#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:33:55 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296379 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572717.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572717 loop_ _publ_author_name 'Larsen, Emil Mickey Hilligsøe' 'Brock-Nannestad, Theis' 'Skibsted, Jørgen' 'Reinholdt, Anders' 'Bendix, Jesper' _publ_section_title ; A homoleptic AgIII complex stabilized by succinimidate ligands. ; _journal_issue 43 _journal_name_full 'Chemical science' _journal_page_first 18067 _journal_page_last 18075 _journal_paper_doi 10.1039/d4sc04843a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety '0.25(C32 H48 Ag4 Cs4 N8 O24), 2(H2 O)' _chemical_formula_sum 'C8 H16 Ag Cs N2 O8' _chemical_formula_weight 509.01 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_date 2018-07-06 _audit_creation_method ; Olex2 1.2 (compiled 2015.09.30 svn.r3233 for OlexSys, GUI svn.r5103) ; _audit_update_record ; 2024-07-21 deposited with the CCDC. 2024-09-17 downloaded from the CCDC. ; _cell_angle_alpha 68.125(2) _cell_angle_beta 73.051(2) _cell_angle_gamma 76.873(2) _cell_formula_units_Z 4 _cell_length_a 9.7035(6) _cell_length_b 13.0999(8) _cell_length_c 13.5608(9) _cell_measurement_reflns_used 9570 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 29.538 _cell_measurement_theta_min 2.446 _cell_volume 1516.49(17) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 120(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0416 _diffrn_reflns_av_unetI/netI 0.0280 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 51926 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 29.575 _diffrn_reflns_theta_min 2.446 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 3.730 _exptl_absorpt_correction_T_max 0.7459 _exptl_absorpt_correction_T_min 0.6596 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0714 before and 0.0555 after correction. The Ratio of minimum to maximum transmission is 0.8843. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 2.229 _exptl_crystal_description plate _exptl_crystal_F_000 976 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: water' _exptl_crystal_size_max 0.226 _exptl_crystal_size_mid 0.098 _exptl_crystal_size_min 0.038 _refine_diff_density_max 0.706 _refine_diff_density_min -0.880 _refine_diff_density_rms 0.118 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.026 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 412 _refine_ls_number_reflns 8488 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.026 _refine_ls_R_factor_all 0.0346 _refine_ls_R_factor_gt 0.0218 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0186P)^2^+0.7325P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0419 _refine_ls_wR_factor_ref 0.0451 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7001 _reflns_number_total 8488 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04843a2.cif _cod_data_source_block mo_d8v3473_0m-1 _cod_depositor_comments 'Adding full bibliography for 1572714--1572719.cif.' _cod_database_code 1572717 _shelxl_version_number 2013-3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.871 _shelx_estimated_absorpt_t_min 0.486 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups, All O(H,H,H,H,H,H,H,H,H,H,H,H,H,H,H,H) groups 2. Restrained distances H12A_$1-H15C 2.2 with sigma of 0.01 3.a Secondary CH2 refined with riding coordinates: C11(H11A,H11B), C7(H7A,H7B), C10(H10A,H10B), C2(H2A,H2B), C3(H3A,H3B), C6(H6A, H6B), C14(H14A,H14B), C15(H15A,H15B) ; _shelx_res_file ; TITL CELL 0.71073 9.7035 13.0999 13.5608 68.125 73.0506 76.8726 ZERR 4 0.0006 0.0008 0.0009 0.0023 0.0024 0.0024 LATT 1 SFAC C H Ag Cs N O UNIT 32 64 4 4 8 32 EQIV $1 -1+X,+Y,+Z DFIX 2.2 0.01 H12a_$1 H15c L.S. 50 PLAN 20 SIZE 0.038 0.098 0.226 TEMP -153(2) CONN 12 2.4 Cs2 CONN 12 2.4 Cs1 MORE -1 BOND $H CONF fmap 2 acta 52 OMIT 10 0 14 OMIT 13 6 2 OMIT 7 -1 16 OMIT 3 -2 4 REM REM REM WGHT 0.018600 0.732500 FVAR 0.08756 CS2 4 0.924244 0.667205 0.077523 11.00000 0.01495 0.01530 = 0.02155 -0.00582 -0.00516 -0.00149 CS1 4 0.059173 0.988991 0.162374 11.00000 0.01448 0.01643 = 0.01666 -0.00218 -0.00437 -0.00349 AG3 3 0.500000 0.500000 0.000000 10.50000 0.01492 0.01608 = 0.01327 -0.00330 -0.00487 -0.00219 AG1 3 0.500000 1.000000 0.000000 10.50000 0.01539 0.01566 = 0.01178 -0.00320 -0.00621 -0.00059 AG2 3 0.499692 0.754940 -0.001956 11.00000 0.01464 0.01666 = 0.01340 -0.00390 -0.00403 -0.00249 O6 6 0.418173 0.857829 -0.250749 11.00000 0.01746 0.02527 = 0.02205 -0.00724 -0.00779 -0.00183 O4 6 0.598607 0.634417 0.230318 11.00000 0.01922 0.02445 = 0.02036 -0.00779 -0.00813 0.00135 C8 1 0.465087 0.648347 0.244159 11.00000 0.01937 0.01107 = 0.01524 -0.00495 -0.00575 -0.00054 N3 5 0.606615 0.810089 -0.165092 11.00000 0.01643 0.01564 = 0.01430 -0.00486 -0.00280 -0.00347 N2 5 0.394632 0.696191 0.161384 11.00000 0.01624 0.01550 = 0.01354 -0.00479 -0.00412 -0.00095 C12 1 0.549290 0.846953 -0.254172 11.00000 0.02048 0.01152 = 0.01621 -0.00504 -0.00573 -0.00118 O3 6 0.156856 0.747899 0.146543 11.00000 0.01987 0.02564 = 0.02266 -0.00712 -0.00836 0.00003 O5 6 0.830829 0.793779 -0.132417 11.00000 0.02182 0.02930 = 0.02294 -0.00567 -0.00951 -0.00706 C11 1 0.666382 0.875101 -0.358835 11.00000 0.02308 0.01890 = 0.01469 -0.00588 -0.00372 -0.00293 AFIX 23 H11A 2 0.650133 0.954563 -0.402570 11.00000 -1.20000 H11B 2 0.669058 0.829437 -0.403543 11.00000 -1.20000 AFIX 0 C5 1 0.247316 0.702278 0.202766 11.00000 0.01807 0.01277 = 0.02124 -0.00783 -0.00529 -0.00189 C7 1 0.358893 0.615988 0.354452 11.00000 0.02391 0.01725 = 0.01528 -0.00400 -0.00419 -0.00440 AFIX 23 H7A 2 0.366043 0.657550 0.400202 11.00000 -1.20000 H7B 2 0.376734 0.535419 0.393846 11.00000 -1.20000 AFIX 0 C10 1 0.806117 0.848048 -0.319161 11.00000 0.01839 0.02210 = 0.01782 -0.00676 -0.00048 -0.00372 AFIX 23 H10A 2 0.871480 0.786616 -0.341556 11.00000 -1.20000 H10B 2 0.858090 0.913785 -0.348043 11.00000 -1.20000 AFIX 0 O1 6 0.338322 0.912964 0.264002 11.00000 0.01508 0.02784 = 0.02076 -0.00755 -0.00547 -0.00097 C2 1 0.556214 0.849769 0.337340 11.00000 0.01793 0.01953 = 0.01318 -0.00418 -0.00486 -0.00185 AFIX 23 H2A 2 0.541776 0.771216 0.377969 11.00000 -1.20000 H2B 2 0.526091 0.891788 0.389269 11.00000 -1.20000 AFIX 0 C9 1 0.753967 0.814151 -0.196246 11.00000 0.01807 0.01220 = 0.02200 -0.00610 -0.00510 -0.00261 C1 1 0.472090 0.899706 0.248204 11.00000 0.01833 0.01088 = 0.01430 -0.00401 -0.00586 -0.00177 N1 5 0.563215 0.928119 0.147332 11.00000 0.01594 0.01267 = 0.01232 -0.00289 -0.00597 -0.00105 C3 1 0.713466 0.859449 0.275325 11.00000 0.01637 0.02421 = 0.01637 -0.00536 -0.00661 -0.00324 AFIX 23 H3A 2 0.754343 0.910961 0.293750 11.00000 -1.20000 H3B 2 0.774218 0.786107 0.291804 11.00000 -1.20000 AFIX 0 O2 6 0.810919 0.917882 0.079650 11.00000 0.01706 0.02475 = 0.01800 -0.00486 -0.00129 -0.00258 C6 1 0.211081 0.647686 0.325108 11.00000 0.02037 0.02177 = 0.01917 -0.00677 -0.00157 -0.00346 AFIX 23 H6A 2 0.162999 0.581174 0.346135 11.00000 -1.20000 H6B 2 0.146723 0.699880 0.361583 11.00000 -1.20000 AFIX 0 N4 5 0.592547 0.432990 0.135721 11.00000 0.01654 0.01353 = 0.01528 -0.00474 -0.00613 -0.00087 C16 1 0.737623 0.426555 0.129029 11.00000 0.01865 0.01381 = 0.02256 -0.00929 -0.00836 -0.00036 C14 1 0.627083 0.347908 0.316824 11.00000 0.02775 0.01742 = 0.01939 -0.00617 -0.01279 0.00080 AFIX 23 H14A 2 0.619922 0.269083 0.361514 11.00000 -1.20000 H14B 2 0.607854 0.392224 0.365859 11.00000 -1.20000 AFIX 0 C15 1 0.774925 0.361344 0.238423 11.00000 0.02142 0.02476 = 0.02296 -0.00909 -0.01222 0.00127 AFIX 23 H15A 2 0.831101 0.402683 0.257624 11.00000 -1.20000 H15B 2 0.831714 0.288303 0.238346 11.00000 -1.20000 AFIX 0 C13 1 0.523026 0.390860 0.241878 11.00000 0.02038 0.01171 = 0.01789 -0.00566 -0.00634 -0.00084 O8 6 0.825896 0.468968 0.045254 11.00000 0.01852 0.02397 = 0.02372 -0.00767 -0.00337 -0.00588 O7 6 0.389868 0.390295 0.273879 11.00000 0.02038 0.02463 = 0.01700 -0.00496 -0.00303 -0.00289 C4 1 0.704570 0.904608 0.156815 11.00000 0.01718 0.01101 = 0.01613 -0.00502 -0.00603 -0.00067 O9 6 -0.050278 0.847661 0.421662 11.00000 0.02036 0.02891 = 0.02507 -0.00903 -0.00369 -0.00638 O13 6 0.210175 0.331685 0.480669 11.00000 0.02619 0.02401 = 0.01816 -0.00569 -0.00328 -0.00737 O11 6 -0.172004 1.183099 0.077475 11.00000 0.01746 0.03631 = 0.02256 -0.00647 -0.00774 -0.00252 O14 6 0.200694 0.840350 0.486812 11.00000 0.02807 0.04318 = 0.02436 -0.01178 -0.00476 -0.00942 O10 6 -0.197500 1.057585 0.369658 11.00000 0.03597 0.02827 = 0.03218 -0.00957 -0.01875 0.00162 O12 6 1.160903 0.463194 0.175366 11.00000 0.02852 0.06167 = 0.02936 -0.01683 -0.01225 0.01090 O15 6 -0.024536 0.410697 0.377887 11.00000 0.02920 0.07548 = 0.04390 -0.03220 -0.02038 0.01230 O16 6 0.750923 0.572496 0.389392 11.00000 0.08344 0.04249 = 0.06416 -0.03509 -0.05883 0.02883 H14C 2 0.240772 0.863751 0.419366 11.00000 -1.20000 H14D 2 0.130568 0.826552 0.484744 11.00000 -1.20000 H12A 2 1.241223 0.447149 0.188624 11.00000 -1.20000 H12B 2 1.180727 0.459516 0.113930 11.00000 -1.20000 H11C 2 -0.185598 1.195778 0.022328 11.00000 -1.20000 H11D 2 -0.257601 1.178715 0.119835 11.00000 -1.20000 H16A 2 0.814305 0.520465 0.384465 11.00000 -1.20000 H16B 2 0.702220 0.586267 0.353976 11.00000 -1.20000 H13A 2 0.272031 0.350716 0.422023 11.00000 -1.20000 H13B 2 0.226776 0.362076 0.521148 11.00000 -1.20000 H9A 2 -0.106414 0.909886 0.416046 11.00000 -1.20000 H9B 2 -0.109880 0.795368 0.450220 11.00000 -1.20000 H10C 2 -0.217869 1.088698 0.418752 11.00000 -1.20000 H10D 2 -0.271762 1.082529 0.357003 11.00000 -1.20000 H15C 2 0.033568 0.422467 0.309527 11.00000 -1.20000 H15D 2 0.033708 0.390908 0.420498 11.00000 -1.20000 HKLF 4 REM REM R1 = 0.0218 for 7001 Fo > 4sig(Fo) and 0.0346 for all 8488 data REM 412 parameters refined using 1 restraints END WGHT 0.0186 0.7325 REM Highest difference peak 0.706, deepest hole -0.880, 1-sigma level 0.118 Q1 1 -0.0837 0.3593 0.4338 11.00000 0.05 0.71 Q2 1 0.5801 0.7756 -0.1128 11.00000 0.05 0.55 Q3 1 0.7924 0.5932 0.3352 11.00000 0.05 0.51 Q4 1 0.6800 0.8463 -0.0780 11.00000 0.05 0.50 Q5 1 0.0147 1.0420 0.2214 11.00000 0.05 0.49 Q6 1 0.9038 0.6592 0.0320 11.00000 0.05 0.49 Q7 1 0.7044 0.5775 0.3979 11.00000 0.05 0.49 Q8 1 0.3184 0.6998 0.1953 11.00000 0.05 0.49 Q9 1 0.4375 0.7128 0.1122 11.00000 0.05 0.49 Q10 1 0.0581 0.7415 0.1636 11.00000 0.05 0.48 Q11 1 0.3206 0.8782 0.3178 11.00000 0.05 0.47 Q12 1 0.2040 0.6098 0.2986 11.00000 0.05 0.47 Q13 1 0.3915 0.6372 0.3021 11.00000 0.05 0.45 Q14 1 0.5337 0.9448 0.1016 11.00000 0.05 0.45 Q15 1 0.5005 0.6690 0.0925 11.00000 0.05 0.45 Q16 1 0.5857 0.8233 -0.0819 11.00000 0.05 0.44 Q17 1 -0.2546 1.0545 0.4186 11.00000 0.05 0.44 Q18 1 0.7552 0.3855 0.1893 11.00000 0.05 0.44 Q19 1 0.1002 0.9516 0.1188 11.00000 0.05 0.43 Q20 1 0.3246 0.6679 0.0980 11.00000 0.05 0.43 ; _shelx_res_checksum 20316 _shelx_hkl_file ; -2 0 0 309.17 6.85 -2 0 0 313.30 6.71 -2 0 0 294.13 6.70 -2 0 0 301.31 6.56 2 0 0 271.07 6.54 2 0 0 311.17 6.69 2 0 0 292.02 6.69 2 0 0 304.94 6.85 -3 0 0 220.55 5.11 -3 0 0 229.42 5.33 -3 0 0 231.07 5.33 3 0 0 237.81 5.31 3 0 0 234.23 5.54 3 0 0 220.00 5.30 3 0 0 230.89 5.12 -4 0 0 87.77 2.51 -4 0 0 90.61 2.41 -4 0 0 84.61 2.38 -4 0 0 84.45 2.11 -4 0 0 89.80 2.65 4 0 0 87.21 2.34 4 0 0 81.64 2.34 4 0 0 87.39 2.61 4 0 0 86.31 2.12 -5 0 0 70.55 2.14 -5 0 0 69.34 2.14 -5 0 0 68.45 1.81 -5 0 0 71.45 2.28 5 0 0 67.88 2.09 5 0 0 68.80 2.07 5 0 0 73.34 2.41 5 0 0 70.28 1.81 -6 0 0 1.45 0.49 -6 0 0 1.60 0.37 -6 0 0 1.82 0.42 -6 0 0 1.55 0.43 6 0 0 0.96 0.37 6 0 0 1.75 0.36 6 0 0 1.56 0.34 6 0 0 1.77 0.25 -7 0 0 301.61 7.60 -7 0 0 312.59 7.64 -7 0 0 305.97 7.79 -7 0 0 302.11 8.08 7 0 0 303.81 6.96 7 0 0 305.38 7.43 7 0 0 303.48 7.50 7 0 0 313.44 8.05 -8 0 0 5.06 0.80 -8 0 0 6.07 0.93 -8 0 0 5.85 0.78 -8 0 0 3.71 0.83 8 0 0 6.17 0.80 8 0 0 5.78 0.96 8 0 0 5.46 0.47 8 0 0 4.94 0.66 -9 0 0 165.86 4.91 -9 0 0 173.65 4.94 -9 0 0 150.85 5.29 -9 0 0 179.64 5.20 9 0 0 144.94 4.46 9 0 0 169.98 4.69 9 0 0 163.08 5.35 -10 0 0 6.47 1.24 -10 0 0 9.42 1.20 -10 0 0 7.13 1.25 -10 0 0 8.87 1.24 10 0 0 8.44 1.15 10 0 0 7.26 1.27 10 0 0 7.65 0.95 -11 0 0 23.59 2.50 -11 0 0 21.44 2.04 -11 0 0 21.84 2.51 -11 0 0 21.94 2.53 -11 0 0 21.63 2.26 11 0 0 24.69 1.71 11 0 0 22.96 1.73 -12 0 0 35.03 2.70 -12 0 0 26.95 3.38 -12 0 0 33.93 3.32 12 0 0 31.83 2.25 12 0 0 29.74 2.20 12 -1 0 4.66 1.30 12 -1 0 5.79 1.22 -12 1 0 4.21 1.37 -12 1 0 5.21 1.72 -12 1 0 4.69 1.78 11 -1 0 16.84 1.71 11 -1 0 18.09 1.76 -11 1 0 12.23 1.58 -11 1 0 18.19 2.49 -11 1 0 17.19 2.37 -11 1 0 14.41 1.90 -11 1 0 17.22 2.06 10 -1 0 30.59 2.47 10 -1 0 31.50 1.77 10 -1 0 34.23 1.88 -10 1 0 29.75 2.49 -10 1 0 32.85 2.11 -10 1 0 31.45 2.04 -10 1 0 30.02 2.29 -10 1 0 32.13 2.50 9 -1 0 36.35 1.36 9 -1 0 31.65 2.22 9 -1 0 34.19 1.74 9 -1 0 36.33 1.82 -9 1 0 36.25 2.14 -9 1 0 40.65 2.40 -9 1 0 36.11 1.95 -9 1 0 33.51 1.92 8 -1 0 45.73 1.53 8 -1 0 46.38 1.89 8 -1 0 48.43 2.35 8 -1 0 44.62 1.91 -8 1 0 44.71 2.02 -8 1 0 43.88 1.99 -8 1 0 45.32 2.16 -8 1 0 43.15 2.33 7 -1 0 10.06 1.10 7 -1 0 9.30 0.84 7 -1 0 9.19 0.64 7 -1 0 11.43 0.90 -7 1 0 8.66 0.89 -7 1 0 10.17 0.66 -7 1 0 8.28 1.10 -7 1 0 8.83 1.02 -7 1 0 6.40 0.82 6 -1 0 0.73 0.24 6 -1 0 0.61 0.31 6 -1 0 1.31 0.43 6 -1 0 0.75 0.34 -6 1 0 1.29 0.41 -6 1 0 1.35 0.38 -6 1 0 1.09 0.26 -6 1 0 1.24 0.44 -6 1 0 0.47 0.36 5 -1 0 7.99 0.52 5 -1 0 8.64 0.66 5 -1 0 9.65 0.67 5 -1 0 9.67 0.85 -5 1 0 9.94 0.88 -5 1 0 8.62 0.77 -5 1 0 8.69 0.53 -5 1 0 9.26 0.70 -5 1 0 8.09 0.67 4 -1 0 78.50 2.16 4 -1 0 84.17 2.56 4 -1 0 87.29 2.36 4 -1 0 80.18 2.35 -4 1 0 85.59 2.39 -4 1 0 83.47 2.38 -4 1 0 81.83 2.57 -4 1 0 83.34 2.50 -4 1 0 86.33 2.20 3 -1 0 61.85 1.81 3 -1 0 64.83 1.72 3 -1 0 64.47 1.98 3 -1 0 64.65 1.81 -3 1 0 64.64 1.98 -3 1 0 64.12 1.83 -3 1 0 65.37 1.71 -3 1 0 65.84 1.93 -3 1 0 63.16 1.83 2 -1 0 75.67 1.90 2 -1 0 76.98 2.04 2 -1 0 70.45 1.90 2 -1 0 72.63 1.83 -2 1 0 73.70 1.91 -2 1 0 71.39 1.83 -2 1 0 72.23 2.01 1 -1 0 39.95 1.04 1 -1 0 36.95 1.01 1 -1 0 38.12 1.07 -1 1 0 38.35 1.03 -1 1 0 38.42 1.02 -1 1 0 37.66 1.02 -1 -1 0 0.19 0.04 -1 -1 0 0.16 0.05 -1 -1 0 0.24 0.09 -1 -1 0 0.27 0.07 1 1 0 0.28 0.06 1 1 0 0.20 0.05 1 1 0 0.15 0.04 -2 -1 0 0.99 0.21 -2 -1 0 1.16 0.16 -2 -1 0 0.94 0.14 2 1 0 1.10 0.15 2 1 0 1.45 0.17 2 1 0 1.41 0.24 -3 -1 0 18.03 0.70 -3 -1 0 18.09 0.69 -3 -1 0 17.99 0.86 3 1 0 18.24 0.68 3 1 0 18.72 0.67 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0.72 -6 2 0 6.25 0.83 -6 2 0 6.04 0.73 5 -2 0 6.57 0.53 5 -2 0 5.74 0.61 5 -2 0 6.09 0.77 5 -2 0 5.83 0.62 -5 2 0 6.21 0.71 -5 2 0 6.52 0.54 -5 2 0 5.99 0.77 -5 2 0 6.20 0.65 -5 2 0 6.73 0.65 4 -2 0 10.13 0.67 4 -2 0 8.93 0.63 4 -2 0 8.93 0.75 4 -2 0 8.99 0.56 -4 2 0 8.75 0.76 -4 2 0 8.47 0.64 -4 2 0 9.09 0.73 -4 2 0 9.19 0.66 -4 2 0 9.53 0.58 3 -2 0 3.65 0.41 3 -2 0 3.52 0.40 3 -2 0 3.88 0.37 3 -2 0 3.39 0.47 -3 2 0 3.48 0.40 -3 2 0 3.34 0.36 -3 2 0 3.41 0.45 -3 2 0 2.42 0.39 -3 2 0 3.12 0.39 2 -2 0 18.34 0.74 2 -2 0 16.59 0.70 2 -2 0 18.71 0.86 2 -2 0 17.34 0.73 -2 2 0 17.14 0.73 -2 2 0 18.15 0.74 -2 2 0 18.40 0.79 -2 2 0 18.11 0.77 -2 2 0 20.18 0.91 -2 2 0 17.98 0.72 1 -2 0 22.66 0.72 1 -2 0 23.58 0.83 1 -2 0 21.77 0.77 1 -2 0 24.08 0.77 1 -2 0 21.52 0.75 -1 2 0 21.86 0.77 -1 2 0 23.04 0.73 -1 2 0 23.31 0.76 -1 2 0 22.45 0.75 -1 2 0 22.46 0.75 -1 2 0 22.00 0.81 0 -2 0 7.76 0.33 0 -2 0 7.23 0.36 0 -2 0 8.17 0.34 0 -2 0 7.76 0.33 0 2 0 7.75 0.32 0 2 0 7.66 0.28 0 2 0 7.03 0.36 -1 -2 0 10.83 0.41 -1 -2 0 10.37 0.36 -1 -2 0 10.63 0.37 1 2 0 10.58 0.40 1 2 0 10.68 0.34 1 2 0 10.73 0.34 -2 -2 0 147.71 3.38 -2 -2 0 155.25 3.47 -2 -2 0 152.22 3.72 2 2 0 150.08 3.44 2 2 0 153.67 3.42 2 2 0 152.03 3.38 -3 -2 0 98.68 2.47 -3 -2 0 98.43 2.75 -3 -2 0 100.03 2.47 3 2 0 97.83 2.42 3 2 0 98.16 2.40 3 2 0 105.61 2.77 -4 -2 0 70.02 1.95 -4 -2 0 70.68 1.95 -4 -2 0 69.51 2.25 4 2 0 70.54 2.23 4 2 0 71.46 1.89 4 2 0 70.45 1.88 -5 -2 0 2.10 0.47 -5 -2 0 3.24 0.43 -5 -2 0 1.96 0.40 -5 -2 0 3.11 0.43 5 2 0 3.17 0.39 5 2 0 3.21 0.39 5 2 0 2.99 0.52 -6 -2 0 7.48 0.74 -6 -2 0 6.66 0.86 -6 -2 0 7.00 0.64 -6 -2 0 7.77 0.67 6 2 0 7.70 0.83 6 2 0 7.47 0.59 6 2 0 6.60 0.55 -7 -2 0 10.40 0.96 -7 -2 0 10.72 0.87 -7 -2 0 9.78 0.83 -7 -2 0 8.79 1.10 7 2 0 10.10 1.06 7 2 0 9.47 0.72 7 2 0 10.12 0.74 -8 -2 0 28.78 1.49 -8 -2 0 28.43 1.86 -8 -2 0 29.16 1.63 -8 -2 0 28.44 1.49 8 2 0 30.45 1.32 8 2 0 29.22 1.32 8 2 0 29.77 1.81 -9 -2 0 46.81 2.10 -9 -2 0 48.08 2.26 -9 -2 0 47.43 2.60 -9 -2 0 48.92 2.11 9 2 0 46.37 2.47 9 2 0 44.87 1.80 9 2 0 45.26 1.82 -10 -2 0 34.74 2.21 -10 -2 0 36.42 2.07 -10 -2 0 35.37 2.01 -10 -2 0 29.73 2.42 10 2 0 31.29 2.38 10 2 0 34.86 1.66 10 2 0 31.68 1.58 -11 -2 0 27.50 2.44 -11 -2 0 24.43 2.65 -11 -2 0 22.00 2.00 -11 -2 0 20.51 2.03 11 2 0 24.46 1.60 11 2 0 21.05 2.42 11 2 0 25.97 1.55 -12 -2 0 12.11 1.64 -12 -2 0 7.00 2.46 -12 -2 0 15.24 2.15 12 2 0 9.05 1.07 12 2 0 14.28 1.52 12 -3 0 -0.24 1.40 12 -3 0 -1.92 1.25 -12 3 0 1.34 1.75 -12 3 0 0.73 1.65 -12 3 0 0.31 1.34 11 -3 0 -0.30 0.97 11 -3 0 -1.45 0.98 11 -3 0 -1.37 0.70 -11 3 0 -0.88 1.19 -11 3 0 1.43 1.34 -11 3 0 1.97 1.12 10 -3 0 3.65 1.28 10 -3 0 4.66 0.73 10 -3 0 4.13 0.97 10 -3 0 2.39 0.84 -10 3 0 4.75 1.12 -10 3 0 3.81 1.12 -10 3 0 2.12 1.06 -10 3 0 3.41 1.12 -10 3 0 2.25 1.16 9 -3 0 20.71 1.53 9 -3 0 18.56 1.22 9 -3 0 20.30 1.99 9 -3 0 19.27 1.54 -9 3 0 18.22 1.96 -9 3 0 20.86 1.89 -9 3 0 19.59 1.73 -9 3 0 17.54 1.58 -9 3 0 18.04 1.83 8 -3 0 18.17 1.12 8 -3 0 21.31 1.41 8 -3 0 21.45 1.39 8 -3 0 17.68 1.67 -8 3 0 19.47 1.44 -8 3 0 18.01 1.16 -8 3 0 18.33 1.72 -8 3 0 18.41 1.62 -8 3 0 21.11 1.70 -8 3 0 19.81 1.47 7 -3 0 113.11 3.47 7 -3 0 113.64 3.56 7 -3 0 111.82 3.89 7 -3 0 110.24 3.25 -7 3 0 119.31 3.79 -7 3 0 116.57 3.93 -7 3 0 112.56 3.57 -7 3 0 113.61 3.29 -7 3 0 111.83 3.60 -7 3 0 114.39 3.95 6 -3 0 127.68 3.57 6 -3 0 132.17 3.75 6 -3 0 132.72 3.81 6 -3 0 128.96 4.07 -6 3 0 129.57 3.80 -6 3 0 128.72 3.57 -6 3 0 135.15 3.96 -6 3 0 128.14 3.82 -6 3 0 126.05 4.08 -6 3 0 129.88 4.07 5 -3 0 45.49 1.68 5 -3 0 42.61 1.70 5 -3 0 43.58 1.58 5 -3 0 43.11 1.89 -5 3 0 44.83 1.72 -5 3 0 44.15 1.91 -5 3 0 44.66 1.81 -5 3 0 45.51 1.87 -5 3 0 43.23 1.72 -5 3 0 43.09 1.58 4 -3 0 12.11 0.78 4 -3 0 13.06 0.74 4 -3 0 13.20 0.80 4 -3 0 12.48 0.92 -4 3 0 12.21 0.80 -4 3 0 13.17 0.82 -4 3 0 12.18 0.86 -4 3 0 14.66 0.93 -4 3 0 13.36 0.77 -4 3 0 14.15 1.03 3 -3 0 28.82 1.13 3 -3 0 29.12 1.28 3 -3 0 27.56 1.13 3 -3 0 30.04 1.17 -3 3 0 30.08 1.23 -3 3 0 29.99 1.19 -3 3 0 29.15 1.14 -3 3 0 29.09 1.14 -3 3 0 28.98 1.13 -3 3 0 29.12 1.28 2 -3 0 100.19 2.74 2 -3 0 92.84 2.60 2 -3 0 96.87 2.62 2 -3 0 104.31 2.65 -2 3 0 96.79 2.60 -2 3 0 95.79 2.61 -2 3 0 104.43 2.60 -2 3 0 99.40 2.63 -2 3 0 97.19 2.72 -2 3 0 97.21 2.61 1 -3 0 171.17 4.28 1 -3 0 189.56 4.16 1 -3 0 181.35 4.37 1 -3 0 184.10 4.25 1 -3 0 174.87 4.24 -1 3 0 171.69 4.29 -1 3 0 181.20 4.20 -1 3 0 176.72 4.22 -1 3 0 177.43 4.23 0 -3 0 116.43 2.74 0 -3 0 113.43 2.77 0 -3 0 112.21 2.86 0 -3 0 119.55 2.79 0 3 0 115.11 2.67 0 3 0 115.17 2.74 0 3 0 115.29 2.87 0 3 0 115.23 2.75 -1 -3 0 163.73 3.63 -1 -3 0 153.13 3.63 -1 -3 0 149.38 3.70 1 3 0 156.71 3.56 1 3 0 152.92 3.70 1 3 0 167.94 3.58 -2 -3 0 123.47 2.91 -2 -3 0 120.82 2.91 -2 -3 0 125.49 2.89 2 3 0 124.30 2.82 2 3 0 121.14 2.90 2 3 0 124.35 2.80 -3 -3 0 88.66 2.17 -3 -3 0 87.14 2.05 -3 -3 0 86.16 2.21 -3 -3 0 89.41 2.53 3 3 0 84.73 2.09 3 3 0 84.17 2.04 3 3 0 85.71 2.07 -4 -3 0 -0.16 0.18 -4 -3 0 0.07 0.15 -4 -3 0 0.01 0.15 4 3 0 0.29 0.13 4 3 0 0.27 0.15 -5 -3 0 15.32 1.03 -5 -3 0 14.15 0.74 -5 -3 0 13.96 0.74 -5 -3 0 14.47 0.81 5 3 0 14.58 0.68 5 3 0 14.58 0.98 5 3 0 14.72 0.65 -6 -3 0 75.91 2.75 -6 -3 0 76.97 2.41 -6 -3 0 75.68 2.32 -6 -3 0 75.50 2.31 6 3 0 77.21 2.16 6 3 0 75.62 2.13 6 3 0 76.96 2.71 -7 -3 0 88.10 2.76 -7 -3 0 91.59 2.78 -7 -3 0 90.57 2.88 -7 -3 0 93.89 3.31 7 3 0 92.00 2.58 7 3 0 92.22 2.55 7 3 0 87.09 3.16 -8 -3 0 48.21 1.96 -8 -3 0 48.24 2.41 -8 -3 0 48.78 2.08 8 3 0 49.84 2.37 8 3 0 51.74 1.72 8 3 0 49.41 1.73 -9 -3 0 11.43 1.56 -9 -3 0 13.00 1.38 -9 -3 0 13.03 1.20 -9 -3 0 12.73 1.20 9 3 0 12.22 0.90 9 3 0 12.47 0.95 9 3 0 11.83 1.56 -10 -3 0 6.34 1.13 -10 -3 0 7.10 1.34 -10 -3 0 7.80 1.07 -10 -3 0 7.30 1.06 10 3 0 7.04 0.91 10 3 0 6.13 0.77 10 3 0 4.35 1.11 -11 -3 0 0.92 1.21 -11 -3 0 0.64 1.11 -11 -3 0 2.14 0.96 -11 -3 0 1.86 1.04 11 3 0 0.00 0.60 11 3 0 0.22 1.18 11 3 0 0.30 0.68 -12 -3 0 0.51 1.15 -12 -3 0 0.90 1.50 -12 -3 0 -3.05 1.52 12 3 0 0.78 0.85 12 3 0 -1.41 0.73 12 -4 0 12.55 1.87 -12 4 0 7.95 1.73 -12 4 0 10.79 2.07 -12 4 0 9.64 2.69 11 -4 0 66.01 3.17 11 -4 0 64.38 2.60 11 -4 0 54.52 3.05 -11 4 0 59.12 3.70 -11 4 0 61.30 3.35 -11 4 0 60.23 3.89 10 -4 0 1.22 1.31 10 -4 0 0.81 0.93 10 -4 0 2.12 0.90 10 -4 0 0.17 0.65 -10 4 0 -1.09 0.98 -10 4 0 -0.48 0.95 -10 4 0 0.65 1.05 -10 4 0 -0.22 0.86 -10 4 0 -0.34 1.13 9 -4 0 160.44 4.89 9 -4 0 159.74 4.96 9 -4 0 162.45 4.56 9 -4 0 147.78 5.39 -9 4 0 160.07 5.26 -9 4 0 157.15 5.38 -9 4 0 161.31 5.07 -9 4 0 159.01 4.57 -9 4 0 152.95 5.42 -9 4 0 164.20 5.11 8 -4 0 7.72 0.95 8 -4 0 10.78 1.20 8 -4 0 7.92 1.25 8 -4 0 9.13 1.12 -8 4 0 6.75 1.09 -8 4 0 7.85 1.17 -8 4 0 9.43 1.21 -8 4 0 9.85 1.39 -8 4 0 7.90 1.08 -8 4 0 8.16 0.99 7 -4 0 68.26 2.57 7 -4 0 66.52 2.34 7 -4 0 67.80 2.85 7 -4 0 66.30 2.51 -7 4 0 65.70 2.36 -7 4 0 67.40 2.62 -7 4 0 67.61 2.89 -7 4 0 69.21 2.81 -7 4 0 66.69 2.55 -7 4 0 65.94 2.70 6 -4 0 75.66 2.62 6 -4 0 76.86 2.55 6 -4 0 75.00 2.45 6 -4 0 72.57 2.84 -6 4 0 70.93 2.71 -6 4 0 71.16 2.43 -6 4 0 72.76 2.68 -6 4 0 71.90 2.59 -6 4 0 74.74 2.59 -6 4 0 69.91 2.82 5 -4 0 64.35 2.18 5 -4 0 66.56 2.24 5 -4 0 63.34 2.27 5 -4 0 65.45 2.50 -5 4 0 63.70 2.49 -5 4 0 62.11 2.26 -5 4 0 66.04 2.20 -5 4 0 68.74 2.40 -5 4 0 66.26 2.37 -5 4 0 66.88 2.29 4 -4 0 161.43 4.32 4 -4 0 164.54 4.42 4 -4 0 166.25 4.37 4 -4 0 164.45 4.60 -4 4 0 165.48 4.63 -4 4 0 165.23 4.38 -4 4 0 165.53 4.35 -4 4 0 166.02 4.44 -4 4 0 165.68 4.41 -4 4 0 168.37 4.47 3 -4 0 47.32 1.82 3 -4 0 49.68 1.70 3 -4 0 49.33 1.73 3 -4 0 48.37 1.69 -3 4 0 50.03 1.69 -3 4 0 49.73 1.71 -3 4 0 52.24 1.71 -3 4 0 48.84 1.71 -3 4 0 52.10 1.76 2 -4 0 345.86 8.39 2 -4 0 344.46 8.33 2 -4 0 372.54 8.53 2 -4 0 372.71 8.38 -2 4 0 359.32 8.33 -2 4 0 360.84 8.31 -2 4 0 358.99 8.32 -2 4 0 352.30 8.37 -2 4 0 372.67 8.25 1 -4 0 13.84 0.68 1 -4 0 12.98 0.66 1 -4 0 14.80 0.62 -1 4 0 14.15 0.64 -1 4 0 14.94 0.61 -1 4 0 13.26 0.72 -1 4 0 12.83 0.65 -1 4 0 13.37 0.65 0 -4 0 21.35 0.78 0 -4 0 22.65 0.83 0 -4 0 20.30 0.79 0 -4 0 21.15 0.89 0 4 0 21.75 0.78 0 4 0 20.94 0.88 0 4 0 21.49 0.77 0 4 0 21.24 0.69 -1 -4 0 10.78 0.57 -1 -4 0 10.47 0.52 -1 -4 0 10.72 0.50 1 4 0 11.32 0.45 1 4 0 10.05 0.45 1 4 0 10.24 0.57 -2 -4 0 86.52 2.22 -2 -4 0 86.03 2.14 -2 -4 0 84.76 2.15 2 4 0 81.43 2.19 2 4 0 85.93 2.01 -3 -4 0 264.04 5.94 -3 -4 0 254.36 5.89 -3 -4 0 256.01 5.98 3 4 0 273.48 5.91 3 4 0 251.61 5.76 -4 -4 0 73.95 1.96 -4 -4 0 69.27 1.99 -4 -4 0 69.04 2.34 -4 -4 0 72.04 1.97 4 4 0 71.39 1.76 4 4 0 72.79 1.77 4 4 0 71.62 1.80 -5 -4 0 159.32 4.06 -5 -4 0 164.26 4.04 -5 -4 0 157.66 4.55 -5 -4 0 166.92 4.09 5 4 0 161.44 3.80 5 4 0 163.30 3.84 -6 -4 0 94.85 2.77 -6 -4 0 97.22 2.74 -6 -4 0 99.94 3.26 -6 -4 0 92.11 2.70 6 4 0 96.00 2.50 6 4 0 90.23 2.42 -7 -4 0 56.97 2.49 -7 -4 0 59.01 2.05 -7 -4 0 60.58 2.12 -7 -4 0 59.18 2.04 7 4 0 57.93 1.77 7 4 0 56.85 1.71 -8 -4 0 49.62 1.96 -8 -4 0 47.66 2.00 -8 -4 0 45.80 2.37 -8 -4 0 47.49 1.91 8 4 0 46.49 1.54 8 4 0 47.65 1.61 -9 -4 0 37.31 1.79 -9 -4 0 30.96 2.18 -9 -4 0 34.66 1.77 -9 -4 0 36.57 1.91 9 4 0 34.69 1.32 9 4 0 34.19 1.37 -10 -4 0 20.06 1.60 -10 -4 0 14.66 1.71 -10 -4 0 17.64 1.52 -10 -4 0 15.79 2.01 10 4 0 17.04 1.06 10 4 0 15.70 0.98 -11 -4 0 32.31 2.46 -11 -4 0 30.51 2.11 -11 -4 0 34.04 2.91 -11 -4 0 34.92 2.29 11 4 0 30.27 1.40 11 4 0 31.92 1.37 -12 -4 0 9.95 1.52 -12 -4 0 10.92 1.98 -12 -4 0 9.61 1.89 11 -5 0 -0.77 0.94 11 -5 0 1.84 1.24 -11 5 0 1.04 1.41 -11 5 0 -1.32 1.30 -11 5 0 -1.06 1.49 10 -5 0 2.12 0.81 10 -5 0 0.18 0.92 10 -5 0 1.37 1.02 -10 5 0 2.00 1.09 -10 5 0 3.13 1.16 -10 5 0 -0.95 1.19 9 -5 0 -0.85 0.79 9 -5 0 0.03 0.65 9 -5 0 -1.00 0.98 9 -5 0 0.67 0.76 -9 5 0 0.98 0.70 -9 5 0 0.64 0.85 -9 5 0 1.66 0.98 -9 5 0 0.56 0.89 -9 5 0 -0.36 0.93 -9 5 0 0.91 0.77 8 -5 0 -0.29 0.52 8 -5 0 -0.86 0.61 8 -5 0 1.24 0.82 8 -5 0 1.50 0.64 -8 5 0 0.30 0.65 -8 5 0 0.41 0.72 -8 5 0 0.07 0.54 -8 5 0 0.01 0.64 -8 5 0 -0.20 0.64 -8 5 0 1.28 0.77 7 -5 0 5.25 0.86 7 -5 0 4.23 0.70 7 -5 0 5.13 0.80 7 -5 0 5.04 0.98 -7 5 0 3.50 0.84 -7 5 0 2.72 0.66 -7 5 0 4.44 0.80 -7 5 0 4.35 0.73 -7 5 0 5.73 0.94 -7 5 0 4.82 0.82 6 -5 0 8.96 1.20 6 -5 0 8.08 0.95 6 -5 0 8.31 0.95 6 -5 0 9.40 0.92 -6 5 0 9.90 0.93 -6 5 0 8.44 0.99 -6 5 0 9.92 1.10 -6 5 0 9.59 1.22 -6 5 0 9.90 1.05 -6 5 0 9.14 0.98 5 -5 0 13.96 1.04 5 -5 0 13.83 1.03 5 -5 0 14.13 0.98 5 -5 0 11.97 1.14 -5 5 0 14.50 1.04 -5 5 0 13.42 0.98 -5 5 0 14.96 1.10 -5 5 0 14.51 1.03 -5 5 0 14.04 1.05 -5 5 0 14.30 1.24 4 -5 0 27.04 1.33 4 -5 0 29.52 1.51 4 -5 0 28.56 1.34 4 -5 0 28.12 1.33 -4 5 0 25.85 1.28 -4 5 0 28.07 1.30 -4 5 0 26.17 1.44 -4 5 0 27.38 1.32 -4 5 0 28.16 1.36 -4 5 0 26.92 1.31 3 -5 0 40.48 1.58 3 -5 0 39.42 1.58 3 -5 0 39.20 1.57 3 -5 0 44.25 1.80 -3 5 0 42.14 1.51 -3 5 0 40.73 1.56 -3 5 0 39.76 1.55 -3 5 0 40.94 1.60 -3 5 0 40.80 1.54 2 -5 0 0.92 0.28 2 -5 0 1.65 0.30 2 -5 0 1.01 0.26 2 -5 0 2.14 0.48 2 -5 0 1.58 0.30 -2 5 0 1.85 0.35 -2 5 0 1.90 0.37 -2 5 0 1.84 0.34 -2 5 0 1.95 0.41 -2 5 0 1.98 0.33 1 -5 0 4.37 0.46 1 -5 0 5.35 0.53 1 -5 0 5.83 0.44 1 -5 0 5.32 0.47 -1 5 0 5.70 0.48 -1 5 0 4.82 0.46 -1 5 0 5.54 0.46 -1 5 0 5.63 0.45 -1 5 0 5.35 0.53 0 -5 0 25.87 0.96 0 -5 0 25.62 1.00 0 -5 0 25.50 0.98 0 -5 0 25.00 1.07 0 5 0 26.15 1.08 0 5 0 25.69 0.92 0 5 0 26.12 0.95 0 5 0 25.76 0.84 -1 -5 0 63.18 1.89 -1 -5 0 61.99 1.77 -1 -5 0 63.72 1.79 1 5 0 60.27 1.68 1 5 0 64.86 1.66 1 5 0 61.71 1.50 1 5 0 60.60 1.87 -2 -5 0 123.22 3.16 -2 -5 0 123.79 3.07 -2 -5 0 118.54 3.03 2 5 0 123.44 3.13 2 5 0 120.69 2.83 2 5 0 123.37 2.85 -3 -5 0 104.22 2.69 -3 -5 0 104.33 2.65 -3 -5 0 104.93 2.41 -3 -5 0 104.31 2.68 3 5 0 103.17 2.68 -4 -5 0 105.67 2.69 -4 -5 0 98.17 2.70 -4 -5 0 104.62 2.55 -4 -5 0 100.86 3.15 -4 -5 0 102.06 2.58 4 5 0 103.93 2.58 -5 -5 0 48.79 1.62 -5 -5 0 49.17 1.54 -5 -5 0 50.57 1.61 -5 -5 0 49.25 2.04 5 5 0 50.92 1.33 -6 -5 0 5.41 0.59 -6 -5 0 5.50 0.60 -6 -5 0 5.14 0.82 -6 -5 0 4.32 0.60 6 5 0 4.75 0.33 -7 -5 0 2.04 0.46 -7 -5 0 2.19 0.46 -7 -5 0 2.70 0.54 -7 -5 0 0.86 0.53 7 5 0 1.93 0.28 7 5 0 2.26 0.26 -8 -5 0 3.21 0.62 -8 -5 0 2.04 0.72 -8 -5 0 3.27 0.65 -8 -5 0 2.79 0.55 8 5 0 2.56 0.31 8 5 0 2.72 0.36 -9 -5 0 54.33 2.25 -9 -5 0 59.05 2.37 -9 -5 0 55.82 2.88 -9 -5 0 53.76 2.24 -10 -5 0 33.84 1.96 -10 -5 0 37.64 2.02 -10 -5 0 37.56 2.10 -10 -5 0 33.23 2.58 -11 -5 0 32.27 2.51 -11 -5 0 33.39 2.96 -11 -5 0 31.77 2.27 -11 -5 0 36.80 2.26 -12 -5 0 11.83 1.52 -12 -5 0 11.13 1.89 -12 -5 0 9.62 1.91 11 -6 0 0.64 1.37 11 -6 0 -1.57 1.13 -11 6 0 0.58 1.36 -11 6 0 -0.62 1.65 -11 6 0 -3.28 1.48 10 -6 0 1.65 0.90 10 -6 0 0.92 1.16 10 -6 0 1.77 1.12 -10 6 0 0.13 1.02 -10 6 0 0.41 1.11 -10 6 0 -0.29 1.36 -10 6 0 0.03 1.20 9 -6 0 12.43 1.72 9 -6 0 17.68 1.92 9 -6 0 19.31 1.81 9 -6 0 17.47 1.57 -9 6 0 19.09 1.96 -9 6 0 17.19 1.71 -9 6 0 16.76 1.87 -9 6 0 16.43 2.27 -9 6 0 15.53 2.09 -9 6 0 17.92 1.99 8 -6 0 27.83 1.87 8 -6 0 24.50 2.21 8 -6 0 25.66 1.63 8 -6 0 23.84 1.83 -8 6 0 26.50 2.21 -8 6 0 26.19 1.91 -8 6 0 24.36 1.91 -8 6 0 23.20 1.98 -8 6 0 24.05 1.66 -8 6 0 23.47 1.81 7 -6 0 114.64 3.79 7 -6 0 114.57 3.70 7 -6 0 113.05 3.85 7 -6 0 111.44 4.17 -7 6 0 115.10 3.83 -7 6 0 115.62 4.20 -7 6 0 113.87 3.72 -7 6 0 115.47 3.97 -7 6 0 117.85 3.92 -7 6 0 116.19 3.96 6 -6 0 68.30 2.56 6 -6 0 69.42 2.91 6 -6 0 67.56 2.65 6 -6 0 70.67 2.61 -6 6 0 70.74 2.68 -6 6 0 61.36 2.50 -6 6 0 69.25 2.71 -6 6 0 69.72 2.61 -6 6 0 69.37 2.68 -6 6 0 69.59 2.93 5 -6 0 28.58 1.71 5 -6 0 30.57 1.55 5 -6 0 29.23 1.52 5 -6 0 29.01 1.49 -5 6 0 29.22 1.51 -5 6 0 30.29 1.51 -5 6 0 28.90 1.50 -5 6 0 28.30 1.71 -5 6 0 29.54 1.51 -5 6 0 22.67 1.43 4 -6 0 23.51 1.30 4 -6 0 22.49 1.28 4 -6 0 24.82 1.49 4 -6 0 26.75 1.37 -4 6 0 24.61 1.34 -4 6 0 25.51 1.26 -4 6 0 24.51 1.33 -4 6 0 25.18 1.30 -4 6 0 25.24 1.29 3 -6 0 3.28 0.62 3 -6 0 2.21 0.45 3 -6 0 3.09 0.53 3 -6 0 2.17 0.47 -3 6 0 1.99 0.38 -3 6 0 1.90 0.40 -3 6 0 2.02 0.43 -3 6 0 3.24 0.56 -3 6 0 2.95 0.49 2 -6 0 16.40 1.15 2 -6 0 12.60 0.88 2 -6 0 15.44 0.90 2 -6 0 14.75 0.78 2 -6 0 13.94 0.87 -2 6 0 15.86 0.81 -2 6 0 14.81 0.85 -2 6 0 14.89 0.85 -2 6 0 14.14 0.85 -2 6 0 15.79 0.98 1 -6 0 104.60 3.02 1 -6 0 114.60 2.86 1 -6 0 110.24 3.04 -1 6 0 109.18 2.95 -1 6 0 108.08 3.16 -1 6 0 112.84 2.89 -1 6 0 110.46 3.00 -1 6 0 107.45 2.87 0 -6 0 176.03 4.26 0 -6 0 173.06 4.36 0 -6 0 166.37 4.50 0 -6 0 180.34 4.39 0 6 0 176.96 4.52 0 6 0 172.21 4.23 0 6 0 174.68 4.11 0 6 0 173.12 4.27 -1 -6 0 159.53 4.06 -1 -6 0 180.69 4.27 -1 -6 0 162.06 4.03 1 6 0 155.09 3.89 1 6 0 159.22 3.84 1 6 0 157.49 4.16 1 6 0 157.19 3.68 -2 -6 0 138.98 3.67 -2 -6 0 139.63 3.52 -2 -6 0 142.22 3.57 2 6 0 138.35 3.28 2 6 0 140.48 3.66 2 6 0 141.88 3.28 -3 -6 0 3.41 0.42 -3 -6 0 3.81 0.45 -3 -6 0 3.42 0.40 3 6 0 3.33 0.43 -4 -6 0 9.59 0.64 -4 -6 0 10.07 0.45 -4 -6 0 10.68 0.64 -4 -6 0 10.45 0.61 4 6 0 11.02 0.61 -5 -6 0 0.80 0.30 -5 -6 0 1.60 0.26 -5 -6 0 1.02 0.27 -5 -6 0 0.93 0.30 -5 -6 0 0.96 0.44 5 6 0 1.00 0.23 -6 -6 0 63.41 2.02 -6 -6 0 62.93 2.55 -6 -6 0 61.65 1.91 -6 -6 0 60.20 2.02 -7 -6 0 36.89 2.01 -7 -6 0 32.31 1.39 -7 -6 0 33.45 1.47 -7 -6 0 33.81 1.45 -8 -6 0 81.13 2.68 -8 -6 0 81.26 2.72 -8 -6 0 83.08 3.39 -8 -6 0 84.32 2.74 -9 -6 0 21.72 1.48 -9 -6 0 23.21 1.48 -9 -6 0 21.51 2.05 -9 -6 0 21.94 1.52 -10 -6 0 8.89 1.54 -10 -6 0 8.77 1.13 -10 -6 0 8.41 1.13 -10 -6 0 10.58 1.47 -11 -6 0 0.49 1.11 -11 -6 0 0.39 0.92 -11 -6 0 0.42 1.03 -11 -6 0 0.55 1.29 -12 -6 0 -1.20 1.11 -12 -6 0 -0.13 1.63 -12 -6 0 1.96 1.61 10 -7 0 17.26 1.96 10 -7 0 17.31 2.39 -10 7 0 14.90 2.07 -10 7 0 24.55 2.53 -10 7 0 19.04 2.46 -10 7 0 17.04 1.92 9 -7 0 7.18 1.11 9 -7 0 5.16 1.56 9 -7 0 8.44 1.30 9 -7 0 5.63 1.27 -9 7 0 4.13 1.40 -9 7 0 6.92 1.31 -9 7 0 5.70 1.26 -9 7 0 5.96 1.20 -9 7 0 3.43 1.29 8 -7 0 18.01 1.76 8 -7 0 20.64 1.68 8 -7 0 24.01 2.30 8 -7 0 24.15 1.97 -8 7 0 21.90 2.19 -8 7 0 19.57 1.83 -8 7 0 20.91 1.75 -8 7 0 20.41 1.81 -8 7 0 19.79 2.00 -8 7 0 21.18 1.88 7 -7 0 0.38 0.71 7 -7 0 0.19 0.57 7 -7 0 0.37 0.62 7 -7 0 0.95 0.81 -7 7 0 -0.33 0.69 -7 7 0 1.08 0.68 -7 7 0 0.00 0.62 -7 7 0 -0.31 0.61 -7 7 0 0.20 0.74 -7 7 0 0.28 0.67 6 -7 0 10.60 1.15 6 -7 0 12.06 1.23 6 -7 0 10.10 1.28 6 -7 0 12.52 1.54 -6 7 0 9.95 1.13 -6 7 0 11.84 1.19 -6 7 0 11.65 1.21 -6 7 0 11.71 1.23 -6 7 0 14.38 1.34 5 -7 0 3.71 0.69 5 -7 0 3.47 0.66 5 -7 0 2.93 0.70 5 -7 0 3.90 0.77 -5 7 0 2.68 0.60 -5 7 0 3.19 0.59 -5 7 0 3.12 0.60 -5 7 0 3.50 0.70 -5 7 0 4.23 0.76 4 -7 0 11.53 1.02 4 -7 0 10.43 0.99 4 -7 0 11.11 1.15 4 -7 0 10.70 0.99 -4 7 0 10.91 0.96 -4 7 0 11.69 1.00 -4 7 0 13.30 1.02 -4 7 0 11.69 0.91 -4 7 0 12.92 1.07 3 -7 0 52.00 2.19 3 -7 0 50.26 2.05 3 -7 0 52.04 1.98 3 -7 0 47.54 1.94 -3 7 0 51.08 1.91 -3 7 0 50.77 1.90 -3 7 0 50.16 1.92 -3 7 0 48.15 1.75 -3 7 0 51.93 2.05 2 -7 0 21.37 0.99 2 -7 0 22.11 1.16 2 -7 0 24.29 1.39 2 -7 0 19.70 1.19 2 -7 0 22.41 1.17 -2 7 0 21.19 0.98 -2 7 0 21.66 1.24 -2 7 0 23.70 1.13 -2 7 0 21.33 1.11 -2 7 0 21.67 1.07 1 -7 0 23.07 1.14 1 -7 0 24.25 1.24 1 -7 0 25.13 1.17 1 -7 0 24.98 1.01 -1 7 0 22.21 1.07 -1 7 0 22.87 1.06 -1 7 0 24.91 1.26 -1 7 0 23.46 1.00 0 -7 0 0.95 0.33 0 -7 0 0.68 0.27 0 -7 0 0.78 0.30 0 -7 0 0.71 0.33 0 7 0 0.60 0.24 0 7 0 0.09 0.25 0 7 0 0.87 0.26 0 7 0 0.96 0.25 -1 -7 0 7.29 0.67 -1 -7 0 6.96 0.63 -1 -7 0 8.09 0.74 -1 -7 0 7.31 0.58 1 7 0 6.91 0.40 1 7 0 6.71 0.51 1 7 0 7.57 0.50 1 7 0 6.31 0.64 -2 -7 0 0.37 0.22 -2 -7 0 -0.19 0.22 -2 -7 0 0.42 0.24 2 7 0 0.24 0.15 2 7 0 0.13 0.24 2 7 0 0.18 0.15 -3 -7 0 2.72 0.42 -3 -7 0 2.92 0.44 -3 -7 0 2.40 0.38 3 7 0 2.37 0.41 -4 -7 0 0.99 0.29 -4 -7 0 1.05 0.31 -4 -7 0 0.70 0.27 4 7 0 0.51 0.26 -5 -7 0 0.68 0.29 -5 -7 0 0.81 0.43 -5 -7 0 1.32 0.36 -5 -7 0 1.25 0.35 -5 -7 0 0.98 0.23 5 7 0 1.27 0.32 -6 -7 0 2.28 0.50 -6 -7 0 3.17 0.51 -6 -7 0 1.85 0.54 -6 -7 0 2.94 0.41 -7 -7 0 3.41 0.59 -7 -7 0 3.56 0.56 -7 -7 0 2.59 0.73 -7 -7 0 5.42 0.72 -8 -7 0 0.33 0.70 -8 -7 0 -0.06 0.47 -8 -7 0 0.62 0.52 -8 -7 0 -0.22 0.46 -9 -7 0 0.68 0.68 -9 -7 0 1.34 0.89 -9 -7 0 2.43 0.70 -9 -7 0 1.37 0.64 -10 -7 0 3.54 0.95 -10 -7 0 2.76 0.86 -10 -7 0 5.42 1.36 -10 -7 0 2.34 0.90 -11 -7 0 1.62 1.13 -11 -7 0 1.63 1.17 -11 -7 0 1.96 1.40 -11 -7 0 0.46 0.97 -12 -7 0 1.95 1.69 -12 -7 0 2.49 1.77 -12 -7 0 4.09 1.36 10 -8 0 19.67 2.30 10 -8 0 25.93 2.76 -10 8 0 21.39 2.68 -10 8 0 17.67 2.13 -10 8 0 21.19 2.25 9 -8 0 8.07 1.41 9 -8 0 7.90 1.24 -9 8 0 7.73 1.37 -9 8 0 8.87 1.47 -9 8 0 6.22 1.39 8 -8 0 17.48 1.86 8 -8 0 14.91 1.95 8 -8 0 16.03 1.66 8 -8 0 13.37 1.96 -8 8 0 15.76 1.84 -8 8 0 15.67 1.91 -8 8 0 14.49 1.97 -8 8 0 13.40 1.75 -8 8 0 14.69 1.83 7 -8 0 33.07 2.57 7 -8 0 37.62 2.20 7 -8 0 38.61 2.13 7 -8 0 33.38 2.15 -7 8 0 34.25 2.25 -7 8 0 36.08 2.18 -7 8 0 37.42 2.07 -7 8 0 39.97 2.24 -7 8 0 36.67 2.16 6 -8 0 18.61 1.61 6 -8 0 17.04 1.83 6 -8 0 16.72 1.46 6 -8 0 15.71 1.48 -6 8 0 16.11 1.34 -6 8 0 18.94 1.50 -6 8 0 17.02 1.54 -6 8 0 17.97 1.52 -6 8 0 17.56 1.46 5 -8 0 125.90 4.10 5 -8 0 124.26 4.36 5 -8 0 131.65 4.14 5 -8 0 128.99 4.06 -5 8 0 130.37 4.05 -5 8 0 122.73 3.78 -5 8 0 126.65 4.03 -5 8 0 122.73 4.08 -5 8 0 125.27 3.96 4 -8 0 4.97 0.79 4 -8 0 5.81 0.82 4 -8 0 5.03 0.75 4 -8 0 6.59 1.05 -4 8 0 5.65 0.79 -4 8 0 4.35 0.80 -4 8 0 6.87 0.89 -4 8 0 4.87 0.70 -4 8 0 6.17 0.87 3 -8 0 124.91 3.96 3 -8 0 124.12 3.85 3 -8 0 127.03 3.84 3 -8 0 128.89 4.12 -3 8 0 122.79 3.75 -3 8 0 129.20 3.71 -3 8 0 132.44 4.01 -3 8 0 127.49 3.71 -3 8 0 128.46 3.50 2 -8 0 29.61 1.45 2 -8 0 27.36 1.40 2 -8 0 27.86 1.17 2 -8 0 27.99 1.64 -2 8 0 27.69 1.30 -2 8 0 27.08 1.26 -2 8 0 26.50 1.32 -2 8 0 27.93 1.51 -2 8 0 27.72 1.19 1 -8 0 148.20 3.73 1 -8 0 142.29 4.02 1 -8 0 140.95 4.20 1 -8 0 148.88 4.04 -1 8 0 144.86 3.75 -1 8 0 142.81 3.87 -1 8 0 141.16 4.19 -1 8 0 144.51 3.84 0 -8 0 89.36 2.68 0 -8 0 86.23 2.85 0 -8 0 87.44 2.67 0 -8 0 87.65 2.48 0 8 0 87.84 2.35 0 8 0 83.15 2.80 0 8 0 84.25 2.50 0 8 0 85.22 2.45 -1 -8 0 17.48 1.02 -1 -8 0 18.96 0.98 -1 -8 0 17.05 1.07 -1 -8 0 18.78 1.02 1 8 0 17.93 0.85 1 8 0 17.99 0.80 1 8 0 17.06 1.06 1 8 0 17.41 0.69 -2 -8 0 398.69 9.45 -2 -8 0 407.10 9.69 2 8 0 397.28 9.05 2 8 0 415.88 9.67 2 8 0 407.30 9.04 -3 -8 0 -0.09 0.28 -3 -8 0 0.06 0.27 -3 -8 0 0.22 0.29 3 8 0 0.34 0.31 -4 -8 0 209.76 5.28 -4 -8 0 204.90 5.31 -4 -8 0 212.51 5.32 4 8 0 216.42 5.34 -5 -8 0 14.91 0.95 -5 -8 0 15.28 0.94 -5 -8 0 13.92 0.85 5 8 0 14.30 0.87 -6 -8 0 113.78 3.06 -6 -8 0 113.33 3.33 -6 -8 0 115.80 3.30 -6 -8 0 117.54 2.84 -6 -8 0 113.32 3.98 6 8 0 117.73 3.08 -7 -8 0 61.16 2.17 -7 -8 0 58.75 2.17 -7 -8 0 58.74 2.77 -7 -8 0 62.35 1.86 -8 -8 0 13.76 1.18 -8 -8 0 12.62 1.02 -8 -8 0 14.50 1.19 -8 -8 0 15.00 1.76 -9 -8 0 116.39 3.41 -9 -8 0 112.92 3.68 -9 -8 0 116.57 4.58 -9 -8 0 112.37 3.65 -10 -8 0 -0.10 0.88 -10 -8 0 1.41 0.92 -10 -8 0 0.69 0.89 -10 -8 0 0.56 1.18 -11 -8 0 86.35 3.48 -11 -8 0 85.76 4.57 -11 -8 0 88.26 3.64 -11 -8 0 90.37 3.56 -12 -8 0 -0.50 1.30 -12 -8 0 1.41 1.83 9 -9 0 9.86 1.66 9 -9 0 11.21 1.55 -9 9 0 11.53 1.88 -9 9 0 10.83 1.67 -9 9 0 7.87 1.43 8 -9 0 14.10 1.85 8 -9 0 12.91 1.57 -8 9 0 12.96 1.75 -8 9 0 10.17 1.54 -8 9 0 14.78 1.92 -8 9 0 9.36 1.51 7 -9 0 46.27 2.57 7 -9 0 43.05 2.52 7 -9 0 37.97 2.91 7 -9 0 43.94 2.45 -7 9 0 47.97 2.64 -7 9 0 43.72 2.28 -7 9 0 42.03 2.58 -7 9 0 43.33 2.49 -7 9 0 44.66 2.51 6 -9 0 30.91 2.42 6 -9 0 34.54 2.10 6 -9 0 34.94 2.20 6 -9 0 33.65 2.09 -6 9 0 35.42 2.07 -6 9 0 37.38 2.23 -6 9 0 35.73 1.90 -6 9 0 35.08 2.13 -6 9 0 35.70 2.07 5 -9 0 49.28 2.45 5 -9 0 58.11 2.58 5 -9 0 55.91 2.56 5 -9 0 53.85 2.81 -5 9 0 60.14 2.50 -5 9 0 56.13 2.22 -5 9 0 57.48 2.47 -5 9 0 58.13 2.46 -5 9 0 56.45 2.62 4 -9 0 1.21 0.62 4 -9 0 1.72 0.71 4 -9 0 0.63 0.51 4 -9 0 0.34 0.52 -4 9 0 1.67 0.57 -4 9 0 1.56 0.52 -4 9 0 1.00 0.52 -4 9 0 0.65 0.54 -4 9 0 0.93 0.44 3 -9 0 -0.21 0.44 3 -9 0 0.13 0.45 3 -9 0 0.94 0.48 3 -9 0 0.99 0.61 -3 9 0 0.36 0.44 -3 9 0 -0.14 0.39 -3 9 0 0.48 0.44 -3 9 0 0.61 0.35 -3 9 0 0.17 0.48 2 -9 0 7.27 0.89 2 -9 0 6.83 0.90 2 -9 0 7.20 1.02 2 -9 0 6.73 0.95 2 -9 0 7.87 0.74 -2 9 0 5.50 0.84 -2 9 0 7.96 0.82 -2 9 0 6.91 0.79 -2 9 0 7.34 0.81 1 -9 0 29.96 1.24 1 -9 0 30.55 1.63 1 -9 0 29.16 1.46 1 -9 0 28.47 1.45 -1 9 0 30.28 1.35 -1 9 0 29.13 1.25 -1 9 0 28.05 1.55 -1 9 0 28.33 1.30 0 -9 0 86.39 2.77 0 -9 0 84.05 2.51 0 -9 0 84.25 2.94 0 -9 0 85.37 2.76 0 9 0 87.07 2.94 0 9 0 85.42 2.49 0 9 0 86.22 2.58 0 9 0 87.51 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2.37 5 4 18 15.28 1.96 -6 -4 -18 12.74 1.87 -6 -4 -18 9.37 2.16 6 4 18 11.49 1.53 -1 -5 -18 0.29 1.54 -1 -5 -18 1.84 1.76 1 5 18 -0.07 1.27 1 5 18 3.72 1.69 -2 -5 -18 0.69 1.35 -2 -5 -18 0.27 1.71 2 5 18 0.05 1.50 2 5 18 0.53 1.25 -3 -5 -18 3.58 1.75 -3 -5 -18 0.24 1.30 3 5 18 0.05 1.35 3 5 18 -1.76 1.10 -4 -5 -18 1.78 1.36 -4 -5 -18 -2.46 1.62 4 5 18 0.23 1.04 -5 -5 -18 2.10 1.84 -5 -5 -18 -0.92 1.38 5 5 18 -0.40 0.90 -6 -5 -18 0.05 1.91 -6 -5 -18 2.93 1.51 -7 -5 -18 -0.65 1.83 -7 -5 -18 1.05 2.06 -7 -5 -18 -1.19 1.49 0 -6 -18 -0.91 1.82 0 -6 -18 1.78 1.60 0 6 18 3.37 1.77 0 6 18 2.13 1.41 -1 -6 -18 -2.26 1.71 -1 -6 -18 1.46 1.50 1 6 18 -1.04 1.55 1 6 18 1.91 1.29 -2 -6 -18 5.51 1.50 -2 -6 -18 9.51 1.88 2 6 18 6.15 1.48 2 6 18 8.02 1.26 -3 -6 -18 7.26 1.72 -3 -6 -18 4.75 1.33 3 6 18 5.66 1.59 3 6 18 5.75 1.11 -4 -6 -18 5.68 1.50 -4 -6 -18 4.21 1.76 4 6 18 5.08 0.93 -5 -6 -18 19.37 2.39 -5 -6 -18 24.46 2.79 -6 -6 -18 6.36 1.47 -6 -6 -18 8.01 2.07 -7 -6 -18 1.57 1.46 -7 -6 -18 1.70 2.01 -7 -6 -18 3.24 2.00 -1 -7 -18 16.85 2.06 -1 -7 -18 11.92 2.03 1 7 18 16.41 2.14 -2 -7 -18 9.38 1.65 -2 -7 -18 7.23 1.86 2 7 18 9.56 1.20 -3 -7 -18 8.64 1.86 -3 -7 -18 4.63 1.35 3 7 18 6.25 0.97 -4 -7 -18 5.76 1.83 -4 -7 -18 5.49 1.39 4 7 18 4.75 1.13 -5 -7 -18 -0.54 1.26 -5 -7 -18 -1.30 1.78 -6 -7 -18 0.15 1.28 -6 -7 -18 1.42 1.86 -7 -7 -18 7.52 1.69 -7 -7 -18 3.46 1.95 -7 -7 -18 0.71 1.90 -1 -8 -18 12.11 2.06 -1 -8 -18 12.96 1.90 1 8 18 10.01 1.25 -2 -8 -18 14.64 1.82 -2 -8 -18 16.32 2.25 2 8 18 13.58 1.66 -3 -8 -18 11.54 2.02 -3 -8 -18 12.02 1.64 3 8 18 3.27 3.27 -4 -8 -18 21.63 3.14 -4 -8 -18 24.19 2.45 -5 -8 -18 14.89 1.82 -5 -8 -18 14.72 2.10 -6 -8 -18 15.09 2.30 -6 -8 -18 15.05 1.84 -7 -8 -18 1.55 2.00 -7 -8 -18 3.23 1.91 -7 -8 -18 6.61 1.51 -1 -9 -18 2.75 1.80 -1 -9 -18 -0.63 1.48 1 9 18 0.54 2.26 -2 -9 -18 2.01 1.84 -2 -9 -18 5.17 1.53 2 9 18 4.80 2.18 -3 -9 -18 6.46 1.39 -3 -9 -18 5.78 1.83 3 9 18 1.54 2.09 -4 -9 -18 18.33 2.40 -4 -9 -18 18.88 2.38 4 9 18 13.84 2.46 -5 -9 -18 10.79 2.04 -5 -9 -18 12.13 1.65 -6 -9 -18 12.14 2.26 -6 -9 -18 5.71 2.11 -6 -9 -18 6.86 1.54 -7 -9 -18 2.27 1.87 -7 -9 -18 2.46 2.02 -7 -9 -18 5.72 2.08 -7 -9 -18 2.73 1.50 -2 -10 -18 10.25 2.00 -2 -10 -18 12.50 1.82 2 10 18 6.60 2.27 -3 -10 -18 14.84 1.81 -3 -10 -18 10.95 2.11 3 10 18 13.11 2.27 -4 -10 -18 2.07 1.82 -4 -10 -18 5.84 1.41 4 10 18 6.77 2.11 -5 -10 -18 0.64 1.24 -5 -10 -18 -0.98 1.83 -5 -10 -18 -1.91 1.74 5 10 18 -3.19 2.01 -6 -10 -18 2.00 1.35 -6 -10 -18 -3.27 1.70 -6 -10 -18 -1.17 1.84 -3 -11 -18 -2.10 1.86 -3 -11 -18 0.42 1.39 3 11 18 5.80 2.10 -4 -11 -18 1.38 1.30 -4 -11 -18 1.48 1.85 4 11 18 -1.46 1.98 -5 -11 -18 0.80 1.82 -5 -11 -18 1.64 1.32 -5 -11 -18 -0.72 1.76 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 69770 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cs2 Cs 0.92424(2) 0.66721(2) 0.07752(2) 0.01721(4) Uani 1 1 d . . . . . Cs1 Cs 0.05917(2) 0.98899(2) 0.16237(2) 0.01640(4) Uani 1 1 d . . . . . Ag3 Ag 0.5000 0.5000 0.0000 0.01482(5) Uani 1 2 d S T P . . Ag1 Ag 0.5000 1.0000 0.0000 0.01422(5) Uani 1 2 d S T P . . Ag2 Ag 0.49969(2) 0.75494(2) -0.00196(2) 0.01496(4) Uani 1 1 d . . . . . O6 O 0.41817(18) 0.85783(14) -0.25075(14) 0.0212(4) Uani 1 1 d . . . . . O4 O 0.59861(18) 0.63442(14) 0.23032(14) 0.0211(4) Uani 1 1 d . . . . . C8 C 0.4651(2) 0.64835(18) 0.24416(18) 0.0149(4) Uani 1 1 d . . . . . N3 N 0.6066(2) 0.81009(15) -0.16509(15) 0.0154(4) Uani 1 1 d . . . . . N2 N 0.3946(2) 0.69619(15) 0.16138(15) 0.0151(4) Uani 1 1 d . . . . . C12 C 0.5493(3) 0.84695(18) -0.25417(19) 0.0157(4) Uani 1 1 d . . . . . O3 O 0.15686(18) 0.74790(14) 0.14654(14) 0.0227(4) Uani 1 1 d . . . . . O5 O 0.83083(18) 0.79378(15) -0.13242(14) 0.0239(4) Uani 1 1 d . . . . . C11 C 0.6664(3) 0.8751(2) -0.35883(19) 0.0189(5) Uani 1 1 d . . . . . H11A H 0.6501 0.9546 -0.4026 0.023 Uiso 1 1 calc R . . . . H11B H 0.6691 0.8294 -0.4035 0.023 Uiso 1 1 calc R . . . . C5 C 0.2473(2) 0.70228(18) 0.20277(19) 0.0165(5) Uani 1 1 d . . . . . C7 C 0.3589(3) 0.6160(2) 0.35445(19) 0.0190(5) Uani 1 1 d . . . . . H7A H 0.3660 0.6575 0.4002 0.023 Uiso 1 1 calc R . . . . H7B H 0.3767 0.5354 0.3938 0.023 Uiso 1 1 calc R . . . . C10 C 0.8061(3) 0.8480(2) -0.31916(19) 0.0200(5) Uani 1 1 d . . . . . H10A H 0.8715 0.7866 -0.3416 0.024 Uiso 1 1 calc R . . . . H10B H 0.8581 0.9138 -0.3480 0.024 Uiso 1 1 calc R . . . . O1 O 0.33832(17) 0.91296(14) 0.26400(14) 0.0214(4) Uani 1 1 d . . . . . C2 C 0.5562(2) 0.84977(19) 0.33734(18) 0.0171(5) Uani 1 1 d . . . . . H2A H 0.5418 0.7712 0.3780 0.020 Uiso 1 1 calc R . . . . H2B H 0.5261 0.8918 0.3893 0.020 Uiso 1 1 calc R . . . . C9 C 0.7540(2) 0.81415(18) -0.1962(2) 0.0171(5) Uani 1 1 d . . . . . C1 C 0.4721(2) 0.89971(18) 0.24820(18) 0.0141(4) Uani 1 1 d . . . . . N1 N 0.5632(2) 0.92812(15) 0.14733(15) 0.0135(4) Uani 1 1 d . . . . . C3 C 0.7135(2) 0.8594(2) 0.27533(19) 0.0186(5) Uani 1 1 d . . . . . H3A H 0.7543 0.9110 0.2937 0.022 Uiso 1 1 calc R . . . . H3B H 0.7742 0.7861 0.2918 0.022 Uiso 1 1 calc R . . . . O2 O 0.81092(17) 0.91788(14) 0.07965(13) 0.0212(4) Uani 1 1 d . . . . . C6 C 0.2111(3) 0.6477(2) 0.3251(2) 0.0210(5) Uani 1 1 d . . . . . H6A H 0.1630 0.5812 0.3461 0.025 Uiso 1 1 calc R . . . . H6B H 0.1467 0.6999 0.3616 0.025 Uiso 1 1 calc R . . . . N4 N 0.5925(2) 0.43299(15) 0.13572(15) 0.0147(4) Uani 1 1 d . . . . . C16 C 0.7376(2) 0.42655(18) 0.1290(2) 0.0168(5) Uani 1 1 d . . . . . C14 C 0.6271(3) 0.3479(2) 0.3168(2) 0.0205(5) Uani 1 1 d . . . . . H14A H 0.6199 0.2691 0.3615 0.025 Uiso 1 1 calc R . . . . H14B H 0.6079 0.3922 0.3659 0.025 Uiso 1 1 calc R . . . . C15 C 0.7749(3) 0.3613(2) 0.2384(2) 0.0218(5) Uani 1 1 d . . . . . H15A H 0.8311 0.4027 0.2576 0.026 Uiso 1 1 calc R . . . . H15B H 0.8317 0.2883 0.2383 0.026 Uiso 1 1 calc R . . . . C13 C 0.5230(3) 0.39086(18) 0.24188(19) 0.0162(5) Uani 1 1 d . . . . . O8 O 0.82590(18) 0.46897(14) 0.04525(14) 0.0219(4) Uani 1 1 d . . . . . O7 O 0.38987(18) 0.39030(14) 0.27388(14) 0.0215(4) Uani 1 1 d . . . . . C4 C 0.7046(2) 0.90461(18) 0.15682(18) 0.0143(4) Uani 1 1 d . . . . . O9 O -0.05028(19) 0.84766(17) 0.42166(15) 0.0245(4) Uani 1 1 d . . . . . O13 O 0.2102(2) 0.33169(15) 0.48067(15) 0.0229(4) Uani 1 1 d . . . . . O11 O -0.1720(2) 1.18310(17) 0.07747(16) 0.0259(4) Uani 1 1 d . . . . . O14 O 0.2007(2) 0.84035(18) 0.48681(17) 0.0311(5) Uani 1 1 d . . . . . O10 O -0.1975(2) 1.05759(17) 0.36966(18) 0.0308(5) Uani 1 1 d . . . . . O12 O 1.1609(2) 0.4632(2) 0.17537(18) 0.0410(6) Uani 1 1 d . . . . . O15 O -0.0245(2) 0.4107(2) 0.3779(2) 0.0464(6) Uani 1 1 d . . . . . O16 O 0.7509(3) 0.5725(2) 0.3894(2) 0.0551(8) Uani 1 1 d . . . . . H14C H 0.241(4) 0.864(3) 0.419(3) 0.066 Uiso 1 1 d R . . . . H14D H 0.131(4) 0.827(3) 0.485(3) 0.066 Uiso 1 1 d R . . . . H12A H 1.241(4) 0.447(3) 0.189(3) 0.066 Uiso 1 1 d DR . . . . H12B H 1.181(4) 0.460(3) 0.114(3) 0.066 Uiso 1 1 d R . . . . H11C H -0.186(4) 1.196(3) 0.022(3) 0.066 Uiso 1 1 d R . . . . H11D H -0.258(4) 1.179(3) 0.120(3) 0.066 Uiso 1 1 d R . . . . H16A H 0.814(4) 0.520(3) 0.384(3) 0.066 Uiso 1 1 d R . . . . H16B H 0.702(5) 0.586(4) 0.354(4) 0.066 Uiso 1 1 d R . . . . H13A H 0.272(4) 0.351(3) 0.422(3) 0.066 Uiso 1 1 d R . . . . H13B H 0.227(4) 0.362(3) 0.521(3) 0.066 Uiso 1 1 d R . . . . H9A H -0.106(4) 0.910(3) 0.416(3) 0.066 Uiso 1 1 d R . . . . H9B H -0.110(4) 0.795(3) 0.450(3) 0.066 Uiso 1 1 d R . . . . H10C H -0.218(4) 1.089(3) 0.419(3) 0.066 Uiso 1 1 d R . . . . H10D H -0.272(4) 1.083(3) 0.357(3) 0.066 Uiso 1 1 d R . . . . H15C H 0.034(3) 0.422(3) 0.310(3) 0.066 Uiso 1 1 d DR . . . . H15D H 0.034(4) 0.391(3) 0.420(3) 0.066 Uiso 1 1 d R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cs2 0.01495(7) 0.01530(7) 0.02155(8) -0.00582(6) -0.00516(6) -0.00149(5) Cs1 0.01448(7) 0.01643(7) 0.01666(7) -0.00218(6) -0.00437(5) -0.00349(5) Ag3 0.01492(11) 0.01608(11) 0.01327(12) -0.00330(9) -0.00487(9) -0.00219(9) Ag1 0.01539(11) 0.01566(11) 0.01178(11) -0.00320(9) -0.00621(9) -0.00059(9) Ag2 0.01464(8) 0.01666(8) 0.01340(8) -0.00390(7) -0.00403(6) -0.00249(6) O6 0.0175(8) 0.0253(9) 0.0220(9) -0.0072(7) -0.0078(7) -0.0018(7) O4 0.0192(8) 0.0244(9) 0.0204(9) -0.0078(7) -0.0081(7) 0.0014(7) C8 0.0194(11) 0.0111(10) 0.0152(11) -0.0049(9) -0.0057(9) -0.0005(8) N3 0.0164(9) 0.0156(9) 0.0143(10) -0.0049(8) -0.0028(7) -0.0035(7) N2 0.0162(9) 0.0155(9) 0.0135(9) -0.0048(8) -0.0041(7) -0.0009(7) C12 0.0205(11) 0.0115(10) 0.0162(11) -0.0050(9) -0.0057(9) -0.0012(8) O3 0.0199(9) 0.0256(9) 0.0227(9) -0.0071(8) -0.0084(7) 0.0000(7) O5 0.0218(9) 0.0293(10) 0.0229(9) -0.0057(8) -0.0095(7) -0.0071(7) C11 0.0231(12) 0.0189(11) 0.0147(11) -0.0059(9) -0.0037(9) -0.0029(9) C5 0.0181(11) 0.0128(10) 0.0212(12) -0.0078(9) -0.0053(9) -0.0019(9) C7 0.0239(12) 0.0173(11) 0.0153(12) -0.0040(9) -0.0042(9) -0.0044(9) C10 0.0184(11) 0.0221(12) 0.0178(12) -0.0068(10) -0.0005(9) -0.0037(9) O1 0.0151(8) 0.0278(9) 0.0208(9) -0.0076(7) -0.0055(7) -0.0010(7) C2 0.0179(11) 0.0195(11) 0.0132(11) -0.0042(9) -0.0049(9) -0.0018(9) C9 0.0181(11) 0.0122(10) 0.0220(12) -0.0061(9) -0.0051(9) -0.0026(9) C1 0.0183(11) 0.0109(10) 0.0143(11) -0.0040(9) -0.0059(9) -0.0018(8) N1 0.0159(9) 0.0127(9) 0.0123(9) -0.0029(7) -0.0060(7) -0.0010(7) C3 0.0164(11) 0.0242(12) 0.0164(12) -0.0054(10) -0.0066(9) -0.0032(9) O2 0.0171(8) 0.0248(9) 0.0180(9) -0.0049(7) -0.0013(7) -0.0026(7) C6 0.0204(12) 0.0218(12) 0.0192(12) -0.0068(10) -0.0016(10) -0.0035(10) N4 0.0165(9) 0.0135(9) 0.0153(10) -0.0047(8) -0.0061(7) -0.0009(7) C16 0.0187(11) 0.0138(11) 0.0226(12) -0.0093(9) -0.0084(9) -0.0004(9) C14 0.0278(13) 0.0174(11) 0.0194(12) -0.0062(10) -0.0128(10) 0.0008(10) C15 0.0214(12) 0.0248(13) 0.0230(13) -0.0091(11) -0.0122(10) 0.0013(10) C13 0.0204(12) 0.0117(10) 0.0179(12) -0.0057(9) -0.0063(9) -0.0008(9) O8 0.0185(8) 0.0240(9) 0.0237(9) -0.0077(8) -0.0034(7) -0.0059(7) O7 0.0204(9) 0.0246(9) 0.0170(9) -0.0050(7) -0.0030(7) -0.0029(7) C4 0.0172(11) 0.0110(10) 0.0161(11) -0.0050(9) -0.0060(9) -0.0007(8) O9 0.0204(9) 0.0289(10) 0.0251(10) -0.0090(8) -0.0037(7) -0.0064(8) O13 0.0262(10) 0.0240(9) 0.0182(9) -0.0057(8) -0.0033(7) -0.0074(7) O11 0.0175(9) 0.0363(11) 0.0226(10) -0.0065(9) -0.0077(8) -0.0025(8) O14 0.0281(11) 0.0432(12) 0.0244(10) -0.0118(9) -0.0048(9) -0.0094(9) O10 0.0360(11) 0.0283(11) 0.0322(11) -0.0096(9) -0.0188(9) 0.0016(9) O12 0.0285(11) 0.0617(15) 0.0294(12) -0.0168(11) -0.0122(9) 0.0109(10) O15 0.0292(12) 0.0755(17) 0.0439(14) -0.0322(13) -0.0204(10) 0.0123(11) O16 0.083(2) 0.0425(14) 0.0642(17) -0.0351(13) -0.0588(16) 0.0288(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cs2 Cs2 H12B 49.2(7) 2_765 . ? Cs1 Cs2 Cs2 150.917(5) 1_655 2_765 ? Cs1 Cs2 Cs2 117.807(7) 2_675 2_765 ? Cs1 Cs2 Cs1 57.762(6) 2_675 1_655 ? Cs1 Cs2 H12B 129.6(7) 2_675 . ? Cs1 Cs2 H12B 108.6(7) 1_655 . ? O4 Cs2 Cs2 104.62(3) . 2_765 ? O4 Cs2 Cs1 111.52(3) . 2_675 ? O4 Cs2 Cs1 103.18(3) . 1_655 ? O4 Cs2 H12B 118.9(7) . . ? O3 Cs2 Cs2 120.39(3) 1_655 2_765 ? O3 Cs2 Cs1 79.40(3) 1_655 2_675 ? O3 Cs2 Cs1 33.51(3) 1_655 1_655 ? O3 Cs2 O4 121.77(4) 1_655 . ? O3 Cs2 O2 71.20(4) 1_655 . ? O3 Cs2 O11 52.06(5) 1_655 2_675 ? O3 Cs2 O12 67.99(6) 1_655 . ? O3 Cs2 H12B 75.1(7) 1_655 . ? O5 Cs2 Cs2 84.46(3) . 2_765 ? O5 Cs2 Cs1 100.94(3) . 1_655 ? O5 Cs2 Cs1 43.90(3) . 2_675 ? O5 Cs2 O4 96.11(4) . . ? O5 Cs2 O3 121.52(5) . 1_655 ? O5 Cs2 O2 73.73(5) . . ? O5 Cs2 O8 81.70(5) . . ? O5 Cs2 O8 89.04(5) . 2_765 ? O5 Cs2 O11 73.34(5) . 2_675 ? O5 Cs2 O12 140.28(5) . . ? O5 Cs2 H12B 125.8(7) . . ? O2 Cs2 Cs2 158.05(3) . 2_765 ? O2 Cs2 Cs1 37.72(3) . 1_655 ? O2 Cs2 Cs1 42.55(3) . 2_675 ? O2 Cs2 O4 80.60(4) . . ? O2 Cs2 O12 137.33(5) . . ? O2 Cs2 H12B 146.3(7) . . ? O8 Cs2 Cs2 33.20(3) 2_765 2_765 ? O8 Cs2 Cs2 32.57(3) . 2_765 ? O8 Cs2 Cs1 101.67(3) 2_765 2_675 ? O8 Cs2 Cs1 117.81(3) 2_765 1_655 ? O8 Cs2 Cs1 175.41(3) . 1_655 ? O8 Cs2 Cs1 125.31(3) . 2_675 ? O8 Cs2 O4 136.90(4) 2_765 . ? O8 Cs2 O4 72.69(4) . . ? O8 Cs2 O3 147.25(4) . 1_655 ? O8 Cs2 O3 90.09(4) 2_765 1_655 ? O8 Cs2 O2 141.30(4) . . ? O8 Cs2 O2 141.02(4) 2_765 . ? O8 Cs2 O8 65.77(5) 2_765 . ? O8 Cs2 O11 128.66(5) . 2_675 ? O8 Cs2 O11 69.62(5) 2_765 2_675 ? O8 Cs2 O12 79.46(6) . . ? O8 Cs2 O12 51.32(5) 2_765 . ? O8 Cs2 H12B 37.0(7) 2_765 . ? O8 Cs2 H12B 72.4(7) . . ? O11 Cs2 Cs2 99.76(4) 2_675 2_765 ? O11 Cs2 Cs1 55.91(4) 2_675 1_655 ? O11 Cs2 Cs1 43.73(3) 2_675 2_675 ? O11 Cs2 O4 152.38(5) 2_675 . ? O11 Cs2 O2 71.98(5) 2_675 . ? O11 Cs2 O12 92.00(6) 2_675 . ? O11 Cs2 H12B 87.0(7) 2_675 . ? O12 Cs2 Cs2 61.39(4) . 2_765 ? O12 Cs2 Cs1 100.49(5) . 1_655 ? O12 Cs2 Cs1 135.70(4) . 2_675 ? O12 Cs2 O4 110.95(5) . . ? O12 Cs2 H12B 14.5(7) . . ? Cs2 Cs1 Cs2 122.237(6) 2_675 1_455 ? Cs2 Cs1 Cs1 69.596(6) 2_675 2_575 ? Cs2 Cs1 H9A 94.6(7) 1_455 . ? Cs2 Cs1 H9A 129.1(7) 2_675 . ? Cs1 Cs1 Cs2 52.641(4) 2_575 1_455 ? Cs1 Cs1 H9A 133.0(7) 2_575 . ? Ag1 Cs1 Cs2 75.063(5) . 2_675 ? Ag1 Cs1 Cs2 103.047(4) . 1_455 ? Ag1 Cs1 Cs1 90.455(6) . 2_575 ? Ag1 Cs1 H9A 133.3(7) . . ? O3 Cs1 Cs2 134.93(3) . 2_675 ? O3 Cs1 Cs2 33.88(3) . 1_455 ? O3 Cs1 Cs1 75.15(3) . 2_575 ? O3 Cs1 Ag1 78.10(3) . . ? O3 Cs1 O1 78.93(4) . . ? O3 Cs1 O2 69.79(4) . 1_455 ? O3 Cs1 O9 81.69(5) . . ? O3 Cs1 O10 125.54(5) . . ? O3 Cs1 H9A 95.5(7) . . ? O5 Cs1 Cs2 161.83(3) 2_675 1_455 ? O5 Cs1 Cs2 41.94(3) 2_675 2_675 ? O5 Cs1 Cs1 110.72(3) 2_675 2_575 ? O5 Cs1 Ag1 66.96(3) 2_675 . ? O5 Cs1 O3 144.37(5) 2_675 . ? O5 Cs1 O1 74.03(4) 2_675 . ? O5 Cs1 O2 137.13(4) 2_675 1_455 ? O5 Cs1 O9 111.47(5) 2_675 . ? O5 Cs1 O10 82.55(5) 2_675 . ? O5 Cs1 H9A 103.2(7) 2_675 . ? O1 Cs1 Cs2 109.61(3) . 2_675 ? O1 Cs1 Cs2 112.40(3) . 1_455 ? O1 Cs1 Cs1 137.53(3) . 2_575 ? O1 Cs1 Ag1 51.23(3) . . ? O1 Cs1 O2 148.01(4) . 1_455 ? O1 Cs1 O9 73.29(4) . . ? O1 Cs1 O10 100.65(5) . . ? O1 Cs1 H9A 82.1(7) . . ? O2 Cs1 Cs2 35.95(3) 1_455 1_455 ? O2 Cs1 Cs2 86.85(3) 2_675 1_455 ? O2 Cs1 Cs2 46.15(3) 2_675 2_675 ? O2 Cs1 Cs2 97.46(3) 1_455 2_675 ? O2 Cs1 Cs1 39.20(3) 1_455 2_575 ? O2 Cs1 Cs1 44.62(3) 2_675 2_575 ? O2 Cs1 Ag1 124.92(3) 1_455 . ? O2 Cs1 Ag1 51.41(3) 2_675 . ? O2 Cs1 O3 88.90(5) 2_675 . ? O2 Cs1 O5 75.05(5) 2_675 2_675 ? O2 Cs1 O1 102.58(4) 2_675 . ? O2 Cs1 O2 83.81(4) 2_675 1_455 ? O2 Cs1 O9 170.27(5) 2_675 . ? O2 Cs1 O11 76.08(5) 2_675 . ? O2 Cs1 O10 141.59(5) 2_675 . ? O2 Cs1 O10 92.32(5) 1_455 . ? O2 Cs1 H9A 94.1(7) 1_455 . ? O2 Cs1 H9A 174.1(7) 2_675 . ? O9 Cs1 Cs2 143.37(3) . 2_675 ? O9 Cs1 Cs2 86.68(3) . 1_455 ? O9 Cs1 Cs1 133.63(3) . 2_575 ? O9 Cs1 Ag1 123.41(3) . . ? O9 Cs1 O2 95.16(4) . 1_455 ? O9 Cs1 O10 48.03(5) . . ? O9 Cs1 H9A 15.2(7) . . ? O11 Cs1 Cs2 101.16(4) . 1_455 ? O11 Cs1 Cs2 45.47(4) . 2_675 ? O11 Cs1 Cs1 63.61(4) . 2_575 ? O11 Cs1 Ag1 119.67(4) . . ? O11 Cs1 O3 134.06(5) . . ? O11 Cs1 O5 73.20(5) . 2_675 ? O11 Cs1 O1 146.35(5) . . ? O11 Cs1 O2 65.63(5) . 1_455 ? O11 Cs1 O9 112.35(5) . . ? O11 Cs1 O10 67.68(5) . . ? O11 Cs1 H9A 98.1(7) . . ? O10 Cs1 Cs2 111.75(4) . 1_455 ? O10 Cs1 Cs2 97.10(3) . 2_675 ? O10 Cs1 Cs1 121.79(3) . 2_575 ? O10 Cs1 Ag1 142.39(4) . . ? O10 Cs1 H9A 32.8(7) . . ? Ag2 Ag3 Ag2 180.0 . 2_665 ? N4 Ag3 Ag2 90.09(5) 2_665 2_665 ? N4 Ag3 Ag2 89.91(5) 2_665 . ? N4 Ag3 Ag2 89.91(5) . 2_665 ? N4 Ag3 Ag2 90.09(5) . . ? N4 Ag3 N4 180.0 . 2_665 ? Cs1 Ag1 Cs1 180.0 2_675 . ? Ag2 Ag1 Cs1 86.045(4) 2_675 2_675 ? Ag2 Ag1 Cs1 86.045(5) . . ? Ag2 Ag1 Cs1 93.955(5) 2_675 . ? Ag2 Ag1 Cs1 93.955(5) . 2_675 ? Ag2 Ag1 Ag2 180.0 2_675 . ? N1 Ag1 Cs1 88.87(5) 2_675 . ? N1 Ag1 Cs1 91.13(5) 2_675 2_675 ? N1 Ag1 Cs1 88.87(5) . 2_675 ? N1 Ag1 Cs1 91.13(5) . . ? N1 Ag1 Ag2 91.15(5) . 2_675 ? N1 Ag1 Ag2 91.15(5) 2_675 . ? N1 Ag1 Ag2 88.85(5) 2_675 2_675 ? N1 Ag1 Ag2 88.85(5) . . ? N1 Ag1 N1 180.0 . 2_675 ? Ag1 Ag2 Ag3 179.110(6) . . ? N3 Ag2 Ag3 94.06(5) . . ? N3 Ag2 Ag1 86.67(5) . . ? N3 Ag2 N2 178.73(7) . . ? N2 Ag2 Ag3 84.78(5) . . ? N2 Ag2 Ag1 94.49(5) . . ? C8 O4 Cs2 152.22(15) . . ? O4 C8 N2 123.7(2) . . ? O4 C8 C7 124.9(2) . . ? N2 C8 C7 111.46(19) . . ? C12 N3 Ag2 128.15(15) . . ? C12 N3 C9 110.22(19) . . ? C9 N3 Ag2 121.63(15) . . ? C8 N2 Ag2 123.71(15) . . ? C8 N2 C5 109.93(19) . . ? C5 N2 Ag2 126.33(15) . . ? O6 C12 N3 124.4(2) . . ? O6 C12 C11 124.2(2) . . ? N3 C12 C11 111.3(2) . . ? Cs1 O3 Cs2 112.60(5) . 1_455 ? C5 O3 Cs2 135.48(15) . 1_455 ? C5 O3 Cs1 106.49(14) . . ? Cs2 O5 Cs1 94.16(5) . 2_675 ? C9 O5 Cs2 153.59(16) . . ? C9 O5 Cs1 109.09(15) . 2_675 ? C12 C11 H11A 111.0 . . ? C12 C11 H11B 111.0 . . ? C12 C11 C10 103.70(19) . . ? H11A C11 H11B 109.0 . . ? C10 C11 H11A 111.0 . . ? C10 C11 H11B 111.0 . . ? N2 C5 C6 111.4(2) . . ? O3 C5 N2 123.8(2) . . ? O3 C5 C6 124.8(2) . . ? C8 C7 H7A 111.1 . . ? C8 C7 H7B 111.1 . . ? C8 C7 C6 103.38(19) . . ? H7A C7 H7B 109.1 . . ? C6 C7 H7A 111.1 . . ? C6 C7 H7B 111.1 . . ? C11 C10 H10A 111.0 . . ? C11 C10 H10B 111.0 . . ? H10A C10 H10B 109.0 . . ? C9 C10 C11 103.61(19) . . ? C9 C10 H10A 111.0 . . ? C9 C10 H10B 111.0 . . ? C1 O1 Cs1 147.98(15) . . ? H2A C2 H2B 109.0 . . ? C1 C2 H2A 111.0 . . ? C1 C2 H2B 111.0 . . ? C1 C2 C3 103.61(18) . . ? C3 C2 H2A 111.0 . . ? C3 C2 H2B 111.0 . . ? N3 C9 C10 110.9(2) . . ? O5 C9 N3 123.9(2) . . ? O5 C9 C10 125.2(2) . . ? O1 C1 C2 124.8(2) . . ? O1 C1 N1 123.9(2) . . ? N1 C1 C2 111.30(19) . . ? C1 N1 Ag1 125.73(15) . . ? C1 N1 C4 109.98(18) . . ? C4 N1 Ag1 124.27(15) . . ? C2 C3 H3A 111.0 . . ? C2 C3 H3B 111.0 . . ? H3A C3 H3B 109.0 . . ? C4 C3 C2 103.63(18) . . ? C4 C3 H3A 111.0 . . ? C4 C3 H3B 111.0 . . ? Cs2 O2 Cs1 106.33(5) . 1_655 ? Cs1 O2 Cs2 91.30(4) 2_675 . ? Cs1 O2 Cs1 96.19(4) 2_675 1_655 ? C4 O2 Cs2 101.69(14) . . ? C4 O2 Cs1 150.22(15) . 2_675 ? C4 O2 Cs1 105.45(14) . 1_655 ? C5 C6 C7 103.65(19) . . ? C5 C6 H6A 111.0 . . ? C5 C6 H6B 111.0 . . ? C7 C6 H6A 111.0 . . ? C7 C6 H6B 111.0 . . ? H6A C6 H6B 109.0 . . ? C16 N4 Ag3 123.45(16) . . ? C13 N4 Ag3 127.22(15) . . ? C13 N4 C16 109.33(19) . . ? N4 C16 C15 111.2(2) . . ? O8 C16 N4 124.4(2) . . ? O8 C16 C15 124.4(2) . . ? H14A C14 H14B 109.1 . . ? C15 C14 H14A 111.1 . . ? C15 C14 H14B 111.1 . . ? C13 C14 H14A 111.1 . . ? C13 C14 H14B 111.1 . . ? C13 C14 C15 103.30(19) . . ? C16 C15 C14 103.29(19) . . ? C16 C15 H15A 111.1 . . ? C16 C15 H15B 111.1 . . ? C14 C15 H15A 111.1 . . ? C14 C15 H15B 111.1 . . ? H15A C15 H15B 109.1 . . ? N4 C13 C14 111.9(2) . . ? O7 C13 N4 124.1(2) . . ? O7 C13 C14 124.0(2) . . ? Cs2 O8 Cs2 114.23(5) 2_765 . ? C16 O8 Cs2 107.51(14) . . ? C16 O8 Cs2 123.70(14) . 2_765 ? N1 C4 C3 111.23(19) . . ? O2 C4 N1 124.8(2) . . ? O2 C4 C3 124.0(2) . . ? Cs1 O9 H9A 78(3) . . ? Cs1 O9 H9B 127(2) . . ? H9A O9 H9B 106(3) . . ? H13A O13 H13B 105(4) . . ? Cs2 O11 H11C 78(3) 2_675 . ? Cs2 O11 H11D 148(3) 2_675 . ? Cs1 O11 Cs2 90.80(5) . 2_675 ? Cs1 O11 H11C 120(3) . . ? Cs1 O11 H11D 114(3) . . ? H11C O11 H11D 103(4) . . ? H14C O14 H14D 101(4) . . ? Cs1 O10 H10C 147(3) . . ? Cs1 O10 H10D 115(3) . . ? H10C O10 H10D 90(4) . . ? Cs2 O12 H12A 144(3) . . ? Cs2 O12 H12B 82(3) . . ? H12A O12 H12B 101(4) . . ? H15C O15 H15D 105(3) . . ? H16A O16 H16B 114(4) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cs2 O4 3.2555(17) . ? Cs2 O3 3.1845(17) 1_655 ? Cs2 O5 2.9967(17) . ? Cs2 O2 3.2258(17) . ? Cs2 O8 3.1189(17) 2_765 ? Cs2 O8 3.1721(17) . ? Cs2 O11 3.189(2) 2_675 ? Cs2 O12 3.244(2) . ? Cs2 H12B 3.24(4) . ? Cs1 O3 3.1537(17) . ? Cs1 O5 3.1093(18) 2_675 ? Cs1 O1 3.1870(16) . ? Cs1 O2 3.0252(17) 2_675 ? Cs1 O2 3.3620(17) 1_455 ? Cs1 O9 3.2839(19) . ? Cs1 O11 3.0914(19) . ? Cs1 O10 3.420(2) . ? Cs1 H9A 3.22(4) . ? Ag3 Ag2 3.3292(3) . ? Ag3 Ag2 3.3293(3) 2_665 ? Ag3 N4 2.0895(19) . ? Ag3 N4 2.0895(19) 2_665 ? Ag1 Ag2 3.2209(3) . ? Ag1 Ag2 3.2209(3) 2_675 ? Ag1 N1 2.0749(18) . ? Ag1 N1 2.0749(18) 2_675 ? Ag2 N3 2.0745(19) . ? Ag2 N2 2.0754(19) . ? O6 C12 1.237(3) . ? O4 C8 1.234(3) . ? C8 N2 1.360(3) . ? C8 C7 1.519(3) . ? N3 C12 1.355(3) . ? N3 C9 1.375(3) . ? N2 C5 1.371(3) . ? C12 C11 1.517(3) . ? O3 Cs2 3.1845(17) 1_455 ? O3 C5 1.233(3) . ? O5 Cs1 3.1093(18) 2_675 ? O5 C9 1.221(3) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C11 C10 1.523(3) . ? C5 C6 1.509(3) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C7 C6 1.525(3) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C10 C9 1.513(3) . ? O1 C1 1.235(3) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C2 C1 1.516(3) . ? C2 C3 1.520(3) . ? C1 N1 1.363(3) . ? N1 C4 1.369(3) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C3 C4 1.513(3) . ? O2 Cs1 3.0252(17) 2_675 ? O2 Cs1 3.3620(17) 1_655 ? O2 C4 1.227(3) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? N4 C16 1.369(3) . ? N4 C13 1.358(3) . ? C16 C15 1.513(3) . ? C16 O8 1.229(3) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C14 C15 1.518(3) . ? C14 C13 1.511(3) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C13 O7 1.238(3) . ? O8 Cs2 3.1189(17) 2_765 ? O9 H9A 0.86(4) . ? O9 H9B 0.90(4) . ? O13 H13A 0.83(4) . ? O13 H13B 0.85(4) . ? O11 Cs2 3.189(2) 2_675 ? O11 H11C 0.75(4) . ? O11 H11D 0.86(4) . ? O14 H14C 0.85(4) . ? O14 H14D 0.75(4) . ? O10 H10C 0.86(4) . ? O10 H10D 0.76(4) . ? O12 H12A 0.81(4) . ? O12 H12B 0.82(4) . ? O15 H15C 0.91(3) . ? O15 H15D 0.86(4) . ? O16 H16A 0.82(4) . ? O16 H16B 0.72(4) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cs2 O4 C8 N2 6.5(5) . . . . ? Cs2 O4 C8 C7 -172.7(2) . . . . ? Cs2 O3 C5 N2 112.2(2) 1_455 . . . ? Cs2 O3 C5 C6 -68.7(3) 1_455 . . . ? Cs2 O5 C9 N3 38.5(5) . . . . ? Cs2 O5 C9 C10 -142.1(3) . . . . ? Cs2 O2 C4 N1 -102.7(2) . . . . ? Cs2 O2 C4 C3 77.1(2) . . . . ? Cs1 O3 C5 N2 -97.1(2) . . . . ? Cs1 O3 C5 C6 82.1(2) . . . . ? Cs1 O5 C9 N3 -111.9(2) 2_675 . . . ? Cs1 O5 C9 C10 67.5(2) 2_675 . . . ? Cs1 O1 C1 C2 -176.38(17) . . . . ? Cs1 O1 C1 N1 3.4(4) . . . . ? Cs1 O2 C4 N1 146.49(18) 1_655 . . . ? Cs1 O2 C4 N1 11.4(4) 2_675 . . . ? Cs1 O2 C4 C3 -33.7(2) 1_655 . . . ? Cs1 O2 C4 C3 -168.84(19) 2_675 . . . ? Ag3 N4 C16 C15 -172.84(14) . . . . ? Ag3 N4 C16 O8 7.7(3) . . . . ? Ag3 N4 C13 C14 178.88(14) . . . . ? Ag3 N4 C13 O7 -2.9(3) . . . . ? Ag1 N1 C4 C3 176.34(14) . . . . ? Ag1 N1 C4 O2 -3.9(3) . . . . ? Ag2 N3 C12 O6 3.3(3) . . . . ? Ag2 N3 C12 C11 -177.69(15) . . . . ? Ag2 N3 C9 O5 -5.3(3) . . . . ? Ag2 N3 C9 C10 175.23(14) . . . . ? Ag2 N2 C5 O3 -2.5(3) . . . . ? Ag2 N2 C5 C6 178.29(15) . . . . ? O6 C12 C11 C10 179.7(2) . . . . ? O4 C8 N2 Ag2 -0.5(3) . . . . ? O4 C8 N2 C5 -178.6(2) . . . . ? O4 C8 C7 C6 -178.4(2) . . . . ? C8 N2 C5 O3 175.5(2) . . . . ? C8 N2 C5 C6 -3.7(3) . . . . ? C8 C7 C6 C5 -4.1(2) . . . . ? N3 C12 C11 C10 0.6(2) . . . . ? N2 C8 C7 C6 2.3(2) . . . . ? N2 C5 C6 C7 5.0(3) . . . . ? C12 N3 C9 O5 174.2(2) . . . . ? C12 N3 C9 C10 -5.3(3) . . . . ? C12 C11 C10 C9 -3.4(2) . . . . ? O3 C5 C6 C7 -174.3(2) . . . . ? C11 C10 C9 N3 5.4(3) . . . . ? C11 C10 C9 O5 -174.1(2) . . . . ? C7 C8 N2 Ag2 178.86(14) . . . . ? C7 C8 N2 C5 0.8(2) . . . . ? O1 C1 N1 Ag1 0.6(3) . . . . ? O1 C1 N1 C4 179.2(2) . . . . ? C2 C1 N1 Ag1 -179.65(14) . . . . ? C2 C1 N1 C4 -1.0(2) . . . . ? C2 C3 C4 N1 4.6(2) . . . . ? C2 C3 C4 O2 -175.3(2) . . . . ? C9 N3 C12 O6 -176.2(2) . . . . ? C9 N3 C12 C11 2.9(2) . . . . ? C1 C2 C3 C4 -4.7(2) . . . . ? C1 N1 C4 C3 -2.3(2) . . . . ? C1 N1 C4 O2 177.5(2) . . . . ? C3 C2 C1 O1 -176.4(2) . . . . ? C3 C2 C1 N1 3.8(2) . . . . ? N4 C16 C15 C14 -10.3(3) . . . . ? N4 C16 O8 Cs2 -112.5(2) . . . 2_765 ? N4 C16 O8 Cs2 110.8(2) . . . . ? C16 N4 C13 C14 -1.7(2) . . . . ? C16 N4 C13 O7 176.5(2) . . . . ? C15 C16 O8 Cs2 -68.6(2) . . . . ? C15 C16 O8 Cs2 68.0(3) . . . 2_765 ? C15 C14 C13 N4 -4.7(3) . . . . ? C15 C14 C13 O7 177.1(2) . . . . ? C13 N4 C16 C15 7.8(3) . . . . ? C13 N4 C16 O8 -171.7(2) . . . . ? C13 C14 C15 C16 8.5(2) . . . . ? O8 C16 C15 C14 169.1(2) . . . . ?