 11 958.749 191.604 23 2 -4 11 1257.86 217.758 13 2 -4 11 1073.66 227.681 77 2 4 11 1097.18 208.290 46 2 -4 11 989.138 166.738 45 -2 -4 -11 787.378 164.824 63 2 4 11 1289.28 210.050 52 2 4 12 79798.0 1997.21 22 2 -4 12 76196.6 1963.43 38 -2 -4 -12 78386.3 1901.71 37 2 4 12 74586.6 1846.80 40 -2 -4 -12 80602.9 1932.80 31 -2 -4 -12 76666.1 1881.53 27 2 4 12 81519.8 2002.89 35 2 -4 12 80634.5 1938.43 26 2 -4 12 77926.6 1948.29 40 2 4 12 78277.6 2034.40 46 2 -4 12 78264.1 1875.04 45 2 4 13 4324.68 360.948 22 2 -4 13 3883.36 330.260 40 -2 -4 -13 4020.44 317.005 37 -2 -4 -13 4213.22 334.230 31 2 -4 13 3889.70 327.423 26 2 4 13 3579.49 294.450 40 -2 -4 -13 3643.15 299.990 27 2 4 13 3836.43 353.075 46 2 -4 13 3673.91 293.072 45 2 4 14-44.4405 79.3910 21 2 4 14-50.4008 106.172 22 -2 -4 -14-94.0192 85.1306 31 2 4 14-14.4525 72.0823 40 2 -4 14-11.1446 90.1703 40 -2 -4 -14-27.8911 70.3596 37 2 -4 14 50.2481 86.0748 26 2 4 14 88.0215 99.0788 46 2 -4 14-141.933 82.3234 45 2 4 15 5668.33 338.108 21 2 4 15 6105.45 379.893 22 2 -4 15 5472.90 343.441 40 -2 -4 -15 5815.39 328.027 37 2 -4 15 5134.99 330.268 26 -2 -4 -15 5489.20 333.629 31 2 4 15 6193.91 338.991 40 2 4 15 5907.11 380.911 46 2 -4 15 5700.02 312.016 45 2 4 16 589.021 99.2866 21 -2 -4 -16 759.554 116.777 31 -2 -4 -16 548.149 96.0509 41 2 -4 16 568.593 108.281 40 2 4 16 726.578 104.867 40 2 4 16 634.872 123.329 46 -2 5 16 803.902 111.161 21 -2 -5 16 746.527 115.486 21 -2 5 16 1019.63 134.403 40 -2 -5 16 950.253 130.495 45 -2 -5 15 112.675 91.8814 21 -2 5 15-107.025 66.8767 21 -2 5 15 42.1333 79.6870 40 -2 -5 15-27.1684 75.5619 26 -2 -5 15 54.9550 77.2538 45 -2 -5 14 9406.63 476.273 21 -2 5 14 8924.98 437.525 21 -2 5 14 9652.98 494.332 40 -2 -5 14 8624.10 472.077 26 -2 5 14 8658.98 470.300 50 -2 -5 14 9788.33 489.627 45 -2 5 14 9934.58 527.748 42 -2 -5 13 532.719 138.546 21 -2 5 13 350.744 113.130 21 -2 5 13 240.779 124.139 42 -2 5 13 497.662 144.922 40 -2 -5 13 426.496 128.339 26 -2 -5 13 297.486 118.280 45 2 -5 -13 437.553 106.922 54 -2 5 13 321.153 134.512 52 -2 -5 12 14512.2 632.426 21 -2 5 12 14710.4 602.881 21 -2 5 12 14588.9 653.665 40 -2 5 12 15309.8 691.998 29 -2 -5 12 14565.2 655.934 26 -2 5 12 15654.2 710.316 42 -2 5 12 15874.3 724.565 52 -2 -5 12 14286.0 628.124 45 -2 -5 12 14186.3 678.137 44 -2 5 11 3764.08 321.591 34 -2 5 11 3631.85 334.599 29 -2 5 11 3607.21 312.950 40 -2 5 11 3518.02 353.778 20 -2 -5 11 3542.50 395.992 10 -2 5 11 3337.50 365.140 16 2 -5 -11 3541.95 361.153 5 2 -5 -11 3399.70 329.880 15 2 -5 -11 3733.14 362.770 9 -2 -5 11 3528.92 298.773 21 2 -5 -11 3483.84 338.745 65 -2 -5 11 3781.92 362.182 77 -2 5 11 3794.78 341.841 42 -2 -5 11 2872.79 295.781 44 -2 -5 11 3492.43 292.670 45 -2 5 11 3920.92 353.937 52 -2 5 10 2106.83 242.322 40 -2 5 10 2583.66 276.493 29 -2 5 10 2543.91 265.298 34 -2 -5 10 2744.63 257.419 21 -2 5 10 2907.23 311.132 20 -2 5 10 3029.19 336.589 16 -2 -5 10 2660.97 331.541 10 2 -5 -10 2770.28 306.892 5 2 -5 -10 2439.29 274.690 15 2 -5 -10 2768.30 303.049 9 -2 -5 10 2931.00 311.484 77 2 -5 -10 2966.36 308.620 65 -2 5 10 3004.87 297.181 42 -2 -5 10 2799.44 260.138 45 -2 5 10 2977.02 302.139 52 -2 -5 10 2665.22 276.531 51 -2 -5 10 2738.83 283.025 44 -2 5 9 13727.3 667.160 20 -2 -5 9 12642.5 700.768 10 -2 5 9 13930.0 699.495 16 2 -5 -9 13811.2 685.291 5 2 -5 -9 13927.2 655.008 15 2 -5 -9 13792.6 668.274 9 2 -5 -9 13029.3 644.166 65 -2 -5 9 13730.7 663.473 77 -2 5 8 901.943 165.602 20 -2 5 8 947.173 196.107 11 -2 -5 8 1121.36 211.857 10 -2 5 8 1009.40 182.230 16 2 -5 -8 872.201 162.229 15 2 -5 -8 1023.99 182.804 9 2 -5 -8 1272.66 204.773 5 2 -5 -8 875.366 161.554 65 -2 -5 8 993.972 169.092 77 -2 5 7 18430.9 709.819 20 -2 5 7 17262.0 767.530 11 -2 -5 7 16408.1 746.145 10 -2 -5 7 18159.7 713.242 16 -2 5 7 18215.7 745.682 16 2 -5 -7 19369.0 757.183 5 2 -5 -7 17846.6 697.369 15 2 -5 -7 16906.7 707.497 9 2 5 -7 17761.3 697.896 6 -2 5 7 16886.3 667.760 66 2 -5 -7 18153.6 664.128 73 2 -5 -7 18567.8 674.488 72 2 -5 -7 19767.6 689.475 71 -2 5 7 17428.5 688.623 67 -2 5 7 17540.2 683.001 64 -2 -5 7 17920.7 704.054 77 2 -5 -7 18484.6 675.731 70 -2 5 7 18138.6 700.422 76 2 -5 -7 17728.8 706.185 65 -2 5 7 17472.9 700.110 75 2 -5 -7 18397.4 674.424 69 -2 5 7 16498.1 650.663 61 -2 5 7 17027.3 755.191 62 -2 5 6 7855.74 473.813 11 2 5 -6 7281.87 413.113 6 -2 5 6 6847.97 388.400 20 -2 -5 6 6997.97 442.633 10 -2 -5 6 7697.70 427.224 16 -2 5 6 8032.11 446.516 16 2 -5 -6 8061.84 448.943 5 2 -5 -6 7808.55 415.857 15 2 -5 -6 7337.43 425.122 9 2 -5 -6 7365.65 395.917 12 -2 5 6 7032.23 410.259 76 2 -5 -6 8490.78 417.163 73 -2 5 6 7193.94 403.356 66 2 -5 -6 7415.96 395.824 72 2 -5 -6 7967.45 406.991 71 -2 5 6 7046.34 409.201 67 -2 5 6 6807.95 398.297 64 -2 -5 6 7373.67 403.750 77 2 -5 -6 7621.68 402.890 70 2 -5 -6 7120.01 411.317 65 -2 5 6 6808.98 411.582 75 2 -5 -6 7478.51 390.083 63 2 -5 -6 7917.04 409.954 69 -2 5 6 6952.10 389.244 61 -2 5 6 7282.67 455.417 62 -2 5 5 2050.76 196.600 20 2 5 -5 1684.84 199.649 6 -2 -5 5 1971.01 210.219 16 2 -5 -5 2330.90 235.005 5 -2 5 5 2075.16 216.649 16 -2 -5 5 1621.04 204.989 10 -2 5 5 2082.82 242.749 11 2 -5 -5 1768.58 193.042 15 2 -5 -5 2050.61 215.094 9 2 -5 -5 2004.85 194.876 12 2 -5 -5 1904.91 193.871 63 -2 5 5 2014.04 207.720 66 2 -5 -5 1990.28 196.391 73 2 -5 -5 1764.28 188.404 72 2 -5 -5 1871.36 192.802 71 -2 5 5 1961.87 208.031 67 -2 5 5 1935.16 204.331 64 -2 -5 5 2015.75 199.757 77 2 -5 -5 1988.80 198.393 70 2 -5 -5 2096.17 212.671 65 -2 5 5 1824.87 199.961 76 -2 5 5 1690.01 197.776 75 2 -5 -5 1786.89 192.799 69 -2 5 5 1448.89 176.921 61 -2 5 5 1844.77 222.745 62 -2 5 4 40971.1 1229.25 11 -2 -5 4 44258.0 1116.34 18 2 -5 -4 42800.7 1173.75 5 -2 -5 4 42778.8 1200.80 10 -2 5 4 43892.1 1147.42 16 2 -5 -4 44625.6 1137.63 15 2 -5 -4 43980.7 1168.82 9 2 5 -4 44458.7 1182.34 6 2 -5 -4 42678.3 1114.84 12 -2 5 4 44427.7 1168.31 66 -2 -5 4 43543.4 1100.25 77 2 -5 -4 46449.4 1164.36 72 2 -5 -4 42632.0 1111.90 63 2 -5 -4 44532.5 1148.74 71 -2 5 4 43298.4 1171.47 67 -2 5 4 44163.3 1171.43 64 2 -5 -4 47668.1 1178.77 70 2 -5 -4 43057.6 1143.56 65 -2 5 4 44389.1 1179.92 76 2 -5 -4 44996.5 1147.58 73 -2 5 4 44654.8 1199.24 75 2 -5 -4 45835.7 1162.21 69 -2 5 4 43952.4 1151.09 61 -2 5 4 42127.4 1232.01 62 2 5 -3 23728.3 686.941 19 -2 5 3 23186.1 815.519 11 -2 -5 3 24284.2 743.601 18 2 -5 -3 22353.7 749.734 5 -2 -5 3 23584.9 788.537 10 -2 5 3 23798.8 720.853 16 2 -5 -3 22814.4 748.949 9 2 -5 -3 23627.3 727.633 15 2 5 -3 23962.1 775.551 6 2 -5 -3 22384.1 710.543 12 2 -5 -3 24250.6 755.630 70 -2 5 3 23810.2 756.910 66 2 -5 -3 24687.0 751.475 73 2 -5 -3 24697.4 756.025 72 2 -5 -3 22098.7 703.934 63 2 -5 -3 25065.1 758.595 71 -2 5 3 23291.8 760.898 67 -2 5 3 23705.1 760.321 64 -2 -5 3 23851.0 683.989 77 2 -5 -3 23370.8 733.710 65 -2 5 3 23483.2 763.777 76 -2 5 3 22931.3 769.684 75 2 -5 -3 23724.3 748.512 69 -2 5 3 22987.7 736.005 61 -2 5 3 24382.4 821.351 62 2 -5 -2 14213.0 528.872 13 2 5 -2 13633.7 489.283 19 -2 5 2 13768.4 585.570 11 -2 -5 2 13829.0 533.185 18 2 5 -2 14236.8 563.026 6 2 -5 -2 13880.8 540.630 5 -2 -5 2 14192.8 576.271 10 -2 5 2 13280.9 478.286 16 2 -5 -2 13519.8 531.595 9 2 -5 -2 13739.3 512.824 15 -2 5 2 13780.9 517.921 8 -2 5 2 12978.8 519.955 66 2 -5 -2 14124.7 529.709 73 2 -5 -2 13683.5 527.352 72 2 -5 -2 14295.6 534.732 71 -2 5 2 13466.9 534.773 67 -2 5 2 13523.7 533.571 64 2 -5 -2 14018.6 533.851 70 2 -5 -2 13786.0 517.011 65 -2 5 2 13651.0 538.721 76 -2 5 2 13832.7 552.417 75 2 -5 -2 14675.1 541.449 69 -2 5 2 13550.1 578.307 62 -2 5 2 13040.9 513.298 61 2 5 -1 5043.18 283.177 19 -2 5 1 4696.50 321.806 11 -2 -5 1 4673.84 298.206 18 -2 5 1 4592.26 273.666 7 2 -5 -1 4296.71 285.679 5 2 -5 -1 4537.50 285.336 13 -2 -5 1 4349.22 310.184 10 2 -5 -1 5175.39 309.064 9 2 -5 -1 4931.21 285.526 15 -2 5 1 4983.37 302.365 8 2 5 -1 4170.02 297.578 6 -2 -5 1 4980.77 252.819 69 2 5 -1 4508.75 261.557 74 -2 -5 1 5129.70 259.576 70 2 5 -1 4071.68 252.977 73 -2 5 1 5470.72 308.469 66 2 5 -1 4546.79 256.925 67 2 5 -1 4494.93 254.521 76 2 5 -1 4410.21 254.718 64 -2 -5 1 4870.45 252.457 68 2 -5 -1 5093.22 292.431 73 2 -5 -1 5068.06 297.123 72 -2 -5 1 4439.95 242.094 72 2 -5 -1 5052.30 293.509 71 -2 5 1 4530.04 288.723 67 -2 5 1 5003.99 297.744 64 2 -5 -1 4678.98 285.841 65 2 -5 -1 4972.20 297.681 70 -2 5 1 4626.50 292.368 76 -2 5 1 5073.65 311.534 75 2 -5 -1 4897.60 292.169 69 2 5 -1 4367.29 253.346 75 -2 5 1 5058.54 328.259 62 -2 -5 1 4532.00 243.079 61 -2 5 1 5113.39 294.249 61 -2 5 0 627.276 125.484 8 2 5 0 654.990 131.960 6 2 5 0 537.985 111.782 19 -2 -5 0 826.560 140.986 18 2 5 0 583.147 101.905 17 -2 5 0 556.505 109.323 7 2 -5 0 526.750 111.653 15 2 -5 0 622.914 125.918 9 -2 -5 0 605.006 117.423 14 2 -5 0 620.135 126.622 5 -2 5 0 747.508 144.445 11 2 -5 0 713.075 124.984 13 2 -5 0 740.908 126.287 65 2 -5 0 795.539 126.741 69 -2 -5 0 518.723 95.7325 69 2 5 0 567.755 116.275 73 2 -5 0 565.068 110.338 73 2 5 0 716.226 116.695 64 2 5 0 657.825 116.377 67 -2 -5 0 727.064 108.043 68 2 -5 0 682.481 116.285 72 -2 -5 0 506.178 94.9672 72 -2 5 0 627.893 118.008 66 2 -5 0 697.948 119.737 71 2 5 0 564.915 109.818 74 2 5 0 618.926 114.589 75 -2 5 0 656.679 121.265 64 -2 -5 0 710.959 109.426 70 -2 5 0 887.065 137.522 75 -2 5 0 669.746 119.101 67 2 5 0 565.544 111.561 76 2 -5 0 652.807 117.353 70 -2 5 0 483.659 102.097 76 -2 5 0 699.747 138.113 62 -2 5 0 776.802 120.058 61 -2 -5 0 647.607 104.216 61 -2 5 -1 1179.35 170.746 8 2 5 1 1228.79 170.769 6 2 5 1 1364.42 163.178 19 -2 -5 -1 1206.73 140.027 12 -2 5 -1 1231.24 167.424 11 -2 -5 -1 1355.37 167.958 18 2 5 1 999.793 150.768 11 2 5 1 1072.41 138.063 17 -2 5 -1 986.196 147.372 7 2 -5 1 1056.33 145.959 15 2 -5 1 1275.14 166.649 9 2 -5 1 1013.81 148.767 5 -2 -5 -1 1042.48 148.542 14 2 -5 1 1036.76 145.650 13 -2 -5 -1 1455.69 155.825 69 2 -5 1 978.497 132.430 69 2 5 1 1097.09 146.191 75 2 5 1 1248.53 159.410 74 2 -5 1 1288.49 151.415 73 2 5 1 1125.75 155.730 73 2 5 1 998.897 145.328 64 -2 -5 -1 1132.68 142.077 68 2 -5 1 1088.14 145.647 72 -2 -5 -1 1133.73 139.002 72 -2 5 -1 1039.49 141.123 66 2 5 1 1008.18 141.325 76 2 -5 1 1349.48 159.185 65 2 -5 1 1069.98 140.966 71 -2 5 -1 1208.32 151.920 64 -2 5 -1 1216.07 151.937 67 2 -5 1 1089.38 146.050 70 -2 5 -1 1275.73 156.911 76 -2 -5 -1 1071.90 136.639 70 -2 5 -1 1419.08 166.837 75 2 5 1 1102.23 148.863 67 -2 -5 -1 1207.99 135.837 63 -2 5 -1 1088.47 140.727 61 -2 5 -1 1040.11 154.518 62 -2 -5 -1 1246.23 143.455 61 2 5 2 10605.1 470.971 19 -2 5 -2 10702.0 472.859 11 2 -5 2 11208.6 488.347 5 -2 -5 -2 10563.6 471.943 18 2 5 2 10425.6 471.926 11 -2 5 -2 10920.3 488.952 7 2 5 2 10707.3 454.107 17 2 -5 2 11401.4 478.704 13 2 -5 2 10058.2 451.079 15 -2 -5 -2 10473.4 478.077 14 -2 5 -2 10748.8 498.509 8 2 5 2 10088.2 485.157 6 -2 -5 -2 9915.10 429.851 12 -2 -5 -2 10385.8 444.677 69 2 5 2 10008.1 469.249 74 -2 5 -2 10525.4 448.286 76 -2 5 -2 10981.5 445.984 66 2 5 2 10143.6 479.767 73 2 -5 2 10166.5 429.525 73 -2 -5 -2 10782.5 449.647 68 2 5 2 10804.1 477.194 76 2 5 2 10224.3 466.708 64 2 -5 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359.834 7 -2 -5 -9 3838.76 355.020 12 2 -5 9 4603.13 412.321 10 -2 -5 -9 3885.33 334.980 9 -2 -5 -9 3843.24 358.334 14 2 -5 9 4333.03 379.903 13 2 5 9 4020.47 337.767 23 -2 5 -9 4269.39 364.007 14 2 5 9 3813.15 385.166 74 2 5 9 3908.10 398.186 73 2 5 9 3873.28 372.929 64 -2 -5 -9 3943.79 341.678 68 -2 -5 -9 4228.51 347.638 72 -2 -5 -9 3428.90 319.835 70 -2 -5 -9 4116.95 365.274 63 2 5 9 3841.50 370.480 67 2 -5 9 4655.43 410.193 77 2 5 9 3404.56 351.460 76 2 5 9 4177.06 392.137 75 -2 -5 -9 3741.78 333.602 69 2 5 9 3952.99 348.483 42 -2 -5 -9 3830.68 340.393 61 2 -5 9 4426.88 328.734 45 2 -5 9 4306.94 338.598 53 2 -5 9 4431.28 385.555 51 2 5 9 3526.81 332.651 52 2 5 9 4442.84 357.019 46 2 5 10 3502.98 313.725 35 -2 -5 -10 3507.37 319.514 31 2 -5 10 3029.51 290.845 36 -2 -5 -10 3665.18 317.330 27 2 -5 10 3574.34 325.013 38 2 -5 10 3798.55 317.620 26 -2 -5 -10 4294.45 336.502 37 -2 -5 -10 3415.16 345.152 12 2 5 10 3967.29 395.494 20 -2 5 -10 3676.22 354.036 7 -2 -5 -10 3560.85 331.898 9 -2 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27 -2 -5 -12 1130.70 186.778 31 2 5 12 1125.31 194.462 42 2 -5 12 1465.87 218.925 26 -2 -5 -12 1415.30 204.541 37 2 5 12 1316.42 225.754 46 2 5 12 1153.00 202.157 52 2 -5 12 909.818 167.457 45 2 5 13 11150.4 568.187 22 2 -5 13 11605.6 565.835 40 -2 -5 -13 10335.5 525.829 31 2 -5 13 10959.9 544.634 26 -2 -5 -13 10922.6 526.381 37 -2 -5 -13 11332.4 522.275 27 2 5 13 10925.0 591.929 46 2 -5 13 10880.4 522.499 45 2 5 13 10419.3 554.678 52 2 5 14 41193.4 1177.71 22 2 -5 14 40171.8 1153.79 40 -2 -5 -14 40065.4 1106.28 37 -2 -5 -14 40505.0 1133.89 31 2 -5 14 40162.8 1145.04 26 2 -5 14 40918.6 1106.76 45 2 5 14 40792.7 1220.20 46 2 5 15 7089.43 382.106 22 2 5 15 6778.29 357.109 21 2 -5 15 7127.85 373.282 26 2 -5 15 6828.95 369.024 40 -2 -5 -15 6914.31 361.387 31 -2 -5 -15 6994.26 348.929 41 -2 -5 -15 6457.54 348.981 30 -2 -5 -15 6766.88 339.377 37 2 5 15 7175.47 405.673 46 2 -5 15 7414.38 352.811 45 2 5 16 1088.94 124.262 21 -2 -5 -16 988.177 122.758 30 2 -5 16 1073.52 123.807 40 -2 -5 -16 1176.66 123.421 41 -2 -5 -16 1137.21 130.845 31 2 5 16 998.022 136.492 46 -2 6 16 1793.85 161.479 40 -2 -6 16 1655.25 149.411 45 2 -6 -16 1452.45 136.871 53 -2 -6 15 29.7991 60.4345 21 -2 6 15 74.2577 77.8300 40 -2 -6 15 91.8104 68.9650 45 -2 -6 14 5202.41 331.392 21 -2 -6 14 4935.69 334.378 26 -2 6 14 5230.21 345.195 40 -2 6 14 4787.21 330.333 50 -2 -6 14 4446.95 310.018 45 2 -6 -14 5083.28 315.988 54 -2 6 14 5333.05 371.588 42 -2 -6 13 25571.6 854.026 21 -2 6 13 25568.6 880.185 40 -2 -6 13 22763.4 840.504 26 -2 -6 13 23705.0 831.946 45 2 -6 -13 26135.0 843.631 54 -2 6 13 26830.1 953.577 52 -2 -6 13 23791.4 880.180 51 -2 6 13 25984.2 929.850 42 -2 -6 12 10764.3 526.129 21 -2 6 12 11501.4 565.726 40 2 -6 -12 11085.8 518.036 25 -2 6 12 11537.2 593.008 29 -2 6 12 11599.3 567.702 34 -2 -6 12 10962.6 548.643 26 -2 6 12 11630.3 604.754 42 -2 -6 12 10234.6 514.029 45 2 -6 -12 10941.4 528.961 54 -2 6 12 11060.9 597.913 52 -2 -6 12 10286.7 573.747 44 -2 -6 12 9901.70 551.277 51 -2 -6 11 1987.15 228.267 21 2 -6 -11 1846.33 221.390 25 -2 6 11 2219.99 248.295 34 -2 6 11 2313.80 256.390 40 -2 6 11 1836.89 251.426 42 -2 6 11 2161.32 264.180 29 -2 -6 11 1665.42 226.518 44 -2 -6 11 1917.81 218.468 45 2 -6 -11 2422.01 246.439 54 -2 6 11 2505.00 293.554 52 -2 -6 11 1972.76 247.574 51 -2 6 10 678.023 151.757 42 2 -6 -10 527.685 125.895 25 -2 6 10 738.794 170.961 29 -2 6 10 830.474 157.612 40 -2 6 10 865.912 163.905 34 -2 6 10 803.740 171.212 20 2 -6 -10 703.749 178.829 5 -2 -6 10 591.885 177.354 10 -2 6 10 1015.49 202.661 16 2 -6 -10 723.302 163.334 15 2 -6 -10 575.964 163.378 9 -2 -6 10 899.057 152.026 21 2 -6 -10 853.213 172.406 65 -2 -6 10 918.359 187.556 77 -2 -6 10 385.019 135.945 44 2 -6 -10 855.300 160.788 54 -2 -6 10 963.754 159.358 45 -2 6 10 916.606 187.521 52 -2 -6 10 523.092 136.787 51 -2 6 9 46101.0 1347.10 34 2 -6 -9 46650.0 1281.63 25 2 -6 -9 47005.8 1241.20 41 -2 6 9 47477.7 1314.66 40 -2 6 9 46722.8 1386.44 29 -2 6 9 46635.0 1400.83 20 -2 -6 9 46834.6 1541.88 10 -2 6 9 46787.9 1475.12 16 2 -6 -9 49335.3 1483.88 5 2 -6 -9 49091.3 1409.89 15 2 -6 -9 47557.6 1450.42 9 -2 -6 9 44952.5 1262.60 21 -2 -6 9 51340.2 1460.02 77 2 -6 -9 47784.2 1429.16 65 -2 -6 9 45479.0 1373.03 51 -2 -6 9 43918.3 1282.66 50 2 -6 -9 48968.5 1313.89 54 -2 6 9 48666.9 1405.50 52 -2 -6 9 44085.4 1222.70 45 -2 -6 9 45456.0 1368.36 44 -2 6 9 46233.9 1356.16 42 -2 6 8 259.236 100.200 20 2 6 -8 376.461 115.808 11 -2 -6 8 402.277 149.545 10 -2 6 8 646.793 167.777 16 2 -6 -8 439.008 121.963 15 2 -6 -8 314.804 104.468 9 2 -6 -8 525.086 143.258 5 2 -6 -8 469.707 134.186 65 -2 -6 8 563.148 138.354 77 2 -6 -8 377.645 106.549 73 2 -6 -8 329.991 110.210 72 -2 6 8 285.831 96.6841 66 -2 6 8 181.531 93.7475 76 2 -6 -8 413.976 113.851 71 2 -6 -8 441.763 113.932 69 -2 6 8 468.987 126.256 64 -2 6 8 208.714 94.6920 67 2 -6 -8 317.322 93.6030 70 -2 6 8 318.349 114.744 75 -2 6 8 313.200 120.033 62 -2 6 8 380.687 112.573 61 -2 6 7 4901.63 406.681 11 -2 -6 7 4898.07 412.805 10 2 -6 -7 4643.46 373.428 5 -2 6 7 5132.37 388.270 16 2 -6 -7 5077.86 360.554 15 2 -6 -7 4943.34 382.636 9 -2 6 7 4410.86 344.932 66 2 -6 -7 5160.45 353.037 73 2 -6 -7 5080.94 353.810 72 2 -6 -7 4620.87 336.944 71 -2 6 7 4324.20 347.512 67 -2 6 7 4262.74 341.592 64 -2 -6 7 5272.42 367.408 77 2 -6 -7 4857.26 347.137 70 2 -6 -7 4919.80 366.789 65 -2 6 7 4588.25 363.136 75 2 -6 -7 4554.32 334.934 69 -2 6 7 4482.05 351.213 76 2 6 -7 5263.39 384.678 62 -2 6 7 4357.52 381.214 62 -2 6 7 4338.49 335.437 61 -2 6 6 15239.9 722.780 11 -2 -6 6 15280.2 718.384 10 2 -6 -6 15345.4 681.111 5 -2 6 6 15548.8 671.718 16 2 -6 -6 15624.2 638.158 15 2 -6 -6 15148.4 672.098 9 2 6 -6 15591.4 650.972 6 2 -6 -6 15201.8 636.506 12 2 -6 -6 14392.4 632.381 65 2 -6 -6 15729.4 633.408 73 2 -6 -6 16188.2 648.611 72 -2 6 6 14444.4 649.831 76 -2 6 6 15419.4 656.767 66 2 -6 -6 15215.8 628.490 71 -2 6 6 14850.9 656.475 67 2 -6 -6 15951.1 641.078 63 -2 6 6 15843.2 669.137 64 -2 -6 6 15265.2 629.052 77 2 -6 -6 15735.1 641.085 70 -2 6 6 14208.5 655.349 75 2 -6 -6 15876.7 644.630 69 -2 6 6 14892.6 636.310 61 -2 6 6 14900.9 707.289 62 -2 6 5 6308.00 445.774 11 -2 -6 5 6647.02 443.026 10 2 -6 -5 6845.69 424.137 5 -2 6 5 7053.31 417.626 16 2 -6 -5 6712.48 389.716 15 2 -6 -5 6256.76 402.160 9 2 6 -5 6583.03 400.893 6 2 -6 -5 6746.19 394.172 12 2 -6 -5 6586.42 393.786 65 -2 6 5 6970.13 413.423 66 2 -6 -5 6488.58 385.014 73 2 -6 -5 7228.95 408.481 72 2 -6 -5 6351.06 378.857 63 2 -6 -5 7733.99 419.013 71 -2 6 5 6541.80 411.388 67 -2 6 5 6833.74 412.949 64 -2 -6 5 6974.09 379.272 77 2 -6 -5 7033.84 405.834 70 -2 6 5 7084.54 425.932 76 -2 6 5 6515.75 417.724 75 2 -6 -5 7180.39 408.523 69 -2 6 5 7025.20 458.872 62 -2 6 5 6559.91 394.931 61 -2 6 4 4405.89 357.717 11 -2 -6 4 4643.92 306.468 18 2 -6 -4 4763.10 339.597 5 -2 -6 4 4506.41 347.608 10 -2 6 4 4175.32 301.847 16 2 -6 -4 4384.35 301.294 15 2 -6 -4 4483.36 329.974 9 2 6 -4 5074.58 342.771 6 2 -6 -4 4535.30 309.617 12 -2 6 4 4820.53 334.038 66 2 -6 -4 4535.54 315.278 73 2 -6 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2 5 7147.07 487.945 74 -4 2 -5 7442.80 439.887 69 4 -2 5 6814.65 453.444 74 -4 2 -5 7537.46 447.055 64 4 2 5 6112.76 460.411 73 4 -2 5 7397.90 482.188 73 -4 -2 -5 6875.07 435.429 68 4 -2 5 7122.07 486.019 72 -4 2 -5 7704.48 443.555 68 4 2 5 6762.09 489.301 71 4 -2 5 7535.67 494.506 71 4 2 5 7028.00 485.105 67 -4 -2 -5 6954.04 442.302 70 4 2 5 7141.86 488.836 76 4 2 5 6916.68 474.188 75 4 -2 5 7790.67 484.501 75 -4 -2 -5 7086.33 443.430 66 -4 -2 -5 7104.45 439.878 61 -4 2 -5 7670.66 441.954 61 -4 2 -6 129.810 92.0155 8 4 2 6 51.8330 103.792 19 -4 -2 -6 253.403 131.475 7 4 2 6 73.4890 88.5436 17 -4 2 -6 96.1623 100.963 7 -4 -2 -6-62.6541 96.8113 14 -4 2 -6 132.553 89.4251 14 4 -2 6 88.1002 83.8568 13 4 -2 6 6.73448 67.2995 75 4 2 6 192.758 110.341 74 -4 -2 -6 166.632 94.8762 69 4 -2 6 64.4268 73.2070 74 -4 2 -6 19.0687 72.5292 69 4 2 6 139.487 104.578 73 4 -2 6 87.6111 67.3134 73 -4 -2 -6 142.194 97.2324 66 -4 2 -6 188.792 90.9271 64 -4 2 -6 134.223 93.3092 66 4 -2 6 73.1227 102.901 72 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4 -2 7 1850.59 262.535 73 -4 -2 -7 2045.37 251.060 68 -4 2 -7 2403.94 262.403 68 -4 2 -7 1821.30 237.442 64 -4 -2 -7 1950.91 245.001 66 4 -2 7 2015.17 270.448 72 4 2 7 1881.00 285.889 71 4 -2 7 2318.49 298.020 71 -4 -2 -7 2155.93 256.943 70 4 2 7 2019.99 275.466 76 4 2 7 2361.21 294.884 67 4 2 7 2025.99 277.051 75 4 2 7 2482.15 270.636 46 -4 -2 -7 2382.62 267.023 49 -4 -2 -7 2115.37 254.570 61 -4 2 -7 2142.47 247.287 61 4 -2 8 1858.93 233.959 38 -4 -2 -8 2348.41 258.992 28 4 -2 8 1820.90 236.302 36 4 2 8 1977.50 243.413 35 4 -2 8 1848.11 245.817 35 -4 2 -8 2228.80 245.582 39 -4 -2 -8 2153.65 246.410 39 -4 2 -8 2183.57 250.575 12 4 2 8 1748.68 269.556 19 4 2 8 1799.71 282.151 17 -4 2 -8 1861.50 264.356 7 -4 2 -8 1713.25 209.770 24 -4 -2 -8 1892.37 251.044 14 4 -2 8 2166.79 261.029 23 -4 2 -8 2156.16 268.170 14 4 2 8 1606.03 227.357 23 4 -2 8 2436.12 305.617 13 4 2 8 1736.97 237.666 22 4 -2 8 1972.85 237.366 22 -4 2 -8 2124.22 276.515 8 -4 2 -8 2719.25 277.718 69 4 -2 8 2973.06 319.472 74 4 2 8 2010.37 278.135 74 -4 -2 -8 1807.23 243.468 69 4 2 8 1958.79 285.342 73 4 -2 8 2423.71 295.759 73 -4 2 -8 2522.06 267.802 68 -4 -2 -8 2099.63 256.291 66 -4 -2 -8 1885.03 247.714 68 4 2 8 2017.11 291.773 71 4 -2 8 2300.73 297.539 71 -4 2 -8 2748.22 274.441 70 4 2 8 1746.62 262.312 76 4 -2 8 2616.15 305.432 76 -4 -2 -8 1861.64 242.094 70 4 2 8 1428.06 236.928 67 4 -2 8 2458.89 295.029 67 4 -2 8 2655.11 302.457 75 -4 2 -8 2685.15 276.610 66 4 2 8 2083.71 283.753 75 -4 -2 -8 2021.22 249.526 61 4 2 8 1724.03 234.359 46 -4 -2 -8 2269.30 258.043 49 -4 2 -8 1756.17 225.418 63 -4 2 -8 2759.92 278.570 61 -4 -2 -9 702.847 155.589 39 -4 -2 -9 395.287 140.069 28 4 -2 9 621.880 154.055 36 4 2 9 537.319 137.321 35 4 -2 9 317.766 124.739 35 -4 -2 -9 519.703 143.507 27 4 -2 9 437.379 139.111 38 -4 2 -9 534.944 142.031 39 -4 2 -9 267.242 115.245 7 -4 2 -9 358.507 120.355 24 4 2 9 379.605 155.945 23 4 -2 9 817.549 200.534 23 4 2 9 440.103 141.422 22 4 -2 9 624.778 150.476 22 4 -2 9 149.391 110.459 77 4 2 9 578.593 156.095 46 -4 -2 -9 572.571 150.083 49 4 -2 10 2133.76 267.656 23 4 2 10 2082.30 268.027 23 4 -2 10 1542.70 223.435 22 4 2 10 1871.71 250.679 22 -4 -2 -10 1693.28 210.836 39 4 -2 10 1924.61 248.866 38 -4 -2 -10 2048.87 248.245 28 4 -2 10 1983.00 254.695 36 -4 -2 -10 2153.41 254.566 27 4 2 10 1777.08 247.017 35 4 -2 10 1880.29 245.834 35 -4 2 -10 2199.74 238.982 39 -4 -2 -10 2112.82 249.223 49 4 2 10 2005.98 259.482 46 4 2 11 3365.43 328.429 23 4 -2 11 3416.31 323.093 23 4 -2 11 3330.38 307.544 22 4 2 11 3174.30 319.968 22 4 -2 11 3663.58 328.823 38 4 -2 11 3762.03 337.702 36 4 2 11 3520.25 334.292 35 4 -2 11 3676.11 333.448 35 -4 -2 -11 3810.29 321.525 27 -4 -2 -11 3464.36 313.285 28 -4 -2 -11 3716.25 298.208 39 -4 2 -11 3944.70 306.517 39 -4 2 -11 3939.08 326.938 49 -4 -2 -11 3612.91 310.645 49 4 2 11 3262.93 318.016 46 4 2 12 94.3581 105.486 23 4 -2 12-39.1131 103.474 23 4 -2 12-30.9316 91.6623 22 4 2 12 184.699 122.248 22 -4 2 -12-29.8979 65.6373 39 4 -2 12-20.8617 93.0845 38 -4 -2 -12-78.2825 90.2336 28 -4 2 -12 44.6020 89.3114 28 -4 -2 -12-26.0811 98.7182 37 4 2 12-49.6296 116.471 35 4 -2 12 28.9035 85.8062 35 -4 -2 -12 152.678 105.473 27 4 -2 12 30.1269 84.1557 40 4 2 12-177.533 97.4626 46 -4 -2 -12-30.2940 91.6471 49 -4 2 -12-140.106 98.2640 49 4 2 13 9471.58 500.076 23 4 -2 13 9083.06 475.445 23 4 -2 13 8500.77 439.093 22 4 2 13 9512.85 493.249 22 -4 -2 -13 8530.18 432.159 31 -4 -2 -13 9248.42 446.557 37 4 -2 13 9364.50 447.754 40 4 2 13 9552.22 489.983 35 4 -2 13 9258.75 482.754 35 -4 -2 -13 9877.14 464.570 27 -4 -2 -13 8687.26 436.301 28 -4 2 -13 9254.42 455.903 28 -4 -2 -13 9401.27 435.036 49 -4 2 -13 9856.59 460.119 49 4 2 13 9095.73 469.075 46 4 -2 14 4306.01 283.865 23 4 2 14 3868.22 278.647 22 -4 -2 -14 3977.68 260.954 31 -4 -2 -14 4083.36 264.259 37 -4 -2 -14 3977.66 261.902 27 4 2 14 4554.23 301.106 35 4 -2 14 4109.38 279.880 35 4 -2 14 4200.96 266.053 40 -4 2 -14 4320.04 274.236 27 -4 -2 -14 3871.24 249.408 28 -4 2 -14 4015.34 261.641 28 -4 2 -14 4104.33 261.119 49 4 2 14 4278.31 279.330 46 4 2 15 5100.19 275.024 22 -4 -2 -15 4797.93 250.310 37 -4 -2 -15 4991.48 250.291 27 -4 2 -15 4639.72 244.967 27 -4 -2 -15 4570.70 242.665 31 4 -2 15 5020.18 252.889 40 -4 -3 15-58.2212 62.2432 21 -4 -3 15-130.541 94.7329 50 -4 3 15 26.4808 61.6592 50 -4 -3 14 5239.67 322.502 21 -4 -3 14 4815.99 319.541 50 -4 3 14 4927.37 324.741 50 -4 -3 13 13397.9 572.443 21 -4 -3 13 12143.1 567.607 50 -4 3 13 12480.2 573.550 50 -4 -3 12 11090.9 537.492 21 -4 -3 12 9556.43 520.928 44 -4 -3 12 10769.3 554.801 50 -4 3 12 10379.4 544.954 50 -4 -3 11 691.938 154.505 21 -4 3 11 469.349 148.327 29 -4 3 11 349.909 110.524 32 -4 -3 11 428.794 141.193 50 -4 3 11 316.697 132.648 50 -4 -3 11 489.913 144.032 44 -4 -3 10 6533.81 419.231 21 -4 3 10 7756.99 508.119 29 -4 3 10 7129.33 464.790 34 -4 3 10 6521.53 396.341 32 -4 3 10 7567.20 469.657 50 -4 -3 10 5825.19 429.948 44 -4 -3 10 6813.02 448.515 50 -4 3 9 5135.97 410.504 29 -4 3 9 5591.95 416.830 34 -4 3 9 4503.68 329.859 32 -4 -3 9 5515.26 455.803 20 -4 3 9 5185.19 429.290 20 4 3 -9 4793.58 399.299 19 -4 -3 9 4646.58 427.309 16 -4 3 9 5333.89 456.671 16 4 -3 -9 4977.62 401.413 15 -4 -3 9 5336.79 371.620 21 4 -3 -9 4695.46 383.266 65 -4 3 9 5037.77 382.778 50 -4 3 9 5023.20 387.837 56 -4 -3 9 4036.30 363.582 44 -4 -3 9 4945.18 379.707 50 -4 3 8 10.0602 86.5177 34 -4 3 8 3.15346 97.0715 29 -4 3 8 57.6335 66.8587 32 -4 3 8-86.9119 86.7301 20 4 3 -8 200.971 99.2606 19 -4 -3 8 54.9101 109.050 16 -4 3 8-160.079 107.946 16 4 -3 -8 8.17513 73.7577 15 -4 -3 8-40.0029 87.6324 21 4 -3 -8 23.0777 65.1290 65 -4 -3 8 168.097 101.199 50 -4 3 8-2.70082 88.3906 50 -4 3 8-31.7093 102.627 43 -4 -3 8 91.6818 99.5187 44 -4 3 8-26.9638 112.682 56 -4 3 7 735.983 135.690 32 -4 3 7 721.261 170.579 34 -4 3 7 674.275 161.566 29 -4 3 7 824.203 169.462 20 4 3 -7 649.391 163.365 19 -4 3 7 569.721 134.944 18 4 -3 -7 681.243 165.004 17 -4 -3 7 532.652 160.580 16 -4 3 7 701.004 172.993 16 4 -3 -7 770.574 167.231 15 -4 -3 7 585.948 118.137 21 4 -3 -7 365.522 103.776 65 -4 -3 7 716.849 150.027 50 -4 3 7 498.684 147.210 56 -4 -3 7 360.376 135.069 44 -4 3 6 1744.04 232.781 20 4 3 -6 1573.43 210.362 19 -4 3 6 1320.04 210.380 18 4 -3 -6 1261.22 206.683 17 -4 -3 6 1534.67 230.229 16 -4 3 6 1443.64 219.061 16 4 -3 -6 1461.05 216.020 15 4 -3 -6 1519.93 213.039 65 -4 3 5 89399.5 2052.99 20 4 3 -5 82278.4 2025.12 19 -4 -3 5 79675.5 2026.74 18 -4 3 5 82052.3 2105.41 18 4 -3 -5 82083.0 1986.20 5 4 3 -5 82831.8 1982.73 17 4 -3 -5 88743.9 2111.07 17 -4 -3 5 85041.3 2118.07 16 -4 3 5 85417.7 2067.91 16 4 -3 -5 82584.6 2030.85 15 4 -3 -5 82856.6 2013.57 65 -4 3 4 7106.00 423.392 20 4 3 -4 6759.43 428.641 19 4 -3 -4 6456.86 405.143 19 -4 -3 4 6525.42 435.017 18 -4 3 4 6217.77 442.830 18 4 -3 -4 6384.26 399.358 5 4 3 -4 6464.58 404.543 17 4 -3 -4 7331.98 453.676 17 -4 -3 4 6765.47 451.621 16 -4 3 4 6829.91 423.111 16 4 -3 -4 6462.40 413.047 15 4 -3 -4 7387.31 420.804 74 -4 3 4 7177.86 418.654 66 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388.955 46 -7 3 4 7038.06 384.801 48 -7 3 4 6691.10 390.235 47 -7 -3 4 7254.71 411.964 44 7 -3 -3 2264.39 227.812 23 7 3 -3 2357.49 217.407 22 7 -3 -3 2575.46 235.419 22 7 -3 -3 2673.62 249.623 35 -7 -3 3 2100.26 209.413 24 -7 -3 3 2132.06 191.467 32 -7 3 3 2667.26 217.286 32 7 3 -3 2181.42 227.346 46 -7 3 3 2078.73 220.301 48 -7 3 3 2075.41 230.396 47 -7 -3 3 2350.26 242.430 44 7 -3 -2 5525.50 359.604 23 7 3 -2 5594.68 339.628 22 7 -3 -2 5628.90 350.384 22 7 -3 -2 6324.11 387.063 35 -7 -3 2 4906.79 302.054 33 -7 -3 2 5525.91 354.810 24 -7 -3 2 5536.01 314.188 32 -7 3 2 6124.68 333.455 32 -7 -3 2 5934.38 377.238 44 7 3 -2 5723.03 369.879 46 -7 3 2 5555.55 363.881 48 -7 3 2 5996.84 388.558 47 7 -3 -1 4185.40 317.850 23 7 3 -1 3625.40 275.353 22 7 -3 -1 3804.32 285.033 22 7 -3 -1 4403.43 322.644 35 -7 -3 1 3462.54 261.786 33 -7 3 1 3390.98 240.736 33 -7 -3 1 3603.83 290.846 24 -7 -3 1 3994.52 266.145 32 -7 3 1 4018.15 265.782 32 -7 -3 1 3947.17 311.658 44 7 3 -1 4354.12 320.005 46 7 -3 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48 -7 3 -1 6119.43 383.271 47 7 3 1 5762.53 387.522 52 -7 3 -2 188.120 100.237 24 7 -3 2 119.551 81.0345 23 7 3 2 303.578 102.883 22 7 -3 2 255.782 94.2205 22 -7 -3 -2 285.410 115.436 24 7 -3 2 268.090 115.936 35 -7 -3 -2 10.2493 70.6220 33 7 3 2 233.149 84.0434 42 -7 3 -2 278.650 101.119 33 -7 -3 -2 208.775 88.4700 32 7 3 2 215.572 100.475 46 -7 -3 -2 102.058 79.9631 44 -7 -3 -2 137.242 92.4682 55 -7 3 -2 127.056 85.1746 55 -7 3 -2 111.538 81.1867 48 -7 3 -2 196.429 105.326 47 7 3 2 264.530 102.178 52 7 -3 3 3326.79 272.112 23 7 3 3 3640.69 268.464 22 7 -3 3 3345.85 252.989 22 -7 3 -3 3831.77 283.893 24 7 -3 3 3600.66 274.172 35 -7 -3 -3 3710.05 263.860 33 -7 3 -3 3659.29 259.515 33 -7 -3 -3 3807.44 245.840 32 -7 -3 -3 3938.65 299.965 24 7 3 3 3704.68 290.823 46 -7 -3 -3 3431.21 256.802 44 -7 -3 -3 3844.32 277.119 55 -7 3 -3 3942.53 278.599 55 -7 3 -3 3636.71 264.331 48 -7 3 -3 3925.16 280.885 47 7 3 3 3565.63 284.355 52 -7 3 -4 155.746 82.8628 24 7 -3 4 418.352 110.219 23 7 3 4 342.470 100.367 22 7 -3 4 390.360 96.7954 22 -7 -3 -4 437.185 101.818 39 -7 -3 -4 479.450 115.586 24 7 -3 4 252.442 84.1353 35 -7 -3 -4 407.732 100.017 33 -7 3 -4 501.987 106.874 33 -7 -3 -4 381.236 85.8727 32 7 3 4 206.581 90.5743 46 -7 -3 -4 443.804 110.673 55 -7 3 -4 344.739 108.907 55 -7 3 -4 405.550 96.7026 48 -7 3 -4 565.705 110.722 47 7 3 4 243.348 91.8311 52 7 -3 5 1488.81 168.151 23 7 3 5 1546.56 166.751 22 7 -3 5 1230.04 141.818 22 -7 3 -5 1294.40 140.025 39 -7 3 -5 1625.54 179.673 24 7 -3 5 1619.45 169.314 35 -7 -3 -5 1389.42 151.676 33 -7 3 -5 1773.81 171.583 33 -7 -3 -5 1503.11 142.652 32 -7 -3 -5 1638.18 178.451 24 -7 -3 -5 1561.03 161.371 39 7 3 5 1574.61 175.730 46 -7 -3 -5 1333.62 144.057 49 -7 -3 -5 1463.39 162.699 55 -7 3 -5 1452.36 162.482 55 7 3 5 1532.32 170.375 52 -7 3 -6 953.999 133.934 24 7 -3 6 782.959 120.014 23 7 3 6 695.625 109.544 22 -7 -3 -6 722.994 116.168 39 -7 3 -6 764.886 105.000 39 7 -3 6 710.221 113.867 35 -7 -3 -6 847.095 110.509 33 -7 -3 -6 786.818 120.018 24 -7 3 -6 761.970 109.647 33 -7 -3 -6 848.462 102.783 32 7 3 6 895.830 131.422 46 -7 -3 -6 742.005 108.880 49 -7 -3 -6 689.693 110.159 55 -7 3 -6 883.343 119.544 55 -7 3 -7 113.308 57.4697 24 7 -3 7 243.845 77.6109 23 7 3 7 237.391 69.8625 22 -7 -3 -7 171.073 57.5831 39 7 -3 7 170.229 65.8001 35 -7 3 -7 209.634 68.2502 33 7 3 7 167.782 67.6365 46 7 -4 -7 2855.26 197.022 23 7 -4 -7 2087.96 168.623 22 7 -4 -7 2522.14 194.492 35 -7 4 7 2555.76 177.773 32 -7 -4 7 2320.59 194.834 44 7 -4 -6 510.333 103.805 23 7 -4 -6 543.906 102.797 22 7 -4 -6 582.936 114.759 35 -7 4 6 496.780 96.2303 32 -7 -4 6 437.961 109.113 44 7 4 -6 625.086 110.381 46 7 -4 -5 33.1918 71.3890 23 7 -4 -5-14.3435 56.7664 22 7 -4 -5 123.091 75.9516 35 -7 4 5-1.83387 67.2907 32 -7 -4 5 57.9191 80.0357 44 -7 4 5 44.2973 73.5855 56 7 4 -5 48.5776 66.5199 46 -7 4 5-14.5417 57.2746 48 -7 4 5-8.91370 64.9049 47 7 -4 -4 1337.02 169.509 23 7 -4 -4 1150.70 144.978 22 7 -4 -4 1298.68 170.561 35 -7 -4 4 1223.30 132.137 32 -7 4 4 1550.83 159.990 32 -7 4 4 1437.10 174.907 56 -7 -4 4 1255.83 169.914 44 7 4 -4 1158.89 151.330 46 -7 4 4 978.088 147.742 48 -7 4 4 1133.11 158.304 47 7 -4 -3 3416.43 275.166 23 7 -4 -3 2954.56 235.234 22 7 -4 -3 3378.40 268.913 35 -7 -4 3 2828.58 237.801 24 -7 -4 3 2983.22 210.182 32 -7 4 3 3148.52 230.004 32 7 4 -3 3277.37 254.668 46 -7 4 3 3230.33 258.091 56 -7 4 3 3120.65 256.802 48 -7 4 3 2724.92 248.384 47 -7 -4 3 2850.07 249.898 44 7 -4 -2 119.810 90.3959 23 7 -4 -2-26.4337 68.9734 22 -7 -4 2 29.5861 66.4412 24 7 -4 -2 175.877 104.591 35 -7 -4 2 4.80869 56.8687 33 -7 -4 2 42.0284 65.0281 32 -7 4 2 94.9064 77.6597 32 -7 4 2 154.224 81.1339 56 -7 -4 2 17.5551 83.8267 44 7 4 -2 6.86311 81.0237 46 -7 4 2 100.047 90.4419 48 -7 4 2 100.461 92.5803 47 7 -4 -1 2849.22 259.700 23 7 4 -1 2474.38 208.743 22 7 -4 -1 2425.67 213.826 22 7 -4 -1 2263.07 224.453 35 -7 -4 1 2152.23 201.725 33 -7 -4 1 2364.38 236.949 24 -7 -4 1 2636.64 207.141 32 -7 4 1 2729.29 206.443 32 -7 -4 1 2257.57 224.274 44 7 4 -1 2418.31 234.025 46 -7 -4 1 2302.03 209.766 55 -7 4 1 1997.77 193.042 55 -7 4 1 2372.18 230.718 48 -7 4 1 2407.22 241.597 47 7 -4 0 1411.35 183.196 23 7 4 0 1296.20 155.451 22 7 -4 0 1259.53 155.021 22 -7 -4 0 1231.34 174.088 24 7 -4 0 1221.35 172.237 35 -7 4 0 1276.98 150.352 33 -7 -4 0 1217.06 155.070 33 -7 4 0 1389.03 145.936 32 -7 -4 0 1356.63 153.056 32 7 4 0 1539.09 191.856 46 -7 -4 0 1368.32 175.300 44 -7 -4 0 1199.63 162.387 55 -7 4 0 1153.86 154.091 55 -7 4 0 1324.58 182.718 48 -7 4 0 1372.81 190.558 47 7 4 0 1309.67 185.881 52 -7 4 -1 1472.56 170.829 24 7 -4 1 1785.75 205.771 23 7 4 1 1617.46 175.424 22 7 -4 1 1652.56 172.089 22 7 -4 1 1692.36 175.145 38 -7 -4 -1 1386.50 188.656 24 7 -4 1 1775.55 197.366 35 -7 -4 -1 1827.10 190.522 33 -7 4 -1 1995.30 180.449 33 -7 -4 -1 1922.06 180.095 32 -7 -4 -1 1942.45 198.255 44 7 4 1 1613.00 189.378 46 -7 4 -1 1693.97 184.731 55 -7 -4 -1 1650.76 183.365 55 -7 4 -1 1559.29 191.031 48 -7 4 -1 2045.12 221.120 47 7 4 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80.2480 24 7 -4 4 148.452 87.5210 23 7 4 4 224.268 75.7552 22 -7 -4 -4 114.643 57.6302 39 7 -4 4 74.2970 66.5075 38 7 -4 4 240.728 79.6684 36 -7 -4 -4 216.014 96.8002 24 7 -4 4 163.332 71.9826 35 -7 -4 -4 111.667 61.5762 33 -7 4 -4 165.755 72.4225 33 -7 -4 -4 198.776 70.5965 32 7 4 4 199.432 83.6685 46 -7 -4 -4 165.575 60.3495 49 -7 -4 -4 181.371 87.3982 55 -7 4 -4 158.194 76.5339 55 -7 4 -4 283.958 85.3097 48 -7 4 -4 255.093 84.5514 47 7 4 4 208.897 88.1960 52 7 -4 5 1600.36 167.555 23 7 4 5 1629.81 153.857 22 7 -4 5 1607.48 149.095 38 -7 4 -5 2008.49 189.233 24 7 -4 5 1824.84 161.636 36 7 -4 5 1630.34 161.018 35 -7 -4 -5 1589.92 152.197 33 -7 4 -5 1995.15 170.241 33 -7 -4 -5 1845.13 176.496 24 -7 -4 -5 1838.51 151.993 32 -7 -4 -5 1901.19 168.956 39 -7 -4 -5 1437.23 147.588 49 -7 -4 -5 1667.93 167.188 55 -7 4 -5 1822.85 168.948 55 7 4 5 1673.89 173.042 52 7 4 5 1982.72 188.801 46 -7 4 -6 39.2667 59.3295 24 7 -4 6 20.2121 51.6532 23 -7 -4 -6 7.58061 48.8033 39 7 -4 6 20.2380 51.8792 35 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389.736 44 7 -5 -2 1704.42 189.432 23 7 -5 -2 1408.11 155.697 38 7 -5 -2 1444.13 171.937 35 -7 -5 2 1315.00 144.843 33 -7 5 2 1362.78 140.126 32 -7 -5 2 1102.33 156.227 24 -7 -5 2 1105.96 128.562 32 -7 5 2 1374.75 160.962 56 -7 -5 2 1250.81 159.300 44 7 5 -2 1181.89 147.642 46 -7 5 2 1463.41 173.250 48 -7 5 2 1316.68 172.445 47 7 5 -2 1218.29 164.514 52 7 -5 -1 4493.81 304.776 23 7 -5 -1 4839.54 289.072 38 7 -5 -1 4762.32 304.304 35 -7 -5 1 4482.57 307.178 24 -7 -5 1 4341.87 270.390 33 -7 -5 1 4384.79 251.688 32 -7 5 1 4510.31 245.751 32 7 5 -1 4161.79 278.926 46 -7 5 1 4412.79 262.610 55 -7 5 1 4481.77 301.400 48 -7 5 1 4541.23 307.430 47 7 5 -1 4991.74 327.681 52 -7 -5 1 4445.00 291.219 44 7 -5 0 8014.44 406.623 23 7 -5 0 7280.17 358.356 38 7 -5 0 7190.35 347.539 36 7 -5 0 7939.14 393.314 35 -7 -5 0 7120.67 357.808 33 -7 -5 0 7490.55 403.054 24 -7 5 0 7436.87 335.689 33 -7 -5 0 7931.39 347.401 32 7 5 0 7144.35 371.243 46 -7 5 0 7111.51 354.157 55 -7 5 0 8096.41 405.476 48 -7 5 0 7709.55 406.665 47 7 5 0 7710.09 413.193 52 -7 -5 0 7072.76 364.190 44 7 -5 1 3843.35 276.497 23 7 -5 1 4055.32 261.359 38 7 -5 1 3973.17 254.764 36 7 -5 1 3945.55 271.610 35 -7 -5 -1 3774.13 256.819 33 -7 5 -1 4047.70 246.530 33 -7 -5 -1 3792.39 285.478 24 7 5 1 4700.63 304.419 42 -7 -5 -1 4297.99 249.509 32 7 5 1 3772.45 266.239 46 -7 5 -1 3862.01 261.068 55 -7 5 -1 4381.25 289.634 48 -7 5 -1 4463.60 298.331 47 7 5 1 4133.65 301.600 52 -7 5 -2 443.310 101.588 24 7 -5 2 415.999 111.378 23 7 -5 2 459.908 91.6623 38 7 -5 2 574.695 108.205 36 7 -5 2 402.372 95.0889 35 -7 -5 -2 397.813 110.790 24 -7 -5 -2 370.811 90.1096 33 7 5 2 546.586 115.741 42 -7 5 -2 463.109 92.6059 33 -7 -5 -2 506.262 97.9280 32 7 5 2 451.136 111.139 46 -7 5 -2 414.903 103.213 55 -7 5 -2 449.930 106.344 48 -7 5 -2 741.212 129.838 47 7 5 2 467.904 119.236 52 -7 5 -3-59.7324 70.9315 24 7 -5 3 13.7810 65.8380 23 7 -5 3-15.9945 55.6937 38 7 -5 3 36.7686 54.2072 36 7 -5 3 13.7322 53.6650 35 -7 -5 -3-24.9475 75.5630 24 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57.4760 53.2125 32 -7 -6 5 17.5441 56.8286 44 -7 6 5 94.8973 64.5865 56 7 -6 -4-5.10806 58.0857 23 7 -6 -4-11.5921 49.4143 38 7 -6 -4 98.7104 70.5448 35 -7 6 4 3.98985 52.6669 32 -7 -6 4-72.0676 62.3463 44 -7 6 4-14.1512 57.4831 56 -7 6 4 123.984 66.4713 48 -7 6 4 62.3800 54.2487 47 7 -6 -3 107.118 81.7778 23 7 -6 -3 14.2895 63.6274 38 7 -6 -3 12.7934 56.5641 35 -7 6 3 110.351 52.5144 32 -7 -6 3 118.873 73.7619 44 -7 6 3 52.8173 60.4656 56 -7 6 3 139.344 79.2112 48 -7 6 3-14.2126 65.6221 47 7 6 -3 61.3257 58.9467 52 7 -6 -2 6459.43 336.604 23 7 -6 -2 6290.49 308.944 38 7 -6 -2 5820.75 285.302 36 7 -6 -2 6066.51 310.434 35 -7 6 2 5916.63 260.476 32 -7 6 2 6040.28 301.344 56 -7 6 2 6355.02 331.048 48 -7 6 2 6160.79 330.777 47 7 6 -2 5853.70 323.888 52 -7 -6 2 6104.00 306.070 44 7 -6 -1 33.7757 65.3175 23 7 -6 -1 83.8872 59.3377 38 7 -6 -1-74.6181 64.2948 36 7 -6 -1 93.5092 64.5938 35 -7 -6 1 2.42695 69.7874 24 7 6 -1 4.86544 65.6193 42 -7 -6 1-101.327 49.6956 32 -7 6 1 33.5147 47.3430 55 -7 6 1-111.342 78.9405 48 -7 6 1 17.2136 74.6043 47 7 6 -1-51.6820 64.0874 52 7 -6 0 228.342 86.7298 23 7 -6 0 328.592 84.9159 38 7 -6 0 258.434 76.4819 36 7 -6 0 189.551 69.9521 35 7 6 0 311.733 90.2763 42 -7 -6 0 218.871 83.3163 24 -7 -6 0 253.969 61.6638 32 7 6 0 221.646 82.2235 46 -7 6 0 338.742 82.9292 55 -7 6 0 298.854 93.5718 48 -7 6 0 92.5792 79.6023 47 7 6 0 195.279 87.0783 52 7 -6 1 145.068 69.7710 23 7 -6 1 264.120 81.4500 38 7 -6 1 213.421 76.8987 36 7 -6 1 176.972 69.7587 35 -7 -6 -1 102.200 60.7632 33 7 6 1 93.1740 72.5386 42 -7 6 -1 156.538 58.2944 33 -7 -6 -1 261.779 70.1460 32 -7 -6 -1 44.5419 66.7340 24 7 6 1 190.157 70.4078 46 -7 6 -1 155.468 70.0754 55 -7 6 -1 232.765 88.2672 48 -7 6 -1 42.8229 75.2097 47 7 6 1 227.585 92.6884 52 7 -6 2 6953.54 335.451 23 7 -6 2 7467.49 336.139 38 7 -6 2 7567.00 336.735 36 7 -6 2 6668.35 310.567 35 -7 -6 -2 7565.98 364.189 24 -7 -6 -2 6853.70 322.577 33 -7 6 -2 7087.08 308.181 33 7 6 2 7254.27 357.063 42 -7 -6 -2 7496.93 310.036 32 7 6 2 6693.25 321.930 46 -7 6 -2 7536.09 340.631 55 -7 6 -2 7495.66 343.422 48 -7 6 -2 7114.04 348.976 47 7 6 2 7103.82 361.823 52 7 -6 3 2215.64 178.136 23 7 -6 3 2666.22 188.968 38 -7 6 -3 2770.23 193.274 24 7 -6 3 3103.31 202.928 36 -7 -6 -3 2557.82 201.345 24 -7 6 -3 2520.45 176.935 33 -7 6 -3 2872.07 200.737 55 -7 6 -3 2776.88 200.105 47 7 6 3 2213.97 195.092 52 7 6 3 2627.10 190.716 46 7 6 3 2832.18 208.433 42 -7 6 -4 9500.14 352.255 33 -7 6 -4 10261.5 380.570 55 7 6 4 9334.47 393.880 52 7 -7 -2 3087.77 204.243 23 7 7 -2 3343.26 221.195 42 -7 7 2 3489.81 218.102 48 -7 7 2 3212.42 212.555 47 7 -7 -1 98.9286 67.8124 23 7 7 -1 65.4515 58.8905 42 -7 7 1 65.0993 57.2291 48 -7 7 1 157.953 66.5874 47 7 -7 0 210.698 74.7612 38 7 7 0 295.641 80.1862 42 -7 7 0 206.325 72.9775 48 -7 7 0 178.489 71.4565 47 7 7 1 47.8328 52.7837 42 -7 7 -1 72.7728 57.0734 47 0 0 0 0.00 0.00 0 TITL K-K7A2 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 6.546185 12.528805 15.120821 90.0000 92.4078 90.0000 ZERR 4.00 0.000053 0.000094 0.000149 0.0000 0.0008 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O UNIT 40.00 40.00 24.00 16.00 TREF HKLF 4 END ; _shelx_hkl_checksum 35490 _olex2_date_sample_data_collection 2021-02-14 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.308 _oxdiff_exptl_absorpt_empirical_full_min 0.769 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.13234(13) 0.49614(7) 0.28448(6) 0.0155(2) Uani 1 1 d . . . . . O3 O 0.28743(15) 0.73216(7) 0.25550(6) 0.0188(2) Uani 1 1 d . . . . . O2 O 0.47317(13) 0.50950(7) 0.30057(6) 0.0167(2) Uani 1 1 d . . . . . O4 O 0.32443(14) 0.87418(7) 0.34544(6) 0.0151(2) Uani 1 1 d D . . . . N1 N 0.23883(16) 0.53496(9) 0.47703(7) 0.0139(2) Uani 1 1 d . . . . . N2 N 0.24963(16) 0.75786(9) 0.48725(7) 0.0134(2) Uani 1 1 d . . . . . N6 N 0.82021(18) 0.83799(9) 0.29222(7) 0.0156(2) Uani 1 1 d . . . . . N4 N 0.78006(16) 0.95408(9) 0.40871(7) 0.0138(2) Uani 1 1 d . . . . . C5 C 0.29660(19) 0.53072(10) 0.32179(8) 0.0125(3) Uani 1 1 d . . . . . C1 C 0.26890(18) 0.59540(10) 0.40525(8) 0.0118(3) Uani 1 1 d . . . . . N3 N 0.76799(16) 0.76754(8) 0.42993(7) 0.0131(2) Uani 1 1 d . . . . . C8 C 0.78963(18) 0.85213(10) 0.37810(9) 0.0126(3) Uani 1 1 d . . . . . C2 C 0.27253(18) 0.70642(10) 0.41044(8) 0.0119(3) Uani 1 1 d . . . . . C6 C 0.29662(19) 0.77282(10) 0.32895(8) 0.0125(3) Uani 1 1 d . . . . . N5 N 0.72957(17) 0.70042(9) 0.56890(8) 0.0156(3) Uani 1 1 d . . . . . C3 C 0.21955(19) 0.69731(11) 0.55792(8) 0.0147(3) Uani 1 1 d . . . . . H3 H 0.202217 0.730816 0.613464 0.018 Uiso 1 1 calc R U . . . C9 C 0.75402(18) 0.97287(10) 0.49651(9) 0.0149(3) Uani 1 1 d . . . . . H9 H 0.746114 1.044079 0.517690 0.018 Uiso 1 1 calc R U . . . C4 C 0.21276(19) 0.58656(11) 0.55286(8) 0.0149(3) Uani 1 1 d . . . . . H4A H 0.188909 0.546584 0.604805 0.018 Uiso 1 1 calc R U . . . C7 C 0.74512(18) 0.78511(10) 0.51691(9) 0.0130(3) Uani 1 1 d . . . . . C10 C 0.7395(2) 0.89036(10) 0.55307(9) 0.0155(3) Uani 1 1 d . . . . . H10 H 0.726143 0.901751 0.614671 0.019 Uiso 1 1 calc R U . . . O5 O 0.20837(16) 0.38507(7) 0.77316(6) 0.0169(2) Uani 1 1 d . . . . . H5A H 0.740(2) 0.6345(14) 0.5459(11) 0.020 Uiso 1 1 d . U . . . H6A H 0.874(3) 0.8899(14) 0.2636(11) 0.020 Uiso 1 1 d . U . . . H5B H 0.734(2) 0.7109(13) 0.6265(12) 0.020 Uiso 1 1 d . U . . . H6B H 0.827(2) 0.7704(14) 0.2727(11) 0.020 Uiso 1 1 d . U . . . H4B H 0.775(2) 1.0081(14) 0.3709(12) 0.020 Uiso 1 1 d . U . . . H4 H 0.334(3) 0.9159(13) 0.2936(10) 0.025 Uiso 1 1 d D U . . . H5C H 0.308(3) 0.4044(14) 0.7384(12) 0.025 Uiso 1 1 d . U . . . H5D H 0.102(3) 0.4155(14) 0.7483(12) 0.025 Uiso 1 1 d . U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0167(5) 0.0141(5) 0.0159(5) -0.0035(3) 0.0016(4) -0.0010(3) O3 0.0312(6) 0.0138(5) 0.0115(5) -0.0006(4) 0.0034(4) -0.0010(4) O2 0.0159(5) 0.0152(5) 0.0195(5) -0.0029(4) 0.0054(4) 0.0015(4) O4 0.0221(5) 0.0099(4) 0.0134(5) 0.0002(3) 0.0018(4) -0.0012(4) N1 0.0140(5) 0.0138(5) 0.0140(5) 0.0013(4) 0.0021(4) -0.0005(4) N2 0.0131(5) 0.0142(5) 0.0129(5) -0.0015(4) 0.0010(4) 0.0001(4) N6 0.0216(6) 0.0115(6) 0.0139(6) 0.0001(4) 0.0048(4) -0.0022(4) N4 0.0162(5) 0.0106(5) 0.0147(6) 0.0013(4) 0.0020(4) -0.0005(4) C5 0.0173(6) 0.0071(6) 0.0135(6) 0.0032(5) 0.0036(5) 0.0005(5) C1 0.0089(6) 0.0131(6) 0.0134(6) 0.0004(5) 0.0013(5) -0.0003(5) N3 0.0137(5) 0.0120(5) 0.0138(5) -0.0002(4) 0.0019(4) -0.0001(4) C8 0.0094(6) 0.0128(6) 0.0158(6) -0.0004(5) 0.0007(5) -0.0002(5) C2 0.0099(6) 0.0129(6) 0.0130(6) -0.0007(5) 0.0012(5) 0.0004(5) C6 0.0117(6) 0.0117(6) 0.0143(6) -0.0002(5) 0.0013(5) 0.0009(5) N5 0.0218(6) 0.0124(6) 0.0127(6) 0.0004(4) 0.0028(4) 0.0006(4) C3 0.0153(6) 0.0181(7) 0.0110(6) -0.0014(5) 0.0017(5) 0.0002(5) C9 0.0135(6) 0.0133(6) 0.0178(7) -0.0033(5) 0.0014(5) -0.0004(5) C4 0.0150(6) 0.0175(7) 0.0123(6) 0.0020(5) 0.0019(5) -0.0006(5) C7 0.0089(6) 0.0152(6) 0.0150(6) 0.0001(5) 0.0016(5) 0.0002(5) C10 0.0164(6) 0.0163(6) 0.0138(6) -0.0025(5) 0.0023(5) 0.0001(5) O5 0.0172(5) 0.0166(5) 0.0173(5) 0.0003(4) 0.0039(4) 0.0006(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 O4 H4 113.1(11) . . ? C4 N1 C1 116.70(11) . . ? C3 N2 C2 116.51(11) . . ? C8 N6 H6A 117.9(11) . . ? C8 N6 H6B 117.1(11) . . ? H6A N6 H6B 121.3(15) . . ? C8 N4 C9 120.11(11) . . ? C8 N4 H4B 119.9(11) . . ? C9 N4 H4B 119.5(11) . . ? O1 C5 C1 115.05(11) . . ? O2 C5 O1 126.35(12) . . ? O2 C5 C1 118.33(11) . . ? N1 C1 C5 113.41(11) . . ? N1 C1 C2 121.29(12) . . ? C2 C1 C5 125.30(11) . . ? C8 N3 C7 117.65(11) . . ? N6 C8 N4 117.82(12) . . ? N3 C8 N6 119.49(12) . . ? N3 C8 N4 122.69(12) . . ? N2 C2 C1 121.73(12) . . ? N2 C2 C6 117.63(11) . . ? C1 C2 C6 120.62(11) . . ? O3 C6 O4 125.50(12) . . ? O3 C6 C2 120.85(11) . . ? O4 C6 C2 113.65(11) . . ? C7 N5 H5A 119.8(11) . . ? C7 N5 H5B 117.8(11) . . ? H5A N5 H5B 121.3(15) . . ? N2 C3 H3 119.0 . . ? N2 C3 C4 121.99(12) . . ? C4 C3 H3 119.0 . . ? N4 C9 H9 120.0 . . ? C10 C9 N4 119.97(12) . . ? C10 C9 H9 120.0 . . ? N1 C4 C3 121.75(12) . . ? N1 C4 H4A 119.1 . . ? C3 C4 H4A 119.1 . . ? N3 C7 C10 121.99(12) . . ? N5 C7 N3 117.51(12) . . ? N5 C7 C10 120.49(12) . . ? C9 C10 C7 117.49(12) . . ? C9 C10 H10 121.3 . . ? C7 C10 H10 121.3 . . ? H5C O5 H5D 102.7(16) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C5 1.2694(16) . ? O3 C6 1.2210(16) . ? O2 C5 1.2413(16) . ? O4 C6 1.3054(15) . ? O4 H4 0.947(14) . ? N1 C1 1.3447(16) . ? N1 C4 1.3336(17) . ? N2 C2 1.3421(16) . ? N2 C3 1.3318(17) . ? N6 C8 1.3339(17) . ? N6 H6A 0.863(18) . ? N6 H6B 0.899(18) . ? N4 C8 1.3610(16) . ? N4 C9 1.3661(17) . ? N4 H4B 0.886(18) . ? C5 C1 1.5169(17) . ? C1 C2 1.3933(17) . ? N3 C8 1.3293(17) . ? N3 C7 1.3479(17) . ? C2 C6 1.5006(17) . ? N5 C7 1.3270(17) . ? N5 H5A 0.900(17) . ? N5 H5B 0.880(18) . ? C3 H3 0.9500 . ? C3 C4 1.3903(19) . ? C9 H9 0.9500 . ? C9 C10 1.3476(19) . ? C4 H4A 0.9500 . ? C7 C10 1.4286(18) . ? C10 H10 0.9500 . ? O5 H5C 0.890(19) . ? O5 H5D 0.863(19) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C9 H9 O4 0.95 2.37 3.1226(16) 135.6 3_676 yes C9 H9 N2 0.95 2.48 3.3826(17) 158.1 3_676 yes N5 H5A N1 0.900(17) 2.157(18) 3.0387(16) 166.5(15) 3_666 yes N6 H6A O2 0.863(18) 2.068(18) 2.9284(15) 174.8(16) 2_655 yes N5 H5B O3 0.880(18) 2.093(18) 2.9544(15) 166.1(15) 4_676 yes N6 H6B O5 0.899(18) 2.077(18) 2.9677(15) 170.8(15) 3_666 yes N4 H4B O5 0.886(18) 2.027(18) 2.8985(15) 167.4(15) 4_675 yes O4 H4 O1 0.947(14) 1.572(14) 2.5142(12) 172.3(17) 2 yes O5 H5C O2 0.890(19) 1.905(19) 2.7439(13) 156.5(16) 3_666 yes O5 H5D O1 0.863(19) 1.94(2) 2.7903(13) 167.3(17) 3_566 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C5 C1 N1 79.49(14) . . . . ? O1 C5 C1 C2 -100.39(14) . . . . ? O2 C5 C1 N1 -94.89(14) . . . . ? O2 C5 C1 C2 85.23(16) . . . . ? N1 C1 C2 N2 1.10(19) . . . . ? N1 C1 C2 C6 -177.17(11) . . . . ? N2 C2 C6 O3 -168.97(11) . . . . ? N2 C2 C6 O4 10.22(16) . . . . ? N2 C3 C4 N1 0.9(2) . . . . ? N4 C9 C10 C7 -2.20(18) . . . . ? C5 C1 C2 N2 -179.04(11) . . . . ? C5 C1 C2 C6 2.69(19) . . . . ? C1 N1 C4 C3 -1.01(18) . . . . ? C1 C2 C6 O3 9.37(18) . . . . ? C1 C2 C6 O4 -171.43(11) . . . . ? N3 C7 C10 C9 1.29(18) . . . . ? C8 N4 C9 C10 0.57(18) . . . . ? C8 N3 C7 N5 -178.07(11) . . . . ? C8 N3 C7 C10 1.32(18) . . . . ? C2 N2 C3 C4 0.20(18) . . . . ? N5 C7 C10 C9 -179.34(12) . . . . ? C3 N2 C2 C1 -1.18(17) . . . . ? C3 N2 C2 C6 177.15(11) . . . . ? C9 N4 C8 N6 -178.39(11) . . . . ? C9 N4 C8 N3 2.24(18) . . . . ? C4 N1 C1 C5 -179.84(10) . . . . ? C4 N1 C1 C2 0.04(17) . . . . ? C7 N3 C8 N6 177.54(11) . . . . ? C7 N3 C8 N4 -3.10(18) . . . . ?