#------------------------------------------------------------------------------ #$Date: 2024-10-01 01:09:10 +0300 (Tue, 01 Oct 2024) $ #$Revision: 294944 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572718.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572718 loop_ _publ_author_name 'Larsen, Emil Mickey Hilligs\/oe' 'Brock-Nannestad, Theis' 'Skibsted, J\/orgen' 'Reinholdt, Anders' 'Bendix, Jesper' _publ_section_title ; A Homoleptic AgIII Complex Stabilized by Succinimidate Ligands ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC04843A _journal_year 2024 _chemical_formula_moiety '2(C16 H16 Ag N4 O8 Rb), 4(H4 O2)' _chemical_formula_sum 'C32 H48 Ag2 N8 O24 Rb2' _chemical_formula_weight 1315.46 _space_group_crystal_system tetragonal _space_group_IT_number 87 _space_group_name_Hall '-I 4' _space_group_name_H-M_alt 'I 4/m' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2020-08-10 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-06-26 deposited with the CCDC. 2024-09-17 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 11.3963(9) _cell_length_b 11.3963(9) _cell_length_c 8.5069(6) _cell_measurement_reflns_used 8673 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 34.78 _cell_measurement_theta_min 2.53 _cell_volume 1104.84(15) _computing_cell_refinement 'SAINT V8.40A (?, 2016)' _computing_data_reduction 'SAINT V8.40A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0571 _diffrn_reflns_av_unetI/netI 0.0275 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 10557 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.480 _diffrn_reflns_theta_min 2.527 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 3.173 _exptl_absorpt_correction_T_max 0.7469 _exptl_absorpt_correction_T_min 0.6301 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1127 before and 0.0797 after correction. The Ratio of minimum to maximum transmission is 0.8436. The \l/2 correction factor is Not present.' _exptl_crystal_colour 'clear yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.977 _exptl_crystal_description plank _exptl_crystal_F_000 656 _exptl_crystal_preparation 'From water' _exptl_crystal_size_max 0.147 _exptl_crystal_size_mid 0.0992 _exptl_crystal_size_min 0.089 _refine_diff_density_max 0.449 _refine_diff_density_min -0.805 _refine_diff_density_rms 0.093 _refine_ls_extinction_coef 0.0007(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.125 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 48 _refine_ls_number_reflns 896 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.125 _refine_ls_R_factor_all 0.0305 _refine_ls_R_factor_gt 0.0214 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0100P)^2^+2.4018P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0438 _refine_ls_wR_factor_ref 0.0459 _reflns_Friedel_coverage 0.000 _reflns_number_gt 779 _reflns_number_total 896 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL mo_d8v4542_0m_a.res in I4/m REM Old TITL mo_D8V4542_0m in I4/m #87 REM SHELXT solution in I4/m REM R1 0.040, Rweak 0.003, Alpha 0.033, Orientation as input REM Formula found by SHELXT: Rb Ag C16 N4 O12 CELL 0.71073 11.3963 11.3963 8.5069 90 90 90 ZERR 1 0.0009 0.0009 0.0006 0 0 0 LATT 2 SYMM -X,-Y,+Z SYMM -Y,+X,+Z SYMM +Y,-X,+Z SFAC C H Ag N O Rb UNIT 32 48 2 8 24 2 L.S. 4 0 0 PLAN 20 SIZE 0.089 0.0992 0.147 TEMP -173(2) BOND $H list 4 fmap 2 53 acta REM REM REM WGHT 0.010000 2.401800 EXTI 0.000670 FVAR 0.35518 AG01 3 0.500000 0.500000 0.500000 10.12500 0.00421 0.00421 = 0.00446 0.00000 0.00000 0.00000 RB02 6 0.500000 0.500000 1.000000 10.12500 0.01352 0.01352 = 0.01094 0.00000 0.00000 0.00000 O003 5 0.688420 0.572383 0.766834 11.00000 0.01339 0.02302 = 0.00928 -0.00014 -0.00001 -0.00329 AFIX 6 O004 5 0.852428 0.643218 1.000000 10.50000 0.01695 0.02298 = 0.01595 0.00000 0.00000 -0.00660 H00C 2 0.801327 0.643025 0.927252 10.50000 -1.50000 H00D 2 0.821711 0.602937 1.073322 10.50000 -1.50000 AFIX 0 N005 4 0.664048 0.562140 0.500000 10.50000 0.00414 0.00922 = 0.00967 0.00000 0.00000 -0.00066 C006 1 0.726604 0.585618 0.633480 11.00000 0.00768 0.00796 = 0.01368 -0.00016 -0.00108 0.00048 C007 1 0.847513 0.629444 0.589883 11.00000 0.00807 0.01480 = 0.01311 0.00026 -0.00130 -0.00251 AFIX 23 H00A 2 0.909055 0.576555 0.631427 11.00000 -1.20000 H00B 2 0.860873 0.709484 0.631428 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_d8v4542_0m_a.res in I4/m REM R1 = 0.0214 for 779 Fo > 4sig(Fo) and 0.0305 for all 896 data REM 48 parameters refined using 0 restraints END WGHT 0.0100 2.4018 REM Highest difference peak 0.449, deepest hole -0.805, 1-sigma level 0.093 Q1 1 0.5547 0.4813 0.5000 10.50000 0.05 0.45 Q2 1 0.7163 0.5405 0.5000 10.50000 0.05 0.42 Q3 1 0.7951 0.5956 0.6188 11.00000 0.05 0.41 Q4 1 0.5000 0.5000 0.8734 10.25000 0.05 0.38 Q5 1 0.6885 0.5831 0.5709 11.00000 0.05 0.37 Q6 1 0.6763 0.6233 0.5000 10.50000 0.05 0.37 Q7 1 0.6206 0.5796 0.5000 10.50000 0.05 0.34 Q8 1 0.8553 0.6206 0.5000 10.50000 0.05 0.33 Q9 1 0.7349 0.5934 0.8282 11.00000 0.05 0.33 Q10 1 0.6513 0.7065 0.5000 10.50000 0.05 0.33 Q11 1 0.6555 0.5404 0.5473 11.00000 0.05 0.31 Q12 1 0.7575 0.5099 1.0000 10.50000 0.05 0.28 Q13 1 0.5058 0.4205 1.0368 11.00000 0.05 0.27 Q14 1 0.6030 0.5971 0.5409 11.00000 0.05 0.27 Q15 1 0.7742 0.4819 0.6945 11.00000 0.05 0.27 Q16 1 0.8959 0.6217 0.6447 11.00000 0.05 0.27 Q17 1 0.6351 0.5673 0.7199 11.00000 0.05 0.26 Q18 1 0.5619 0.5373 0.7161 11.00000 0.05 0.26 Q19 1 0.6376 0.5249 0.7799 11.00000 0.05 0.25 Q20 1 0.8980 0.6596 0.6352 11.00000 0.05 0.25 REM The information below was added by Olex2. REM REM R1 = 0.0214 for 779 Fo > 4sig(Fo) and 0.0305 for all 10557 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.45, deepest hole -0.80 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0305 REM R1_gt = 0.0214 REM wR_ref = 0.0459 REM GOOF = 1.125 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 10557 REM Reflections_gt = 779 REM Parameters = n/a REM Hole = -0.80 REM Peak = 0.45 REM Flack = n/a ; _cod_data_source_file d4sc04843a2.cif _cod_data_source_block mo_d8v4542_0m _cod_original_cell_volume 1104.84(19) _cod_database_code 1572718 _shelxl_version_number 2013-3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.765 _shelx_estimated_absorpt_t_min 0.653 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups At 1.5 times of: All O(H,H) groups 2. Others Fixed Sof: H00C(0.5) H00D(0.5) 3.a Free rotating group: O004(H00C,H00D) 3.b Secondary CH2 refined with riding coordinates: C007(H00A,H00B) ; _olex2_exptl_crystal_mounting_method 'silicone grease on Kapton loop' _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-y, x, z' 'y, -x, z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-y+1/2, x+1/2, z+1/2' 'y+1/2, -x+1/2, z+1/2' '-x, -y, -z' 'x, y, -z' 'y, -x, -z' '-y, x, -z' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, y+1/2, -z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ag01 Ag 0.5000 0.5000 0.5000 0.00429(11) Uani 1 8 d S T P . . Rb02 Rb 0.5000 0.5000 1.0000 0.01266(13) Uani 1 8 d S T P . . O003 O 0.68842(11) 0.57238(12) 0.76683(16) 0.0152(3) Uani 1 1 d . . . . . O004 O 0.85243(18) 0.6432(2) 1.0000 0.0186(4) Uani 1 2 d S T P . . H00C H 0.8013 0.6430 0.9273 0.028 Uiso 0.5 1 d G . . . . H00D H 0.8217 0.6029 1.0733 0.028 Uiso 0.5 1 d G . . . . N005 N 0.66405(18) 0.56214(19) 0.5000 0.0077(4) Uani 1 2 d S T P . . C006 C 0.72660(15) 0.58562(15) 0.6335(2) 0.0098(3) Uani 1 1 d . . . . . C007 C 0.84751(16) 0.62944(17) 0.5899(2) 0.0120(4) Uani 1 1 d . . . . . H00A H 0.9091 0.5766 0.6314 0.014 Uiso 1 1 calc R . . . . H00B H 0.8609 0.7095 0.6314 0.014 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ag01 0.00421(13) 0.00421(13) 0.00446(19) 0.000 0.000 0.000 Rb02 0.01352(18) 0.01352(18) 0.0109(3) 0.000 0.000 0.000 O003 0.0134(6) 0.0230(7) 0.0093(7) -0.0001(5) 0.0000(5) -0.0033(5) O004 0.0169(11) 0.0230(11) 0.0160(11) 0.000 0.000 -0.0066(9) N005 0.0041(9) 0.0092(10) 0.0097(10) 0.000 0.000 -0.0007(8) C006 0.0077(8) 0.0080(8) 0.0137(9) -0.0002(7) -0.0011(7) 0.0005(6) C007 0.0081(8) 0.0148(9) 0.0131(9) 0.0003(7) -0.0013(7) -0.0025(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Rb02 Ag01 Rb02 180.0 . 1_554 ? N005 Ag01 Rb02 90.0 9_666 . ? N005 Ag01 Rb02 90.0 9_666 1_554 ? N005 Ag01 Rb02 90.0 3_655 1_554 ? N005 Ag01 Rb02 90.0 . 1_554 ? N005 Ag01 Rb02 90.0 11_566 1_554 ? N005 Ag01 Rb02 90.0 3_655 . ? N005 Ag01 Rb02 90.0 . . ? N005 Ag01 Rb02 90.0 11_566 . ? N005 Ag01 N005 90.0 11_566 . ? N005 Ag01 N005 180.0 9_666 . ? N005 Ag01 N005 180.0 11_566 3_655 ? N005 Ag01 N005 90.0 3_655 . ? N005 Ag01 N005 90.0 9_666 3_655 ? N005 Ag01 N005 90.0 9_666 11_566 ? Ag01 Rb02 Ag01 180.0 . 1_556 ? O003 Rb02 Ag01 130.77(3) 4_565 1_556 ? O003 Rb02 Ag01 49.23(3) 10_557 1_556 ? O003 Rb02 Ag01 130.77(3) 9_667 . ? O003 Rb02 Ag01 49.23(3) 3_655 . ? O003 Rb02 Ag01 49.23(3) 9_667 1_556 ? O003 Rb02 Ag01 49.23(3) 12_657 1_556 ? O003 Rb02 Ag01 49.23(3) . . ? O003 Rb02 Ag01 130.77(3) 11_567 . ? O003 Rb02 Ag01 130.77(3) 10_557 . ? O003 Rb02 Ag01 130.77(3) . 1_556 ? O003 Rb02 Ag01 49.23(3) 2_665 . ? O003 Rb02 Ag01 130.77(3) 2_665 1_556 ? O003 Rb02 Ag01 130.77(3) 12_657 . ? O003 Rb02 Ag01 130.77(3) 3_655 1_556 ? O003 Rb02 Ag01 49.23(3) 4_565 . ? O003 Rb02 Ag01 49.23(3) 11_567 1_556 ? O003 Rb02 O003 115.24(3) 2_665 11_567 ? O003 Rb02 O003 180.0 12_657 4_565 ? O003 Rb02 O003 115.24(3) 2_665 12_657 ? O003 Rb02 O003 98.46(5) 12_657 11_567 ? O003 Rb02 O003 98.46(5) . 2_665 ? O003 Rb02 O003 81.54(5) 4_565 11_567 ? O003 Rb02 O003 115.24(3) 10_557 4_565 ? O003 Rb02 O003 64.76(3) 9_667 11_567 ? O003 Rb02 O003 98.46(5) 10_557 9_667 ? O003 Rb02 O003 115.24(3) 10_557 3_655 ? O003 Rb02 O003 115.24(3) . 11_567 ? O003 Rb02 O003 64.76(3) 2_665 3_655 ? O003 Rb02 O003 64.76(3) . 4_565 ? O003 Rb02 O003 81.54(5) 12_657 3_655 ? O003 Rb02 O003 64.76(3) 2_665 4_565 ? O003 Rb02 O003 98.46(5) 4_565 3_655 ? O003 Rb02 O003 180.0 . 9_667 ? O003 Rb02 O003 115.24(3) 9_667 3_655 ? O003 Rb02 O003 81.54(5) 2_665 9_667 ? O003 Rb02 O003 180.0 11_567 3_655 ? O003 Rb02 O003 180.0 10_557 2_665 ? O003 Rb02 O003 115.24(3) . 12_657 ? O003 Rb02 O003 64.76(3) 10_557 11_567 ? O003 Rb02 O003 64.76(3) 10_557 12_657 ? O003 Rb02 O003 64.76(3) 12_657 9_667 ? O003 Rb02 O003 81.54(5) . 10_557 ? O003 Rb02 O003 115.24(3) 4_565 9_667 ? O003 Rb02 O003 64.76(3) . 3_655 ? C006 O003 Rb02 152.85(12) . . ? H00C O004 H00D 104.5 . . ? C006 N005 Ag01 123.85(11) . . ? C006 N005 Ag01 123.84(11) 10_556 . ? C006 N005 C006 112.3(2) . 10_556 ? O003 C006 N005 124.06(17) . . ? O003 C006 C007 126.29(17) . . ? N005 C006 C007 109.64(16) . . ? C006 C007 C007 104.20(10) . 10_556 ? C006 C007 H00A 110.9 . . ? C006 C007 H00B 110.9 . . ? C007 C007 H00A 110.9 10_556 . ? C007 C007 H00B 110.9 10_556 . ? H00A C007 H00B 108.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ag01 Rb02 4.2534(3) 1_554 ? Ag01 Rb02 4.2534(3) . ? Ag01 N005 1.999(2) 9_666 ? Ag01 N005 1.999(2) . ? Ag01 N005 1.999(2) 11_566 ? Ag01 N005 1.999(2) 3_655 ? Rb02 Ag01 4.2534(3) 1_556 ? Rb02 O003 3.0374(14) 10_557 ? Rb02 O003 3.0374(14) 11_567 ? Rb02 O003 3.0374(14) 4_565 ? Rb02 O003 3.0374(14) 2_665 ? Rb02 O003 3.0374(14) 3_655 ? Rb02 O003 3.0374(14) 12_657 ? Rb02 O003 3.0374(14) . ? Rb02 O003 3.0374(14) 9_667 ? O003 C006 1.224(2) . ? O004 H00C 0.8498 . ? O004 H00D 0.8499 . ? N005 C006 1.367(2) . ? N005 C006 1.367(2) 10_556 ? C006 C007 1.512(2) . ? C007 C007 1.529(4) 10_556 ? C007 H00A 0.9900 . ? C007 H00B 0.9900 . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 1 -1 0 3174.28 104.79 1 1 0 3139.09 104.49 1 -1 0 2870.71 103.89 1 -1 0 3065.79 104.09 1 -1 0 3062.89 104.29 -1 1 0 3042.2 104.59 -1 1 0 2985.1 103.89 2 0 0 1145.69 41 0 2 0 1159.78 40.1 0 2 0 1083.99 41.8 2 0 0 1117.59 41.4 0 -2 0 1143.59 40.2 0 -2 0 1106.09 42 -2 0 0 1192.98 41 -2 0 0 1169.68 41.6 2 -2 0 381.36 17.9 2 -2 0 405.76 18.2 2 -2 0 416.56 19.3 2 -2 0 408.16 19.5 2 2 0 447.36 19 -2 -2 0 409.96 17.7 -2 -2 0 435.56 19.4 -2 2 0 411.46 19.6 -2 2 0 405.46 17.8 -2 2 0 422.16 18.5 1 -3 0 9999 335.47 3 1 0 9544.04 333.37 -3 -1 0 9878.71 334.17 -3 -1 0 9871.31 333.47 3 -1 0 22 6.8 3 -1 0 19.9 7.4 -3 1 0 15.7 6.2 3 -1 0 21.6 5.8 -3 1 0 18 7.2 3 -3 0 30.2 8.8 -3 3 0 27.9 7.6 3 3 0 17 6 -3 3 0 26.9 8.7 -3 -3 0 18.3 7.3 3 -3 0 19.2 6.4 3 -3 0 23 7.9 -3 -3 0 15.4 5.7 3 -3 0 34.8 8 -3 3 0 28.9 6.9 -2 4 0 9168.98 307.97 -2 4 0 8846.71 310.57 4 2 0 8926.21 308.77 -4 -2 0 8798.62 308.57 2 -4 0 9260.27 310.67 -4 -2 0 9114.69 310.07 2 -4 0 8891.91 308.27 2 -4 0 9168.98 311.37 -2 4 0 9199.98 311.67 4 0 0 31.8 7.6 0 -4 0 36.8 6.3 0 4 0 21.2 9.4 0 4 0 24.6 7.8 -4 0 0 39.7 8.3 -4 0 0 34.2 7.7 0 4 0 26.4 5.2 4 -2 0 895.41 37.5 -4 2 0 899.91 36.7 -4 2 0 928.51 38.6 2 4 0 989.3 38.7 -2 -4 0 847.72 38.6 -4 2 0 932.31 37.6 4 -2 0 928.91 38.6 4 -2 0 945.81 36.4 4 -4 0 3097.29 113.59 4 -4 0 2679.33 110.09 4 -4 0 3077.49 111.09 -4 4 0 3173.78 111.09 4 4 0 3335.67 112.99 -4 4 0 3219.28 110.59 -4 -4 0 3053.69 110.29 4 -4 0 3024.8 111.99 -4 4 0 3250.37 114.19 -4 -4 0 3046.6 113.09 -5 -3 0 2724.13 100.39 -3 5 0 2826.22 102.69 3 -5 0 2749.92 103.69 3 -5 0 2874.11 102.59 -3 5 0 2871.11 99.79 -3 5 0 2818.12 104.29 3 -5 0 2715.83 100.19 -5 -3 0 2712.33 102.39 -1 5 0 6985.8 244.48 1 -5 0 6887.11 239.18 -1 5 0 6535.45 237.58 -5 -1 0 7049.79 240.68 -5 -1 0 7176.68 241.88 -1 5 0 7171.78 243.98 5 1 0 7262.17 240.88 -1 5 0 6982.8 238.98 1 -5 0 6773.12 243.18 -5 1 0 1600.14 63.19 -5 1 0 1781.52 62.89 1 5 0 1581.24 63.79 5 -1 0 1647.24 62.59 -1 -5 0 1653.13 60.09 -1 -5 0 1629.44 64.69 5 -1 0 1635.14 63.59 -5 3 0 2570.14 94.79 5 -3 0 2618.94 97.39 -5 3 0 2601.24 97.39 5 -3 0 2670.93 94.49 5 -3 0 2532.65 95.89 -5 3 0 2603.94 96.09 -3 -5 0 2471.05 97.49 3 5 0 2844.22 97.89 -5 5 0 222.68 18.4 5 -5 0 185.68 21.9 5 5 0 242.08 19.7 -5 5 0 231.88 22.3 -5 -5 0 211.38 21.2 -5 5 0 254.17 19.4 5 -5 0 251.77 12 5 -5 0 253.37 19.2 5 -5 0 226.58 21.9 -5 -5 0 246.58 16.8 4 -6 0 16 10.6 -6 -4 0 11.2 8.2 4 -6 0 11.4 12.8 -4 6 0 10 12.5 -4 6 0 13.8 10.7 -6 -4 0 6.2 9.6 4 -6 0 -16.3 11.8 -4 6 0 6.2 8.7 4 -6 0 -8.8 9.6 -2 6 0 2683.83 107.99 6 2 0 2813.02 104.59 -6 -2 0 2968.8 104.79 2 -6 0 2902.21 108.49 -6 -2 0 2968.1 106.49 -2 6 0 2970.2 103.09 -2 6 0 2925.51 99.09 2 -6 0 2819.02 103.39 -6 0 0 1748.72 67.19 0 6 0 1722.03 71.29 0 6 0 1694.43 68.49 6 0 0 1718.63 66.39 0 -6 0 1742.13 63.79 -6 0 0 1714.13 66.09 2 6 0 3644.64 128.89 -6 2 0 3740.53 128.69 6 -2 0 3555.54 125.09 -6 2 0 3589.54 126.99 -2 -6 0 3526.85 123.79 -6 2 0 3408.46 125.59 6 -2 0 3405.26 127.79 -2 -6 0 3108.39 128.39 6 -2 0 3641.54 127.09 6 -4 0 1788.22 70.09 4 6 0 2105.09 74.79 6 -4 0 1812.42 72.89 6 -4 0 1853.51 74.49 -4 -6 0 1714.73 74.19 -6 4 0 1819.42 70.79 -6 4 0 1817.32 74.39 6 -6 0 986.2 35 6 -6 0 993.8 44.8 6 -6 0 917.51 48.4 -6 -6 0 937.41 43.3 -6 6 0 899.41 48.8 6 -6 0 961.7 48.1 -6 6 0 1056.59 44.8 6 6 0 1094.59 48 -6 -6 0 972.3 48.3 -6 6 0 950 43.9 5 -7 0 561.54 36.3 5 -7 0 582.14 36.1 -5 7 0 569.44 36.8 -5 7 0 631.34 35.8 -7 -5 0 573.24 31.6 5 -7 0 508.95 31.6 -7 -5 0 581.44 35 -5 7 0 587.44 30.9 -7 -3 0 3253.87 126.19 -3 7 0 3656.73 123.19 -3 7 0 3464.25 128.39 3 -7 0 3372.76 123.59 7 3 0 3353.16 124.79 -7 -3 0 3534.55 124.69 3 -7 0 3333.47 128.39 -1 7 0 3.3 6.8 1 -7 0 6.7 7.8 -7 -1 0 3.8 9.6 -7 -1 0 22.7 11.1 -1 7 0 7.4 10 7 1 0 11 10.7 1 -7 0 10.9 12.1 -1 7 0 7 7.9 -1 7 0 9 12.7 7 -1 0 587.94 31.3 -1 -7 0 511.95 32.6 7 -1 0 593.24 32.9 1 7 0 597.14 32.7 -7 1 0 607.14 30.9 1 7 0 611.14 37.4 7 -1 0 612.34 29.9 -1 -7 0 576.74 27.5 -7 1 0 619.94 32.5 -3 -7 0 4851.61 188.38 -7 3 0 5098.09 184.58 7 -3 0 5110.89 183.48 7 -3 0 5177.98 187.48 -7 3 0 5276.87 187.88 -7 3 0 5322.97 186.28 7 -3 0 5204.68 186.08 3 7 0 5705.73 188.98 -3 -7 0 5223.48 182.28 7 -5 0 963.7 44.1 7 -5 0 998.2 47.8 -5 -7 0 1021.4 49.99 -5 -7 0 984 44 7 -5 0 1038.4 49.99 -7 5 0 982.3 45.2 -7 5 0 921.51 49.5 5 7 0 1080.39 48.7 7 -7 0 650.33 43.1 -7 -7 0 627.64 34.2 -7 -7 0 624.34 40.5 -7 7 0 575.64 37 7 -7 0 665.33 36.6 7 -7 0 601.04 39.4 -7 7 0 580.14 43.1 7 7 0 717.93 41.6 -7 7 0 643.74 36.3 6 -8 0 512.15 37.4 -8 -6 0 504.65 36.1 -8 -6 0 486.75 32.6 -6 8 0 486.15 32 6 -8 0 475.85 36.8 6 -8 0 434.06 31.8 -6 8 0 458.65 39.6 -6 8 0 497.15 34 4 -8 0 1003.7 50.69 -8 -4 0 982.2 45.9 4 -8 0 964.7 45 -4 8 0 976.6 49.99 -8 -4 0 985.5 48.6 -4 8 0 1042.1 44.2 -8 -2 0 1404.76 58.29 -2 8 0 1388.36 50.89 -8 -2 0 1423.96 60.29 -2 8 0 1455.35 55.79 8 2 0 1410.36 59.29 2 -8 0 1362.76 56.29 2 -8 0 1362.46 62.59 -2 8 0 1316.87 62.59 -2 8 0 1444.06 64.69 -8 -2 0 1434.36 60.79 0 -8 0 515.85 26.7 0 -8 0 488.95 33.8 0 8 0 474.55 36.3 -8 0 0 519.25 31.6 0 8 0 588.34 26.7 0 8 0 505.85 32.3 -8 0 0 522.15 31.2 8 0 0 512.95 31.8 -8 2 0 843.12 40.6 8 -2 0 886.51 42.6 -2 -8 0 774.12 44 2 8 0 863.41 50.29 2 8 0 882.01 43.7 8 -2 0 885.51 40 -8 2 0 848.22 43.8 8 -2 0 848.72 44 -2 -8 0 877.61 37.7 -8 2 0 883.51 42.5 8 -4 0 339.97 24.4 8 -4 0 318.47 28.5 -8 4 0 329.57 26.3 -4 -8 0 312.77 21.2 -8 4 0 365.76 31 8 -4 0 306.47 30.7 4 8 0 356.86 28 -4 -8 0 306.77 28.8 8 -6 0 1955.4 79.09 8 -6 0 2066.69 84.39 6 8 0 2159.78 85.49 -6 -8 0 1957.2 79.09 -6 -8 0 1910.01 85.39 8 -6 0 2073.79 86.89 -8 6 0 1852.11 84.79 8 -8 0 1407.16 67.69 8 -8 0 1306.07 67.99 -8 -8 0 1362.16 67.49 -8 8 0 1358.66 60.89 7 -9 0 889.81 55.49 -9 -7 0 877.31 51.09 7 -9 0 852.71 52.79 -7 9 0 893.71 48.7 -9 -5 0 518.65 36.8 5 -9 0 498.65 37.6 -5 9 0 511.45 37.5 5 -9 0 511.25 37.6 -5 9 0 459.15 31.2 5 -9 0 467.25 32.1 -9 -5 0 467.85 33.7 3 -9 0 1717.73 69.39 3 -9 0 1752.72 77.09 -9 -3 0 1679.03 71.49 -9 -3 0 1690.23 73.39 9 3 0 1739.03 71.79 -9 -3 0 1813.72 74.29 -3 9 0 1745.83 76.79 -3 9 0 1775.42 68.29 -3 9 0 1597.14 76.79 -9 -1 0 407.26 31.1 -9 -1 0 443.96 31.9 1 -9 0 441.16 26 -1 9 0 437.06 23.7 -1 9 0 455.15 25.6 9 1 0 428.06 31.5 -1 9 0 470.45 36.6 -1 9 0 395.16 32.8 1 -9 0 430.76 33.7 -1 -9 0 1363.76 56.89 -9 1 0 1406.76 61.79 9 -1 0 1423.56 62.59 1 9 0 1416.06 64.29 9 -1 0 1407.66 60.29 -9 1 0 1453.55 64.09 1 9 0 1485.35 70.79 9 -3 0 493.75 29.4 -9 3 0 449.36 32.2 9 -3 0 473.55 34.8 -3 -9 0 436.96 34 3 9 0 419.96 40.2 -9 3 0 438.46 37.7 3 9 0 475.45 34.4 9 -3 0 459.15 34.4 -3 -9 0 457.25 26.1 -9 3 0 447.56 32.6 5 9 0 380.66 33.1 -5 -9 0 372.26 24.6 -5 -9 0 348.77 33.5 9 -5 0 347.77 27 9 -5 0 404.66 37.1 9 -5 0 413.26 36.2 9 -7 0 653.03 46.6 9 -7 0 697.63 47.7 9 -7 0 662.73 38.5 9 -7 0 675.53 28.3 -7 -9 0 609.34 44.2 9 -9 0 878.21 57.29 -9 -9 0 851.51 55.39 9 -9 0 904.31 58.49 8 -10 0 331.87 40.5 8 -10 0 370.36 42.4 -8 10 0 294.47 36 -10 -8 0 262.87 36.5 -10 -6 0 202.68 31 6 -10 0 183.28 28.9 6 -10 0 244.38 36.6 -6 10 0 277.97 36.9 6 -10 0 178.08 27 -4 10 0 2340.47 94.49 4 -10 0 2489.35 103.49 -4 10 0 2516.15 103.59 4 -10 0 2441.06 96.09 -10 -4 0 2525.25 101.29 -2 10 0 435.96 20.4 10 2 0 411.26 32.1 2 -10 0 379.46 27 2 -10 0 374.76 34.8 -2 10 0 391.26 27 -10 -2 0 451.95 34.5 -10 -2 0 426.56 33.7 -10 -2 0 371.26 35.9 -2 10 0 414.26 37.6 -2 10 0 370.86 36.1 0 10 0 409.86 34.9 -10 0 0 474.45 33.5 10 0 0 428.66 34.2 -10 0 0 389.06 35 0 -10 0 390.56 26 0 10 0 414.56 27.8 0 10 0 435.56 40.1 0 -10 0 428.96 35.8 2 10 0 1612.54 74.49 -10 2 0 1557.94 73.09 10 -2 0 1747.53 73.69 2 10 0 1740.83 82.69 10 -2 0 1656.03 68.99 -10 2 0 1549.94 91.89 -2 -10 0 1737.63 66.79 10 -4 0 575.94 40 -4 -10 0 591.24 32.2 10 -4 0 648.54 44.5 4 10 0 558.34 49.1 -4 -10 0 528.85 40.5 10 -4 0 622.14 35.7 -6 -10 0 243.18 22.7 10 -6 0 218.88 34.9 10 -6 0 254.87 28 10 -6 0 248.38 34 -6 -10 0 189.08 31.4 10 -8 0 337.47 43.2 10 -8 0 398.66 46 -8 -10 0 338.07 39 10 -10 0 674.03 55.89 10 -10 0 674.93 62.49 -10 -10 0 565.14 51.69 9 -11 0 706.83 59.09 -11 -9 0 667.53 54.79 -9 11 0 587.04 48.5 9 -11 0 800.42 60.29 7 -11 0 413.06 46 -11 -7 0 404.46 40.2 7 -11 0 373.86 46.9 -7 11 0 322.37 40.8 5 -11 0 520.65 43.6 5 -11 0 477.45 36.4 -11 -5 0 564.84 42.7 -5 11 0 581.54 46.1 5 -11 0 559.24 43.1 -11 -3 0 485.05 38.4 3 -11 0 510.65 41.2 3 -11 0 506.45 33.2 -3 11 0 460.25 44 11 3 0 540.15 40.8 -1 11 0 973.6 42.5 11 1 0 999 51.49 1 -11 0 948.01 55.69 -1 11 0 957.3 59.39 -11 -1 0 1054.09 54.49 1 -11 0 890.11 45.4 1 11 0 1249.38 58.19 11 -1 0 1319.07 61.99 -1 -11 0 1342.57 55.79 -1 -11 0 1247.78 66.09 1 11 0 1283.57 71.49 11 -1 0 1244.38 60.49 11 -3 0 163.08 26.5 -3 -11 0 172.18 20.2 3 11 0 118.89 28.7 -3 -11 0 136.99 26.1 11 -5 0 844.32 55.99 11 -5 0 868.61 45.9 -5 -11 0 868.41 42.5 -5 -11 0 807.52 52.49 11 -5 0 882.71 52.89 5 11 0 833.52 61.29 11 -7 0 734.43 37.2 11 -7 0 806.82 45 11 -7 0 823.72 58.39 -7 -11 0 852.21 42.3 11 -7 0 815.02 59.69 -7 -11 0 747.43 53.19 11 -9 0 104.39 37.8 -9 -11 0 215.88 25.7 -9 -11 0 161.78 32.5 11 -9 0 174.98 37 -11 -11 0 101.19 33.1 11 -11 0 67.09 41.3 11 -11 0 158.78 41.4 10 -12 0 428.06 60.59 10 -12 0 438.26 63.69 -12 -10 0 303.87 52.69 8 -12 0 172.98 40.2 -12 -8 0 286.37 39.3 8 -12 0 242.88 38.5 -8 12 0 222.88 33.9 6 -12 0 337.97 35.3 -12 -6 0 339.17 40.1 -6 12 0 356.56 47.5 6 -12 0 415.16 45.3 6 -12 0 347.17 45.4 -12 -4 0 881.31 54.39 4 -12 0 880.71 47.9 4 -12 0 894.71 59.39 -4 12 0 895.31 59.79 12 2 0 195.88 28.5 -12 -2 0 147.79 25.6 2 -12 0 209.98 34.7 2 -12 0 198.58 24.6 -2 12 0 198.18 15.1 -2 12 0 220.28 40.2 0 12 0 976.4 63.19 12 0 0 989.3 54.69 0 -12 0 881.31 55.89 0 12 0 877.01 45.4 12 0 0 857.91 55.49 0 -12 0 932.31 45.6 12 -2 0 711.73 47.5 2 12 0 639.64 55.99 12 -2 0 828.72 45.9 -2 -12 0 679.93 37.7 -2 -12 0 642.14 49.99 4 12 0 563.54 54.59 -4 -12 0 551.04 33.2 12 -4 0 463.85 39.5 -4 -12 0 493.75 43.7 12 -4 0 541.25 46.9 12 -4 0 601.04 49.4 12 -6 0 379.46 34.6 -6 -12 0 321.67 28.1 12 -6 0 352.46 49.5 6 12 0 407.16 54.39 -6 -12 0 288.17 39.1 12 -6 0 335.37 48.1 12 -8 0 458.35 53.19 12 -8 0 368.26 54.59 -8 -12 0 360.56 45 -8 -12 0 486.15 33.5 8 12 0 346.97 59.09 -10 -12 0 341.67 48.9 10 12 0 420.26 65.29 12 -10 0 365.56 54.99 -10 -12 0 278.37 32.5 12 -10 0 380.26 64.29 9 -13 0 445.66 59.99 9 -13 0 430.56 63.89 -9 13 0 259.17 42.1 -13 -9 0 383.06 49.7 7 -13 0 83.89 35.9 -13 -7 0 54.29 28.5 7 -13 0 67.69 34 -7 13 0 -8.6 30.8 5 -13 0 891.31 62.59 5 -13 0 867.11 61.99 5 -13 0 871.31 51.99 -13 -5 0 933.71 61.09 -5 13 0 1031.4 66.79 3 -13 0 341.77 32.5 13 3 0 291.47 42.3 -13 -3 0 320.57 40.9 -3 13 0 313.87 47.8 3 -13 0 324.87 45.8 13 1 0 280.37 41.4 1 -13 0 320.87 29.4 -13 -1 0 383.96 41.2 -1 13 0 340.57 47.4 -1 13 0 305.17 26.1 1 -13 0 317.17 41.5 1 13 0 630.24 57.79 1 13 0 609.14 40.7 13 -1 0 633.44 52.19 -1 -13 0 581.44 36.4 13 -1 0 558.64 49.1 -1 -13 0 587.94 50.09 13 -3 0 595.04 52.09 -3 -13 0 576.84 35.7 3 13 0 575.64 57.59 5 13 0 469.85 57.69 13 -5 0 429.86 49.9 13 -5 0 457.05 54.09 -5 -13 0 456.65 32.3 -5 -13 0 411.66 44.3 13 -7 0 365.06 52.59 -7 -13 0 303.47 43.5 7 13 0 344.47 62.19 -7 -13 0 370.16 31.8 13 -7 0 401.76 53.39 -9 -13 0 398.96 49.4 13 -9 0 347.87 49.2 -9 -13 0 371.16 34.8 9 13 0 462.45 70.29 13 -9 0 418.26 59.79 8 -14 0 405.56 65.29 -8 14 0 456.85 58.79 8 -14 0 479.75 61.49 -14 -8 0 367.66 53.69 6 -14 0 410.96 43.5 -6 14 0 521.95 65.09 6 -14 0 476.95 59.99 -14 -6 0 442.26 52.69 6 -14 0 465.65 56.99 4 -14 0 82.39 33 4 -14 0 78.39 23.9 -4 14 0 68.99 34.7 -14 -4 0 81.89 28.7 -2 14 0 356.26 52.49 2 -14 0 281.17 45.9 2 -14 0 352.36 34.2 14 2 0 368.36 42.3 -14 -2 0 378.46 44.7 -14 0 0 944.31 63.29 0 -14 0 990.8 64.69 0 14 0 936.91 49.99 14 0 0 988.8 64.49 0 14 0 968.5 72.29 0 -14 0 953.9 50.19 -2 -14 0 99.69 19.6 -2 -14 0 94.59 35.7 2 14 0 120.59 39.1 14 -2 0 123.29 34 2 14 0 173.78 30 4 14 0 391.56 48.7 4 14 0 316.87 57.49 -4 -14 0 348.87 31.1 14 -4 0 434.06 55.99 -6 -14 0 665.83 40.4 14 -6 0 618.64 64.89 6 14 0 678.93 73.39 14 -6 0 691.63 62.99 -6 -14 0 581.34 54.99 14 -8 0 296.07 48.5 -8 -14 0 352.66 34.7 14 -8 0 377.36 59.29 -8 -14 0 275.27 48.5 8 14 0 339.27 63.69 -5 15 0 844.02 75.79 -15 -5 0 774.52 65.69 5 -15 0 776.92 52.79 5 -15 0 803.12 72.79 5 -15 0 761.52 65.29 3 -15 0 208.18 41.3 3 -15 0 133.59 27.5 -15 -3 0 142.69 36.1 -3 15 0 133.19 40.6 -1 15 0 278.27 49.7 15 1 0 279.17 42 1 -15 0 285.47 33.3 1 -15 0 188.78 40.1 -15 -1 0 192.58 34.9 -1 -15 0 285.47 45.9 -1 -15 0 219.98 30.7 15 -1 0 325.17 44.2 1 15 0 187.68 42.8 1 15 0 295.27 34 15 -3 0 581.34 62.09 3 15 0 534.85 69.09 -3 -15 0 590.24 40.5 3 15 0 579.54 54.89 -3 -15 0 670.53 61.29 15 -5 0 327.77 48.3 -5 -15 0 239.18 31.8 5 15 0 287.97 58.19 5 15 0 284.37 46.9 2 -16 0 479.45 44.9 -16 -2 0 529.75 60.89 2 -16 0 394.36 62.59 16 2 0 479.55 60.79 -2 16 0 530.55 73.39 0 16 0 169.18 45.9 0 -16 0 259.87 45.5 -16 0 0 142.69 38.7 0 -16 0 243.98 36 16 0 0 312.57 46.2 2 16 0 217.88 37.2 2 16 0 133.89 43.9 16 -2 0 145.79 41.3 -16 2 0 195.78 44.5 -2 -16 0 132.19 41.9 -2 -16 0 135.19 24.9 0 -1 -1 806.62 28.7 1 0 -1 829.12 29.8 -1 0 -1 801.92 29 -1 0 -1 837.72 29.4 0 -1 -1 862.71 29.5 0 1 -1 827.42 32.1 0 1 -1 868.31 31.1 1 0 -1 829.72 31.1 0 1 -1 810.62 30.4 0 1 -1 849.41 29.7 1 0 -1 857.31 30.3 -1 0 -1 893.01 32 -1 0 1 825.32 31 1 0 1 891.51 31.9 0 -1 1 850.91 31.1 1 0 1 818.72 29.3 -1 0 1 818.32 29.8 1 0 1 796.42 29.4 0 -1 1 870.11 32.3 0 1 1 746.33 29.3 0 -1 1 804.92 30.5 1 0 1 809.72 29 0 -1 1 839.72 29.7 -1 0 1 842.32 30.2 -1 2 -1 161.68 9.1 -1 2 -1 135.29 12.8 -2 -1 -1 161.98 8.9 2 1 -1 142.89 9.7 1 -2 -1 150.18 10.5 -1 2 -1 153.88 9.7 1 -2 -1 138.29 8 -2 -1 -1 153.38 8.4 1 -2 -1 149.29 9.2 2 1 -1 174.58 10.7 -1 2 1 155.58 10.5 1 -2 1 152.78 9.7 1 -2 1 134.49 10.8 1 -2 1 158.78 9.5 1 -2 1 157.88 12.5 2 1 1 143.49 8.2 -1 2 1 151.68 7.7 -2 -1 1 156.18 10.8 -2 -1 1 149.29 9.6 -1 2 1 149.49 8 1 2 -1 122.89 9.6 -2 1 -1 122.69 11.7 2 -1 -1 114.99 9.4 -2 1 -1 119.69 8.5 2 -1 -1 121.19 10.4 2 -1 -1 96.39 8.6 -2 1 -1 120.19 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32.8 -4 -6 2 559.14 35.1 6 -4 2 609.64 34.3 6 -4 2 618.84 36 4 6 2 661.53 31.1 -6 -6 -2 1485.75 64.29 6 6 -2 1705.93 67.99 6 -6 -2 1471.25 63.49 -6 6 -2 1490.95 67.59 6 6 -2 1496.85 72.09 -6 6 -2 1558.04 62.69 -6 -6 -2 1528.05 59.79 -6 6 -2 1463.95 66.79 6 -6 -2 1529.95 67.49 6 6 2 1749.12 64.69 6 -6 2 1521.85 59.39 6 -6 2 1483.15 67.89 6 -6 2 1514.15 66.59 6 -6 2 1436.56 63.89 -6 6 2 1464.05 67.49 -6 -6 2 1467.85 62.79 -6 -6 2 1463.95 67.89 6 -6 2 1520.85 66.19 -7 -5 -2 1557.04 64.79 -7 -5 -2 1543.65 60.79 5 -7 -2 1487.85 63.79 5 -7 -2 1562.04 68.09 -5 7 -2 1525.25 62.69 -5 7 -2 1530.15 69.99 5 -7 2 1534.95 69.79 -5 7 2 1493.95 68.99 -5 7 2 1574.94 61.19 5 -7 2 1482.75 58.89 5 -7 2 1561.64 68.89 -7 -5 2 1529.35 68.39 5 -7 2 1448.96 64.09 -7 -5 2 1524.55 64.59 -5 7 2 1612.64 60.29 -3 7 -2 1952.8 84.39 3 -7 -2 1758.72 73.49 -7 -3 -2 1995.2 76.79 -3 7 -2 2113.99 76.29 3 -7 -2 2029.2 80.49 -7 -3 -2 2033 75.19 3 -7 -2 1952.6 76.99 -7 -3 -2 1987.9 76.99 -3 7 -2 1845.22 81.49 -3 7 2 2071.39 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1567.54 62.19 7 -3 -2 1506.25 65.39 3 7 -2 1618.34 66.19 -3 -7 -2 1365.26 62.99 -3 -7 2 1445.06 67.09 -7 3 2 1586.64 64.19 -3 -7 2 1548.65 60.79 -7 3 2 1585.64 66.19 7 -3 2 1484.75 63.69 7 -3 2 1537.15 63.99 7 -3 2 1509.05 66.19 3 7 2 1640.84 63.59 -7 5 -2 965 49.4 -7 5 -2 1008.5 50.49 7 -5 -2 981.4 49.7 5 7 -2 945.81 54.19 -5 -7 -2 931.41 46.9 5 7 -2 1015.2 49.9 7 -5 -2 999.8 39.6 -5 -7 -2 979 41.8 7 -5 -2 963.5 47.1 -7 5 -2 1037.1 46.2 5 7 2 1100.59 46.8 -5 -7 2 945.31 51.39 7 -5 2 929.71 43 7 -5 2 1015.4 49.9 7 -5 2 1006.6 49.3 -7 5 2 974.9 45.5 7 -5 2 937.81 50.09 -7 5 2 995.6 52.09 -7 7 -2 86.29 22 7 -7 -2 139.79 21.3 7 7 -2 137.89 28.2 -7 -7 -2 129.59 15.6 -7 7 -2 122.19 23.5 7 -7 -2 200.28 30.6 -7 -7 -2 127.69 20.2 -7 7 2 104.89 25.4 7 -7 2 126.99 22.5 7 -7 2 142.59 23.4 7 -7 2 126.39 18.7 7 7 2 146.49 25.3 7 -7 2 122.89 24.2 -7 -7 2 122.69 19.1 -7 -7 2 137.39 23.2 7 -7 2 93.39 22.9 -8 -6 -2 609.24 37.5 -8 -6 -2 647.64 34.2 6 -8 -2 623.24 41.3 6 -8 -2 638.74 39.1 -6 8 -2 618.94 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105.69 38.7 -4 -15 -3 10.5 16 4 15 -3 2.5 40.6 15 -4 -3 17.3 31.4 -4 -15 -3 32 34.8 4 15 -3 15 35.6 -4 -15 3 -6.4 23.4 15 -4 3 -26.6 36.8 4 15 3 13.5 43.3 0 0 -4 3724.33 135.19 0 0 -4 4043.6 136.49 0 0 4 3826.02 135.39 0 0 4 3553.14 128.79 0 0 4 3596.34 128.99 0 0 4 3775.72 136.59 1 1 -4 3014.7 115.09 -1 1 -4 3393.16 115.89 1 1 -4 3164.98 115.89 1 1 -4 3404.26 110.89 1 -1 -4 3087.29 114.19 -1 1 -4 3196.98 109.39 1 -1 -4 3139.79 113.59 -1 1 -4 3139.59 109.09 -1 1 -4 3161.58 117.39 1 -1 4 3033.3 117.49 1 -1 4 3144.79 114.99 1 1 4 3261.97 116.49 -1 1 4 3120.49 114.29 -1 1 4 3040 108.69 1 -1 4 3172.98 109.79 -1 1 4 3265.37 109.29 1 1 4 3294.57 114.99 -1 1 4 3081.59 109.19 1 1 4 3059.49 107.69 -1 -1 4 3285.47 116.99 -1 -1 4 3061.89 110.99 -1 1 4 2674.13 113.39 -1 -1 4 3157.38 115.89 -1 -1 4 3093.79 109.59 0 2 -4 1908.01 79.39 2 0 -4 1997.3 75.69 -2 0 -4 1999.3 70.49 2 0 -4 2018.2 77.39 0 2 -4 2074.69 73.09 -2 0 -4 2038.3 79.59 0 2 -4 1942.31 77.49 -2 0 -4 1950.01 68.79 0 2 4 1947.51 69.79 0 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