#------------------------------------------------------------------------------ #$Date: 2024-10-03 01:10:38 +0300 (Thu, 03 Oct 2024) $ #$Revision: 294989 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572731.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572731 loop_ _publ_author_name 'Ma, Yu-Juan' 'Xu, Fei' 'Ren, Xin-Ye' 'Chen, Fan-Yao' 'Pan, Jie' 'Li, Jinhua' 'Han, Song-De' 'Wang, Guo-Ming' _publ_section_title ; Photoinduced electron-transfer strategy for switchable fluorescence and phosphorescence in lanthanide-based coordination polymers ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC04632C _journal_year 2024 _chemical_formula_moiety 'C34 H57 La2 Li N8 O38 P10' _chemical_formula_sum 'C34 H57 La2 Li N8 O38 P10' _chemical_formula_weight 1780.28 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-05-14 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-05-14 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 68.463(2) _cell_angle_beta 69.625(2) _cell_angle_gamma 79.152(2) _cell_formula_units_Z 2 _cell_length_a 12.1985(2) _cell_length_b 16.4328(3) _cell_length_c 16.9643(4) _cell_measurement_reflns_used 22808 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 30.6900 _cell_measurement_theta_min 1.9620 _cell_volume 2958.13(11) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'multiwire proportional' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0453 _diffrn_reflns_av_unetI/netI 0.0359 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 44686 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.010 _diffrn_reflns_theta_max 25.010 _diffrn_reflns_theta_min 1.883 _diffrn_source 'Rotating-anode X-ray tube' _exptl_absorpt_coefficient_mu 1.806 _exptl_absorpt_correction_T_max 0.965 _exptl_absorpt_correction_T_min 0.897 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.110a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.992 _exptl_crystal_description stick _exptl_crystal_F_000 1764 _exptl_crystal_size_max 0.20 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.680 _refine_diff_density_min -0.784 _refine_diff_density_rms 0.108 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.118 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 843 _refine_ls_number_reflns 10438 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.118 _refine_ls_R_factor_all 0.0387 _refine_ls_R_factor_gt 0.0334 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0334P)^2^+7.1813P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0838 _refine_ls_wR_factor_ref 0.0859 _reflns_Friedel_coverage 0.000 _reflns_number_gt 9218 _reflns_number_total 10438 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04632c2.cif _cod_data_source_block Laa _cod_original_cell_volume 2958.14(12) _cod_database_code 1572731 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: C12(H12A), C14(H14), C17(H17), C18(H18A), C20(H20A), N4(H4A), C22(H22), C24(H24), C26(H26), C28(H28), C29(H29A), C30(H30), C31(H31), C32(H32A), C33(H33), C34(H34), C19A(H19A), C16C(H16C), N2(H2D), C4(H4B), N6(H6), N8(H8) 2.b Tetrahedral OH refined with riding coordinates: O2(H2), O4(H4), O5(H5), O9(H9), O11(H11), O12(H12), O16(H16), O18(H18), O20(H20), O23(H23), O25(H25), O27(H27), O29(H29), O32(H32) 2.c Idealised Me refined as rotating group: C2(H2A,H2B,H2C), C1AA(H1AA,H1AB,H1AC), C2AA(H2AA,H2AB,H2AC), C0AA(H0AA,H0AB, H0AC), C10B(H10A,H10B,H10C) ; _shelx_res_file ; TITL 1_a.res in P-1 1.res created by SHELXL-2018/3 at 17:55:00 on 14-May-2024 CELL 0.71073 12.1985 16.4328 16.9643 68.463 69.625 79.152 ZERR 2 0.0002 0.0003 0.0004 0.002 0.002 0.002 LATT 1 SFAC C H N O P La Li UNIT 68 102 16 76 20 4 2 L.S. 8 PLAN 5 FREE P9 Li1 FREE La1 Li1 FREE La1 P1 BOND LIST 4 fmap 2 acta OMIT 0 50.02 REM REM REM WGHT 0.033400 7.181300 FVAR 0.27561 C1 1 0.103700 0.336538 0.903426 11.00000 0.01866 0.01803 = 0.01641 -0.00540 -0.00315 -0.00607 C2 1 0.194866 0.323739 0.820395 11.00000 0.02350 0.04042 = 0.01994 -0.01650 -0.00029 -0.00396 AFIX 137 H2A 2 0.245334 0.272373 0.837028 11.00000 -1.50000 H2B 2 0.240561 0.374049 0.788760 11.00000 -1.50000 H2C 2 0.156364 0.316701 0.782880 11.00000 -1.50000 AFIX 0 C3 1 0.266778 0.652636 0.610499 11.00000 0.02177 0.02505 = 0.01684 -0.00831 -0.00207 -0.00779 C1AA 1 0.321996 0.686491 0.510296 11.00000 0.02968 0.05363 = 0.01087 -0.01194 0.00056 -0.00412 AFIX 137 H1AA 2 0.378497 0.642712 0.491621 11.00000 -1.50000 H1AB 2 0.360188 0.738886 0.494038 11.00000 -1.50000 H1AC 2 0.262240 0.699295 0.481829 11.00000 -1.50000 AFIX 0 C5 1 0.376573 0.748594 0.878673 11.00000 0.02042 0.02541 = 0.02246 -0.00806 -0.00246 -0.00688 C2AA 1 0.448711 0.804935 0.893610 11.00000 0.03529 0.03177 = 0.04797 -0.00966 -0.01859 -0.01245 AFIX 137 H2AA 2 0.522925 0.774171 0.897081 11.00000 -1.50000 H2AB 2 0.407269 0.816920 0.948170 11.00000 -1.50000 H2AC 2 0.461308 0.859147 0.844972 11.00000 -1.50000 AFIX 0 C7 1 0.729536 0.964182 0.582158 11.00000 0.01783 0.02294 = 0.02145 -0.00817 -0.00670 -0.00371 C0AA 1 0.763868 0.895173 0.660442 11.00000 0.03864 0.03306 = 0.03295 -0.00968 -0.01934 0.00113 AFIX 137 H0AA 2 0.838312 0.866093 0.638736 11.00000 -1.50000 H0AB 2 0.705529 0.852996 0.692213 11.00000 -1.50000 H0AC 2 0.769365 0.923007 0.699633 11.00000 -1.50000 AFIX 0 C9 1 0.670952 0.331533 0.747449 11.00000 0.02069 0.03078 = 0.02929 -0.01458 -0.00586 -0.00566 C11 1 0.052201 0.472833 0.482984 11.00000 0.02310 0.03442 = 0.02386 -0.01116 -0.00694 -0.00246 C12 1 0.077397 0.458684 0.401804 11.00000 0.02210 0.03865 = 0.02884 -0.01632 -0.01040 0.00298 AFIX 43 H12A 2 0.027527 0.484038 0.367066 11.00000 -1.20000 AFIX 0 C13 1 0.175919 0.407275 0.372943 11.00000 0.02391 0.03565 = 0.02365 -0.01765 -0.00418 -0.00508 C14 1 0.253998 0.369349 0.420114 11.00000 0.02505 0.02813 = 0.02933 -0.01360 -0.01044 0.00185 AFIX 43 H14 2 0.320131 0.335157 0.399618 11.00000 -1.20000 AFIX 0 C15 1 0.229569 0.384441 0.499670 11.00000 0.02439 0.03301 = 0.02415 -0.01152 -0.01037 -0.00389 C17 1 0.129824 0.369683 0.261159 11.00000 0.02764 0.04137 = 0.02476 -0.01127 -0.00461 -0.01377 AFIX 43 H17 2 0.055383 0.351065 0.295869 11.00000 -1.20000 AFIX 0 C18 1 0.288268 0.406056 0.147820 11.00000 0.03488 0.07724 = 0.03318 -0.03047 0.00337 -0.01156 AFIX 43 H18A 2 0.341527 0.415085 0.091153 11.00000 -1.20000 AFIX 0 C20 1 0.355954 0.261851 0.570872 11.00000 0.03167 0.02821 = 0.03755 -0.01699 -0.01905 0.00360 AFIX 43 H20A 2 0.349690 0.219853 0.548217 11.00000 -1.20000 AFIX 0 N4 3 0.415213 0.251875 0.628096 11.00000 0.04273 0.05290 = 0.04904 -0.01352 -0.01784 0.00100 AFIX 43 H4A 2 0.454512 0.205150 0.650691 11.00000 -1.20000 AFIX 0 C22 1 0.337160 0.385928 0.597628 11.00000 0.02972 0.03289 = 0.03095 -0.01731 -0.00699 -0.00255 AFIX 43 H22 2 0.316151 0.443718 0.596323 11.00000 -1.20000 AFIX 0 C23 1 0.561823 0.984939 -0.000065 11.00000 0.02643 0.02324 = 0.02508 -0.00817 -0.00243 -0.00616 C24 1 0.648251 0.972022 -0.075476 11.00000 0.03089 0.02883 = 0.02322 -0.00871 -0.00422 -0.00308 AFIX 43 H24 2 0.628371 0.980053 -0.126145 11.00000 -1.20000 AFIX 0 C25 1 0.761477 0.947701 -0.074824 11.00000 0.02488 0.02667 = 0.02069 -0.00828 0.00235 -0.00139 C26 1 0.796307 0.934605 -0.001567 11.00000 0.02396 0.03480 = 0.02881 -0.01408 -0.00460 0.00150 AFIX 43 H26 2 0.874299 0.919971 -0.003099 11.00000 -1.20000 AFIX 0 C27 1 0.711056 0.944045 0.074012 11.00000 0.02968 0.02623 = 0.02325 -0.01136 -0.00465 -0.00310 C28 1 0.594669 0.967187 0.075904 11.00000 0.02595 0.03697 = 0.02371 -0.01346 -0.00029 -0.00383 AFIX 43 H28 2 0.538249 0.970857 0.128290 11.00000 -1.20000 AFIX 0 C29 1 0.904518 0.857409 -0.154889 11.00000 0.07164 0.02497 = 0.02604 -0.00308 0.00091 0.00902 AFIX 43 H29A 2 0.882233 0.803686 -0.111880 11.00000 -1.20000 AFIX 0 C30 1 0.997587 0.954944 -0.274188 11.00000 0.04155 0.05261 = 0.03200 -0.01517 0.00877 -0.00897 AFIX 43 H30 2 1.051779 0.980550 -0.328827 11.00000 -1.20000 AFIX 0 C31 1 0.910410 0.996791 -0.227035 11.00000 0.04994 0.02639 = 0.03171 -0.00484 0.00551 -0.00186 AFIX 43 H31 2 0.892699 1.057074 -0.242536 11.00000 -1.20000 AFIX 0 C32 1 0.843767 0.878915 0.171024 11.00000 0.03588 0.04297 = 0.04277 -0.02425 -0.01382 0.00694 AFIX 43 H32A 2 0.898639 0.847138 0.137537 11.00000 -1.20000 AFIX 0 C33 1 0.844420 0.885467 0.247123 11.00000 0.04414 0.03977 = 0.04664 -0.02396 -0.02234 0.00841 AFIX 43 H33 2 0.899385 0.858291 0.277065 11.00000 -1.20000 AFIX 0 C34 1 0.690985 0.965047 0.214728 11.00000 0.03436 0.02407 = 0.02768 -0.01106 -0.00301 -0.00251 AFIX 43 H34 2 0.623127 1.002263 0.217460 11.00000 -1.20000 AFIX 0 C19A 1 0.302037 0.423770 0.215139 11.00000 0.02451 0.08292 = 0.03983 -0.02938 0.00311 -0.01883 AFIX 43 H19A 2 0.365643 0.448255 0.213945 11.00000 -1.20000 AFIX 0 C10B 1 0.704601 0.395394 0.651991 11.00000 0.04093 0.03135 = 0.03754 -0.00882 -0.00161 -0.00938 AFIX 137 H10A 2 0.690117 0.454525 0.653041 11.00000 -1.50000 H10B 2 0.658542 0.386933 0.620190 11.00000 -1.50000 H10C 2 0.786245 0.384769 0.622884 11.00000 -1.50000 AFIX 0 C16C 1 0.131225 0.434485 0.531315 11.00000 0.02836 0.03848 = 0.02371 -0.01473 -0.01074 0.00251 AFIX 43 H16C 2 0.117624 0.442665 0.585442 11.00000 -1.20000 AFIX 0 LA1 6 0.127624 0.594923 0.884642 11.00000 0.01661 0.01570 = 0.01307 -0.00449 -0.00281 -0.00208 LA2 6 0.406141 0.863031 0.620153 11.00000 0.01630 0.01700 = 0.01806 -0.00596 -0.00237 -0.00514 LI1 7 0.375758 0.497261 0.870512 11.00000 0.02532 0.02473 = 0.03444 -0.01087 -0.01060 -0.00118 N1 3 0.201928 0.398038 0.286731 11.00000 0.02021 0.03580 = 0.02090 -0.01524 -0.00579 -0.00220 N2 3 0.181412 0.372343 0.178377 11.00000 0.02925 0.04476 = 0.03130 -0.02070 -0.01118 -0.00445 AFIX 43 H2D 2 0.152350 0.355419 0.147941 11.00000 -1.20000 AFIX 0 N3 3 0.306789 0.346243 0.552756 11.00000 0.02540 0.02734 = 0.02434 -0.01271 -0.01007 0.00051 C4 1 0.401340 0.329378 0.643473 11.00000 0.01493 0.02780 = 0.01496 -0.01249 -0.00836 0.00048 AFIX 43 H4B 2 0.432823 0.340359 0.680961 11.00000 -1.20000 AFIX 0 N5 3 0.852175 0.934743 -0.151947 11.00000 0.02772 0.02184 = 0.02050 -0.00554 -0.00128 0.00095 N6 3 0.992366 0.868556 -0.227748 11.00000 0.04514 0.04104 = 0.02980 -0.01658 -0.01127 0.02121 AFIX 43 H6 2 1.039477 0.827442 -0.243687 11.00000 -1.20000 AFIX 0 N7 3 0.745173 0.928808 0.151653 11.00000 0.02821 0.02920 = 0.02585 -0.01356 -0.00413 -0.00164 N8 3 0.749705 0.939295 0.272637 11.00000 0.04869 0.02766 = 0.02851 -0.01499 -0.01139 -0.00077 AFIX 43 H8 2 0.731116 0.954184 0.319496 11.00000 -1.20000 AFIX 0 O1 4 0.081784 0.509029 0.802162 11.00000 0.02588 0.02409 = 0.01907 -0.00022 -0.00658 -0.01251 O2 4 -0.076854 0.413906 0.833653 11.00000 0.02542 0.03288 = 0.02468 -0.00961 -0.00789 -0.01243 AFIX 83 H2 2 -0.114027 0.372273 0.870847 11.00000 -1.50000 AFIX 0 O3 4 -0.055534 0.459913 0.955015 11.00000 0.03178 0.02418 = 0.01533 -0.00916 -0.00473 0.00330 O4 4 0.037861 0.259171 0.949307 11.00000 0.02830 0.01974 = 0.02525 -0.00696 -0.00041 -0.01106 AFIX 83 H4 2 -0.011897 0.264404 0.994704 11.00000 -1.50000 AFIX 0 O5 4 0.270657 0.275969 0.990882 11.00000 0.01981 0.02580 = 0.02199 -0.00306 -0.00086 0.00088 AFIX 83 H5 2 0.317318 0.274957 0.942815 11.00000 -1.50000 AFIX 0 O6 4 0.084179 0.342709 1.065881 11.00000 0.01682 0.02171 = 0.01609 -0.00837 -0.00275 -0.00172 O7 4 0.227606 0.440354 0.927638 11.00000 0.01670 0.01987 = 0.01927 -0.00623 -0.00331 -0.00402 O8 4 0.322391 0.590242 0.765859 11.00000 0.02180 0.02951 = 0.01699 -0.00728 -0.00205 -0.00165 O9 4 0.466655 0.555191 0.632854 11.00000 0.02948 0.02165 = 0.02889 -0.00930 0.00234 0.00097 AFIX 83 H9 2 0.432555 0.510634 0.648964 11.00000 -1.50000 AFIX 0 O10 4 0.442468 0.708240 0.636342 11.00000 0.02014 0.02061 = 0.03571 -0.00773 -0.00832 -0.00454 O11 4 0.209852 0.574296 0.631355 11.00000 0.03970 0.02876 = 0.03233 -0.01508 -0.00467 -0.01398 AFIX 83 H11 2 0.179259 0.554355 0.685309 11.00000 -1.50000 AFIX 0 O12 4 0.062849 0.751153 0.597205 11.00000 0.02002 0.04033 = 0.01759 -0.00374 -0.00652 -0.01104 AFIX 83 H12 2 0.093520 0.765113 0.543152 11.00000 -1.50000 AFIX 0 O13 4 0.097220 0.704150 0.742441 11.00000 0.01947 0.02413 = 0.01449 -0.00611 -0.00186 0.00027 O14 4 0.218726 0.822057 0.612480 11.00000 0.02046 0.01966 = 0.02632 -0.00132 -0.00872 -0.00649 O15 4 0.314593 0.584671 0.931522 11.00000 0.02633 0.02334 = 0.02690 -0.01095 -0.01031 -0.00222 O16 4 0.464511 0.606188 0.990300 11.00000 0.02397 0.04112 = 0.03161 -0.01469 -0.01286 0.00151 AFIX 83 H16 2 0.488680 0.642172 1.002220 11.00000 -1.50000 AFIX 0 O17 4 0.256168 0.662267 1.049098 11.00000 0.02437 0.02964 = 0.02104 -0.00962 -0.00266 -0.00534 O18 4 0.444770 0.733066 0.795604 11.00000 0.02656 0.04163 = 0.02862 -0.01558 0.00386 -0.00558 AFIX 83 H18 2 0.408970 0.702855 0.784943 11.00000 -1.50000 AFIX 0 O19 4 0.148138 0.738944 0.891845 11.00000 0.01956 0.02407 = 0.02377 -0.00544 -0.00595 -0.00715 O20 4 0.192249 0.871766 0.914752 11.00000 0.04145 0.02424 = 0.02369 -0.01110 -0.00364 -0.00719 AFIX 83 H20 2 0.175681 0.844225 0.968159 11.00000 -1.50000 AFIX 0 O21 4 0.264791 0.860680 0.763967 11.00000 0.02858 0.02854 = 0.01671 -0.00206 -0.00206 -0.00733 O22 4 0.620762 0.856113 0.548497 11.00000 0.01944 0.02573 = 0.03141 -0.01620 -0.00211 -0.00630 O23 4 0.832942 0.853157 0.482821 11.00000 0.01978 0.03113 = 0.05258 -0.02256 -0.00611 0.00028 AFIX 83 H23 2 0.890507 0.882302 0.458121 11.00000 -1.50000 AFIX 0 O24 4 0.711616 0.989730 0.420981 11.00000 0.04133 0.01971 = 0.02322 -0.00839 -0.01109 0.00203 O25 4 0.820928 1.025768 0.535162 11.00000 0.02126 0.02932 = 0.03134 -0.00740 -0.00770 -0.01191 AFIX 83 H25 2 0.804163 1.063807 0.492853 11.00000 -1.50000 AFIX 0 O26 4 0.575676 1.099993 0.538892 11.00000 0.02905 0.02749 = 0.02235 -0.00956 -0.00614 0.00401 O27 4 0.595401 1.054092 0.694633 11.00000 0.03835 0.03203 = 0.02311 -0.01195 -0.00768 -0.01142 AFIX 83 H27 2 0.652514 1.083035 0.675975 11.00000 -1.50000 AFIX 0 O28 4 0.494356 0.959805 0.660534 11.00000 0.02179 0.02853 = 0.03044 -0.01697 0.00324 -0.01263 O29 4 0.659208 0.163391 0.849793 11.00000 0.05127 0.03645 = 0.03814 -0.00236 -0.01718 0.00059 AFIX 83 H29 2 0.703037 0.172931 0.872231 11.00000 -1.50000 AFIX 0 O30 4 0.616460 0.200695 0.704194 11.00000 0.04152 0.03629 = 0.05307 -0.02328 -0.02005 -0.00401 O31 4 0.824237 0.196978 0.707096 11.00000 0.03161 0.03850 = 0.04671 -0.02518 -0.00893 0.00548 O32 4 0.751310 0.340799 0.787222 11.00000 0.02609 0.06861 = 0.05267 -0.03722 -0.01114 -0.00386 AFIX 83 H32 2 0.736549 0.307281 0.838666 11.00000 -1.50000 AFIX 0 O33 4 0.469999 0.272376 0.879754 11.00000 0.02431 0.02560 = 0.03252 -0.00625 -0.00155 0.00063 O34 4 0.519012 0.425309 0.851742 11.00000 0.02585 0.03441 = 0.03379 -0.01666 -0.01276 -0.00011 O35 4 0.452888 0.397851 0.740642 11.00000 0.03808 0.02549 = 0.03536 -0.01275 -0.01980 0.00177 P1 5 0.008383 0.435617 0.871989 11.00000 0.01921 0.01761 = 0.01409 -0.00489 -0.00383 -0.00579 P2 5 0.175698 0.352585 0.975291 11.00000 0.01552 0.01573 = 0.01477 -0.00425 -0.00262 -0.00337 P3 5 0.159350 0.738328 0.643682 11.00000 0.01677 0.01967 = 0.01353 -0.00444 -0.00340 -0.00448 P4 5 0.379473 0.626693 0.666305 11.00000 0.01731 0.01712 = 0.01711 -0.00639 -0.00151 -0.00273 P5 5 0.236337 0.806339 0.860842 11.00000 0.02035 0.01781 = 0.01546 -0.00502 -0.00290 -0.00590 P6 5 0.346252 0.643530 0.969756 11.00000 0.01855 0.02130 = 0.01954 -0.00702 -0.00677 -0.00332 P7 5 0.719463 0.915012 0.503982 11.00000 0.01687 0.01834 = 0.02126 -0.00939 -0.00412 -0.00217 P8 5 0.588236 1.024380 0.618929 11.00000 0.01974 0.02082 = 0.01790 -0.00893 -0.00330 -0.00534 P9 5 0.518147 0.357907 0.809502 11.00000 0.01961 0.02383 = 0.02321 -0.00910 -0.00698 -0.00174 P10 5 0.695699 0.217844 0.745661 11.00000 0.02848 0.02392 = 0.03139 -0.01170 -0.00997 -0.00010 O36 4 0.070074 0.859399 0.434682 11.00000 0.02958 0.03823 = 0.02876 -0.00733 -0.00893 -0.00914 O37 4 0.140989 0.841631 0.084574 11.00000 0.06579 0.06765 = 0.03726 -0.01552 -0.01758 0.00580 O38 4 0.007111 0.715226 0.272421 11.00000 0.04570 0.11241 = 0.17935 -0.09737 -0.03965 0.01900 HKLF 4 REM 1_a.res in P-1 REM wR2 = 0.0859, GooF = S = 1.118, Restrained GooF = 1.118 for all data REM R1 = 0.0334 for 9218 Fo > 4sig(Fo) and 0.0387 for all 10438 data REM 843 parameters refined using 0 restraints END WGHT 0.0293 10.0388 REM Highest difference peak 0.680, deepest hole -0.784, 1-sigma level 0.108 Q1 1 0.1147 0.8312 0.3855 11.00000 0.05 0.68 Q2 1 0.6688 1.1357 0.5587 11.00000 0.05 0.68 Q3 1 -0.1216 0.3341 0.9384 11.00000 0.05 0.67 Q4 1 0.1446 0.6114 0.6729 11.00000 0.05 0.65 Q5 1 0.1048 0.9056 0.4390 11.00000 0.05 0.64 ; _shelx_res_checksum 9130 _shelx_hkl_file ; 0 0 2 41.51 3.82 0 0 -2 49.68 4.03 0 0 -2 42.79 3.41 0 0 3 0.93 1.14 0 0 -3 2.54 1.35 0 0 4 3749.39 136.84 0 0 -4 3783.84 135.22 0 0 5 14.74 3.72 0 0 -5 19.93 3.84 0 0 -6 122.56 10.34 0 0 6 116.97 9.22 0 0 7 267.35 16.09 0 0 -7 265.08 17.33 0 0 -8 3988.60 147.41 0 0 8 3867.23 144.47 0 0 -9 59.92 9.61 0 0 -9 65.68 9.75 0 0 9 55.10 7.46 0 0 -10 15.68 6.01 0 0 -10 3.02 3.15 0 0 -10 21.39 5.96 0 0 10 9.91 3.80 0 0 -11 22.57 7.25 0 0 -11 19.94 6.39 0 0 -11 10.39 5.83 0 0 11 23.78 5.70 0 0 -11 14.89 6.37 0 0 -12 636.33 39.67 0 0 -12 594.87 37.02 0 0 12 611.72 33.46 0 0 -12 678.34 40.34 0 0 -12 675.38 39.75 0 0 -13 10.35 7.72 0 0 -13 23.48 8.55 0 0 -13 7.13 6.22 0 0 13 27.48 6.70 0 0 -13 20.51 7.64 0 0 -14 61.76 11.83 0 0 -14 69.41 14.27 0 0 -14 58.95 11.93 0 0 -14 54.06 11.95 0 0 14 65.43 9.77 0 0 -14 61.86 12.66 0 0 -15 11.07 6.50 0 0 -15 7.20 6.70 0 0 -15 6.74 6.92 0 0 -15 8.30 6.96 0 0 15 4.24 3.72 0 0 -15 4.73 5.82 0 0 15 1.27 3.06 0 0 16 384.12 21.10 0 0 -16 451.72 36.15 0 0 -16 453.77 34.44 0 0 -16 528.69 39.25 0 0 -16 453.67 35.59 0 0 16 459.58 29.77 0 0 16 449.04 21.65 0 0 -17 10.91 10.14 0 0 -17 30.08 10.42 0 0 17 13.28 3.92 0 0 -17 28.15 10.68 0 0 17 12.56 6.53 0 0 17 10.27 4.01 0 0 -18 60.54 15.21 0 0 -18 58.15 13.75 0 0 18 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361.00 26.39 -2 11 -6 327.05 17.10 2 -11 6 320.90 28.20 -2 11 -6 349.85 16.50 -2 11 -6 360.05 22.90 -2 11 -7 96.13 8.58 -2 11 -7 121.99 12.56 -2 11 -7 110.48 9.72 2 -11 7 134.26 15.65 -2 11 -8 10.74 3.62 2 -11 8 24.10 7.85 -2 11 -8 11.20 5.07 -2 11 -8 27.87 6.03 -2 11 -9 87.94 9.43 2 -11 9 108.37 15.13 -2 11 -9 85.15 11.85 -2 11 -9 96.31 10.89 -2 11 -10 504.44 27.87 2 -11 10 582.86 36.19 -2 11 -10 577.72 30.41 -2 11 -11 20.72 7.35 2 -11 11 33.54 9.61 -2 11 -11 18.87 6.24 -2 11 -11 34.31 9.07 -2 11 -12 19.29 5.85 -2 11 -12 6.79 9.72 -2 11 -12 16.71 6.34 2 -11 12 15.76 6.73 2 -11 13 60.13 12.21 -2 11 -13 90.66 13.28 2 -10 -18 13.18 8.13 2 -10 -18 3.04 11.28 2 -10 -17 29.84 10.11 2 -10 -17 31.11 11.95 2 -10 -17 11.47 10.01 2 -10 -16 30.21 11.25 2 -10 -16 41.49 13.23 2 -10 -16 10.81 10.69 2 -10 -15 406.80 32.34 2 -10 -15 453.94 36.55 2 -10 -15 411.35 36.50 2 -10 -14 -2.03 5.35 2 -10 -14 -2.67 7.85 2 -10 -14 -4.75 9.85 2 -10 -13 361.18 28.73 2 -10 -13 355.18 30.36 2 -10 -13 387.03 33.02 2 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48.97 8.87 -2 10 3 32.76 7.15 -2 10 2 9.07 2.76 -2 10 2 15.89 4.84 2 -10 -2 17.42 5.72 -2 10 2 9.74 5.35 2 -10 -2 13.33 4.40 -2 10 1 831.47 40.73 2 -10 -1 838.67 32.73 -2 10 1 856.60 33.51 -2 10 1 909.16 44.63 2 -10 -1 871.43 41.20 -2 10 0 7.87 3.30 -2 10 0 15.03 5.69 2 -10 0 4.21 3.54 -2 10 -1 264.25 17.55 -2 10 -1 249.34 19.81 -2 10 -2 37.20 6.26 2 -10 2 35.61 7.83 -2 10 -2 31.06 7.17 2 -10 3 953.85 40.42 -2 10 -3 971.63 48.45 -2 10 -3 950.78 43.64 2 -10 3 969.18 50.02 2 -10 4 25.08 4.60 -2 10 -4 24.82 3.48 2 -10 4 21.00 7.33 -2 10 -4 27.56 3.61 -2 10 -4 32.00 8.06 -2 10 -4 31.45 6.06 -2 10 -5 53.97 5.56 2 -10 5 68.89 12.06 -2 10 -5 68.28 6.42 -2 10 -5 73.93 9.00 -2 10 -5 69.56 6.53 -2 10 -6 81.91 8.01 2 -10 6 68.68 11.47 -2 10 -6 80.97 7.35 2 -10 6 84.98 14.11 -2 10 -6 68.57 9.13 -2 10 -6 69.71 7.54 -2 10 -7 769.32 34.47 2 -10 7 756.45 41.62 -2 10 -7 764.82 33.41 -2 10 -7 740.33 34.19 -2 10 -7 669.87 36.34 -2 10 -8 24.90 6.40 -2 10 -8 37.51 6.09 -2 10 -8 34.96 6.96 2 -10 8 15.99 6.71 -2 10 -8 30.59 6.71 -2 10 -9 11.33 4.13 -2 10 -9 18.67 5.38 -2 10 -9 10.66 5.27 2 -10 9 13.08 6.63 -2 10 -9 8.84 5.14 -2 10 -10 5.36 4.11 -2 10 -10 2.34 5.12 2 -10 10 6.63 5.96 -2 10 -10 6.71 5.98 -2 10 -11 526.30 30.57 2 -10 11 533.34 34.86 -2 10 -11 486.21 31.11 -2 10 -11 585.33 33.35 -2 10 -12 -7.87 8.87 2 -10 12 4.94 6.31 -2 10 -12 -1.50 4.62 -2 10 -13 41.38 8.79 -2 10 -13 56.80 12.01 -2 10 -13 55.10 10.61 2 -10 13 73.56 12.01 2 -10 14 48.76 10.89 -2 10 -14 41.98 11.47 -2 10 -15 711.92 43.72 2 -9 -19 5.69 10.56 2 -9 -18 332.77 31.92 2 -9 -18 338.28 34.39 2 -9 -17 42.34 12.34 2 -9 -17 49.02 15.47 2 -9 -16 16.27 8.68 2 -9 -16 46.16 13.13 2 -9 -15 213.39 23.66 2 -9 -15 254.28 27.66 2 -9 -15 298.21 28.99 2 -9 -14 495.31 35.43 2 -9 -14 493.02 37.93 2 -9 -14 528.79 40.21 2 -9 -13 -1.89 6.58 2 -9 -13 7.41 7.26 2 -9 -13 6.65 8.24 2 -9 -12 44.00 10.42 2 -9 -12 44.26 11.52 2 -9 -12 28.73 9.23 2 -9 -11 2.19 8.40 2 -9 -11 1.89 4.65 2 -9 -11 0.73 1.50 2 -9 -11 3.30 3.75 -2 9 11 -1.95 6.81 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52.48 -2 9 0 1220.93 45.46 -2 9 -1 155.55 12.01 -2 9 -1 137.49 13.88 -2 9 -1 127.00 6.92 -2 9 -2 19.62 5.61 -2 9 -2 18.72 4.45 2 -9 2 18.37 6.05 2 -9 3 6.01 4.86 -2 9 -3 5.43 3.79 -2 9 -3 8.60 3.41 -2 9 -3 9.91 2.37 2 -9 3 14.27 3.58 2 -9 4 1584.86 72.70 -2 9 -4 1603.94 59.37 2 -9 4 1565.65 60.33 -2 9 -4 1681.22 65.66 -2 9 -4 1573.15 60.05 2 -9 5 34.54 9.43 -2 9 -5 33.02 4.94 -2 9 -5 33.17 6.18 -2 9 -5 40.08 6.65 -2 9 -6 70.24 7.38 2 -9 6 60.80 11.51 2 -9 6 68.06 10.66 -2 9 -6 86.51 8.66 -2 9 -6 77.39 9.31 -2 9 -7 15.99 4.40 -2 9 -7 23.19 5.74 -2 9 -7 25.39 5.87 2 -9 7 22.79 7.15 -2 9 -7 13.64 5.20 -2 9 -8 1298.06 55.40 -2 9 -8 1428.42 57.78 2 -9 8 1374.53 62.07 -2 9 -8 1351.64 57.00 -2 9 -9 -1.12 5.61 -2 9 -9 3.46 4.29 -2 9 -9 3.07 3.92 2 -9 9 6.05 5.44 -2 9 -9 3.62 3.88 -2 9 -10 33.24 7.48 2 -9 10 46.16 9.46 -2 9 -10 22.59 7.57 -2 9 -10 51.91 9.65 -2 9 -11 46.94 8.74 2 -9 11 52.92 10.47 -2 9 -11 44.47 9.80 -2 9 -11 51.91 10.60 -2 9 -12 878.68 46.48 2 -9 12 944.31 49.02 -2 9 -12 959.25 49.23 -2 9 -12 963.59 49.62 -2 9 -13 3.01 5.23 2 -9 13 13.96 7.77 -2 9 -13 1.64 8.26 -2 9 -13 -1.72 9.48 2 -9 14 18.63 8.04 -2 9 -14 24.28 7.23 -2 9 -14 7.44 7.93 -2 9 -15 3.98 9.95 2 -9 15 15.52 7.07 -2 9 -16 533.03 38.81 2 -8 -19 62.88 15.18 2 -8 -18 3.15 8.29 2 -8 -18 -3.06 12.06 2 -8 -18 -2.70 7.51 2 -8 -17 370.36 34.62 2 -8 -17 273.88 28.78 2 -8 -16 158.18 22.04 2 -8 -16 194.38 22.05 2 -8 -15 76.86 15.96 -2 8 15 62.88 11.51 2 -8 -15 65.68 13.54 2 -8 -14 579.38 41.17 2 -8 -14 594.82 42.53 -2 8 14 584.21 36.52 2 -8 -14 525.50 37.17 2 -8 -13 1019.97 58.61 2 -8 -13 1153.33 62.25 -2 8 13 1058.82 54.53 2 -8 -13 1065.07 56.30 2 -8 -12 227.14 23.09 2 -8 -12 204.39 20.45 -2 8 12 222.27 23.65 2 -8 -11 -2.13 5.95 2 -8 -11 -1.90 5.30 2 -8 -11 1.89 1.17 2 -8 -11 3.23 4.97 -2 8 11 3.93 5.49 -2 8 10 21.63 7.33 2 -8 -10 13.52 5.95 2 -8 -10 15.37 3.09 2 -8 -10 27.89 9.18 2 -8 -10 19.96 8.11 -2 8 9 1106.90 57.01 2 -8 -9 1147.66 56.62 2 -8 -9 1200.14 59.73 2 -8 -9 1262.17 55.92 2 -8 -9 1105.94 45.04 2 -8 -8 102.03 13.42 -2 8 8 91.35 12.29 2 -8 -8 97.30 12.82 2 -8 -8 122.12 12.79 2 -8 -8 83.39 7.70 2 -8 -7 2032.83 83.62 -2 8 7 1860.02 80.71 2 -8 -7 2003.22 81.05 2 -8 -7 1923.29 79.62 2 -8 -7 1828.50 73.01 -2 8 6 281.28 21.47 2 -8 -6 263.99 20.53 -2 8 6 247.62 18.61 -2 8 5 1824.13 75.69 2 -8 -5 1760.34 74.76 2 -8 -5 1692.62 72.16 -2 8 5 1695.72 71.36 -2 8 4 35.24 7.13 2 -8 -4 39.51 7.43 2 -8 -4 25.47 5.46 -2 8 4 29.89 5.54 -2 8 3 173.06 14.68 2 -8 -3 163.42 14.66 2 -8 -3 173.07 13.55 -2 8 3 168.13 12.11 -2 8 2 342.94 18.24 -2 8 2 351.54 22.18 2 -8 -2 418.38 24.41 -2 8 2 334.93 23.00 2 -8 -2 377.69 21.44 -2 8 2 374.36 18.72 2 -8 -1 71.04 5.75 -2 8 1 55.57 5.46 -2 8 1 63.25 8.89 2 -8 -1 58.09 7.31 -2 8 1 57.96 5.54 2 -8 0 170.47 12.95 -2 8 0 164.83 14.59 -2 8 0 181.57 9.72 -2 8 0 183.39 13.08 2 -8 0 179.52 9.39 -2 8 -1 2789.54 100.47 -2 8 -1 2682.11 105.04 2 -8 1 2703.38 100.78 2 -8 1 2575.38 93.84 -2 8 -2 -1.20 3.53 -2 8 -2 2.99 2.41 2 -8 2 3.85 3.36 -2 8 -3 76.66 8.01 -2 8 -3 84.89 6.01 2 -8 3 85.11 11.18 2 -8 4 -0.39 2.11 -2 8 -4 1.80 1.38 2 -8 4 1.48 4.34 -2 8 -4 -1.02 2.76 -2 8 -4 0.78 2.19 -2 8 -5 755.70 31.64 2 -8 5 696.54 40.66 -2 8 -5 729.28 34.21 -2 8 -5 700.31 32.00 -2 8 -6 53.24 6.81 2 -8 6 59.84 11.44 2 -8 6 69.04 10.09 -2 8 -6 66.10 8.13 -2 8 -6 79.23 8.92 -2 8 -7 34.36 6.47 -2 8 -7 28.78 5.44 2 -8 7 29.86 7.20 -2 8 -7 24.43 5.69 -2 8 -8 137.62 12.92 -2 8 -8 165.56 14.22 2 -8 8 138.21 14.79 -2 8 -9 1582.36 68.97 2 -8 9 1672.72 73.07 -2 8 -9 1728.88 71.22 -2 8 -9 1671.59 71.33 -2 8 -10 -1.20 4.32 2 -8 10 1.43 6.78 -2 8 -10 5.27 7.64 -2 8 -10 9.51 5.51 -2 8 -11 -1.33 3.48 2 -8 11 7.22 5.53 -2 8 -11 12.06 6.42 -2 8 -12 5.79 4.66 2 -8 12 8.70 6.32 -2 8 -12 4.75 7.93 -2 8 -12 1.66 8.13 2 -8 13 835.45 42.71 -2 8 -13 767.91 44.01 -2 8 -13 788.76 45.15 -2 8 -14 26.98 8.04 2 -8 14 29.45 9.04 -2 8 -14 25.79 9.28 -2 8 -14 40.70 10.39 -2 8 -15 95.43 14.35 -2 8 -15 114.14 17.26 2 -8 15 112.50 14.04 -2 8 -16 -4.42 10.45 -2 8 -17 335.20 31.12 -2 8 -18 21.94 11.12 2 -7 -19 19.49 10.91 2 -7 -19 20.28 12.35 2 -7 -18 -3.10 14.16 2 -7 -18 -3.07 10.66 2 -7 -18 2.73 7.17 2 -7 -17 106.58 19.31 2 -7 -17 121.91 20.23 2 -7 -17 134.62 20.85 2 -7 -16 444.29 39.43 2 -7 -16 525.58 40.61 2 -7 -16 494.27 37.48 2 -7 -15 208.10 24.46 -2 7 15 183.03 19.57 2 -7 -15 204.96 22.41 2 -7 -14 192.25 22.51 -2 7 14 160.98 17.73 2 -7 -14 195.69 20.71 2 -7 -13 315.23 28.23 -2 7 13 311.35 24.52 2 -7 -13 282.06 24.90 2 -7 -12 884.26 52.41 2 -7 -12 987.75 55.18 -2 7 12 964.24 54.71 -2 7 12 953.44 54.28 2 -7 -12 983.92 51.05 2 -7 -11 -2.08 6.11 2 -7 -11 3.82 5.88 2 -7 -11 1.59 4.21 -2 7 11 -1.98 7.80 -2 7 11 -2.06 6.06 2 -7 -10 36.83 9.22 2 -7 -10 17.49 6.92 2 -7 -10 18.89 2.67 2 -7 -10 22.09 6.74 -2 7 10 25.37 8.61 -2 7 9 18.11 7.85 -2 7 9 38.31 7.41 2 -7 -9 23.13 5.98 2 -7 -9 22.79 3.49 2 -7 -9 18.04 6.96 2 -7 -9 30.26 8.01 -2 7 8 4078.28 157.84 2 -7 -8 4024.67 154.75 2 -7 -8 4036.86 145.21 2 -7 -8 4119.52 157.37 2 -7 -8 4183.83 160.28 -2 7 7 22.51 6.71 2 -7 -7 34.06 8.32 2 -7 -7 38.57 8.17 2 -7 -7 38.23 7.13 2 -7 -7 28.18 4.40 2 -7 -6 1072.01 48.51 2 -7 -6 1093.80 50.48 -2 7 6 1105.91 49.26 2 -7 -6 959.04 42.22 2 -7 -5 498.10 28.80 -2 7 5 463.03 26.54 -2 7 4 2638.05 101.93 2 -7 -4 2635.84 101.71 2 -7 -4 2465.16 98.36 -2 7 4 2492.95 97.84 -2 7 3 188.41 15.33 -2 7 3 192.40 13.10 2 -7 -3 219.86 16.51 2 -7 -3 195.60 14.11 -2 7 3 194.09 13.31 -2 7 2 532.46 24.88 -2 7 2 531.53 28.49 -2 7 2 538.25 29.48 2 -7 -2 546.96 29.17 2 -7 -2 564.22 27.24 -2 7 2 521.77 24.83 2 -7 -1 1.04 2.36 2 -7 -1 4.49 2.41 -2 7 1 1.07 2.44 -2 7 1 2.29 1.71 2 -7 0 1990.18 77.46 -2 7 0 2008.56 81.26 -2 7 0 2098.21 77.38 2 -7 0 1972.48 73.28 -2 7 -1 306.32 16.82 2 -7 1 304.83 17.00 -2 7 -1 262.43 19.02 2 -7 1 291.00 13.52 -2 7 -2 1236.33 48.95 -2 7 -2 1117.54 52.84 2 -7 2 1203.96 45.17 -2 7 -3 120.74 9.69 -2 7 -3 138.24 8.40 2 -7 3 131.56 13.46 2 -7 4 162.46 15.78 -2 7 -4 195.82 11.28 2 -7 4 176.58 9.54 -2 7 -4 185.55 12.66 -2 7 -5 18.87 3.85 -2 7 -5 15.73 3.87 2 -7 5 27.74 6.68 -2 7 -5 18.93 4.36 -2 7 -6 894.90 40.57 2 -7 6 947.14 43.91 2 -7 6 894.64 47.42 -2 7 -6 890.40 39.66 -2 7 -6 968.45 41.33 2 -7 7 896.79 44.11 -2 7 -7 906.28 41.18 -2 7 -7 956.42 42.56 2 -7 8 432.39 26.15 -2 7 -8 409.62 24.90 -2 7 -8 392.69 23.50 -2 7 -9 -1.12 3.74 -2 7 -9 1.22 4.08 2 -7 9 3.85 4.78 -2 7 -10 234.68 18.89 2 -7 10 272.52 20.49 -2 7 -10 238.67 20.41 -2 7 -11 339.32 25.32 -2 7 -11 327.81 23.32 2 -7 11 312.94 23.42 -2 7 -11 331.69 24.83 -2 7 -12 5.10 6.32 -2 7 -12 4.47 3.92 2 -7 12 4.05 4.36 -2 7 -12 -1.63 7.26 -2 7 -13 92.62 14.71 -2 7 -13 70.97 12.37 2 -7 13 104.39 12.79 -2 7 -13 84.69 13.94 -2 7 -14 485.69 34.72 -2 7 -14 392.20 30.23 2 -7 14 463.19 29.77 -2 7 -14 504.21 34.49 -2 7 -15 8.55 7.72 -2 7 -15 24.10 7.72 2 -7 15 14.22 6.76 -2 7 -15 20.23 9.04 2 -7 16 2.88 5.02 -2 7 -16 2.28 9.22 -2 7 -17 48.16 14.24 2 -7 18 163.14 18.79 -2 7 -18 225.05 26.02 -2 7 -18 203.32 22.77 2 -6 -19 41.56 13.99 2 -6 -19 38.13 13.13 2 -6 -18 18.33 8.99 2 -6 -18 9.22 10.29 2 -6 -18 2.76 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2 -6 -5 1295.52 57.52 2 -6 -5 1243.44 50.82 -2 6 5 1339.45 56.57 -2 6 4 674.72 32.86 2 -6 -4 727.03 35.84 -2 6 4 693.41 33.51 -2 6 3 3991.50 145.54 -2 6 3 3805.70 148.38 2 -6 -3 4115.70 149.57 -2 6 3 4017.84 145.77 -2 6 2 225.05 13.83 -2 6 2 240.24 16.67 2 -6 -2 258.17 17.23 2 -6 -2 257.49 15.37 -2 6 2 241.22 14.22 2 -6 -1 1053.66 43.96 2 -6 -1 1058.50 46.99 -2 6 1 1066.04 42.09 2 -6 0 177.28 11.73 2 -6 0 156.90 9.52 -2 6 -1 152.76 10.17 2 -6 1 153.00 8.70 -2 6 -1 137.58 12.37 2 -6 1 163.12 10.69 2 -6 2 37.14 3.92 -2 6 -2 35.19 4.45 -2 6 -2 38.08 4.00 -2 6 -3 239.09 13.93 2 -6 3 255.34 18.20 -2 6 -3 249.99 12.97 -2 6 -4 993.15 41.62 -2 6 -4 1015.85 40.81 2 -6 4 996.07 47.72 2 -6 4 1007.76 37.40 2 -6 5 163.56 12.94 2 -6 5 154.25 14.82 -2 6 -5 148.77 10.63 -2 6 -5 124.31 10.16 2 -6 6 65.06 8.70 2 -6 6 88.30 11.59 -2 6 -6 71.53 8.29 -2 6 -6 69.19 7.85 -2 6 -7 129.78 11.64 -2 6 -7 124.66 11.96 2 -6 8 54.62 8.56 -2 6 -8 41.78 7.15 -2 6 -8 48.58 7.98 2 -6 9 1.17 4.73 -2 6 -9 2.29 3.19 -2 6 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799.44 39.80 -4 -8 -6 791.41 38.06 -4 -8 -7 158.31 12.42 -4 -8 -7 144.27 11.67 -4 -8 -7 159.86 14.03 -4 -8 -7 145.39 13.15 4 8 7 134.00 12.87 -4 -8 -7 154.27 14.24 4 8 8 2012.37 84.64 -4 -8 -8 2022.85 85.08 -4 -8 -8 2025.42 84.12 -4 -8 -8 1997.04 79.83 -4 -8 -8 2083.05 82.30 -4 -8 -8 2175.59 85.13 -4 -8 -9 336.31 18.71 -4 -8 -9 276.94 20.49 -4 -8 -9 336.34 22.95 -4 -8 -9 342.68 22.59 -4 -8 -10 662.23 30.44 -4 -8 -10 720.84 37.38 -4 -8 -10 673.79 34.08 -4 -8 -10 679.56 37.85 -4 -8 -10 635.76 35.67 -4 -8 -11 157.63 11.10 -4 -8 -11 146.66 15.96 -4 -8 -11 163.99 15.54 -4 -8 -11 155.99 13.78 -4 -8 -11 132.46 15.15 -4 -8 -12 1969.01 84.02 -4 -8 -12 1851.45 82.32 -4 -8 -12 1731.77 76.45 -4 -8 -12 1780.19 79.21 -4 -8 -12 1905.54 70.68 -4 -8 -13 12.60 6.06 -4 -8 -13 19.45 5.90 -4 -8 -13 15.23 8.32 -4 -8 -13 23.50 3.95 -4 -8 -13 10.42 5.57 -4 -8 -13 14.77 7.30 -4 -8 -14 31.76 9.64 -4 -8 -14 43.00 11.15 -4 -8 -14 37.30 9.70 -4 -8 -14 26.87 6.48 -4 -8 -14 31.77 4.27 -4 -8 -14 20.33 6.73 -4 -8 -15 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15.68 8 -9 9 47.55 6.58 8 -9 9 57.19 5.75 -8 9 -10 3.02 4.44 8 -9 10 2.68 7.04 8 -9 10 0.72 1.80 8 -9 10 -0.88 2.45 8 -9 10 2.18 6.70 -8 9 -10 -2.73 5.67 -8 9 -11 56.10 10.50 8 -9 11 49.81 13.25 8 -9 11 46.45 11.59 8 -9 11 55.13 4.47 8 -9 11 52.41 4.62 -8 9 -12 6.45 5.82 8 -9 12 11.43 9.20 8 -9 12 4.49 8.09 -8 9 -13 31.79 8.58 8 -9 13 31.85 10.63 -8 8 12 127.08 21.58 -8 8 12 112.09 21.24 8 -8 -12 116.16 19.15 8 -8 -11 254.85 20.35 -8 8 11 258.44 30.96 -8 8 11 299.73 32.57 8 -8 -11 334.03 31.17 -8 8 10 3.06 7.51 8 -8 -10 -1.30 5.80 -8 8 10 -5.66 8.30 8 -8 -10 2.44 6.42 8 -8 -9 52.51 9.54 -8 8 9 41.43 13.02 8 -8 -9 61.48 13.16 -8 8 9 59.22 13.59 -8 8 8 18.82 9.05 -8 8 8 11.46 8.03 8 -8 -8 34.42 7.61 8 -8 -8 23.34 9.28 -8 8 8 30.65 11.41 -8 8 7 266.72 27.17 8 -8 -7 344.26 23.96 -8 8 7 247.25 28.13 8 -8 -7 301.61 26.52 -8 8 7 320.51 25.48 -8 8 7 290.71 29.50 -8 8 6 8.53 6.86 8 -8 -6 2.86 5.49 8 -8 -6 -1.84 7.26 -8 8 6 11.47 7.39 -8 8 5 210.81 22.04 8 -8 -5 214.56 18.98 8 -8 -5 207.58 19.93 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14.22 8 -8 9 119.23 18.20 8 -8 9 114.82 7.36 8 -8 9 102.02 8.14 8 -8 9 155.63 18.69 8 -8 9 98.64 14.12 8 -8 10 43.46 3.72 8 -8 10 44.14 4.01 -8 8 -10 38.99 9.05 8 -8 10 37.90 11.83 8 -8 10 39.17 10.42 -8 8 -11 192.07 18.82 8 -8 11 164.93 22.28 8 -8 11 157.57 19.44 -8 8 -12 256.15 22.70 8 -8 12 211.33 25.39 8 -8 12 247.59 24.54 -8 8 -13 22.59 8.43 8 -8 13 25.92 9.23 -8 8 -14 1.80 5.80 -8 8 -14 8.40 7.31 8 -8 14 6.57 7.35 8 -8 15 74.96 14.85 -8 7 13 26.30 11.86 -8 7 12 19.10 10.24 -8 7 12 3.12 8.73 8 -7 -12 11.34 10.21 8 -7 -11 -1.20 6.47 -8 7 11 6.16 7.57 -8 7 11 -2.97 9.18 8 -7 -11 -2.65 8.53 8 -7 -10 130.54 14.35 -8 7 10 122.01 20.17 -8 7 10 88.17 18.95 8 -7 -10 135.95 19.24 -8 7 9 28.77 10.40 8 -7 -9 26.78 7.33 8 -7 -9 37.09 10.82 -8 7 9 27.04 11.28 8 -7 -8 1.37 4.23 -8 7 8 5.56 7.30 -8 7 8 -2.36 6.58 8 -7 -8 2.15 6.00 -8 7 8 5.14 6.74 -8 7 8 1.85 4.86 8 -7 -7 52.48 8.97 -8 7 7 40.32 11.51 8 -7 -7 46.40 11.07 -8 7 7 29.27 10.32 -8 7 7 29.97 9.91 8 -7 -7 17.96 7.52 -8 7 7 51.08 12.45 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8 -7 5 124.27 15.76 8 -7 6 86.43 12.86 8 -7 6 101.82 7.96 8 -7 7 160.18 19.06 8 -7 7 143.00 9.00 8 -7 7 147.98 16.67 8 -7 8 1157.28 43.57 8 -7 8 1198.19 42.40 8 -7 8 1354.76 64.98 -8 7 -8 1279.08 57.09 8 -7 8 1197.08 57.55 -8 7 -9 435.38 28.96 8 -7 9 440.28 33.59 8 -7 9 409.88 15.57 8 -7 9 380.18 15.83 8 -7 9 438.29 31.85 8 -7 9 470.51 31.01 8 -7 10 165.90 19.55 8 -7 10 180.63 19.32 -8 7 -10 212.92 20.06 8 -7 10 225.49 24.05 -8 7 -11 4.97 5.12 8 -7 11 4.94 7.95 8 -7 11 5.96 6.13 -8 7 -12 411.67 29.89 8 -7 12 411.98 35.32 8 -7 12 340.03 29.43 -8 7 -13 202.10 20.36 8 -7 13 204.15 25.53 8 -7 13 153.55 19.76 -8 7 -14 64.99 12.66 8 -7 14 74.60 14.35 8 -7 15 33.46 9.59 8 -7 16 79.85 14.48 -8 6 13 109.26 21.03 -8 6 12 3.14 8.24 -8 6 12 3.10 9.13 -8 6 11 3.01 6.24 -8 6 11 -6.00 9.23 8 -6 -11 -2.71 8.37 8 -6 -10 50.27 9.62 -8 6 10 60.75 13.57 -8 6 10 54.20 14.87 8 -6 -10 60.74 14.61 8 -6 -9 594.56 34.24 -8 6 9 628.15 46.11 8 -6 -9 583.04 41.48 -8 6 9 588.37 44.69 -8 6 8 21.55 9.39 8 -6 -8 19.11 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610.32 40.81 -9 -15 -14 246.58 25.21 -9 -15 -14 295.63 29.06 -9 -15 -14 287.73 23.31 -9 -15 -15 35.82 11.28 -9 -15 -15 62.08 10.86 -9 -15 -16 227.84 21.84 -9 -15 -16 234.65 26.36 -9 -15 -16 234.64 20.41 -9 -15 -17 91.05 16.89 -9 -15 -17 99.24 14.30 -9 -15 -18 44.58 12.27 -9 -15 -18 44.82 9.98 -9 -15 -19 29.14 11.83 -9 -15 -19 21.49 7.85 -9 -15 -20 67.82 11.95 9 16 -1 15.86 6.45 9 16 0 115.81 14.35 9 16 1 -3.10 5.38 9 16 1 2.81 7.38 9 16 2 15.50 6.14 9 16 2 29.99 10.47 9 16 3 157.19 16.58 9 16 3 138.45 19.83 9 16 4 255.80 21.97 9 16 4 257.44 27.03 9 16 5 19.15 7.13 9 16 6 354.92 26.39 9 16 7 240.79 21.81 9 16 8 17.28 7.02 9 16 9 26.96 7.31 9 16 9 16.72 7.74 9 16 10 54.36 11.04 -9 -16 -10 56.10 11.02 9 16 10 54.49 13.16 9 16 11 224.71 22.07 -9 -16 -11 211.41 24.83 -9 -16 -11 187.18 20.53 9 16 11 170.18 21.79 -9 -16 -12 208.71 24.28 9 16 12 104.00 15.88 9 16 12 175.33 20.84 -9 -16 -12 121.99 16.56 -9 -16 -13 15.36 8.70 -9 -16 -13 5.22 8.40 9 16 13 21.53 8.91 -9 -16 -13 18.71 7.49 -9 -16 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18 7 29.40 11.13 9 18 7 22.66 7.20 9 18 8 228.80 20.66 9 18 9 34.70 8.91 9 18 11 -2.58 8.32 9 18 12 406.99 34.60 9 18 13 96.60 16.51 -9 -18 -13 67.45 16.33 -9 -18 -17 100.29 15.86 -9 -18 -18 25.61 9.13 -9 -18 -19 2.11 6.83 9 19 6 1.30 5.80 9 19 7 68.88 10.50 -9 -19 -16 -2.52 9.90 -9 -19 -17 188.93 24.00 -9 -19 -18 28.82 11.72 10 -16 -3 36.10 10.37 10 -16 -2 187.63 20.02 10 -16 -1 40.99 10.61 -10 15 7 48.69 13.78 -10 15 6 -2.44 9.88 -10 15 5 445.20 36.50 10 -15 -4 23.74 9.22 -10 15 4 17.60 9.62 10 -15 -3 44.82 10.53 10 -15 -2 12.38 6.58 10 -15 -1 147.07 17.19 10 -15 0 135.43 16.30 10 -15 1 -5.90 6.14 -10 14 8 350.60 34.21 10 -14 -8 336.59 31.63 -10 14 7 23.76 11.28 10 -14 -7 32.05 10.79 10 -14 -6 15.15 8.79 10 -14 -6 21.36 8.29 -10 14 6 22.69 10.24 10 -14 -5 2.05 5.74 10 -14 -5 4.01 5.90 -10 14 5 9.61 8.04 10 -14 -4 140.29 18.17 10 -14 -4 149.29 19.73 -10 14 4 153.29 20.79 10 -14 -3 -1.84 6.14 10 -14 -3 8.55 6.87 -10 14 3 10.89 8.58 10 -14 -2 -1.74 5.57 10 -14 -2 4.40 6.47 -10 14 2 2.08 6.66 10 -14 -1 48.98 9.78 -10 14 1 66.93 13.20 10 -14 0 470.83 30.98 -10 14 0 444.55 33.77 10 -14 1 10.04 5.96 10 -14 2 6.68 4.81 -10 13 8 36.67 14.17 10 -13 -7 42.22 9.93 -10 13 7 70.16 15.94 10 -13 -7 40.58 11.17 10 -13 -6 41.64 10.06 10 -13 -6 32.41 10.35 -10 13 6 61.99 14.87 10 -13 -6 53.11 12.58 10 -13 -5 17.52 7.69 10 -13 -5 -2.03 11.18 -10 13 5 17.28 9.46 10 -13 -5 25.29 9.07 10 -13 -4 20.07 8.79 10 -13 -4 32.29 8.01 10 -13 -4 21.13 8.60 -10 13 4 35.32 10.53 10 -13 -4 24.07 9.57 10 -13 -3 277.96 27.04 10 -13 -3 319.02 28.60 10 -13 -3 349.64 27.92 -10 13 3 395.76 32.39 10 -13 -2 4.24 6.24 -10 13 2 20.12 8.37 10 -13 -2 9.95 6.66 10 -13 -2 8.53 6.92 -10 13 2 4.29 8.70 10 -13 -1 4.36 7.83 -10 13 1 1.93 7.17 10 -13 -1 -1.90 5.61 10 -13 -1 -1.59 5.33 -10 13 1 -2.06 7.64 -10 13 0 42.52 11.56 10 -13 0 53.03 10.92 10 -13 0 67.12 11.08 10 -13 0 60.36 13.28 10 -13 1 162.67 16.38 10 -13 1 121.42 18.54 10 -13 2 23.31 7.93 10 -13 3 17.86 6.29 10 -13 4 70.88 10.06 -10 12 8 111.91 19.60 10 -12 -7 2.28 9.72 -10 12 7 8.24 8.47 10 -12 -7 1.80 5.01 10 -12 -6 131.22 17.06 10 -12 -6 170.89 21.44 10 -12 -6 132.94 18.53 -10 12 6 176.24 23.09 10 -12 -5 163.53 18.28 10 -12 -5 167.63 21.50 10 -12 -5 184.22 21.19 -10 12 5 218.76 25.06 10 -12 -5 189.53 20.41 10 -12 -4 154.92 16.69 10 -12 -4 186.89 21.47 10 -12 -4 150.56 19.24 -10 12 4 180.58 22.74 10 -12 -4 163.37 19.28 10 -12 -3 23.97 9.65 10 -12 -3 9.83 5.70 10 -12 -3 19.36 9.17 10 -12 -3 12.47 8.13 -10 12 3 13.81 8.01 10 -12 -2 122.51 13.73 10 -12 -2 139.41 18.28 -10 12 2 119.50 17.96 10 -12 -2 152.32 18.84 10 -12 -2 150.32 16.66 -10 12 2 156.92 20.25 10 -12 -1 61.32 12.82 -10 12 1 81.16 15.36 10 -12 -1 81.26 12.38 10 -12 -1 59.19 9.00 10 -12 -1 77.83 13.75 10 -12 0 5.72 5.62 -10 12 0 17.11 8.11 10 -12 0 12.09 5.30 10 -12 0 10.19 5.90 10 -12 0 8.63 7.23 10 -12 1 11.08 6.19 10 -12 1 1.35 4.70 10 -12 1 2.21 6.81 -10 12 -1 9.17 6.83 10 -12 2 180.03 19.55 10 -12 2 170.75 16.06 10 -12 2 169.58 21.42 10 -12 3 264.17 23.22 -10 12 -3 248.55 29.25 10 -12 3 232.55 18.63 10 -12 3 201.07 23.22 -10 12 -4 -3.12 9.61 10 -12 4 -5.22 6.06 10 -12 4 -3.10 4.31 10 -12 4 11.82 8.21 -10 12 -5 40.63 13.07 10 -12 5 40.83 7.20 -10 11 9 205.79 27.30 10 -11 -8 270.88 27.32 -10 11 8 217.96 27.60 10 -11 -8 241.01 22.28 10 -11 -7 50.01 12.25 -10 11 7 50.09 14.72 10 -11 -7 49.41 10.76 10 -11 -6 -2.52 6.63 10 -11 -6 -8.58 9.96 -10 11 6 5.33 7.83 10 -11 -6 1.80 5.31 10 -11 -5 197.76 23.22 10 -11 -5 189.89 21.40 -10 11 5 196.67 24.02 10 -11 -5 179.30 19.83 10 -11 -4 460.20 30.85 10 -11 -4 478.39 34.15 10 -11 -4 506.49 37.75 10 -11 -4 507.02 35.09 -10 11 4 555.55 40.52 10 -11 -3 57.09 10.08 10 -11 -3 65.85 12.47 -10 11 3 93.78 16.02 10 -11 -3 92.51 15.65 10 -11 -3 68.83 12.84 -10 11 3 96.30 16.95 10 -11 -2 -2.11 5.20 10 -11 -2 -11.54 7.18 10 -11 -2 1.98 6.65 10 -11 -2 1.27 3.74 -10 11 2 -4.19 7.78 10 -11 -1 101.67 15.11 10 -11 -1 112.04 13.99 10 -11 -1 78.27 10.39 10 -11 -1 99.63 15.23 -10 11 1 106.84 16.54 10 -11 0 344.19 28.18 -10 11 0 328.31 28.82 10 -11 0 365.84 24.98 10 -11 0 343.67 28.83 10 -11 0 284.17 19.99 10 -11 1 24.83 7.96 10 -11 1 28.91 7.35 10 -11 1 8.52 7.93 10 -11 1 13.31 4.21 10 -11 2 5.61 6.26 10 -11 2 4.81 4.19 10 -11 2 2.18 7.00 10 -11 2 1.79 2.29 10 -11 3 328.85 22.23 10 -11 3 315.93 29.08 10 -11 3 364.52 28.21 10 -11 4 184.61 15.44 10 -11 4 184.07 21.81 10 -11 4 175.57 19.26 10 -11 5 12.69 6.32 10 -11 5 15.73 5.02 10 -11 5 4.65 7.17 -10 11 -6 91.35 17.89 10 -11 6 64.52 11.98 10 -11 6 83.05 8.89 10 -11 6 99.29 16.38 -10 11 -7 159.45 23.06 10 -11 7 154.09 21.08 -10 10 9 110.11 20.84 10 -10 -8 17.06 9.09 -10 10 8 23.47 11.26 10 -10 -8 17.08 7.64 10 -10 -7 166.72 21.34 -10 10 7 163.19 22.95 10 -10 -7 149.65 18.06 -10 10 7 137.80 24.17 10 -10 -6 4.31 7.48 -10 10 6 16.17 9.38 10 -10 -6 -1.77 8.09 10 -10 -5 16.30 8.45 10 -10 -5 26.25 9.59 -10 10 5 23.24 10.48 10 -10 -5 24.52 9.96 10 -10 -4 101.56 15.46 10 -10 -4 129.03 18.22 10 -10 -4 133.40 16.84 -10 10 4 146.25 20.27 -10 10 3 222.72 24.09 10 -10 -3 222.32 23.84 10 -10 -3 254.32 22.87 10 -10 -3 229.50 22.83 10 -10 -2 2.16 6.34 -10 10 2 -2.11 9.85 10 -10 -2 1.63 7.57 10 -10 -2 1.92 5.66 10 -10 -2 3.80 4.24 10 -10 -1 22.85 8.00 -10 10 1 16.33 8.08 10 -10 -1 22.67 7.33 10 -10 -1 20.46 5.64 10 -10 -1 15.72 8.60 -10 10 1 23.60 10.63 10 -10 0 76.42 13.03 10 -10 0 64.13 10.48 10 -10 0 64.25 8.63 10 -10 0 78.30 13.91 -10 10 0 90.61 17.13 10 -10 1 199.79 20.56 10 -10 1 202.08 17.33 10 -10 1 170.55 19.99 10 -10 1 172.21 13.59 -10 10 -1 168.50 22.95 10 -10 2 84.33 13.86 -10 10 -2 89.79 17.47 10 -10 2 91.37 11.30 10 -10 2 81.80 8.09 10 -10 2 69.12 13.78 10 -10 3 18.98 6.00 10 -10 3 24.61 8.09 10 -10 3 17.13 8.92 10 -10 4 524.76 28.57 10 -10 4 494.09 37.49 10 -10 4 605.47 37.58 10 -10 5 143.17 12.35 10 -10 5 160.35 18.69 10 -10 5 164.98 20.22 10 -10 6 -0.70 2.89 10 -10 6 1.89 5.25 10 -10 6 -2.28 6.68 10 -10 7 22.54 8.21 10 -10 7 17.13 4.01 10 -10 7 6.96 7.78 10 -10 7 27.89 10.69 10 -10 8 124.40 16.33 10 -10 8 125.55 19.94 -10 10 -9 24.48 10.68 10 -10 9 36.02 9.38 10 -10 9 23.35 12.17 10 -9 -9 91.37 16.71 -10 9 9 77.13 18.14 10 -9 -8 59.11 13.91 -10 9 8 88.79 17.54 10 -9 -8 66.44 11.64 -10 9 8 53.60 15.41 10 -9 -7 9.20 8.29 -10 9 7 2.83 6.97 10 -9 -7 1.72 5.30 10 -9 -6 36.73 10.50 -10 9 6 38.10 13.90 10 -9 -6 31.51 8.37 10 -9 -5 32.36 9.78 -10 9 5 20.85 10.29 10 -9 -5 8.89 8.13 10 -9 -4 131.01 19.05 10 -9 -4 143.51 17.41 10 -9 -4 119.58 15.80 -10 9 3 344.47 30.81 10 -9 -3 378.48 31.35 10 -9 -3 333.56 26.87 10 -9 -3 370.98 28.54 -10 9 2 4.27 7.69 10 -9 -2 19.44 7.07 10 -9 -2 -1.87 9.18 10 -9 -2 15.34 6.76 -10 9 1 2.84 5.92 10 -9 -1 -7.48 7.48 10 -9 -1 1.90 6.13 10 -9 -1 -2.28 4.49 10 -9 -1 -2.11 7.09 -10 9 0 369.64 34.41 10 -9 0 367.09 25.65 10 -9 0 364.28 29.16 10 -9 0 367.01 22.54 10 -9 0 382.89 30.33 -10 9 -1 64.36 14.71 10 -9 1 86.77 11.20 10 -9 1 68.89 8.65 10 -9 1 83.24 14.38 10 -9 1 79.86 13.25 10 -9 2 60.28 7.05 -10 9 -2 72.45 15.49 10 -9 2 79.51 10.17 10 -9 2 70.81 12.97 10 -9 2 74.34 12.68 10 -9 3 95.14 7.41 -10 9 -3 111.47 19.06 10 -9 3 166.10 18.89 10 -9 3 142.84 12.92 10 -9 3 148.42 18.48 10 -9 4 52.51 12.69 10 -9 4 105.38 10.66 -10 9 -4 69.72 15.81 10 -9 4 105.74 15.02 -10 9 -5 479.31 39.74 10 -9 5 497.87 34.65 10 -9 5 515.64 36.50 10 -9 5 473.32 25.01 10 -9 6 1.95 5.72 10 -9 6 -2.18 7.04 10 -9 6 4.50 3.54 10 -9 7 1.95 6.29 10 -9 7 4.36 2.76 10 -9 7 -4.45 8.78 10 -9 8 114.24 7.30 10 -9 8 108.61 6.94 10 -9 9 171.97 23.47 10 -9 9 163.06 19.42 10 -9 10 45.57 12.47 10 -9 10 28.05 10.48 10 -9 10 34.18 9.78 10 -9 11 26.35 11.25 10 -8 -9 275.62 28.82 10 -8 -9 241.17 22.51 -10 8 9 247.85 30.67 -10 8 9 288.79 32.70 10 -8 -8 92.28 16.25 10 -8 -8 100.63 14.42 -10 8 8 111.02 19.96 -10 8 8 101.22 18.87 10 -8 -7 9.36 7.54 10 -8 -7 5.18 5.33 -10 8 7 -3.19 6.61 -10 8 7 11.43 9.18 10 -8 -6 2.18 6.06 10 -8 -6 1.74 5.83 -10 8 6 -3.10 8.17 -10 8 6 -2.73 8.43 10 -8 -5 60.98 12.09 10 -8 -5 59.78 11.59 -10 8 5 39.41 13.28 10 -8 -4 195.04 22.96 10 -8 -4 259.32 23.78 10 -8 -4 234.77 22.09 -10 8 3 82.59 15.68 10 -8 -3 66.94 13.25 10 -8 -3 56.18 11.07 10 -8 -3 72.10 12.29 -10 8 2 79.52 14.92 10 -8 -2 102.15 15.94 10 -8 -2 74.58 12.17 10 -8 -2 71.17 13.20 10 -8 -1 147.72 18.69 10 -8 -1 141.54 15.67 10 -8 -1 144.42 18.15 -10 8 1 153.83 21.18 10 -8 0 107.90 16.32 10 -8 0 100.72 12.94 10 -8 0 116.81 15.70 -10 8 0 111.44 18.41 10 -8 1 95.04 14.30 10 -8 1 99.33 11.98 10 -8 1 65.17 12.50 10 -8 1 100.98 10.22 -10 8 -1 113.20 18.33 10 -8 2 39.70 9.83 10 -8 2 38.10 7.30 10 -8 2 32.23 5.30 10 -8 2 23.44 9.33 -10 8 -2 34.80 10.61 10 -8 3 7.83 6.05 10 -8 3 11.96 4.73 10 -8 3 11.93 6.91 10 -8 3 4.40 2.21 -10 8 -3 5.35 6.09 10 -8 4 19.54 7.30 10 -8 4 26.96 5.82 10 -8 4 24.31 9.05 -10 8 -4 10.71 7.49 10 -8 5 181.00 19.94 -10 8 -5 142.65 20.67 10 -8 5 169.74 12.64 10 -8 5 179.20 20.17 -10 8 -6 157.19 22.05 10 -8 6 190.87 21.18 10 -8 6 168.65 11.73 10 -8 6 201.56 21.94 -10 8 -7 87.96 16.80 10 -8 7 114.64 16.01 10 -8 7 80.42 6.74 10 -8 7 78.94 14.72 10 -8 8 7.67 6.71 -10 8 -8 -5.61 9.74 10 -8 8 -2.03 4.99 10 -8 9 169.77 12.68 10 -8 9 242.52 23.58 10 -8 9 225.05 23.45 10 -8 9 267.90 27.79 10 -8 10 299.55 27.39 10 -8 10 291.31 28.10 10 -8 10 355.36 32.72 10 -8 11 27.60 8.39 10 -8 11 11.36 7.91 10 -8 11 8.32 7.31 10 -8 12 32.20 12.14 10 -8 12 40.05 13.34 10 -7 -10 14.38 8.87 -10 7 9 81.10 17.52 10 -7 -9 84.15 12.79 -10 7 9 81.62 18.32 10 -7 -9 27.13 11.47 -10 7 8 412.79 38.05 10 -7 -8 348.65 27.00 -10 7 8 324.14 34.47 10 -7 -8 364.67 32.78 -10 7 7 54.49 14.64 10 -7 -7 25.92 8.42 -10 7 7 43.33 12.90 10 -7 -7 28.47 10.40 -10 7 6 16.50 9.25 10 -7 -6 27.84 8.29 -10 7 6 21.13 9.75 10 -7 -6 26.61 9.70 -10 7 5 1.74 5.62 10 -7 -5 -4.13 7.91 10 -7 -5 -1.74 6.70 -10 7 4 445.53 36.28 -10 7 4 425.93 30.25 10 -7 -4 502.26 34.26 10 -7 -4 418.01 30.65 -10 7 3 107.57 17.33 10 -7 -3 129.32 16.20 10 -7 -3 133.06 18.53 10 -7 -3 131.29 16.14 10 -7 -2 2.24 7.51 10 -7 -2 4.89 6.06 10 -7 -2 -3.59 5.77 10 -7 -1 -2.16 5.69 -10 7 1 -2.65 6.96 10 -7 -1 1.50 4.79 10 -7 -1 -5.43 7.33 10 -7 0 293.21 24.83 10 -7 0 240.31 19.75 10 -7 0 230.75 23.70 -10 7 0 227.48 25.96 10 -7 1 71.56 12.87 10 -7 1 84.90 11.39 10 -7 1 63.29 11.64 -10 7 -1 90.62 15.62 10 -7 2 48.20 10.68 10 -7 2 46.32 8.29 10 -7 2 47.54 6.39 10 -7 2 45.36 10.66 -10 7 -2 51.44 12.29 10 -7 3 7.93 5.53 10 -7 3 2.93 4.05 10 -7 3 4.03 2.24 10 -7 3 3.84 6.68 -10 7 -3 -2.57 5.83 10 -7 4 63.17 12.17 -10 7 -4 97.45 16.54 10 -7 4 69.15 8.63 10 -7 4 101.43 14.84 -10 7 -5 18.04 7.98 10 -7 5 24.00 5.18 10 -7 5 11.90 7.41 -10 7 -6 96.13 16.66 10 -7 6 96.82 14.61 10 -7 6 87.08 7.87 10 -7 6 96.86 14.97 10 -7 7 1.30 2.16 10 -7 7 2.05 5.36 -10 7 -7 5.28 6.94 10 -7 8 120.74 18.20 10 -7 8 122.49 16.72 -10 7 -8 142.71 20.48 10 -7 9 26.35 5.98 10 -7 9 42.14 10.43 10 -7 9 61.79 14.03 10 -7 9 38.08 10.66 -10 7 -9 66.00 14.29 10 -7 10 275.02 24.78 10 -7 10 223.83 25.14 10 -7 10 203.93 22.05 -10 7 -10 247.65 26.43 -10 7 -11 17.10 7.28 10 -7 11 2.62 7.31 10 -7 11 8.70 7.00 10 -7 11 -2.19 6.45 -10 7 -12 205.84 21.29 10 -7 12 173.35 23.37 10 -7 12 185.03 21.62 10 -7 12 172.01 20.88 10 -7 13 19.50 10.04 10 -7 13 13.36 8.55 10 -7 14 141.64 19.63 -10 6 10 22.87 11.41 10 -6 -10 49.85 14.20 10 -6 -9 5.09 6.86 -10 6 9 9.52 11.43 -10 6 9 3.14 7.13 10 -6 -9 8.29 8.89 10 -6 -8 -6.92 7.00 -10 6 8 -6.18 10.35 -10 6 8 -3.01 8.83 10 -6 -8 2.60 7.62 10 -6 -7 662.92 40.50 -10 6 7 706.26 50.56 -10 6 7 751.09 51.80 10 -6 -7 641.22 45.25 10 -6 -6 33.14 8.92 -10 6 6 35.11 12.79 -10 6 6 33.14 11.80 10 -6 -6 17.99 8.68 10 -6 -5 71.54 12.09 10 -6 -5 62.72 12.76 -10 6 5 53.41 10.82 10 -6 -4 17.49 7.82 -10 6 4 18.71 9.98 10 -6 -4 9.69 7.43 -10 6 4 16.27 7.12 10 -6 -3 668.41 43.87 10 -6 -3 680.65 39.95 10 -6 -3 658.32 43.70 -10 6 3 627.16 43.49 10 -6 -3 657.93 39.72 -10 6 3 530.69 35.25 10 -6 -2 40.44 10.74 10 -6 -2 47.70 10.22 10 -6 -2 41.23 9.80 -10 6 2 37.01 8.50 10 -6 -2 58.83 12.53 10 -6 -1 3.01 4.42 10 -6 -1 1.79 4.68 10 -6 -1 -2.18 6.08 -10 6 0 60.25 13.72 10 -6 0 57.13 12.09 10 -6 0 43.83 8.63 10 -6 0 61.03 11.46 10 -6 1 1397.30 68.71 10 -6 1 1462.48 63.63 10 -6 1 1463.93 71.43 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118.17 15.62 -10 4 3 105.15 14.20 -10 4 2 83.23 12.63 10 -4 -2 88.93 13.59 10 -4 -2 68.75 13.54 10 -4 -2 76.53 13.68 10 -4 -2 75.98 12.48 -10 4 2 59.17 9.72 -10 4 1 830.95 46.27 10 -4 -1 801.42 45.36 10 -4 -1 837.53 49.54 10 -4 -1 889.13 45.73 -10 4 1 793.37 41.36 -10 4 0 41.09 9.75 10 -4 0 33.12 9.38 -10 4 0 23.05 8.11 10 -4 0 34.28 9.20 10 -4 0 41.56 8.71 -10 4 0 38.71 7.33 10 -4 1 7.00 6.08 -10 4 -1 1.74 5.10 -10 4 -1 -2.28 6.66 10 -4 1 4.18 5.14 10 -4 1 -1.28 5.35 -10 4 -1 -2.15 3.46 -10 4 -2 15.75 7.83 10 -4 2 18.43 7.13 10 -4 2 10.34 5.46 10 -4 2 10.56 6.35 10 -4 3 1127.00 57.96 10 -4 3 1054.23 47.94 -10 4 -3 982.49 58.15 10 -4 3 1115.56 55.65 10 -4 4 76.39 12.81 10 -4 4 50.25 7.72 10 -4 4 46.38 10.11 -10 4 -4 51.41 12.42 10 -4 5 6.05 5.92 10 -4 5 2.67 1.25 -10 4 -5 2.24 6.26 10 -4 5 5.46 2.97 10 -4 5 7.22 5.80 10 -4 5 2.18 1.07 10 -4 6 517.18 33.95 10 -4 6 473.80 31.68 -10 4 -6 461.52 34.31 -10 4 -7 671.74 43.88 10 -4 7 652.76 42.13 -10 4 -8 33.15 9.65 10 -4 8 34.89 7.75 10 -4 8 29.87 9.78 -10 4 -9 406.31 33.80 10 -4 9 399.34 30.44 10 -4 9 367.04 23.48 10 -4 9 463.63 33.93 10 -4 9 445.80 32.72 -10 4 -9 448.52 32.21 10 -4 10 64.77 12.60 10 -4 10 67.79 8.56 10 -4 10 62.64 12.50 -10 4 -10 66.44 12.51 10 -4 10 60.93 12.40 10 -4 11 456.24 33.67 10 -4 11 457.52 35.45 -10 4 -11 474.16 34.34 10 -4 11 544.75 37.15 10 -4 12 21.40 9.31 10 -4 12 40.39 11.12 -10 4 -12 51.29 11.18 10 -4 12 42.79 10.95 10 -4 13 17.67 8.39 10 -4 13 17.06 8.79 -10 4 -13 14.76 7.09 10 -4 13 30.36 10.42 10 -4 14 268.33 27.35 10 -4 14 247.21 24.36 10 -4 15 244.87 24.02 10 -4 16 33.95 9.88 10 -4 17 15.99 8.32 10 -4 18 5.98 6.44 -10 3 11 3.07 8.58 -10 3 10 -9.83 9.13 -10 3 10 -8.96 7.85 -10 3 10 -1.40 6.08 10 -3 -10 3.10 8.65 -10 3 9 40.52 12.66 -10 3 9 27.42 7.77 10 -3 -9 23.45 11.91 -10 3 8 193.52 24.62 10 -3 -8 204.71 20.38 -10 3 8 216.14 19.71 10 -3 -8 204.13 25.82 10 -3 -7 34.26 9.23 -10 3 7 29.89 10.76 10 -3 -7 25.86 10.79 -10 3 7 27.26 8.61 -10 3 6 32.11 8.53 10 -3 -6 34.29 9.10 -10 3 6 36.84 11.26 10 -3 -6 24.46 9.75 10 -3 -6 21.71 8.47 -10 3 6 49.33 9.88 -10 3 5 8.40 5.18 10 -3 -5 -12.60 7.48 -10 3 5 2.55 6.27 10 -3 -5 2.15 7.48 -10 3 5 7.43 6.91 10 -3 -5 -2.24 7.22 -10 3 5 -6.26 7.56 10 -3 -4 528.56 33.84 10 -3 -4 426.01 33.11 -10 3 4 458.20 36.65 -10 3 4 436.31 36.05 10 -3 -4 442.28 34.08 -10 3 4 460.49 30.72 -10 3 4 512.53 32.46 10 -3 -3 7.05 6.57 -10 3 3 4.42 4.11 10 -3 -3 2.03 4.99 10 -3 -3 -7.72 6.47 -10 3 3 1.59 7.13 10 -3 -2 96.44 14.07 10 -3 -2 110.45 16.59 10 -3 -2 122.66 16.89 10 -3 -2 123.86 15.81 -10 3 2 121.65 13.46 -10 3 2 108.40 14.63 -10 3 1 22.92 8.08 10 -3 -1 24.36 8.27 10 -3 -1 15.54 7.48 10 -3 -1 21.34 8.29 10 -3 -1 27.52 8.40 -10 3 1 18.92 6.87 10 -3 0 461.45 31.58 10 -3 0 482.03 34.68 -10 3 0 440.31 33.92 -10 3 0 436.18 26.95 10 -3 0 471.59 30.03 -10 3 0 503.03 32.34 -10 3 -1 95.87 13.83 10 -3 1 65.77 11.83 10 -3 1 73.41 13.23 -10 3 -1 93.14 14.92 10 -3 1 88.67 11.75 -10 3 -1 82.04 10.03 -10 3 -2 63.09 11.17 10 -3 2 63.73 11.95 -10 3 -2 74.94 13.64 10 -3 2 60.75 11.25 10 -3 2 57.94 9.09 -10 3 -2 50.24 7.64 10 -3 3 211.04 21.42 10 -3 3 184.90 19.15 -10 3 -3 202.28 21.42 10 -3 3 160.18 14.46 -10 3 -3 162.25 13.03 10 -3 4 167.20 13.77 10 -3 4 203.76 20.93 10 -3 4 174.88 18.63 -10 3 -4 195.26 21.40 10 -3 5 -1.76 5.17 10 -3 5 -0.70 3.02 10 -3 5 0.42 1.67 -10 3 -5 2.13 3.95 10 -3 6 320.64 25.19 10 -3 6 245.78 13.73 -10 3 -6 276.89 25.50 10 -3 6 334.62 26.85 -10 3 -7 -2.21 6.16 10 -3 7 2.08 5.48 -10 3 -8 1472.97 72.92 10 -3 8 1369.03 61.03 10 -3 8 1449.61 71.51 -10 3 -9 2.32 6.13 10 -3 9 3.64 5.61 -10 3 -9 3.87 6.97 10 -3 9 6.13 5.36 10 -3 9 2.19 6.11 10 -3 10 552.89 37.30 -10 3 -10 599.16 39.28 10 -3 10 607.35 39.18 10 -3 10 632.59 41.56 10 -3 10 583.51 30.38 10 -3 11 3.71 6.21 -10 3 -11 8.11 6.24 10 -3 11 -2.02 5.93 10 -3 11 -2.31 5.27 10 -3 11 -0.81 4.49 10 -3 12 576.00 37.43 -10 3 -12 538.54 38.24 10 -3 12 544.94 38.27 10 -3 12 648.14 42.91 10 -3 13 22.62 8.26 10 -3 13 28.41 10.17 -10 3 -13 23.50 8.91 10 -3 13 14.81 8.61 10 -3 14 64.52 12.06 10 -3 14 61.26 13.54 10 -3 14 86.19 15.98 10 -3 15 95.37 14.45 10 -3 16 333.35 27.58 10 -3 17 13.42 7.98 10 -3 18 78.37 13.78 10 -3 19 70.37 12.86 -10 2 11 285.85 31.61 -10 2 10 13.13 11.82 -10 2 10 5.77 8.48 10 -2 -10 9.48 10.58 -10 2 10 8.42 5.69 -10 2 9 72.52 16.43 10 -2 -9 59.71 15.31 -10 2 9 50.35 10.19 -10 2 9 53.05 13.86 -10 2 8 30.25 11.64 -10 2 8 45.93 12.08 10 -2 -8 36.57 12.01 -10 2 8 19.11 7.56 -10 2 7 240.96 28.93 -10 2 7 284.79 28.73 10 -2 -7 276.62 24.69 10 -2 -7 289.54 27.06 10 -2 -7 295.58 30.00 -10 2 7 306.45 23.86 10 -2 -6 91.66 14.16 -10 2 6 93.58 16.30 10 -2 -6 70.83 13.31 -10 2 6 50.07 10.53 10 -2 -6 66.65 14.53 -10 2 6 78.81 12.19 -10 2 6 69.40 14.22 10 -2 -5 1.82 5.88 -10 2 5 -2.45 5.57 -10 2 5 2.41 6.34 -10 2 5 5.05 4.14 10 -2 -5 2.31 6.06 -10 2 5 3.07 5.51 10 -2 -4 12.68 7.77 -10 2 4 26.13 9.15 10 -2 -4 22.05 8.17 -10 2 4 37.53 10.71 -10 2 4 33.22 8.09 10 -2 -4 32.07 10.17 -10 2 4 27.84 8.55 10 -2 -3 396.83 30.38 -10 2 3 419.42 29.14 10 -2 -3 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95.87 20.17 10 4 -8 130.73 16.38 10 4 -7 59.30 10.73 -10 -4 7 86.41 17.49 -10 -4 7 54.53 11.17 10 4 -7 79.62 17.24 10 4 -6 127.06 15.44 -10 -4 6 120.77 16.92 10 4 -6 78.24 16.67 -10 -4 6 122.02 20.33 -10 -4 6 121.94 15.49 10 4 -5 171.58 23.27 -10 -4 5 158.90 19.16 10 4 -5 220.74 19.67 -10 -4 5 163.09 17.86 -10 -4 5 170.52 18.19 -10 -4 4 665.37 37.62 10 4 -4 557.68 34.60 -10 -4 4 542.96 38.01 10 4 -4 676.60 44.92 -10 -4 4 599.87 42.53 -10 -4 4 648.18 39.67 -10 -4 4 598.41 36.84 -10 -4 3 25.01 8.01 -10 -4 3 19.00 6.97 -10 -4 3 35.27 9.82 10 4 -3 39.67 10.89 -10 -4 3 28.77 8.42 10 4 -3 37.28 7.87 -10 -4 2 272.78 22.70 -10 -4 2 339.63 25.13 10 4 -2 295.96 27.50 10 4 -2 327.57 28.54 -10 -4 2 307.61 24.96 10 4 -2 283.28 21.81 -10 -4 1 208.39 19.68 -10 -4 1 281.26 22.69 10 4 -1 285.62 25.13 10 4 -1 224.57 23.40 10 4 -1 270.62 25.35 -10 -4 1 281.80 23.01 10 4 -1 278.32 20.28 -10 -4 0 288.98 22.67 10 4 0 251.07 24.56 -10 -4 0 308.60 23.55 10 4 0 252.30 23.70 -10 -4 -1 47.64 9.31 -10 -4 -1 38.45 9.49 10 4 1 42.45 9.93 10 4 2 321.42 26.25 -10 -4 -2 320.81 23.14 10 4 3 158.12 17.91 -10 -4 -3 131.40 13.88 -10 -4 -3 128.72 14.27 10 4 4 2142.22 91.50 -10 -4 -4 1926.65 86.90 10 4 4 2007.20 92.72 -10 -4 -4 2236.88 86.87 -10 -4 -4 2220.54 90.64 10 4 5 69.69 11.70 -10 -4 -5 57.14 9.87 10 4 5 66.65 9.91 10 4 5 50.12 10.74 -10 -4 -5 74.45 9.77 -10 -4 -5 60.20 10.95 -10 -4 -6 421.70 28.93 10 4 6 516.40 29.22 10 4 6 534.49 32.42 -10 -4 -6 515.23 27.30 -10 -4 -6 537.92 32.34 10 4 7 1123.09 60.59 -10 -4 -7 1145.09 60.20 10 4 7 1171.92 56.10 10 4 7 1177.14 52.48 -10 -4 -7 1038.17 54.30 -10 -4 -7 1190.31 49.80 -10 -4 -7 1224.27 57.16 -10 -4 -8 215.70 21.60 10 4 8 173.10 20.14 10 4 8 202.99 18.58 -10 -4 -8 173.69 17.65 10 4 8 171.82 18.32 -10 -4 -8 211.80 14.19 10 4 8 217.72 16.40 -10 -4 -8 240.16 20.10 10 4 9 59.42 9.96 10 4 9 71.61 12.66 -10 -4 -9 66.55 12.51 10 4 9 71.49 12.29 -10 -4 -9 66.75 7.18 10 4 9 82.90 9.49 -10 -4 -9 79.30 11.93 10 4 10 260.35 20.53 10 4 10 216.95 23.29 -10 -4 -10 260.38 24.70 10 4 10 218.51 16.71 10 4 10 231.92 21.10 -10 -4 -10 270.94 13.80 10 4 10 272.58 17.78 -10 -4 -10 209.92 20.02 -10 -4 -11 495.76 32.00 10 4 11 488.77 30.13 10 4 11 427.58 34.32 10 4 11 443.43 26.57 10 4 11 444.89 31.32 -10 -4 -11 477.27 20.01 -10 -4 -11 511.62 19.91 10 4 12 150.89 16.76 10 4 12 152.20 14.04 10 4 12 162.31 20.25 -10 -4 -12 142.73 16.40 10 4 13 14.81 7.17 10 4 13 2.47 5.14 -10 -4 -13 -1.64 6.63 10 4 14 379.57 28.20 10 4 14 471.87 36.41 -10 -4 -14 433.29 30.16 10 4 15 286.40 28.75 10 4 15 214.58 20.36 10 4 16 -2.78 7.28 10 4 16 1.61 4.75 10 4 17 62.44 10.84 10 4 18 196.05 19.10 10 4 19 147.99 16.33 10 4 20 12.25 6.22 10 4 21 147.13 16.12 -10 -5 9 3.09 8.61 10 5 -9 -1.84 5.41 -10 -5 8 2.97 9.59 10 5 -8 1.76 5.40 10 5 -7 448.00 38.52 10 5 -7 364.82 28.31 -10 -5 7 395.53 36.94 -10 -5 6 37.35 9.70 10 5 -6 34.29 12.76 10 5 -6 21.75 6.97 -10 -5 6 46.30 10.11 -10 -5 6 8.29 8.16 -10 -5 5 135.71 16.84 10 5 -5 161.42 16.35 -10 -5 5 167.85 18.28 -10 -5 4 57.65 11.21 -10 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11.38 -10 -5 -6 108.47 13.46 -10 -5 -7 1104.43 58.10 10 5 7 1038.77 53.29 10 5 7 1170.40 51.78 -10 -5 -7 971.94 50.72 -10 -5 -7 1162.30 49.50 -10 -5 -7 1087.74 53.49 -10 -5 -8 474.16 33.54 10 5 8 359.62 27.35 -10 -5 -8 469.12 29.03 10 5 8 419.25 30.33 -10 -5 -8 468.33 25.14 -10 -5 -8 503.43 30.46 10 5 8 437.50 26.51 10 5 9 322.98 24.54 -10 -5 -9 327.60 27.92 10 5 9 324.67 25.84 -10 -5 -9 329.45 19.80 10 5 9 382.71 23.34 -10 -5 -9 364.87 25.81 10 5 10 26.77 8.81 10 5 10 18.85 7.02 10 5 10 14.64 4.45 -10 -5 -10 22.77 7.95 10 5 10 18.89 6.99 -10 -5 -10 14.14 4.45 10 5 10 22.01 5.35 -10 -5 -10 21.16 7.72 10 5 11 211.91 23.40 -10 -5 -11 208.44 22.53 10 5 11 220.09 15.60 10 5 11 256.58 22.05 -10 -5 -11 214.48 13.72 10 5 11 278.40 18.56 -10 -5 -11 250.79 21.31 -10 -5 -12 13.99 6.83 -10 -5 -12 37.25 9.80 10 5 12 30.94 9.43 10 5 12 15.13 7.54 -10 -5 -12 25.55 4.39 -10 -5 -12 29.24 3.90 -10 -5 -13 498.25 36.39 10 5 13 486.50 36.99 10 5 13 433.91 30.81 -10 -5 -13 470.88 20.20 -10 -5 -13 462.10 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87.24 10.58 -10 -6 0 72.19 12.40 10 6 0 66.72 12.76 -10 -6 -1 107.05 11.73 -10 -6 -1 117.18 14.68 -10 -6 -1 97.69 14.19 10 6 1 134.83 17.28 10 6 1 123.53 16.27 10 6 2 564.61 38.21 -10 -6 -2 564.18 34.94 10 6 2 574.89 37.09 10 6 3 51.03 11.77 10 6 3 34.72 9.41 -10 -6 -3 47.36 10.04 10 6 3 44.04 10.58 10 6 4 696.92 44.91 -10 -6 -4 774.16 41.36 -10 -6 -4 759.70 37.90 10 6 4 831.42 43.69 -10 -6 -4 823.70 43.17 10 6 4 738.86 45.04 10 6 5 147.49 18.27 -10 -6 -5 119.88 15.98 -10 -6 -5 163.45 16.66 -10 -6 -5 167.14 14.98 10 6 5 158.54 16.46 10 6 6 108.42 13.12 -10 -6 -6 80.04 10.40 10 6 6 85.29 14.17 -10 -6 -6 119.68 13.29 -10 -6 -6 115.57 13.99 10 6 6 122.62 14.76 10 6 7 2.71 3.79 -10 -6 -7 2.41 3.53 -10 -6 -7 1.97 5.79 10 6 7 4.79 5.35 -10 -6 -7 -2.34 4.62 -10 -6 -7 4.52 5.79 -10 -6 -8 441.77 32.36 10 6 8 412.63 28.73 10 6 8 396.52 29.77 -10 -6 -8 442.50 25.76 -10 -6 -8 434.70 28.83 10 6 8 474.28 27.97 -10 -6 -8 403.33 26.33 -10 -6 -9 14.19 7.54 10 6 9 6.14 5.54 10 6 9 5.36 5.25 -10 -6 -9 9.87 5.02 -10 -6 -9 5.98 5.74 10 6 9 17.70 5.53 10 6 10 539.97 34.16 -10 -6 -10 541.87 28.83 -10 -6 -10 526.49 37.41 10 6 10 579.15 26.87 -10 -6 -10 569.34 34.49 10 6 10 653.57 33.40 10 6 10 567.66 36.21 10 6 11 15.76 4.36 -10 -6 -11 10.66 6.87 10 6 11 13.91 7.07 -10 -6 -11 17.78 4.71 10 6 11 23.19 6.03 -10 -6 -11 4.50 5.93 10 6 12 295.55 24.22 -10 -6 -12 259.83 16.59 -10 -6 -12 311.77 27.48 -10 -6 -12 275.83 22.62 -10 -6 -13 88.48 14.85 10 6 13 81.20 14.89 10 6 13 69.76 12.43 -10 -6 -13 82.94 8.16 -10 -6 -13 78.43 7.18 -10 -6 -13 69.07 12.48 -10 -6 -14 253.49 25.21 10 6 14 171.82 22.33 10 6 14 245.15 21.78 -10 -6 -14 199.12 13.16 -10 -6 -14 197.29 11.73 -10 -6 -14 246.56 21.31 -10 -6 -15 145.41 16.67 10 6 15 138.52 19.50 10 6 15 134.49 16.14 -10 -6 -15 88.88 8.17 -10 -6 -15 99.16 7.51 -10 -6 -15 118.76 12.84 10 6 16 422.37 35.19 -10 -6 -16 322.27 22.67 10 6 16 391.41 27.00 -10 -6 -16 275.36 14.48 -10 -6 -16 363.13 26.23 10 6 17 138.93 16.56 -10 -6 -17 135.56 14.35 10 6 18 125.37 15.16 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17.91 -10 -7 -4 147.95 16.95 10 7 4 123.39 16.51 -10 -7 -4 141.57 16.07 10 7 4 165.73 17.33 -10 -7 -5 548.06 33.50 -10 -7 -5 557.34 32.99 -10 -7 -5 493.76 27.21 10 7 5 504.39 32.42 10 7 5 465.92 34.52 -10 -7 -6 -4.05 3.38 10 7 6 3.09 5.18 10 7 6 2.03 4.21 -10 -7 -6 1.40 4.86 -10 -7 -6 1.54 5.20 10 7 7 209.51 20.06 -10 -7 -7 202.16 18.87 -10 -7 -7 198.38 17.50 10 7 7 196.98 21.39 -10 -7 -7 212.71 16.38 10 7 7 217.49 18.72 -10 -7 -8 109.70 16.04 10 7 8 95.79 13.73 10 7 8 88.19 14.81 10 7 8 132.93 16.82 -10 -7 -8 111.67 12.92 -10 -7 -8 100.02 13.72 10 7 8 130.47 14.14 -10 -7 -8 99.59 12.06 10 7 9 314.66 28.07 10 7 9 313.49 24.70 -10 -7 -9 346.92 25.24 10 7 9 306.49 25.84 -10 -7 -9 326.56 22.05 10 7 9 388.17 24.85 -10 -7 -9 328.82 27.43 10 7 9 319.88 16.41 10 7 10 95.01 13.47 -10 -7 -10 108.22 12.32 10 7 10 87.55 8.06 -10 -7 -10 122.45 16.85 10 7 10 118.71 13.52 -10 -7 -10 118.01 14.85 10 7 10 134.63 17.11 -10 -7 -11 4.92 4.66 -10 -7 -11 -6.40 6.57 10 7 11 4.05 3.32 -10 -7 -11 -2.97 6.35 10 7 11 5.38 5.27 -10 -7 -12 103.84 10.86 10 7 12 131.47 13.90 -10 -7 -12 126.82 14.87 10 7 12 104.16 14.82 -10 -7 -12 114.25 17.05 10 7 13 297.26 25.29 -10 -7 -13 322.33 28.80 -10 -7 -13 355.55 19.28 -10 -7 -13 334.73 25.24 -10 -7 -14 232.73 24.61 -10 -7 -14 229.37 14.51 -10 -7 -14 207.80 20.28 10 7 14 255.83 22.53 -10 -7 -15 74.47 11.08 10 7 15 103.22 14.16 -10 -7 -15 73.33 7.59 -10 -7 -15 101.51 13.70 10 7 16 2.75 8.09 -10 -7 -16 12.64 5.83 -10 -7 -16 -3.10 8.42 -10 -7 -16 5.82 3.01 10 7 16 -3.33 8.89 -10 -7 -17 428.27 28.33 -10 -7 -17 481.13 30.60 10 7 17 501.92 32.02 -10 -7 -18 53.91 9.85 10 7 18 57.29 11.43 10 7 19 68.36 11.70 10 7 20 46.27 10.60 10 7 21 113.28 14.76 -10 -8 8 198.96 26.04 -10 -8 7 13.96 10.06 -10 -8 6 105.09 17.99 10 8 -6 89.70 11.30 10 8 -5 14.77 9.22 -10 -8 5 41.61 12.60 10 8 -5 34.68 7.05 10 8 -4 781.20 37.09 10 8 -4 691.38 47.23 -10 -8 3 2.81 4.13 -10 -8 3 4.50 7.54 10 8 -3 2.31 5.67 10 8 -3 -0.88 3.23 -10 -8 2 109.85 13.25 -10 -8 2 95.99 15.99 -10 -8 2 73.46 13.46 10 8 -2 82.29 14.12 10 8 -2 85.21 14.46 10 8 -1 80.68 14.16 -10 -8 1 72.52 12.37 -10 -8 1 66.24 10.89 -10 -8 1 101.54 16.11 10 8 -1 85.13 14.01 -10 -8 0 263.13 22.87 10 8 0 231.22 23.57 -10 -8 0 228.83 23.53 10 8 0 230.36 23.11 -10 -8 -1 228.09 21.21 10 8 1 236.50 23.00 -10 -8 -1 250.42 23.37 10 8 1 204.81 22.09 -10 -8 -2 1.80 2.44 10 8 2 1.90 5.30 -10 -8 -2 1.87 6.00 10 8 2 -2.05 4.68 10 8 3 12.19 6.29 -10 -8 -3 15.50 3.93 10 8 3 16.69 7.72 -10 -8 -3 16.04 7.61 10 8 3 15.21 6.86 10 8 4 1724.11 81.78 -10 -8 -4 1711.41 78.00 10 8 4 1797.85 80.55 -10 -8 -4 1710.85 78.60 10 8 4 1731.98 79.64 10 8 5 20.10 7.72 -10 -8 -5 27.55 8.55 10 8 5 13.90 6.27 -10 -8 -5 16.14 6.91 10 8 6 54.64 11.49 -10 -8 -6 58.49 10.74 10 8 6 58.18 10.48 -10 -8 -6 64.54 8.16 10 8 7 12.30 6.60 10 8 7 15.57 7.67 -10 -8 -7 10.97 6.18 -10 -8 -7 4.36 4.88 10 8 7 9.61 5.57 -10 -8 -7 4.66 3.36 -10 -8 -8 83.98 13.28 10 8 8 75.78 12.51 10 8 8 90.17 14.43 10 8 8 96.12 14.09 -10 -8 -8 83.75 11.65 -10 -8 -8 83.33 12.12 10 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107.96 18.09 -10 -11 -16 129.76 17.52 -10 -11 -17 555.77 38.60 -10 -11 -17 501.61 37.45 -10 -11 -17 477.41 34.96 -10 -11 -17 510.81 30.13 -10 -11 -17 561.96 33.15 -10 -11 -18 23.60 8.19 -10 -11 -18 12.79 6.76 -10 -11 -18 20.33 6.11 -10 -11 -18 18.32 8.53 -10 -11 -18 6.55 7.61 -10 -11 -19 83.15 14.66 -10 -11 -20 94.36 16.25 -10 -11 -21 41.74 12.16 -10 -11 -22 63.61 14.58 10 12 -7 152.95 20.48 10 12 -6 9.48 6.96 10 12 -5 122.06 17.80 -10 -12 5 136.96 20.45 10 12 -4 103.20 16.48 -10 -12 4 126.09 19.18 10 12 -3 186.02 21.45 -10 -12 3 174.88 22.40 -10 -12 2 22.72 9.64 10 12 -2 41.91 12.22 10 12 -2 28.46 8.48 10 12 -2 23.50 8.24 -10 -12 1 124.93 17.28 10 12 -1 91.94 15.02 10 12 -1 121.11 15.68 10 12 0 378.32 27.37 10 12 0 374.73 30.51 10 12 1 431.40 28.12 10 12 1 445.59 32.86 10 12 2 79.51 13.54 10 12 2 66.94 9.82 -10 -12 -3 172.26 22.02 10 12 3 216.04 23.05 10 12 3 190.79 20.80 10 12 3 203.45 16.01 -10 -12 -4 688.92 44.43 10 12 4 629.37 31.30 10 12 4 637.06 41.02 10 12 4 690.64 44.13 10 12 5 12.56 3.59 10 12 5 19.62 7.74 10 12 5 5.96 9.80 -10 -12 -5 13.07 7.85 10 12 5 15.33 7.62 -10 -12 -6 46.25 11.59 -10 -12 -6 70.63 12.03 10 12 6 77.47 12.97 10 12 6 55.23 12.34 10 12 6 63.90 12.06 -10 -12 -7 14.19 8.00 -10 -12 -7 14.50 7.35 10 12 7 6.06 5.64 10 12 7 24.96 8.43 -10 -12 -8 265.82 24.52 -10 -12 -8 285.10 23.76 10 12 8 301.66 25.92 10 12 8 207.74 22.77 10 12 9 156.07 18.74 -10 -12 -9 124.15 16.90 -10 -12 -9 144.56 17.08 -10 -12 -9 121.15 8.79 10 12 9 171.98 18.77 -10 -12 -9 136.13 9.00 -10 -12 -10 26.05 5.23 -10 -12 -10 41.91 9.91 10 12 10 49.75 10.87 10 12 10 27.66 8.68 -10 -12 -10 37.30 9.69 -10 -12 -11 13.96 4.66 -10 -12 -11 11.43 6.44 10 12 11 -2.23 4.16 10 12 11 21.52 7.51 -10 -12 -11 21.23 7.90 -10 -12 -12 336.33 29.27 10 12 12 350.87 30.38 -10 -12 -12 410.86 27.56 10 12 12 335.85 27.71 -10 -12 -12 302.15 21.99 10 12 13 -2.41 7.05 -10 -12 -13 3.98 4.78 -10 -12 -13 15.75 9.35 -10 -12 -13 3.10 5.01 10 12 13 3.93 4.84 -10 -12 -13 2.26 6.29 -10 -12 -14 245.51 21.31 -10 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3 22.83 6.29 10 13 3 11.62 7.44 10 13 4 112.06 15.86 10 13 4 102.06 10.58 10 13 4 109.20 16.76 10 13 5 637.61 40.16 10 13 5 573.84 41.18 -10 -13 -5 646.99 43.39 -10 -13 -6 123.40 18.17 10 13 6 177.69 20.90 10 13 6 153.44 18.89 -10 -13 -7 132.31 17.73 10 13 7 103.95 15.34 10 13 7 147.44 18.77 -10 -13 -8 46.21 11.95 -10 -13 -8 42.60 10.27 10 13 8 36.63 9.49 10 13 8 34.63 9.56 -10 -13 -9 300.94 25.37 10 13 9 361.87 28.80 10 13 9 315.17 27.47 10 13 10 98.49 15.55 -10 -13 -10 117.88 16.45 -10 -13 -10 80.51 13.62 10 13 10 102.47 15.21 -10 -13 -10 75.88 6.84 -10 -13 -11 58.69 7.59 -10 -13 -11 45.78 10.68 10 13 11 79.57 13.80 10 13 11 80.92 13.39 -10 -13 -11 74.08 12.94 -10 -13 -12 -3.30 8.79 -10 -13 -12 7.83 4.18 10 13 12 4.58 6.39 10 13 12 -2.06 6.92 -10 -13 -12 -2.18 5.72 -10 -13 -13 220.06 23.40 -10 -13 -13 250.16 25.45 10 13 13 195.16 22.49 -10 -13 -13 198.55 19.70 10 13 13 235.24 23.03 -10 -13 -13 190.88 16.98 -10 -13 -14 52.22 13.59 -10 -13 -14 59.89 10.58 10 13 14 71.54 14.48 -10 -13 -14 74.61 11.85 -10 -13 -15 88.69 12.71 -10 -13 -15 74.00 11.73 10 13 15 92.10 16.35 -10 -13 -15 69.22 15.46 -10 -13 -16 109.62 15.85 -10 -13 -16 124.12 15.16 -10 -13 -16 129.61 15.03 -10 -13 -16 105.71 17.62 -10 -13 -17 19.49 8.71 -10 -13 -17 24.02 6.87 -10 -13 -17 20.14 6.99 -10 -13 -17 31.42 11.47 -10 -13 -18 2.44 7.83 -10 -13 -18 -1.48 4.76 -10 -13 -18 -6.37 7.64 -10 -13 -19 227.32 25.78 -10 -13 -20 24.56 11.21 -10 -13 -21 4.92 10.50 10 14 -4 44.39 11.04 10 14 -3 6.21 5.09 10 14 -2 131.89 17.67 -10 -14 1 246.66 24.95 10 14 -1 283.51 24.52 10 14 -1 248.99 24.28 10 14 0 -1.95 4.81 10 14 0 -1.51 5.59 10 14 0 2.83 6.42 10 14 1 127.61 14.24 10 14 1 136.91 17.11 10 14 2 288.61 21.26 10 14 2 280.27 25.27 10 14 3 31.68 7.51 10 14 3 15.18 7.31 10 14 4 9.49 6.13 10 14 5 126.04 18.45 10 14 5 137.93 17.39 10 14 6 234.29 24.43 10 14 6 236.68 22.95 -10 -14 -7 122.51 18.54 10 14 7 149.70 18.41 10 14 7 129.82 17.96 -10 -14 -8 35.97 11.88 10 14 8 31.81 10.63 10 14 8 38.24 10.97 10 14 9 380.65 31.45 10 14 9 472.18 35.04 10 14 10 230.64 23.96 -10 -14 -10 267.95 25.01 10 14 11 28.44 9.12 10 14 11 17.50 7.09 -10 -14 -11 29.50 9.00 -10 -14 -11 21.27 8.43 10 14 12 11.34 8.17 -10 -14 -12 15.42 7.13 10 14 12 10.94 6.74 -10 -14 -12 6.50 6.37 10 14 13 2.36 6.57 -10 -14 -13 6.63 6.34 -10 -14 -13 3.12 4.10 -10 -14 -13 -2.47 7.95 10 14 13 -2.19 6.13 -10 -14 -13 -4.47 6.22 -10 -14 -14 216.56 20.14 10 14 14 197.56 22.98 -10 -14 -14 203.82 23.71 -10 -14 -15 166.15 18.11 -10 -14 -15 212.78 24.74 -10 -14 -16 367.90 26.44 -10 -14 -16 325.16 31.27 -10 -14 -17 11.65 5.43 -10 -14 -17 4.91 5.27 -10 -14 -17 15.23 8.83 -10 -14 -18 54.71 10.22 -10 -14 -18 61.34 14.38 -10 -14 -19 49.28 10.39 -10 -14 -19 54.02 13.85 10 15 -3 27.78 8.70 10 15 -2 35.06 9.13 10 15 -1 158.96 18.95 10 15 0 154.62 18.30 10 15 1 1.35 4.86 10 15 1 5.59 5.75 10 15 1 2.83 6.45 10 15 2 170.31 18.89 10 15 3 414.09 30.68 10 15 4 3.72 4.89 10 15 5 -1.87 6.03 10 15 6 89.50 15.39 10 15 6 74.00 13.25 10 15 7 274.55 25.09 10 15 7 318.84 29.19 10 15 8 211.12 21.75 10 15 8 169.54 21.47 10 15 9 2.02 4.60 10 15 9 -2.36 5.79 10 15 10 314.58 27.50 10 15 10 281.20 27.52 10 15 11 151.10 19.10 -10 -15 -11 125.73 17.42 10 15 11 145.20 19.15 10 15 12 6.71 6.91 10 15 12 9.20 7.41 -10 -15 -12 12.92 7.49 10 15 13 113.60 17.34 -10 -15 -13 134.10 20.20 10 15 13 129.48 18.09 -10 -15 -13 119.84 17.76 10 15 14 40.86 11.82 -10 -15 -14 59.73 16.69 -10 -15 -15 766.83 51.70 -10 -15 -15 795.39 44.30 -10 -15 -16 20.06 7.74 -10 -15 -16 10.55 9.51 -10 -15 -17 281.83 29.50 -10 -15 -17 271.61 23.91 -10 -15 -18 40.16 12.97 -10 -15 -18 24.28 7.62 -10 -15 -19 41.17 9.54 10 16 -1 18.14 6.97 10 16 0 41.30 9.98 10 16 1 96.15 13.94 10 16 2 3.56 5.72 10 16 3 287.15 24.70 10 16 4 136.49 16.92 10 16 5 25.39 7.59 10 16 6 3.69 4.53 10 16 7 9.39 5.25 10 16 7 2.55 6.27 10 16 8 78.78 13.52 10 16 8 82.64 15.15 10 16 9 1.98 5.20 10 16 9 2.47 6.48 10 16 10 49.03 10.86 10 16 10 41.51 10.99 -10 -16 -11 191.03 20.95 10 16 11 154.72 19.75 10 16 11 196.12 23.74 -10 -16 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-10 -18 -18 8.35 6.73 -10 -18 -19 2.06 6.65 10 19 7 14.45 6.16 10 19 8 193.79 19.54 10 19 9 -1.74 5.12 10 19 10 201.84 20.61 11 -15 -3 5.85 7.02 -11 14 5 7.82 9.05 11 -14 -4 2.05 6.60 -11 14 4 4.99 9.56 11 -14 -3 307.46 27.32 -11 14 3 338.88 31.40 11 -14 -2 114.43 15.73 -11 14 2 100.47 17.88 11 -14 -1 17.00 7.25 -11 14 1 10.92 8.61 11 -14 0 9.51 6.08 11 -13 -6 139.43 18.04 -11 13 6 139.12 22.33 11 -13 -6 153.00 21.44 11 -13 -5 57.31 12.71 11 -13 -5 64.78 13.68 -11 13 5 96.20 18.90 11 -13 -5 84.30 15.65 11 -13 -4 8.40 5.87 11 -13 -4 2.37 5.83 -11 13 4 17.94 10.39 11 -13 -4 18.33 8.47 11 -13 -3 27.24 9.22 11 -13 -3 19.16 8.19 -11 13 3 12.30 8.87 11 -13 -2 46.69 10.53 -11 13 2 44.91 13.08 11 -13 -1 103.89 14.66 -11 13 1 90.88 16.56 11 -13 0 7.83 6.18 11 -13 1 76.66 11.78 11 -12 -6 1.95 6.03 11 -12 -6 4.58 9.28 -11 12 6 5.67 8.74 11 -12 -6 -13.28 9.23 11 -12 -5 2.00 6.73 11 -12 -5 2.16 6.35 -11 12 5 8.17 8.39 11 -12 -5 17.83 8.53 11 -12 -4 16.41 8.09 11 -12 -4 14.25 7.57 -11 12 4 7.87 9.44 11 -12 -4 9.77 7.54 11 -12 -3 88.19 14.81 11 -12 -3 80.29 14.66 -11 12 3 103.22 17.63 11 -12 -3 98.39 16.01 11 -12 -2 -6.45 9.15 11 -12 -2 -1.79 5.75 -11 12 2 2.42 7.48 11 -12 -2 2.24 5.92 11 -12 -1 182.99 19.00 11 -12 -1 187.29 21.27 11 -12 -1 141.10 19.37 11 -12 0 90.83 12.99 11 -12 0 58.54 13.33 11 -12 0 79.72 13.75 11 -12 1 10.17 6.31 11 -12 1 27.08 7.39 11 -12 2 85.76 11.67 11 -12 2 75.56 13.73 11 -12 3 89.62 11.43 11 -11 -7 22.69 8.97 11 -11 -7 5.64 7.43 11 -11 -6 11.56 7.17 11 -11 -6 35.27 11.00 11 -11 -6 9.22 7.74 -11 11 6 5.75 10.35 11 -11 -5 -1.97 6.34 11 -11 -5 -2.16 8.01 -11 11 5 -5.53 9.95 11 -11 -5 2.60 6.40 11 -11 -4 80.47 13.94 11 -11 -4 99.24 13.39 11 -11 -4 76.92 14.14 -11 11 4 98.51 17.93 11 -11 -4 90.02 16.22 11 -11 -3 73.87 11.36 11 -11 -3 53.34 12.19 11 -11 -3 100.44 15.18 -11 11 3 87.28 16.22 11 -11 -3 91.27 15.85 11 -11 -2 124.85 18.02 11 -11 -2 129.76 17.52 11 -11 -2 122.48 13.23 11 -11 -2 93.66 14.85 11 -11 -1 2.23 6.87 11 -11 -1 -1.66 5.09 11 -11 -1 -2.15 7.44 11 -11 0 140.58 18.79 11 -11 0 149.25 16.54 11 -11 0 133.33 18.97 -11 11 0 186.43 25.66 11 -11 1 16.82 7.35 11 -11 1 40.76 8.89 11 -11 1 13.38 7.78 -11 11 -1 19.19 10.32 11 -11 2 35.01 9.46 -11 11 -2 54.15 14.55 11 -11 2 45.91 8.71 11 -11 2 18.24 8.83 11 -11 3 25.30 6.73 11 -11 3 20.27 7.57 11 -11 3 23.24 10.16 11 -11 4 173.32 19.89 11 -11 4 144.65 13.72 11 -11 5 44.01 10.29 11 -10 -7 78.91 15.94 11 -10 -7 73.22 13.57 -11 10 7 99.72 19.45 11 -10 -6 45.85 11.04 11 -10 -6 57.92 13.39 11 -10 -6 39.18 11.43 -11 10 6 23.26 11.54 11 -10 -5 29.14 9.96 11 -10 -5 39.75 11.07 11 -10 -5 36.83 10.34 -11 10 5 30.80 11.39 11 -10 -4 3.95 7.78 11 -10 -4 16.24 8.00 -11 10 4 5.40 8.32 11 -10 -4 -2.55 7.85 11 -10 -3 102.89 17.44 11 -10 -3 76.37 14.16 11 -10 -3 85.21 15.11 11 -10 -2 108.60 17.24 11 -10 -2 103.85 14.90 11 -10 -2 116.63 16.98 11 -10 -2 105.28 12.63 11 -10 -1 166.41 20.92 11 -10 -1 187.41 20.92 11 -10 -1 185.24 18.64 11 -10 -1 131.06 13.81 11 -10 0 13.28 8.00 11 -10 0 15.08 7.18 11 -10 0 25.48 9.28 11 -10 0 24.31 5.77 -11 10 0 28.05 11.60 11 -10 1 265.99 21.19 11 -10 1 259.73 26.38 11 -10 1 218.43 15.94 -11 10 -1 247.52 29.01 11 -10 2 12.66 7.33 11 -10 2 1.25 4.83 11 -10 2 2.21 7.10 11 -10 2 2.37 2.75 -11 10 -2 -3.09 7.02 11 -10 3 8.34 7.52 11 -10 3 21.45 6.74 11 -10 3 15.75 8.11 -11 10 -3 21.55 11.46 11 -10 4 33.15 10.08 11 -10 4 52.92 8.50 11 -10 4 20.62 9.61 -11 10 -4 33.92 13.18 11 -10 5 335.84 28.10 11 -10 5 272.89 18.07 11 -10 5 247.31 26.15 -11 10 -5 284.99 31.42 11 -10 6 2.37 7.31 11 -10 6 4.81 3.38 11 -10 6 8.27 6.08 11 -10 7 16.53 7.20 11 -10 8 78.45 13.70 11 -9 -7 4.96 8.30 11 -9 -7 7.51 6.29 -11 9 7 -3.04 9.80 11 -9 -6 4.66 7.49 11 -9 -6 -3.79 7.25 -11 9 6 -2.94 9.44 11 -9 -5 51.89 11.57 11 -9 -5 67.27 14.25 11 -9 -5 39.30 11.07 -11 9 5 62.17 16.07 11 -9 -4 103.95 15.44 11 -9 -4 77.57 15.10 11 -9 -4 79.93 13.75 11 -9 -3 -2.49 6.94 11 -9 -3 11.83 7.10 11 -9 -3 15.18 7.88 11 -9 -2 33.59 11.02 11 -9 -2 46.12 10.95 11 -9 -2 46.03 10.50 11 -9 -1 37.14 10.87 11 -9 -1 44.08 10.60 11 -9 -1 42.73 11.90 11 -9 -1 42.40 7.95 11 -9 0 2.24 8.37 11 -9 0 19.57 7.52 11 -9 0 7.20 3.82 11 -9 0 -2.06 8.37 -11 9 0 3.01 6.86 11 -9 1 244.00 24.88 11 -9 1 255.80 21.06 11 -9 1 281.95 26.02 11 -9 1 250.66 17.03 -11 9 -1 263.37 29.69 11 -9 2 195.99 21.29 11 -9 2 167.11 16.19 11 -9 2 149.83 20.51 11 -9 2 161.26 11.83 -11 9 -2 199.48 25.26 11 -9 3 8.50 6.24 11 -9 3 4.00 1.82 -11 9 -3 14.85 9.56 11 -9 3 10.00 5.27 11 -9 3 -2.18 6.71 -11 9 -4 86.27 17.57 11 -9 4 101.30 16.15 11 -9 4 87.55 10.19 11 -9 4 128.64 17.67 -11 9 -5 74.70 17.80 11 -9 5 118.79 16.40 11 -9 5 78.74 9.23 11 -9 5 81.12 15.23 -11 9 -6 177.28 23.96 11 -9 6 238.71 23.94 11 -9 6 175.64 12.92 11 -9 6 240.21 24.75 -11 9 -7 21.18 10.53 11 -9 7 16.69 3.84 11 -9 7 34.96 10.17 11 -9 7 25.71 9.15 11 -9 8 -2.80 9.02 11 -9 8 2.15 5.28 11 -9 9 25.81 10.69 11 -9 9 21.62 8.08 11 -9 10 83.05 14.64 11 -8 -8 368.28 34.36 11 -8 -8 365.63 28.86 11 -8 -7 20.25 10.29 11 -8 -7 35.80 9.48 -11 8 7 23.63 11.36 -11 8 7 36.80 13.70 11 -8 -6 9.43 8.50 11 -8 -6 5.70 6.84 -11 8 6 19.84 10.65 -11 8 6 14.77 9.52 11 -8 -5 1.92 7.12 11 -8 -5 2.71 8.00 11 -8 -5 13.23 7.93 -11 8 5 2.84 9.17 11 -8 -4 142.78 18.58 11 -8 -4 132.99 17.67 11 -8 -4 154.49 20.93 11 -8 -3 32.65 9.52 11 -8 -3 40.89 11.07 11 -8 -3 32.80 10.55 11 -8 -2 7.30 7.15 11 -8 -2 1.77 6.79 11 -8 -2 -1.97 6.06 11 -8 -1 231.64 21.57 11 -8 -1 263.45 24.87 11 -8 -1 301.32 27.79 -11 8 0 87.41 17.29 11 -8 0 88.45 12.22 11 -8 0 64.68 13.38 11 -8 0 50.27 12.61 -11 8 -1 60.57 14.04 11 -8 1 39.61 8.79 11 -8 1 52.72 7.56 11 -8 1 71.69 13.85 11 -8 1 57.96 11.85 -11 8 -2 189.57 24.00 11 -8 2 173.30 16.07 11 -8 2 141.53 18.28 11 -8 2 138.08 11.26 11 -8 2 170.58 19.78 -11 8 -3 94.59 17.16 11 -8 3 107.40 11.96 11 -8 3 84.22 7.13 11 -8 3 107.72 16.85 11 -8 3 131.56 17.65 -11 8 -4 223.97 26.35 11 -8 4 253.34 24.38 11 -8 4 185.75 15.46 11 -8 4 244.68 23.97 11 -8 5 12.92 6.94 11 -8 5 13.57 4.65 -11 8 -5 11.51 8.03 11 -8 5 13.10 8.61 11 -8 6 4.36 6.39 11 -8 6 4.42 6.83 11 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7 -1 492.22 40.22 11 -7 1 565.76 38.92 -11 7 -2 5.53 6.81 11 -7 2 7.43 4.88 11 -7 2 8.11 6.24 11 -7 2 6.79 3.38 11 -7 2 4.42 6.18 -11 7 -3 -5.51 8.09 11 -7 3 4.39 4.45 11 -7 3 8.22 6.61 11 -7 3 1.61 2.06 11 -7 3 2.18 5.74 -11 7 -4 57.94 13.70 11 -7 4 58.62 11.93 11 -7 4 60.54 8.29 11 -7 4 47.94 12.09 11 -7 5 56.44 11.93 11 -7 5 54.28 7.36 -11 7 -5 66.41 14.22 11 -7 5 65.53 13.33 11 -7 6 -2.19 6.13 11 -7 6 -4.29 6.91 11 -7 6 1.17 2.88 -11 7 -6 -2.78 6.34 11 -7 7 11.56 2.16 11 -7 7 15.21 8.58 11 -7 7 24.51 9.49 -11 7 -7 25.26 10.76 11 -7 8 2.26 5.56 -11 7 -8 2.86 5.93 11 -7 9 269.90 27.63 11 -7 9 198.12 16.12 11 -7 9 244.58 25.01 -11 7 -9 296.64 30.51 11 -7 10 17.78 4.62 11 -7 10 5.27 7.38 11 -7 10 24.88 9.18 -11 7 -10 26.70 10.69 11 -7 11 68.54 14.14 11 -7 11 110.68 19.26 11 -7 11 128.05 17.99 -11 7 -11 127.22 20.59 11 -7 12 241.80 27.89 11 -7 12 242.58 25.43 11 -7 12 251.91 26.39 11 -6 -8 50.07 14.22 -11 6 8 41.78 14.38 11 -6 -8 47.47 11.65 -11 6 8 22.95 12.25 11 -6 -7 47.07 13.67 -11 6 7 58.82 16.38 -11 6 7 57.58 15.85 11 -6 -7 63.42 12.64 11 -6 -6 633.50 43.83 -11 6 6 561.14 45.91 11 -6 -6 587.43 38.84 -11 6 6 627.58 48.74 11 -6 -5 4.57 7.35 11 -6 -5 -1.93 6.92 -11 6 5 3.06 7.51 11 -6 -4 37.35 10.87 11 -6 -4 46.95 11.30 -11 6 4 24.09 7.43 11 -6 -4 51.89 10.94 11 -6 -3 -2.57 9.56 11 -6 -3 1.97 7.56 -11 6 3 3.23 6.37 11 -6 -3 -9.62 9.46 11 -6 -2 918.75 56.09 11 -6 -2 989.57 52.35 -11 6 2 871.19 47.57 11 -6 -2 1000.84 53.00 11 -6 -1 51.86 10.40 11 -6 -1 65.87 12.38 11 -6 -1 69.72 14.45 -11 6 0 -2.71 5.62 11 -6 0 2.34 5.74 11 -6 0 12.24 6.52 11 -6 0 19.50 8.70 11 -6 1 303.16 26.51 11 -6 1 305.09 28.25 11 -6 1 356.79 24.52 -11 6 -1 350.45 32.55 11 -6 2 464.15 34.32 11 -6 2 485.36 29.19 -11 6 -2 489.54 38.75 11 -6 2 518.32 37.12 -11 6 -3 2.65 8.16 11 -6 3 4.39 4.57 11 -6 3 2.00 6.18 11 -6 3 -4.40 7.67 -11 6 -4 -5.30 11.02 11 -6 4 7.59 4.50 11 -6 4 1.97 1.67 11 -6 4 8.11 6.24 11 -6 4 -4.37 9.31 -11 6 -5 124.70 19.08 11 -6 5 122.66 17.67 11 -6 5 122.19 10.97 11 -6 5 125.21 17.05 11 -6 6 96.72 8.53 11 -6 6 139.22 18.61 11 -6 6 135.02 17.86 -11 6 -6 152.19 21.11 11 -6 7 -2.10 8.04 11 -6 7 2.26 5.54 -11 6 -7 5.40 7.52 11 -6 8 -2.29 7.95 -11 6 -8 -2.75 7.67 11 -6 9 12.12 7.82 11 -6 9 5.95 5.53 11 -6 9 4.65 6.11 -11 6 -9 11.21 7.38 11 -6 10 243.46 25.14 11 -6 10 186.63 14.81 11 -6 10 226.51 25.34 11 -6 10 250.86 25.06 -11 6 -10 226.25 26.95 11 -6 11 65.03 13.67 11 -6 11 25.50 10.94 11 -6 11 26.46 9.91 -11 6 -11 46.84 13.39 11 -6 12 91.09 16.33 11 -6 12 78.81 16.32 11 -6 12 93.55 15.94 -11 6 -12 120.12 20.19 11 -6 13 21.65 10.37 11 -6 13 13.47 8.61 11 -6 13 2.50 6.58 11 -6 14 13.88 9.31 -11 5 9 124.02 21.00 11 -5 -8 42.52 13.80 11 -5 -8 44.26 10.87 -11 5 8 76.43 17.34 -11 5 8 61.34 16.53 11 -5 -7 8.00 8.58 11 -5 -7 -1.93 6.24 -11 5 7 12.42 9.57 -11 5 7 3.10 7.64 11 -5 -6 17.50 9.31 -11 5 6 9.09 9.75 11 -5 -6 13.65 8.11 -11 5 6 11.98 10.79 11 -5 -5 357.36 31.85 11 -5 -5 412.32 30.86 -11 5 5 375.15 35.56 11 -5 -4 13.54 6.73 11 -5 -4 8.68 7.28 -11 5 4 10.19 6.11 11 -5 -4 10.74 8.29 11 -5 -3 -3.85 6.21 11 -5 -3 -2.02 5.93 -11 5 3 1.59 4.91 11 -5 -3 5.18 6.81 11 -5 -2 125.09 16.82 11 -5 -2 126.96 16.61 -11 5 2 79.21 12.53 11 -5 -2 142.53 19.24 11 -5 -1 427.13 31.29 11 -5 -1 440.75 34.34 11 -5 -1 369.94 28.13 -11 5 1 354.82 25.52 11 -5 0 50.22 10.55 -11 5 0 23.44 9.77 11 -5 0 42.34 11.85 11 -5 0 34.49 8.60 -11 5 0 44.86 8.27 -11 5 -1 36.05 11.78 11 -5 1 52.79 11.75 11 -5 1 31.16 7.77 11 -5 1 31.04 9.10 11 -5 2 161.94 19.96 11 -5 2 184.17 16.80 -11 5 -2 168.55 21.66 11 -5 2 179.69 19.62 11 -5 3 767.89 47.02 11 -5 3 730.32 37.66 -11 5 -3 765.05 49.37 11 -5 3 755.15 45.21 -11 5 -4 -10.14 9.72 11 -5 4 5.75 4.71 11 -5 4 1.98 6.11 11 -5 4 6.60 7.09 -11 5 -5 17.83 8.55 11 -5 5 13.23 8.21 11 -5 5 14.74 4.53 11 -5 5 32.00 10.19 -11 5 -6 513.85 38.31 11 -5 6 535.12 36.47 11 -5 6 553.43 36.10 11 -5 7 393.83 32.00 -11 5 -7 334.64 31.72 11 -5 7 355.26 29.60 -11 5 -8 79.28 14.92 11 -5 8 61.91 9.57 11 -5 8 75.98 14.38 11 -5 9 24.38 6.65 11 -5 9 14.11 7.28 -11 5 -9 27.00 10.37 11 -5 10 44.19 7.88 11 -5 10 62.21 13.26 11 -5 10 79.57 14.69 11 -5 10 37.88 11.02 -11 5 -10 49.63 13.18 11 -5 11 361.70 21.91 11 -5 11 449.38 35.51 11 -5 11 447.22 36.03 -11 5 -11 457.00 33.71 11 -5 11 420.84 32.68 -11 5 -11 384.79 35.22 11 -5 12 7.52 6.60 11 -5 12 7.43 7.96 11 -5 12 15.02 9.13 -11 5 -12 5.80 6.05 11 -5 13 25.55 10.89 11 -5 13 15.15 9.22 11 -5 13 5.12 7.52 11 -5 14 52.56 13.80 11 -5 14 100.07 15.83 11 -5 14 62.57 13.70 11 -5 15 8.09 8.70 11 -5 15 15.31 8.14 11 -4 -9 9.13 11.67 -11 4 9 3.17 8.83 -11 4 9 -1.58 4.86 11 -4 -8 109.44 20.01 -11 4 8 135.77 21.75 11 -4 -8 168.36 19.31 -11 4 8 122.09 15.34 11 -4 -7 -1.97 6.84 -11 4 7 3.01 9.26 11 -4 -7 5.41 7.56 -11 4 7 -1.67 7.10 -11 4 7 9.35 9.15 11 -4 -6 53.16 11.78 -11 4 6 52.71 13.93 11 -4 -6 40.61 12.09 -11 4 6 29.03 8.19 -11 4 6 33.06 10.89 -11 4 5 1.74 6.66 -11 4 5 5.70 8.79 11 -4 -5 5.93 8.21 11 -4 -5 4.76 7.35 -11 4 4 210.01 20.88 -11 4 4 178.68 18.53 11 -4 -4 194.74 22.09 11 -4 -4 195.86 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5 -3 69.69 15.16 11 5 -3 65.82 10.69 -11 -5 3 70.76 13.64 -11 -5 3 73.05 11.70 -11 -5 3 71.38 12.24 11 5 -2 260.82 27.06 -11 -5 2 284.12 24.22 11 5 -2 270.98 21.27 -11 -5 2 244.06 24.25 -11 -5 2 320.19 25.78 -11 -5 2 254.40 21.83 11 5 -1 4.89 6.01 -11 -5 1 1.79 8.47 -11 -5 1 15.52 7.17 -11 -5 1 10.14 5.22 -11 -5 0 285.51 23.87 11 5 0 264.62 26.02 -11 -5 0 232.33 20.23 -11 -5 0 263.87 22.79 11 5 1 86.41 14.63 -11 -5 -1 71.30 11.67 -11 -5 -1 78.26 12.73 11 5 1 73.77 13.62 -11 -5 -2 488.35 30.44 11 5 2 440.70 34.06 11 5 3 118.85 17.41 -11 -5 -3 133.19 14.64 11 5 4 133.84 17.54 -11 -5 -4 113.67 13.52 -11 -5 -4 145.13 15.10 11 5 4 99.12 13.26 11 5 5 -1.79 9.69 -11 -5 -5 30.90 7.52 11 5 5 27.16 7.44 11 5 5 26.72 8.99 -11 -5 -5 20.10 7.04 -11 -5 -5 16.63 7.28 11 5 6 667.11 38.86 -11 -5 -6 613.75 32.89 -11 -5 -6 647.90 37.51 11 5 6 583.18 34.28 -11 -5 -6 527.15 33.43 11 5 7 162.28 19.13 11 5 7 228.13 18.63 -11 -5 -7 213.64 18.89 -11 -5 -7 219.44 17.05 -11 -5 -7 277.61 22.48 -11 -5 -8 745.06 48.11 11 5 8 858.86 46.03 -11 -5 -8 747.95 43.25 11 5 8 781.22 47.60 -11 -5 -8 856.03 39.40 11 5 8 897.00 42.94 -11 -5 -8 932.97 47.46 -11 -5 -9 188.04 21.99 11 5 9 197.40 22.35 11 5 9 170.84 18.20 -11 -5 -9 149.25 17.05 11 5 9 168.47 19.62 -11 -5 -9 194.77 14.48 -11 -5 -9 244.83 21.29 11 5 9 212.08 16.80 11 5 10 80.58 12.40 11 5 10 79.47 14.92 11 5 10 68.44 8.68 -11 -5 -10 75.72 13.67 11 5 10 59.37 11.98 -11 -5 -10 84.97 8.68 -11 -5 -10 108.27 14.09 11 5 10 79.21 10.35 11 5 11 24.75 8.63 11 5 11 20.19 7.09 -11 -5 -11 15.93 7.93 11 5 11 14.06 5.10 11 5 11 15.16 7.70 -11 -5 -11 20.49 4.16 11 5 11 12.22 5.09 -11 -5 -11 18.48 7.67 -11 -5 -12 214.43 20.36 11 5 12 211.20 23.84 -11 -5 -12 181.95 21.45 11 5 12 176.16 14.81 11 5 12 163.03 18.77 -11 -5 -12 176.99 10.34 -11 -5 -12 173.23 10.04 -11 -5 -13 350.68 27.53 11 5 13 338.89 27.40 11 5 13 322.56 31.07 -11 -5 -14 224.62 21.97 11 5 14 253.94 23.34 11 5 14 249.44 26.98 -11 -5 -15 -3.56 10.19 11 5 15 11.25 7.39 11 5 15 1.82 8.63 11 5 16 583.74 45.05 11 5 16 539.50 36.29 11 5 17 173.66 24.05 11 5 17 180.99 19.37 11 5 18 121.67 15.75 11 5 19 43.44 10.81 11 5 20 71.36 12.47 11 5 21 53.03 10.92 -11 -6 7 -3.07 9.04 11 6 -6 1.50 4.39 -11 -6 6 2.97 8.30 11 6 -5 335.03 32.11 11 6 -5 378.65 26.20 -11 -6 5 352.71 35.15 -11 -6 5 369.30 29.27 11 6 -4 13.25 5.64 11 6 -4 10.56 7.77 -11 -6 4 1.87 5.53 11 6 -3 24.83 6.66 -11 -6 3 14.87 6.73 11 6 -3 23.06 8.61 -11 -6 2 29.43 9.23 11 6 -2 22.43 9.00 -11 -6 2 17.15 7.30 -11 -6 1 434.17 32.50 -11 -6 1 440.31 27.97 -11 -6 1 478.50 32.73 11 6 0 163.87 20.75 -11 -6 0 202.65 20.06 -11 -6 0 197.87 19.86 -11 -6 0 153.88 15.37 11 6 1 171.79 19.97 11 6 1 211.80 22.79 -11 -6 -1 175.92 18.95 -11 -6 -1 194.18 19.29 -11 -6 -1 158.74 15.54 11 6 2 13.68 8.32 11 6 2 6.87 7.38 -11 -6 -2 9.93 5.77 11 6 3 250.73 24.70 -11 -6 -3 291.86 23.48 11 6 3 287.00 26.51 11 6 4 -2.24 6.91 11 6 4 1.71 3.90 11 6 4 -2.15 5.96 -11 -6 -4 7.43 5.53 -11 -6 -4 -1.69 6.29 11 6 5 15.62 7.22 11 6 5 7.35 7.67 -11 -6 -5 25.26 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565.47 39.43 -11 -8 -1 583.78 38.05 -11 -8 -1 504.26 26.23 11 8 2 113.59 16.63 11 8 2 98.59 15.59 -11 -8 -2 88.25 14.29 -11 -8 -2 118.84 10.56 11 8 3 28.13 9.57 11 8 3 31.48 9.62 -11 -8 -3 27.91 5.43 -11 -8 -3 18.41 8.09 11 8 3 40.48 9.64 11 8 4 80.51 14.29 -11 -8 -4 91.60 13.88 11 8 4 57.99 12.90 -11 -8 -4 109.30 14.55 11 8 4 73.57 12.51 -11 -8 -5 393.47 28.80 -11 -8 -5 366.62 27.63 11 8 5 414.63 29.81 11 8 5 348.71 30.39 -11 -8 -6 92.54 10.34 11 8 6 99.06 14.01 11 8 6 118.09 17.19 -11 -8 -6 115.10 14.55 -11 -8 -6 117.13 15.52 -11 -8 -7 127.78 15.37 11 8 7 87.50 14.95 11 8 7 99.84 14.74 -11 -8 -7 104.54 13.54 11 8 7 98.25 13.20 -11 -8 -7 79.13 9.87 11 8 8 185.11 21.29 11 8 8 160.12 18.24 -11 -8 -8 179.83 18.28 11 8 8 169.25 19.81 -11 -8 -8 158.93 16.43 -11 -8 -8 132.46 13.73 11 8 8 155.65 16.72 -11 -8 -9 523.31 37.12 11 8 9 476.47 36.84 11 8 9 518.01 33.93 11 8 9 439.14 34.06 -11 -8 -9 524.19 33.51 -11 -8 -9 461.71 29.74 11 8 9 566.35 33.25 -11 -8 -9 481.74 28.96 -11 -8 -10 11.17 7.77 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37.93 10.30 11 11 5 48.09 11.05 -11 -11 -6 185.02 20.79 11 11 6 180.43 20.90 11 11 6 179.85 11.98 11 11 6 207.01 21.71 11 11 7 0.21 1.40 11 11 7 2.23 5.85 -11 -11 -7 1.95 5.74 11 11 7 2.05 4.68 11 11 8 498.64 37.80 -11 -11 -8 581.88 36.44 -11 -11 -8 572.46 36.78 11 11 8 565.87 37.12 -11 -11 -8 501.97 23.22 11 11 9 4.62 6.08 -11 -11 -9 7.10 8.74 -11 -11 -9 12.61 7.12 11 11 9 9.78 6.31 -11 -11 -9 17.81 4.10 -11 -11 -10 102.78 16.51 11 11 10 125.19 17.94 -11 -11 -10 115.60 15.16 11 11 10 101.84 14.66 -11 -11 -10 113.39 15.23 -11 -11 -10 103.90 10.61 11 11 11 142.68 20.10 -11 -11 -11 198.85 19.45 -11 -11 -11 162.26 18.09 11 11 11 177.67 19.05 -11 -11 -11 200.23 22.28 11 11 12 429.83 35.80 -11 -11 -12 486.19 32.55 -11 -11 -12 488.33 32.15 11 11 12 477.95 33.32 -11 -11 -12 451.86 35.84 11 11 13 61.42 13.70 -11 -11 -13 69.50 12.38 11 11 14 354.95 32.39 -11 -11 -14 341.23 26.28 11 11 15 21.91 9.20 -11 -11 -15 17.75 7.22 11 11 16 189.52 24.96 -11 -11 -16 229.87 17.91 -11 -11 -16 172.80 20.36 -11 -11 -16 222.02 20.87 11 11 17 26.30 10.53 -11 -11 -17 25.40 8.63 -11 -11 -17 23.16 9.62 -11 -11 -17 18.24 5.56 -11 -11 -18 264.13 23.99 -11 -11 -18 226.61 24.64 11 12 -5 22.41 9.57 -11 -12 4 61.55 13.83 11 12 -4 53.60 13.34 -11 -12 3 208.19 25.03 11 12 -3 167.01 21.27 11 12 -2 184.71 22.01 11 12 -2 188.41 20.87 11 12 -1 13.77 7.41 11 12 -1 20.49 7.96 11 12 0 63.22 13.05 11 12 0 84.45 13.03 11 12 0 104.03 17.65 11 12 1 299.47 23.50 11 12 1 251.54 25.55 11 12 1 288.11 29.60 11 12 2 241.93 24.02 11 12 2 209.49 18.12 11 12 2 206.65 24.39 11 12 3 91.52 15.23 11 12 3 92.30 11.30 11 12 3 101.07 16.19 11 12 4 73.77 14.06 11 12 4 73.15 9.57 11 12 4 78.65 14.06 -11 -12 -5 554.22 40.24 11 12 5 597.08 28.31 11 12 5 612.27 41.09 11 12 5 609.87 41.49 11 12 6 85.21 14.12 -11 -12 -6 63.08 12.86 11 12 6 66.03 6.35 11 12 6 91.55 14.72 11 12 7 2.18 5.72 -11 -12 -7 8.40 6.76 11 12 7 -4.44 9.88 11 12 8 2.13 5.59 11 12 8 13.51 6.94 11 12 9 263.79 25.91 -11 -12 -9 215.25 11.90 -11 -12 -9 263.45 24.33 11 12 9 282.32 25.14 -11 -12 -9 230.95 12.06 -11 -12 -10 277.01 16.54 -11 -12 -10 297.04 27.48 11 12 10 363.57 30.70 -11 -12 -10 324.85 26.67 11 12 10 363.71 28.41 -11 -12 -10 250.30 16.32 -11 -12 -11 20.45 8.21 11 12 11 9.61 7.75 -11 -12 -11 34.94 6.60 -11 -12 -11 10.55 7.15 -11 -12 -11 30.80 10.26 11 12 11 16.09 7.02 -11 -12 -11 22.83 5.40 11 12 12 197.34 23.19 11 12 12 203.33 21.42 -11 -12 -12 187.57 16.27 -11 -12 -12 191.24 20.19 11 12 13 198.44 23.45 11 12 13 231.29 22.75 -11 -12 -13 211.48 18.35 -11 -12 -13 251.25 22.02 11 12 14 15.80 8.50 -11 -12 -14 17.80 6.92 -11 -12 -14 18.19 7.39 11 12 14 30.15 8.79 11 12 15 35.37 10.76 -11 -12 -15 23.26 7.30 -11 -12 -15 21.14 7.44 11 12 16 42.14 11.99 -11 -12 -16 19.99 6.60 -11 -12 -16 29.38 8.40 -11 -12 -16 20.79 8.96 -11 -12 -17 124.49 17.94 -11 -12 -17 142.48 14.79 -11 -12 -18 47.12 13.59 -11 -12 -19 336.98 30.86 -11 -12 -20 30.64 11.64 -11 -12 -21 150.58 20.69 11 13 -5 60.59 13.85 11 13 -4 28.51 10.16 11 13 -3 9.33 7.51 11 13 -2 151.08 19.57 -11 -13 2 116.97 18.85 11 13 -1 9.00 10.47 11 13 -1 12.01 7.48 11 13 0 6.65 7.43 11 13 0 4.70 5.62 -11 -13 0 -4.29 12.30 11 13 1 65.64 12.92 11 13 1 74.73 11.38 11 13 1 71.43 15.50 11 13 2 344.03 30.10 11 13 2 400.95 25.69 11 13 2 372.05 33.61 11 13 3 161.16 19.31 11 13 3 133.76 13.54 11 13 3 172.27 21.70 11 13 4 6.06 4.26 11 13 4 4.29 6.31 11 13 4 -2.49 6.55 11 13 5 85.93 14.58 11 13 5 58.87 7.30 11 13 5 79.54 14.17 11 13 6 275.14 26.98 11 13 6 301.51 27.26 -11 -13 -7 164.04 20.33 11 13 7 190.54 21.81 11 13 7 160.65 20.27 -11 -13 -8 -2.18 6.39 11 13 8 -2.24 5.51 11 13 8 2.23 6.57 -11 -13 -9 71.38 13.38 11 13 9 107.69 15.93 11 13 9 68.24 14.45 -11 -13 -10 399.91 30.26 11 13 10 393.58 30.44 11 13 10 367.22 30.83 -11 -13 -10 291.49 14.12 11 13 11 102.36 17.19 11 13 11 149.21 18.19 -11 -13 -11 126.96 17.60 -11 -13 -11 115.57 10.01 11 13 12 122.54 17.47 11 13 12 112.58 17.78 11 13 13 44.35 11.10 11 13 13 80.84 15.34 11 13 14 212.52 22.14 11 13 14 180.35 23.39 -11 -13 -15 31.33 8.73 11 13 15 24.28 9.43 -11 -13 -16 43.67 10.78 11 13 16 64.03 14.04 -11 -13 -17 17.33 11.04 -11 -13 -17 8.65 5.69 -11 -13 -17 1.58 5.88 -11 -13 -18 371.72 33.17 -11 -13 -19 74.47 15.85 -11 -13 -20 24.85 10.86 11 14 -4 92.02 15.73 11 14 -3 52.04 12.21 11 14 -2 64.62 13.12 11 14 -1 357.96 30.88 11 14 0 15.16 8.06 11 14 1 38.50 10.60 11 14 2 59.37 12.42 11 14 2 88.14 11.65 11 14 3 102.97 11.72 11 14 3 109.83 16.38 11 14 3 128.43 19.45 11 14 4 7.78 6.83 11 14 4 8.43 5.54 11 14 5 2.54 5.75 11 14 5 2.13 4.84 11 14 6 76.45 14.14 11 14 6 62.25 12.68 11 14 7 45.85 11.36 11 14 7 60.82 12.24 11 14 8 11.80 7.93 11 14 8 17.65 8.21 11 14 9 6.94 6.09 -11 -14 -9 11.23 8.61 11 14 9 2.24 7.82 11 14 10 84.48 15.28 -11 -14 -10 102.49 16.46 11 14 10 71.20 13.96 11 14 11 602.67 42.50 -11 -14 -11 605.38 42.43 11 14 11 657.12 43.13 11 14 12 2.23 5.87 11 14 12 -2.42 5.96 11 14 13 361.05 30.34 11 14 13 330.67 31.40 11 14 14 38.10 10.26 11 14 14 25.87 10.26 11 14 15 232.12 27.08 11 14 16 104.70 18.71 -11 -14 -16 129.27 20.06 -11 -14 -17 20.48 7.20 -11 -14 -17 15.57 11.33 -11 -14 -18 10.40 11.08 11 15 -2 81.57 14.66 11 15 -1 -8.48 8.83 11 15 0 153.00 19.00 11 15 1 35.30 10.09 11 15 2 20.67 8.40 11 15 3 80.29 13.67 11 15 4 285.38 26.26 11 15 4 338.60 31.48 11 15 5 6.26 5.48 11 15 5 7.93 6.50 11 15 6 2.11 6.50 11 15 6 -5.17 6.79 11 15 7 36.28 10.39 11 15 7 43.00 11.59 11 15 8 136.80 18.40 11 15 8 128.72 18.95 11 15 9 -2.44 7.15 11 15 9 2.21 7.69 11 15 10 2.41 5.46 11 15 10 6.79 5.57 11 15 11 533.13 38.66 11 15 11 448.52 35.85 11 15 12 443.71 35.64 11 15 12 515.35 38.03 11 15 13 37.51 10.50 11 15 13 22.28 9.25 11 15 14 77.69 14.94 11 15 14 86.77 16.32 11 15 15 42.14 11.57 -11 -15 -16 208.08 26.22 -11 -15 -17 11.90 6.13 11 16 0 6.03 6.19 11 16 1 111.90 15.89 11 16 2 271.09 25.27 11 16 3 10.01 6.45 11 16 4 88.58 14.20 11 16 5 166.54 19.28 11 16 5 148.84 21.05 11 16 6 2.05 6.03 11 16 6 10.81 7.93 11 16 7 12.51 7.26 11 16 7 15.86 8.16 11 16 8 95.84 16.53 11 16 8 110.35 16.53 11 16 9 308.23 29.69 11 16 9 285.86 27.24 11 16 10 20.10 9.91 11 16 10 13.31 7.17 11 16 11 -2.49 6.09 11 16 11 4.57 6.01 11 16 12 51.75 12.71 11 16 12 70.84 13.86 11 16 13 46.71 11.73 11 16 13 34.06 10.69 11 16 14 17.28 9.18 11 16 14 5.02 5.72 -11 -16 -17 243.95 22.59 11 17 2 80.16 13.44 11 17 3 349.12 28.52 11 17 4 7.74 7.20 11 17 5 136.94 17.50 11 17 6 3.97 6.11 11 17 7 395.35 31.14 11 17 8 -2.06 6.63 11 17 9 146.42 20.67 11 17 9 137.02 18.07 11 17 10 259.68 27.21 11 17 10 212.48 23.11 11 17 11 72.57 14.56 11 17 11 107.38 16.38 11 17 12 131.32 19.00 11 17 12 115.41 17.54 11 17 13 66.85 14.92 11 17 13 73.82 14.71 11 17 14 79.93 15.60 11 17 14 88.53 15.93 11 18 5 35.25 9.04 11 18 6 67.95 12.12 11 18 7 5.79 6.47 11 18 8 300.44 26.64 11 18 9 -2.03 5.67 11 18 10 210.37 22.75 11 18 11 225.60 23.83 11 18 12 279.95 26.75 11 18 13 18.53 7.78 11 19 8 45.02 10.56 11 19 9 205.92 21.14 11 19 10 6.03 6.19 11 19 11 106.08 16.12 -12 13 3 31.94 11.62 12 -13 -3 18.19 9.61 -12 13 2 35.92 11.96 12 -13 -2 24.72 9.74 -12 13 1 79.21 16.17 12 -12 -4 62.96 13.88 12 -12 -4 34.67 11.49 12 -12 -3 2.52 6.63 -12 12 3 13.62 11.04 12 -12 -3 6.09 8.65 12 -12 -2 73.02 14.90 -12 12 2 94.80 18.02 12 -12 -2 77.62 13.67 12 -12 -1 7.07 8.86 12 -12 -1 28.23 10.03 12 -12 0 84.80 13.00 12 -11 -5 34.65 11.41 12 -11 -5 25.06 9.36 12 -11 -4 -4.26 6.57 12 -11 -4 -6.50 9.00 -12 11 4 -2.86 9.61 12 -11 -4 -10.76 9.67 12 -11 -3 19.52 8.84 12 -11 -3 32.41 10.19 12 -11 -3 28.51 9.69 12 -11 -2 2.50 6.58 12 -11 -2 3.80 6.84 12 -11 -1 108.96 17.44 12 -11 -1 121.29 15.99 12 -11 0 -2.36 6.91 12 -11 0 3.25 6.92 12 -11 1 310.99 28.77 12 -11 1 303.14 24.23 12 -11 2 -6.73 5.90 12 -11 2 -4.06 5.77 12 -11 3 6.61 6.16 12 -10 -6 122.85 17.00 12 -10 -5 60.69 13.23 12 -10 -5 70.41 13.26 12 -10 -5 79.54 16.22 12 -10 -4 35.72 10.03 12 -10 -4 35.64 10.87 12 -10 -4 26.23 9.80 -12 10 4 34.88 11.51 12 -10 -3 10.21 7.82 12 -10 -3 -2.65 8.16 12 -10 -3 12.82 8.19 12 -10 -2 190.85 20.62 12 -10 -2 176.52 22.35 12 -10 -2 199.84 22.14 12 -10 -1 37.14 12.03 12 -10 -1 42.29 10.32 12 -10 -1 39.70 11.49 12 -10 0 170.81 18.14 12 -10 0 190.27 22.64 12 -10 0 174.86 21.39 12 -10 1 39.88 11.57 12 -10 1 29.77 8.58 12 -10 1 20.51 9.52 12 -10 2 486.77 37.79 12 -10 2 455.03 35.72 12 -10 2 479.07 30.26 12 -10 3 20.40 8.94 12 -10 3 7.22 5.82 12 -10 4 18.02 8.13 12 -10 5 17.99 8.13 12 -10 6 24.70 8.65 12 -9 -6 -2.50 8.70 12 -9 -6 -6.14 8.71 12 -9 -5 191.81 21.65 12 -9 -5 213.33 25.82 12 -9 -5 177.17 22.48 -12 9 5 185.21 25.60 12 -9 -4 210.91 22.40 12 -9 -4 217.31 25.96 12 -9 -4 225.42 24.17 -12 9 4 235.19 28.60 12 -9 -3 24.69 9.38 12 -9 -3 13.46 7.91 12 -9 -3 4.23 7.09 12 -9 -2 19.19 8.40 12 -9 -2 23.44 8.76 12 -9 -2 23.52 8.92 12 -9 -1 103.45 16.66 12 -9 -1 84.72 14.84 12 -9 -1 70.75 12.40 12 -9 0 176.57 22.54 12 -9 0 172.71 18.40 12 -9 0 175.90 20.88 12 -9 1 189.53 21.60 12 -9 1 162.10 17.49 12 -9 1 153.19 20.71 -12 9 -1 168.63 24.51 12 -9 2 44.56 11.60 -12 9 -2 41.12 13.85 12 -9 2 31.04 7.95 12 -9 2 47.47 11.96 -12 9 -3 350.51 34.85 12 -9 3 344.60 30.54 12 -9 3 298.18 22.18 12 -9 3 328.66 29.43 12 -9 4 94.08 15.85 12 -9 4 97.32 11.49 12 -9 4 86.38 16.11 -12 9 -4 85.28 17.89 12 -9 5 2.31 6.76 12 -9 5 4.32 4.32 12 -9 5 2.37 7.93 -12 9 -5 3.17 9.77 12 -9 6 13.85 8.04 12 -9 7 229.48 24.49 12 -9 8 20.92 8.11 12 -9 9 44.26 11.95 12 -8 -7 324.64 28.10 12 -8 -6 141.92 20.75 12 -8 -6 154.58 19.44 12 -8 -5 35.17 10.58 12 -8 -5 20.43 10.55 12 -8 -5 21.53 9.48 -12 8 5 45.91 14.53 12 -8 -4 131.84 18.76 12 -8 -4 143.93 21.60 12 -8 -4 120.66 17.11 12 -8 -3 440.68 33.95 12 -8 -3 453.23 37.62 12 -8 -3 393.88 32.11 12 -8 -2 185.98 20.98 12 -8 -2 248.35 26.67 12 -8 -2 192.01 21.88 12 -8 -1 -7.17 8.66 12 -8 -1 -6.42 8.43 12 -8 0 89.66 15.89 12 -8 0 87.39 13.52 12 -8 0 132.07 17.63 12 -8 1 333.38 29.84 12 -8 1 341.09 29.30 12 -8 1 286.66 23.52 12 -8 1 277.04 18.74 -12 8 -1 298.75 31.69 12 -8 2 4.78 6.27 12 -8 2 1.37 5.49 12 -8 2 -2.21 8.22 12 -8 2 -0.72 2.60 -12 8 -2 -3.06 7.52 12 -8 3 -2.36 8.17 12 -8 3 1.20 5.14 12 -8 3 2.24 6.58 12 -8 3 5.12 2.60 -12 8 -3 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92.33 18.56 12 -6 12 26.17 10.34 12 -6 12 5.40 9.39 12 -6 13 42.55 13.15 12 -6 14 91.50 16.51 12 -5 -7 14.16 12.09 12 -5 -7 31.81 10.27 -12 5 7 29.56 11.85 12 -5 -6 2.67 8.58 12 -5 -6 4.26 7.67 -12 5 6 16.06 10.76 -12 5 6 12.86 11.57 12 -5 -5 70.23 15.16 -12 5 5 44.01 13.13 12 -5 -5 38.40 11.47 12 -5 -5 23.96 10.50 12 -5 -4 112.35 17.57 12 -5 -4 141.95 18.07 12 -5 -4 147.95 21.70 12 -5 -3 50.63 11.78 12 -5 -3 65.55 13.78 -12 5 3 62.49 11.18 12 -5 -3 70.21 14.68 12 -5 -2 73.54 13.72 12 -5 -2 81.10 14.17 -12 5 2 93.63 13.03 12 -5 -2 119.78 18.66 12 -5 -1 16.77 9.36 12 -5 -1 20.58 9.05 -12 5 1 11.80 7.41 12 -5 -1 31.69 10.71 12 -5 0 239.25 23.94 12 -5 0 254.66 26.44 12 -5 0 236.50 21.88 -12 5 0 198.86 18.48 12 -5 1 27.61 10.48 12 -5 1 32.76 8.52 -12 5 -1 47.05 12.38 12 -5 1 21.06 9.44 12 -5 2 12.32 7.61 12 -5 2 18.22 7.04 -12 5 -2 21.96 9.88 12 -5 2 12.68 7.62 -12 5 -3 49.18 12.74 12 -5 3 101.93 16.33 12 -5 3 89.16 11.49 12 -5 3 95.56 15.41 12 -5 4 217.64 17.03 12 -5 4 235.22 23.40 -12 5 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21.37 12 6 13 36.08 11.34 -12 -6 -13 43.26 4.83 12 6 13 45.93 10.73 -12 -6 -13 46.77 5.41 -12 -6 -13 44.00 11.00 -12 -6 -14 46.37 11.34 12 6 14 16.48 8.40 12 6 14 25.69 9.96 -12 -6 -15 331.65 28.51 12 6 15 400.25 36.00 12 6 15 367.08 30.23 12 6 16 30.39 10.97 12 6 16 26.20 8.63 12 6 17 131.17 20.71 12 6 17 109.39 16.30 12 6 18 250.29 29.69 12 6 18 247.34 24.18 12 6 19 192.56 20.98 12 6 20 35.80 10.14 12 6 21 3.67 6.37 -12 -7 5 6.21 10.01 12 7 -5 11.59 8.52 12 7 -4 2.83 10.50 12 7 -3 270.46 28.44 -12 -7 2 42.32 11.98 12 7 -2 61.95 14.69 -12 -7 1 49.91 11.36 12 7 -1 31.63 10.19 -12 -7 1 39.23 7.69 12 7 0 56.87 14.37 -12 -7 0 63.64 9.49 12 7 1 961.78 57.08 -12 -7 -1 1028.95 53.11 -12 -7 -1 856.82 43.67 -12 -7 -2 178.86 19.06 12 7 2 154.97 20.45 -12 -7 -2 149.21 15.20 12 7 3 14.20 6.81 12 7 3 14.84 7.96 -12 -7 -3 7.00 6.32 12 7 4 163.24 18.58 -12 -7 -4 136.54 16.71 12 7 4 147.07 19.97 12 7 5 70.16 12.04 12 7 5 44.68 11.10 -12 -7 -5 59.89 11.23 12 7 5 60.98 13.16 12 7 6 2.44 5.54 12 7 6 1.98 7.80 -12 -7 -6 11.96 6.37 -12 -7 -6 3.66 5.64 -12 -7 -6 12.87 5.22 12 7 6 -1.76 4.00 12 7 7 9.67 6.48 12 7 7 14.71 7.90 12 7 7 8.34 5.38 -12 -7 -7 9.39 4.52 -12 -7 -7 18.25 7.04 -12 -7 -7 10.91 6.55 12 7 8 148.84 20.88 12 7 8 235.29 22.69 -12 -7 -8 190.09 17.85 12 7 8 213.43 23.19 -12 -7 -8 189.58 17.89 -12 -7 -8 215.07 21.26 12 7 8 250.76 20.93 12 7 9 145.62 17.55 -12 -7 -9 105.88 14.25 -12 -7 -9 143.54 14.56 12 7 9 138.00 15.28 -12 -7 -9 136.80 16.89 12 7 10 17.41 4.31 12 7 10 12.84 6.16 -12 -7 -10 10.92 6.16 12 7 10 8.86 7.43 -12 -7 -10 6.61 4.49 12 7 10 16.24 5.67 -12 -7 -10 7.18 7.46 12 7 11 101.41 9.57 12 7 11 132.13 16.25 12 7 11 111.28 17.63 -12 -7 -11 106.50 14.53 -12 -7 -11 135.43 12.84 -12 -7 -11 100.26 15.29 12 7 11 122.77 14.20 -12 -7 -12 15.88 5.23 12 7 12 18.12 6.37 -12 -7 -12 16.12 8.35 12 7 12 36.63 10.03 -12 -7 -13 3.79 3.59 12 7 13 12.81 7.69 -12 -7 -13 10.81 6.70 12 7 14 2.10 8.74 -12 -7 -14 1.82 8.78 -12 -7 -14 12.86 3.15 -12 -7 -15 95.32 15.03 12 7 15 99.77 18.40 12 7 15 103.87 16.27 12 7 16 172.68 23.63 12 7 16 110.65 16.20 12 7 17 6.22 9.61 12 7 17 14.12 8.17 12 7 18 25.61 11.56 12 7 18 29.81 10.16 12 7 19 50.45 12.74 12 7 20 79.49 13.67 12 8 -5 5.72 7.52 -12 -8 5 18.46 11.44 12 8 -4 30.77 10.78 -12 -8 4 42.09 13.73 12 8 -3 16.38 10.17 12 8 -2 381.82 33.90 -12 -8 1 27.00 9.02 12 8 -1 5.23 9.10 12 8 0 7.70 6.74 12 8 1 47.94 11.60 -12 -8 -1 46.21 7.13 12 8 2 504.98 37.75 12 8 2 488.22 35.77 -12 -8 -2 471.72 34.24 -12 -8 -2 433.81 24.91 12 8 3 7.39 6.87 -12 -8 -3 7.56 6.57 12 8 3 2.15 5.62 -12 -8 -3 0.91 4.96 -12 -8 -4 84.79 13.65 12 8 4 63.60 12.17 12 8 4 75.72 14.74 -12 -8 -5 280.21 24.38 12 8 5 286.19 25.17 12 8 5 279.49 27.87 -12 -8 -6 286.56 24.31 12 8 6 286.04 24.75 12 8 6 306.60 28.91 -12 -8 -7 136.55 14.32 12 8 7 184.03 19.11 -12 -8 -7 188.14 18.28 12 8 7 151.62 20.33 12 8 7 184.87 20.59 12 8 8 -4.96 7.28 12 8 8 5.87 6.03 -12 -8 -8 -10.94 6.99 12 8 8 2.31 6.79 -12 -8 -8 1.46 4.92 -12 -8 -8 1.25 4.01 12 8 8 1.72 4.23 -12 -8 -9 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9 1 122.85 18.53 12 9 2 65.56 13.02 12 9 2 49.49 12.11 12 9 3 744.39 45.80 12 9 3 724.89 46.89 -12 -9 -3 730.07 43.87 -12 -9 -3 612.73 29.14 12 9 4 2.44 7.15 -12 -9 -4 -1.95 5.72 12 9 4 2.16 6.03 -12 -9 -4 2.62 3.28 12 9 5 140.45 19.28 12 9 5 186.76 20.38 -12 -9 -5 174.06 19.26 12 9 6 7.28 5.96 12 9 6 5.96 5.22 -12 -9 -6 3.59 7.82 12 9 7 451.15 35.80 12 9 7 477.02 32.72 -12 -9 -7 372.80 23.53 -12 -9 -7 461.76 31.12 12 9 8 99.06 17.23 -12 -9 -8 94.04 14.04 12 9 8 107.09 15.13 -12 -9 -8 93.69 11.59 -12 -9 -9 161.27 17.05 12 9 9 128.43 19.10 12 9 9 118.17 15.46 -12 -9 -9 123.06 13.25 12 9 10 13.90 6.68 12 9 10 12.82 6.78 12 9 10 20.67 8.83 -12 -9 -10 17.41 6.76 -12 -9 -10 30.73 7.26 12 9 11 684.39 47.26 12 9 11 667.57 44.22 -12 -9 -11 668.26 37.51 -12 -9 -11 636.59 36.99 12 9 11 742.52 41.13 12 9 12 8.97 7.52 12 9 12 14.95 6.39 -12 -9 -12 16.06 8.63 -12 -9 -12 16.56 6.29 12 9 12 21.45 9.35 12 9 13 2.21 6.83 -12 -9 -13 1.77 6.79 12 9 13 3.30 4.84 12 9 13 -2.75 7.22 -12 -9 -13 4.73 4.40 12 9 14 19.63 9.12 -12 -9 -14 35.02 7.39 12 9 14 22.57 9.85 12 9 15 171.84 23.66 12 9 15 148.42 19.60 -12 -9 -15 173.15 13.65 12 9 16 69.74 13.94 12 9 17 47.60 11.96 12 9 18 70.78 12.84 12 9 19 229.69 23.05 12 9 20 66.20 12.87 12 10 -4 252.97 27.87 -12 -10 4 271.93 30.12 12 10 -3 98.62 17.49 12 10 -2 -2.62 7.28 12 10 -1 2.57 5.83 12 10 0 681.05 46.81 12 10 1 12.43 8.65 12 10 1 -2.54 5.79 12 10 2 12.29 7.91 12 10 2 9.82 6.86 12 10 3 -2.44 7.83 12 10 3 2.36 5.80 -12 -10 -4 479.75 35.33 12 10 4 444.75 35.58 12 10 4 438.20 34.42 12 10 5 26.51 9.26 -12 -10 -5 24.13 8.99 -12 -10 -5 17.54 2.91 12 10 5 24.00 8.86 -12 -10 -6 50.30 11.57 12 10 6 79.72 14.53 12 10 6 63.04 12.06 12 10 7 119.76 16.33 -12 -10 -7 135.54 17.08 12 10 7 114.48 17.60 -12 -10 -8 1079.29 48.35 -12 -10 -8 1143.76 58.51 12 10 8 1143.29 64.41 12 10 8 1260.86 61.35 -12 -10 -9 15.86 5.05 12 10 9 9.57 5.92 -12 -10 -9 6.78 6.70 12 10 9 12.55 9.04 -12 -10 -10 177.13 18.50 12 10 10 155.99 21.05 12 10 10 171.28 19.13 -12 -10 -10 150.63 14.46 12 10 11 7.83 8.06 -12 -10 -11 6.24 4.50 -12 -10 -11 9.17 6.66 12 10 11 10.95 5.88 12 10 12 454.76 31.77 -12 -10 -12 463.71 29.81 12 10 12 421.78 36.60 12 10 13 3.56 5.72 12 10 13 2.73 5.69 -12 -10 -13 4.10 5.38 12 10 14 106.79 18.20 -12 -10 -14 89.86 12.82 12 10 15 28.98 11.78 12 10 16 436.10 38.45 12 10 17 -3.07 10.69 12 10 18 31.59 12.16 12 11 -4 8.03 7.87 -12 -11 4 22.93 11.91 12 11 -3 309.62 30.70 -12 -11 3 320.64 32.85 12 11 -2 82.48 15.78 12 11 -1 81.03 15.85 12 11 0 7.48 5.69 12 11 0 19.19 9.20 12 11 1 364.52 31.98 12 11 1 371.53 34.08 12 11 2 31.64 10.47 12 11 2 66.55 14.16 12 11 3 9.65 6.73 12 11 3 -2.47 6.48 12 11 4 2.41 6.68 12 11 4 -2.39 5.87 12 11 5 280.19 26.74 -12 -11 -5 278.09 26.41 12 11 5 299.63 27.92 -12 -11 -6 193.66 21.60 12 11 6 189.73 22.54 12 11 6 172.84 20.64 12 11 7 21.84 9.88 -12 -11 -7 38.10 10.92 12 11 7 34.45 4.60 12 11 7 25.82 8.32 12 11 8 12.55 6.16 -12 -11 -8 15.42 8.03 12 11 8 12.30 7.59 -12 -11 -9 284.53 25.55 12 11 9 317.34 30.05 12 11 9 313.54 26.85 -12 -11 -9 295.21 17.91 12 11 10 17.81 8.55 -12 -11 -10 23.99 5.61 -12 -11 -10 21.19 7.90 12 11 10 19.86 8.29 -12 -11 -11 281.99 23.83 -12 -11 -11 283.77 19.86 12 11 11 278.89 24.75 12 11 11 254.64 27.79 -12 -11 -12 1.61 5.80 -12 -11 -12 2.47 4.13 12 11 12 -1.92 5.04 12 11 12 15.93 8.55 12 11 13 343.96 28.57 -12 -11 -13 377.79 27.56 12 11 13 369.97 33.74 12 11 14 -1.90 9.02 12 11 14 2.80 7.35 -12 -11 -14 1.46 6.35 12 11 15 89.42 17.02 12 11 16 11.88 8.29 12 11 17 180.24 24.87 -12 -12 3 38.42 13.08 12 12 -3 46.34 12.51 12 12 -2 96.25 16.80 12 12 -1 29.90 11.15 12 12 0 12.30 9.17 12 12 0 21.24 8.61 12 12 1 7.28 6.39 12 12 1 1.48 6.03 12 12 1 5.51 6.78 12 12 2 315.18 30.13 12 12 2 337.11 24.48 12 12 2 338.31 32.18 12 12 3 83.50 14.84 12 12 3 87.60 11.15 12 12 3 90.15 15.42 12 12 4 2.37 9.62 12 12 4 9.90 4.23 12 12 4 14.94 7.67 12 12 5 11.88 7.33 12 12 5 10.29 4.89 12 12 5 16.82 8.06 12 12 6 290.46 16.43 12 12 6 312.55 28.88 12 12 6 347.35 29.68 12 12 7 115.62 17.13 12 12 7 106.18 16.74 -12 -12 -7 105.67 16.33 12 12 8 2.21 6.18 12 12 8 -12.24 8.52 -12 -12 -8 -2.08 7.96 12 12 9 -6.48 7.77 -12 -12 -9 2.00 7.20 12 12 9 2.49 6.92 -12 -12 -10 675.17 41.72 12 12 10 624.58 41.48 12 12 10 665.68 45.95 -12 -12 -11 61.03 12.11 -12 -12 -11 67.24 8.53 12 12 11 62.21 12.69 12 12 11 72.29 15.34 -12 -12 -12 31.95 10.24 -12 -12 -12 35.97 6.86 12 12 12 44.91 10.63 12 12 12 36.91 11.30 12 12 13 34.39 9.65 -12 -12 -13 34.02 9.43 12 12 13 35.15 11.30 12 12 14 188.25 20.49 12 12 14 155.83 21.63 -12 -12 -14 128.85 16.09 12 12 15 20.09 9.26 -12 -12 -16 125.00 13.70 12 12 16 120.92 20.02 12 12 17 -9.10 8.45 12 13 -3 143.39 20.17 12 13 -2 17.36 8.32 12 13 -1 252.04 26.36 12 13 0 19.34 9.30 12 13 1 9.57 6.68 12 13 2 2.78 6.31 12 13 2 2.37 5.82 12 13 3 158.36 21.45 12 13 3 167.17 21.16 12 13 4 59.06 8.21 12 13 4 46.99 12.14 12 13 5 17.62 8.11 12 13 5 9.28 3.93 12 13 5 4.70 7.57 12 13 6 80.82 14.77 12 13 6 61.61 13.07 12 13 7 431.32 34.98 12 13 7 429.55 34.44 12 13 8 -2.42 5.96 12 13 8 -2.32 7.18 12 13 9 22.75 8.73 -12 -13 -9 10.76 6.65 12 13 9 9.85 6.89 12 13 10 2.52 8.74 12 13 10 22.30 10.97 -12 -13 -10 20.80 9.67 12 13 11 184.24 22.83 12 13 11 147.12 18.98 -12 -13 -11 200.51 21.42 12 13 12 211.98 25.14 12 13 12 194.52 21.83 -12 -13 -12 231.82 22.80 12 13 13 32.20 10.32 12 13 13 27.89 8.50 -12 -13 -13 18.63 8.52 12 13 14 24.87 9.98 12 13 14 21.45 9.17 -12 -13 -14 23.39 8.06 12 13 15 250.38 28.17 12 13 16 -5.85 7.69 12 13 17 39.05 12.24 12 14 -3 24.44 9.93 12 14 -2 45.91 12.79 12 14 -1 7.17 6.27 12 14 0 278.73 27.58 12 14 1 156.80 20.53 12 14 2 20.92 8.94 12 14 3 2.32 6.09 12 14 4 216.50 25.19 12 14 4 233.63 24.49 12 14 5 2.32 5.28 12 14 5 10.52 8.11 12 14 6 16.41 7.87 12 14 6 12.82 7.56 12 14 7 211.07 23.57 12 14 7 165.30 21.26 12 14 8 160.87 21.08 12 14 8 193.39 22.53 12 14 9 34.16 10.91 12 14 9 14.37 8.35 12 14 10 14.90 8.34 12 14 10 11.75 7.88 12 14 11 48.09 12.27 12 14 11 25.42 8.92 12 14 12 372.78 33.93 12 14 12 383.26 32.49 -12 -14 -12 415.70 32.52 12 14 13 -5.31 6.99 12 14 13 2.26 7.59 -12 -14 -13 -2.03 6.24 12 14 14 36.18 10.16 12 14 14 35.59 11.17 12 14 15 50.71 14.45 12 14 16 306.80 31.74 12 15 -1 39.28 12.42 12 15 0 29.81 9.82 12 15 1 316.60 29.04 12 15 2 31.77 9.72 12 15 3 115.51 17.55 12 15 4 2.28 8.70 12 15 5 343.46 30.65 12 15 6 29.45 10.32 12 15 6 34.68 10.35 12 15 7 13.12 8.09 12 15 7 7.00 8.40 12 15 8 115.34 17.57 12 15 8 63.87 13.31 12 15 9 320.04 29.87 12 15 9 273.61 28.26 12 15 10 22.02 9.43 12 15 10 37.04 10.81 12 15 11 37.49 11.44 12 15 11 36.45 11.13 12 15 12 5.12 7.13 12 15 12 4.79 7.05 12 15 13 350.03 32.65 12 15 13 326.27 30.03 12 15 14 -4.76 7.65 12 15 15 88.98 17.21 12 15 16 263.04 28.80 12 16 1 -2.19 7.38 12 16 2 59.34 13.07 12 16 3 328.96 29.38 12 16 4 11.10 6.86 12 16 5 11.20 6.91 12 16 6 307.19 28.56 12 16 7 212.60 23.44 12 16 8 25.53 9.93 12 16 9 9.43 7.59 12 16 9 2.62 8.09 12 16 10 221.13 25.21 12 16 10 260.74 27.52 12 16 11 39.33 11.34 12 16 11 81.36 15.60 12 16 12 2.52 6.63 12 16 12 2.52 5.72 12 16 13 158.46 22.20 12 16 13 177.33 22.40 12 16 14 136.03 20.79 12 16 14 129.58 19.21 12 16 15 54.79 13.83 12 17 3 4.26 6.26 12 17 4 791.44 49.29 12 17 5 19.49 9.02 12 17 6 52.56 11.65 12 17 7 193.50 22.28 12 17 8 300.12 28.36 12 17 9 29.89 9.83 12 17 10 105.75 17.57 12 17 11 94.00 16.32 12 17 12 326.83 30.41 12 17 13 10.17 7.10 12 17 14 -2.62 7.69 12 17 15 51.06 12.86 12 18 6 4.21 6.48 12 18 7 91.78 15.03 12 18 8 93.60 15.21 12 18 9 178.00 21.05 12 18 10 11.41 7.65 12 18 11 11.73 6.91 12 18 12 101.35 16.69 12 18 13 230.65 25.74 12 18 14 2.55 7.49 12 19 10 46.16 11.30 12 19 11 9.04 6.97 12 19 12 142.01 19.23 12 19 13 201.45 23.65 13 -11 -3 10.79 9.43 13 -11 -2 188.07 21.65 13 -11 -1 20.82 10.56 13 -11 0 20.22 9.12 13 -11 1 17.23 8.87 13 -10 -4 232.42 25.79 13 -10 -3 113.69 17.78 13 -10 -2 5.49 7.22 13 -10 -2 8.17 8.71 13 -10 -1 292.93 30.20 13 -10 -1 332.18 27.79 13 -10 0 54.45 13.25 13 -10 0 24.49 8.83 13 -10 1 48.04 12.53 13 -10 2 2.47 7.98 13 -10 3 258.90 26.69 13 -10 4 29.09 10.13 13 -10 5 79.82 15.16 13 -9 -4 113.18 18.61 13 -9 -3 141.67 19.13 13 -9 -2 11.20 8.22 13 -9 -2 4.13 6.92 13 -9 -1 5.43 7.57 13 -9 -1 -3.84 8.55 13 -9 0 74.11 15.16 13 -9 0 68.86 12.51 13 -9 1 170.52 21.60 13 -9 1 147.80 17.54 13 -9 2 22.79 9.15 13 -9 2 27.58 8.58 13 -9 3 7.49 7.69 13 -9 4 454.79 36.67 13 -9 5 185.31 22.80 13 -9 6 71.79 14.76 13 -9 7 -9.91 8.00 13 -9 8 114.29 18.45 13 -8 -5 269.25 26.64 13 -8 -5 229.48 26.26 13 -8 -4 6.70 8.03 13 -8 -4 7.18 7.38 13 -8 -3 116.55 17.98 13 -8 -3 109.98 17.88 13 -8 -2 187.44 21.86 13 -8 -2 125.09 20.64 13 -8 -2 159.08 19.80 13 -8 -1 11.39 7.93 13 -8 -1 8.29 8.13 13 -8 -1 5.82 7.65 13 -8 0 2.31 7.41 13 -8 0 2.70 7.07 13 -8 0 -1.79 7.77 13 -8 1 4.65 8.63 13 -8 1 -2.63 5.98 13 -8 1 -1.63 6.42 13 -8 2 320.22 30.12 13 -8 2 268.07 27.97 13 -8 2 256.48 22.44 13 -8 3 149.68 20.49 13 -8 3 121.23 14.27 13 -8 4 -2.52 9.64 13 -8 5 92.88 16.14 13 -8 6 330.49 31.04 13 -8 8 10.21 8.22 13 -8 9 364.02 32.78 13 -8 10 20.61 9.61 13 -7 -6 -2.24 9.31 13 -7 -5 126.52 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8 15 95.27 16.63 14 8 16 328.72 30.73 14 8 17 2.44 9.04 14 8 18 145.72 20.35 14 8 19 56.12 13.18 14 8 20 114.34 17.44 14 9 1 58.26 13.90 14 9 1 78.78 16.43 14 9 2 5.12 6.73 14 9 2 -2.89 6.00 14 9 3 2.45 6.05 14 9 3 2.86 5.95 14 9 4 7.10 7.30 14 9 4 14.22 8.35 14 9 5 687.72 45.10 14 9 5 673.87 48.77 14 9 6 82.16 16.35 -14 -9 -6 97.69 14.35 14 9 6 110.94 16.25 -14 -9 -7 8.60 6.19 14 9 7 8.34 6.13 14 9 7 -2.84 11.20 -14 -9 -8 14.66 7.26 14 9 8 8.03 5.92 14 9 8 14.33 9.98 14 9 9 325.16 33.15 -14 -9 -9 279.49 24.12 14 9 9 326.72 27.17 14 9 10 -8.83 8.19 14 9 10 -2.02 3.74 14 9 10 -2.68 7.07 -14 -9 -10 -1.45 5.04 14 9 10 1.85 5.18 14 9 11 -5.31 10.19 14 9 11 5.38 6.22 -14 -9 -11 4.63 4.96 14 9 11 8.96 8.78 14 9 12 78.99 16.90 14 9 12 69.14 11.88 -14 -9 -12 49.36 10.69 14 9 12 60.77 15.86 14 9 13 390.51 35.37 14 9 13 452.12 30.65 14 9 13 398.31 38.18 -14 -9 -13 391.91 30.13 14 9 14 9.44 7.74 14 9 14 2.57 9.25 -14 -9 -14 9.44 6.34 14 9 15 5.07 8.81 14 9 16 89.89 16.85 14 9 17 242.96 26.43 14 9 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11 11 59.17 14.97 14 11 12 71.87 12.71 14 11 12 33.11 12.63 14 11 13 44.91 11.04 14 11 13 70.32 15.93 14 11 14 -1.92 7.15 14 12 3 63.89 14.53 14 12 4 376.99 34.85 14 12 5 80.34 14.98 14 12 5 47.12 13.05 14 12 6 -2.50 5.70 14 12 6 2.78 8.96 14 12 7 17.08 7.20 14 12 7 19.60 10.09 14 12 8 359.65 35.24 14 12 8 457.99 35.09 14 12 9 4.62 7.10 14 12 9 2.86 7.52 14 12 10 2.24 5.51 14 12 10 2.89 8.09 14 12 11 15.29 7.62 14 12 11 20.61 9.88 14 12 12 219.28 23.01 14 12 12 236.24 28.04 14 12 13 16.67 8.00 14 12 13 15.20 10.58 14 12 14 10.27 6.89 14 13 3 8.22 7.20 14 13 4 62.99 15.21 14 13 5 320.69 31.97 14 13 6 5.51 7.69 14 13 7 2.55 4.75 14 13 7 -2.78 10.34 14 13 8 14.95 7.69 14 13 8 11.23 9.05 14 13 9 344.01 30.25 14 13 9 267.17 30.42 14 13 10 33.04 10.14 14 13 10 48.92 12.89 14 13 11 6.91 6.78 14 13 11 2.93 7.18 14 13 12 15.78 8.40 14 13 12 20.75 9.95 14 13 13 353.42 30.00 14 13 13 328.62 34.03 14 13 14 113.39 17.03 14 13 15 8.66 6.37 14 14 4 2.70 7.91 14 14 5 65.03 15.28 14 14 6 289.31 29.92 14 14 7 19.29 8.89 14 14 8 -11.12 11.26 14 14 9 2.81 6.92 14 14 9 5.07 7.82 14 14 10 287.96 30.62 14 14 10 265.06 27.40 14 14 11 8.68 8.50 14 14 11 4.86 7.82 14 14 12 88.09 18.09 14 14 12 135.51 18.87 14 14 13 27.99 10.43 14 14 14 610.39 42.50 14 14 15 6.86 7.05 14 15 5 -5.35 7.85 14 15 6 -2.70 7.07 14 15 7 95.03 17.42 14 15 8 98.78 17.44 14 15 9 16.64 9.31 14 15 10 16.90 9.09 14 15 11 308.27 32.03 14 16 7 -5.33 9.59 14 16 8 86.25 16.30 14 16 9 256.98 28.62 15 -6 -2 150.30 20.88 15 -5 -2 7.15 9.13 15 -5 -1 236.94 24.74 15 -5 0 95.91 15.52 15 -4 -2 21.71 11.00 15 -4 -1 24.69 10.26 15 -4 0 207.14 22.25 15 -4 1 92.75 15.26 15 -4 2 132.88 16.46 15 -3 -2 24.48 11.17 15 -3 -1 72.96 14.89 15 -3 0 4.21 7.07 15 -3 1 57.86 12.04 15 -3 2 33.07 9.90 15 -3 3 18.51 7.33 -15 3 -4 18.15 10.16 -15 3 -5 321.29 33.48 -15 3 -6 57.84 14.84 15 -3 11 2.44 7.51 15 -2 -2 69.53 15.31 15 -2 -1 9.26 8.87 15 -2 0 2.15 7.46 15 -2 1 -3.93 7.96 15 -2 2 92.78 15.07 -15 2 -4 2.91 6.65 15 -2 4 19.96 5.88 15 -2 5 9.09 6.91 -15 2 -5 5.83 8.13 15 -2 6 244.57 28.30 -15 2 -6 269.16 29.45 15 -2 7 72.47 16.30 -15 2 -7 70.78 15.70 15 -2 8 -6.09 11.67 -15 2 -8 -2.97 9.98 -15 2 -9 21.06 10.86 15 -2 11 11.51 9.07 15 -2 12 23.32 10.42 15 -2 13 89.89 15.68 15 -2 14 7.23 7.43 -15 1 2 -3.02 7.93 15 -1 -2 2.52 8.76 15 -1 -1 148.27 21.01 15 -1 0 21.84 9.10 15 -1 1 12.06 8.35 15 -1 2 1.84 6.37 15 -1 4 24.62 10.71 -15 1 -4 25.16 10.08 15 -1 4 11.82 5.88 15 -1 5 -1.12 3.61 15 -1 6 3.04 6.92 -15 1 -6 8.43 9.05 15 -1 7 327.52 32.94 -15 1 -7 285.55 30.26 15 -1 8 3.06 6.96 -15 1 -8 2.86 7.51 15 -1 9 -3.09 9.51 -15 1 -9 2.89 8.06 -15 1 -10 -5.87 8.63 15 -1 11 43.31 11.99 15 -1 12 72.23 14.45 15 -1 13 162.25 20.77 15 -1 14 113.18 17.65 15 -1 15 218.63 24.49 -15 0 3 -2.91 8.13 -15 0 2 155.55 23.06 15 0 -2 130.47 19.76 -15 0 1 2.84 7.49 15 0 -1 -2.39 8.03 15 0 0 151.67 19.91 -15 0 -4 160.44 22.48 15 0 4 165.99 17.13 15 0 4 222.62 27.61 15 0 4 178.89 23.32 -15 0 -5 34.76 11.95 15 0 5 21.65 6.65 15 0 5 18.38 9.48 15 0 5 37.54 12.24 15 0 6 -6.09 10.97 -15 0 -6 -2.68 11.43 15 0 6 5.41 4.03 15 0 7 3.04 6.94 15 0 7 1.76 3.06 -15 0 -7 -8.13 7.54 15 0 8 302.85 32.20 -15 0 -8 281.60 29.89 15 0 9 3.09 7.04 -15 0 -9 -2.76 7.28 15 0 10 18.79 12.37 -15 0 -10 22.53 9.82 -15 0 -11 -2.86 8.83 -15 0 -12 108.60 19.24 15 0 12 157.71 19.39 15 0 13 10.37 8.61 15 0 14 2.11 7.09 15 0 15 8.60 8.48 15 0 16 78.56 15.00 -15 -1 2 2.73 8.03 15 1 -2 7.82 8.39 -15 -1 1 129.89 20.59 15 1 3 122.43 20.46 15 1 4 -2.75 10.22 15 1 4 3.10 7.62 15 1 4 3.14 5.04 15 1 5 188.04 23.68 15 1 5 168.96 24.96 -15 -1 -5 201.42 23.83 15 1 5 123.10 15.37 15 1 6 2.70 9.36 15 1 6 12.24 9.85 -15 -1 -6 7.69 7.88 15 1 6 1.25 4.63 15 1 7 10.68 8.94 15 1 7 4.27 3.58 -15 -1 -7 5.15 7.18 15 1 7 3.06 9.43 -15 -1 -8 47.05 12.22 15 1 8 39.66 6.86 15 1 8 49.13 13.77 15 1 9 269.90 30.90 -15 -1 -9 338.65 32.13 15 1 10 -6.27 10.11 -15 -1 -10 -2.70 7.51 -15 -1 -11 -2.75 7.22 15 1 12 -1.90 6.37 -15 -1 -12 -5.64 9.09 15 1 13 123.23 16.67 -15 -1 -13 107.30 18.90 15 1 14 3.92 7.51 15 1 15 35.87 10.22 15 1 16 -4.05 10.30 -15 -2 1 17.85 9.49 -15 -2 0 134.10 20.46 15 2 3 2.83 9.49 15 2 4 167.90 22.96 15 2 4 155.36 23.32 15 2 4 143.36 17.24 15 2 5 2.76 11.20 15 2 5 3.07 7.00 -15 -2 -5 9.69 8.13 15 2 5 10.82 6.27 15 2 6 436.96 36.47 15 2 6 434.86 38.50 -15 -2 -6 347.80 32.63 15 2 6 357.19 25.84 15 2 7 35.20 12.64 15 2 7 32.05 7.52 -15 -2 -7 34.31 10.74 15 2 7 45.93 13.39 15 2 8 89.05 18.71 15 2 8 78.61 9.87 -15 -2 -8 94.49 17.06 15 2 9 3.10 8.16 -15 -2 -9 2.52 6.63 15 2 9 11.80 4.92 -15 -2 -10 156.53 21.96 15 2 10 214.86 24.54 15 2 10 138.41 23.18 -15 -2 -11 2.62 8.08 15 2 12 10.53 7.31 -15 -2 -12 18.90 8.71 15 2 13 8.87 7.74 -15 -2 -13 -2.78 8.56 15 2 14 124.66 16.51 -15 -2 -14 157.50 22.43 15 2 15 82.48 13.91 15 2 16 22.31 7.95 -15 -3 -1 141.20 20.02 15 3 3 161.34 22.75 15 3 4 31.32 13.26 15 3 4 21.76 10.47 15 3 4 34.26 9.67 15 3 5 306.45 30.70 15 3 5 289.70 32.39 15 3 5 255.41 22.92 15 3 6 13.88 10.94 15 3 6 -3.07 6.97 -15 -3 -6 6.89 7.39 15 3 6 1.53 5.12 15 3 7 478.03 38.65 -15 -3 -7 366.77 32.88 15 3 7 399.52 27.63 15 3 7 527.57 41.78 15 3 8 -3.07 7.56 15 3 8 2.50 3.85 -15 -3 -8 4.71 5.79 15 3 9 130.56 23.11 -15 -3 -9 124.40 18.48 15 3 9 165.40 14.53 15 3 10 -2.65 9.87 15 3 10 9.44 7.74 -15 -3 -10 7.33 6.42 15 3 10 7.59 4.58 -15 -3 -11 199.50 24.13 15 3 11 244.13 26.54 15 3 11 258.05 30.20 -15 -3 -12 23.18 10.48 15 3 12 41.75 10.08 -15 -3 -13 31.92 10.82 15 3 13 27.50 9.07 -15 -3 -14 24.74 10.56 15 3 14 19.71 7.82 -15 -3 -15 198.49 25.63 15 3 15 221.47 21.16 15 4 3 8.13 7.05 15 4 3 2.93 10.16 15 4 4 197.38 21.49 15 4 4 237.35 27.86 15 4 5 46.58 10.63 15 4 5 37.17 13.10 -15 -4 -6 19.42 8.76 15 4 6 16.61 8.34 15 4 6 12.27 11.05 15 4 6 36.67 12.58 -15 -4 -7 30.54 9.56 15 4 7 22.92 7.30 15 4 7 27.61 11.78 15 4 7 36.29 13.00 15 4 8 559.68 33.41 -15 -4 -8 498.61 38.45 15 4 9 34.21 12.01 -15 -4 -9 45.20 11.96 15 4 9 47.21 8.43 15 4 10 -10.76 10.89 15 4 10 -6.29 13.41 -15 -4 -10 2.31 6.79 15 4 10 9.18 4.89 15 4 11 18.61 10.22 15 4 11 28.69 12.24 -15 -4 -11 28.41 9.87 15 4 11 20.36 5.41 -15 -4 -12 249.70 26.41 15 4 12 229.37 20.40 15 4 12 207.88 25.21 -15 -4 -13 -5.07 7.82 15 4 13 -1.46 8.03 -15 -4 -14 102.52 18.30 15 4 14 106.14 13.90 -15 -4 -15 8.16 9.12 15 4 15 -2.97 5.36 15 5 3 2.13 6.58 15 5 4 22.33 9.46 15 5 4 14.64 10.56 15 5 5 162.17 19.62 15 5 5 174.27 23.76 15 5 6 37.49 9.49 15 5 6 51.65 14.92 -15 -5 -7 16.28 7.80 15 5 7 3.33 6.18 15 5 7 2.84 11.51 15 5 8 7.74 4.78 -15 -5 -8 2.08 6.96 15 5 9 351.46 35.06 -15 -5 -9 321.96 28.91 15 5 9 347.17 25.40 15 5 10 87.44 17.78 15 5 10 62.95 15.41 -15 -5 -10 75.98 14.06 15 5 10 75.31 10.73 15 5 11 40.47 13.31 15 5 11 44.61 14.84 -15 -5 -11 26.80 9.57 15 5 11 28.96 6.99 15 5 12 6.44 5.36 -15 -5 -12 6.94 7.13 15 5 12 17.65 5.72 15 5 12 5.33 10.52 -15 -5 -13 130.02 18.93 15 5 13 120.82 13.75 15 5 13 124.09 19.16 -15 -5 -14 105.14 17.57 15 5 14 92.98 12.27 -15 -5 -15 23.42 9.70 -15 -5 -16 2.70 7.95 15 6 3 166.05 20.79 15 6 4 29.94 10.37 15 6 5 111.20 16.32 15 6 5 89.08 18.15 15 6 6 62.99 12.16 15 6 6 58.15 15.15 15 6 6 37.90 12.24 15 6 7 191.84 20.15 -15 -6 -7 146.19 18.61 15 6 7 216.32 26.41 15 6 8 67.48 11.59 -15 -6 -8 51.81 11.18 -15 -6 -9 116.29 16.84 15 6 9 156.87 16.85 -15 -6 -10 214.73 23.32 15 6 10 265.06 21.62 15 6 10 247.10 27.95 15 6 11 103.38 11.85 -15 -6 -11 66.98 13.28 15 6 11 91.09 12.30 15 6 11 117.86 19.15 15 6 12 78.86 10.66 -15 -6 -12 93.39 15.07 15 6 12 88.69 11.46 15 6 12 51.62 14.09 15 6 13 8.04 8.97 -15 -6 -13 -2.28 5.57 15 6 13 -1.11 4.79 -15 -6 -14 68.73 14.30 -15 -6 -15 84.17 16.19 -15 -6 -16 -5.17 8.66 15 7 2 -2.44 7.18 15 7 3 44.65 12.45 15 7 4 190.90 22.36 15 7 5 121.88 17.24 15 7 5 88.77 17.67 15 7 6 12.16 7.05 15 7 6 3.06 10.24 15 7 7 32.65 8.81 15 7 7 29.12 12.74 15 7 7 30.55 11.75 15 7 8 316.04 33.33 15 7 8 320.38 26.39 15 7 9 112.30 14.90 -15 -7 -9 97.69 14.12 15 7 9 105.92 19.88 15 7 9 111.62 20.28 -15 -7 -10 39.36 9.93 15 7 10 37.51 8.65 15 7 10 25.50 10.92 15 7 11 53.63 8.40 -15 -7 -11 56.53 12.29 15 7 11 55.36 10.37 15 7 11 41.98 13.13 -15 -7 -12 70.80 12.94 15 7 12 94.39 12.42 15 7 12 93.92 17.28 -15 -7 -13 12.76 8.16 15 7 13 17.94 6.44 15 7 13 8.16 9.80 -15 -7 -14 102.81 16.20 -15 -7 -15 201.50 23.55 -15 -7 -16 191.91 23.22 15 8 2 101.93 17.26 15 8 3 36.78 10.76 15 8 4 119.70 17.93 15 8 5 166.41 21.05 15 8 6 -2.15 6.60 15 8 6 -9.13 9.38 15 8 7 -6.09 9.80 15 8 7 2.05 5.36 15 8 8 214.60 27.52 15 8 8 259.37 23.81 15 8 9 179.67 25.11 15 8 9 164.02 19.15 15 8 10 53.29 14.68 15 8 10 60.21 11.88 15 8 10 40.03 13.91 15 8 11 27.04 8.39 15 8 11 53.81 14.22 15 8 12 11.25 6.34 15 8 12 8.40 8.24 15 8 13 388.37 27.55 15 9 3 -2.55 7.85 15 9 4 7.36 6.03 15 9 5 37.71 11.23 15 9 6 88.02 15.42 15 9 7 124.36 20.92 15 9 7 159.99 19.47 15 9 8 -2.08 5.79 15 9 9 101.89 19.06 15 9 9 139.61 17.59 15 9 10 284.46 25.29 15 9 11 -1.84 5.10 15 9 12 10.53 5.66 15 9 13 11.85 5.90 15 9 14 141.15 16.77 15 10 5 19.68 8.27 15 10 6 7.10 6.61 15 10 7 155.16 20.04 15 10 8 26.39 10.04 15 10 9 19.11 8.16 15 10 10 81.64 13.42 15 10 11 106.34 15.41 15 10 12 1.90 4.97 15 10 13 1.84 4.83 15 10 14 21.45 8.83 15 11 6 9.91 6.52 15 11 7 4.79 6.31 15 11 8 37.14 10.86 15 11 9 33.66 11.10 15 11 10 15.18 7.00 15 11 11 69.32 12.56 15 11 12 150.43 18.84 15 11 13 9.87 6.61 15 11 14 53.99 11.75 15 12 8 7.31 6.42 15 12 9 229.65 24.67 15 12 10 2.29 7.98 15 12 11 8.91 6.87 15 12 12 17.29 8.30 15 12 13 477.92 35.37 15 12 14 148.50 18.67 15 12 15 36.57 10.06 15 13 10 550.21 40.34 15 13 11 -2.36 6.91 15 13 12 4.58 7.96 15 13 13 20.12 9.98 15 13 14 471.29 36.19 15 13 15 -2.16 5.69 16 -2 -1 102.06 17.99 16 -1 -1 31.42 11.05 16 -1 0 188.85 22.56 -16 1 -5 49.99 14.04 -16 1 -6 -2.94 13.41 16 -1 11 -2.24 8.06 16 -1 12 56.35 13.23 16 -1 13 38.68 12.03 -16 0 0 -5.88 9.48 -16 0 -5 317.98 32.28 -16 0 -6 8.47 9.82 -16 0 -7 48.42 13.07 -16 0 -8 112.06 19.99 -16 0 -9 401.97 36.89 16 0 12 2.11 6.81 16 0 13 125.84 18.35 16 0 14 58.28 13.15 16 1 4 169.80 18.19 -16 -1 -6 205.01 25.42 -16 -1 -7 -2.71 8.37 -16 -1 -8 8.24 10.21 -16 -1 -9 66.91 15.72 -16 -1 -10 214.76 26.49 16 1 12 35.46 10.42 16 1 13 -5.96 7.15 16 1 14 266.93 25.50 16 2 3 123.03 17.03 16 2 4 21.10 8.52 16 2 5 144.34 16.72 -16 -2 -6 2.57 5.83 16 2 6 1.45 5.98 -16 -2 -7 196.33 23.86 -16 -2 -8 23.53 10.34 -16 -2 -9 76.94 16.01 -16 -2 -10 10.79 7.95 -16 -2 -11 201.17 25.76 16 2 12 23.71 9.02 -16 -2 -12 36.58 12.58 16 2 13 98.99 14.74 16 3 3 14.03 7.46 16 3 4 231.08 23.00 16 3 5 -1.74 6.24 -16 -3 -6 60.57 14.27 16 3 6 80.73 12.81 -16 -3 -7 4.89 6.42 16 3 7 -1.43 5.79 -16 -3 -8 170.94 22.01 -16 -3 -9 2.52 7.02 -16 -3 -10 59.09 13.65 -16 -3 -11 28.83 11.20 16 3 12 120.74 15.91 -16 -3 -12 126.12 19.60 16 3 13 -1.67 6.44 -16 -3 -13 -5.51 8.48 16 4 3 27.48 9.48 16 4 4 27.89 9.85 16 4 5 206.21 21.62 16 4 6 42.99 9.83 -16 -4 -7 9.22 7.41 16 4 7 -1.58 7.04 16 4 8 33.24 8.47 -16 -4 -8 37.33 10.69 -16 -4 -9 163.82 20.87 -16 -4 -10 36.36 11.10 -16 -4 -11 -7.46 9.23 16 4 12 -4.55 6.31 -16 -4 -12 -2.55 5.80 -16 -4 -13 159.97 21.53 -16 -4 -14 -5.43 8.74 16 5 2 2.32 8.92 16 5 3 199.92 22.80 16 5 4 69.41 13.47 16 5 5 47.51 11.31 16 5 6 155.31 18.87 16 5 7 -1.72 5.30 16 5 8 12.77 6.48 16 5 9 22.05 7.26 -16 -5 -10 111.86 17.13 -16 -5 -11 44.48 11.60 -16 -5 -12 -4.81 8.37 -16 -5 -13 -2.49 8.63 -16 -5 -14 167.79 22.46 -16 -5 -15 10.71 7.88 16 6 3 48.89 13.08 16 6 4 48.64 13.26 16 6 5 64.93 13.67 16 6 6 75.05 13.73 16 6 7 101.85 15.41 16 6 8 52.20 10.74 16 6 9 73.17 11.96 16 6 10 39.17 8.61 16 7 3 2.42 6.78 16 7 4 192.43 23.34 16 7 5 85.99 15.47 16 7 6 66.94 12.81 16 7 7 3.97 6.11 16 7 8 28.15 8.78 16 7 9 164.65 18.07 16 7 10 422.63 30.20 16 7 11 34.26 8.76 16 8 4 -2.42 7.46 16 8 5 143.80 20.12 16 8 6 57.52 12.48 16 8 7 14.74 7.83 16 8 8 40.18 10.14 16 8 9 7.65 6.42 16 8 10 146.47 17.37 16 8 11 123.50 15.62 16 8 12 12.94 5.64 16 9 6 37.19 11.51 16 9 7 17.83 8.04 16 9 8 -4.27 5.95 16 9 9 38.86 9.78 16 9 10 37.06 10.17 16 9 11 68.78 12.56 16 9 12 58.48 11.10 16 9 13 3.38 5.22 16 10 7 14.07 7.56 16 10 8 117.44 17.39 16 10 9 6.52 6.70 16 10 10 -2.08 7.49 16 10 11 38.01 10.92 16 10 12 84.22 13.85 16 10 13 -1.84 5.14 16 11 9 362.65 31.77 16 11 10 4.42 11.99 16 11 11 -2.13 5.25 16 11 12 16.45 7.65 16 11 13 263.82 25.00 16 11 14 15.41 6.94 16 12 11 61.11 13.13 16 12 12 2.19 6.09 16 12 13 16.95 8.14 16 12 14 323.89 28.39 -17 -2 -8 84.43 16.46 17 4 3 23.97 8.86 17 5 4 -4.32 7.23 17 5 5 105.46 16.71 17 6 5 32.23 10.43 17 6 6 226.18 23.52 17 7 6 30.00 10.21 17 7 7 131.86 17.55 17 8 7 109.87 16.33 17 8 8 10.26 7.38 17 9 8 152.50 19.37 17 9 9 -8.30 6.97 17 10 10 29.53 9.65 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 10863 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.1037(3) 0.3365(3) 0.9034(3) 0.0177(8) Uani 1 1 d . . . . . C2 C 0.1949(4) 0.3237(3) 0.8204(3) 0.0275(10) Uani 1 1 d . . . . . H2A H 0.245334 0.272373 0.837028 0.041 Uiso 1 1 calc GR . . . . H2B H 0.240561 0.374049 0.788760 0.041 Uiso 1 1 calc GR . . . . H2C H 0.156364 0.316701 0.782880 0.041 Uiso 1 1 calc GR . . . . C3 C 0.2668(4) 0.6526(3) 0.6105(3) 0.0210(9) Uani 1 1 d . . . . . C1AA C 0.3220(4) 0.6865(4) 0.5103(3) 0.0327(11) Uani 1 1 d . . . . . H1AA H 0.378497 0.642712 0.491621 0.049 Uiso 1 1 calc GR . . . . H1AB H 0.360188 0.738886 0.494038 0.049 Uiso 1 1 calc GR . . . . H1AC H 0.262240 0.699295 0.481829 0.049 Uiso 1 1 calc GR . . . . C5 C 0.3766(4) 0.7486(3) 0.8787(3) 0.0231(9) Uani 1 1 d . . . . . C2AA C 0.4487(4) 0.8049(3) 0.8936(4) 0.0362(12) Uani 1 1 d . . . . . H2AA H 0.522925 0.774171 0.897081 0.054 Uiso 1 1 calc GR . . . . H2AB H 0.407269 0.816920 0.948170 0.054 Uiso 1 1 calc GR . . . . H2AC H 0.461308 0.859147 0.844972 0.054 Uiso 1 1 calc GR . . . . C7 C 0.7295(4) 0.9642(3) 0.5822(3) 0.0199(9) Uani 1 1 d . . . . . C0AA C 0.7639(4) 0.8952(3) 0.6604(3) 0.0334(11) Uani 1 1 d . . . . . H0AA H 0.838312 0.866093 0.638736 0.050 Uiso 1 1 calc GR . . . . H0AB H 0.705529 0.852996 0.692213 0.050 Uiso 1 1 calc GR . . . . H0AC H 0.769365 0.923007 0.699633 0.050 Uiso 1 1 calc GR . . . . C9 C 0.6710(4) 0.3315(3) 0.7474(3) 0.0254(10) Uani 1 1 d . . . . . C11 C 0.0522(4) 0.4728(3) 0.4830(3) 0.0266(10) Uani 1 1 d . . . . . C12 C 0.0774(4) 0.4587(3) 0.4018(3) 0.0283(10) Uani 1 1 d . . . . . H12A H 0.027527 0.484038 0.367066 0.034 Uiso 1 1 calc R . . . . C13 C 0.1759(4) 0.4073(3) 0.3729(3) 0.0258(10) Uani 1 1 d . . . . . C14 C 0.2540(4) 0.3693(3) 0.4201(3) 0.0262(10) Uani 1 1 d . . . . . H14 H 0.320131 0.335157 0.399618 0.031 Uiso 1 1 calc R . . . . C15 C 0.2296(4) 0.3844(3) 0.4997(3) 0.0254(9) Uani 1 1 d . . . . . C17 C 0.1298(4) 0.3697(3) 0.2612(3) 0.0304(11) Uani 1 1 d . . . . . H17 H 0.055383 0.351065 0.295869 0.037 Uiso 1 1 calc R . . . . C18 C 0.2883(5) 0.4061(4) 0.1478(4) 0.0475(14) Uani 1 1 d . . . . . H18A H 0.341527 0.415085 0.091153 0.057 Uiso 1 1 calc R . . . . C20 C 0.3560(4) 0.2619(3) 0.5709(3) 0.0291(10) Uani 1 1 d . . . . . H20A H 0.349690 0.219853 0.548217 0.035 Uiso 1 1 calc R . . . . N4 N 0.4152(4) 0.2519(3) 0.6281(3) 0.0487(12) Uani 1 1 d . . . . . H4A H 0.454512 0.205150 0.650691 0.058 Uiso 1 1 calc R . . . . C22 C 0.3372(4) 0.3859(3) 0.5976(3) 0.0297(10) Uani 1 1 d . . . . . H22 H 0.316151 0.443718 0.596323 0.036 Uiso 1 1 calc R . . . . C23 C 0.5618(4) 0.9849(3) -0.0001(3) 0.0257(10) Uani 1 1 d . . . . . C24 C 0.6483(4) 0.9720(3) -0.0755(3) 0.0286(10) Uani 1 1 d . . . . . H24 H 0.628371 0.980053 -0.126145 0.034 Uiso 1 1 calc R . . . . C25 C 0.7615(4) 0.9477(3) -0.0748(3) 0.0266(10) Uani 1 1 d . . . . . C26 C 0.7963(4) 0.9346(3) -0.0016(3) 0.0296(10) Uani 1 1 d . . . . . H26 H 0.874299 0.919971 -0.003099 0.036 Uiso 1 1 calc R . . . . C27 C 0.7111(4) 0.9440(3) 0.0740(3) 0.0262(10) Uani 1 1 d . . . . . C28 C 0.5947(4) 0.9672(3) 0.0759(3) 0.0296(10) Uani 1 1 d . . . . . H28 H 0.538249 0.970857 0.128290 0.036 Uiso 1 1 calc R . . . . C29 C 0.9045(6) 0.8574(3) -0.1549(3) 0.0487(15) Uani 1 1 d . . . . . H29A H 0.882233 0.803686 -0.111880 0.058 Uiso 1 1 calc R . . . . C30 C 0.9976(5) 0.9549(4) -0.2742(4) 0.0464(14) Uani 1 1 d . . . . . H30 H 1.051779 0.980550 -0.328827 0.056 Uiso 1 1 calc R . . . . C31 C 0.9104(5) 0.9968(3) -0.2270(3) 0.0426(13) Uani 1 1 d . . . . . H31 H 0.892699 1.057074 -0.242536 0.051 Uiso 1 1 calc R . . . . C32 C 0.8438(5) 0.8789(3) 0.1710(4) 0.0384(12) Uani 1 1 d . . . . . H32A H 0.898639 0.847138 0.137537 0.046 Uiso 1 1 calc R . . . . C33 C 0.8444(5) 0.8855(3) 0.2471(4) 0.0399(12) Uani 1 1 d . . . . . H33 H 0.899385 0.858291 0.277065 0.048 Uiso 1 1 calc R . . . . C34 C 0.6910(4) 0.9650(3) 0.2147(3) 0.0297(10) Uani 1 1 d . . . . . H34 H 0.623127 1.002263 0.217460 0.036 Uiso 1 1 calc R . . . . C19A C 0.3020(4) 0.4238(4) 0.2151(4) 0.0478(15) Uani 1 1 d . . . . . H19A H 0.365643 0.448255 0.213945 0.057 Uiso 1 1 calc R . . . . C10B C 0.7046(5) 0.3954(3) 0.6520(3) 0.0393(12) Uani 1 1 d . . . . . H10A H 0.690117 0.454525 0.653041 0.059 Uiso 1 1 calc GR . . . . H10B H 0.658542 0.386933 0.620190 0.059 Uiso 1 1 calc GR . . . . H10C H 0.786245 0.384769 0.622884 0.059 Uiso 1 1 calc GR . . . . C16C C 0.1312(4) 0.4345(3) 0.5313(3) 0.0287(10) Uani 1 1 d . . . . . H16C H 0.117624 0.442665 0.585442 0.034 Uiso 1 1 calc R . . . . La1 La 0.12762(2) 0.59492(2) 0.88464(2) 0.01554(7) Uani 1 1 d . . . . . La2 La 0.40614(2) 0.86303(2) 0.62015(2) 0.01728(7) Uani 1 1 d . . . . . Li1 Li 0.3758(6) 0.4973(5) 0.8705(5) 0.0275(16) Uani 1 1 d . . . . . N1 N 0.2019(3) 0.3980(2) 0.2867(2) 0.0240(8) Uani 1 1 d . . . . . N2 N 0.1814(3) 0.3723(3) 0.1784(3) 0.0318(9) Uani 1 1 d . . . . . H2D H 0.152350 0.355419 0.147941 0.038 Uiso 1 1 calc R . . . . N3 N 0.3068(3) 0.3462(2) 0.5528(2) 0.0241(8) Uani 1 1 d . . . . . C4 C 0.4013(3) 0.3294(3) 0.6435(3) 0.0168(8) Uani 1 1 d . . . . . H4B H 0.432823 0.340359 0.680961 0.020 Uiso 1 1 calc R . . . . N5 N 0.8522(3) 0.9347(2) -0.1519(2) 0.0259(8) Uani 1 1 d . . . . . N6 N 0.9924(4) 0.8686(3) -0.2277(3) 0.0407(11) Uani 1 1 d . . . . . H6 H 1.039477 0.827442 -0.243687 0.049 Uiso 1 1 calc R . . . . N7 N 0.7452(3) 0.9288(2) 0.1517(2) 0.0276(8) Uani 1 1 d . . . . . N8 N 0.7497(4) 0.9393(3) 0.2726(3) 0.0336(9) Uani 1 1 d . . . . . H8 H 0.731116 0.954184 0.319496 0.040 Uiso 1 1 calc R . . . . O1 O 0.0818(3) 0.50903(19) 0.80216(19) 0.0236(6) Uani 1 1 d . . . . . O2 O -0.0769(3) 0.4139(2) 0.8337(2) 0.0260(7) Uani 1 1 d . . . . . H2 H -0.114027 0.372273 0.870847 0.039 Uiso 1 1 calc R . . . . O3 O -0.0555(3) 0.45991(19) 0.95501(19) 0.0244(6) Uani 1 1 d . . . . . O4 O 0.0379(3) 0.25917(19) 0.9493(2) 0.0254(7) Uani 1 1 d . . . . . H4 H -0.011897 0.264404 0.994704 0.038 Uiso 1 1 calc R . . . . O5 O 0.2707(3) 0.27597(19) 0.9909(2) 0.0259(7) Uani 1 1 d . . . . . H5 H 0.317318 0.274957 0.942815 0.039 Uiso 1 1 calc R . . . . O6 O 0.0842(2) 0.34271(18) 1.06588(18) 0.0181(6) Uani 1 1 d . . . . . O7 O 0.2276(2) 0.44035(18) 0.92764(18) 0.0189(6) Uani 1 1 d . . . . . O8 O 0.3224(2) 0.5902(2) 0.76586(19) 0.0240(6) Uani 1 1 d . . . . . O9 O 0.4667(3) 0.5552(2) 0.6329(2) 0.0299(7) Uani 1 1 d . . . . . H9 H 0.432555 0.510634 0.648964 0.045 Uiso 1 1 calc R . . . . O10 O 0.4425(2) 0.70824(19) 0.6363(2) 0.0255(7) Uani 1 1 d . . . . . O11 O 0.2099(3) 0.5743(2) 0.6314(2) 0.0322(7) Uani 1 1 d . . . . . H11 H 0.179259 0.554355 0.685309 0.048 Uiso 1 1 calc R . . . . O12 O 0.0628(2) 0.7512(2) 0.59720(19) 0.0262(7) Uani 1 1 d . . . . . H12 H 0.093520 0.765113 0.543152 0.039 Uiso 1 1 calc R . . . . O13 O 0.0972(2) 0.70415(18) 0.74244(18) 0.0206(6) Uani 1 1 d . . . . . O14 O 0.2187(2) 0.82206(18) 0.61248(19) 0.0228(6) Uani 1 1 d . . . . . O15 O 0.3146(3) 0.58467(19) 0.9315(2) 0.0240(6) Uani 1 1 d . . . . . O16 O 0.4645(3) 0.6062(2) 0.9903(2) 0.0307(7) Uani 1 1 d . . . . . H16 H 0.488680 0.642172 1.002220 0.046 Uiso 1 1 calc R . . . . O17 O 0.2562(3) 0.6623(2) 1.04910(19) 0.0253(7) Uani 1 1 d . . . . . O18 O 0.4448(3) 0.7331(2) 0.7956(2) 0.0340(8) Uani 1 1 d . . . . . H18 H 0.408970 0.702855 0.784943 0.051 Uiso 1 1 calc R . . . . O19 O 0.1481(2) 0.73894(19) 0.89184(19) 0.0225(6) Uani 1 1 d . . . . . O20 O 0.1922(3) 0.8718(2) 0.9148(2) 0.0299(7) Uani 1 1 d . . . . . H20 H 0.175681 0.844225 0.968159 0.045 Uiso 1 1 calc R . . . . O21 O 0.2648(3) 0.8607(2) 0.76397(19) 0.0268(7) Uani 1 1 d . . . . . O22 O 0.6208(2) 0.85611(19) 0.5485(2) 0.0244(7) Uani 1 1 d . . . . . O23 O 0.8329(3) 0.8532(2) 0.4828(2) 0.0335(8) Uani 1 1 d . . . . . H23 H 0.890507 0.882302 0.458121 0.050 Uiso 1 1 calc R . . . . O24 O 0.7116(3) 0.98973(19) 0.4210(2) 0.0279(7) Uani 1 1 d . . . . . O25 O 0.8209(3) 1.0258(2) 0.5352(2) 0.0267(7) Uani 1 1 d . . . . . H25 H 0.804163 1.063807 0.492853 0.040 Uiso 1 1 calc R . . . . O26 O 0.5757(3) 1.1000(2) 0.5389(2) 0.0272(7) Uani 1 1 d . . . . . O27 O 0.5954(3) 1.0541(2) 0.6946(2) 0.0295(7) Uani 1 1 d . . . . . H27 H 0.652514 1.083035 0.675975 0.044 Uiso 1 1 calc R . . . . O28 O 0.4944(3) 0.9598(2) 0.6605(2) 0.0263(7) Uani 1 1 d . . . . . O29 O 0.6592(3) 0.1634(2) 0.8498(2) 0.0444(9) Uani 1 1 d . . . . . H29 H 0.703037 0.172931 0.872231 0.067 Uiso 1 1 calc R . . . . O30 O 0.6165(3) 0.2007(2) 0.7042(2) 0.0393(8) Uani 1 1 d . . . . . O31 O 0.8242(3) 0.1970(2) 0.7071(2) 0.0376(8) Uani 1 1 d . . . . . O32 O 0.7513(3) 0.3408(3) 0.7872(3) 0.0441(9) Uani 1 1 d . . . . . H32 H 0.736549 0.307281 0.838666 0.066 Uiso 1 1 calc R . . . . O33 O 0.4700(3) 0.2724(2) 0.8798(2) 0.0308(7) Uani 1 1 d . . . . . O34 O 0.5190(3) 0.4253(2) 0.8517(2) 0.0290(7) Uani 1 1 d . . . . . O35 O 0.4529(3) 0.3979(2) 0.7406(2) 0.0303(7) Uani 1 1 d . . . . . P1 P 0.00838(9) 0.43562(7) 0.87199(7) 0.0168(2) Uani 1 1 d . . . . . P2 P 0.17570(9) 0.35258(7) 0.97529(7) 0.0158(2) Uani 1 1 d . . . . . P3 P 0.15935(9) 0.73833(7) 0.64368(7) 0.0168(2) Uani 1 1 d . . . . . P4 P 0.37947(9) 0.62669(7) 0.66630(7) 0.0178(2) Uani 1 1 d . . . . . P5 P 0.23634(9) 0.80634(7) 0.86084(7) 0.0181(2) Uani 1 1 d . . . . . P6 P 0.34625(9) 0.64353(7) 0.96976(7) 0.0192(2) Uani 1 1 d . . . . . P7 P 0.71946(9) 0.91501(7) 0.50398(7) 0.0183(2) Uani 1 1 d . . . . . P8 P 0.58824(9) 1.02438(7) 0.61893(7) 0.0188(2) Uani 1 1 d . . . . . P9 P 0.51815(9) 0.35791(7) 0.80950(7) 0.0216(2) Uani 1 1 d . . . . . P10 P 0.69570(11) 0.21784(8) 0.74566(8) 0.0272(3) Uani 1 1 d . . . . . O36 O 0.0701(3) 0.8594(2) 0.4347(2) 0.0323(7) Uani 1 1 d . . . . . O37 O 0.1410(4) 0.8416(3) 0.0846(3) 0.0584(11) Uani 1 1 d . . . . . O38 O 0.0071(4) 0.7152(4) 0.2724(5) 0.100(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.019(2) 0.018(2) 0.016(2) -0.0054(16) -0.0031(16) -0.0061(16) C2 0.023(2) 0.040(3) 0.020(2) -0.017(2) -0.0003(18) -0.004(2) C3 0.022(2) 0.025(2) 0.017(2) -0.0083(17) -0.0021(17) -0.0078(17) C1AA 0.030(2) 0.054(3) 0.011(2) -0.012(2) 0.0006(19) -0.004(2) C5 0.020(2) 0.025(2) 0.022(2) -0.0081(18) -0.0025(18) -0.0069(17) C2AA 0.035(3) 0.032(3) 0.048(3) -0.010(2) -0.019(2) -0.012(2) C7 0.018(2) 0.023(2) 0.021(2) -0.0082(18) -0.0067(17) -0.0037(17) C0AA 0.039(3) 0.033(3) 0.033(3) -0.010(2) -0.019(2) 0.001(2) C9 0.021(2) 0.031(2) 0.029(2) -0.015(2) -0.0059(19) -0.0057(18) C11 0.023(2) 0.034(3) 0.024(2) -0.011(2) -0.0069(19) -0.0025(19) C12 0.022(2) 0.039(3) 0.029(2) -0.016(2) -0.0104(19) 0.0030(19) C13 0.024(2) 0.036(3) 0.024(2) -0.018(2) -0.0042(19) -0.0051(19) C14 0.025(2) 0.028(2) 0.029(2) -0.014(2) -0.0104(19) 0.0019(18) C15 0.024(2) 0.033(2) 0.024(2) -0.0115(19) -0.0104(19) -0.0039(19) C17 0.028(2) 0.041(3) 0.025(2) -0.011(2) -0.005(2) -0.014(2) C18 0.035(3) 0.077(4) 0.033(3) -0.030(3) 0.003(2) -0.012(3) C20 0.032(2) 0.028(2) 0.038(3) -0.017(2) -0.019(2) 0.004(2) N4 0.043(3) 0.053(3) 0.049(3) -0.014(2) -0.018(2) 0.001(2) C22 0.030(2) 0.033(3) 0.031(3) -0.017(2) -0.007(2) -0.003(2) C23 0.026(2) 0.023(2) 0.025(2) -0.0082(19) -0.0024(19) -0.0062(18) C24 0.031(2) 0.029(2) 0.023(2) -0.0087(19) -0.004(2) -0.0031(19) C25 0.025(2) 0.027(2) 0.021(2) -0.0083(19) 0.0024(18) -0.0014(18) C26 0.024(2) 0.035(3) 0.029(3) -0.014(2) -0.005(2) 0.0015(19) C27 0.030(2) 0.026(2) 0.023(2) -0.0114(19) -0.0046(19) -0.0031(19) C28 0.026(2) 0.037(3) 0.024(2) -0.013(2) -0.0003(19) -0.004(2) C29 0.072(4) 0.025(3) 0.026(3) -0.003(2) 0.001(3) 0.009(3) C30 0.042(3) 0.053(4) 0.032(3) -0.015(3) 0.009(2) -0.009(3) C31 0.050(3) 0.026(3) 0.032(3) -0.005(2) 0.006(2) -0.002(2) C32 0.036(3) 0.043(3) 0.043(3) -0.024(3) -0.014(2) 0.007(2) C33 0.044(3) 0.040(3) 0.047(3) -0.024(3) -0.022(3) 0.008(2) C34 0.034(3) 0.024(2) 0.028(2) -0.011(2) -0.003(2) -0.003(2) C19A 0.025(3) 0.083(4) 0.040(3) -0.029(3) 0.003(2) -0.019(3) C10B 0.041(3) 0.031(3) 0.038(3) -0.009(2) -0.002(2) -0.009(2) C16C 0.028(2) 0.038(3) 0.024(2) -0.015(2) -0.011(2) 0.003(2) La1 0.01661(12) 0.01570(12) 0.01307(12) -0.00449(9) -0.00281(9) -0.00208(9) La2 0.01630(12) 0.01700(13) 0.01806(13) -0.00596(10) -0.00237(9) -0.00514(9) Li1 0.025(4) 0.025(4) 0.034(4) -0.011(3) -0.011(3) -0.001(3) N1 0.0202(18) 0.036(2) 0.0209(19) -0.0152(16) -0.0058(15) -0.0022(16) N2 0.029(2) 0.045(2) 0.031(2) -0.0207(19) -0.0112(18) -0.0045(18) N3 0.0254(19) 0.027(2) 0.0243(19) -0.0127(16) -0.0101(16) 0.0005(15) C4 0.0149(19) 0.028(2) 0.0150(19) -0.0125(17) -0.0084(16) 0.0005(16) N5 0.028(2) 0.0218(19) 0.0205(19) -0.0055(15) -0.0013(16) 0.0009(15) N6 0.045(3) 0.041(3) 0.030(2) -0.017(2) -0.011(2) 0.021(2) N7 0.028(2) 0.029(2) 0.026(2) -0.0136(17) -0.0041(17) -0.0016(16) N8 0.049(3) 0.028(2) 0.029(2) -0.0150(17) -0.0114(19) -0.0008(18) O1 0.0259(16) 0.0241(16) 0.0191(15) -0.0002(12) -0.0066(13) -0.0125(13) O2 0.0254(16) 0.0329(17) 0.0247(16) -0.0096(14) -0.0079(13) -0.0124(13) O3 0.0318(17) 0.0242(16) 0.0153(15) -0.0092(12) -0.0047(13) 0.0033(13) O4 0.0283(16) 0.0197(15) 0.0253(16) -0.0070(13) -0.0004(13) -0.0111(13) O5 0.0198(15) 0.0258(16) 0.0220(16) -0.0031(13) -0.0009(12) 0.0009(12) O6 0.0168(14) 0.0217(15) 0.0161(14) -0.0084(12) -0.0028(11) -0.0017(11) O7 0.0167(14) 0.0199(15) 0.0193(14) -0.0062(12) -0.0033(12) -0.0040(11) O8 0.0218(15) 0.0295(17) 0.0170(15) -0.0073(13) -0.0020(12) -0.0016(13) O9 0.0295(17) 0.0217(16) 0.0289(17) -0.0093(13) 0.0023(14) 0.0010(13) O10 0.0201(15) 0.0206(15) 0.0357(18) -0.0077(13) -0.0083(13) -0.0045(12) O11 0.0397(19) 0.0288(17) 0.0323(18) -0.0151(14) -0.0047(15) -0.0140(15) O12 0.0200(15) 0.0403(18) 0.0176(15) -0.0037(13) -0.0065(12) -0.0110(13) O13 0.0195(14) 0.0241(15) 0.0145(14) -0.0061(12) -0.0019(12) 0.0003(12) O14 0.0205(15) 0.0197(15) 0.0263(16) -0.0013(12) -0.0087(13) -0.0065(12) O15 0.0263(16) 0.0233(16) 0.0269(16) -0.0109(13) -0.0103(13) -0.0022(12) O16 0.0240(16) 0.0411(19) 0.0316(18) -0.0147(15) -0.0129(14) 0.0015(14) O17 0.0244(16) 0.0296(17) 0.0210(15) -0.0096(13) -0.0027(13) -0.0053(13) O18 0.0266(17) 0.042(2) 0.0286(18) -0.0156(15) 0.0039(14) -0.0056(15) O19 0.0196(15) 0.0241(16) 0.0238(16) -0.0054(13) -0.0060(12) -0.0072(12) O20 0.0414(19) 0.0242(16) 0.0237(16) -0.0111(13) -0.0036(14) -0.0072(14) O21 0.0286(16) 0.0285(17) 0.0167(15) -0.0021(13) -0.0021(13) -0.0073(13) O22 0.0194(15) 0.0257(16) 0.0314(17) -0.0162(14) -0.0021(13) -0.0063(12) O23 0.0198(16) 0.0311(18) 0.053(2) -0.0226(16) -0.0061(15) 0.0003(13) O24 0.0413(19) 0.0197(16) 0.0232(16) -0.0084(13) -0.0111(14) 0.0020(13) O25 0.0213(15) 0.0293(17) 0.0313(17) -0.0074(14) -0.0077(13) -0.0119(13) O26 0.0291(17) 0.0275(17) 0.0223(16) -0.0096(13) -0.0061(13) 0.0040(13) O27 0.0384(18) 0.0320(18) 0.0231(16) -0.0120(14) -0.0077(14) -0.0114(14) O28 0.0218(15) 0.0285(17) 0.0304(17) -0.0170(14) 0.0032(13) -0.0126(13) O29 0.051(2) 0.036(2) 0.038(2) -0.0024(16) -0.0172(18) 0.0006(17) O30 0.042(2) 0.036(2) 0.053(2) -0.0233(17) -0.0200(18) -0.0040(16) O31 0.0316(18) 0.039(2) 0.047(2) -0.0252(17) -0.0089(16) 0.0055(15) O32 0.0261(18) 0.069(3) 0.053(2) -0.037(2) -0.0111(17) -0.0039(17) O33 0.0243(16) 0.0256(17) 0.0325(18) -0.0063(14) -0.0015(14) 0.0006(13) O34 0.0259(16) 0.0344(18) 0.0338(18) -0.0167(15) -0.0128(14) -0.0001(14) O35 0.0381(18) 0.0255(17) 0.0354(18) -0.0127(14) -0.0198(15) 0.0018(14) P1 0.0192(5) 0.0176(5) 0.0141(5) -0.0049(4) -0.0038(4) -0.0058(4) P2 0.0155(5) 0.0157(5) 0.0148(5) -0.0043(4) -0.0026(4) -0.0034(4) P3 0.0168(5) 0.0197(5) 0.0135(5) -0.0044(4) -0.0034(4) -0.0045(4) P4 0.0173(5) 0.0171(5) 0.0171(5) -0.0064(4) -0.0015(4) -0.0027(4) P5 0.0204(5) 0.0178(5) 0.0155(5) -0.0050(4) -0.0029(4) -0.0059(4) P6 0.0185(5) 0.0213(5) 0.0195(5) -0.0070(4) -0.0068(4) -0.0033(4) P7 0.0169(5) 0.0183(5) 0.0213(5) -0.0094(4) -0.0041(4) -0.0022(4) P8 0.0197(5) 0.0208(5) 0.0179(5) -0.0089(4) -0.0033(4) -0.0053(4) P9 0.0196(5) 0.0238(6) 0.0232(6) -0.0091(5) -0.0070(5) -0.0017(4) P10 0.0285(6) 0.0239(6) 0.0314(6) -0.0117(5) -0.0100(5) -0.0001(5) O36 0.0296(17) 0.0382(19) 0.0288(17) -0.0073(15) -0.0089(14) -0.0091(14) O37 0.066(3) 0.068(3) 0.037(2) -0.016(2) -0.018(2) 0.006(2) O38 0.046(3) 0.112(5) 0.179(6) -0.097(5) -0.040(4) 0.019(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' La La -0.2871 2.4523 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 P1 109.6(3) . . ? C2 C1 P2 110.2(3) . . ? O4 C1 C2 107.6(3) . . ? O4 C1 P1 111.5(3) . . ? O4 C1 P2 110.6(3) . . ? P1 C1 P2 107.4(2) . . ? C1AA C3 P3 108.2(3) . . ? C1AA C3 P4 110.3(3) . . ? O11 C3 C1AA 107.3(3) . . ? O11 C3 P3 110.9(3) . . ? O11 C3 P4 110.1(3) . . ? P4 C3 P3 110.1(2) . . ? C2AA C5 P5 112.9(3) . . ? C2AA C5 P6 112.5(3) . . ? O18 C5 C2AA 106.2(4) . . ? O18 C5 P5 105.4(3) . . ? O18 C5 P6 110.1(3) . . ? P6 C5 P5 109.4(2) . . ? C0AA C7 P7 111.5(3) . . ? C0AA C7 P8 112.0(3) . . ? O25 C7 C0AA 107.7(3) . . ? O25 C7 P7 108.1(3) . . ? O25 C7 P8 109.1(3) . . ? P7 C7 P8 108.5(2) . . ? C10B C9 P9 110.6(3) . . ? C10B C9 P10 109.6(3) . . ? O32 C9 C10B 106.3(4) . . ? O32 C9 P9 110.8(3) . . ? O32 C9 P10 106.5(3) . . ? P10 C9 P9 112.7(2) . . ? C12 C11 C11 122.6(5) . 2_566 ? C16C C11 C11 120.2(5) . 2_566 ? C16C C11 C12 117.2(4) . . ? C13 C12 C11 120.4(4) . . ? C12 C13 N1 118.6(4) . . ? C14 C13 C12 122.7(4) . . ? C14 C13 N1 118.5(4) . . ? C13 C14 C15 116.7(4) . . ? C14 C15 N3 119.7(4) . . ? C16C C15 C14 122.3(4) . . ? C16C C15 N3 118.0(4) . . ? N2 C17 N1 108.2(4) . . ? C19A C18 N2 107.1(5) . . ? N4 C20 N3 106.3(4) . . ? C20 N4 C4 107.4(4) . . ? C4 C22 N3 108.1(4) . . ? C24 C23 C23 121.6(5) . 2_675 ? C28 C23 C23 120.8(5) . 2_675 ? C28 C23 C24 117.6(4) . . ? C25 C24 C23 120.3(4) . . ? C24 C25 C26 122.5(4) . . ? C24 C25 N5 121.3(4) . . ? C26 C25 N5 116.2(4) . . ? C27 C26 C25 117.5(4) . . ? C26 C27 C28 121.2(4) . . ? C26 C27 N7 118.4(4) . . ? C28 C27 N7 120.4(4) . . ? C27 C28 C23 120.6(4) . . ? N6 C29 N5 109.0(5) . . ? C31 C30 N6 107.1(5) . . ? C30 C31 N5 107.2(5) . . ? C33 C32 N7 106.7(4) . . ? C32 C33 N8 107.3(5) . . ? N8 C34 N7 108.3(4) . . ? C18 C19A N1 106.0(5) . . ? C15 C16C C11 120.7(4) . . ? O1 La1 O6 94.06(9) . 2_567 ? O1 La1 O7 72.10(9) . . ? O1 La1 O15 130.14(9) . . ? O3 La1 O1 116.57(10) 2_567 . ? O3 La1 O6 71.67(9) 2_567 2_567 ? O3 La1 O7 75.30(9) 2_567 . ? O3 La1 O8 136.51(10) 2_567 . ? O3 La1 O13 147.06(9) 2_567 . ? O3 La1 O15 76.89(10) 2_567 . ? O3 La1 O19 89.35(10) 2_567 . ? O6 La1 O7 133.07(9) 2_567 . ? O6 La1 O15 134.14(9) 2_567 . ? O7 La1 O15 65.47(9) . . ? O8 La1 O1 78.49(9) . . ? O8 La1 O6 151.24(9) . 2_567 ? O8 La1 O7 71.35(9) . . ? O8 La1 O15 64.32(9) . . ? O13 La1 O1 72.56(9) . . ? O13 La1 O6 76.25(9) . 2_567 ? O13 La1 O7 134.96(9) . . ? O13 La1 O8 75.01(9) . . ? O13 La1 O15 123.24(9) . . ? O19 La1 O1 148.23(9) . . ? O19 La1 O6 76.16(9) . 2_567 ? O19 La1 O7 135.91(9) . . ? O19 La1 O8 95.56(10) . . ? O19 La1 O13 75.76(9) . . ? O19 La1 O15 70.89(9) . . ? O10 La2 O14 75.86(9) . . ? O10 La2 O21 102.13(10) . . ? O10 La2 O22 80.03(10) . . ? O10 La2 O24 151.16(10) . 2_676 ? O10 La2 O26 90.55(10) . 2_676 ? O10 La2 O28 132.24(10) . . ? O14 La2 O24 76.19(10) . 2_676 ? O21 La2 O14 76.85(10) . . ? O21 La2 O22 139.49(10) . . ? O21 La2 O24 78.16(10) . 2_676 ? O21 La2 O26 142.57(10) . 2_676 ? O21 La2 O28 79.03(10) . . ? O22 La2 O14 140.42(9) . . ? O22 La2 O24 118.72(10) . 2_676 ? O22 La2 O26 77.03(10) . 2_676 ? O26 La2 O14 72.35(10) 2_676 . ? O26 La2 O24 74.30(9) 2_676 2_676 ? O28 La2 O14 146.57(10) . . ? O28 La2 O22 70.96(9) . . ? O28 La2 O24 76.47(10) . 2_676 ? O28 La2 O26 117.58(10) . 2_676 ? O7 Li1 O8 94.6(3) . . ? O7 Li1 O15 91.4(3) . . ? O15 Li1 O8 85.5(3) . . ? O34 Li1 O7 118.5(4) . . ? O34 Li1 O8 122.5(4) . . ? O34 Li1 O15 133.8(4) . . ? C17 N1 C13 125.1(4) . . ? C17 N1 C19A 108.9(4) . . ? C19A N1 C13 125.8(4) . . ? C17 N2 C18 109.7(4) . . ? C20 N3 C15 126.1(4) . . ? C22 N3 C15 125.2(4) . . ? C22 N3 C20 108.6(4) . . ? C22 C4 N4 109.6(4) . . ? C29 N5 C25 123.6(4) . . ? C29 N5 C31 107.7(4) . . ? C31 N5 C25 128.1(4) . . ? C29 N6 C30 109.0(4) . . ? C32 N7 C27 126.5(4) . . ? C34 N7 C27 125.3(4) . . ? C34 N7 C32 108.1(4) . . ? C34 N8 C33 109.6(4) . . ? P1 O1 La1 106.88(15) . . ? P1 O3 La1 145.05(18) . 2_567 ? P2 O6 La1 133.58(15) . 2_567 ? Li1 O7 La1 86.3(2) . . ? P2 O7 La1 130.31(15) . . ? P2 O7 Li1 143.4(3) . . ? Li1 O8 La1 84.4(2) . . ? P4 O8 La1 141.17(17) . . ? P4 O8 Li1 134.2(3) . . ? P4 O10 La2 141.59(17) . . ? P3 O13 La1 141.01(16) . . ? P3 O14 La2 135.35(16) . . ? Li1 O15 La1 84.5(2) . . ? P6 O15 La1 129.14(16) . . ? P6 O15 Li1 144.9(3) . . ? P5 O19 La1 141.95(17) . . ? P5 O21 La2 140.49(19) . . ? P7 O22 La2 139.67(17) . . ? P7 O24 La2 138.11(18) . 2_676 ? P8 O26 La2 142.03(18) . 2_676 ? P8 O28 La2 139.94(17) . . ? P9 O34 Li1 113.4(3) . . ? O1 P1 C1 109.70(18) . . ? O1 P1 O2 109.79(17) . . ? O1 P1 O3 110.10(17) . . ? O2 P1 C1 107.81(18) . . ? O3 P1 C1 107.15(17) . . ? O3 P1 O2 112.20(17) . . ? O5 P2 C1 108.14(18) . . ? O6 P2 C1 107.40(17) . . ? O6 P2 O5 106.22(16) . . ? O7 P2 C1 106.97(17) . . ? O7 P2 O5 112.24(16) . . ? O7 P2 O6 115.58(16) . . ? O12 P3 C3 105.93(18) . . ? O13 P3 C3 109.32(18) . . ? O13 P3 O12 105.58(16) . . ? O14 P3 C3 109.74(18) . . ? O14 P3 O12 110.78(16) . . ? O14 P3 O13 115.05(17) . . ? O8 P4 C3 109.03(18) . . ? O8 P4 O9 109.85(17) . . ? O9 P4 C3 106.17(19) . . ? O10 P4 C3 107.85(18) . . ? O10 P4 O8 114.42(18) . . ? O10 P4 O9 109.18(18) . . ? O19 P5 C5 108.69(18) . . ? O19 P5 O20 110.86(17) . . ? O20 P5 C5 108.72(19) . . ? O21 P5 C5 106.54(19) . . ? O21 P5 O19 114.98(17) . . ? O21 P5 O20 106.83(18) . . ? O15 P6 C5 105.47(18) . . ? O15 P6 O16 108.74(18) . . ? O16 P6 C5 106.17(19) . . ? O17 P6 C5 107.83(19) . . ? O17 P6 O15 117.62(17) . . ? O17 P6 O16 110.33(18) . . ? O22 P7 C7 109.31(18) . . ? O22 P7 O23 105.22(17) . . ? O22 P7 O24 116.12(18) . . ? O23 P7 C7 108.56(19) . . ? O24 P7 C7 106.74(18) . . ? O24 P7 O23 110.73(19) . . ? O26 P8 C7 106.56(18) . . ? O26 P8 O27 112.87(18) . . ? O26 P8 O28 115.78(19) . . ? O27 P8 C7 106.46(18) . . ? O28 P8 C7 107.48(18) . . ? O28 P8 O27 107.20(17) . . ? O33 P9 C9 107.32(19) . . ? O34 P9 C9 108.71(18) . . ? O34 P9 O33 111.67(19) . . ? O35 P9 C9 106.0(2) . . ? O35 P9 O33 113.05(19) . . ? O35 P9 O34 109.82(18) . . ? O29 P10 C9 101.3(2) . . ? O30 P10 C9 111.3(2) . . ? O30 P10 O29 109.8(2) . . ? O30 P10 O31 116.1(2) . . ? O31 P10 C9 109.6(2) . . ? O31 P10 O29 107.5(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.518(6) . ? C1 O4 1.446(5) . ? C1 P1 1.835(4) . ? C1 P2 1.843(4) . ? C3 C1AA 1.517(6) . ? C3 O11 1.448(5) . ? C3 P3 1.841(4) . ? C3 P4 1.832(4) . ? C5 C2AA 1.526(6) . ? C5 O18 1.453(5) . ? C5 P5 1.859(4) . ? C5 P6 1.841(4) . ? C7 C0AA 1.526(6) . ? C7 O25 1.455(5) . ? C7 P7 1.834(4) . ? C7 P8 1.844(4) . ? C9 C10B 1.531(7) . ? C9 O32 1.425(5) . ? C9 P9 1.853(4) . ? C9 P10 1.845(5) . ? C11 C11 1.480(9) 2_566 ? C11 C12 1.399(6) . ? C11 C16C 1.393(6) . ? C12 C13 1.382(6) . ? C13 C14 1.370(6) . ? C13 N1 1.444(5) . ? C14 C15 1.382(6) . ? C15 C16C 1.381(6) . ? C15 N3 1.430(6) . ? C17 N1 1.322(6) . ? C17 N2 1.311(6) . ? C18 C19A 1.347(8) . ? C18 N2 1.366(7) . ? C20 N4 1.349(6) . ? C20 N3 1.371(6) . ? N4 C4 1.360(6) . ? C22 N3 1.339(6) . ? C22 C4 1.304(6) . ? C23 C23 1.496(9) 2_675 ? C23 C24 1.403(6) . ? C23 C28 1.395(6) . ? C24 C25 1.366(6) . ? C25 C26 1.381(7) . ? C25 N5 1.445(6) . ? C26 C27 1.381(6) . ? C27 C28 1.391(6) . ? C27 N7 1.439(6) . ? C29 N5 1.321(6) . ? C29 N6 1.302(7) . ? C30 C31 1.334(7) . ? C30 N6 1.348(7) . ? C31 N5 1.362(6) . ? C32 C33 1.337(7) . ? C32 N7 1.390(6) . ? C33 N8 1.361(6) . ? C34 N7 1.328(6) . ? C34 N8 1.314(6) . ? C19A N1 1.389(6) . ? La1 O1 2.560(3) . ? La1 O3 2.412(3) 2_567 ? La1 O6 2.560(3) 2_567 ? La1 O7 2.562(3) . ? La1 O8 2.534(3) . ? La1 O13 2.524(3) . ? La1 O15 2.623(3) . ? La1 O19 2.477(3) . ? La2 O10 2.427(3) . ? La2 O14 2.559(3) . ? La2 O21 2.440(3) . ? La2 O22 2.473(3) . ? La2 O24 2.560(3) 2_676 ? La2 O26 2.476(3) 2_676 ? La2 O28 2.473(3) . ? Li1 O7 1.957(8) . ? Li1 O8 2.085(8) . ? Li1 O15 1.960(8) . ? Li1 O34 1.914(8) . ? O1 P1 1.510(3) . ? O2 P1 1.553(3) . ? O3 P1 1.511(3) . ? O5 P2 1.555(3) . ? O6 P2 1.525(3) . ? O7 P2 1.505(3) . ? O8 P4 1.514(3) . ? O9 P4 1.560(3) . ? O10 P4 1.503(3) . ? O12 P3 1.576(3) . ? O13 P3 1.511(3) . ? O14 P3 1.507(3) . ? O15 P6 1.510(3) . ? O16 P6 1.562(3) . ? O17 P6 1.504(3) . ? O19 P5 1.512(3) . ? O20 P5 1.563(3) . ? O21 P5 1.504(3) . ? O22 P7 1.492(3) . ? O23 P7 1.572(3) . ? O24 P7 1.510(3) . ? O26 P8 1.498(3) . ? O27 P8 1.565(3) . ? O28 P8 1.510(3) . ? O29 P10 1.600(4) . ? O30 P10 1.493(3) . ? O31 P10 1.501(3) . ? O33 P9 1.528(3) . ? O34 P9 1.527(3) . ? O35 P9 1.522(3) . ?