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Information card for entry 1572687
Preview
| Coordinates | 1572687.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H31 Cl2 F12 N9 P2 Pd Ru |
|---|---|
| Calculated formula | C42 H31 Cl2 F12 N9 P2 Pd Ru |
| Title of publication | Di(pyridin-2-yl)amino-substituted 1,10-phenanthrolines and their Ru(II)-Pd(II) dinuclear complexes: synthesis, characterization and application in Cu-free Sonogashira reaction. |
| Authors of publication | Ionova, Violetta A.; Dmitrieva, Alena V.; Abel, Anton S.; Sergeev, Aleksandr D.; Evko, Grigory S.; Yakushev, Alexei A.; Gontcharenko, Victoria E.; Nefedov, Sergei E.; Roznyatovsky, Vitaly A.; Cheprakov, Andrey V.; Averin, Alexei D.; Magdesieva, Tatiana V.; Beletskaya, Irina P. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2024 |
| Journal volume | 53 |
| Journal issue | 41 |
| Pages of publication | 17021 - 17035 |
| a | 12.8044 ± 0.0011 Å |
| b | 12.9789 ± 0.0012 Å |
| c | 17.6396 ± 0.0014 Å |
| α | 86.755 ± 0.003° |
| β | 71.875 ± 0.002° |
| γ | 76.129 ± 0.003° |
| Cell volume | 2704.3 ± 0.4 Å3 |
| Cell temperature | 120 K |
| Ambient diffraction temperature | 120 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0863 |
| Residual factor for significantly intense reflections | 0.0678 |
| Weighted residual factors for significantly intense reflections | 0.1664 |
| Weighted residual factors for all reflections included in the refinement | 0.1801 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 296510 (current) | 2024-12-06 | cif/ Updating files of 1572684, 1572685, 1572686, 1572687 Original log message: Adding full bibliography for 1572684--1572687.cif. |
1572687.cif |
| 294872 | 2024-09-25 | cif/ Adding structures of 1572684, 1572685, 1572686, 1572687 via cif-deposit CGI script. |
1572687.cif |
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Users of the data should acknowledge the original authors of the
structural data.