#------------------------------------------------------------------------------ #$Date: 2024-10-03 01:10:38 +0300 (Thu, 03 Oct 2024) $ #$Revision: 294989 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572730.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572730 loop_ _publ_author_name 'Ma, Yu-Juan' 'Xu, Fei' 'Ren, Xin-Ye' 'Chen, Fan-Yao' 'Pan, Jie' 'Li, Jinhua' 'Han, Song-De' 'Wang, Guo-Ming' _publ_section_title ; Photoinduced electron-transfer strategy for switchable fluorescence and phosphorescence in lanthanide-based coordination polymers ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC04632C _journal_year 2024 _chemical_formula_moiety 'C10 H29 La2 Li O35 P10, 2(C12 H11 N4), 3(O H2)' _chemical_formula_sum 'C34 H57 La2 Li N8 O38 P10' _chemical_formula_weight 1780.28 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-05-14 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-05-14 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 68.4420(10) _cell_angle_beta 69.632(2) _cell_angle_gamma 79.1400(10) _cell_formula_units_Z 2 _cell_length_a 12.2018(2) _cell_length_b 16.4476(2) _cell_length_c 16.9585(3) _cell_measurement_reflns_used 22808 _cell_measurement_temperature 293 _cell_measurement_theta_max 30.6900 _cell_measurement_theta_min 1.9620 _cell_volume 2960.26(9) _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2013/2 (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293 _diffrn_measured_fraction_theta_full 0.973 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'multiwire proportional' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0547 _diffrn_reflns_av_unetI/netI 0.0444 _diffrn_reflns_Laue_measured_fraction_full 0.973 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 42386 _diffrn_reflns_point_group_measured_fraction_full 0.973 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.010 _diffrn_reflns_theta_min 1.952 _diffrn_source 'Rotating-anode X-ray tube' _exptl_absorpt_coefficient_mu 1.805 _exptl_absorpt_correction_T_max 0.965 _exptl_absorpt_correction_T_min 0.897 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.110a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.991 _exptl_crystal_description stick _exptl_crystal_F_000 1764 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.648 _refine_diff_density_min -0.613 _refine_diff_density_rms 0.096 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 843 _refine_ls_number_reflns 10440 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.053 _refine_ls_R_factor_all 0.0356 _refine_ls_R_factor_gt 0.0297 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0370P)^2^+1.3612P] where P=(Fo^2^+2Fc^2^)/3 ; _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0757 _refine_ls_wR_factor_ref 0.0785 _reflns_Friedel_coverage 0.000 _reflns_number_gt 9106 _reflns_number_total 10440 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04632c2.cif _cod_data_source_block La _cod_database_code 1572730 _shelxl_version_number 2013-2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: C12(H12), C14(H14), C16(H16A), C17(H17), C18(H18A), C19(H19A), C20(H20), N4(H4A), C22(H22), C24(H24), C26(H26), C28(H28), C29(H29A), C30(H30), C31(H31), C32(H32), C33(H33), C34(H34), N2(H2D), C21(H21), N6(H6D), N8(H8) 2.b Tetrahedral OH refined with riding coordinates: O2(H2), O4(H4), O6(H6), O9(H9), O11(H11), O13(H13), O16(H16), O18(H18), O19(H19), O23(H23), O25(H25), O27(H27), O29(H29), O35(H35) 2.c Idealised Me refined as rotating group: C2(H2A,H2B,H2C), C0AA(H0AA,H0AB,H0AC), C6(H6A,H6B,H6C), C8(H8A,H8B,H8C), C10(H10A,H10B,H10C) ; _shelx_res_file ; TITL 1_a.res in P-1 CELL 0.71073 12.2018 16.4476 16.9585 68.442 69.632 79.14 ZERR 2 0.0002 0.0002 0.0003 0.001 0.002 0.001 LATT 1 SFAC C H Li N O P La UNIT 68 102 2 16 76 20 4 L.S. 20 PLAN 19 CONF FREE La1 Li1 FREE La1 P1 FREE Li1 P9 BOND LIST 4 fmap 2 acta MORE -1 BOND $H OMIT 0 50.02 REM REM REM WGHT 0.037000 1.361200 FVAR 0.26474 LA1 7 0.872343 0.405026 0.115462 11.00000 0.01581 0.01487 = 0.01189 -0.00435 -0.00225 -0.00123 LA2 7 0.593832 0.136889 0.379650 11.00000 0.01534 0.01600 = 0.01650 -0.00566 -0.00169 -0.00412 LI1 3 0.624420 0.502415 0.130117 11.00000 0.02834 0.02281 = 0.03335 -0.00934 -0.00663 -0.00174 C1 1 0.896259 0.663654 0.096560 11.00000 0.01646 0.01683 = 0.01471 -0.00521 -0.00106 -0.00622 C2 1 0.805398 0.675790 0.179854 11.00000 0.02146 0.03341 = 0.02137 -0.01512 -0.00196 -0.00163 AFIX 137 H2A 2 0.844043 0.681569 0.217906 11.00000 -1.50000 H2B 2 0.759066 0.625839 0.210748 11.00000 -1.50000 H2C 2 0.755545 0.727647 0.163656 11.00000 -1.50000 AFIX 0 C3 1 0.732622 0.346500 0.389983 11.00000 0.01875 0.02471 = 0.01657 -0.01025 0.00050 -0.00434 C0AA 1 0.677846 0.312071 0.490127 11.00000 0.02580 0.06250 = 0.01340 -0.01624 0.00098 -0.00072 AFIX 137 H0AA 2 0.736271 0.304805 0.518636 11.00000 -1.50000 H0AB 2 0.646841 0.256621 0.506690 11.00000 -1.50000 H0AC 2 0.615733 0.352982 0.508482 11.00000 -1.50000 AFIX 0 C5 1 0.623706 0.251133 0.121230 11.00000 0.02024 0.02767 = 0.01813 -0.00857 -0.00385 -0.00551 C6 1 0.552191 0.195238 0.105925 11.00000 0.03087 0.03215 = 0.04625 -0.00963 -0.01741 -0.01007 AFIX 137 H6A 2 0.540788 0.140516 0.153898 11.00000 -1.50000 H6B 2 0.593161 0.184365 0.050731 11.00000 -1.50000 H6C 2 0.477446 0.225522 0.103477 11.00000 -1.50000 AFIX 0 C7 1 0.270206 0.035525 0.417978 11.00000 0.01778 0.02008 = 0.02139 -0.00655 -0.00671 -0.00455 C8 1 0.235565 0.104788 0.339504 11.00000 0.03994 0.02855 = 0.02825 -0.00859 -0.01793 -0.00034 AFIX 137 H8A 2 0.232636 0.077328 0.299226 11.00000 -1.50000 H8B 2 0.292423 0.148080 0.308929 11.00000 -1.50000 H8C 2 0.159913 0.132390 0.361145 11.00000 -1.50000 AFIX 0 C9 1 0.329599 0.668325 0.252636 11.00000 0.02102 0.02544 = 0.02560 -0.01165 -0.00588 -0.00394 C10 1 0.296580 0.605161 0.348497 11.00000 0.04439 0.03175 = 0.03422 -0.00920 -0.00006 -0.00786 AFIX 137 H10A 2 0.216314 0.618205 0.378891 11.00000 -1.50000 H10B 2 0.346254 0.611652 0.378692 11.00000 -1.50000 H10C 2 0.306472 0.546030 0.348001 11.00000 -1.50000 AFIX 0 C11 1 0.561265 0.984465 0.000238 11.00000 0.02610 0.02384 = 0.02387 -0.00848 -0.00529 -0.00289 C12 1 0.595245 0.967471 0.075776 11.00000 0.02178 0.03219 = 0.02147 -0.01332 0.00265 -0.00030 AFIX 43 H12 2 0.539172 0.972507 0.127774 11.00000 -1.20000 AFIX 0 C13 1 0.711044 0.943206 0.074859 11.00000 0.03138 0.02360 = 0.02104 -0.00917 -0.00276 -0.00339 C14 1 0.796358 0.934144 -0.001157 11.00000 0.02146 0.03120 = 0.03160 -0.01385 -0.00411 0.00110 AFIX 43 H14 2 0.874451 0.919611 -0.003016 11.00000 -1.20000 AFIX 0 C15 1 0.760803 0.947534 -0.073848 11.00000 0.02579 0.02775 = 0.01774 -0.01122 0.00483 -0.00012 C16 1 0.648272 0.972569 -0.075790 11.00000 0.03016 0.02661 = 0.02010 -0.00885 -0.00371 -0.00008 AFIX 43 H16A 2 0.629198 0.981715 -0.127080 11.00000 -1.20000 AFIX 0 C17 1 0.910535 0.996714 -0.227007 11.00000 0.05054 0.02038 = 0.03226 -0.00464 0.00430 -0.00227 AFIX 43 H17 2 0.892660 1.056937 -0.242587 11.00000 -1.20000 AFIX 0 C18 1 0.998629 0.954396 -0.274264 11.00000 0.03972 0.04847 = 0.03027 -0.01561 0.01088 -0.00799 AFIX 43 H18A 2 1.053379 0.979632 -0.328728 11.00000 -1.20000 AFIX 0 C19 1 0.903616 0.857490 -0.154421 11.00000 0.06472 0.02400 = 0.02315 -0.00406 0.00177 0.00879 AFIX 43 H19A 2 0.880837 0.803882 -0.111450 11.00000 -1.20000 AFIX 0 C20 1 0.843957 0.878944 0.170342 11.00000 0.03599 0.04045 = 0.03989 -0.02345 -0.01314 0.00925 AFIX 43 H20 2 0.898654 0.847181 0.136786 11.00000 -1.20000 AFIX 0 N4 4 0.750186 0.939291 0.272759 11.00000 0.04336 0.02742 = 0.02495 -0.01360 -0.01035 0.00020 AFIX 43 H4A 2 0.731611 0.954120 0.319656 11.00000 -1.20000 AFIX 0 C22 1 0.691803 0.964726 0.214793 11.00000 0.03200 0.02429 = 0.02344 -0.01080 -0.00331 -0.00008 AFIX 43 H22 2 0.623958 1.001918 0.217620 11.00000 -1.20000 AFIX 0 C23 1 0.052484 0.472495 0.483064 11.00000 0.02154 0.03121 = 0.02210 -0.01176 -0.00509 -0.00115 C24 1 0.131211 0.434320 0.530835 11.00000 0.02574 0.03617 = 0.02251 -0.01559 -0.00832 0.00020 AFIX 43 H24 2 0.117689 0.442558 0.584936 11.00000 -1.20000 AFIX 0 C25 1 0.229274 0.384320 0.499605 11.00000 0.02498 0.02917 = 0.02223 -0.00965 -0.01284 -0.00050 C26 1 0.254470 0.369411 0.419899 11.00000 0.02351 0.02683 = 0.02320 -0.01180 -0.00784 -0.00043 AFIX 43 H26 2 0.320646 0.335304 0.399387 11.00000 -1.20000 AFIX 0 C27 1 0.176090 0.407894 0.372605 11.00000 0.02343 0.03038 = 0.01879 -0.01112 -0.00490 -0.00529 C28 1 0.077410 0.458543 0.402072 11.00000 0.01927 0.03380 = 0.02479 -0.01374 -0.00904 0.00315 AFIX 43 H28 2 0.027076 0.483598 0.367663 11.00000 -1.20000 AFIX 0 C29 1 0.336579 0.385578 0.597625 11.00000 0.03051 0.03301 = 0.02804 -0.01645 -0.01292 0.00276 AFIX 43 H29A 2 0.315296 0.443226 0.596583 11.00000 -1.20000 AFIX 0 C30 1 0.414516 0.251324 0.627450 11.00000 0.02416 0.03216 = 0.03282 -0.01243 -0.01433 0.00506 AFIX 43 H30 2 0.456770 0.200693 0.651939 11.00000 -1.20000 AFIX 0 C31 1 0.356112 0.260965 0.570948 11.00000 0.03058 0.02550 = 0.03338 -0.01631 -0.01199 0.00563 AFIX 43 H31 2 0.350043 0.219016 0.548208 11.00000 -1.20000 AFIX 0 C32 1 0.130836 0.369605 0.260536 11.00000 0.02589 0.04527 = 0.02151 -0.01270 -0.00608 -0.01415 AFIX 43 H32 2 0.056721 0.350401 0.295313 11.00000 -1.20000 AFIX 0 C33 1 0.288220 0.407279 0.147730 11.00000 0.03280 0.07689 = 0.02596 -0.02870 0.00655 -0.00919 AFIX 43 H33 2 0.341311 0.417350 0.090880 11.00000 -1.20000 AFIX 0 C34 1 0.301862 0.424172 0.214783 11.00000 0.02617 0.08064 = 0.03416 -0.02916 0.00468 -0.02012 AFIX 43 H34 2 0.365647 0.448326 0.213685 11.00000 -1.20000 AFIX 0 N1 4 0.852423 0.934402 -0.151854 11.00000 0.02392 0.02245 = 0.01864 -0.00727 -0.00041 0.00318 N2 4 0.992041 0.868634 -0.227431 11.00000 0.04592 0.03774 = 0.02870 -0.01608 -0.01190 0.02177 AFIX 43 H2D 2 1.038873 0.827309 -0.243081 11.00000 -1.20000 AFIX 0 N3 4 0.745355 0.928709 0.151337 11.00000 0.02600 0.02605 = 0.02462 -0.01199 -0.00511 -0.00024 C21 1 0.844924 0.885642 0.246780 11.00000 0.04284 0.03854 = 0.04303 -0.02100 -0.02170 0.00809 AFIX 43 H21 2 0.900181 0.858589 0.276480 11.00000 -1.20000 AFIX 0 N5 4 0.306415 0.345750 0.552944 11.00000 0.02502 0.03014 = 0.02188 -0.01370 -0.00965 0.00063 N6 4 0.401512 0.328667 0.643100 11.00000 0.02586 0.04238 = 0.02623 -0.01812 -0.01137 -0.00094 AFIX 43 H6D 2 0.431337 0.338565 0.677516 11.00000 -1.20000 AFIX 0 N7 4 0.201818 0.398513 0.286667 11.00000 0.01854 0.03189 = 0.02012 -0.01344 -0.00323 -0.00168 N8 4 0.181868 0.372409 0.177709 11.00000 0.03083 0.04518 = 0.02560 -0.02026 -0.01086 -0.00241 AFIX 43 H8 2 0.153323 0.355202 0.147188 11.00000 -1.20000 AFIX 0 O1 5 0.918573 0.490867 0.197480 11.00000 0.02542 0.02168 = 0.01969 -0.00144 -0.00593 -0.01021 O2 5 1.077098 0.586153 0.166420 11.00000 0.02454 0.03023 = 0.02128 -0.00907 -0.00674 -0.00859 AFIX 83 H2 2 1.114149 0.627801 0.129193 11.00000 -1.50000 AFIX 0 O3 5 1.055611 0.540514 0.045083 11.00000 0.02989 0.02239 = 0.01596 -0.00828 -0.00854 0.00522 O4 5 0.962779 0.740371 0.050971 11.00000 0.02601 0.02091 = 0.02629 -0.01104 0.00208 -0.00928 AFIX 83 H4 2 1.012659 0.734921 0.005711 11.00000 -1.50000 AFIX 0 O5 5 0.915806 0.657260 -0.065893 11.00000 0.01556 0.02148 = 0.01247 -0.00516 -0.00109 -0.00261 O6 5 0.729262 0.724123 0.009264 11.00000 0.02018 0.02264 = 0.02008 -0.00403 -0.00053 0.00210 AFIX 83 H6 2 0.682640 0.725124 0.057355 11.00000 -1.50000 AFIX 0 O7 5 0.772399 0.559607 0.072513 11.00000 0.01659 0.01750 = 0.01739 -0.00471 -0.00121 -0.00434 O8 5 0.677704 0.409264 0.234431 11.00000 0.01964 0.02768 = 0.01548 -0.00572 -0.00185 -0.00019 O9 5 0.533254 0.444274 0.367681 11.00000 0.02773 0.02380 = 0.02872 -0.01178 0.00214 0.00113 AFIX 83 H9 2 0.567181 0.488847 0.351673 11.00000 -1.50000 AFIX 0 O10 5 0.557250 0.291333 0.363848 11.00000 0.02268 0.02025 = 0.03149 -0.00642 -0.00786 -0.00397 O11 5 0.789482 0.425528 0.369225 11.00000 0.03806 0.03108 = 0.03569 -0.01938 -0.00410 -0.01268 AFIX 83 H11 2 0.819993 0.445660 0.315258 11.00000 -1.50000 AFIX 0 O12 5 0.781395 0.177556 0.387560 11.00000 0.02216 0.01996 = 0.02660 -0.00332 -0.00541 -0.00624 O13 5 0.937890 0.248378 0.402839 11.00000 0.02209 0.03679 = 0.01728 -0.00259 -0.00648 -0.01078 AFIX 83 H13 2 0.908644 0.229657 0.457052 11.00000 -1.50000 AFIX 0 O14 5 0.902930 0.295330 0.258146 11.00000 0.02362 0.02017 = 0.01393 -0.00438 -0.00374 -0.00080 O15 5 0.852040 0.261032 0.108154 11.00000 0.01760 0.02069 = 0.02292 -0.00552 -0.00495 -0.00516 O16 5 0.808302 0.127829 0.085125 11.00000 0.03713 0.02480 = 0.02069 -0.01090 -0.00432 -0.00473 AFIX 83 H16 2 0.824629 0.155228 0.031672 11.00000 -1.50000 AFIX 0 O17 5 0.735567 0.139372 0.235533 11.00000 0.02660 0.02715 = 0.01688 -0.00260 -0.00315 -0.00784 O18 5 0.554771 0.266556 0.204514 11.00000 0.02686 0.03866 = 0.02634 -0.01417 0.00527 -0.00746 AFIX 83 H18 2 0.590302 0.296703 0.215429 11.00000 -1.50000 AFIX 0 O19 5 0.535440 0.393952 0.009330 11.00000 0.02612 0.03630 = 0.03224 -0.01412 -0.01276 0.00124 AFIX 83 H19 2 0.511303 0.358020 -0.002630 11.00000 -1.50000 AFIX 0 O20 5 0.685358 0.415331 0.068422 11.00000 0.02588 0.02275 = 0.02392 -0.01013 -0.01129 0.00017 O21 5 0.743398 0.337871 -0.049215 11.00000 0.02071 0.03050 = 0.01988 -0.01043 -0.00223 -0.00512 O22 5 0.505524 0.039783 0.339644 11.00000 0.02194 0.02698 = 0.03142 -0.01794 0.00208 -0.00778 O23 5 0.404725 -0.054252 0.305232 11.00000 0.03612 0.03043 = 0.02474 -0.01326 -0.00802 -0.00936 AFIX 83 H23 2 0.347797 -0.083330 0.323873 11.00000 -1.50000 AFIX 0 O24 5 0.424347 -0.100004 0.460919 11.00000 0.02841 0.02598 = 0.02059 -0.00790 -0.00569 0.00345 O25 5 0.178665 -0.025779 0.464645 11.00000 0.01987 0.02781 = 0.03249 -0.00726 -0.00931 -0.01081 AFIX 83 H25 2 0.194935 -0.063708 0.507241 11.00000 -1.50000 AFIX 0 O26 5 0.287218 0.010363 0.579225 11.00000 0.04096 0.02161 = 0.01797 -0.00766 -0.00818 0.00084 O27 5 0.166849 0.146745 0.516912 11.00000 0.01673 0.02947 = 0.05052 -0.02273 -0.00380 0.00174 AFIX 83 H27 2 0.109328 0.117603 0.541623 11.00000 -1.50000 AFIX 0 O28 5 0.379079 0.143659 0.451434 11.00000 0.01991 0.02581 = 0.02694 -0.01527 -0.00072 -0.00544 O29 5 0.250014 0.659527 0.211831 11.00000 0.01653 0.07238 = 0.05892 -0.04689 -0.00992 0.00225 AFIX 83 H29 2 0.182839 0.671856 0.239465 11.00000 -1.50000 AFIX 0 O30 5 0.480925 0.574523 0.148385 11.00000 0.02374 0.03170 = 0.03085 -0.01650 -0.00966 -0.00070 O31 5 0.547191 0.602037 0.259715 11.00000 0.03246 0.02432 = 0.03471 -0.01257 -0.01823 0.00215 O32 5 0.530311 0.727246 0.120647 11.00000 0.02650 0.02441 = 0.02950 -0.00432 0.00219 -0.00107 O34 5 0.383569 0.799575 0.295470 11.00000 0.04047 0.03296 = 0.05379 -0.02420 -0.02150 0.00049 O35 5 0.341179 0.836708 0.149960 11.00000 0.04548 0.03350 = 0.03680 -0.00241 -0.01549 0.00294 AFIX 83 H35 2 0.297483 0.827270 0.127360 11.00000 -1.50000 AFIX 0 O36 5 0.175816 0.802881 0.292883 11.00000 0.02943 0.03685 = 0.03952 -0.02124 -0.00753 0.00677 O37 5 0.007436 0.714620 0.272394 11.00000 0.04481 0.10170 = 0.16176 -0.08499 -0.03783 0.01918 O38 5 0.069709 0.859804 0.434198 11.00000 0.02430 0.03573 = 0.02810 -0.00915 -0.00660 -0.00639 O39 5 0.858892 0.158088 0.914973 11.00000 0.06645 0.06887 = 0.03349 -0.01826 -0.01850 0.00625 P1 6 0.991870 0.564242 0.128043 11.00000 0.01708 0.01840 = 0.01259 -0.00543 -0.00289 -0.00439 P2 6 0.824374 0.647430 0.024876 11.00000 0.01463 0.01471 = 0.01403 -0.00453 -0.00181 -0.00204 P3 6 0.620588 0.373119 0.333961 11.00000 0.01608 0.01634 = 0.01529 -0.00617 -0.00081 -0.00165 P4 6 0.840887 0.261231 0.356485 11.00000 0.01580 0.01968 = 0.01274 -0.00442 -0.00291 -0.00390 P5 6 0.653757 0.356439 0.030187 11.00000 0.01792 0.02047 = 0.01823 -0.00704 -0.00577 -0.00242 P6 6 0.763442 0.193626 0.139030 11.00000 0.01966 0.01760 = 0.01383 -0.00532 -0.00247 -0.00512 P7 6 0.411563 -0.024481 0.381034 11.00000 0.01911 0.01983 = 0.01511 -0.00874 -0.00237 -0.00440 P8 6 0.280571 0.084842 0.495769 11.00000 0.01561 0.01782 = 0.01968 -0.00903 -0.00387 -0.00102 P9 6 0.482061 0.641912 0.190838 11.00000 0.01869 0.02132 = 0.02226 -0.00881 -0.00609 -0.00074 P10 6 0.304284 0.782231 0.254179 11.00000 0.02571 0.02215 = 0.03011 -0.01228 -0.00925 0.00136 HKLF 4 REM 1_a.res in P-1 REM R1 = 0.0297 for 9106 Fo > 4sig(Fo) and 0.0356 for all 10440 data REM 843 parameters refined using 0 restraints END WGHT 0.0333 1.4962 REM Highest difference peak 0.648, deepest hole -0.613, 1-sigma level 0.096 Q1 1 0.1039 0.9155 0.4211 11.00000 0.05 0.65 Q2 1 0.7763 0.1638 0.9077 11.00000 0.05 0.60 Q3 1 0.1137 0.8354 0.3882 11.00000 0.05 0.55 Q4 1 0.5316 0.4052 -0.0489 11.00000 0.05 0.54 Q5 1 0.2917 0.6535 0.1504 11.00000 0.05 0.47 Q6 1 0.5324 0.5289 0.1181 11.00000 0.05 0.46 Q7 1 0.0569 0.6578 0.2701 11.00000 0.05 0.46 Q8 1 0.7791 0.3025 0.3786 11.00000 0.05 0.44 Q9 1 0.2798 0.0536 0.4530 11.00000 0.05 0.44 Q10 1 0.5304 0.4949 0.3174 11.00000 0.05 0.44 Q11 1 0.0547 0.7251 0.3058 11.00000 0.05 0.44 Q12 1 0.2910 0.3490 0.1816 11.00000 0.05 0.43 Q13 1 0.9453 0.6216 0.1210 11.00000 0.05 0.42 Q14 1 0.3941 0.8316 0.2171 11.00000 0.05 0.42 Q15 1 0.4062 -0.0820 0.5069 11.00000 0.05 0.40 Q16 1 0.7844 0.1540 0.3647 11.00000 0.05 0.40 Q17 1 0.8231 0.1987 0.9342 11.00000 0.05 0.39 Q18 1 0.8852 0.2455 0.1388 11.00000 0.05 0.39 Q19 1 0.4381 0.8253 0.1220 11.00000 0.05 0.38 ; _shelx_res_checksum 55840 _shelx_hkl_file ; 0 0 -2 42.81 3.47 0 0 2 40.71 3.18 0 0 2 41.71 4.89 0 0 2 45.23 5.32 0 0 -2 41.81 5.18 0 0 3 1.14 0.86 0 0 -3 4.47 2.47 0 0 3 6.79 2.47 0 0 4 3856.99 154.97 0 0 4 3409.31 155.45 0 0 -4 3644.72 163.95 0 0 4 3542.67 161.72 0 0 -4 3456.92 153.74 0 0 5 19.38 2.76 0 0 5 18.24 5.04 0 0 -5 19.38 5.56 0 0 5 12.45 2.61 0 0 6 115.59 8.41 0 0 -6 117.11 14.54 0 0 6 128.84 14.02 0 0 6 119.25 9.26 0 0 7 260.73 15.39 0 0 -7 262.30 24.28 0 0 7 242.15 21.81 0 0 7 238.54 15.92 0 0 8 3858.22 169.18 0 0 8 4041.23 182.62 0 0 -8 3849.48 185.71 0 0 8 3710.76 170.32 0 0 9 53.92 6.84 0 0 -9 53.73 7.22 0 0 9 44.85 10.78 0 0 -9 67.32 15.44 0 0 9 51.83 6.27 0 0 -10 14.11 7.93 0 0 10 5.84 7.13 0 0 10 22.23 4.56 0 0 -10 11.40 3.61 0 0 -11 22.71 10.45 0 0 -11 13.78 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2795.98 115.87 0 -1 -5 2598.20 115.83 0 1 5 2512.02 115.07 0 -1 -5 2463.13 114.07 0 -1 -5 2655.64 123.38 0 -1 -5 2721.91 122.14 0 1 6 801.71 38.96 0 1 6 764.18 38.39 0 -1 -6 751.87 37.01 0 -1 -6 812.11 47.22 0 -1 -6 815.30 46.32 0 1 7 1385.92 64.80 0 1 7 1308.91 64.14 0 -1 -7 1372.10 62.57 0 -1 -7 1368.77 75.35 0 -1 -7 1401.69 74.26 0 1 8 139.96 11.54 0 1 8 168.09 18.67 0 -1 -8 125.99 16.91 0 1 8 128.94 10.83 0 1 9 1414.09 69.03 0 1 9 1475.43 82.43 0 -1 -9 1389.82 81.43 0 1 9 1436.76 68.79 0 1 10 0.95 1.76 0 1 10 0.90 1.85 0 -1 -10 -2.61 4.80 0 1 10 2.66 4.85 0 1 11 126.09 11.92 0 1 11 135.16 20.52 0 -1 -11 120.24 21.57 0 -1 -12 168.51 26.79 0 1 12 151.08 23.37 0 -1 -12 186.47 16.58 0 1 12 189.94 15.49 0 -1 -13 2121.17 118.39 0 1 13 1830.51 90.31 0 1 13 2124.59 113.88 0 1 13 1766.61 89.65 0 -1 -14 115.83 22.42 0 1 14 127.18 12.97 0 1 14 108.94 21.19 0 1 14 96.20 11.40 0 -1 -15 13.25 10.74 0 1 15 17.20 5.04 0 1 15 8.03 7.41 0 1 15 21.38 5.08 0 -1 -16 13.49 9.22 0 1 16 1.43 4.28 0 1 16 12.78 10.36 0 1 16 2.99 2.76 0 -1 -17 226.19 33.92 0 1 17 255.74 21.81 0 -1 -18 4.80 8.84 0 1 18 12.64 5.46 0 -1 -19 144.19 27.51 0 1 19 156.83 17.20 0 -1 -20 -5.65 8.98 0 -1 -21 171.41 33.73 0 2 -19 -7.22 13.25 0 -2 19 11.45 5.80 0 2 -18 13.11 14.73 0 -2 18 -1.57 5.13 0 2 -17 87.56 23.66 0 -2 17 92.50 12.35 0 2 -16 218.16 34.92 0 -2 16 236.83 20.24 0 2 -15 14.78 11.07 0 -2 15 16.91 5.37 0 -2 14 325.43 38.77 0 2 -14 263.10 36.53 0 -2 14 313.03 22.80 0 -2 13 12.45 8.50 0 2 -13 -4.37 8.98 0 -2 13 12.40 4.37 0 -2 12 202.20 28.93 0 2 -12 169.46 26.89 0 -2 12 151.03 13.87 0 2 -11 23.52 11.40 0 -2 11 19.10 4.70 0 -2 11 24.61 10.59 0 2 -10 179.63 26.37 0 -2 10 176.87 13.78 0 2 -10 149.18 13.97 0 -2 10 184.90 23.61 0 2 -9 103.19 19.48 0 2 -9 107.27 10.69 0 -2 9 112.69 10.17 0 -2 9 108.32 17.67 0 2 -8 43.99 12.35 0 2 -8 36.25 5.61 0 -2 8 40.71 5.56 0 -2 8 50.31 11.45 0 2 -7 2.85 5.27 0 -2 7 9.26 6.70 0 2 -7 2.14 1.62 0 -2 7 3.71 1.81 0 2 -6 1750.74 83.38 0 -2 6 1861.96 82.86 0 -2 6 1809.32 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48.41 0 -9 10 532.10 36.82 0 -9 9 71.22 7.51 0 -9 9 38.34 11.31 0 -9 9 79.05 22.85 0 -9 9 53.73 15.87 0 -9 9 72.55 11.26 0 -9 8 -0.62 2.04 0 -9 8 -2.61 4.13 0 -9 8 -5.08 12.30 0 -9 8 -3.90 5.04 0 -9 8 -1.47 3.04 0 -9 7 48.70 11.31 0 -9 7 30.26 6.56 0 -9 7 44.28 5.13 0 -9 6 166.66 28.84 0 -9 6 173.69 20.62 0 -9 6 191.51 11.45 0 -9 6 148.89 14.11 0 9 -5 21.66 5.94 0 -9 5 18.67 6.70 0 -9 5 26.32 13.40 0 -9 5 37.15 5.08 0 -9 5 27.41 5.08 0 -9 5 29.84 3.56 0 9 -4 147.04 17.29 0 -9 4 172.74 9.64 0 -9 4 215.36 20.52 0 -9 4 161.20 26.18 0 9 -4 184.43 17.77 0 -9 4 155.02 12.59 0 -9 4 214.83 32.40 0 -9 4 164.76 11.97 0 9 -3 6.41 4.42 0 -9 3 1.71 2.23 0 -9 3 3.28 1.38 0 9 -3 4.18 3.85 0 -9 3 7.60 1.28 0 -9 3 1.71 3.14 0 -9 2 749.40 44.85 0 -9 2 746.60 40.14 0 -9 2 733.30 34.92 0 9 -2 677.38 48.55 0 -9 1 1.09 2.00 0 -9 1 2.76 3.33 0 -9 1 1.66 1.14 0 -9 0 198.92 17.29 0 -9 0 203.05 25.75 0 9 0 240.82 21.66 0 -9 0 237.40 18.91 0 -9 0 216.59 12.59 0 9 0 228.66 18.53 0 9 1 330.95 23.09 0 9 1 308.57 26.08 0 -9 -1 287.28 29.98 0 -9 -1 334.27 23.75 0 9 2 1819.44 96.59 0 9 2 1887.95 91.26 0 9 2 1890.51 86.70 0 -9 -2 1766.42 102.52 0 -9 -2 1951.61 93.54 0 9 3 100.67 6.37 0 9 3 102.48 11.64 0 9 3 114.07 10.36 0 9 3 104.90 8.31 0 -9 -3 104.90 17.72 0 -9 -3 88.84 11.54 0 -9 -4 134.83 14.54 0 9 4 148.51 12.83 0 9 4 117.11 7.93 0 -9 -5 724.32 43.23 0 9 5 707.69 34.11 0 9 5 689.30 40.52 0 -9 -6 815.58 47.41 0 9 6 792.49 38.77 0 9 6 762.89 50.36 0 9 6 802.47 45.85 0 9 7 151.27 11.07 0 9 7 167.56 19.10 0 9 7 135.35 15.30 0 9 8 316.79 20.24 0 -9 -8 343.25 21.62 0 9 8 384.58 31.26 0 -9 -8 372.33 25.80 0 9 8 345.77 26.98 0 9 9 166.47 12.87 0 -9 -9 161.24 13.59 0 9 9 157.92 17.86 0 -9 -9 144.81 16.01 0 9 9 159.49 19.43 0 9 10 68.89 13.06 0 9 10 62.38 7.79 0 -9 -10 73.02 9.12 0 -9 -10 80.91 11.83 0 -9 -10 81.43 12.68 0 9 10 81.95 13.49 0 9 11 49.88 11.59 0 9 11 39.24 6.46 0 -9 -11 31.97 7.60 0 -9 -11 53.07 10.74 0 9 11 49.31 10.83 0 9 12 44.28 11.64 0 9 12 50.31 7.41 0 -9 -12 46.51 9.17 0 -9 -12 50.07 11.21 0 9 12 34.11 9.17 0 9 13 46.23 12.59 0 9 13 63.90 9.07 0 -9 -13 75.35 11.50 0 -9 -13 91.22 15.54 0 9 13 81.71 14.82 0 9 14 317.26 32.12 0 9 14 333.89 23.75 0 -9 -14 329.47 27.08 0 9 14 331.09 32.50 0 -9 -14 275.17 30.26 0 -9 -14 361.35 30.07 0 9 15 47.18 13.30 0 9 15 27.79 6.41 0 -9 -15 27.70 9.45 0 -9 -15 31.97 9.69 0 -9 -15 23.80 7.03 0 9 16 84.99 11.50 0 -9 -16 92.97 15.58 0 -9 -16 131.08 21.05 0 9 17 6.03 4.37 0 -9 -17 12.92 7.51 0 -9 -17 3.61 5.70 0 9 18 40.00 8.12 0 -9 -18 16.25 8.69 0 9 19 9.69 7.27 0 -9 -19 3.37 6.18 0 9 19 5.08 4.09 0 -9 -20 34.73 12.02 0 -10 14 21.09 10.26 0 -10 13 296.88 44.14 0 -10 13 259.49 31.88 0 -10 12 3.33 6.08 0 -10 12 -6.18 15.01 0 -10 12 7.51 3.66 0 -10 11 6.03 14.63 0 -10 11 15.87 8.27 0 -10 11 14.92 5.70 0 -10 11 19.81 7.32 0 -10 11 12.78 3.80 0 -10 10 3.04 4.85 0 -10 10 3.56 4.32 0 -10 10 3.04 2.23 0 -10 9 181.06 13.02 0 -10 9 134.45 25.04 0 -10 9 182.05 18.29 0 -10 9 185.14 33.40 0 -10 9 177.06 23.52 0 -10 8 160.34 11.07 0 -10 8 120.72 19.15 0 -10 8 108.22 26.03 0 -10 8 134.97 23.61 0 -10 8 128.04 14.44 0 -10 7 5.13 5.80 0 -10 7 -5.18 11.69 0 -10 7 6.51 2.14 0 -10 7 8.17 3.99 0 -10 6 37.06 6.32 0 -10 6 40.29 4.37 0 -10 6 49.69 16.53 0 -10 6 23.99 8.41 0 -10 5 838.91 54.25 0 -10 5 866.27 70.41 0 10 -5 780.33 48.65 0 -10 5 872.54 42.71 0 -10 5 851.88 39.00 0 -10 5 802.18 42.38 0 10 -4 34.82 8.36 0 -10 4 42.76 4.89 0 -10 4 45.99 6.65 0 -10 4 45.89 3.71 0 10 -4 26.70 8.22 0 -10 4 40.38 9.79 0 10 -3 118.63 15.68 0 -10 3 136.92 16.49 0 -10 3 153.60 13.06 0 10 -3 147.80 19.15 0 -10 3 150.27 9.74 0 10 -2 151.32 18.10 0 -10 2 173.03 18.20 0 -10 2 172.31 15.01 0 -10 2 192.89 10.59 0 10 -2 173.79 22.38 0 -10 1 69.08 9.26 0 -10 1 64.75 16.58 0 -10 1 50.83 4.47 0 -10 1 64.42 9.98 0 -10 0 325.29 34.06 0 -10 0 321.78 23.14 0 10 0 313.03 27.17 0 10 0 297.12 23.18 0 -10 -1 107.27 12.54 0 -10 -1 95.06 17.48 0 10 1 134.21 16.53 0 10 1 117.92 13.06 0 -10 -2 236.88 19.48 0 -10 -2 209.56 25.18 0 10 2 195.31 21.09 0 10 2 182.91 17.01 0 10 3 1275.80 67.98 0 10 3 1264.25 74.11 0 -10 -3 1307.11 69.65 0 -10 -3 1397.18 82.24 0 10 3 1330.34 64.18 0 10 3 1334.23 60.62 0 10 3 1302.54 58.20 0 -10 -4 12.45 4.99 0 10 4 18.58 2.61 0 10 4 27.65 6.75 0 10 4 13.59 3.28 0 10 4 21.47 4.85 0 -10 -5 1006.47 57.06 0 10 5 992.93 46.94 0 10 5 1040.82 54.11 0 -10 -6 97.54 12.83 0 10 6 90.27 7.51 0 10 6 73.83 13.25 0 10 6 102.86 12.45 0 -10 -7 1426.83 77.68 0 10 7 1450.01 83.00 0 10 7 1476.38 76.77 0 10 7 1476.76 68.27 0 10 8 230.37 15.49 0 10 8 227.19 24.42 0 10 8 256.17 22.33 0 10 9 682.32 36.39 0 10 9 745.93 45.89 0 -10 -9 703.60 42.76 0 10 9 621.27 47.37 0 -10 -10 174.21 18.43 0 10 10 168.47 13.59 0 -10 -10 170.18 18.39 0 10 10 168.42 19.67 0 10 10 160.10 21.24 0 -10 -11 422.54 32.12 0 10 11 448.91 26.70 0 10 11 467.58 36.25 0 -10 -11 420.97 33.30 0 10 11 382.40 35.92 0 10 12 86.89 16.01 0 10 12 80.24 9.55 0 -10 -12 77.82 12.59 0 -10 -12 77.53 13.59 0 10 12 69.55 13.30 0 10 13 61.33 14.35 0 10 13 55.40 8.12 0 -10 -13 56.77 10.83 0 -10 -13 53.92 11.92 0 10 13 45.70 11.54 0 10 14 197.02 24.94 0 10 14 168.89 15.44 0 -10 -14 149.37 18.01 0 -10 -14 154.74 21.43 0 10 14 170.56 23.14 0 -10 -15 89.36 14.73 0 10 15 100.86 19.24 0 10 15 117.01 12.87 0 -10 -15 111.41 15.06 0 -10 -15 71.22 15.30 0 10 15 114.45 18.91 0 10 16 19.57 9.98 0 -10 -16 22.85 8.41 0 -10 -16 25.94 10.78 0 10 16 15.49 5.37 0 -10 -16 22.04 7.84 0 -10 -17 338.74 31.97 0 10 17 389.14 27.98 0 -10 -17 384.20 38.91 0 10 18 104.85 13.63 0 -10 -18 102.10 17.20 0 10 19 18.53 6.79 0 10 19 24.09 10.50 0 -10 -19 18.91 8.69 0 -11 14 3.61 6.65 0 -11 13 42.28 13.44 0 -11 12 175.59 34.11 0 -11 12 181.77 25.56 0 -11 11 53.02 13.73 0 -11 11 44.52 21.90 0 -11 11 46.04 6.65 0 -11 10 8.12 4.75 0 -11 10 12.73 7.17 0 -11 10 12.30 12.64 0 -11 10 13.21 3.61 0 -11 9 4.32 3.94 0 -11 9 8.50 3.52 0 -11 9 2.57 1.85 0 -11 9 -3.04 6.22 0 -11 8 376.93 20.62 0 -11 8 363.25 34.54 0 -11 8 345.34 46.46 0 -11 8 255.22 35.92 0 -11 8 364.87 25.42 0 -11 7 31.88 6.46 0 -11 7 33.30 14.44 0 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650.73 33.21 0 11 4 634.10 29.88 0 -11 -5 154.83 17.34 0 11 5 184.81 10.97 0 11 5 177.16 17.96 0 11 5 151.55 15.01 0 11 5 168.99 14.02 0 -11 -6 1520.28 81.95 0 11 6 1561.47 70.93 0 11 6 1540.99 79.15 0 -11 -7 5.32 4.61 0 11 7 2.33 1.71 0 11 7 12.64 7.32 0 11 7 6.22 4.70 0 -11 -8 512.95 35.92 0 11 8 496.70 40.43 0 11 8 500.60 35.11 0 11 8 492.57 27.36 0 11 9 -5.42 7.41 0 -11 -9 -1.57 2.85 0 11 9 -1.90 4.28 0 11 9 5.32 2.52 0 11 10 367.91 22.99 0 11 10 365.20 30.74 0 -11 -10 384.96 29.27 0 11 10 352.23 34.16 0 11 11 104.47 17.77 0 11 11 109.27 10.93 0 -11 -11 123.71 15.54 0 -11 -11 147.85 17.48 0 11 11 114.97 16.53 0 11 12 102.14 18.20 0 11 12 126.85 12.26 0 -11 -12 134.40 16.68 0 -11 -12 128.75 17.44 0 11 12 120.24 18.01 0 -11 -13 221.34 22.42 0 11 13 238.30 18.58 0 -11 -13 207.99 24.23 0 11 13 255.31 27.27 0 11 13 230.99 27.60 0 -11 -14 452.09 35.20 0 11 14 462.21 30.26 0 11 14 506.44 42.05 0 -11 -14 453.71 38.72 0 11 14 520.98 44.61 0 -11 -15 5.99 4.85 0 11 15 -3.37 6.18 0 11 15 1.28 3.61 0 -11 -15 8.31 5.37 0 -11 -15 5.75 5.89 0 11 15 3.14 4.99 0 11 16 347.10 37.53 0 -11 -16 359.12 30.50 0 -11 -16 340.16 34.87 0 11 16 331.99 25.46 0 -11 -16 387.96 31.88 0 -11 -17 37.20 13.21 0 11 17 31.31 7.32 0 -11 -17 20.10 8.03 0 -11 -18 219.54 30.69 0 11 18 308.33 24.28 0 -11 -18 295.84 28.46 0 11 19 159.06 17.34 0 -12 13 54.49 14.73 0 -12 12 3.56 5.61 0 -12 11 632.48 52.35 0 -12 11 591.15 66.08 0 -12 10 -6.46 17.82 0 -12 10 33.21 11.40 0 -12 9 22.42 4.04 0 -12 9 18.77 14.11 0 -12 9 9.50 7.74 0 -12 8 24.23 5.56 0 -12 8 30.41 14.78 0 -12 8 15.06 7.89 0 -12 8 35.44 5.89 0 -12 8 22.71 3.85 0 -12 7 249.52 27.70 0 -12 7 211.56 36.30 0 -12 7 225.71 32.12 0 -12 7 239.49 15.96 0 -12 7 229.66 13.49 0 -12 7 220.92 16.49 0 -12 6 10.55 6.84 0 -12 6 5.56 2.57 0 -12 6 3.75 2.00 0 -12 6 3.04 2.09 0 12 -5 41.00 9.60 0 -12 5 38.96 10.59 0 -12 5 37.53 4.09 0 -12 5 29.55 3.71 0 12 -4 2.47 5.04 0 -12 4 5.99 3.18 0 -12 4 2.23 4.09 0 12 -4 -2.19 5.99 0 -12 3 1433.91 72.07 0 12 -3 1450.49 81.86 0 12 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24.51 0 12 9 473.09 33.73 0 12 10 6.03 6.18 0 12 10 8.50 5.51 0 -12 -10 6.98 3.94 0 12 10 12.59 3.56 0 -12 -11 468.01 37.20 0 12 11 522.88 30.74 0 12 11 567.54 41.29 0 -12 -11 536.37 38.29 0 12 11 630.77 48.32 0 12 12 22.52 9.83 0 12 12 20.14 8.36 0 -12 -12 14.73 6.46 0 -12 -12 19.43 6.94 0 12 12 22.47 4.94 0 -12 -13 429.38 34.02 0 12 13 420.07 27.36 0 -12 -13 425.96 35.44 0 12 13 431.57 37.53 0 12 13 402.54 39.76 0 12 14 148.04 23.71 0 12 14 114.97 18.86 0 -12 -14 134.83 18.01 0 -12 -14 161.20 20.76 0 12 14 132.12 13.73 0 -12 -15 687.54 46.84 0 12 15 655.19 55.06 0 12 15 797.72 55.97 0 -12 -15 725.50 51.83 0 12 15 633.43 39.76 0 -12 -16 -2.00 5.23 0 -12 -16 6.03 6.79 0 12 16 1.38 2.85 0 -12 -16 2.23 5.04 0 -12 -17 257.78 25.46 0 -12 -17 277.64 31.64 0 12 17 217.35 20.52 0 -12 -17 273.36 26.51 0 -12 -18 46.42 10.50 0 12 18 62.81 10.36 0 -12 -18 52.31 14.16 0 12 19 564.74 37.86 0 -13 13 3.75 6.84 0 -13 12 270.66 33.87 0 -13 11 28.46 11.40 0 -13 10 326.38 36.01 0 -13 10 351.80 49.36 0 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25.94 6.08 0 13 5 25.65 3.28 0 -13 -5 19.76 8.60 0 -13 -5 15.06 6.08 0 13 6 1382.98 76.87 0 13 6 1367.11 73.21 0 13 6 1401.31 70.22 0 13 6 1449.11 65.37 0 -13 -6 1420.70 77.96 0 -13 -6 1437.04 89.60 0 -13 -7 8.03 5.51 0 13 7 6.27 2.38 0 13 7 8.93 3.71 0 13 7 4.75 3.56 0 -13 -8 130.70 17.25 0 13 8 165.00 12.02 0 13 8 147.04 22.09 0 13 8 173.17 18.34 0 -13 -9 2.09 4.32 0 13 9 -3.14 5.75 0 13 9 -1.95 3.56 0 13 9 0.76 2.19 0 13 10 443.07 41.38 0 -13 -10 426.34 32.54 0 13 10 530.91 37.67 0 13 10 455.42 26.84 0 13 11 123.19 21.09 0 13 11 158.63 13.44 0 -13 -11 160.82 18.72 0 13 11 174.59 20.57 0 13 12 3.42 9.98 0 13 12 14.16 4.28 0 -13 -12 24.42 8.17 0 -13 -12 19.29 7.13 0 13 12 15.20 7.74 0 13 13 3.52 5.61 0 13 13 3.28 2.85 0 -13 -13 -2.28 3.61 0 -13 -13 2.33 3.71 0 13 13 2.76 5.61 0 -13 -14 601.89 43.38 0 13 14 575.57 35.39 0 13 14 657.00 49.03 0 -13 -14 570.82 44.23 0 13 14 562.45 50.83 0 -13 -15 13.59 7.89 0 13 15 10.26 4.42 0 -13 -15 11.69 6.46 0 -13 -16 280.49 25.94 0 -13 -16 249.90 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874.92 50.69 0 -14 -3 772.02 62.95 0 -14 -3 787.84 49.98 0 -14 -4 -1.90 4.28 0 14 4 -6.18 8.03 0 14 4 6.98 3.90 0 14 5 25.27 7.65 0 14 5 15.63 8.65 0 14 5 16.63 3.56 0 -14 -5 21.85 7.55 0 -14 -5 13.78 8.98 0 14 5 18.48 5.13 0 14 5 20.19 2.90 0 14 6 1.90 3.94 0 14 6 6.37 5.84 0 14 6 1.90 2.52 0 14 6 4.23 3.42 0 14 6 6.18 2.14 0 -14 -6 6.13 4.56 0 -14 -6 3.37 5.37 0 14 7 796.77 51.55 0 14 7 812.73 48.70 0 14 7 768.55 45.18 0 14 7 844.13 40.14 0 -14 -7 807.50 52.16 0 -14 -7 767.69 60.10 0 -14 -8 4.28 4.42 0 -14 -8 -3.56 12.30 0 14 8 6.51 2.47 0 14 8 7.27 4.04 0 14 8 12.40 5.89 0 -14 -9 13.21 7.55 0 14 9 11.07 3.33 0 14 9 3.37 8.79 0 14 9 8.46 4.89 0 14 9 3.90 4.04 0 -14 -10 13.49 8.03 0 14 10 13.83 8.98 0 14 10 10.69 5.89 0 14 10 8.27 3.04 0 14 11 514.99 47.41 0 -14 -11 545.30 38.77 0 14 11 541.27 41.43 0 14 11 576.56 32.07 0 14 12 43.80 13.63 0 14 12 61.14 8.27 0 -14 -12 68.08 12.59 0 14 12 48.08 12.07 0 14 13 3.75 9.12 0 -14 -13 -2.38 3.80 0 14 13 10.93 4.13 0 -14 -13 2.33 4.23 0 14 13 5.46 5.04 0 -14 -14 7.27 5.89 0 14 14 1.19 3.75 0 -14 -14 -2.47 6.03 0 14 14 2.95 5.42 0 -14 -15 259.30 27.79 0 14 15 265.95 20.71 0 -14 -15 235.98 25.94 0 -14 -16 51.40 12.59 0 14 16 65.37 9.64 0 -14 -16 64.66 13.16 0 -14 -17 242.63 23.71 0 -14 -17 263.86 27.36 0 -14 -17 271.89 30.26 0 14 17 246.71 21.28 0 -14 -18 6.51 6.70 0 14 18 16.96 6.18 0 14 19 27.70 8.65 0 -15 9 3.42 6.32 0 -15 8 195.69 26.37 0 -15 7 12.26 8.46 0 -15 6 28.70 10.26 0 -15 5 7.98 5.99 0 15 -5 2.42 4.47 0 15 -4 197.73 24.94 0 -15 4 209.99 24.23 0 -15 4 235.12 38.62 0 15 -4 184.71 24.99 0 -15 3 29.36 6.79 0 15 -3 50.83 13.21 0 -15 3 13.73 7.08 0 -15 3 41.76 17.34 0 15 -3 47.13 13.87 0 -15 2 24.75 6.60 0 15 -2 27.94 9.88 0 -15 2 11.50 12.92 0 15 -2 7.65 9.31 0 -15 1 17.25 5.80 0 15 -1 18.91 8.74 0 -15 1 24.61 15.96 0 15 -1 21.05 10.26 0 -15 0 627.68 40.43 0 15 0 544.50 47.41 0 -15 -1 31.93 14.68 0 -15 -1 15.82 6.32 0 15 1 28.79 10.21 0 -15 -2 7.36 4.80 0 -15 -2 4.85 6.32 0 15 2 7.17 4.66 0 -15 -3 9.64 5.32 0 15 3 10.88 5.80 0 -15 -4 594.14 41.14 0 -15 -4 595.47 53.78 0 15 4 589.44 40.10 0 15 5 13.54 9.36 0 15 5 17.15 2.71 0 -15 -5 11.26 7.74 0 -15 -5 18.67 6.60 0 15 5 15.30 2.76 0 15 5 7.55 5.51 0 15 6 150.13 17.91 0 15 6 154.50 23.47 0 15 6 148.56 12.30 0 15 6 143.57 15.06 0 15 6 136.63 9.50 0 -15 -6 149.27 23.14 0 -15 -6 109.22 16.44 0 15 7 73.16 17.06 0 15 7 77.77 13.35 0 15 7 89.22 12.54 0 15 7 89.36 10.93 0 15 7 99.29 8.08 0 -15 -7 89.98 14.73 0 -15 -7 62.43 15.39 0 15 8 687.07 47.46 0 15 8 617.18 43.00 0 15 8 705.41 41.71 0 15 8 700.89 35.68 0 -15 -8 726.93 48.13 0 -15 -8 713.10 56.01 0 -15 -9 -3.56 9.79 0 -15 -9 2.33 5.18 0 15 9 1.47 2.42 0 15 9 -1.62 4.23 0 15 9 -1.95 5.08 0 -15 -10 99.67 16.06 0 -15 -10 99.53 20.00 0 15 10 84.95 18.72 0 15 10 99.15 14.11 0 15 10 87.56 14.30 0 15 10 99.06 9.64 0 15 11 26.46 10.97 0 15 11 16.30 4.32 0 15 11 12.64 6.18 0 15 11 27.94 8.84 0 -15 -11 31.50 8.50 0 15 12 183.76 14.97 0 -15 -12 146.42 19.19 0 15 12 199.58 23.42 0 15 12 157.49 20.43 0 15 13 86.42 10.36 0 -15 -13 87.32 15.01 0 15 13 84.66 16.06 0 -15 -13 72.69 13.68 0 15 14 14.02 4.99 0 -15 -14 19.67 8.17 0 15 14 23.56 8.12 0 -15 -14 12.68 7.03 0 -15 -15 2.57 5.75 0 15 15 5.04 3.47 0 -15 -15 -2.61 5.84 0 -15 -16 390.81 34.16 0 15 16 341.78 25.61 0 -15 -16 351.80 34.06 0 15 17 48.84 9.31 0 -15 -17 69.03 13.97 0 15 18 154.07 16.44 0 15 19 3.23 4.42 0 -16 7 71.31 15.87 0 -16 6 92.83 17.29 0 -16 5 13.40 12.30 0 -16 5 -2.71 6.56 0 -16 4 100.62 17.06 0 16 -4 112.31 18.72 0 -16 4 110.55 27.70 0 16 -4 94.30 17.77 0 16 -3 94.26 18.48 0 -16 3 94.45 24.99 0 16 -2 43.57 12.83 0 16 -2 47.89 14.35 0 -16 2 47.03 9.17 0 16 -1 3.42 6.27 0 16 -1 -4.42 7.03 0 -16 1 -5.84 9.26 0 -16 1 4.89 3.99 0 -16 0 69.98 11.26 0 -16 0 56.11 20.00 0 16 0 62.24 14.82 0 -16 -1 282.87 24.85 0 -16 -1 296.55 42.66 0 16 1 257.07 31.17 0 -16 -2 38.72 8.69 0 -16 -2 43.19 16.53 0 16 2 55.68 15.11 0 -16 -3 4.99 9.12 0 -16 -3 2.00 4.51 0 16 3 1.90 3.47 0 -16 -4 9.12 8.36 0 -16 -4 -2.09 5.08 0 16 4 1.90 3.94 0 -16 -5 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240.44 35.20 0 19 9 477.75 29.69 0 -19 -9 522.88 50.88 0 -19 -9 486.96 40.76 0 19 9 518.13 40.57 0 19 9 436.41 34.59 0 19 10 10.64 6.94 0 19 10 12.68 5.32 0 -19 -10 8.12 8.31 0 -19 -10 11.02 7.17 0 19 10 9.88 3.14 0 19 10 6.18 5.99 0 19 11 64.94 14.59 0 19 11 47.51 9.74 0 19 11 45.99 6.89 0 19 11 51.45 12.02 0 -19 -11 75.92 17.58 0 -19 -11 67.56 14.11 0 19 12 155.35 22.47 0 -19 -12 146.42 21.52 0 -19 -12 154.40 24.42 0 19 12 171.41 14.44 0 19 12 150.03 20.52 0 19 12 169.13 19.48 0 19 13 102.38 11.26 0 19 13 107.08 16.25 0 19 13 114.69 18.62 0 19 14 3.37 2.33 0 19 15 84.95 10.69 0 19 16 146.66 14.97 0 19 17 91.03 12.11 0 19 18 32.16 7.22 0 20 -1 19.53 11.88 0 20 0 99.01 24.04 0 -20 -1 202.39 22.23 0 -20 -1 181.29 36.39 0 20 1 216.26 36.30 0 -20 -2 104.71 15.73 0 -20 -2 64.90 22.66 0 20 2 121.48 28.46 0 -20 -3 -6.22 8.12 0 -20 -3 9.26 5.23 0 -20 -4 60.34 12.59 0 20 5 34.25 9.60 0 -20 -5 47.41 11.59 0 20 6 122.29 17.10 0 -20 -6 100.53 16.72 0 20 7 46.08 11.16 0 -20 -7 47.60 11.78 0 20 8 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108.51 16.34 8 -10 4 166.14 22.38 -8 10 -4 100.81 10.59 -8 10 -4 110.51 15.54 -8 10 -4 109.60 23.80 8 -10 5 38.81 9.98 8 -10 5 26.46 9.88 -8 10 -5 50.03 6.98 -8 10 -5 40.62 9.55 -8 10 -5 27.22 15.11 8 -10 6 109.08 16.30 -8 10 -6 113.07 15.06 -8 10 -6 134.97 28.84 8 -10 6 80.72 16.63 -8 10 -6 106.32 10.40 -8 10 -7 108.18 15.16 -8 10 -7 140.53 12.45 8 -10 7 158.63 22.42 8 -10 7 135.87 18.96 8 -10 8 -2.47 5.08 -8 10 -8 2.71 2.76 -8 10 -8 -1.85 4.47 -8 10 -8 -6.70 10.64 8 -10 8 3.14 5.75 -8 10 -8 1.00 3.04 -8 10 -9 184.24 37.25 -8 10 -9 129.79 16.49 -8 10 -9 134.26 12.54 8 -10 9 145.90 19.81 -8 10 -10 44.47 20.57 -8 10 -10 53.54 10.69 -8 10 -10 67.70 8.50 8 -10 10 58.44 12.92 -8 10 -11 23.14 15.96 8 -10 11 63.42 13.73 -8 10 -11 40.67 6.89 8 -9 -12 115.92 25.08 -8 9 12 138.77 18.34 8 -9 -11 14.44 10.88 -8 9 11 31.93 9.41 8 -9 -10 9.17 9.41 -8 9 10 2.00 4.51 8 -9 -9 17.44 9.83 -8 9 9 21.05 7.27 8 -9 -8 1106.81 80.67 8 -9 -8 1048.14 75.59 -8 9 8 1201.45 65.75 8 -9 -7 10.17 8.27 -8 9 7 6.60 8.03 8 -9 -7 7.89 7.27 -8 9 6 38.77 11.54 8 -9 -6 23.14 10.55 -8 9 6 16.01 8.36 -8 9 5 11.26 6.22 -8 9 5 15.44 7.55 -8 9 5 27.22 6.22 8 -9 -5 6.41 6.60 -8 9 4 678.61 48.84 -8 9 4 814.25 56.54 8 -9 -4 716.00 55.01 -8 9 4 762.23 41.09 -8 9 3 2.85 3.71 -8 9 3 0.62 1.66 8 -9 -3 2.66 6.03 8 -9 -3 3.04 4.85 8 -9 -2 288.85 28.98 8 -9 -2 263.77 29.74 -8 9 2 255.93 27.84 -8 9 2 257.26 25.08 -8 9 2 265.43 26.46 8 -9 -1 135.02 18.62 8 -9 -1 129.46 20.48 -8 9 1 118.68 18.24 -8 9 1 112.83 15.68 -8 9 1 112.50 17.48 8 -9 0 736.38 52.54 8 -9 0 864.66 58.25 -8 9 0 782.28 53.21 -8 9 0 789.55 50.88 -8 9 0 829.45 58.20 8 -9 1 206.81 22.80 8 -9 1 201.10 24.75 -8 9 -1 180.44 21.00 -8 9 -1 151.98 18.62 -8 9 -1 171.08 26.03 8 -9 2 353.61 33.73 8 -9 2 319.35 30.07 -8 9 -2 348.52 29.36 -8 9 -2 306.81 37.53 -8 9 -2 353.99 28.84 8 -9 3 44.47 10.40 8 -9 3 51.50 13.11 -8 9 -3 60.48 11.16 8 -9 4 428.29 35.16 8 -9 4 434.99 38.20 -8 9 -4 399.31 25.51 -8 9 -4 373.13 30.64 -8 9 -4 392.09 46.89 8 -9 5 119.01 17.82 8 -9 5 122.43 19.76 -8 9 -5 113.50 11.31 -8 9 -5 115.59 15.06 8 -9 6 213.98 24.28 8 -9 6 204.81 26.08 -8 9 -6 221.82 16.58 -8 9 -6 268.14 40.24 -8 9 -6 211.18 20.95 8 -9 7 135.40 19.24 -8 9 -7 119.77 15.20 -8 9 -7 130.65 30.50 8 -9 7 121.86 19.76 -8 9 -7 140.58 12.30 -8 9 -8 322.96 27.51 -8 9 -8 390.09 53.07 -8 9 -8 372.56 23.85 8 -9 8 393.66 34.54 -8 9 -8 379.59 25.46 -8 9 -9 67.70 11.21 -8 9 -9 58.67 22.47 -8 9 -9 67.18 8.55 8 -9 9 56.25 13.30 -8 9 -10 -7.60 9.88 -8 9 -10 -1.57 4.61 -8 9 -10 1.00 2.28 8 -9 10 -2.76 5.70 -8 9 -11 71.50 27.32 -8 9 -11 42.05 8.84 -8 9 -11 39.76 7.03 8 -9 11 60.38 13.83 -8 9 -12 -8.17 16.77 8 -9 12 2.99 6.70 -8 9 -12 2.28 2.80 -8 9 -13 28.41 6.41 8 -8 -13 15.87 9.74 -8 8 12 138.25 18.48 8 -8 -12 101.53 23.42 -8 8 11 332.13 29.36 8 -8 -11 300.68 39.67 -8 8 10 10.26 5.94 8 -8 -10 9.22 8.46 -8 8 9 49.08 10.74 8 -8 -9 52.45 16.68 -8 8 8 18.86 7.36 8 -8 -8 27.70 12.73 8 -8 -8 16.58 10.07 -8 8 8 10.12 10.78 8 -8 -7 283.29 35.25 8 -8 -7 371.23 37.06 -8 8 7 360.88 35.96 -8 8 7 295.12 28.41 -8 8 6 3.14 5.04 8 -8 -6 12.97 8.41 -8 8 6 3.18 5.08 -8 8 6 8.74 5.70 -8 8 5 188.47 24.75 -8 8 5 208.28 19.00 8 -8 -5 182.58 24.66 -8 8 5 214.45 22.23 -8 8 4 158.16 22.00 -8 8 4 124.14 13.54 8 -8 -4 156.54 22.04 -8 8 4 139.06 17.63 -8 8 3 484.30 39.81 -8 8 3 447.29 31.78 -8 8 3 399.26 25.27 8 -8 -3 390.24 37.20 8 -8 -3 390.47 36.01 -8 8 2 13.40 5.65 -8 8 2 41.05 11.26 8 -8 -2 10.50 6.46 8 -8 -2 38.15 11.16 -8 8 2 29.03 4.13 8 -8 -1 348.62 34.44 8 -8 -1 422.16 35.20 -8 8 1 377.31 30.41 -8 8 1 353.13 32.83 -8 8 1 418.69 35.63 8 -8 0 309.52 31.17 8 -8 0 292.08 28.65 -8 8 0 275.88 30.98 -8 8 0 301.82 26.03 -8 8 0 283.06 28.46 8 -8 1 585.69 43.52 8 -8 1 479.17 43.04 -8 8 -1 610.15 52.02 -8 8 -1 651.96 41.24 -8 8 -1 570.15 42.14 -8 8 -2 23.56 6.89 -8 8 -2 21.33 13.02 8 -8 2 12.07 7.36 8 -8 2 8.41 5.80 -8 8 -2 27.22 8.17 -8 8 -3 414.42 47.18 -8 8 -3 475.37 33.45 8 -8 3 377.69 34.44 8 -8 3 482.02 39.72 -8 8 -3 454.23 34.25 8 -8 4 68.13 14.11 -8 8 -4 69.22 11.31 8 -8 4 67.79 13.30 -8 8 -4 57.72 18.91 -8 8 -4 76.68 9.36 -8 8 -5 561.74 58.15 -8 8 -5 443.92 32.78 8 -8 5 444.40 37.25 8 -8 5 527.25 42.28 -8 8 -5 454.94 28.08 8 -8 6 38.34 11.54 8 -8 6 25.27 8.41 -8 8 -6 18.58 12.73 -8 8 -6 18.72 4.56 -8 8 -6 23.04 6.65 8 -8 7 244.57 26.79 -8 8 -7 273.22 23.14 -8 8 -7 284.91 44.80 -8 8 -7 251.18 18.43 -8 8 -8 445.20 32.69 -8 8 -8 535.42 63.14 -8 8 -8 509.48 29.55 -8 8 -8 485.92 31.83 8 -8 8 507.25 41.33 -8 8 -9 148.84 35.16 -8 8 -9 110.79 13.59 -8 8 -9 108.22 11.35 8 -8 9 111.03 18.43 8 -8 9 112.79 9.22 -8 8 -10 55.78 9.41 -8 8 -10 46.70 20.29 -8 8 -10 42.62 7.13 8 -8 10 48.70 13.06 8 -8 10 53.16 7.32 -8 8 -11 187.28 38.81 -8 8 -11 179.06 17.15 -8 8 -11 173.36 15.35 8 -8 11 168.28 23.09 -8 8 -12 194.22 41.05 -8 8 -12 169.75 17.10 -8 8 -12 204.90 17.06 8 -8 12 194.83 25.32 -8 8 -13 34.82 19.62 8 -8 13 12.59 8.69 -8 8 -13 28.74 6.27 8 -8 14 9.74 8.41 -8 8 -14 6.75 4.28 8 -7 -13 5.32 16.25 8 -7 -12 15.35 12.45 -8 7 12 9.26 6.37 8 -7 -11 14.68 10.02 -8 7 11 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13 8 553.95 47.22 -9 -13 -8 463.21 48.79 9 13 8 560.51 50.83 -9 -13 -8 523.88 31.12 9 13 8 391.99 51.02 9 13 9 61.29 16.06 -9 -13 -9 60.10 15.87 -9 -13 -9 45.37 7.41 9 13 9 64.71 21.00 9 13 9 33.83 13.06 9 13 10 21.05 9.50 -9 -13 -10 23.66 5.42 9 13 10 35.49 15.39 9 13 10 27.65 10.93 9 13 11 8.60 7.93 -9 -13 -11 7.74 3.94 9 13 11 11.88 9.45 9 13 11 4.09 7.46 -9 -13 -12 29.65 6.18 9 13 12 11.92 12.30 9 13 12 20.57 10.74 9 13 13 41.95 17.58 9 13 13 57.49 16.15 -9 -13 -13 59.58 8.74 9 13 14 6.03 9.60 9 13 14 8.17 7.51 -9 -13 -14 4.23 7.79 -9 -13 -14 9.98 3.99 9 13 15 151.17 31.12 9 13 15 162.34 26.41 -9 -13 -15 159.87 26.75 9 13 16 121.34 27.98 9 13 16 141.48 24.56 -9 -13 -16 174.74 27.17 9 13 17 91.26 23.47 9 13 17 121.53 22.19 -9 -13 -17 114.26 22.00 9 13 18 18.29 13.73 9 13 18 8.17 9.22 -9 -13 -18 11.97 9.69 9 13 19 55.01 21.19 9 13 19 99.48 20.67 -9 -13 -19 54.54 16.63 -9 -13 -20 15.30 9.31 9 13 20 6.13 9.74 9 13 20 4.23 7.74 -9 -13 -21 30.26 12.54 9 13 21 6.13 11.26 -9 -13 -22 155.02 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14 12 50.22 20.05 -9 -14 -12 50.64 7.84 9 14 12 33.49 12.87 -9 -14 -13 150.79 14.25 9 14 13 113.55 27.17 9 14 13 126.33 23.28 9 14 14 8.36 7.70 -9 -14 -14 11.12 4.28 -9 -14 -14 17.34 10.55 -9 -14 -15 102.95 21.76 9 14 15 146.23 30.12 9 14 15 108.22 21.81 -9 -14 -16 139.53 25.80 9 14 16 191.36 35.30 9 14 16 170.03 26.98 -9 -14 -17 4.18 6.60 9 14 17 12.78 11.73 9 14 17 8.27 8.50 -9 -14 -18 16.30 9.88 9 14 18 6.41 10.21 9 14 18 12.45 10.12 -9 -14 -19 4.04 7.36 9 14 19 12.87 10.21 9 14 19 8.41 7.70 -9 -14 -20 3.94 7.27 9 14 20 6.46 8.36 -9 -14 -21 11.83 10.88 9 14 21 6.46 11.83 -9 -15 2 106.75 21.95 -9 -15 1 195.12 29.22 -9 -15 1 249.18 33.83 -9 -15 0 7.93 6.41 -9 -15 0 4.18 11.50 -9 -15 -1 196.73 23.52 -9 -15 -1 197.68 29.50 9 15 1 218.78 23.23 9 15 2 256.31 25.80 -9 -15 -2 255.74 19.72 -9 -15 -2 242.10 25.51 9 15 3 346.58 31.26 -9 -15 -3 374.08 24.70 9 15 4 40.95 5.65 -9 -15 -4 32.64 6.27 9 15 4 32.40 9.60 9 15 5 127.75 12.54 -9 -15 -5 169.23 14.44 9 15 5 170.79 21.14 9 15 6 328.90 23.18 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47.94 13.63 10 -10 9 23.94 9.64 -10 10 -10 -7.93 14.59 -10 10 -10 -2.19 3.56 10 -10 11 46.27 15.16 -10 9 13 41.67 11.73 -10 9 12 39.48 11.12 -10 9 11 5.32 5.99 -10 9 10 52.45 11.88 -10 9 9 81.29 14.78 -10 9 9 100.77 15.92 10 -9 -8 60.76 16.96 10 -9 -8 70.79 20.52 -10 9 8 82.81 13.78 -10 9 8 97.49 15.06 10 -9 -7 4.85 6.32 10 -9 -7 15.77 11.45 -10 9 7 5.75 5.27 10 -9 -6 60.86 17.29 10 -9 -6 46.51 13.44 -10 9 6 36.68 8.27 10 -9 -5 26.51 11.02 -10 9 5 15.11 5.23 10 -9 -4 122.81 23.09 -10 9 4 133.64 12.83 -10 9 3 350.61 37.10 10 -9 -3 337.88 36.01 10 -9 -3 395.60 39.86 -10 9 2 16.39 9.03 10 -9 -2 3.23 5.89 10 -9 -2 7.22 8.79 -10 9 2 2.14 4.85 -10 9 1 3.09 6.37 10 -9 -1 3.14 5.75 10 -9 -1 -7.13 8.65 -10 9 1 2.52 5.18 -10 9 0 317.45 33.54 10 -9 0 386.96 38.67 10 -9 0 351.23 35.35 -10 9 0 368.90 36.72 10 -9 1 108.98 18.34 -10 9 -1 68.08 14.54 10 -9 1 87.27 17.86 -10 9 -1 64.42 16.68 10 -9 2 47.70 12.83 -10 9 -2 73.88 14.30 10 -9 2 62.62 15.54 -10 9 -2 87.75 20.29 10 -9 3 124.28 20.76 -10 9 -3 150.41 19.76 10 -9 3 180.01 25.42 -10 9 -3 179.30 29.93 -10 9 -3 141.20 18.43 10 -9 4 100.62 18.24 -10 9 -4 84.47 11.02 10 -9 4 69.36 16.39 -10 9 -4 104.57 25.56 -10 9 -4 119.67 16.58 10 -9 5 465.39 41.19 -10 9 -5 448.53 29.55 10 -9 5 453.23 43.61 -10 9 -5 578.09 60.95 -10 9 -5 463.97 36.20 10 -9 6 -2.99 6.13 -10 9 -6 -1.09 3.23 10 -9 6 -3.52 10.21 -10 9 -6 2.09 4.28 -10 9 -6 6.56 10.40 10 -9 7 -6.03 10.69 -10 9 -7 2.19 2.99 10 -9 7 -3.56 8.65 -10 9 -7 4.09 4.18 -10 9 -7 7.03 9.07 10 -9 8 159.30 22.90 -10 9 -8 192.70 20.43 -10 9 -8 237.21 42.62 -10 9 -8 147.09 19.48 -10 9 -8 192.31 15.96 10 -9 8 181.01 26.41 10 -9 9 150.60 22.71 -10 9 -9 155.12 14.54 -10 9 -9 172.79 38.01 -10 9 -9 142.34 17.58 -10 9 -9 154.36 16.30 10 -9 9 187.94 27.03 10 -9 10 22.52 9.83 -10 9 -10 27.89 6.32 -10 9 -10 16.39 15.06 -10 9 -10 22.28 7.70 10 -9 11 13.21 9.07 -10 9 -11 8.55 13.59 -10 9 -11 12.68 4.66 -10 8 13 143.33 22.23 -10 8 12 2.95 6.08 -10 8 11 5.61 5.75 -10 8 10 5.27 7.27 10 -8 -9 332.32 42.38 -10 8 9 273.60 27.46 -10 8 9 249.52 27.22 -10 8 8 82.33 14.73 10 -8 -8 111.27 24.94 -10 8 7 4.18 4.28 10 -8 -7 -3.90 6.18 10 -8 -7 -4.85 8.93 -10 8 6 5.65 5.18 10 -8 -6 -3.80 8.55 10 -8 -6 -4.66 6.03 -10 8 5 63.52 10.55 10 -8 -5 78.29 18.01 -10 8 4 228.42 19.81 10 -8 -4 212.65 29.12 -10 8 3 45.28 13.30 10 -8 -3 43.57 13.54 10 -8 -3 61.29 15.96 -10 8 3 38.77 6.70 -10 8 2 80.05 17.10 10 -8 -2 68.51 15.92 10 -8 -2 74.73 17.29 -10 8 2 87.13 13.59 -10 8 1 149.08 22.28 10 -8 -1 102.19 18.91 10 -8 -1 136.87 23.23 -10 8 1 151.51 20.90 10 -8 0 109.55 18.96 -10 8 0 113.88 18.81 10 -8 0 110.98 20.62 -10 8 0 94.11 19.29 -10 8 -1 95.92 21.00 -10 8 -1 80.57 13.92 10 -8 1 110.08 19.72 -10 8 -1 61.95 14.02 10 -8 1 55.44 13.63 10 -8 2 30.45 10.93 10 -8 2 30.83 10.55 -10 8 -2 32.16 8.93 -10 8 -2 45.66 16.30 -10 8 -2 44.85 11.21 -10 8 -3 19.81 7.55 10 -8 3 15.16 7.36 -10 8 -3 7.93 7.27 -10 8 -3 12.68 6.46 -10 8 -3 15.30 10.45 10 -8 3 3.42 6.27 -10 8 -4 8.65 10.55 -10 8 -4 10.40 5.75 10 -8 4 27.22 9.64 -10 8 -4 32.88 9.69 10 -8 4 20.57 9.45 -10 8 -5 163.95 28.51 -10 8 -5 174.93 20.00 10 -8 5 179.16 24.47 -10 8 -5 168.23 15.96 10 -8 5 200.01 27.13 -10 8 -6 186.38 32.12 -10 8 -6 201.01 21.38 10 -8 6 208.37 25.94 -10 8 -6 191.93 16.72 10 -8 6 209.13 28.22 -10 8 -7 134.31 27.32 10 -8 7 99.53 18.10 -10 8 -7 108.89 15.11 10 -8 7 91.98 19.10 -10 8 -7 91.83 11.12 10 -8 8 -3.61 8.08 10 -8 8 6.37 6.51 -10 8 -8 5.56 3.52 -10 8 -8 -7.51 11.92 -10 8 -8 8.55 6.51 -10 8 -8 -1.90 3.47 10 -8 9 185.52 25.61 -10 8 -9 214.41 21.24 -10 8 -9 158.77 36.01 -10 8 -9 200.96 20.38 -10 8 -9 214.60 17.34 -10 8 -10 309.57 26.22 -10 8 -10 339.21 23.09 10 -8 11 20.52 9.45 -10 8 -11 17.63 5.04 -10 8 -11 22.19 6.51 -10 8 -11 17.44 13.87 10 -8 12 59.72 15.63 -10 8 -12 59.81 9.03 -10 8 -12 45.18 23.56 10 -8 13 223.72 30.41 -10 7 12 530.91 45.66 -10 7 11 14.73 8.55 -10 7 10 11.12 7.22 10 -7 -9 95.44 22.57 -10 7 9 108.89 16.72 -10 7 9 62.85 14.49 -10 7 8 370.99 32.78 10 -7 -8 377.46 40.62 10 -7 -8 309.09 41.48 -10 7 7 27.13 8.93 10 -7 -7 34.54 12.78 10 -7 -7 53.35 16.11 -10 7 6 8.22 4.99 10 -7 -6 15.01 9.74 10 -7 -6 13.97 10.45 -10 7 5 3.71 4.47 10 -7 -5 -4.47 8.17 10 -7 -5 3.66 7.51 -10 7 4 499.46 45.94 -10 7 4 479.46 33.30 10 -7 -4 454.23 43.85 10 -7 -4 441.64 42.47 -10 7 3 94.78 19.05 -10 7 3 123.57 13.11 -10 7 3 113.59 13.06 10 -7 -3 97.96 19.15 10 -7 -3 85.14 18.72 -10 7 2 2.14 5.23 -10 7 2 3.37 6.94 10 -7 -2 -6.60 8.55 10 -7 -2 -3.52 7.17 -10 7 2 2.00 2.99 10 -7 -1 3.42 7.74 -10 7 1 2.85 5.89 -10 7 1 3.23 5.94 10 -7 -1 -6.46 5.94 -10 7 0 222.63 26.70 10 -7 0 243.91 28.84 10 -7 0 224.53 28.74 -10 7 0 275.88 29.93 -10 7 -1 89.60 17.53 10 -7 1 61.05 15.25 -10 7 -1 83.95 16.01 10 -7 1 68.65 15.49 -10 7 -2 37.77 12.35 -10 7 -2 65.32 13.59 10 -7 2 40.38 12.87 10 -7 2 52.54 14.06 -10 7 -3 3.80 6.94 -10 7 -3 10.26 6.65 10 -7 3 10.07 8.74 10 -7 3 12.35 7.51 -10 7 -4 94.78 20.48 -10 7 -4 94.35 15.82 10 -7 4 111.79 19.67 10 -7 4 111.22 18.86 -10 7 -5 35.68 13.63 -10 7 -5 26.37 6.18 10 -7 5 17.06 8.93 10 -7 5 27.94 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99.72 17.10 -10 -5 -6 102.67 21.57 -10 -5 -6 97.49 16.87 10 5 7 1015.31 65.37 -10 -5 -7 991.32 54.78 -10 -5 -7 932.17 72.78 10 5 8 384.72 36.49 -10 -5 -8 428.77 28.84 10 5 9 279.64 30.50 -10 -5 -9 317.60 23.42 -10 -5 -10 15.06 9.79 10 5 10 14.59 8.46 -10 -5 -10 12.78 4.99 10 5 10 3.99 7.32 -10 -5 -11 165.81 25.89 10 5 11 202.34 25.18 -10 -5 -11 192.31 17.01 10 5 11 152.55 26.18 10 5 12 12.07 10.50 -10 -5 -12 18.81 9.17 -10 -5 -12 28.32 6.32 -10 -5 -13 406.06 41.43 -10 -5 -13 483.50 30.36 10 5 13 342.39 40.29 10 5 14 28.27 11.73 -10 -5 -14 7.36 7.55 -10 -5 -14 12.11 4.99 10 5 15 244.10 32.45 -10 -5 -15 241.20 30.60 10 5 16 28.74 12.02 -10 -5 -16 38.53 12.92 10 5 17 149.70 25.04 -10 -5 -17 111.60 19.86 10 5 18 122.19 20.67 10 5 18 88.89 19.91 10 5 19 70.50 15.96 10 5 19 99.25 21.28 -10 -5 -19 100.86 18.67 10 5 20 294.13 33.92 -10 -5 -20 195.93 25.51 -10 -5 -21 13.21 6.89 -10 -6 9 2.19 4.04 -10 -6 8 -2.19 4.85 -10 -6 8 -4.56 9.31 10 6 -8 5.99 9.50 -10 -6 7 11.59 11.88 -10 -6 7 4.32 7.93 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588.82 55.49 -10 -6 -3 42.76 10.88 -10 -6 -3 26.75 9.60 10 6 3 38.72 11.92 10 6 3 17.01 7.93 10 6 3 28.60 9.93 10 6 3 39.34 10.17 -10 -6 -4 720.99 52.02 10 6 4 680.66 54.92 10 6 4 788.74 54.21 10 6 4 755.10 52.45 10 6 4 678.57 50.07 10 6 5 96.63 17.72 10 6 5 141.67 18.86 -10 -6 -5 104.85 22.99 -10 -6 -5 92.45 16.53 10 6 5 107.56 19.62 10 6 6 97.54 17.34 10 6 6 116.02 16.58 -10 -6 -6 98.15 21.66 -10 -6 -6 84.38 15.92 10 6 6 94.16 18.96 10 6 7 8.74 7.55 10 6 7 3.99 3.66 -10 -6 -7 -1.38 2.80 -10 -6 -7 4.32 7.98 -10 -6 -8 372.80 26.56 10 6 8 382.97 35.96 -10 -6 -9 11.73 10.17 10 6 9 9.12 7.89 -10 -6 -9 9.12 4.94 -10 -6 -10 532.24 49.74 -10 -6 -10 567.78 34.78 10 6 10 533.71 45.51 -10 -6 -11 -3.90 8.03 10 6 11 15.82 8.22 -10 -6 -11 16.53 5.61 -10 -6 -12 228.80 31.21 -10 -6 -12 239.35 19.72 -10 -6 -13 92.17 19.43 10 6 13 97.35 20.48 -10 -6 -13 98.44 12.07 -10 -6 -14 204.67 18.53 10 6 14 239.35 31.55 -10 -6 -14 196.78 29.36 -10 -6 -15 122.38 22.04 10 6 15 155.16 25.51 10 6 16 378.50 41.00 -10 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3.90 7.17 11 -8 9 -3.47 8.46 -11 8 -9 2.38 3.28 -11 8 -9 -2.00 4.09 -11 8 -9 8.08 10.45 -11 8 -9 -2.14 4.37 -11 8 -10 62.24 11.54 -11 8 -10 74.16 10.02 -11 8 -10 50.93 22.23 11 -8 10 74.68 16.58 -11 8 -11 88.65 29.55 -11 8 -11 82.43 13.40 11 -8 11 94.40 18.62 11 -8 12 29.69 12.35 -11 7 12 9.50 6.51 -11 7 11 290.37 31.50 -11 7 10 45.70 12.16 -11 7 9 81.05 15.87 -11 7 8 65.75 13.40 -11 7 7 747.69 51.12 11 -7 -7 679.66 65.75 11 -7 -7 750.83 61.71 -11 7 6 -2.14 3.94 11 -7 -6 4.04 6.41 11 -7 -6 -5.13 9.45 -11 7 5 5.75 4.66 11 -7 -5 14.87 11.16 11 -7 -5 11.88 9.60 -11 7 4 8.22 4.80 11 -7 -4 11.69 10.74 11 -7 -3 554.14 51.40 11 -7 -3 602.27 52.45 -11 7 3 613.53 37.53 11 -7 -2 318.17 35.35 11 -7 -2 224.43 31.50 -11 7 2 289.33 27.08 11 -7 -1 14.21 7.98 11 -7 -1 22.57 11.97 -11 7 1 2.90 6.51 -11 7 1 7.03 8.50 -11 7 0 16.58 8.84 11 -7 0 11.16 9.07 11 -7 0 38.39 12.45 -11 7 0 26.75 11.50 -11 7 -1 465.44 42.90 11 -7 1 519.13 45.51 11 -7 1 502.31 46.27 -11 7 -1 471.90 42.71 -11 7 -2 3.52 5.56 -11 7 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58.58 -11 6 5 -4.23 6.18 11 -6 -5 -3.90 7.13 11 -6 -5 -4.94 6.41 -11 6 4 28.36 8.08 11 -6 -4 28.51 12.40 11 -6 -4 41.90 13.59 11 -6 -4 42.19 13.25 11 -6 -3 7.46 8.36 11 -6 -3 3.80 8.50 -11 6 3 -1.66 2.99 -11 6 3 2.90 5.18 11 -6 -2 1114.79 75.21 11 -6 -2 969.51 71.07 -11 6 2 1034.17 56.20 -11 6 2 979.11 59.15 -11 6 1 39.15 14.02 11 -6 -1 39.38 12.87 11 -6 -1 66.46 17.72 -11 6 1 50.03 11.40 11 -6 0 7.03 6.46 -11 6 0 13.59 7.65 11 -6 0 25.61 11.64 -11 6 0 7.98 5.46 -11 6 -1 356.08 36.06 11 -6 1 345.58 36.91 11 -6 1 350.85 36.53 -11 6 -1 303.30 32.83 -11 6 -2 447.29 40.62 11 -6 2 452.00 42.95 11 -6 2 562.17 47.89 -11 6 -2 466.68 43.57 11 -6 3 3.42 5.46 -11 6 -3 5.80 6.51 11 -6 3 3.61 5.75 -11 6 -3 7.32 6.70 11 -6 4 10.31 7.08 -11 6 -4 10.97 7.13 11 -6 4 3.66 8.17 -11 6 -4 11.97 8.98 11 -6 5 107.32 19.57 -11 6 -5 107.32 17.25 11 -6 5 102.62 20.95 -11 6 -5 103.28 21.71 11 -6 6 143.10 23.09 -11 6 -6 142.67 14.92 11 -6 6 129.75 22.76 -11 6 -6 97.25 22.80 11 -6 7 3.56 5.65 -11 6 -7 6.51 3.80 11 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6 164.95 20.86 -11 -11 -6 178.39 17.63 11 11 7 -3.99 6.32 -11 -11 -7 -1.43 3.18 11 11 7 1.95 4.32 -11 -11 -7 4.99 6.46 -11 -11 -8 480.41 51.31 11 11 8 519.22 48.79 11 11 8 430.29 46.37 11 11 8 514.23 34.44 -11 -11 -8 495.90 32.69 11 11 9 22.23 10.02 -11 -11 -9 21.66 6.03 11 11 9 20.71 5.56 -11 -11 -9 19.67 13.54 -11 -11 -10 90.74 11.54 11 11 10 46.51 15.20 -11 -11 -11 178.16 16.49 11 11 11 138.58 26.56 -11 -11 -12 461.45 30.26 11 11 12 447.29 51.40 11 11 12 362.97 44.56 -11 -11 -13 37.53 15.11 11 11 13 73.26 20.19 11 11 13 77.63 20.05 -11 -11 -14 300.40 38.01 11 11 14 263.96 38.91 11 11 14 246.85 36.25 11 11 15 11.16 10.26 11 11 15 14.44 10.83 -11 -11 -15 -4.56 10.21 11 11 16 166.95 31.12 11 11 16 181.77 29.74 11 11 17 16.63 12.49 11 11 17 28.60 13.16 11 11 18 192.74 33.35 11 11 18 238.21 34.87 -11 -11 -18 238.83 34.06 11 11 19 27.32 13.30 -11 -11 -19 34.44 13.16 11 11 20 37.82 17.29 -11 -11 -20 45.85 15.39 11 11 21 53.40 17.82 -11 -11 -21 47.89 16.11 -11 -11 -22 117.25 21.71 -11 -12 4 65.13 16.91 -11 -12 3 153.55 26.46 -11 -12 2 155.31 26.89 11 12 -1 3.14 4.99 -11 -12 1 13.78 11.12 -11 -12 1 17.20 11.16 11 12 0 33.07 8.12 11 12 0 31.26 10.45 -11 -12 0 59.05 13.73 -11 -12 0 23.56 12.35 -11 -12 -1 258.16 29.12 11 12 1 231.89 28.55 11 12 1 286.43 24.66 -11 -12 -1 227.00 34.63 -11 -12 -2 206.57 32.12 11 12 2 230.89 27.79 11 12 2 180.39 20.05 -11 -12 -2 217.87 26.32 11 12 3 86.94 17.29 11 12 3 78.67 12.92 -11 -12 -3 94.78 21.76 -11 -12 -3 72.93 14.73 11 12 4 89.79 17.72 11 12 4 42.47 10.50 -11 -12 -4 60.43 17.48 -11 -12 -4 97.96 16.77 -11 -12 -5 612.62 59.01 11 12 5 576.37 42.19 11 12 5 597.80 50.31 11 12 6 65.47 16.20 11 12 6 52.02 11.92 -11 -12 -6 45.66 16.96 -11 -12 -6 59.81 9.45 11 12 7 3.90 6.18 11 12 7 2.61 5.89 -11 -12 -7 -1.38 3.80 -11 -12 -7 5.08 9.26 11 12 8 4.13 6.60 -11 -12 -8 17.53 5.27 -11 -12 -8 5.04 8.03 11 12 9 264.81 34.68 -11 -12 -9 244.53 20.62 -11 -12 -9 304.91 39.38 11 12 10 329.90 41.00 -11 -12 -10 318.55 24.04 -11 -12 -10 351.18 42.90 11 12 11 19.29 11.73 11 12 11 23.90 13.49 -11 -12 -11 26.22 6.56 -11 -12 -12 161.81 15.87 11 12 12 172.69 32.54 11 12 12 127.61 26.70 -11 -12 -13 166.85 29.55 11 12 13 207.85 35.01 11 12 13 222.44 33.45 -11 -12 -14 9.41 7.51 11 12 14 23.71 12.16 11 12 14 24.66 12.02 11 12 15 29.50 15.35 11 12 15 19.62 11.97 11 12 16 23.52 14.35 11 12 16 53.59 16.77 11 12 17 158.30 31.74 11 12 17 188.85 30.69 -11 -12 -17 166.19 29.03 11 12 18 58.34 19.43 11 12 18 38.62 14.87 -11 -12 -18 67.75 18.67 11 12 19 324.82 45.04 -11 -12 -19 321.82 39.53 11 12 20 40.24 17.53 -11 -12 -20 21.28 11.78 11 12 21 159.44 31.07 -11 -12 -21 135.30 24.28 -11 -13 3 4.23 6.75 -11 -13 2 106.23 22.33 -11 -13 1 22.99 12.68 11 13 0 18.20 8.79 -11 -13 0 5.99 6.13 -11 -13 0 9.50 8.74 -11 -13 0 21.52 11.16 11 13 1 46.32 9.12 11 13 1 66.94 14.68 -11 -13 -1 57.91 13.73 -11 -13 -1 68.22 19.62 -11 -13 -1 37.53 13.44 -11 -13 -2 422.49 36.68 11 13 2 347.24 35.35 11 13 2 342.82 27.17 -11 -13 -2 328.24 42.09 11 13 3 131.17 21.19 -11 -13 -3 121.15 25.70 11 13 3 155.83 17.29 -11 -13 -3 157.25 21.28 11 13 4 5.46 4.42 11 13 4 12.87 8.36 -11 -13 -4 -5.08 6.60 11 13 5 53.73 14.06 -11 -13 -5 82.05 21.76 11 13 5 62.81 11.59 -11 -13 -5 68.22 10.12 11 13 6 247.42 30.98 -11 -13 -6 236.31 35.25 11 13 6 259.06 25.80 -11 -13 -6 238.87 20.57 11 13 7 154.36 24.70 -11 -13 -7 184.52 31.64 11 13 7 161.77 21.00 -11 -13 -7 166.52 16.34 -11 -13 -8 6.56 4.51 11 13 8 -4.04 6.46 -11 -13 -8 -5.08 8.12 -11 -13 -9 60.72 9.50 11 13 9 34.73 13.97 -11 -13 -9 45.61 16.25 -11 -13 -10 407.39 27.36 11 13 10 313.70 40.38 -11 -13 -10 391.85 45.99 -11 -13 -11 142.05 14.54 11 13 11 119.06 28.17 11 13 11 144.90 26.51 -11 -13 -11 124.14 26.41 11 13 12 93.69 24.09 11 13 12 129.03 25.37 11 13 13 62.28 20.76 11 13 13 55.30 17.44 11 13 14 180.39 34.02 11 13 14 155.97 28.93 11 13 15 12.40 11.45 11 13 15 40.10 15.25 11 13 16 43.38 17.20 11 13 16 54.68 17.20 -11 -13 -16 62.19 17.72 11 13 17 12.35 11.35 11 13 17 9.88 7.84 -11 -13 -17 14.11 12.92 11 13 18 258.92 41.29 11 13 18 343.49 42.09 -11 -13 -18 317.98 39.57 -11 -13 -19 99.01 21.62 11 13 19 36.77 17.06 11 13 20 24.42 13.73 11 13 21 12.11 11.12 -11 -14 2 39.34 16.15 -11 -14 1 411.52 46.42 11 14 0 17.53 8.50 -11 -14 0 18.96 12.30 11 14 1 26.37 10.12 -11 -14 -1 34.16 14.87 11 14 2 53.35 13.73 -11 -14 -2 79.86 21.28 11 14 2 93.69 11.69 -11 -14 -2 91.07 16.11 11 14 3 129.56 20.57 -11 -14 -3 152.12 28.36 11 14 3 104.57 13.44 -11 -14 -3 130.36 19.05 11 14 4 6.18 6.37 -11 -14 -4 5.13 9.41 11 14 4 11.07 5.46 -11 -14 -4 8.46 4.32 11 14 5 3.23 5.94 -11 -14 -5 10.36 9.50 11 14 5 5.18 4.23 -11 -14 -5 1.38 3.33 11 14 6 47.70 14.06 -11 -14 -6 57.06 17.86 11 14 6 32.73 8.60 -11 -14 -6 33.26 7.36 11 14 7 47.08 13.83 -11 -14 -7 41.48 15.87 11 14 7 26.18 8.46 -11 -14 -7 64.75 9.41 11 14 8 19.57 9.55 -11 -14 -8 20.62 12.54 11 14 8 22.42 8.60 -11 -14 -8 12.68 4.85 11 14 9 8.46 8.69 -11 -14 -9 10.26 11.54 -11 -14 -9 18.86 5.80 11 14 10 54.44 16.91 -11 -14 -10 81.24 21.05 -11 -14 -10 75.44 10.17 11 14 10 65.70 21.95 -11 -14 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17.44 11 16 12 39.15 15.01 11 16 13 42.57 18.48 -11 -16 -13 31.12 13.54 11 16 13 35.82 14.92 11 16 14 14.16 11.26 11 16 14 10.50 9.64 11 16 15 -7.08 11.26 11 16 15 15.87 11.88 11 16 16 42.28 16.15 11 16 17 257.35 37.67 -11 -17 -1 4.80 8.84 -11 -17 -2 54.92 17.29 11 17 3 348.14 33.07 -11 -17 -3 405.72 47.08 11 17 4 21.14 8.79 -11 -17 -4 5.23 9.64 11 17 5 98.96 17.25 11 17 6 14.49 8.84 -11 -17 -6 -5.37 9.83 11 17 7 340.49 35.49 -11 -17 -7 383.20 47.32 11 17 8 3.33 5.27 -11 -17 -8 10.78 12.16 11 17 9 134.31 22.57 11 17 9 124.76 16.34 -11 -17 -9 156.30 29.36 11 17 10 219.77 31.55 -11 -17 -10 284.29 40.43 11 17 11 78.86 19.57 11 17 12 118.34 24.70 11 17 13 50.31 17.39 11 17 14 73.21 20.62 11 17 15 10.64 11.97 11 17 16 16.06 11.02 11 17 17 192.46 32.83 11 18 6 24.13 9.26 11 18 7 5.70 5.89 11 18 8 286.95 32.21 11 18 9 6.75 10.26 11 18 10 155.92 24.99 11 18 11 226.19 31.45 11 18 12 234.17 33.54 11 18 13 19.43 12.64 11 18 14 56.49 18.39 11 18 15 5.32 9.74 11 18 16 161.72 30.45 11 18 17 5.42 9.93 11 19 10 17.01 8.84 11 19 11 120.91 21.43 11 19 12 54.54 16.06 11 19 13 206.76 32.50 11 19 14 29.65 14.40 11 19 15 41.62 16.63 11 19 16 -5.37 9.83 12 -11 -1 104.90 20.67 12 -11 0 -3.52 8.60 12 -11 1 354.08 37.48 12 -11 2 3.42 9.41 12 -11 3 6.75 7.60 12 -11 3 16.44 9.26 12 -11 4 32.88 13.16 -12 11 -5 32.78 16.68 -12 11 -6 5.94 9.45 -12 11 -7 128.56 28.79 12 -10 -2 166.23 25.99 12 -10 -1 59.10 15.73 12 -10 0 141.34 24.18 12 -10 0 171.22 28.65 12 -10 1 14.25 9.31 12 -10 1 28.98 12.02 12 -10 2 530.96 47.56 12 -10 2 497.13 49.12 12 -10 3 13.92 9.60 12 -10 3 4.09 6.51 -12 10 -4 26.03 12.64 12 -10 4 10.31 8.36 12 -10 4 12.26 9.22 -12 10 -5 17.34 11.88 12 -10 5 6.84 7.70 12 -10 5 24.47 11.21 -12 10 -6 12.64 14.21 12 -10 6 30.74 10.88 12 -10 6 20.38 10.59 -12 10 -7 20.48 15.35 12 -10 7 -4.09 8.41 -12 10 -8 72.78 26.03 12 -9 -2 38.34 12.68 12 -9 -2 4.18 7.74 12 -9 -1 87.61 20.29 12 -9 -1 101.48 20.19 12 -9 0 198.16 29.50 12 -9 0 188.51 27.32 12 -9 1 171.13 25.56 12 -9 1 205.05 29.98 -12 9 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-4 -3 85.85 18.01 -12 -4 -4 334.03 34.82 12 4 4 330.28 35.25 -12 -4 -4 243.43 36.72 12 4 4 292.42 32.64 -12 -4 -5 250.28 35.73 -12 -4 -5 188.56 25.80 12 4 5 205.47 26.94 12 4 5 253.70 30.55 12 4 5 195.21 24.37 12 4 6 187.47 24.09 -12 -4 -6 144.95 27.98 -12 -4 -6 166.28 23.80 12 4 6 205.76 27.70 12 4 7 -4.37 6.94 -12 -4 -7 4.75 11.54 -12 -4 -7 5.99 8.22 12 4 7 5.75 5.89 12 4 8 260.82 35.68 -12 -4 -8 271.13 23.42 -12 -4 -8 316.36 40.10 12 4 8 333.99 32.78 12 4 9 434.37 47.08 -12 -4 -9 465.82 48.27 -12 -4 -9 492.00 33.02 12 4 9 422.54 39.72 12 4 10 676.38 62.19 12 4 10 692.49 53.45 -12 -4 -10 741.61 44.09 12 4 11 4.80 7.65 12 4 11 3.04 7.41 12 4 12 418.46 39.00 12 4 12 334.98 42.43 -12 -4 -12 459.79 45.94 12 4 13 102.81 23.47 -12 -4 -13 141.39 25.70 12 4 13 125.71 20.43 12 4 14 98.34 23.71 -12 -4 -14 123.52 23.14 12 4 14 181.39 24.56 12 4 15 -4.94 9.07 -12 -4 -15 4.18 8.60 12 4 15 6.41 7.79 12 4 16 84.57 22.19 -12 -4 -16 86.13 19.53 -12 -4 -17 115.11 22.28 12 4 17 85.14 21.95 -12 -4 -18 60.81 16.20 -12 -4 -19 14.40 8.74 12 5 -5 337.50 35.44 12 5 -5 401.35 49.08 -12 -5 5 385.30 41.90 -12 -5 4 86.42 19.43 12 5 -4 88.32 22.95 12 5 -4 65.37 15.01 12 5 -4 88.03 19.43 12 5 -3 36.87 12.49 12 5 -3 86.61 18.91 -12 -5 3 52.73 14.87 12 5 -3 78.25 21.00 12 5 -2 77.91 17.67 12 5 -2 64.14 14.49 12 5 -2 29.69 14.54 -12 -5 2 64.99 16.06 12 5 -1 77.25 17.72 12 5 -1 82.38 16.72 12 5 -1 70.41 19.57 -12 -5 1 114.12 20.14 12 5 0 172.88 25.70 12 5 0 149.56 22.09 12 5 0 115.64 23.23 -12 -5 0 162.29 23.61 12 5 1 34.59 12.78 12 5 1 33.68 10.97 12 5 1 25.23 11.64 -12 -5 -1 25.37 10.17 -12 -5 -2 35.35 12.26 12 5 2 62.00 15.96 12 5 2 24.75 9.98 12 5 2 35.68 12.16 -12 -5 -2 42.43 12.54 12 5 3 23.56 10.21 12 5 3 28.32 9.60 12 5 3 22.33 10.83 -12 -5 -3 10.26 7.08 -12 -5 -4 10.31 10.59 -12 -5 -4 -3.28 8.55 12 5 4 -3.99 7.32 12 5 4 -3.47 6.37 12 5 4 -3.23 5.13 12 5 4 2.99 6.08 -12 -5 -5 35.68 14.11 -12 -5 -5 38.20 12.49 12 5 5 42.14 12.73 12 5 5 40.19 13.16 12 5 5 39.24 11.88 -12 -5 -6 196.78 26.13 -12 -5 -6 236.50 35.49 12 5 6 251.70 28.93 12 5 6 225.81 29.12 12 5 6 199.82 25.94 12 5 7 650.44 50.74 -12 -5 -7 616.42 49.31 -12 -5 -7 577.66 58.67 12 5 7 683.46 50.17 12 5 8 24.80 9.88 -12 -5 -8 20.76 6.79 -12 -5 -8 14.49 9.93 12 5 9 119.77 20.38 -12 -5 -9 104.23 13.87 -12 -5 -10 74.07 11.35 12 5 10 76.63 16.68 12 5 11 311.61 34.16 12 5 11 344.44 42.38 -12 -5 -12 8.88 8.12 12 5 12 6.60 7.41 12 5 12 9.79 10.07 -12 -5 -13 114.88 23.23 12 5 13 149.79 22.66 12 5 13 113.36 24.94 12 5 14 339.54 35.77 -12 -5 -14 306.57 39.00 12 5 14 341.35 42.47 -12 -5 -15 176.68 28.51 12 5 15 182.77 25.56 12 5 15 124.19 25.46 -12 -5 -16 4.23 8.65 12 5 16 -4.99 7.93 12 5 17 120.20 25.08 -12 -5 -17 77.72 19.19 12 5 18 247.23 36.39 -12 -5 -18 271.51 34.54 -12 -5 -19 11.26 9.74 -12 -5 -21 91.17 18.48 12 6 -5 -5.89 7.65 -12 -6 5 8.50 7.79 12 6 -4 223.77 27.17 12 6 -4 251.56 37.91 -12 -6 4 216.54 31.74 -12 -6 4 231.08 38.67 12 6 -3 62.09 13.68 12 6 -3 19.48 10.83 -12 -6 3 39.24 13.54 12 6 -3 37.20 15.49 12 6 -2 176.07 23.85 12 6 -2 215.88 29.27 12 6 -2 180.39 30.60 -12 -6 2 211.08 29.27 12 6 -1 45.89 13.68 12 6 -1 37.72 14.44 -12 -6 1 32.54 11.12 12 6 -1 32.26 11.21 -12 -6 0 288.19 34.63 12 6 0 360.78 42.19 12 6 0 370.14 35.35 12 6 0 415.37 41.29 12 6 1 106.75 20.86 12 6 1 109.13 19.34 -12 -6 -1 143.14 22.47 -12 -6 -2 91.22 18.48 12 6 2 100.10 19.62 12 6 2 65.89 14.87 12 6 2 126.94 22.38 -12 -6 -2 47.94 13.21 12 6 3 168.09 25.75 12 6 3 133.83 21.43 12 6 3 212.41 28.60 -12 -6 -3 152.60 23.47 -12 -6 -4 5.37 8.55 -12 -6 -4 22.90 9.50 12 6 4 19.95 9.69 12 6 4 6.32 7.13 12 6 4 13.97 9.07 12 6 4 25.08 9.55 -12 -6 -5 10.59 11.92 -12 -6 -5 12.68 7.70 12 6 5 8.17 9.22 12 6 5 12.78 7.22 12 6 5 25.99 9.45 12 6 5 29.31 10.36 -12 -6 -6 41.76 15.20 -12 -6 -6 39.81 11.69 12 6 6 46.56 15.63 12 6 6 28.93 9.88 12 6 6 24.09 10.07 12 6 6 40.71 11.73 12 6 7 201.10 26.79 12 6 7 243.72 26.98 -12 -6 -7 214.88 26.37 -12 -6 -7 225.14 35.01 12 6 7 175.78 28.51 12 6 8 245.05 26.41 -12 -6 -8 274.17 37.06 -12 -6 -8 221.96 20.76 12 6 8 217.35 28.32 -12 -6 -9 12.45 5.75 12 6 9 16.72 9.74 -12 -6 -10 130.17 14.78 -12 -6 -10 105.42 22.80 12 6 10 101.67 19.34 -12 -6 -11 252.22 35.39 12 6 11 258.26 30.93 -12 -6 -12 173.93 28.74 12 6 12 160.44 24.32 12 6 13 49.69 17.15 -12 -6 -13 36.39 13.30 12 6 13 31.69 11.73 12 6 14 19.91 13.78 -12 -6 -14 35.92 13.73 12 6 14 46.18 13.49 12 6 15 289.47 39.24 -12 -6 -15 260.96 35.68 12 6 16 35.01 14.59 -12 -6 -16 38.96 14.92 12 6 17 110.41 24.47 -12 -6 -17 125.99 23.66 12 6 18 292.80 39.19 -12 -6 -18 231.56 32.16 -12 -6 -21 -3.56 8.03 12 7 -5 -5.99 10.97 12 7 -4 2.85 9.50 12 7 -4 11.35 9.03 -12 -7 4 4.23 8.69 12 7 -3 246.71 36.68 12 7 -3 238.07 27.84 12 7 -3 265.43 32.54 -12 -7 3 244.62 32.83 12 7 -2 45.66 13.73 12 7 -2 53.35 13.06 -12 -7 2 74.54 17.77 12 7 -2 45.70 16.96 12 7 -1 22.71 11.07 12 7 -1 28.08 10.07 12 7 -1 33.40 14.59 -12 -7 1 56.58 15.16 12 7 0 56.58 15.25 12 7 0 59.24 13.40 -12 -7 0 43.47 13.87 12 7 0 44.66 14.92 12 7 1 936.73 69.55 12 7 1 908.37 62.62 12 7 1 1016.73 73.88 -12 -7 -1 900.24 66.65 12 7 2 160.34 25.32 12 7 2 132.41 20.43 12 7 2 141.48 24.75 -12 -7 -2 174.59 25.27 12 7 3 11.64 8.69 12 7 3 17.63 8.93 12 7 3 -3.71 6.79 -12 -7 -3 6.70 6.89 -12 -7 -4 152.60 22.47 12 7 4 142.43 23.80 12 7 4 96.49 19.05 12 7 4 128.27 21.24 12 7 4 105.94 18.53 -12 -7 -5 38.43 16.11 -12 -7 -5 50.22 13.40 12 7 5 48.84 16.01 12 7 5 91.17 18.24 12 7 5 54.92 13.78 12 7 5 63.09 15.20 -12 -7 -6 5.42 8.60 -12 -7 -6 12.16 7.36 12 7 6 4.23 5.46 12 7 6 -3.42 6.22 12 7 6 5.99 6.13 12 7 6 3.33 5.27 12 7 7 10.31 7.74 12 7 7 11.12 7.22 -12 -7 -7 5.27 8.41 12 7 7 26.37 12.11 12 7 8 212.79 28.36 12 7 8 263.29 27.22 -12 -7 -8 225.43 20.86 12 7 8 228.42 32.88 12 7 9 123.90 21.85 12 7 9 137.06 25.99 12 7 9 141.62 19.05 -12 -7 -9 146.94 16.11 -12 -7 -10 18.96 11.50 12 7 10 -3.61 7.36 12 7 10 4.85 7.74 -12 -7 -10 10.55 4.80 12 7 10 17.48 6.94 -12 -7 -11 127.80 24.61 12 7 11 98.39 19.76 -12 -7 -12 18.86 10.59 12 7 12 11.07 8.31 -12 -7 -13 4.66 8.55 12 7 13 3.71 5.94 -12 -7 -14 4.61 5.99 12 7 14 7.51 8.41 -12 -7 -15 104.14 22.80 12 7 16 115.68 24.99 -12 -7 -16 132.83 24.28 12 7 17 10.07 9.26 -12 -7 -17 17.25 8.88 12 7 18 15.16 11.40 -12 -7 -18 16.72 9.41 -12 -7 -21 -3.75 6.84 -12 -7 -22 10.40 7.84 -12 -8 6 145.90 23.75 12 8 -5 -6.03 9.60 12 8 -4 34.54 15.01 12 8 -3 27.22 14.16 12 8 -3 24.18 9.60 -12 -8 3 12.68 8.69 12 8 -3 7.60 6.98 12 8 -2 371.99 33.68 12 8 -2 251.42 38.01 12 8 -2 363.92 38.81 -12 -8 2 346.05 38.77 12 8 -1 13.35 6.51 12 8 -1 22.38 9.69 12 8 -1 4.85 9.93 -12 -8 1 31.40 13.02 12 8 0 3.71 7.65 12 8 0 2.71 4.94 12 8 0 4.51 9.26 -12 -8 0 -3.80 6.94 12 8 1 26.13 10.93 12 8 1 46.08 12.26 12 8 1 25.37 11.73 -12 -8 -1 58.29 15.39 12 8 2 482.07 44.90 12 8 2 487.06 40.81 12 8 2 469.67 46.23 -12 -8 -2 396.79 40.95 12 8 3 3.85 6.08 12 8 3 5.65 5.80 12 8 3 3.66 4.75 -12 -8 -3 3.33 6.08 -12 -8 -4 89.93 17.53 12 8 4 70.60 17.20 12 8 4 73.35 16.68 12 8 4 102.10 18.77 12 8 4 69.84 15.49 -12 -8 -5 257.88 29.93 12 8 5 248.19 30.64 12 8 5 255.03 33.87 12 8 5 281.35 31.21 12 8 5 270.47 29.93 -12 -8 -6 319.83 31.93 -12 -8 -6 269.23 37.77 12 8 6 257.07 31.45 12 8 6 193.12 30.12 12 8 6 266.29 29.65 12 8 6 256.50 30.31 -12 -8 -7 135.83 26.37 12 8 7 188.47 26.37 12 8 7 149.27 25.65 12 8 7 151.84 20.81 -12 -8 -7 149.03 16.77 -12 -8 -8 4.89 7.74 12 8 8 -3.66 8.27 12 8 8 7.46 6.03 -12 -8 -8 3.14 4.09 12 8 8 -4.56 7.27 12 8 9 175.64 26.75 12 8 9 196.16 21.85 -12 -8 -9 172.36 17.58 12 8 9 166.23 28.93 12 8 10 362.63 45.09 12 8 10 386.63 41.90 12 8 11 109.98 24.80 -12 -8 -11 141.34 26.94 12 8 11 107.70 21.47 12 8 11 120.20 16.06 12 8 12 30.31 13.97 -12 -8 -12 14.49 11.78 12 8 12 31.21 12.45 12 8 12 40.38 8.65 -12 -8 -13 -4.80 9.79 12 8 13 15.20 10.40 -12 -8 -14 197.87 31.40 -12 -8 -15 92.59 21.19 -12 -8 -16 4.51 7.17 12 8 17 50.55 10.97 -12 -8 -17 35.39 14.21 -12 -8 -18 -4.28 8.79 -12 -8 -20 32.83 13.11 -12 -8 -21 23.37 10.78 -12 -8 -22 3.66 6.70 -12 -9 5 319.83 36.87 12 9 -4 11.54 10.59 -12 -9 4 3.99 10.97 12 9 -3 5.46 10.07 -12 -9 3 4.13 7.55 12 9 -2 15.58 11.69 -12 -9 2 12.73 8.69 -12 -9 2 12.68 9.50 12 9 -2 12.64 6.98 12 9 -2 7.41 6.79 -12 -9 1 379.21 43.19 -12 -9 1 403.25 43.00 12 9 -1 389.90 45.61 12 9 -1 413.80 35.63 12 9 -1 437.17 42.57 12 9 0 36.68 12.21 12 9 0 25.42 10.26 12 9 0 36.53 14.59 -12 -9 0 31.31 13.06 -12 -9 0 43.23 15.35 12 9 1 84.61 18.05 12 9 1 139.06 19.10 12 9 1 144.57 25.04 -12 -9 -1 68.74 19.29 -12 -9 -1 91.12 19.57 12 9 2 51.93 14.54 12 9 2 34.02 10.02 12 9 2 59.29 15.49 -12 -9 -2 28.13 13.02 -12 -9 -2 29.31 11.78 12 9 3 605.07 53.49 -12 -9 -3 640.56 51.55 12 9 3 612.53 47.22 12 9 3 680.70 55.06 -12 -9 -3 659.51 60.95 -12 -9 -4 9.74 8.93 12 9 4 2.80 5.13 12 9 4 11.59 7.93 12 9 4 6.75 6.18 -12 -9 -4 3.18 5.04 -12 -9 -5 152.79 28.27 12 9 5 215.55 25.32 12 9 5 144.09 24.66 12 9 5 129.84 21.05 -12 -9 -5 131.65 21.43 -12 -9 -6 11.92 6.70 -12 -9 -6 4.99 6.46 12 9 6 18.72 10.31 12 9 6 12.49 10.78 12 9 6 2.80 4.51 12 9 6 12.35 6.94 -12 -9 -7 394.89 29.17 -12 -9 -7 386.58 45.75 12 9 7 399.69 41.19 12 9 7 331.94 41.38 12 9 7 389.62 34.68 12 9 7 384.34 38.29 -12 -9 -8 115.97 25.13 12 9 8 65.70 17.34 12 9 8 54.87 16.63 12 9 8 117.25 16.63 -12 -9 -8 77.96 11.59 12 9 9 149.60 24.89 12 9 9 141.91 18.58 -12 -9 -9 176.40 17.39 12 9 9 119.25 24.89 12 9 10 4.94 7.84 12 9 10 17.25 6.84 12 9 10 23.99 11.64 12 9 11 755.91 45.51 12 9 11 581.17 60.29 -12 -9 -11 673.58 63.09 12 9 12 16.91 5.99 12 9 12 5.13 8.12 -12 -9 -12 4.94 6.41 12 9 13 9.64 5.04 12 9 13 -5.13 11.54 -12 -9 -13 4.89 7.74 12 9 14 35.06 6.84 12 9 14 30.83 12.54 -12 -9 -14 28.84 12.54 12 9 15 158.96 29.41 -12 -9 -15 160.48 28.89 12 9 16 109.55 12.87 12 9 16 102.33 24.37 -12 -9 -16 106.51 22.57 12 9 17 35.73 15.58 -12 -9 -17 18.10 11.02 -12 -9 -20 76.25 18.91 -12 -9 -21 145.42 25.61 -12 -9 -22 15.25 9.26 -12 -10 4 236.55 32.45 -12 -10 3 76.11 18.05 -12 -10 2 -4.37 6.94 12 10 -2 -3.61 5.75 12 10 -2 -2.38 4.85 12 10 -2 5.18 9.50 -12 -10 1 13.49 10.12 -12 -10 1 8.41 6.70 12 10 -1 -3.61 8.12 12 10 -1 4.75 4.85 12 10 -1 4.89 8.98 -12 -10 0 628.02 55.01 -12 -10 0 578.28 56.82 12 10 0 661.23 59.86 12 10 0 652.25 46.08 12 10 0 558.65 50.93 12 10 1 14.49 8.79 -12 -10 -1 4.75 9.74 -12 -10 -1 7.89 8.08 12 10 1 -4.28 6.79 12 10 1 2.42 5.42 12 10 2 18.24 10.02 -12 -10 -2 -4.85 6.32 -12 -10 -2 11.45 9.26 12 10 2 27.70 12.07 12 10 2 12.35 6.41 12 10 3 -3.71 7.65 -12 -10 -3 9.88 10.17 12 10 3 -3.66 8.17 12 10 3 2.52 4.66 -12 -10 -4 478.79 40.57 12 10 4 381.73 40.81 -12 -10 -4 392.37 47.08 12 10 4 366.72 37.82 12 10 4 361.02 34.49 12 10 5 19.38 8.50 12 10 5 27.65 12.59 -12 -10 -5 30.60 14.06 12 10 5 39.48 11.54 -12 -10 -5 18.10 8.84 12 10 6 53.35 16.11 -12 -10 -6 25.70 12.68 12 10 6 54.92 13.25 12 10 6 76.73 15.25 12 10 7 113.69 20.24 12 10 7 120.96 22.95 -12 -10 -7 108.60 24.23 12 10 7 112.55 17.39 -12 -10 -7 120.24 14.54 12 10 8 1046.52 81.76 -12 -10 -8 1092.89 86.42 12 10 8 1137.74 67.27 -12 -10 -8 1153.18 62.28 12 10 9 20.76 7.55 12 10 9 14.30 8.74 -12 -10 -9 5.18 9.50 12 10 10 145.47 16.49 12 10 10 128.84 26.03 12 10 11 2.71 3.28 12 10 11 5.08 9.36 12 10 12 395.32 25.37 12 10 12 306.05 41.43 -12 -10 -12 322.73 43.28 12 10 13 -2.52 5.56 12 10 13 -5.23 11.73 -12 -10 -13 4.99 6.46 12 10 14 91.03 8.41 12 10 14 104.33 24.75 -12 -10 -14 127.18 25.70 12 10 15 15.58 10.69 -12 -10 -15 19.24 11.73 12 10 16 326.29 44.09 -12 -10 -16 504.83 50.07 12 10 17 5.18 9.45 -12 -10 -17 -4.61 8.46 -12 -10 -19 18.05 10.97 -12 -10 -20 440.17 46.99 -12 -10 -21 -16.72 13.30 -12 -11 4 12.35 8.46 -12 -11 3 266.33 35.11 -12 -11 2 89.17 20.81 -12 -11 1 50.74 15.49 12 11 -1 63.47 15.73 12 11 -1 69.70 13.54 12 11 0 -3.52 4.56 12 11 0 4.42 4.94 -12 -11 0 19.00 9.74 -12 -11 0 8.41 8.65 -12 -11 -1 343.68 39.62 -12 -11 -1 331.80 42.43 12 11 1 398.60 42.52 12 11 1 400.17 39.48 12 11 1 307.14 29.84 12 11 2 39.34 13.21 -12 -11 -2 19.95 11.31 -12 -11 -2 39.53 12.64 12 11 2 23.56 11.50 12 11 2 39.15 10.02 12 11 3 3.66 6.70 -12 -11 -3 15.25 11.45 12 11 3 -3.61 7.41 12 11 3 4.75 4.37 12 11 4 -3.75 6.84 -12 -11 -4 -5.18 8.22 12 11 4 3.28 6.75 12 11 4 2.47 5.56 12 11 5 214.17 25.94 12 11 5 279.26 33.87 -12 -11 -5 345.15 42.71 12 11 5 288.85 30.93 -12 -11 -5 242.82 28.41 12 11 6 162.05 22.47 12 11 6 157.73 26.27 -12 -11 -6 179.25 30.93 12 11 6 185.57 22.76 -12 -11 -6 134.21 16.11 12 11 7 45.13 12.78 12 11 7 38.29 13.11 -12 -11 -7 52.92 17.63 12 11 7 41.90 10.45 -12 -11 -7 52.83 9.36 12 11 8 4.51 8.27 -12 -11 -8 5.27 8.41 12 11 8 9.98 5.18 -12 -11 -8 15.20 5.75 12 11 9 290.33 24.51 12 11 9 298.92 39.05 -12 -11 -9 232.32 35.92 12 11 10 19.48 5.37 12 11 10 -4.94 7.89 -12 -11 -10 15.73 12.73 12 11 11 220.92 16.72 12 11 11 215.83 34.30 12 11 12 -5.23 6.79 -12 -11 -13 313.37 40.95 12 11 13 301.68 41.29 -12 -11 -14 9.98 9.12 12 11 14 -5.32 8.41 -12 -11 -15 122.43 25.42 12 11 15 95.02 24.18 -12 -11 -16 -4.80 12.45 12 11 16 21.00 13.63 12 11 17 73.50 21.71 12 11 17 99.34 22.80 12 11 18 22.38 13.63 -12 -11 -19 87.80 22.00 12 11 19 99.63 24.13 -12 -11 -20 -4.47 9.17 -12 -12 3 38.91 13.83 -12 -12 2 81.19 19.72 12 12 -1 55.06 14.97 -12 -12 1 46.80 16.77 12 12 0 6.89 6.32 12 12 0 9.98 5.80 -12 -12 0 24.18 13.30 12 12 1 -3.47 4.47 12 12 1 2.04 3.75 -12 -12 -1 9.93 9.12 12 12 2 316.03 28.70 12 12 2 304.20 34.25 -12 -12 -2 351.37 43.95 12 12 3 87.61 14.49 -12 -12 -3 83.14 22.19 12 12 3 113.69 20.48 12 12 4 6.89 6.32 -12 -12 -4 15.82 10.83 12 12 4 -3.66 11.12 12 12 5 2.42 6.65 -12 -12 -5 5.32 8.50 12 12 5 3.80 6.94 12 12 6 253.51 27.75 -12 -12 -6 279.64 39.10 12 12 6 336.88 37.77 12 12 7 85.04 17.48 -12 -12 -7 161.86 29.65 12 12 7 125.00 23.09 12 12 8 -3.09 7.51 -12 -12 -8 -5.37 11.07 12 12 8 8.88 9.07 -12 -12 -9 -5.37 11.02 12 12 9 -4.70 7.46 -12 -12 -10 559.27 57.82 12 12 10 588.87 57.25 -12 -12 -11 47.41 16.25 12 12 11 82.47 21.28 12 12 12 26.51 13.78 -12 -12 -13 30.83 14.21 12 12 13 37.58 17.10 -12 -12 -14 161.86 29.98 12 12 14 123.90 26.84 12 12 15 24.23 13.63 -12 -12 -15 14.92 11.21 12 12 15 5.37 8.55 12 12 16 72.12 21.62 12 12 16 80.15 21.05 12 12 17 -5.99 7.74 12 12 17 -5.32 6.89 -12 -12 -18 164.47 29.08 12 12 18 200.96 34.30 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26.65 13 2 6 179.68 22.00 -13 -2 -6 165.28 28.70 13 2 6 138.39 23.94 13 2 6 152.31 27.79 13 2 7 33.40 10.12 -13 -2 -7 66.89 19.19 13 2 7 36.49 13.54 13 2 7 36.77 14.06 13 2 8 146.33 26.18 -13 -2 -8 126.52 24.89 13 2 8 116.68 18.91 13 2 9 145.09 27.41 -13 -2 -9 205.28 31.21 13 2 9 208.37 24.51 13 2 10 34.63 14.35 -13 -2 -10 13.21 9.07 13 2 10 16.20 8.22 13 2 11 191.74 31.55 13 2 11 162.24 22.19 13 2 12 343.87 44.33 13 2 12 398.41 36.39 13 2 13 37.29 11.59 13 2 13 46.84 16.63 -13 -2 -14 30.36 12.68 13 2 14 40.86 12.07 13 2 14 36.77 14.54 -13 -2 -15 8.60 9.64 13 2 15 -10.59 16.11 -13 -2 -16 105.28 21.71 13 2 16 122.90 26.37 -13 -2 -17 4.09 7.46 -13 -2 -18 54.44 15.73 -13 -2 -19 14.59 10.02 13 3 -6 135.83 22.57 -13 -3 5 66.04 17.91 13 3 -5 36.20 12.59 13 3 -4 5.84 9.31 -13 -3 4 -3.75 5.94 13 3 -4 3.61 6.60 13 3 -3 11.21 10.31 -13 -3 3 14.35 9.88 13 3 -3 21.43 10.36 13 3 -3 12.97 10.50 13 3 -2 226.14 35.44 13 3 -2 249.28 31.59 13 3 -2 269.99 35.54 -13 -3 2 344.20 35.77 13 3 -1 138.87 22.90 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696.67 63.57 13 4 10 605.59 50.41 13 4 11 154.55 29.74 13 4 11 135.97 22.00 13 4 12 47.08 17.34 13 4 12 6.41 6.60 13 4 13 264.67 38.29 13 4 13 309.33 33.73 -13 -4 -13 272.46 36.49 13 4 14 708.88 66.89 13 4 14 710.35 55.21 -13 -4 -14 624.88 59.53 -13 -4 -15 13.63 10.21 13 4 15 3.33 6.08 13 4 15 5.37 9.83 -13 -4 -16 17.82 10.83 13 4 16 16.15 12.11 -13 -4 -17 17.29 10.55 -13 -4 -18 29.12 12.11 -13 -4 -19 39.53 13.68 -13 -4 -20 14.82 9.64 13 5 -5 44.14 14.40 -13 -5 4 252.08 33.07 13 5 -4 272.18 31.21 13 5 -3 216.64 31.07 -13 -5 3 168.47 26.51 13 5 -3 141.67 29.65 13 5 -3 260.44 29.88 13 5 -2 -4.23 5.46 13 5 -2 3.33 6.84 13 5 -2 -5.37 6.98 -13 -5 2 3.75 5.99 13 5 -1 100.62 20.71 13 5 -1 76.68 17.48 13 5 -1 92.45 22.95 -13 -5 1 105.09 19.76 13 5 0 54.40 15.92 13 5 0 36.82 12.02 13 5 0 19.62 12.83 -13 -5 0 69.60 15.73 13 5 1 129.60 22.85 13 5 1 77.44 17.82 13 5 1 125.66 26.03 -13 -5 -1 123.76 20.86 13 5 2 181.01 29.60 13 5 2 168.66 27.27 13 5 2 173.55 25.08 13 5 3 288.66 36.06 13 5 3 243.43 33.45 13 5 3 248.85 30.74 13 5 4 522.55 49.46 13 5 4 524.16 50.83 13 5 4 505.63 46.32 13 5 5 -3.71 4.80 13 5 5 14.49 8.79 13 5 5 3.14 5.75 13 5 6 20.86 9.60 13 5 6 30.03 11.45 13 5 6 15.87 8.79 -13 -5 -7 249.61 36.91 13 5 7 176.30 24.99 13 5 7 159.20 25.32 13 5 7 172.65 24.51 -13 -5 -8 67.56 18.62 13 5 8 48.46 13.44 -13 -5 -9 55.59 18.05 13 5 9 36.06 12.16 13 5 10 5.08 9.36 13 5 10 6.65 9.17 13 5 11 499.41 55.06 13 5 11 632.43 51.12 -13 -5 -12 162.05 29.50 13 5 12 221.53 28.79 13 5 12 184.90 31.69 -13 -5 -13 38.05 14.49 13 5 13 20.71 10.55 13 5 13 16.01 12.02 -13 -5 -14 18.91 9.74 13 5 14 38.29 11.97 13 5 14 16.11 12.11 -13 -5 -15 139.68 26.94 13 5 15 124.09 26.32 -13 -5 -16 -4.56 8.41 13 5 16 -10.83 11.12 -13 -5 -17 4.47 7.08 -13 -5 -18 4.28 7.84 -13 -5 -19 131.08 24.42 13 6 -4 41.95 13.35 13 6 -4 48.22 19.24 13 6 -3 389.43 38.39 13 6 -3 367.00 47.18 13 6 -3 391.00 42.52 -13 -6 3 367.10 41.09 13 6 -2 8.36 6.65 13 6 -2 6.41 7.22 -13 -6 2 3.94 7.22 13 6 -2 5.42 7.08 13 6 -1 4.18 6.60 13 6 -1 3.23 5.08 13 6 -1 -5.13 8.17 -13 -6 1 -3.80 7.79 13 6 0 145.19 25.32 13 6 0 125.99 20.90 13 6 0 141.39 26.32 -13 -6 0 127.51 22.66 13 6 1 24.94 11.59 13 6 1 48.74 13.78 13 6 1 60.15 18.10 -13 -6 -1 59.67 15.20 13 6 2 4.18 8.60 13 6 2 19.76 8.55 13 6 2 13.21 9.88 -13 -6 -2 10.12 7.60 13 6 3 8.31 8.55 13 6 3 20.14 9.26 13 6 3 12.73 10.31 13 6 4 255.26 32.21 13 6 4 209.09 27.94 13 6 4 207.23 30.60 13 6 5 72.93 16.58 13 6 5 81.14 18.01 13 6 5 127.42 21.66 13 6 5 114.88 22.57 13 6 6 3.37 4.37 13 6 6 -3.47 5.46 13 6 6 3.66 8.27 13 6 6 4.51 8.31 13 6 7 -3.37 4.42 13 6 7 -3.23 7.22 13 6 7 -3.80 7.84 13 6 7 4.70 7.46 13 6 8 195.88 26.94 13 6 8 195.97 25.80 13 6 9 187.94 26.89 13 6 9 203.29 24.61 13 6 10 116.54 20.86 13 6 11 35.68 12.78 -13 -6 -11 44.23 18.67 -13 -6 -12 245.48 34.73 13 6 12 173.36 25.75 -13 -6 -13 -4.89 10.02 13 6 13 -3.66 5.80 13 6 13 -5.37 13.06 -13 -6 -14 48.41 16.15 13 6 14 43.28 15.82 -13 -6 -15 9.55 9.79 13 6 15 -5.42 11.12 -13 -6 -16 60.81 17.86 13 6 16 48.93 18.15 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36.25 15.06 13 7 10 14.92 8.46 -13 -7 -10 25.32 14.73 13 7 10 23.09 8.22 13 7 11 79.29 17.63 -13 -7 -11 81.00 21.05 13 7 11 74.11 14.78 -13 -7 -12 116.25 24.61 -13 -7 -13 311.13 41.00 -13 -7 -14 -4.94 9.12 -13 -7 -15 -4.89 8.98 -13 -7 -16 23.90 12.45 13 7 16 10.93 10.07 -13 -7 -17 135.11 25.23 -13 -7 -18 9.03 11.73 -13 -7 -19 8.69 7.98 -13 -7 -21 162.72 26.22 13 8 -3 20.52 9.36 13 8 -3 23.47 15.25 13 8 -2 8.79 7.13 13 8 -2 8.12 6.46 13 8 -2 5.51 10.17 -13 -8 1 343.77 39.43 13 8 -1 325.91 33.30 13 8 -1 287.85 41.05 13 8 -1 320.30 37.67 13 8 0 12.16 9.12 13 8 0 8.88 8.17 13 8 0 9.88 12.02 -13 -8 0 15.82 10.26 13 8 1 28.51 11.92 13 8 1 44.99 12.40 13 8 1 51.26 16.68 -13 -8 -1 42.09 14.59 13 8 2 41.05 13.21 13 8 2 48.70 13.54 13 8 2 52.26 15.58 -13 -8 -2 47.89 14.87 13 8 3 730.02 60.91 13 8 3 676.81 53.49 13 8 3 780.04 62.28 13 8 4 55.40 16.30 13 8 4 57.53 13.97 13 8 4 57.34 15.87 13 8 5 4.37 6.98 13 8 5 26.56 10.12 13 8 5 10.74 8.03 13 8 6 94.68 20.90 13 8 6 70.27 16.25 13 8 6 65.85 16.53 13 8 7 201.15 31.64 13 8 7 192.74 28.46 -13 -8 -7 256.55 37.48 13 8 7 293.27 31.07 13 8 8 19.48 10.97 -13 -8 -8 31.07 13.49 13 8 8 26.03 9.64 13 8 9 15.16 10.36 13 8 9 5.37 7.41 13 8 10 297.07 40.67 13 8 10 276.03 28.36 13 8 11 422.16 48.79 13 8 11 361.54 31.55 13 8 12 65.28 20.81 -13 -8 -12 51.83 18.05 13 8 12 86.13 14.11 13 8 13 38.43 16.01 -13 -8 -13 25.65 12.54 13 8 13 35.06 9.03 -13 -8 -14 111.55 24.18 -13 -8 -15 94.73 22.76 -13 -8 -16 97.68 22.80 -13 -8 -17 71.41 19.29 -13 -8 -18 27.75 12.78 -13 -8 -19 80.38 20.76 -13 -8 -21 29.50 13.44 -13 -9 4 248.80 32.83 -13 -9 3 4.23 7.74 13 9 -3 -5.89 13.25 13 9 -2 27.98 12.21 13 9 -2 27.75 10.21 -13 -9 2 17.44 12.07 13 9 -2 39.15 18.53 13 9 -1 3.99 6.32 13 9 -1 2.80 5.70 -13 -9 1 8.98 7.13 13 9 -1 -5.32 6.89 13 9 0 196.64 24.75 13 9 0 203.81 29.46 -13 -9 0 175.54 29.12 -13 -9 0 188.80 28.74 13 9 1 3.99 5.23 13 9 1 5.70 5.84 13 9 1 4.66 11.31 -13 -9 -1 -4.75 7.55 13 9 2 -4.04 8.31 13 9 2 -5.80 5.94 13 9 2 4.37 8.03 -13 -9 -2 4.85 6.32 13 9 3 45.32 14.25 13 9 3 47.56 12.64 13 9 3 28.55 12.54 -13 -9 -3 49.74 15.92 13 9 4 569.68 54.30 13 9 4 620.84 49.60 13 9 4 654.76 55.01 -13 -9 -4 614.19 60.29 13 9 5 43.33 14.40 13 9 5 19.15 8.36 13 9 5 17.53 9.69 -13 -9 -5 41.29 15.01 13 9 6 85.14 20.38 13 9 6 63.61 15.68 13 9 6 87.61 17.86 -13 -9 -6 57.63 18.24 13 9 7 23.28 12.83 13 9 7 31.78 12.59 13 9 7 14.92 9.93 -13 -9 -7 21.19 12.87 13 9 8 467.01 52.02 13 9 8 555.71 49.31 -13 -9 -8 533.71 56.01 13 9 8 498.94 42.43 13 9 9 -5.08 11.40 -13 -9 -9 16.11 11.02 13 9 9 12.64 6.98 13 9 10 125.76 26.03 13 9 10 131.84 18.81 13 9 11 199.30 33.78 13 9 11 233.08 23.99 13 9 12 368.14 47.75 13 9 12 471.67 35.44 13 9 13 5.56 8.84 -13 -9 -13 5.23 9.64 13 9 13 5.18 4.75 13 9 14 44.61 17.01 -13 -9 -14 46.51 17.15 13 9 14 31.31 7.74 13 9 15 -5.56 10.21 -13 -9 -15 -5.08 9.31 13 9 15 8.60 4.89 13 9 16 472.66 53.87 -13 -9 -16 472.14 51.26 -13 -9 -17 68.08 19.15 -13 -9 -18 56.77 17.53 -13 -10 4 4.13 6.56 -13 -10 3 365.20 41.62 13 10 -2 15.73 10.21 -13 -10 2 8.88 10.02 13 10 -2 23.47 8.65 13 10 -2 16.72 12.54 13 10 -1 20.95 9.41 13 10 -1 58.72 15.30 -13 -10 1 27.60 12.73 13 10 -1 47.70 17.58 13 10 0 19.62 10.26 13 10 0 23.75 8.46 13 10 0 30.03 14.54 -13 -10 0 28.41 13.06 13 10 1 55.25 15.01 13 10 1 34.92 10.31 13 10 1 37.48 14.97 -13 -10 -1 34.11 14.92 -13 -10 -1 32.97 12.64 13 10 2 -3.99 6.32 13 10 2 -2.76 4.37 13 10 2 8.74 10.59 -13 -10 -2 -4.99 9.17 13 10 3 5.65 6.32 13 10 3 -8.12 10.55 -13 -10 -3 -5.13 8.12 13 10 4 4.13 6.60 13 10 4 5.84 6.60 13 10 4 11.21 7.70 -13 -10 -4 15.68 11.73 13 10 5 539.03 52.78 13 10 5 587.73 47.18 13 10 5 593.19 49.65 -13 -10 -5 468.29 53.54 13 10 6 4.42 5.75 13 10 6 -6.41 8.31 13 10 6 -3.18 6.46 -13 -10 -6 5.42 8.55 13 10 7 18.43 12.02 13 10 7 20.43 9.41 13 10 7 28.60 10.55 -13 -10 -7 54.49 17.34 13 10 8 4.85 6.27 13 10 8 -3.61 8.12 -13 -10 -8 -5.46 8.69 13 10 8 -2.57 5.27 13 10 9 571.96 59.43 -13 -10 -9 537.89 59.67 13 10 10 -5.27 13.63 13 10 10 2.04 3.75 13 10 11 363.20 45.51 13 10 11 313.60 27.08 13 10 12 72.17 20.67 -13 -10 -12 64.85 19.53 13 10 12 94.83 12.49 13 10 13 489.29 54.40 -13 -10 -13 416.56 50.17 13 10 13 482.97 31.26 13 10 14 158.06 31.26 13 10 14 185.14 16.01 13 10 15 28.22 15.63 -13 -10 -15 67.13 18.43 13 10 16 5.61 8.93 -13 -10 -16 15.20 11.40 -13 -10 -17 267.52 37.82 -13 -10 -18 4.80 11.69 -13 -11 3 4.32 7.93 -13 -11 2 230.04 33.02 13 11 -1 3.85 9.31 -13 -11 1 -4.70 9.60 13 11 -1 16.96 7.70 13 11 0 46.70 11.16 13 11 0 26.89 11.78 -13 -11 0 29.03 13.40 13 11 1 3.85 7.13 13 11 1 15.01 7.27 -13 -11 -1 4.99 7.93 13 11 1 4.66 8.55 13 11 2 226.24 26.13 13 11 2 328.47 36.30 13 11 2 238.87 33.73 -13 -11 -2 277.02 39.19 13 11 3 -3.99 7.32 13 11 3 2.66 4.85 13 11 3 -4.04 9.79 -13 -11 -3 5.27 6.79 13 11 4 20.38 10.69 13 11 4 55.06 12.49 13 11 4 40.76 14.92 -13 -11 -4 37.53 16.39 13 11 5 -4.23 6.70 13 11 5 -2.90 8.79 13 11 5 -3.37 5.37 -13 -11 -5 -5.46 10.02 13 11 6 366.86 42.38 13 11 6 393.32 37.15 13 11 6 353.94 35.68 -13 -11 -6 320.16 43.95 13 11 7 4.56 7.27 13 11 7 -3.23 8.93 13 11 7 2.71 4.99 -13 -11 -7 5.56 7.22 13 11 8 57.39 17.25 13 11 8 55.59 14.92 -13 -11 -8 61.52 19.43 13 11 8 95.92 15.35 13 11 9 60.34 18.58 -13 -11 -9 72.78 20.00 13 11 9 37.29 8.93 13 11 10 241.72 36.58 -13 -11 -10 201.06 35.44 13 11 10 303.39 24.99 13 11 11 16.34 11.16 13 11 11 6.89 4.75 13 11 12 -5.61 8.88 13 11 12 2.95 2.57 13 11 13 22.76 12.78 -13 -11 -13 5.42 12.21 13 11 13 10.78 2.42 13 11 14 108.75 25.18 -13 -11 -14 133.45 27.32 13 11 15 11.45 11.78 -13 -11 -15 31.55 14.49 13 11 16 159.68 31.55 -13 -11 -16 216.40 33.35 -13 -11 -17 5.04 10.31 13 12 -1 209.66 28.41 -13 -12 1 137.11 26.65 13 12 0 18.77 10.36 -13 -12 0 9.79 10.07 13 12 1 105.52 16.34 13 12 1 90.69 18.72 -13 -12 -1 60.76 18.96 13 12 2 -3.80 6.08 13 12 2 2.38 4.32 -13 -12 -2 5.23 9.55 13 12 3 287.81 29.27 13 12 3 388.95 40.10 -13 -12 -3 309.85 42.33 13 12 4 3.99 8.17 13 12 4 5.13 5.75 -13 -12 -4 -5.46 8.69 13 12 5 16.49 12.02 13 12 5 26.98 8.98 -13 -12 -5 38.86 16.15 13 12 6 4.28 5.56 13 12 6 -2.85 8.31 13 12 6 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321.82 35.49 -14 -1 3 -3.37 7.55 14 1 -2 64.90 17.10 -14 -1 2 32.12 11.12 14 1 -2 23.61 14.40 14 1 -1 -4.61 8.46 14 1 -1 4.04 5.27 14 1 -1 5.70 10.45 -14 -1 1 -3.04 4.85 14 1 0 45.89 16.53 14 1 0 93.40 19.91 14 1 0 49.03 16.82 -14 -1 0 81.24 15.54 14 1 1 20.81 13.59 14 1 1 27.46 11.92 14 1 1 36.63 12.97 14 1 2 4.99 9.17 14 1 2 9.17 9.41 14 1 2 4.09 6.51 14 1 3 57.20 18.29 14 1 3 82.95 19.62 14 1 3 78.29 18.39 14 1 4 86.61 20.57 14 1 4 116.40 22.71 14 1 4 125.38 24.51 14 1 5 71.64 17.86 14 1 5 37.53 14.44 14 1 6 4.28 6.84 14 1 6 4.75 7.55 14 1 7 53.16 17.34 14 1 8 83.90 21.66 14 1 8 105.90 16.30 14 1 9 10.07 9.26 -14 -1 -9 9.55 9.79 14 1 10 -5.18 9.45 -14 -1 -10 4.61 8.46 14 1 11 5.27 10.78 14 1 12 396.55 47.89 14 1 13 -5.46 9.98 -14 -1 -15 18.01 10.12 -14 -1 -16 119.25 23.47 -14 -1 -17 4.28 7.84 -14 -1 -18 28.65 12.49 -14 -2 4 3.66 8.27 14 2 -3 383.16 41.62 -14 -2 3 413.33 40.67 14 2 -2 47.41 14.73 -14 -2 2 71.26 16.68 14 2 -2 88.18 23.04 14 2 -1 308.81 37.77 14 2 -1 328.90 44.99 14 2 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606.54 55.25 14 3 1 5.18 8.22 14 3 2 315.22 41.43 14 3 2 324.48 37.20 14 3 3 60.86 19.43 14 3 3 71.26 17.63 14 3 4 89.13 20.38 14 3 4 80.00 18.72 14 3 4 93.50 21.76 14 3 5 21.19 12.30 14 3 5 8.17 8.36 14 3 5 4.75 9.74 14 3 6 350.42 40.76 14 3 6 414.61 46.75 14 3 6 401.21 42.95 14 3 7 39.29 15.73 14 3 7 34.25 14.25 14 3 7 45.80 12.45 14 3 8 407.81 46.56 14 3 8 360.12 41.81 14 3 8 293.70 32.12 14 3 9 111.65 18.77 14 3 9 87.84 21.62 14 3 10 232.70 27.13 14 3 10 169.13 31.55 14 3 11 3.04 7.89 14 3 12 142.05 21.66 14 3 12 142.86 28.27 14 3 13 22.33 14.49 14 3 14 327.52 44.75 -14 -3 -14 383.44 44.61 -14 -3 -15 56.96 17.58 -14 -3 -16 28.03 12.16 -14 -3 -17 -4.56 7.22 -14 -3 -18 30.60 12.73 -14 -3 -19 4.13 7.60 14 4 -3 70.65 17.01 -14 -4 3 73.54 17.67 -14 -4 2 56.06 14.68 14 4 -2 48.41 14.63 14 4 -2 35.01 17.86 -14 -4 1 43.14 14.11 14 4 -1 22.42 14.63 14 4 -1 52.31 14.25 14 4 0 118.15 24.09 -14 -4 0 138.39 23.14 14 4 0 161.62 25.46 14 4 1 40.95 14.49 -14 -4 -1 16.58 10.12 14 4 1 10.31 9.50 14 4 1 30.22 14.30 14 4 2 14.68 9.03 14 4 2 11.40 7.84 14 4 3 364.39 43.14 14 4 3 297.78 36.06 14 4 4 163.48 28.36 14 4 4 117.49 22.00 14 4 5 25.13 12.26 14 4 5 56.06 15.68 14 4 6 19.86 10.93 14 4 6 8.22 10.69 14 4 7 432.23 40.05 14 4 7 417.70 42.76 14 4 7 503.88 51.36 14 4 7 392.61 43.71 14 4 8 106.51 23.99 14 4 8 78.20 19.43 14 4 8 78.29 16.63 14 4 9 79.01 16.82 14 4 9 109.46 24.66 14 4 10 12.83 8.84 14 4 10 5.32 8.50 14 4 11 410.14 40.19 14 4 11 496.23 53.87 14 4 12 9.93 7.46 14 4 12 16.68 11.40 14 4 13 67.65 21.57 -14 -4 -13 74.21 20.10 14 4 13 93.50 18.20 14 4 14 5.70 9.07 -14 -4 -14 19.67 11.07 -14 -4 -15 195.02 31.45 -14 -4 -16 4.80 7.60 -14 -4 -17 -4.66 8.55 -14 -4 -18 4.51 7.17 -14 -4 -19 107.32 22.38 -14 -4 -20 4.04 6.46 14 5 -3 25.23 11.02 -14 -5 2 35.11 12.54 14 5 -2 46.75 13.73 14 5 -2 75.59 20.76 -14 -5 1 3.75 8.46 14 5 -1 5.61 8.88 14 5 -1 3.61 8.12 14 5 0 180.63 29.65 -14 -5 0 210.61 28.36 14 5 0 191.79 33.16 14 5 0 204.00 28.03 14 5 1 58.77 16.68 -14 -5 -1 34.92 12.11 14 5 1 56.16 17.01 14 5 1 40.38 13.63 14 5 2 4.89 6.32 14 5 2 -3.71 6.79 14 5 2 -4.56 5.89 14 5 3 9.26 9.50 14 5 3 11.31 9.79 14 5 3 4.61 8.46 14 5 4 30.79 13.49 14 5 4 42.19 13.73 14 5 4 37.34 14.30 14 5 5 149.03 25.27 14 5 5 161.96 26.65 14 5 6 61.62 14.59 14 5 6 68.55 18.01 14 5 6 94.02 19.57 14 5 7 3.33 6.79 14 5 7 4.13 6.60 14 5 7 -3.71 7.60 14 5 8 337.07 35.92 14 5 8 304.10 38.34 14 5 8 409.33 39.34 14 5 9 64.18 16.06 14 5 10 21.57 14.82 14 5 10 10.31 9.45 14 5 11 38.53 15.20 14 5 11 13.92 11.07 14 5 12 308.33 41.62 -14 -5 -12 239.49 35.44 14 5 12 239.11 30.83 14 5 13 17.06 14.78 -14 -5 -13 5.08 10.45 14 5 14 -5.75 9.12 -14 -5 -14 5.04 6.56 -14 -5 -15 4.99 6.51 -14 -5 -16 352.89 43.42 -14 -5 -17 4.80 8.79 -14 -5 -18 13.87 8.50 -14 -5 -19 4.42 8.12 -14 -5 -20 176.54 28.55 14 6 -4 3.47 7.79 14 6 -3 79.81 17.48 14 6 -2 269.80 41.48 14 6 -2 263.39 31.93 -14 -6 1 31.40 12.02 14 6 -1 22.38 12.64 14 6 -1 27.89 12.02 14 6 0 17.91 10.07 -14 -6 0 22.76 11.02 14 6 0 37.25 16.91 14 6 0 3.52 8.55 14 6 1 76.44 19.10 -14 -6 -1 76.87 17.06 14 6 1 76.01 20.48 14 6 1 49.69 14.49 14 6 2 106.37 22.38 14 6 2 46.65 13.87 14 6 2 81.38 19.67 14 6 3 92.02 20.57 14 6 3 80.48 17.82 14 6 3 96.20 20.95 14 6 4 69.70 18.48 14 6 4 40.95 13.44 14 6 4 60.57 18.29 14 6 5 8.27 8.46 14 6 5 15.30 10.55 14 6 5 9.50 10.69 14 6 6 314.65 37.58 14 6 6 315.69 37.20 14 6 6 397.93 45.04 14 6 7 12.21 8.36 14 6 7 -4.99 11.16 14 6 8 59.01 17.10 14 6 8 68.65 16.58 14 6 9 193.65 27.32 14 6 9 212.89 27.51 14 6 10 9.12 7.36 -14 -6 -11 5.23 6.79 -14 -6 -12 52.31 17.44 14 6 13 418.98 51.55 -14 -6 -13 428.05 49.84 14 6 14 81.10 24.70 -14 -6 -14 108.75 24.09 -14 -6 -15 5.13 9.36 -14 -6 -16 40.10 15.35 -14 -6 -17 117.44 24.70 -14 -6 -19 4.56 5.94 14 7 -3 -3.33 6.79 14 7 -2 65.18 21.14 14 7 -2 36.63 12.73 14 7 -1 433.18 50.93 14 7 -1 368.10 38.01 14 7 0 31.02 13.54 -14 -7 0 23.75 11.50 14 7 0 37.44 15.54 14 7 0 6.75 9.83 14 7 1 -4.47 8.17 -14 -7 -1 -3.80 7.03 14 7 1 3.42 6.27 14 7 1 10.12 9.26 14 7 2 53.83 16.58 14 7 2 65.89 15.06 14 7 2 33.49 13.35 14 7 3 313.94 39.05 14 7 3 325.62 35.63 14 7 3 313.75 39.72 14 7 4 9.26 7.36 14 7 4 21.71 10.50 14 7 4 4.32 7.93 14 7 5 -4.75 9.69 14 7 5 3.71 7.65 14 7 5 4.09 6.46 14 7 6 164.71 27.98 14 7 6 99.96 21.33 14 7 6 157.35 25.32 14 7 7 258.68 37.82 14 7 7 347.67 38.86 14 7 7 339.21 36.91 14 7 8 66.89 19.19 14 7 8 70.41 18.53 14 7 8 104.61 18.91 14 7 9 236.21 29.03 14 7 9 186.04 32.16 14 7 10 114.88 19.67 14 7 10 109.41 24.89 -14 -7 -10 59.05 18.81 -14 -7 -11 209.80 35.06 14 7 11 220.63 25.99 -14 -7 -12 26.89 14.06 14 7 12 51.74 11.78 -14 -7 -13 42.81 17.10 -14 -7 -14 169.51 31.93 -14 -7 -15 130.55 27.27 -14 -7 -16 5.13 8.12 -14 -7 -17 109.98 24.70 -14 -7 -18 4.85 10.88 14 8 -3 88.75 17.86 14 8 -2 -3.18 5.84 14 8 -1 16.96 13.73 14 8 -1 9.60 7.74 14 8 0 193.36 33.54 14 8 0 219.77 27.98 14 8 1 17.63 9.88 -14 -8 -1 -3.99 13.16 14 8 1 13.11 9.03 14 8 1 -5.08 8.03 14 8 2 -4.42 7.08 14 8 2 3.33 6.13 14 8 2 -4.80 6.22 14 8 3 13.49 12.45 14 8 3 23.85 10.40 14 8 3 40.52 14.92 14 8 4 211.56 32.40 14 8 4 251.99 31.21 14 8 4 271.13 34.78 14 8 5 94.26 22.19 14 8 5 133.07 22.47 14 8 5 131.79 23.42 14 8 6 48.36 16.72 14 8 6 63.90 16.34 14 8 6 44.85 13.87 14 8 7 189.18 31.26 -14 -8 -7 145.85 29.08 14 8 7 239.44 30.07 14 8 7 159.44 26.60 14 8 8 555.76 58.39 -14 -8 -8 643.50 62.76 14 8 8 605.36 55.87 14 8 8 767.74 55.59 14 8 9 31.97 15.58 14 8 9 76.44 19.19 14 8 9 46.13 13.68 14 8 10 42.76 12.11 14 8 10 38.48 16.06 14 8 11 28.98 9.45 14 8 11 39.53 16.44 -14 -8 -11 22.14 13.49 14 8 12 399.22 34.21 14 8 12 357.07 46.70 -14 -8 -12 270.04 41.95 14 8 13 6.84 6.27 14 8 13 17.53 13.16 -14 -8 -13 5.46 10.02 -14 -8 -14 48.70 17.39 14 8 14 74.16 13.06 -14 -8 -15 37.29 14.78 -14 -8 -16 229.85 35.92 -14 -8 -17 15.30 10.50 14 9 -2 42.09 11.50 14 9 -1 91.22 24.28 14 9 -1 94.11 18.05 14 9 0 96.87 23.04 14 9 0 101.29 18.72 14 9 1 104.33 21.71 -14 -9 -1 68.65 19.38 14 9 1 71.07 20.57 14 9 1 74.92 16.06 14 9 2 -4.37 6.98 -14 -9 -2 10.07 9.26 14 9 2 -9.55 13.16 14 9 2 3.18 7.17 14 9 3 -4.47 7.08 -14 -9 -3 -5.18 11.59 14 9 3 4.47 8.22 14 9 3 -3.28 6.70 14 9 4 9.12 8.36 -14 -9 -4 5.27 6.84 14 9 4 4.18 6.65 14 9 4 3.37 6.18 14 9 5 634.15 58.91 -14 -9 -5 645.40 62.14 14 9 5 624.88 54.59 14 9 5 557.80 49.60 14 9 6 71.98 19.48 -14 -9 -6 43.76 16.96 14 9 6 101.95 20.05 14 9 6 101.34 19.34 14 9 7 -4.94 9.07 -14 -9 -7 -5.56 7.17 14 9 7 6.79 6.94 14 9 7 -3.75 7.74 14 9 8 25.70 12.49 -14 -9 -8 16.82 11.50 14 9 8 18.91 8.69 14 9 8 7.93 9.64 14 9 9 282.91 39.76 -14 -9 -9 270.99 40.52 14 9 9 253.51 34.87 14 9 9 300.44 31.83 14 9 10 -10.74 9.55 14 9 10 5.51 11.35 14 9 11 2.47 5.56 14 9 11 -5.70 10.40 14 9 12 83.71 14.25 14 9 12 58.10 19.43 -14 -9 -12 61.90 18.86 14 9 13 438.31 33.92 14 9 13 330.61 46.23 -14 -9 -13 385.15 48.60 14 9 14 13.11 6.70 14 9 14 11.92 10.93 -14 -9 -14 11.02 12.40 -14 -9 -15 10.83 9.98 -14 -9 -16 85.09 22.14 14 10 -1 20.00 8.69 14 10 -1 5.70 12.78 14 10 0 170.60 23.18 14 10 0 204.95 34.44 14 10 1 17.10 9.60 14 10 1 15.25 11.45 14 10 1 8.84 6.65 14 10 2 121.05 24.04 -14 -10 -2 143.95 29.41 14 10 2 142.86 27.36 14 10 2 202.39 25.32 14 10 3 4.37 8.03 -14 -10 -3 5.27 8.41 14 10 3 -8.93 12.26 14 10 3 6.22 6.37 14 10 4 121.24 23.85 -14 -10 -4 145.85 28.08 14 10 4 120.53 22.80 14 10 4 105.56 19.48 14 10 5 4.61 7.32 -14 -10 -5 -5.51 12.40 14 10 5 3.85 6.13 14 10 5 9.98 8.65 14 10 6 270.70 36.53 -14 -10 -6 162.76 32.07 14 10 6 277.64 32.40 14 10 6 243.10 30.41 14 10 7 4.94 9.03 -14 -10 -7 5.70 7.41 14 10 7 -3.28 6.70 14 10 7 -3.66 9.45 14 10 8 -5.08 8.12 -14 -10 -8 5.75 10.55 14 10 8 -2.99 3.85 14 10 8 -3.85 9.36 14 10 9 31.97 14.73 -14 -10 -9 40.43 16.82 14 10 9 45.89 11.69 14 10 9 24.28 11.26 14 10 10 264.48 26.84 -14 -10 -10 260.25 38.72 14 10 11 6.51 5.99 14 10 11 -5.70 11.69 14 10 12 63.38 11.35 14 10 12 58.53 20.29 -14 -10 -12 91.83 23.71 14 10 13 98.63 13.63 14 10 13 59.58 20.05 -14 -10 -13 96.63 23.61 14 10 14 180.68 33.92 -14 -10 -14 156.97 30.83 -14 -10 -15 11.02 8.79 14 11 0 42.62 17.06 14 11 1 140.34 20.76 14 11 1 176.26 30.26 14 11 2 -4.23 6.75 14 11 2 5.65 5.80 14 11 2 -4.75 9.74 14 11 3 219.77 31.02 14 11 3 190.18 30.17 14 11 3 187.18 24.70 14 11 4 13.25 9.07 -14 -11 -4 22.04 12.40 14 11 4 20.48 9.98 14 11 4 21.19 8.84 14 11 5 54.44 17.39 -14 -11 -5 95.78 24.94 14 11 5 56.63 15.73 14 11 5 66.32 15.01 14 11 6 9.41 9.64 -14 -11 -6 11.45 10.55 14 11 6 20.67 10.93 14 11 6 13.25 10.07 14 11 7 224.19 33.73 -14 -11 -7 179.87 33.26 14 11 7 181.01 24.99 14 11 7 157.02 24.09 14 11 8 10.12 9.31 -14 -11 -8 5.84 9.31 14 11 8 5.61 4.47 14 11 8 3.71 8.31 14 11 9 5.27 10.88 -14 -11 -9 5.89 9.36 14 11 9 2.47 5.56 14 11 9 3.90 6.22 14 11 10 6.41 5.56 14 11 10 -5.51 8.79 -14 -11 -10 5.89 7.65 14 11 11 57.25 18.48 14 11 11 90.17 13.25 14 11 12 58.86 21.09 14 11 13 30.03 14.63 14 11 14 -6.08 9.69 14 12 2 7.84 5.89 14 12 2 -4.13 6.60 14 12 3 51.64 11.92 14 12 3 67.60 17.91 14 12 4 390.52 36.39 14 12 4 464.73 44.66 14 12 5 75.63 18.96 14 12 5 74.02 15.39 14 12 5 58.25 16.96 14 12 6 -4.61 8.46 14 12 6 3.14 6.41 14 12 6 -3.28 6.03 14 12 7 14.40 11.64 14 12 7 3.33 8.60 14 12 7 20.62 8.98 14 12 8 395.08 45.85 14 12 8 446.91 36.72 14 12 9 10.45 8.31 14 12 9 -7.55 9.17 14 12 9 15.39 6.70 14 12 10 5.51 12.35 14 12 10 28.22 11.73 14 12 11 -5.70 9.07 14 12 12 183.15 33.45 14 12 13 18.15 12.45 14 13 3 12.35 9.26 14 13 4 37.91 15.63 14 13 4 59.96 13.25 14 13 5 269.23 35.87 14 13 5 287.66 30.22 14 13 6 9.03 9.26 14 13 6 8.74 7.08 14 13 7 -4.70 12.92 14 13 7 3.09 5.70 14 13 8 4.89 9.03 14 13 8 3.33 5.32 14 13 9 308.47 41.71 14 13 9 358.64 38.10 14 13 10 37.91 16.58 14 13 10 42.43 14.25 14 13 11 5.70 11.64 14 13 12 29.50 15.39 14 13 13 285.53 42.71 14 14 4 12.26 9.93 14 14 5 63.14 17.06 14 14 6 302.01 37.82 14 14 6 265.81 28.60 14 14 7 9.12 9.41 14 14 7 11.45 7.46 14 14 8 -9.60 15.25 14 14 8 3.09 5.70 14 14 9 -10.07 10.36 14 14 9 13.44 8.74 14 14 10 223.29 35.30 14 14 10 252.41 31.36 14 14 11 11.21 10.31 14 14 12 64.52 20.33 14 15 4 118.20 22.28 14 15 5 -4.04 7.46 14 15 6 -4.23 10.26 14 15 7 110.32 23.04 14 15 8 65.04 18.29 14 15 9 4.89 10.02 14 15 9 6.18 6.37 14 15 10 10.31 9.50 14 15 10 3.42 6.27 14 15 11 262.87 39.24 14 15 11 308.95 35.63 14 16 5 70.08 17.39 14 16 6 4.04 6.41 14 16 7 12.68 9.55 14 16 8 102.57 22.47 14 16 9 249.33 35.35 14 16 10 114.92 24.75 14 17 7 12.07 9.03 14 17 9 40.43 14.40 -15 2 2 71.17 15.20 -15 1 4 -3.18 6.56 -15 1 3 51.59 13.25 -15 1 2 5.75 7.46 15 -1 2 5.61 8.93 15 -1 3 86.32 24.04 15 -1 5 -4.94 14.97 15 -1 6 4.94 9.07 15 -1 7 255.26 37.48 15 -1 8 20.24 13.16 -15 0 4 131.55 22.57 -15 0 3 3.23 5.94 -15 0 2 142.19 21.71 -15 0 1 2.95 4.66 15 0 1 5.80 10.64 15 0 2 89.03 23.71 15 0 3 -10.69 13.87 15 0 4 240.20 33.21 15 0 4 118.01 26.32 15 0 5 9.93 10.21 15 0 5 22.85 11.12 15 0 6 4.99 9.17 15 0 7 -5.08 10.40 15 0 8 364.63 45.18 15 0 9 -5.23 9.60 -15 -1 3 181.48 25.94 -15 -1 2 3.28 5.23 -15 -1 1 182.39 24.70 15 1 1 143.67 30.45 15 1 2 22.09 11.35 15 1 3 84.14 19.81 15 1 3 89.98 22.04 15 1 4 -4.94 6.41 15 1 4 4.47 5.80 15 1 4 -5.08 9.31 15 1 5 160.15 29.50 15 1 5 171.22 28.89 15 1 5 155.35 27.98 15 1 6 5.04 8.03 15 1 6 4.56 8.41 15 1 7 -5.13 8.12 15 1 7 4.66 7.36 15 1 8 25.99 13.54 15 1 9 285.72 40.43 15 1 10 -5.42 12.16 -15 -1 -15 14.44 11.69 -15 -1 -16 -4.75 10.64 -15 -2 2 285.10 33.40 -15 -2 1 26.75 10.21 15 2 0 107.18 26.03 15 2 1 51.45 20.43 15 2 2 210.84 31.26 15 2 2 186.28 34.06 15 2 3 21.71 11.97 15 2 3 10.45 11.78 15 2 4 203.76 33.16 15 2 4 219.68 32.02 15 2 4 210.37 33.07 15 2 5 -5.04 9.22 15 2 5 4.42 9.12 15 2 5 9.60 10.78 15 2 6 345.77 44.14 15 2 6 420.45 45.42 15 2 6 398.12 44.71 15 2 7 67.27 20.19 15 2 7 27.60 12.07 15 2 8 157.49 30.17 15 2 8 108.08 23.42 15 2 9 -5.37 9.83 15 2 9 4.80 8.79 15 2 10 262.87 38.77 15 2 10 241.06 35.73 -15 -2 -15 44.42 17.63 -15 -2 -16 29.17 13.44 -15 -3 2 43.90 13.54 -15 -3 1 215.21 29.12 -15 -3 0 3.37 8.22 15 3 0 11.78 10.83 15 3 1 205.05 29.79 15 3 1 164.24 31.31 15 3 2 -4.23 6.70 15 3 2 5.42 11.16 15 3 3 196.02 29.36 15 3 3 145.19 28.65 15 3 4 24.94 12.97 15 3 4 17.25 9.74 15 3 4 24.75 13.63 15 3 5 176.78 31.59 15 3 5 262.72 35.68 15 3 5 269.14 36.01 15 3 6 5.13 8.12 15 3 6 4.47 9.17 15 3 6 13.49 10.93 15 3 7 416.51 48.79 15 3 7 427.91 47.65 15 3 7 514.76 49.46 15 3 8 10.59 10.88 15 3 8 -4.66 10.45 15 3 9 173.45 31.45 15 3 9 161.77 28.51 15 3 10 5.56 11.40 15 3 10 4.89 8.98 -15 -3 -14 25.56 13.30 -15 -3 -15 177.25 30.69 -15 -4 1 -3.71 7.60 -15 -4 0 99.96 19.62 15 4 0 110.89 27.17 15 4 0 113.31 22.14 15 4 1 190.84 33.97 15 4 1 256.97 33.16 15 4 2 26.94 14.06 15 4 2 49.31 15.16 15 4 3 5.13 8.17 15 4 3 4.18 6.60 15 4 4 299.16 39.19 15 4 4 198.63 29.93 15 4 5 55.87 16.72 15 4 5 60.10 16.44 15 4 6 8.88 9.12 15 4 6 26.27 12.07 15 4 7 46.32 15.49 15 4 7 13.44 9.26 15 4 7 20.95 12.73 15 4 8 520.74 46.13 15 4 8 560.55 51.31 15 4 8 570.67 57.63 15 4 8 548.20 54.16 15 4 9 60.19 18.86 15 4 9 33.02 15.06 15 4 9 32.26 12.30 15 4 10 14.59 9.98 15 4 10 5.61 8.88 -15 -4 -13 -10.55 11.83 -15 -4 -14 130.98 26.89 -15 -4 -15 -5.18 6.75 -15 -5 0 71.12 16.58 15 5 0 80.95 22.61 15 5 0 27.46 12.11 15 5 1 44.42 17.67 15 5 1 3.99 8.93 15 5 2 207.71 34.02 15 5 2 220.39 30.79 15 5 3 5.08 8.12 15 5 3 4.09 7.46 15 5 4 9.69 11.83 15 5 4 33.07 12.59 15 5 4 29.93 12.97 15 5 5 156.87 27.22 15 5 5 151.36 26.13 15 5 6 39.38 13.97 15 5 6 21.52 13.16 15 5 7 8.27 8.50 15 5 7 13.25 9.93 15 5 8 7.84 8.03 15 5 8 4.56 9.31 15 5 9 331.09 37.39 15 5 9 354.65 42.05 15 5 10 86.75 22.42 15 5 10 84.71 22.90 15 5 11 5.80 10.59 -15 -5 -12 5.42 8.60 -15 -5 -13 107.94 25.18 -15 -5 -14 75.16 20.57 15 6 0 63.19 21.19 15 6 0 49.31 14.54 15 6 1 -5.51 11.26 15 6 1 3.85 8.65 15 6 2 57.72 19.48 15 6 2 77.82 18.10 15 6 3 120.48 25.13 15 6 3 173.98 27.60 15 6 4 14.40 11.73 15 6 4 52.50 16.20 15 6 5 91.07 21.24 15 6 5 86.47 20.33 15 6 5 81.14 22.14 15 6 6 47.51 15.49 15 6 6 50.60 16.11 15 6 6 61.95 17.86 15 6 7 155.21 25.99 15 6 7 147.47 25.99 15 6 7 158.39 28.60 15 6 8 49.27 16.11 15 6 8 69.17 18.15 15 6 9 119.67 24.47 15 6 9 127.09 22.23 15 6 10 243.10 35.44 15 6 10 243.15 30.93 -15 -6 -11 77.63 21.24 15 6 11 80.91 18.15 -15 -6 -12 83.19 21.85 -15 -6 -13 5.51 7.17 15 7 -1 61.24 15.73 15 7 0 166.71 32.16 15 7 0 273.65 32.40 15 7 1 142.34 28.41 15 7 1 103.76 20.43 15 7 2 5.18 10.64 15 7 2 -3.75 7.74 15 7 3 89.27 21.81 15 7 3 118.72 21.81 15 7 4 245.14 34.78 15 7 4 203.76 29.17 15 7 5 98.49 21.38 15 7 5 108.03 21.24 15 7 5 101.15 23.61 15 7 6 16.96 11.02 15 7 6 12.40 9.26 15 7 6 5.18 10.59 15 7 7 28.08 12.83 15 7 7 38.34 13.63 15 7 7 63.42 19.48 15 7 8 283.39 34.49 15 7 8 264.05 35.20 15 7 8 254.69 37.63 15 7 9 138.44 23.09 15 7 9 127.18 25.65 15 7 9 144.95 28.60 -15 -7 -10 39.62 16.49 15 7 10 53.26 13.73 15 7 10 47.08 17.34 15 7 10 5.75 10.59 -15 -7 -11 56.82 18.96 15 7 11 62.43 15.11 -15 -7 -12 119.34 27.98 15 7 12 102.67 17.82 15 7 13 5.51 6.22 15 8 -1 72.40 16.11 15 8 0 24.47 10.21 15 8 0 28.84 15.01 15 8 1 241.58 30.22 15 8 1 159.11 31.40 15 8 2 90.55 18.77 15 8 2 56.96 18.67 15 8 3 40.67 13.63 15 8 3 29.41 14.30 15 8 4 113.69 21.43 15 8 4 111.31 23.80 15 8 5 136.44 23.99 15 8 5 219.58 31.50 15 8 6 5.13 8.17 15 8 6 -3.99 6.37 15 8 6 8.27 8.50 15 8 7 10.55 10.83 15 8 7 -4.13 7.60 15 8 7 3.90 8.03 15 8 8 249.75 37.53 15 8 8 167.99 27.22 15 8 8 195.02 27.84 15 8 9 156.45 31.83 15 8 9 223.15 32.78 15 8 9 203.38 27.94 15 8 10 28.79 16.01 15 8 10 55.63 17.67 15 8 10 77.34 16.87 15 8 11 36.01 11.12 15 8 12 2.80 6.27 15 8 13 366.29 33.78 15 9 -1 39.38 12.54 15 9 0 126.14 21.33 15 9 1 23.71 10.36 15 9 1 32.78 14.25 15 9 2 190.60 27.27 15 9 2 232.89 35.68 15 9 3 -3.56 7.27 15 9 3 4.89 7.74 15 9 4 3.66 6.70 15 9 4 4.61 7.32 15 9 5 18.77 10.93 15 9 5 12.87 11.16 15 9 6 71.64 19.62 15 9 6 85.33 18.72 15 9 6 60.29 16.77 15 9 7 152.79 29.08 15 9 7 80.86 19.62 15 9 7 169.46 25.89 15 9 8 4.18 7.70 15 9 8 -3.52 8.55 15 9 9 94.97 24.47 15 9 9 131.27 21.52 15 9 9 87.70 20.62 15 9 10 228.66 27.84 15 9 10 182.05 30.55 15 9 11 2.80 9.69 15 10 1 114.64 26.03 15 10 1 121.62 20.95 15 10 2 30.93 15.01 15 10 2 39.38 13.21 15 10 3 164.24 30.07 15 10 3 195.78 26.70 15 10 4 22.66 11.83 15 10 4 34.73 12.83 15 10 5 -4.23 8.69 15 10 5 3.61 6.60 15 10 6 15.73 9.60 15 10 6 22.38 9.74 15 10 7 211.46 28.13 15 10 7 136.49 24.51 15 10 8 36.91 12.40 15 10 8 28.55 12.49 15 10 9 36.72 11.69 15 10 9 42.76 15.30 15 10 10 58.67 13.59 15 10 10 62.43 17.06 15 11 1 10.78 12.11 15 11 2 35.73 15.58 15 11 2 24.66 10.64 15 11 3 -4.80 9.83 15 11 3 -3.18 5.08 15 11 4 375.46 42.71 15 11 4 316.74 34.87 15 11 5 4.13 6.60 15 11 5 3.42 6.27 15 11 6 30.60 12.16 15 11 6 7.17 7.36 15 11 7 10.45 7.84 15 11 7 -3.75 9.07 15 11 8 31.45 12.02 15 11 9 24.80 12.07 15 11 10 30.45 13.30 15 12 4 3.09 6.32 15 12 5 309.33 33.68 15 12 6 30.41 12.07 15 12 7 24.85 10.36 15 12 8 18.81 9.17 15 12 9 227.38 31.69 15 12 10 -4.23 9.50 15 12 11 22.19 10.83 15 13 6 447.01 41.19 15 13 7 13.40 7.55 15 13 8 7.13 7.32 15 13 9 15.16 9.83 15 13 10 440.50 45.66 15 13 11 -4.28 7.89 15 14 9 3.56 6.56 15 14 10 7.65 9.31 15 14 11 340.97 39.86 15 14 12 48.13 15.68 15 15 12 133.17 24.23 16 1 5 53.54 18.53 16 1 6 189.70 32.21 16 2 4 11.02 12.40 16 2 5 158.30 29.84 16 2 6 -5.04 8.03 16 2 7 236.59 34.92 16 3 3 11.40 11.69 16 3 4 234.31 37.72 16 3 5 5.18 9.55 16 3 6 99.39 23.61 16 3 7 9.50 8.69 16 3 8 194.69 31.88 16 4 3 22.42 12.64 16 4 4 16.11 12.07 16 4 5 323.15 43.04 16 4 6 58.63 18.67 16 4 7 -4.66 10.45 16 4 8 44.33 14.78 16 4 9 206.90 30.55 16 5 3 204.29 34.73 16 5 4 74.07 21.38 16 5 5 40.43 15.49 16 5 6 226.19 34.11 16 5 7 13.68 10.26 16 5 8 4.32 7.98 16 5 9 57.72 16.25 16 5 10 144.81 24.85 16 5 11 81.76 19.00 16 6 2 50.88 18.81 16 6 3 81.57 22.04 16 6 4 57.25 17.39 16 6 5 89.46 23.56 16 6 6 104.09 22.99 16 6 7 242.58 34.78 16 6 8 93.59 20.29 16 6 9 80.34 19.48 16 6 10 38.05 14.49 16 6 11 46.75 14.16 16 6 12 85.14 17.77 16 7 2 268.66 40.76 16 7 3 5.32 9.79 16 7 4 280.40 39.81 16 7 5 87.51 21.71 16 7 6 69.55 19.24 16 7 7 17.58 10.69 16 7 8 62.38 17.67 16 7 9 169.18 26.75 16 7 10 318.36 36.72 16 7 11 20.86 10.12 16 8 2 172.41 33.11 16 8 3 337.74 44.33 16 8 4 -4.99 9.17 16 8 5 171.17 29.22 16 8 5 175.54 27.56 16 8 6 49.60 17.15 16 8 6 38.53 13.73 16 8 7 29.93 14.68 16 8 7 4.42 7.03 16 8 8 20.14 11.12 16 8 8 22.76 12.54 16 8 9 -3.80 8.55 16 8 10 128.42 22.61 16 9 3 84.04 22.38 16 9 4 79.39 21.05 16 9 4 50.88 14.59 16 9 5 42.00 14.82 16 9 5 4.04 7.41 16 9 6 26.27 14.59 16 9 6 49.98 15.35 16 9 7 8.27 7.60 16 9 7 25.70 11.12 16 9 8 -3.85 10.02 16 9 8 -4.47 5.75 16 9 9 36.82 14.06 16 10 3 72.78 16.96 16 10 4 131.22 22.47 16 10 5 3.85 7.08 16 10 6 16.06 9.79 16 10 7 4.13 10.07 16 10 8 69.22 18.86 16 10 9 13.44 9.22 16 11 5 140.10 23.47 16 11 6 7.65 7.03 16 11 7 3.99 7.32 16 11 8 4.18 10.78 16 11 9 322.54 39.53 16 11 10 9.12 11.07 16 12 7 3.80 6.03 16 12 8 -3.99 7.32 16 12 9 4.18 8.60 16 12 10 401.31 44.47 16 13 9 3.99 6.37 16 13 10 -4.23 8.69 17 3 8 -4.94 10.17 17 3 9 56.73 16.96 17 4 6 69.27 20.38 17 4 7 25.37 13.21 17 4 8 19.38 11.78 17 4 9 4.61 11.21 17 4 10 61.67 18.24 17 4 11 8.41 10.17 17 5 6 26.13 15.20 17 5 7 84.71 21.76 17 5 8 75.92 19.24 17 5 9 9.03 8.27 17 5 10 -4.28 11.12 17 6 5 37.39 16.34 17 6 6 224.72 35.11 17 6 7 -4.89 8.98 17 6 8 125.14 24.28 17 6 9 26.41 12.83 17 7 5 67.79 21.05 17 7 6 4.99 10.21 17 7 7 165.95 29.08 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 89475 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group La1 La 0.87234(2) 0.40503(2) 0.11546(2) 0.01473(6) Uani 1 1 d . . . . . La2 La 0.59383(2) 0.13689(2) 0.37965(2) 0.01630(6) Uani 1 1 d . . . . . Li1 Li 0.6244(6) 0.5024(4) 0.1301(4) 0.0289(15) Uani 1 1 d . . . . . C1 C 0.8963(3) 0.6637(2) 0.0966(2) 0.0163(7) Uani 1 1 d . . . . . C2 C 0.8054(3) 0.6758(2) 0.1799(2) 0.0249(8) Uani 1 1 d . . . . . H2A H 0.8440 0.6816 0.2179 0.037 Uiso 1 1 calc R U . . . H2B H 0.7591 0.6258 0.2107 0.037 Uiso 1 1 calc R U . . . H2C H 0.7555 0.7276 0.1637 0.037 Uiso 1 1 calc R U . . . C3 C 0.7326(3) 0.3465(2) 0.3900(2) 0.0202(8) Uani 1 1 d . . . . . C0AA C 0.6778(4) 0.3121(3) 0.4901(2) 0.0351(10) Uani 1 1 d . . . . . H0AA H 0.7363 0.3048 0.5186 0.053 Uiso 1 1 calc R U . . . H0AB H 0.6468 0.2566 0.5067 0.053 Uiso 1 1 calc R U . . . H0AC H 0.6157 0.3530 0.5085 0.053 Uiso 1 1 calc R U . . . C5 C 0.6237(3) 0.2511(2) 0.1212(2) 0.0217(8) Uani 1 1 d . . . . . C6 C 0.5522(4) 0.1952(3) 0.1059(3) 0.0347(10) Uani 1 1 d . . . . . H6A H 0.5408 0.1405 0.1539 0.052 Uiso 1 1 calc R U . . . H6B H 0.5932 0.1844 0.0507 0.052 Uiso 1 1 calc R U . . . H6C H 0.4774 0.2255 0.1035 0.052 Uiso 1 1 calc R U . . . C7 C 0.2702(3) 0.0355(2) 0.4180(2) 0.0192(7) Uani 1 1 d . . . . . C8 C 0.2356(4) 0.1048(2) 0.3395(3) 0.0306(9) Uani 1 1 d . . . . . H8A H 0.2326 0.0773 0.2992 0.046 Uiso 1 1 calc R U . . . H8B H 0.2924 0.1481 0.3089 0.046 Uiso 1 1 calc R U . . . H8C H 0.1599 0.1324 0.3611 0.046 Uiso 1 1 calc R U . . . C9 C 0.3296(3) 0.6683(2) 0.2526(2) 0.0230(8) Uani 1 1 d . . . . . C10 C 0.2966(4) 0.6052(3) 0.3485(3) 0.0399(11) Uani 1 1 d . . . . . H10A H 0.2163 0.6182 0.3789 0.060 Uiso 1 1 calc R U . . . H10B H 0.3463 0.6117 0.3787 0.060 Uiso 1 1 calc R U . . . H10C H 0.3065 0.5460 0.3480 0.060 Uiso 1 1 calc R U . . . C11 C 0.5613(3) 0.9845(2) 0.0002(2) 0.0249(8) Uani 1 1 d . . . . . C12 C 0.5952(3) 0.9675(2) 0.0758(2) 0.0266(9) Uani 1 1 d . . . . . H12 H 0.5392 0.9725 0.1278 0.032 Uiso 1 1 calc R U . . . C13 C 0.7110(4) 0.9432(2) 0.0749(2) 0.0260(9) Uani 1 1 d . . . . . C14 C 0.7964(4) 0.9341(2) -0.0012(3) 0.0286(9) Uani 1 1 d . . . . . H14 H 0.8745 0.9196 -0.0030 0.034 Uiso 1 1 calc R U . . . C15 C 0.7608(4) 0.9475(2) -0.0738(2) 0.0261(9) Uani 1 1 d . . . . . C16 C 0.6483(4) 0.9726(2) -0.0758(2) 0.0267(9) Uani 1 1 d . . . . . H16A H 0.6292 0.9817 -0.1271 0.032 Uiso 1 1 calc R U . . . C17 C 0.9105(4) 0.9967(3) -0.2270(3) 0.0404(11) Uani 1 1 d . . . . . H17 H 0.8927 1.0569 -0.2426 0.048 Uiso 1 1 calc R U . . . C18 C 0.9986(4) 0.9544(3) -0.2743(3) 0.0440(12) Uani 1 1 d . . . . . H18A H 1.0534 0.9796 -0.3287 0.053 Uiso 1 1 calc R U . . . C19 C 0.9036(5) 0.8575(3) -0.1544(3) 0.0444(13) Uani 1 1 d . . . . . H19A H 0.8808 0.8039 -0.1114 0.053 Uiso 1 1 calc R U . . . C20 C 0.8440(4) 0.8789(3) 0.1703(3) 0.0370(10) Uani 1 1 d . . . . . H20 H 0.8987 0.8472 0.1368 0.044 Uiso 1 1 calc R U . . . N4 N 0.7502(3) 0.9393(2) 0.2728(2) 0.0308(8) Uani 1 1 d . . . . . H4A H 0.7316 0.9541 0.3197 0.037 Uiso 1 1 calc R U . . . C22 C 0.6918(4) 0.9647(2) 0.2148(2) 0.0274(9) Uani 1 1 d . . . . . H22 H 0.6240 1.0019 0.2176 0.033 Uiso 1 1 calc R U . . . C23 C 0.0525(3) 0.4725(2) 0.4831(2) 0.0246(8) Uani 1 1 d . . . . . C24 C 0.1312(3) 0.4343(2) 0.5308(2) 0.0264(8) Uani 1 1 d . . . . . H24 H 0.1177 0.4426 0.5849 0.032 Uiso 1 1 calc R U . . . C25 C 0.2293(3) 0.3843(2) 0.4996(2) 0.0237(8) Uani 1 1 d . . . . . C26 C 0.2545(3) 0.3694(2) 0.4199(2) 0.0234(8) Uani 1 1 d . . . . . H26 H 0.3206 0.3353 0.3994 0.028 Uiso 1 1 calc R U . . . C27 C 0.1761(3) 0.4079(2) 0.3726(2) 0.0232(8) Uani 1 1 d . . . . . C28 C 0.0774(3) 0.4585(2) 0.4021(2) 0.0248(8) Uani 1 1 d . . . . . H28 H 0.0271 0.4836 0.3677 0.030 Uiso 1 1 calc R U . . . C29 C 0.3366(4) 0.3856(3) 0.5976(3) 0.0282(9) Uani 1 1 d . . . . . H29A H 0.3153 0.4432 0.5966 0.034 Uiso 1 1 calc R U . . . C30 C 0.4145(4) 0.2513(2) 0.6274(3) 0.0286(9) Uani 1 1 d . . . . . H30 H 0.4568 0.2007 0.6519 0.034 Uiso 1 1 calc R U . . . C31 C 0.3561(4) 0.2610(2) 0.5709(3) 0.0283(9) Uani 1 1 d . . . . . H31 H 0.3500 0.2190 0.5482 0.034 Uiso 1 1 calc R U . . . C32 C 0.1308(4) 0.3696(3) 0.2605(2) 0.0290(9) Uani 1 1 d . . . . . H32 H 0.0567 0.3504 0.2953 0.035 Uiso 1 1 calc R U . . . C33 C 0.2882(4) 0.4073(3) 0.1477(3) 0.0453(12) Uani 1 1 d . . . . . H33 H 0.3413 0.4174 0.0909 0.054 Uiso 1 1 calc R U . . . C34 C 0.3019(4) 0.4242(3) 0.2148(3) 0.0454(12) Uani 1 1 d . . . . . H34 H 0.3656 0.4483 0.2137 0.055 Uiso 1 1 calc R U . . . N1 N 0.8524(3) 0.93440(18) -0.15185(19) 0.0239(7) Uani 1 1 d . . . . . N2 N 0.9920(3) 0.8686(2) -0.2274(2) 0.0393(9) Uani 1 1 d . . . . . H2D H 1.0389 0.8273 -0.2431 0.047 Uiso 1 1 calc R U . . . N3 N 0.7454(3) 0.92871(19) 0.1513(2) 0.0254(7) Uani 1 1 d . . . . . C21 C 0.8449(4) 0.8856(3) 0.2468(3) 0.0384(10) Uani 1 1 d . . . . . H21 H 0.9002 0.8586 0.2765 0.046 Uiso 1 1 calc R U . . . N5 N 0.3064(3) 0.34575(19) 0.5529(2) 0.0238(7) Uani 1 1 d . . . . . N6 N 0.4015(3) 0.3287(2) 0.6431(2) 0.0287(7) Uani 1 1 d . . . . . H6D H 0.4313 0.3386 0.6775 0.034 Uiso 1 1 calc R U . . . N7 N 0.2018(3) 0.39851(19) 0.2867(2) 0.0228(7) Uani 1 1 d . . . . . N8 N 0.1819(3) 0.3724(2) 0.1777(2) 0.0307(8) Uani 1 1 d . . . . . H8 H 0.1533 0.3552 0.1472 0.037 Uiso 1 1 calc R U . . . O1 O 0.9186(2) 0.49087(15) 0.19748(16) 0.0229(6) Uani 1 1 d . . . . . O2 O 1.0771(2) 0.58615(16) 0.16642(16) 0.0243(6) Uani 1 1 d . . . . . H2 H 1.1141 0.6278 0.1292 0.036 Uiso 1 1 calc R U . . . O3 O 1.0556(2) 0.54051(15) 0.04508(15) 0.0227(6) Uani 1 1 d . . . . . O4 O 0.9628(2) 0.74037(15) 0.05097(17) 0.0251(6) Uani 1 1 d . . . . . H4 H 1.0127 0.7349 0.0057 0.038 Uiso 1 1 calc R U . . . O5 O 0.9158(2) 0.65726(14) -0.06589(14) 0.0173(5) Uani 1 1 d . . . . . O6 O 0.7293(2) 0.72412(15) 0.00926(16) 0.0239(6) Uani 1 1 d . . . . . H6 H 0.6826 0.7251 0.0574 0.036 Uiso 1 1 calc R U . . . O7 O 0.7724(2) 0.55961(14) 0.07251(15) 0.0181(5) Uani 1 1 d . . . . . O8 O 0.6777(2) 0.40926(15) 0.23443(15) 0.0225(5) Uani 1 1 d . . . . . O9 O 0.5333(2) 0.44427(16) 0.36768(17) 0.0292(6) Uani 1 1 d . . . . . H9 H 0.5672 0.4888 0.3517 0.044 Uiso 1 1 calc R U . . . O10 O 0.5573(2) 0.29133(15) 0.36385(17) 0.0252(6) Uani 1 1 d . . . . . O11 O 0.7895(3) 0.42553(16) 0.36923(18) 0.0329(7) Uani 1 1 d . . . . . H11 H 0.8200 0.4457 0.3153 0.049 Uiso 1 1 calc R U . . . O12 O 0.7814(2) 0.17756(15) 0.38756(16) 0.0241(6) Uani 1 1 d . . . . . O13 O 0.9379(2) 0.24838(16) 0.40284(16) 0.0259(6) Uani 1 1 d . . . . . H13 H 0.9086 0.2297 0.4571 0.039 Uiso 1 1 calc R U . . . O14 O 0.9029(2) 0.29533(14) 0.25815(15) 0.0203(5) Uani 1 1 d . . . . . O15 O 0.8520(2) 0.26103(14) 0.10815(16) 0.0207(5) Uani 1 1 d . . . . . O16 O 0.8083(2) 0.12783(15) 0.08513(17) 0.0274(6) Uani 1 1 d . . . . . H16 H 0.8246 0.1552 0.0317 0.041 Uiso 1 1 calc R U . . . O17 O 0.7356(2) 0.13937(15) 0.23553(16) 0.0250(6) Uani 1 1 d . . . . . O18 O 0.5548(2) 0.26656(17) 0.20451(17) 0.0326(7) Uani 1 1 d . . . . . H18 H 0.5903 0.2967 0.2154 0.049 Uiso 1 1 calc R U . . . O19 O 0.5354(2) 0.39395(17) 0.00933(18) 0.0301(6) Uani 1 1 d . . . . . H19 H 0.5113 0.3580 -0.0026 0.045 Uiso 1 1 calc R U . . . O20 O 0.6854(2) 0.41533(15) 0.06842(16) 0.0227(5) Uani 1 1 d . . . . . O21 O 0.7434(2) 0.33787(16) -0.04921(16) 0.0237(6) Uani 1 1 d . . . . . O22 O 0.5055(2) 0.03978(16) 0.33964(17) 0.0263(6) Uani 1 1 d . . . . . O23 O 0.4047(3) -0.05425(16) 0.30523(17) 0.0285(6) Uani 1 1 d . . . . . H23 H 0.3478 -0.0833 0.3239 0.043 Uiso 1 1 calc R U . . . O24 O 0.4243(2) -0.10000(15) 0.46092(16) 0.0262(6) Uani 1 1 d . . . . . O25 O 0.1787(2) -0.02578(16) 0.46464(17) 0.0258(6) Uani 1 1 d . . . . . H25 H 0.1949 -0.0637 0.5072 0.039 Uiso 1 1 calc R U . . . O26 O 0.2872(3) 0.01036(15) 0.57923(16) 0.0272(6) Uani 1 1 d . . . . . O27 O 0.1668(2) 0.14675(16) 0.51691(19) 0.0317(6) Uani 1 1 d . . . . . H27 H 0.1093 0.1176 0.5416 0.047 Uiso 1 1 calc R U . . . O28 O 0.3791(2) 0.14366(15) 0.45143(16) 0.0235(6) Uani 1 1 d . . . . . O29 O 0.2500(3) 0.6595(2) 0.2118(2) 0.0429(8) Uani 1 1 d . . . . . H29 H 0.1828 0.6719 0.2395 0.064 Uiso 1 1 calc R U . . . O30 O 0.4809(2) 0.57452(16) 0.14839(17) 0.0267(6) Uani 1 1 d . . . . . O31 O 0.5472(2) 0.60204(15) 0.25972(18) 0.0280(6) Uani 1 1 d . . . . . O32 O 0.5303(2) 0.72725(16) 0.12065(17) 0.0313(6) Uani 1 1 d . . . . . O34 O 0.3836(3) 0.79957(17) 0.2955(2) 0.0379(7) Uani 1 1 d . . . . . O35 O 0.3412(3) 0.83671(18) 0.14996(19) 0.0413(7) Uani 1 1 d . . . . . H35 H 0.2975 0.8273 0.1274 0.062 Uiso 1 1 calc R U . . . O36 O 0.1758(3) 0.80288(17) 0.29288(19) 0.0348(7) Uani 1 1 d . . . . . O37 O 0.0074(4) 0.7146(3) 0.2724(4) 0.0920(16) Uani 1 1 d . . . . . O38 O 0.0697(2) 0.85980(17) 0.43420(17) 0.0295(6) Uani 1 1 d . . . . . O39 O 0.8589(3) 0.1581(2) 0.9150(2) 0.0565(10) Uani 1 1 d . . . . . P1 P 0.99187(8) 0.56424(5) 0.12804(6) 0.01592(19) Uani 1 1 d . . . . . P2 P 0.82437(8) 0.64743(5) 0.02488(6) 0.01508(18) Uani 1 1 d . . . . . P3 P 0.62059(8) 0.37312(5) 0.33396(6) 0.01665(19) Uani 1 1 d . . . . . P4 P 0.84089(8) 0.26123(5) 0.35648(6) 0.01636(19) Uani 1 1 d . . . . . P5 P 0.65376(8) 0.35644(6) 0.03019(6) 0.01844(19) Uani 1 1 d . . . . . P6 P 0.76344(8) 0.19363(5) 0.13903(6) 0.01716(19) Uani 1 1 d . . . . . P7 P 0.41156(8) -0.02448(6) 0.38103(6) 0.01748(19) Uani 1 1 d . . . . . P8 P 0.28057(8) 0.08484(5) 0.49577(6) 0.01729(19) Uani 1 1 d . . . . . P9 P 0.48206(9) 0.64191(6) 0.19084(6) 0.0204(2) Uani 1 1 d . . . . . P10 P 0.30428(9) 0.78223(6) 0.25418(7) 0.0251(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 La1 0.01581(12) 0.01487(10) 0.01189(11) -0.00435(7) -0.00225(8) -0.00123(7) La2 0.01534(12) 0.01600(10) 0.01650(11) -0.00566(8) -0.00169(8) -0.00412(7) Li1 0.028(4) 0.023(3) 0.033(4) -0.009(3) -0.007(3) -0.002(3) C1 0.0165(19) 0.0168(16) 0.0147(16) -0.0052(13) -0.0011(14) -0.0062(13) C2 0.021(2) 0.033(2) 0.0214(19) -0.0151(16) -0.0020(16) -0.0016(16) C3 0.019(2) 0.0247(18) 0.0166(18) -0.0102(14) 0.0005(15) -0.0043(14) C0AA 0.026(2) 0.062(3) 0.0134(19) -0.0162(18) 0.0010(17) -0.001(2) C5 0.020(2) 0.0277(18) 0.0181(18) -0.0086(15) -0.0038(15) -0.0055(15) C6 0.031(2) 0.032(2) 0.046(3) -0.0096(18) -0.017(2) -0.0101(17) C7 0.0178(19) 0.0201(17) 0.0214(18) -0.0066(14) -0.0067(15) -0.0046(14) C8 0.040(3) 0.029(2) 0.028(2) -0.0086(16) -0.0179(19) -0.0003(17) C9 0.021(2) 0.0254(18) 0.026(2) -0.0117(15) -0.0059(16) -0.0039(15) C10 0.044(3) 0.032(2) 0.034(2) -0.0092(18) 0.000(2) -0.0079(19) C11 0.026(2) 0.0238(18) 0.0239(19) -0.0085(15) -0.0053(17) -0.0029(15) C12 0.022(2) 0.032(2) 0.0215(19) -0.0133(16) 0.0026(16) -0.0003(16) C13 0.031(2) 0.0236(18) 0.0210(19) -0.0092(15) -0.0028(17) -0.0034(16) C14 0.021(2) 0.031(2) 0.032(2) -0.0139(17) -0.0041(18) 0.0011(16) C15 0.026(2) 0.0278(19) 0.0177(18) -0.0112(15) 0.0048(16) -0.0001(16) C16 0.030(2) 0.0266(19) 0.0201(19) -0.0088(15) -0.0037(17) -0.0001(16) C17 0.051(3) 0.0204(19) 0.032(2) -0.0046(17) 0.004(2) -0.0023(18) C18 0.040(3) 0.048(3) 0.030(2) -0.016(2) 0.011(2) -0.008(2) C19 0.065(3) 0.024(2) 0.023(2) -0.0041(16) 0.002(2) 0.009(2) C20 0.036(3) 0.040(2) 0.040(2) -0.023(2) -0.013(2) 0.0092(19) N4 0.043(2) 0.0274(16) 0.0249(17) -0.0136(14) -0.0103(16) 0.0002(15) C22 0.032(2) 0.0243(19) 0.023(2) -0.0108(15) -0.0033(18) -0.0001(16) C23 0.022(2) 0.0312(19) 0.0221(19) -0.0118(16) -0.0051(16) -0.0011(16) C24 0.026(2) 0.036(2) 0.0225(19) -0.0156(16) -0.0083(17) 0.0002(16) C25 0.025(2) 0.0292(19) 0.0222(19) -0.0096(15) -0.0128(17) -0.0005(15) C26 0.024(2) 0.0268(18) 0.0232(19) -0.0118(15) -0.0078(16) -0.0004(15) C27 0.023(2) 0.0304(19) 0.0188(18) -0.0111(15) -0.0049(16) -0.0053(15) C28 0.019(2) 0.034(2) 0.025(2) -0.0137(16) -0.0090(16) 0.0031(15) C29 0.031(2) 0.033(2) 0.028(2) -0.0165(17) -0.0129(18) 0.0028(17) C30 0.024(2) 0.032(2) 0.033(2) -0.0124(17) -0.0143(18) 0.0051(16) C31 0.031(2) 0.0255(19) 0.033(2) -0.0163(16) -0.0120(19) 0.0056(16) C32 0.026(2) 0.045(2) 0.022(2) -0.0127(17) -0.0061(17) -0.0142(18) C33 0.033(3) 0.077(3) 0.026(2) -0.029(2) 0.007(2) -0.009(2) C34 0.026(3) 0.081(3) 0.034(2) -0.029(2) 0.005(2) -0.020(2) N1 0.0239(18) 0.0224(15) 0.0186(16) -0.0073(12) -0.0004(13) 0.0032(12) N2 0.046(2) 0.038(2) 0.0287(19) -0.0161(16) -0.0119(18) 0.0218(17) N3 0.0260(19) 0.0261(16) 0.0246(17) -0.0120(13) -0.0051(14) -0.0002(13) C21 0.043(3) 0.039(2) 0.043(3) -0.021(2) -0.022(2) 0.0081(19) N5 0.0250(19) 0.0301(16) 0.0219(16) -0.0137(13) -0.0096(14) 0.0006(13) N6 0.0259(19) 0.0424(19) 0.0262(17) -0.0181(15) -0.0114(15) -0.0009(14) N7 0.0185(17) 0.0319(16) 0.0201(16) -0.0134(13) -0.0032(13) -0.0017(13) N8 0.031(2) 0.0452(19) 0.0256(18) -0.0203(15) -0.0109(15) -0.0024(15) O1 0.0254(15) 0.0217(12) 0.0197(13) -0.0014(10) -0.0059(11) -0.0102(10) O2 0.0245(15) 0.0302(13) 0.0213(13) -0.0091(11) -0.0067(11) -0.0086(11) O3 0.0299(16) 0.0224(12) 0.0160(12) -0.0083(10) -0.0085(11) 0.0052(10) O4 0.0260(15) 0.0209(12) 0.0263(14) -0.0110(10) 0.0021(12) -0.0093(10) O5 0.0156(13) 0.0215(12) 0.0125(11) -0.0052(9) -0.0011(10) -0.0026(9) O6 0.0202(14) 0.0226(12) 0.0201(13) -0.0040(10) -0.0005(11) 0.0021(10) O7 0.0166(13) 0.0175(11) 0.0174(12) -0.0047(9) -0.0012(10) -0.0043(9) O8 0.0196(14) 0.0277(13) 0.0155(12) -0.0057(10) -0.0019(11) -0.0002(10) O9 0.0277(16) 0.0238(13) 0.0287(14) -0.0118(11) 0.0021(12) 0.0011(11) O10 0.0227(15) 0.0203(12) 0.0315(14) -0.0064(11) -0.0079(12) -0.0040(10) O11 0.0381(18) 0.0311(14) 0.0357(16) -0.0194(12) -0.0041(14) -0.0127(12) O12 0.0222(15) 0.0200(12) 0.0266(14) -0.0033(10) -0.0054(11) -0.0062(10) O13 0.0221(15) 0.0368(14) 0.0173(13) -0.0026(11) -0.0065(11) -0.0108(11) O14 0.0236(14) 0.0202(12) 0.0139(12) -0.0044(9) -0.0037(11) -0.0008(10) O15 0.0176(14) 0.0207(12) 0.0229(13) -0.0055(10) -0.0050(11) -0.0052(10) O16 0.0371(17) 0.0248(13) 0.0207(13) -0.0109(11) -0.0043(12) -0.0047(11) O17 0.0266(15) 0.0272(13) 0.0169(13) -0.0026(10) -0.0031(11) -0.0078(11) O18 0.0269(16) 0.0387(15) 0.0263(15) -0.0142(12) 0.0053(12) -0.0075(12) O19 0.0261(16) 0.0363(15) 0.0322(15) -0.0141(12) -0.0128(13) 0.0012(12) O20 0.0259(15) 0.0228(12) 0.0239(13) -0.0101(10) -0.0113(11) 0.0002(10) O21 0.0207(14) 0.0305(13) 0.0199(13) -0.0104(11) -0.0022(11) -0.0051(10) O22 0.0219(15) 0.0270(13) 0.0314(14) -0.0179(11) 0.0021(12) -0.0078(11) O23 0.0361(17) 0.0304(14) 0.0247(14) -0.0133(11) -0.0080(12) -0.0094(12) O24 0.0284(16) 0.0260(13) 0.0206(13) -0.0079(10) -0.0057(12) 0.0035(11) O25 0.0199(15) 0.0278(13) 0.0325(15) -0.0073(11) -0.0093(12) -0.0108(11) O26 0.0410(18) 0.0216(13) 0.0180(13) -0.0077(10) -0.0082(12) 0.0008(11) O27 0.0167(15) 0.0295(14) 0.0505(18) -0.0227(13) -0.0038(13) 0.0017(11) O28 0.0199(14) 0.0258(13) 0.0269(14) -0.0153(11) -0.0007(11) -0.0054(10) O29 0.0165(16) 0.072(2) 0.059(2) -0.0469(18) -0.0099(15) 0.0023(14) O30 0.0237(15) 0.0317(14) 0.0308(14) -0.0165(11) -0.0097(12) -0.0007(11) O31 0.0325(16) 0.0243(13) 0.0347(15) -0.0126(11) -0.0182(13) 0.0021(11) O32 0.0265(16) 0.0244(13) 0.0295(15) -0.0043(11) 0.0022(12) -0.0011(11) O34 0.0405(19) 0.0330(15) 0.0538(19) -0.0242(14) -0.0215(16) 0.0005(13) O35 0.045(2) 0.0335(15) 0.0368(17) -0.0024(13) -0.0155(15) 0.0029(13) O36 0.0294(17) 0.0369(15) 0.0395(17) -0.0212(13) -0.0075(14) 0.0068(12) O37 0.045(3) 0.102(3) 0.162(5) -0.085(3) -0.038(3) 0.019(2) O38 0.0243(16) 0.0357(14) 0.0281(14) -0.0091(12) -0.0066(12) -0.0064(11) O39 0.066(3) 0.069(2) 0.0335(18) -0.0183(16) -0.0185(18) 0.0063(19) P1 0.0171(5) 0.0184(4) 0.0126(4) -0.0054(3) -0.0029(4) -0.0044(3) P2 0.0146(5) 0.0147(4) 0.0140(4) -0.0045(3) -0.0018(4) -0.0020(3) P3 0.0161(5) 0.0163(4) 0.0153(4) -0.0062(3) -0.0008(4) -0.0017(3) P4 0.0158(5) 0.0197(4) 0.0127(4) -0.0044(3) -0.0029(4) -0.0039(3) P5 0.0179(5) 0.0205(4) 0.0182(4) -0.0070(3) -0.0058(4) -0.0024(3) P6 0.0197(5) 0.0176(4) 0.0138(4) -0.0053(3) -0.0025(4) -0.0051(3) P7 0.0191(5) 0.0198(4) 0.0151(4) -0.0087(3) -0.0024(4) -0.0044(3) P8 0.0156(5) 0.0178(4) 0.0197(5) -0.0090(3) -0.0039(4) -0.0010(3) P9 0.0187(5) 0.0213(4) 0.0223(5) -0.0088(4) -0.0061(4) -0.0007(4) P10 0.0257(6) 0.0221(5) 0.0301(5) -0.0123(4) -0.0092(4) 0.0014(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' La La -0.2871 2.4523 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 La1 O5 93.96(8) . 2_765 ? O1 La1 O7 72.02(8) . . ? O1 La1 O20 130.23(8) . . ? O3 La1 O1 116.58(8) 2_765 . ? O3 La1 O5 71.60(8) 2_765 2_765 ? O3 La1 O7 75.46(7) 2_765 . ? O3 La1 O8 136.62(8) 2_765 . ? O3 La1 O14 146.93(8) 2_765 . ? O3 La1 O15 89.14(8) 2_765 . ? O3 La1 O20 76.80(8) 2_765 . ? O5 La1 O7 133.03(7) 2_765 . ? O5 La1 O20 134.11(7) 2_765 . ? O7 La1 O20 65.52(7) . . ? O8 La1 O1 78.70(8) . . ? O8 La1 O5 151.15(7) . 2_765 ? O8 La1 O7 71.49(7) . . ? O8 La1 O20 64.37(8) . . ? O14 La1 O1 72.70(7) . . ? O14 La1 O5 76.25(7) . 2_765 ? O14 La1 O7 134.98(7) . . ? O14 La1 O8 74.93(8) . . ? O14 La1 O20 123.24(8) . . ? O15 La1 O1 148.32(8) . . ? O15 La1 O5 76.12(8) . 2_765 ? O15 La1 O7 135.99(8) . . ? O15 La1 O8 95.49(8) . . ? O15 La1 O14 75.71(8) . . ? O15 La1 O20 70.93(8) . . ? O10 La2 O12 75.97(8) . . ? O10 La2 O17 102.23(8) . . ? O10 La2 O22 132.39(9) . . ? O10 La2 O24 90.36(8) . 2_656 ? O10 La2 O26 150.92(9) . 2_656 ? O10 La2 O28 79.99(8) . . ? O12 La2 O26 75.84(8) . 2_656 ? O17 La2 O12 76.81(8) . . ? O17 La2 O22 79.21(8) . . ? O17 La2 O24 142.53(9) . 2_656 ? O17 La2 O26 78.06(8) . 2_656 ? O17 La2 O28 139.55(9) . . ? O22 La2 O12 146.50(8) . . ? O22 La2 O24 117.48(8) . 2_656 ? O22 La2 O26 76.57(9) . 2_656 ? O22 La2 O28 70.89(8) . . ? O24 La2 O12 72.25(8) 2_656 . ? O24 La2 O26 74.35(8) 2_656 2_656 ? O28 La2 O12 140.45(8) . . ? O28 La2 O24 77.02(9) . 2_656 ? O28 La2 O26 118.90(8) . 2_656 ? O7 Li1 O8 94.9(3) . . ? O7 Li1 O20 91.4(3) . . ? O20 Li1 O8 85.6(3) . . ? O30 Li1 O7 118.4(3) . . ? O30 Li1 O8 122.9(3) . . ? O30 Li1 O20 133.4(4) . . ? C2 C1 P1 109.3(2) . . ? C2 C1 P2 110.2(3) . . ? O4 C1 C2 108.0(3) . . ? O4 C1 P1 111.0(2) . . ? O4 C1 P2 111.0(2) . . ? P2 C1 P1 107.21(16) . . ? C1 C2 H2A 109.5 . . ? C1 C2 H2B 109.5 . . ? C1 C2 H2C 109.5 . . ? H2A C2 H2B 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? C0AA C3 P3 110.6(3) . . ? C0AA C3 P4 108.0(3) . . ? O11 C3 C0AA 107.3(3) . . ? O11 C3 P3 109.6(2) . . ? O11 C3 P4 110.8(2) . . ? P3 C3 P4 110.48(18) . . ? C3 C0AA H0AA 109.5 . . ? C3 C0AA H0AB 109.5 . . ? C3 C0AA H0AC 109.5 . . ? H0AA C0AA H0AB 109.5 . . ? H0AA C0AA H0AC 109.5 . . ? H0AB C0AA H0AC 109.5 . . ? C6 C5 P5 112.4(3) . . ? C6 C5 P6 112.9(3) . . ? O18 C5 C6 106.2(3) . . ? O18 C5 P5 110.0(2) . . ? O18 C5 P6 105.7(2) . . ? P5 C5 P6 109.44(19) . . ? C5 C6 H6A 109.5 . . ? C5 C6 H6B 109.5 . . ? C5 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C8 C7 P7 112.0(3) . . ? C8 C7 P8 111.3(2) . . ? O25 C7 C8 107.4(3) . . ? O25 C7 P7 109.2(2) . . ? O25 C7 P8 108.4(2) . . ? P8 C7 P7 108.46(19) . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C10 C9 P9 110.5(3) . . ? C10 C9 P10 109.2(3) . . ? O29 C9 C10 107.5(3) . . ? O29 C9 P9 110.3(2) . . ? O29 C9 P10 106.2(2) . . ? P10 C9 P9 112.89(19) . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C12 C11 C11 121.3(4) . 2_675 ? C12 C11 C16 117.2(4) . . ? C16 C11 C11 121.5(4) . 2_675 ? C11 C12 H12 119.3 . . ? C13 C12 C11 121.4(3) . . ? C13 C12 H12 119.3 . . ? C12 C13 N3 121.0(3) . . ? C14 C13 C12 120.7(4) . . ? C14 C13 N3 118.3(4) . . ? C13 C14 H14 121.4 . . ? C15 C14 C13 117.2(4) . . ? C15 C14 H14 121.4 . . ? C14 C15 N1 115.7(4) . . ? C16 C15 C14 123.7(3) . . ? C16 C15 N1 120.6(3) . . ? C11 C16 H16A 120.2 . . ? C15 C16 C11 119.7(4) . . ? C15 C16 H16A 120.2 . . ? C18 C17 H17 126.5 . . ? C18 C17 N1 106.9(3) . . ? N1 C17 H17 126.5 . . ? C17 C18 H18A 126.7 . . ? N2 C18 C17 106.6(4) . . ? N2 C18 H18A 126.7 . . ? N1 C19 H19A 125.7 . . ? N2 C19 H19A 125.7 . . ? N2 C19 N1 108.6(3) . . ? N3 C20 H20 126.7 . . ? C21 C20 H20 126.7 . . ? C21 C20 N3 106.6(4) . . ? C22 N4 H4A 125.4 . . ? C22 N4 C21 109.1(3) . . ? C21 N4 H4A 125.4 . . ? N4 C22 H22 125.5 . . ? N4 C22 N3 109.0(4) . . ? N3 C22 H22 125.5 . . ? C24 C23 C23 120.6(4) . 2_566 ? C24 C23 C28 117.1(3) . . ? C28 C23 C23 122.3(4) . 2_566 ? C23 C24 H24 119.5 . . ? C25 C24 C23 121.1(3) . . ? C25 C24 H24 119.5 . . ? C24 C25 C26 122.4(4) . . ? C24 C25 N5 118.2(3) . . ? C26 C25 N5 119.4(3) . . ? C25 C26 H26 121.9 . . ? C27 C26 C25 116.2(3) . . ? C27 C26 H26 121.9 . . ? C26 C27 C28 122.7(3) . . ? C26 C27 N7 118.3(3) . . ? C28 C27 N7 118.9(3) . . ? C23 C28 H28 119.7 . . ? C27 C28 C23 120.5(4) . . ? C27 C28 H28 119.7 . . ? N5 C29 H29A 126.2 . . ? N6 C29 H29A 126.2 . . ? N6 C29 N5 107.6(3) . . ? C31 C30 H30 126.0 . . ? C31 C30 N6 108.0(3) . . ? N6 C30 H30 126.0 . . ? C30 C31 H31 126.9 . . ? C30 C31 N5 106.1(3) . . ? N5 C31 H31 126.9 . . ? N7 C32 H32 125.5 . . ? N8 C32 H32 125.5 . . ? N8 C32 N7 109.0(4) . . ? C34 C33 H33 126.2 . . ? C34 C33 N8 107.7(4) . . ? N8 C33 H33 126.2 . . ? C33 C34 H34 126.8 . . ? C33 C34 N7 106.4(4) . . ? N7 C34 H34 126.8 . . ? C17 N1 C15 127.9(3) . . ? C19 N1 C15 123.3(3) . . ? C19 N1 C17 108.2(3) . . ? C18 N2 H2D 125.2 . . ? C19 N2 C18 109.6(3) . . ? C19 N2 H2D 125.2 . . ? C20 N3 C13 126.3(3) . . ? C22 N3 C13 125.8(3) . . ? C22 N3 C20 107.8(3) . . ? C20 C21 N4 107.5(4) . . ? C20 C21 H21 126.2 . . ? N4 C21 H21 126.2 . . ? C29 N5 C25 124.8(3) . . ? C29 N5 C31 108.9(3) . . ? C31 N5 C25 126.2(3) . . ? C29 N6 C30 109.5(3) . . ? C29 N6 H6D 125.3 . . ? C30 N6 H6D 125.3 . . ? C32 N7 C27 125.8(3) . . ? C32 N7 C34 108.1(3) . . ? C34 N7 C27 125.9(3) . . ? C32 N8 C33 108.8(3) . . ? C32 N8 H8 125.6 . . ? C33 N8 H8 125.6 . . ? P1 O1 La1 107.28(12) . . ? P1 O2 H2 109.5 . . ? P1 O3 La1 145.44(14) . 2_765 ? C1 O4 H4 109.5 . . ? P2 O5 La1 133.55(13) . 2_765 ? P2 O6 H6 109.5 . . ? Li1 O7 La1 86.1(2) . . ? P2 O7 La1 130.32(14) . . ? P2 O7 Li1 143.6(2) . . ? Li1 O8 La1 84.4(2) . . ? P3 O8 La1 141.36(15) . . ? P3 O8 Li1 134.0(2) . . ? P3 O9 H9 109.5 . . ? P3 O10 La2 141.48(16) . . ? C3 O11 H11 109.5 . . ? P4 O12 La2 135.34(14) . . ? P4 O13 H13 109.5 . . ? P4 O14 La1 140.91(15) . . ? P6 O15 La1 141.87(14) . . ? P6 O16 H16 109.5 . . ? P6 O17 La2 140.29(16) . . ? C5 O18 H18 109.5 . . ? P5 O19 H19 109.5 . . ? Li1 O20 La1 84.3(2) . . ? P5 O20 La1 129.10(14) . . ? P5 O20 Li1 145.1(3) . . ? P7 O22 La2 140.14(15) . . ? P7 O23 H23 109.5 . . ? P7 O24 La2 141.90(14) . 2_656 ? C7 O25 H25 109.5 . . ? P8 O26 La2 137.55(15) . 2_656 ? P8 O27 H27 109.5 . . ? P8 O28 La2 139.67(14) . . ? C9 O29 H29 109.5 . . ? P9 O30 Li1 113.1(3) . . ? P10 O35 H35 109.5 . . ? O1 P1 C1 109.71(15) . . ? O1 P1 O2 110.08(14) . . ? O2 P1 C1 107.62(15) . . ? O3 P1 C1 107.01(14) . . ? O3 P1 O1 110.13(14) . . ? O3 P1 O2 112.18(15) . . ? O5 P2 C1 107.47(15) . . ? O5 P2 O6 106.21(13) . . ? O6 P2 C1 108.04(15) . . ? O7 P2 C1 107.15(14) . . ? O7 P2 O5 115.46(13) . . ? O7 P2 O6 112.22(14) . . ? O8 P3 C3 109.21(16) . . ? O8 P3 O9 110.20(14) . . ? O9 P3 C3 106.32(16) . . ? O10 P3 C3 107.60(15) . . ? O10 P3 O8 114.16(15) . . ? O10 P3 O9 109.03(15) . . ? O12 P4 C3 109.37(15) . . ? O12 P4 O13 110.95(14) . . ? O13 P4 C3 106.24(16) . . ? O14 P4 C3 109.51(14) . . ? O14 P4 O12 115.06(14) . . ? O14 P4 O13 105.30(14) . . ? O19 P5 C5 106.36(16) . . ? O20 P5 C5 105.61(15) . . ? O20 P5 O19 108.72(15) . . ? O21 P5 C5 107.75(15) . . ? O21 P5 O19 110.03(15) . . ? O21 P5 O20 117.73(15) . . ? O15 P6 C5 108.84(15) . . ? O15 P6 O16 110.74(14) . . ? O16 P6 C5 109.04(16) . . ? O17 P6 C5 106.75(16) . . ? O17 P6 O15 114.72(15) . . ? O17 P6 O16 106.57(14) . . ? O22 P7 C7 107.66(15) . . ? O22 P7 O23 107.21(15) . . ? O23 P7 C7 106.63(16) . . ? O24 P7 C7 106.57(15) . . ? O24 P7 O22 115.54(16) . . ? O24 P7 O23 112.78(14) . . ? O26 P8 C7 106.70(15) . . ? O26 P8 O27 110.22(15) . . ? O27 P8 C7 108.48(16) . . ? O28 P8 C7 109.59(15) . . ? O28 P8 O26 116.45(16) . . ? O28 P8 O27 105.21(14) . . ? O30 P9 C9 108.60(16) . . ? O31 P9 C9 106.03(16) . . ? O31 P9 O30 109.99(14) . . ? O31 P9 O32 112.98(16) . . ? O32 P9 C9 107.33(15) . . ? O32 P9 O30 111.63(15) . . ? O34 P10 C9 111.17(17) . . ? O34 P10 O35 109.52(18) . . ? O34 P10 O36 116.15(17) . . ? O35 P10 C9 101.42(16) . . ? O36 P10 C9 109.70(16) . . ? O36 P10 O35 107.81(17) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag La1 O1 2.556(2) . ? La1 O3 2.414(2) 2_765 ? La1 O5 2.561(2) 2_765 ? La1 O7 2.563(2) . ? La1 O8 2.534(2) . ? La1 O14 2.533(2) . ? La1 O15 2.479(2) . ? La1 O20 2.625(3) . ? La2 O10 2.425(2) . ? La2 O12 2.561(3) . ? La2 O17 2.445(2) . ? La2 O22 2.475(2) . ? La2 O24 2.481(2) 2_656 ? La2 O26 2.569(2) 2_656 ? La2 O28 2.476(3) . ? Li1 O7 1.959(7) . ? Li1 O8 2.082(7) . ? Li1 O20 1.964(7) . ? Li1 O30 1.918(7) . ? C1 C2 1.516(5) . ? C1 O4 1.443(4) . ? C1 P1 1.842(4) . ? C1 P2 1.840(4) . ? C2 H2A 0.9600 . ? C2 H2B 0.9600 . ? C2 H2C 0.9600 . ? C3 C0AA 1.516(5) . ? C3 O11 1.459(4) . ? C3 P3 1.826(4) . ? C3 P4 1.844(4) . ? C0AA H0AA 0.9600 . ? C0AA H0AB 0.9600 . ? C0AA H0AC 0.9600 . ? C5 C6 1.520(5) . ? C5 O18 1.457(4) . ? C5 P5 1.843(4) . ? C5 P6 1.853(4) . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C7 C8 1.531(5) . ? C7 O25 1.454(4) . ? C7 P7 1.845(4) . ? C7 P8 1.832(4) . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C9 C10 1.531(5) . ? C9 O29 1.427(5) . ? C9 P9 1.850(4) . ? C9 P10 1.849(3) . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C11 C11 1.488(8) 2_675 ? C11 C12 1.398(6) . ? C11 C16 1.408(5) . ? C12 H12 0.9300 . ? C12 C13 1.390(6) . ? C13 C14 1.384(5) . ? C13 N3 1.424(5) . ? C14 H14 0.9300 . ? C14 C15 1.376(6) . ? C15 C16 1.365(6) . ? C15 N1 1.461(5) . ? C16 H16A 0.9300 . ? C17 H17 0.9300 . ? C17 C18 1.346(6) . ? C17 N1 1.365(5) . ? C18 H18A 0.9300 . ? C18 N2 1.342(6) . ? C19 H19A 0.9300 . ? C19 N1 1.310(5) . ? C19 N2 1.307(6) . ? C20 H20 0.9300 . ? C20 N3 1.388(5) . ? C20 C21 1.345(6) . ? N4 H4A 0.8600 . ? N4 C22 1.312(5) . ? N4 C21 1.362(5) . ? C22 H22 0.9300 . ? C22 N3 1.330(5) . ? C23 C23 1.491(7) 2_566 ? C23 C24 1.383(6) . ? C23 C28 1.395(5) . ? C24 H24 0.9300 . ? C24 C25 1.377(5) . ? C25 C26 1.381(5) . ? C25 N5 1.433(5) . ? C26 H26 0.9300 . ? C26 C27 1.375(5) . ? C27 C28 1.379(5) . ? C27 N7 1.440(5) . ? C28 H28 0.9300 . ? C29 H29A 0.9300 . ? C29 N5 1.337(5) . ? C29 N6 1.309(5) . ? C30 H30 0.9300 . ? C30 C31 1.331(6) . ? C30 N6 1.363(5) . ? C31 H31 0.9300 . ? C31 N5 1.379(5) . ? C32 H32 0.9300 . ? C32 N7 1.323(5) . ? C32 N8 1.310(5) . ? C33 H33 0.9300 . ? C33 C34 1.334(6) . ? C33 N8 1.371(6) . ? C34 H34 0.9300 . ? C34 N7 1.391(5) . ? N2 H2D 0.8600 . ? C21 H21 0.9300 . ? N6 H6D 0.8600 . ? N8 H8 0.8600 . ? O1 P1 1.507(2) . ? O2 H2 0.8200 . ? O2 P1 1.556(3) . ? O3 La1 2.414(2) 2_765 ? O3 P1 1.505(2) . ? O4 H4 0.8200 . ? O5 La1 2.561(2) 2_765 ? O5 P2 1.526(2) . ? O6 H6 0.8200 . ? O6 P2 1.557(2) . ? O7 P2 1.507(2) . ? O8 P3 1.513(2) . ? O9 H9 0.8200 . ? O9 P3 1.559(3) . ? O10 P3 1.511(2) . ? O11 H11 0.8200 . ? O12 P4 1.509(2) . ? O13 H13 0.8200 . ? O13 P4 1.580(3) . ? O14 P4 1.504(2) . ? O15 P6 1.518(2) . ? O16 H16 0.8200 . ? O16 P6 1.569(2) . ? O17 P6 1.498(2) . ? O18 H18 0.8200 . ? O19 H19 0.8200 . ? O19 P5 1.565(3) . ? O20 P5 1.511(2) . ? O21 P5 1.501(3) . ? O22 P7 1.509(3) . ? O23 H23 0.8200 . ? O23 P7 1.566(3) . ? O24 La2 2.481(2) 2_656 ? O24 P7 1.497(3) . ? O25 H25 0.8200 . ? O26 La2 2.569(2) 2_656 ? O26 P8 1.510(3) . ? O27 H27 0.8200 . ? O27 P8 1.575(3) . ? O28 P8 1.490(3) . ? O29 H29 0.8200 . ? O30 P9 1.532(3) . ? O31 P9 1.521(3) . ? O32 P9 1.526(3) . ? O34 P10 1.493(3) . ? O35 H35 0.8200 . ? O35 P10 1.601(3) . ? O36 P10 1.500(3) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag La1 O1 P1 C1 92.55(15) . . . . ? La1 O1 P1 O2 -149.19(12) . . . . ? La1 O1 P1 O3 -24.99(17) . . . . ? La1 O3 P1 C1 25.9(3) 2_765 . . . ? La1 O3 P1 O1 145.1(3) 2_765 . . . ? La1 O3 P1 O2 -91.9(3) 2_765 . . . ? La1 O5 P2 C1 47.4(2) 2_765 . . . ? La1 O5 P2 O6 162.86(16) 2_765 . . . ? La1 O5 P2 O7 -72.1(2) 2_765 . . . ? La1 O7 P2 C1 -64.3(2) . . . . ? La1 O7 P2 O5 55.4(2) . . . . ? La1 O7 P2 O6 177.29(15) . . . . ? La1 O8 P3 C3 25.6(3) . . . . ? La1 O8 P3 O9 142.0(2) . . . . ? La1 O8 P3 O10 -94.9(2) . . . . ? La1 O14 P4 C3 -26.7(3) . . . . ? La1 O14 P4 O12 97.0(2) . . . . ? La1 O14 P4 O13 -140.5(2) . . . . ? La1 O15 P6 C5 44.6(3) . . . . ? La1 O15 P6 O16 164.5(2) . . . . ? La1 O15 P6 O17 -74.9(3) . . . . ? La1 O20 P5 C5 69.0(2) . . . . ? La1 O20 P5 O19 -177.23(15) . . . . ? La1 O20 P5 O21 -51.3(2) . . . . ? La2 O10 P3 C3 -50.3(3) . . . . ? La2 O10 P3 O8 71.1(3) . . . . ? La2 O10 P3 O9 -165.2(2) . . . . ? La2 O12 P4 C3 48.2(2) . . . . ? La2 O12 P4 O13 165.12(17) . . . . ? La2 O12 P4 O14 -75.5(2) . . . . ? La2 O17 P6 C5 -27.1(3) . . . . ? La2 O17 P6 O15 93.5(3) . . . . ? La2 O17 P6 O16 -143.5(2) . . . . ? La2 O22 P7 C7 61.5(3) . . . . ? La2 O22 P7 O23 175.9(2) . . . . ? La2 O22 P7 O24 -57.4(3) . . . . ? La2 O24 P7 C7 -47.4(3) 2_656 . . . ? La2 O24 P7 O22 72.1(3) 2_656 . . . ? La2 O24 P7 O23 -164.1(2) 2_656 . . . ? La2 O26 P8 C7 49.8(3) 2_656 . . . ? La2 O26 P8 O27 167.4(2) 2_656 . . . ? La2 O26 P8 O28 -72.9(2) 2_656 . . . ? La2 O28 P8 C7 -59.7(3) . . . . ? La2 O28 P8 O26 61.4(3) . . . . ? La2 O28 P8 O27 -176.2(2) . . . . ? Li1 O7 P2 C1 113.9(4) . . . . ? Li1 O7 P2 O5 -126.4(4) . . . . ? Li1 O7 P2 O6 -4.5(5) . . . . ? Li1 O8 P3 C3 -146.8(3) . . . . ? Li1 O8 P3 O9 -30.3(4) . . . . ? Li1 O8 P3 O10 92.7(3) . . . . ? Li1 O20 P5 C5 -91.1(4) . . . . ? Li1 O20 P5 O19 22.7(4) . . . . ? Li1 O20 P5 O21 148.7(4) . . . . ? Li1 O30 P9 C9 -153.2(3) . . . . ? Li1 O30 P9 O31 -37.6(3) . . . . ? Li1 O30 P9 O32 88.6(3) . . . . ? C2 C1 P1 O1 44.3(3) . . . . ? C2 C1 P1 O2 -75.5(3) . . . . ? C2 C1 P1 O3 163.8(2) . . . . ? C2 C1 P2 O5 166.9(2) . . . . ? C2 C1 P2 O6 52.7(3) . . . . ? C2 C1 P2 O7 -68.4(3) . . . . ? C0AA C3 P3 O8 178.6(3) . . . . ? C0AA C3 P3 O9 59.8(3) . . . . ? C0AA C3 P3 O10 -56.9(3) . . . . ? C0AA C3 P4 O12 56.8(3) . . . . ? C0AA C3 P4 O13 -63.0(3) . . . . ? C0AA C3 P4 O14 -176.3(3) . . . . ? C6 C5 P5 O19 45.2(3) . . . . ? C6 C5 P5 O20 160.6(3) . . . . ? C6 C5 P5 O21 -72.7(3) . . . . ? C6 C5 P6 O15 151.9(3) . . . . ? C6 C5 P6 O16 31.0(3) . . . . ? C6 C5 P6 O17 -83.7(3) . . . . ? C8 C7 P7 O22 65.7(3) . . . . ? C8 C7 P7 O23 -49.1(3) . . . . ? C8 C7 P7 O24 -169.8(2) . . . . ? C8 C7 P8 O26 167.3(3) . . . . ? C8 C7 P8 O27 48.5(3) . . . . ? C8 C7 P8 O28 -65.8(3) . . . . ? C10 C9 P9 O30 88.9(3) . . . . ? C10 C9 P9 O31 -29.3(3) . . . . ? C10 C9 P9 O32 -150.3(3) . . . . ? C10 C9 P10 O34 64.6(3) . . . . ? C10 C9 P10 O35 -179.1(3) . . . . ? C10 C9 P10 O36 -65.3(3) . . . . ? C11 C11 C12 C13 -176.3(4) 2_675 . . . ? C11 C11 C16 C15 177.2(4) 2_675 . . . ? C11 C12 C13 C14 -0.8(6) . . . . ? C11 C12 C13 N3 178.0(3) . . . . ? C12 C11 C16 C15 -1.6(5) . . . . ? C12 C13 C14 C15 -1.9(5) . . . . ? C12 C13 N3 C20 157.8(4) . . . . ? C12 C13 N3 C22 -26.2(5) . . . . ? C13 C14 C15 C16 2.9(6) . . . . ? C13 C14 C15 N1 -177.9(3) . . . . ? C14 C13 N3 C20 -23.4(5) . . . . ? C14 C13 N3 C22 152.6(4) . . . . ? C14 C15 C16 C11 -1.1(6) . . . . ? C14 C15 N1 C17 -101.0(5) . . . . ? C14 C15 N1 C19 68.9(5) . . . . ? C16 C11 C12 C13 2.5(5) . . . . ? C16 C15 N1 C17 78.2(6) . . . . ? C16 C15 N1 C19 -111.9(5) . . . . ? C17 C18 N2 C19 0.3(6) . . . . ? C18 C17 N1 C15 170.8(4) . . . . ? C18 C17 N1 C19 -0.4(6) . . . . ? N4 C22 N3 C13 -177.5(3) . . . . ? N4 C22 N3 C20 -0.9(4) . . . . ? C22 N4 C21 C20 0.4(5) . . . . ? C23 C23 C24 C25 -179.1(4) 2_566 . . . ? C23 C23 C28 C27 179.4(4) 2_566 . . . ? C23 C24 C25 C26 -0.1(6) . . . . ? C23 C24 C25 N5 -179.2(3) . . . . ? C24 C23 C28 C27 0.7(6) . . . . ? C24 C25 C26 C27 0.4(6) . . . . ? C24 C25 N5 C29 -40.4(5) . . . . ? C24 C25 N5 C31 135.7(4) . . . . ? C25 C26 C27 C28 -0.1(5) . . . . ? C25 C26 C27 N7 176.5(3) . . . . ? C26 C25 N5 C29 140.5(4) . . . . ? C26 C25 N5 C31 -43.5(5) . . . . ? C26 C27 C28 C23 -0.4(6) . . . . ? C26 C27 N7 C32 127.3(4) . . . . ? C26 C27 N7 C34 -57.7(5) . . . . ? C28 C23 C24 C25 -0.4(6) . . . . ? C28 C27 N7 C32 -56.0(5) . . . . ? C28 C27 N7 C34 119.0(5) . . . . ? C30 C31 N5 C25 -175.8(4) . . . . ? C30 C31 N5 C29 0.7(5) . . . . ? C31 C30 N6 C29 0.0(5) . . . . ? C33 C34 N7 C27 -177.3(4) . . . . ? C33 C34 N7 C32 -1.6(5) . . . . ? C34 C33 N8 C32 1.1(6) . . . . ? N1 C15 C16 C11 179.7(3) . . . . ? N1 C17 C18 N2 0.0(6) . . . . ? N1 C19 N2 C18 -0.6(6) . . . . ? N2 C19 N1 C15 -171.1(4) . . . . ? N2 C19 N1 C17 0.6(6) . . . . ? N3 C13 C14 C15 179.3(3) . . . . ? N3 C20 C21 N4 -0.9(5) . . . . ? C21 C20 N3 C13 177.7(4) . . . . ? C21 C20 N3 C22 1.1(5) . . . . ? C21 N4 C22 N3 0.4(5) . . . . ? N5 C25 C26 C27 179.5(3) . . . . ? N5 C29 N6 C30 0.4(5) . . . . ? N6 C29 N5 C25 175.9(3) . . . . ? N6 C29 N5 C31 -0.7(5) . . . . ? N6 C30 C31 N5 -0.4(5) . . . . ? N7 C27 C28 C23 -177.0(3) . . . . ? N7 C32 N8 C33 -2.2(5) . . . . ? N8 C32 N7 C27 178.1(3) . . . . ? N8 C32 N7 C34 2.3(5) . . . . ? N8 C33 C34 N7 0.3(6) . . . . ? O4 C1 P1 O1 163.4(2) . . . . ? O4 C1 P1 O2 43.6(3) . . . . ? O4 C1 P1 O3 -77.1(2) . . . . ? O4 C1 P2 O5 47.2(3) . . . . ? O4 C1 P2 O6 -67.0(3) . . . . ? O4 C1 P2 O7 171.8(2) . . . . ? O11 C3 P3 O8 60.5(3) . . . . ? O11 C3 P3 O9 -58.4(3) . . . . ? O11 C3 P3 O10 -175.1(2) . . . . ? O11 C3 P4 O12 174.1(2) . . . . ? O11 C3 P4 O13 54.2(3) . . . . ? O11 C3 P4 O14 -59.0(3) . . . . ? O18 C5 P5 O19 -72.9(3) . . . . ? O18 C5 P5 O20 42.6(3) . . . . ? O18 C5 P5 O21 169.2(2) . . . . ? O18 C5 P6 O15 -92.5(2) . . . . ? O18 C5 P6 O16 146.6(2) . . . . ? O18 C5 P6 O17 31.8(3) . . . . ? O25 C7 P7 O22 -175.5(2) . . . . ? O25 C7 P7 O23 69.7(3) . . . . ? O25 C7 P7 O24 -51.0(3) . . . . ? O25 C7 P8 O26 49.4(3) . . . . ? O25 C7 P8 O27 -69.3(3) . . . . ? O25 C7 P8 O28 176.3(2) . . . . ? O29 C9 P9 O30 -29.9(3) . . . . ? O29 C9 P9 O31 -148.1(2) . . . . ? O29 C9 P9 O32 90.9(3) . . . . ? O29 C9 P10 O34 -179.8(2) . . . . ? O29 C9 P10 O35 -63.5(3) . . . . ? O29 C9 P10 O36 50.4(3) . . . . ? P1 C1 P2 O5 -74.24(18) . . . . ? P1 C1 P2 O6 171.53(15) . . . . ? P1 C1 P2 O7 50.42(19) . . . . ? P2 C1 P1 O1 -75.16(19) . . . . ? P2 C1 P1 O2 165.07(15) . . . . ? P2 C1 P1 O3 44.3(2) . . . . ? P3 C3 P4 O12 -64.2(2) . . . . ? P3 C3 P4 O13 175.94(16) . . . . ? P3 C3 P4 O14 62.7(2) . . . . ? P4 C3 P3 O8 -61.9(2) . . . . ? P4 C3 P3 O9 179.23(16) . . . . ? P4 C3 P3 O10 62.5(2) . . . . ? P5 C5 P6 O15 25.9(2) . . . . ? P5 C5 P6 O16 -94.96(19) . . . . ? P5 C5 P6 O17 150.28(16) . . . . ? P6 C5 P5 O19 171.44(16) . . . . ? P6 C5 P5 O20 -73.1(2) . . . . ? P6 C5 P5 O21 53.5(2) . . . . ? P7 C7 P8 O26 -69.1(2) . . . . ? P7 C7 P8 O27 172.17(15) . . . . ? P7 C7 P8 O28 57.8(2) . . . . ? P8 C7 P7 O22 -57.5(2) . . . . ? P8 C7 P7 O23 -172.31(15) . . . . ? P8 C7 P7 O24 67.0(2) . . . . ? P9 C9 P10 O34 -58.8(2) . . . . ? P9 C9 P10 O35 57.6(2) . . . . ? P9 C9 P10 O36 171.38(19) . . . . ? P10 C9 P9 O30 -148.54(18) . . . . ? P10 C9 P9 O31 93.3(2) . . . . ? P10 C9 P9 O32 -27.7(2) . . . . ?