#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:41:39 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296393 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572740.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572740 loop_ _publ_author_name 'Valdés, Hugo' 'Alpuente, Nora' 'Salvador, Pedro' 'Hashmi, A Stephen K' 'Ribas, Xavi' _publ_section_title ; CCC-NHC Au(iii) pincer complexes as a reliable platform for isolating elusive species. ; _journal_issue 42 _journal_name_full 'Chemical science' _journal_page_first 17618 _journal_page_last 17628 _journal_paper_doi 10.1039/d4sc02999b _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C30 H33 Au Cl N4, B F4, C H2 Cl2' _chemical_formula_sum 'C31 H35 Au B Cl3 F4 N4' _chemical_formula_weight 853.75 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_update_record ; 2024-02-20 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 86.0800(10) _cell_angle_beta 89.9980(10) _cell_angle_gamma 69.3010(10) _cell_formula_units_Z 2 _cell_length_a 10.0080(4) _cell_length_b 10.3247(4) _cell_length_c 16.4908(6) _cell_measurement_reflns_used 9982 _cell_measurement_temperature 100.(2) _cell_measurement_theta_max 27.3560 _cell_measurement_theta_min 2.7794 _cell_volume 1589.73(11) _computing_cell_refinement 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_data_collection 'Bruker Instrument Service vV6.2.9' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 882)' _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100.(2) _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.992 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'D8 QUEST ECO' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator 'doubly curved silicon crystal Bruker Triumph' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0759 _diffrn_reflns_av_unetI/netI 0.0331 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 97134 _diffrn_reflns_theta_full 27.62 _diffrn_reflns_theta_max 27.62 _diffrn_reflns_theta_min 3.14 _diffrn_source_type 'Ceramic x-ray tube' _exptl_absorpt_coefficient_mu 4.932 _exptl_absorpt_correction_T_max 0.69 _exptl_absorpt_correction_T_min 0.57 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.784 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 840 _exptl_crystal_size_max 0.140 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.080 _refine_diff_density_max 4.965 _refine_diff_density_min -1.574 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.172 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 407 _refine_ls_number_reflns 7327 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.172 _refine_ls_R_factor_all 0.0520 _refine_ls_R_factor_gt 0.0331 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0223P)^2^+8.3902P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0689 _refine_ls_wR_factor_ref 0.0818 _reflns_number_gt 6249 _reflns_number_total 7327 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc02999b3.cif _cod_data_source_block HV2_23R _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'Multi-Scan' was changed to 'multi-scan' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas Adding full bibliography for 1572736--1572746.cif. ; _cod_database_code 1572740 _shelx_res_file ; TITL HV2_23R_0m_a.res in P-1 HV2_23R_0m_a.res created by SHELXL-2017/1 at 13:40:50 on 17-Mar-2022 REM Old TITL HV2_23R_0m in P-1 REM SHELXT solution in P-1 REM R1 0.081, Rweak 0.004, Alpha 0.070, Orientation as input REM Formula found by SHELXT: C35 Au Cl3 N5 CELL 0.71073 10.0080 10.3247 16.4908 86.080 89.998 69.301 ZERR 2.000 0.0004 0.0004 0.0006 0.001 0.001 0.001 LATT 1 SFAC C H AU CL N O B F UNIT 62 70 2 6 8 0 2 8 TEMP -173.180 SIZE 0.08 0.10 0.14 L.S. 10 BOND $H conf acta LIST 6 FMAP 2 eadp c35' c35 eadp c36' c36 PLAN 20 OMIT -1 -1 1 OMIT 1 1 1 OMIT 0 -1 1 OMIT 1 0 1 OMIT -1 0 1 WGHT 0.022300 8.390202 FVAR 0.34975 0.65525 AU1 3 0.576000 0.161336 0.276272 11.00000 0.01655 0.01732 = 0.01760 -0.00299 0.00095 -0.00692 CL2 4 0.783633 0.218456 0.275782 11.00000 0.01659 0.02532 = 0.02222 -0.00492 0.00106 -0.01082 N4 5 0.668152 0.094254 0.099754 11.00000 0.01691 0.01651 = 0.01673 -0.00130 0.00221 -0.00645 N11 5 0.608020 -0.063623 0.168677 11.00000 0.01814 0.01354 = 0.01585 -0.00174 0.00196 -0.00749 N20 5 0.363584 0.338475 0.383457 11.00000 0.01889 0.01721 = 0.02142 -0.00658 0.00429 -0.00696 N22 5 0.564630 0.255188 0.452034 11.00000 0.02267 0.02911 = 0.01911 -0.00580 0.00249 -0.01420 C3 1 0.625243 0.059910 0.172226 11.00000 0.01325 0.01338 = 0.01799 -0.00079 -0.00110 -0.00068 C5 1 0.679838 -0.009724 0.047653 11.00000 0.01190 0.01528 = 0.01671 -0.00210 -0.00169 -0.00285 C6 1 0.717717 -0.022162 -0.033845 11.00000 0.01707 0.01985 = 0.02050 -0.00169 0.00053 -0.00377 AFIX 43 H6 2 0.742037 0.047284 -0.064486 11.00000 -1.20000 AFIX 0 C7 1 0.717715 -0.141540 -0.067273 11.00000 0.02092 0.02402 = 0.01648 -0.00409 -0.00184 -0.00361 AFIX 43 H7 2 0.744538 -0.154970 -0.122197 11.00000 -1.20000 AFIX 0 C8 1 0.679545 -0.243187 -0.022933 11.00000 0.02188 0.01791 = 0.02311 -0.00552 -0.00321 -0.00368 AFIX 43 H8 2 0.680076 -0.322884 -0.048708 11.00000 -1.20000 AFIX 0 C9 1 0.640941 -0.230284 0.057799 11.00000 0.01534 0.01968 = 0.02027 -0.00318 0.00006 -0.00363 AFIX 43 H9 2 0.615485 -0.299107 0.088338 11.00000 -1.20000 AFIX 0 C10 1 0.641780 -0.110678 0.091232 11.00000 0.01099 0.01872 = 0.01808 -0.00234 0.00004 -0.00168 C12 1 0.546667 -0.125364 0.234374 11.00000 0.02221 0.01809 = 0.01643 -0.00059 0.00358 -0.00913 AFIX 23 H12A 2 0.613480 -0.154215 0.282007 11.00000 -1.20000 H12B 2 0.531695 -0.208811 0.216288 11.00000 -1.20000 AFIX 0 C13 1 0.405859 -0.021280 0.258038 11.00000 0.01540 0.01731 = 0.01437 0.00027 -0.00142 -0.00664 C14 1 0.394198 0.109756 0.277198 11.00000 0.01929 0.01479 = 0.00438 0.00023 -0.00058 -0.00565 C15 1 0.266770 0.209219 0.296119 11.00000 0.01758 0.01759 = 0.01703 -0.00062 0.00208 -0.00657 C16 1 0.144116 0.177114 0.292252 11.00000 0.01508 0.02298 = 0.02270 -0.00375 0.00154 -0.00572 AFIX 43 H16 2 0.054276 0.245095 0.302885 11.00000 -1.20000 AFIX 0 C17 1 0.151627 0.045942 0.272896 11.00000 0.01924 0.02458 = 0.02600 -0.00246 -0.00052 -0.01112 AFIX 43 H17 2 0.066994 0.024368 0.270897 11.00000 -1.20000 AFIX 0 C18 1 0.281292 -0.053197 0.256558 11.00000 0.02263 0.01741 = 0.01845 -0.00281 0.00106 -0.00730 AFIX 43 H18 2 0.285953 -0.143242 0.244288 11.00000 -1.20000 AFIX 0 C19 1 0.258522 0.351644 0.318580 11.00000 0.01653 0.01877 = 0.02143 -0.00159 0.00035 -0.00706 AFIX 23 H19A 2 0.277482 0.404237 0.270236 11.00000 -1.20000 H19B 2 0.161320 0.403531 0.337061 11.00000 -1.20000 AFIX 0 C21 1 0.502470 0.257103 0.380204 11.00000 0.01950 0.01905 = 0.01553 -0.00354 0.00090 -0.01007 C23 1 0.464982 0.338054 0.503235 11.00000 0.02670 0.02147 = 0.02080 -0.00600 0.00602 -0.01304 C24 1 0.475710 0.370528 0.582982 11.00000 0.04342 0.03325 = 0.02121 -0.00654 0.00416 -0.02285 AFIX 43 H24 2 0.563160 0.332612 0.613443 11.00000 -1.20000 AFIX 0 C25 1 0.354483 0.459764 0.615847 11.00000 0.05331 0.03733 = 0.02342 -0.01212 0.01153 -0.02697 AFIX 43 H25 2 0.358398 0.483917 0.670131 11.00000 -1.20000 AFIX 0 C26 1 0.225382 0.515823 0.571059 11.00000 0.05000 0.03163 = 0.03496 -0.01578 0.02109 -0.02143 AFIX 43 H26 2 0.143971 0.577770 0.595520 11.00000 -1.20000 AFIX 0 C27 1 0.213650 0.483018 0.491882 11.00000 0.03258 0.02568 = 0.03124 -0.00891 0.01086 -0.01367 AFIX 43 H27 2 0.126061 0.520525 0.461527 11.00000 -1.20000 AFIX 0 C28 1 0.336121 0.392739 0.459203 11.00000 0.02786 0.02302 = 0.02283 -0.00893 0.00497 -0.01564 C29 1 0.699913 0.221552 0.074639 11.00000 0.03178 0.01755 = 0.02018 0.00280 -0.00358 -0.01337 AFIX 23 H29A 2 0.668213 0.288449 0.117136 11.00000 -1.20000 H29B 2 0.646048 0.265839 0.023644 11.00000 -1.20000 AFIX 0 C30 1 0.859569 0.186919 0.061514 11.00000 0.03486 0.03346 = 0.02627 0.00395 -0.00150 -0.02134 AFIX 23 H30A 2 0.912309 0.148688 0.113655 11.00000 -1.20000 H30B 2 0.892296 0.114350 0.022277 11.00000 -1.20000 AFIX 0 C31 1 0.895062 0.312604 0.029779 11.00000 0.03477 0.03999 = 0.03970 0.00927 -0.00653 -0.01927 AFIX 23 H31A 2 0.989524 0.280046 0.004150 11.00000 -1.20000 H31B 2 0.823297 0.366092 -0.012782 11.00000 -1.20000 AFIX 0 C32 1 0.898103 0.406432 0.093992 11.00000 0.04411 0.02880 = 0.06399 0.00640 -0.00911 -0.01938 AFIX 137 H32A 2 0.919504 0.485832 0.069455 11.00000 -1.50000 H32B 2 0.971978 0.355538 0.135166 11.00000 -1.50000 H32C 2 0.804827 0.439616 0.119571 11.00000 -1.50000 AFIX 0 C33 1 0.711217 0.169314 0.477928 11.00000 0.02352 0.04855 = 0.02149 -0.00194 -0.00244 -0.01507 AFIX 23 H33A 2 0.747988 0.220154 0.515694 11.00000 -1.20000 H33B 2 0.772579 0.152983 0.429817 11.00000 -1.20000 AFIX 0 C34 1 0.720855 0.033096 0.518916 11.00000 0.03053 0.08741 = 0.08582 0.06486 -0.00331 -0.01154 AFIX 23 part 1 21 H31C 2 0.816351 -0.007622 0.546010 21.00000 -1.20000 H31D 2 0.649896 0.052638 0.562500 21.00000 -1.20000 AFIX 23 part 2 -21 H31E 2 0.635813 0.012566 0.502275 -21.00000 -1.20000 H31F 2 0.716657 0.042008 0.578339 -21.00000 -1.20000 AFIX 0 part 0 part 1 21 C35 1 0.702070 -0.065653 0.476697 21.00000 0.04291 0.02981 = 0.03286 0.00333 -0.00287 -0.01354 AFIX 23 H35A 2 0.615912 -0.023639 0.440935 21.00000 -1.20000 H35B 2 0.685368 -0.136151 0.515012 21.00000 -1.20000 AFIX 0 C36 1 0.828845 -0.136310 0.425287 21.00000 0.05928 0.03347 = 0.04549 -0.00585 0.00247 -0.01083 AFIX 137 H36A 2 0.806235 -0.200953 0.391718 21.00000 -1.50000 H36B 2 0.911936 -0.187489 0.460778 21.00000 -1.50000 H36C 2 0.850448 -0.066237 0.390080 21.00000 -1.50000 AFIX 0 part 2 -21 C35' 1 0.872718 -0.107824 0.499422 -21.00000 0.04291 0.02981 = 0.03286 0.00333 -0.00287 -0.01354 AFIX 23 H35C 2 0.952220 -0.098966 0.531543 -21.00000 -1.20000 H35D 2 0.856763 -0.191828 0.522945 -21.00000 -1.20000 AFIX 0 C36' 1 0.925847 -0.137955 0.417008 -21.00000 0.05928 0.03347 = 0.04549 -0.00585 0.00247 -0.01083 AFIX 137 H36D 2 0.904217 -0.217469 0.399662 -21.00000 -1.50000 H36E 2 1.029435 -0.159747 0.417222 -21.00000 -1.50000 H36F 2 0.879254 -0.056705 0.379279 -21.00000 -1.50000 AFIX 0 part 0 CL2S 4 -0.023660 0.844886 0.180890 11.00000 0.03362 0.03073 = 0.08549 -0.00447 -0.01166 -0.01177 CL3S 4 -0.091198 0.613239 0.256424 11.00000 0.03460 0.04340 = 0.05193 0.00603 0.01084 -0.00503 C1S 1 0.013254 0.668385 0.186940 11.00000 0.07351 0.02846 = 0.07539 0.00622 0.03675 -0.00830 AFIX 23 H1SA 2 0.115253 0.620326 0.202696 11.00000 -1.20000 H1SB 2 -0.001906 0.640491 0.132437 11.00000 -1.20000 AFIX 0 F2R 8 0.343236 0.688126 0.127664 11.00000 0.03913 0.03466 = 0.02877 0.00329 -0.00215 -0.00946 F3R 8 0.554336 0.544241 0.183024 11.00000 0.02590 0.04079 = 0.05224 0.00679 0.00053 -0.00873 F4R 8 0.380399 0.459025 0.154970 11.00000 0.07685 0.04513 = 0.04338 -0.02426 0.02668 -0.04266 F5R 8 0.354657 0.599564 0.258087 11.00000 0.04953 0.03138 = 0.02529 -0.00767 0.00598 -0.02412 B1R 7 0.410085 0.570782 0.179332 11.00000 0.02721 0.02251 = 0.02838 -0.00280 0.00231 -0.01470 HKLF 4 REM HV2_23R_0m_a.res in P-1 REM R1 = 0.0331 for 6249 Fo > 4sig(Fo) and 0.0520 for all 7327 data REM 407 parameters refined using 0 restraints END WGHT 0.0223 8.3960 REM Highest difference peak 4.965, deepest hole -1.574, 1-sigma level 0.168 Q1 1 0.2732 0.5147 0.1704 11.00000 0.05 4.97 Q2 1 0.2414 0.7146 0.2943 11.00000 0.05 1.23 Q3 1 0.8176 0.3851 0.0513 11.00000 0.05 1.14 Q4 1 0.6056 0.0954 0.2116 11.00000 0.05 1.14 Q5 1 0.9699 0.3890 0.0477 11.00000 0.05 1.08 Q6 1 0.5207 0.2147 0.3424 11.00000 0.05 1.02 Q7 1 1.0644 0.4562 0.1725 11.00000 0.05 0.93 Q8 1 0.1702 0.4729 0.3708 11.00000 0.05 0.92 Q9 1 0.7369 -0.0171 0.4871 11.00000 0.05 0.88 Q10 1 -0.1059 0.5541 0.2160 11.00000 0.05 0.86 Q11 1 0.6598 0.1978 0.2212 11.00000 0.05 0.86 Q12 1 0.6620 0.2341 0.2786 11.00000 0.05 0.83 Q13 1 0.8804 -0.1788 0.3428 11.00000 0.05 0.83 Q14 1 0.7096 0.0629 0.5297 11.00000 0.05 0.80 Q15 1 0.4620 0.1244 0.2728 11.00000 0.05 0.76 Q16 1 0.9327 0.0655 0.1910 11.00000 0.05 0.76 Q17 1 0.4396 0.1579 0.2710 11.00000 0.05 0.75 Q18 1 -0.0227 0.6516 0.2951 11.00000 0.05 0.74 Q19 1 0.5152 0.1145 0.2172 11.00000 0.05 0.74 Q20 1 0.2619 0.5831 0.1127 11.00000 0.05 0.74 ; _shelx_res_checksum 56288 _shelx_hkl_file ; -2 0 0 100.59 13.10 -2 0 0 100.89 11.60 -2 0 0 102.49 10.00 -2 0 0 112.99 11.30 -2 0 0 104.79 12.40 -2 0 0 117.59 14.60 -2 0 0 101.99 12.40 -2 0 0 113.99 14.40 2 0 0 112.09 11.70 2 0 0 95.09 12.60 2 0 0 92.49 11.80 2 0 0 111.99 13.60 2 0 0 116.59 14.30 2 0 0 101.69 10.00 2 0 0 97.59 11.70 2 0 0 87.49 11.40 2 0 0 99.79 13.10 2 0 0 105.79 13.10 -3 0 0 519.75 28.20 -3 0 0 507.25 30.60 -3 0 0 539.85 25.00 -3 0 0 564.44 33.40 -3 0 0 599.34 29.10 -3 0 0 600.14 34.20 -3 0 0 542.35 31.00 -3 0 0 561.34 31.60 3 0 0 541.95 30.00 3 0 0 596.14 30.20 3 0 0 540.15 25.40 3 0 0 536.15 30.00 3 0 0 601.94 32.90 3 0 0 573.14 30.70 3 0 0 522.15 31.60 3 0 0 572.44 27.20 3 0 0 546.75 32.00 3 0 0 551.24 32.40 -4 0 0 713.43 42.40 -4 0 0 683.83 40.40 -4 0 0 648.54 35.90 -4 0 0 718.63 41.10 -4 0 0 644.74 41.70 -4 0 0 685.43 39.60 -4 0 0 680.73 31.60 -4 0 0 662.53 35.30 4 0 0 573.74 38.20 4 0 0 711.13 38.50 4 0 0 647.34 40.00 4 0 0 660.13 34.00 4 0 0 600.64 39.10 4 0 0 684.73 38.60 4 0 0 677.03 37.70 4 0 0 686.63 40.60 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825.32 51.29 4 -3 0 -9.60 15.20 4 -3 0 10.10 9.90 4 -3 0 12.50 7.70 4 -3 0 5.30 9.00 4 -3 0 3.70 9.40 4 -3 0 2.70 9.90 4 -3 0 -4.70 12.90 4 -3 0 4.50 16.50 4 -3 0 4.50 11.90 4 -3 0 1.10 12.70 4 -3 0 -3.80 7.60 4 -3 0 -9.20 6.40 -4 3 0 12.60 8.00 -4 3 0 10.00 10.40 -4 3 0 11.70 16.30 -4 3 0 -5.80 10.10 -4 3 0 -0.70 9.90 -4 3 0 7.30 7.50 -4 3 0 34.00 21.40 -4 3 0 10.90 10.20 3 -3 0 288.47 21.40 3 -3 0 242.48 22.60 3 -3 0 297.77 25.20 3 -3 0 249.18 32.40 3 -3 0 260.47 17.50 3 -3 0 253.27 22.00 3 -3 0 255.47 17.90 3 -3 0 270.47 32.40 3 -3 0 241.98 29.30 3 -3 0 249.97 27.90 3 -3 0 277.87 19.50 3 -3 0 307.17 27.80 -3 3 0 292.97 25.40 -3 3 0 264.47 37.70 -3 3 0 256.07 17.60 -3 3 0 281.67 18.30 -3 3 0 214.08 24.60 -3 3 0 267.17 29.20 -3 3 0 276.97 24.70 -3 3 0 274.27 24.50 2 -3 0 197.68 21.00 2 -3 0 191.78 12.70 2 -3 0 199.78 23.30 2 -3 0 216.48 18.90 2 -3 0 238.38 28.60 2 -3 0 186.08 12.90 2 -3 0 215.08 19.10 2 -3 0 173.08 22.90 2 -3 0 247.28 30.10 2 -3 0 228.58 20.70 2 -3 0 193.18 28.00 2 -3 0 214.88 17.70 -2 3 0 198.78 13.60 -2 3 0 204.38 19.20 -2 3 0 195.78 22.30 -2 3 0 184.08 18.50 -2 3 0 189.18 26.50 -2 3 0 207.98 13.50 -2 3 0 209.18 18.70 -2 3 0 231.08 23.20 -2 3 0 188.48 30.40 1 -3 0 2016.00 72.99 1 -3 0 1982.20 49.00 1 -3 0 2018.00 73.49 1 -3 0 2017.80 60.49 1 -3 0 1982.30 58.19 1 -3 0 1962.00 70.29 1 -3 0 2067.39 62.29 1 -3 0 1922.11 49.00 1 -3 0 2006.00 58.59 1 -3 0 2012.90 77.09 1 -3 0 2022.80 65.79 1 -3 0 2003.90 55.89 1 -3 0 1886.91 66.79 -1 3 0 1943.91 49.10 -1 3 0 1980.30 50.59 -1 3 0 1948.80 77.19 -1 3 0 1937.51 56.89 -1 3 0 2046.50 72.69 -1 3 0 1999.40 63.69 -1 3 0 1962.80 69.29 -1 3 0 1939.11 58.69 -1 3 0 2080.09 65.29 0 -3 0 2713.23 85.39 0 -3 0 2903.81 84.69 0 -3 0 2799.62 88.59 0 -3 0 2703.43 88.69 0 -3 0 2728.63 69.09 0 -3 0 2726.53 72.69 0 -3 0 2729.83 77.39 0 -3 0 2720.43 66.99 0 -3 0 2793.22 85.29 0 -3 0 2751.42 69.79 0 -3 0 2835.72 74.19 0 -3 0 2717.63 72.19 0 3 0 2746.53 72.79 0 3 0 2763.62 69.79 0 3 0 2652.43 85.19 0 3 0 2836.32 79.69 0 3 0 2817.22 87.49 0 3 0 2762.22 71.99 0 3 0 2827.72 73.39 0 3 0 2736.73 66.39 0 3 0 2739.03 82.09 0 3 0 2781.42 71.69 -1 -3 0 249.08 12.30 -1 -3 0 278.27 20.60 -1 -3 0 244.28 21.80 -1 -3 0 248.48 17.30 -1 -3 0 241.98 17.30 -1 -3 0 216.08 19.30 -1 -3 0 225.28 16.70 -1 -3 0 227.38 22.90 -1 -3 0 253.37 14.90 -1 -3 0 247.48 23.30 -1 -3 0 246.38 18.10 1 3 0 254.57 16.50 1 3 0 260.17 19.40 1 3 0 260.97 16.40 1 3 0 227.88 24.40 1 3 0 240.38 18.60 1 3 0 222.08 20.70 1 3 0 245.88 23.80 1 3 0 268.47 17.60 1 3 0 241.88 21.30 -2 -3 0 678.93 35.70 -2 -3 0 720.33 34.10 -2 -3 0 751.52 33.60 -2 -3 0 733.73 34.10 -2 -3 0 699.63 35.80 -2 -3 0 709.13 37.00 -2 -3 0 678.23 35.90 -2 -3 0 718.53 34.30 -2 -3 0 728.33 36.00 -2 -3 0 735.23 30.70 -2 -3 0 725.53 31.00 2 3 0 713.63 30.60 2 3 0 707.03 32.80 2 3 0 721.63 41.90 2 3 0 682.23 37.20 2 3 0 740.83 35.70 2 3 0 674.33 36.00 2 3 0 714.23 35.30 2 3 0 698.63 30.20 -3 -3 0 55.09 14.60 -3 -3 0 60.49 14.70 -3 -3 0 85.39 16.60 -3 -3 0 66.49 14.70 -3 -3 0 80.99 13.90 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84.89 5 3 0 2305.87 86.59 5 3 0 2211.88 76.19 5 3 0 2216.48 77.59 5 3 0 2299.27 89.09 5 3 0 2325.67 85.99 5 3 0 2237.08 87.69 5 3 0 2273.77 77.79 5 3 0 2377.16 87.89 5 3 0 2352.06 78.49 5 3 0 2349.06 85.99 -6 -3 0 1126.89 57.19 -6 -3 0 1125.39 59.89 -6 -3 0 1252.57 67.39 -6 -3 0 1121.19 62.89 -6 -3 0 1120.09 63.29 -6 -3 0 1112.09 48.10 -6 -3 0 1114.89 56.99 -6 -3 0 1124.09 60.49 -6 -3 0 1094.09 52.89 -6 -3 0 1133.09 61.29 6 3 0 1061.49 48.50 6 3 0 1076.79 59.19 6 3 0 1069.39 61.59 6 3 0 1154.08 62.89 6 3 0 1073.29 61.19 6 3 0 1045.60 53.99 6 3 0 1017.00 54.19 6 3 0 1105.99 59.49 6 3 0 1131.39 59.69 6 3 0 1041.60 50.79 6 3 0 1140.69 53.59 6 3 0 1114.79 62.89 -7 -3 0 1455.25 72.69 -7 -3 0 1373.76 74.69 -7 -3 0 1169.48 67.79 -7 -3 0 1337.17 71.79 -7 -3 0 1272.87 74.19 -7 -3 0 1404.06 79.19 -7 -3 0 1175.48 68.09 -7 -3 0 1355.16 64.09 -7 -3 0 1298.87 51.19 -7 -3 0 1329.37 66.29 7 3 0 1272.07 64.59 7 3 0 1376.06 69.69 7 3 0 1342.47 73.69 7 3 0 1221.28 80.89 7 3 0 1317.07 73.19 7 3 0 1217.68 64.39 7 3 0 1233.88 60.89 7 3 0 1332.97 71.29 7 3 0 1366.56 66.79 7 3 0 1427.36 75.69 7 3 0 1214.08 70.89 -8 -3 0 878.01 38.60 -8 -3 0 800.32 52.99 -8 -3 0 833.92 60.89 -8 -3 0 878.21 62.79 -8 -3 0 992.80 57.69 -8 -3 0 1014.40 72.39 -8 -3 0 944.21 64.59 -8 -3 0 872.61 39.10 -8 -3 0 922.71 66.29 -8 -3 0 870.21 65.69 8 3 0 825.62 52.99 8 3 0 784.42 59.79 8 3 0 761.12 56.79 8 3 0 887.71 61.29 8 3 0 1017.10 63.69 8 3 0 957.20 67.69 8 3 0 834.22 62.99 8 3 0 842.12 60.29 8 3 0 897.01 57.79 8 3 0 1017.40 67.19 -9 -3 0 201.68 41.70 -9 -3 0 141.89 17.10 -9 -3 0 174.28 16.30 -9 -3 0 166.68 39.10 -9 -3 0 210.28 35.50 -9 -3 0 212.18 40.40 -9 -3 0 207.08 39.40 -9 -3 0 279.27 45.70 9 3 0 234.78 42.40 9 3 0 196.08 37.50 9 3 0 177.38 34.20 9 3 0 205.18 36.60 9 3 0 143.69 27.50 9 3 0 197.58 41.90 9 3 0 188.38 37.90 -10 -3 0 14.20 31.90 -10 -3 0 33.20 27.30 -10 -3 0 21.30 28.90 -10 -3 0 74.19 30.00 -10 -3 0 -31.50 29.10 -10 -3 0 6.80 22.50 10 3 0 15.60 23.50 10 3 0 33.60 26.80 10 3 0 18.20 28.30 10 3 0 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2014.40 84.19 0 -4 4 1896.91 77.89 0 -4 4 1815.72 80.39 0 -4 4 1910.41 61.09 0 -4 4 1862.31 75.39 0 -4 4 1897.21 73.09 0 -4 4 1890.41 70.79 0 -4 4 1964.20 77.69 0 -4 4 1962.40 73.99 0 -4 4 1924.61 79.69 0 -4 4 1901.11 76.99 -1 4 -4 2017.50 72.59 -1 4 -4 2068.09 83.19 -1 4 -4 1991.10 52.59 -1 4 -4 1983.60 83.49 -1 4 -4 2009.70 78.69 -1 4 -4 2025.40 60.59 -1 4 -4 2088.49 87.19 -1 4 -4 2018.10 75.39 1 -4 4 2002.80 58.09 1 -4 4 2062.79 54.99 1 -4 4 2023.80 78.79 1 -4 4 2109.69 79.99 1 -4 4 2118.99 88.49 1 -4 4 2048.30 78.69 1 -4 4 2056.99 89.59 1 -4 4 1944.31 79.09 1 -4 4 2026.90 75.49 1 -4 4 1942.81 81.69 -2 4 -4 1945.91 77.59 -2 4 -4 1933.91 53.69 -2 4 -4 1956.00 82.09 -2 4 -4 2106.89 89.39 -2 4 -4 1991.10 88.79 -2 4 -4 1986.80 87.39 -2 4 -4 1903.01 72.59 -2 4 -4 2011.70 95.69 -2 4 -4 2095.09 82.09 -2 4 -4 1924.51 60.49 2 -4 4 2154.38 85.79 2 -4 4 2169.98 92.79 2 -4 4 2123.89 64.79 2 -4 4 1931.81 85.39 2 -4 4 2070.69 87.49 2 -4 4 2009.20 79.59 2 -4 4 2043.80 76.79 2 -4 4 2124.89 94.29 2 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206.38 45.50 1 0 21 163.08 52.99 1 0 21 246.98 63.79 1 0 21 186.18 48.80 1 0 21 43.40 36.40 1 0 21 163.78 66.69 2 0 21 149.59 61.09 2 -1 -21 -8.00 28.60 2 -1 -21 -6.80 37.00 2 -1 -21 -17.40 29.80 2 -1 -21 46.20 42.30 -2 1 21 5.60 34.70 -2 1 21 -6.10 36.30 -2 1 21 11.20 33.50 1 -1 -21 137.59 52.79 1 -1 -21 126.49 37.10 1 -1 -21 27.30 40.50 1 -1 -21 168.18 50.09 -1 1 21 93.89 41.70 -1 1 21 84.59 48.30 -1 1 21 109.89 49.30 -1 1 21 142.09 52.49 0 -1 -21 324.07 65.09 0 -1 -21 256.87 57.89 0 -1 -21 250.47 55.89 0 -1 -21 485.15 61.29 0 1 21 360.96 64.99 0 1 21 458.65 84.49 0 1 21 281.87 60.39 0 1 21 312.37 50.69 -1 -1 -21 155.88 47.90 -1 -1 -21 231.58 52.89 -1 -1 -21 281.07 62.79 -1 -1 -21 358.86 56.89 1 1 21 270.77 65.39 1 1 21 284.27 50.29 1 1 21 218.68 56.79 1 1 21 299.77 66.69 -2 -1 -21 111.19 43.40 -2 -1 -21 66.79 47.90 -2 -1 -21 111.39 43.80 -2 -1 -21 70.09 41.10 2 1 21 191.08 55.49 2 1 21 132.29 47.20 2 1 21 100.49 37.70 2 1 21 105.59 50.69 1 -2 -21 305.77 63.89 1 -2 -21 286.07 47.60 1 -2 -21 339.97 70.29 1 -2 -21 345.87 64.59 -1 2 21 328.47 55.29 -1 2 21 412.26 67.89 -1 2 21 519.45 76.79 -1 2 21 346.07 73.09 0 -2 -21 23.70 42.20 0 -2 -21 87.39 43.10 0 -2 -21 150.08 49.80 0 -2 -21 169.48 40.70 0 2 21 188.78 54.59 0 2 21 43.50 37.60 0 2 21 150.38 52.49 0 2 21 140.79 54.19 -1 -2 -21 -31.90 32.10 -1 -2 -21 -9.00 32.50 -1 -2 -21 -37.60 31.90 -1 -2 -21 -11.00 37.60 1 2 21 26.30 43.70 1 2 21 15.10 37.40 1 2 21 17.50 34.10 1 2 21 -58.49 29.60 -2 -2 -21 -67.09 33.30 -2 -2 -21 -44.90 33.60 -2 -2 -21 31.10 39.40 2 2 21 -44.90 37.60 2 2 21 -57.79 27.80 2 2 21 6.20 37.80 2 2 21 -40.00 26.40 0 -3 -21 38.80 35.70 0 -3 -21 62.79 46.40 0 -3 -21 25.20 39.00 0 -3 -21 15.40 28.50 0 3 21 97.89 45.50 0 3 21 19.70 31.20 0 3 21 59.69 38.00 0 3 21 -45.80 36.10 -1 -3 -21 158.58 48.40 -1 -3 -21 97.19 49.99 -1 -3 -21 203.58 55.29 -1 -3 -21 246.18 56.49 1 3 21 228.48 60.99 1 3 21 201.78 41.00 1 3 21 182.68 53.09 1 3 21 250.27 58.49 -2 -3 -21 155.08 49.00 -2 -3 -21 152.78 50.59 2 3 21 216.58 69.89 2 3 21 111.59 35.10 2 3 21 116.39 44.70 2 3 21 204.48 55.99 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 47214 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au Au1 0.57600(2) 0.16134(2) 0.27627(2) 0.01682(6) Uani d . . . 1.0 . . Cl Cl2 0.78363(12) 0.21846(12) 0.27578(7) 0.0203(2) Uani d . . . 1.0 . . N N4 0.6682(4) 0.0943(4) 0.0998(2) 0.0166(8) Uani d . . . 1.0 . . N N11 0.6080(4) -0.0636(4) 0.1687(2) 0.0153(8) Uani d . . . 1.0 . . N N20 0.3636(4) 0.3385(4) 0.3835(2) 0.0188(8) Uani d . . . 1.0 . . N N22 0.5646(5) 0.2552(4) 0.4520(3) 0.0221(9) Uani d . . . 1.0 . . C C3 0.6252(5) 0.0599(5) 0.1722(3) 0.0160(9) Uani d . . . 1.0 . . C C5 0.6798(5) -0.0097(5) 0.0477(3) 0.0151(9) Uani d . . . 1.0 . . C C6 0.7177(5) -0.0222(5) -0.0338(3) 0.0199(10) Uani d . . . 1.0 . . H H6 0.742037 0.047284 -0.064486 0.024 Uiso calc U . R 1.0 . . C C7 0.7177(5) -0.1415(5) -0.0673(3) 0.0215(10) Uani d . . . 1.0 . . H H7 0.744538 -0.15497 -0.122197 0.026 Uiso calc U . R 1.0 . . C C8 0.6795(5) -0.2432(5) -0.0229(3) 0.0217(10) Uani d . . . 1.0 . . H H8 0.680076 -0.322884 -0.048708 0.026 Uiso calc U . R 1.0 . . C C9 0.6409(5) -0.2303(5) 0.0578(3) 0.0190(10) Uani d . . . 1.0 . . H H9 0.615485 -0.299107 0.088338 0.023 Uiso calc U . R 1.0 . . C C10 0.6418(5) -0.1107(5) 0.0912(3) 0.0169(9) Uani d . . . 1.0 . . C C12 0.5467(5) -0.1254(5) 0.2344(3) 0.0184(9) Uani d . . . 1.0 . . H H12A 0.61348 -0.154215 0.282007 0.022 Uiso calc U . R 1.0 . . H H12B 0.531695 -0.208811 0.216288 0.022 Uiso calc U . R 1.0 . . C C13 0.4059(5) -0.0213(5) 0.2580(3) 0.0155(9) Uani d . . . 1.0 . . C C14 0.3942(5) 0.1098(4) 0.2772(2) 0.0130(9) Uani d . . . 1.0 . . C C15 0.2668(5) 0.2092(5) 0.2961(3) 0.0173(9) Uani d . . . 1.0 . . C C16 0.1441(5) 0.1771(5) 0.2923(3) 0.0204(10) Uani d . . . 1.0 . . H H16 0.054276 0.245095 0.302885 0.025 Uiso calc U . R 1.0 . . C C17 0.1516(5) 0.0459(5) 0.2729(3) 0.0223(10) Uani d . . . 1.0 . . H H17 0.066994 0.024368 0.270897 0.027 Uiso calc U . R 1.0 . . C C18 0.2813(5) -0.0532(5) 0.2566(3) 0.0194(10) Uani d . . . 1.0 . . H H18 0.285953 -0.143242 0.244288 0.023 Uiso calc U . R 1.0 . . C C19 0.2585(5) 0.3516(5) 0.3186(3) 0.0187(9) Uani d . . . 1.0 . . H H19A 0.277482 0.404237 0.270236 0.022 Uiso calc U . R 1.0 . . H H19B 0.16132 0.403531 0.337061 0.022 Uiso calc U . R 1.0 . . C C21 0.5025(5) 0.2571(5) 0.3802(3) 0.0170(9) Uani d . . . 1.0 . . C C23 0.4650(6) 0.3381(5) 0.5032(3) 0.0216(10) Uani d . . . 1.0 . . C C24 0.4757(7) 0.3705(6) 0.5830(3) 0.0299(12) Uani d . . . 1.0 . . H H24 0.56316 0.332612 0.613443 0.036 Uiso calc U . R 1.0 . . C C25 0.3545(7) 0.4598(6) 0.6158(3) 0.0346(14) Uani d . . . 1.0 . . H H25 0.358398 0.483917 0.670131 0.042 Uiso calc U . R 1.0 . . C C26 0.2254(7) 0.5158(6) 0.5711(4) 0.0363(14) Uani d . . . 1.0 . . H H26 0.143971 0.57777 0.59552 0.044 Uiso calc U . R 1.0 . . C C27 0.2136(6) 0.4830(6) 0.4919(3) 0.0286(12) Uani d . . . 1.0 . . H H27 0.126061 0.520525 0.461527 0.034 Uiso calc U . R 1.0 . . C C28 0.3361(6) 0.3927(5) 0.4592(3) 0.0224(10) Uani d . . . 1.0 . . C C29 0.6999(6) 0.2216(5) 0.0746(3) 0.0221(10) Uani d . . . 1.0 . . H H29A 0.668213 0.288449 0.117136 0.027 Uiso calc U . R 1.0 . . H H29B 0.646048 0.265839 0.023644 0.027 Uiso calc U . R 1.0 . . C C30 0.8596(6) 0.1869(6) 0.0615(3) 0.0293(12) Uani d . . . 1.0 . . H H30A 0.912309 0.148688 0.113655 0.035 Uiso calc U . R 1.0 . . H H30B 0.892296 0.11435 0.022277 0.035 Uiso calc U . R 1.0 . . C C31 0.8951(7) 0.3126(6) 0.0298(4) 0.0371(14) Uani d . . . 1.0 . . H H31A 0.989524 0.280046 0.00415 0.045 Uiso calc U . R 1.0 . . H H31B 0.823297 0.366092 -0.012782 0.045 Uiso calc U . R 1.0 . . C C32 0.8981(7) 0.4064(6) 0.0940(5) 0.0444(16) Uani d . . . 1.0 . . H H32A 0.919504 0.485832 0.069455 0.067 Uiso calc U . R 1.0 . . H H32B 0.971978 0.355538 0.135166 0.067 Uiso calc U . R 1.0 . . H H32C 0.804827 0.439616 0.119571 0.067 Uiso calc U . R 1.0 . . C C33 0.7112(6) 0.1693(6) 0.4779(3) 0.0306(12) Uani d . . . 1.0 . . H H33A 0.747988 0.220154 0.515694 0.037 Uiso calc U . R 1.0 . . H H33B 0.772579 0.152983 0.429817 0.037 Uiso calc U . R 1.0 . . C C34 0.7209(8) 0.0331(10) 0.5189(6) 0.074(3) Uani d . . . 1.0 . . H H31C 0.816351 -0.007622 0.54601 0.089 Uiso calc U P R 0.655(8) A 1 H H31D 0.649896 0.052638 0.5625 0.089 Uiso calc U P R 0.655(8) A 1 H H31E 0.635813 0.012566 0.502275 0.089 Uiso calc U P R 0.345(8) A 2 H H31F 0.716657 0.042008 0.578339 0.089 Uiso calc U P R 0.345(8) A 2 C C35 0.7021(11) -0.0657(10) 0.4767(6) 0.0353(18) Uani d . P . 0.655(8) A 1 H H35A 0.615912 -0.023639 0.440935 0.042 Uiso calc U P R 0.655(8) A 1 H H35B 0.685368 -0.136151 0.515012 0.042 Uiso calc U P R 0.655(8) A 1 C C36 0.8288(13) -0.1363(11) 0.4253(7) 0.047(2) Uani d . P . 0.655(8) A 1 H H36A 0.806235 -0.200953 0.391718 0.071 Uiso calc U P R 0.655(8) A 1 H H36B 0.911936 -0.187489 0.460778 0.071 Uiso calc U P R 0.655(8) A 1 H H36C 0.850448 -0.066237 0.39008 0.071 Uiso calc U P R 0.655(8) A 1 C C35' 0.873(2) -0.1078(18) 0.4994(11) 0.0353(18) Uani d . P . 0.345(8) A 2 H H35C 0.95222 -0.098966 0.531543 0.042 Uiso calc U P R 0.345(8) A 2 H H35D 0.856763 -0.191828 0.522945 0.042 Uiso calc U P R 0.345(8) A 2 C C36' 0.926(3) -0.138(2) 0.4170(13) 0.047(2) Uani d . P . 0.345(8) A 2 H H36D 0.904217 -0.217469 0.399662 0.071 Uiso calc U P R 0.345(8) A 2 H H36E 1.029435 -0.159747 0.417222 0.071 Uiso calc U P R 0.345(8) A 2 H H36F 0.879254 -0.056705 0.379279 0.071 Uiso calc U P R 0.345(8) A 2 Cl Cl2S -0.02366(17) 0.84489(16) 0.18089(13) 0.0498(4) Uani d . . . 1.0 . . Cl Cl3S -0.09120(17) 0.61324(17) 0.25642(11) 0.0461(4) Uani d . . . 1.0 . . C C1S 0.0133(9) 0.6684(7) 0.1869(5) 0.062(2) Uani d . . . 1.0 . . H H1SA 0.115253 0.620326 0.202696 0.075 Uiso calc U . R 1.0 . . H H1SB -0.001906 0.640491 0.132437 0.075 Uiso calc U . R 1.0 . . F F2R 0.3432(4) 0.6881(3) 0.1277(2) 0.0354(8) Uani d . . . 1.0 . . F F3R 0.5543(4) 0.5442(4) 0.1830(2) 0.0410(8) Uani d . . . 1.0 . . F F4R 0.3804(5) 0.4590(4) 0.1550(2) 0.0484(10) Uani d . . . 1.0 . . F F5R 0.3547(4) 0.5996(3) 0.25809(19) 0.0325(7) Uani d . . . 1.0 . . B B1R 0.4101(7) 0.5708(6) 0.1793(4) 0.0244(12) Uani d . . . 1.0 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01655(9) 0.01732(9) 0.01760(9) -0.00692(7) 0.00095(6) -0.00299(6) Cl2 0.0166(5) 0.0253(6) 0.0222(6) -0.0108(5) 0.0011(4) -0.0049(5) N4 0.0169(19) 0.0165(19) 0.0167(19) -0.0065(16) 0.0022(15) -0.0013(15) N11 0.0181(19) 0.0135(18) 0.0159(19) -0.0075(15) 0.0020(15) -0.0017(15) N20 0.019(2) 0.0172(19) 0.021(2) -0.0070(16) 0.0043(16) -0.0066(16) N22 0.023(2) 0.029(2) 0.019(2) -0.0142(18) 0.0025(17) -0.0058(17) C3 0.013(2) 0.013(2) 0.018(2) -0.0007(17) -0.0011(17) -0.0008(17) C5 0.012(2) 0.015(2) 0.017(2) -0.0028(17) -0.0017(17) -0.0021(17) C6 0.017(2) 0.020(2) 0.020(2) -0.0038(19) 0.0005(19) -0.0017(19) C7 0.021(2) 0.024(2) 0.016(2) -0.004(2) -0.0018(19) -0.0041(19) C8 0.022(3) 0.018(2) 0.023(3) -0.0037(19) -0.003(2) -0.0055(19) C9 0.015(2) 0.020(2) 0.020(2) -0.0036(19) 0.0001(18) -0.0032(19) C10 0.011(2) 0.019(2) 0.018(2) -0.0017(18) 0.0000(17) -0.0023(18) C12 0.022(2) 0.018(2) 0.016(2) -0.0091(19) 0.0036(18) -0.0006(18) C13 0.015(2) 0.017(2) 0.014(2) -0.0066(18) -0.0014(17) 0.0003(17) C14 0.019(2) 0.015(2) 0.0044(19) -0.0057(18) -0.0006(16) 0.0002(15) C15 0.018(2) 0.018(2) 0.017(2) -0.0066(18) 0.0021(18) -0.0006(18) C16 0.015(2) 0.023(2) 0.023(2) -0.0057(19) 0.0015(19) -0.0038(19) C17 0.019(2) 0.025(3) 0.026(3) -0.011(2) -0.001(2) -0.002(2) C18 0.023(2) 0.017(2) 0.018(2) -0.0073(19) 0.0011(19) -0.0028(18) C19 0.017(2) 0.019(2) 0.021(2) -0.0071(19) 0.0004(18) -0.0016(18) C21 0.020(2) 0.019(2) 0.016(2) -0.0101(19) 0.0009(18) -0.0035(18) C23 0.027(3) 0.021(2) 0.021(2) -0.013(2) 0.006(2) -0.0060(19) C24 0.043(3) 0.033(3) 0.021(3) -0.023(3) 0.004(2) -0.007(2) C25 0.053(4) 0.037(3) 0.023(3) -0.027(3) 0.012(3) -0.012(2) C26 0.050(4) 0.032(3) 0.035(3) -0.021(3) 0.021(3) -0.016(3) C27 0.033(3) 0.026(3) 0.031(3) -0.014(2) 0.011(2) -0.009(2) C28 0.028(3) 0.023(2) 0.023(3) -0.016(2) 0.005(2) -0.009(2) C29 0.032(3) 0.018(2) 0.020(2) -0.013(2) -0.004(2) 0.0028(19) C30 0.035(3) 0.033(3) 0.026(3) -0.021(3) -0.002(2) 0.004(2) C31 0.035(3) 0.040(3) 0.040(3) -0.019(3) -0.007(3) 0.009(3) C32 0.044(4) 0.029(3) 0.064(5) -0.019(3) -0.009(3) 0.006(3) C33 0.024(3) 0.049(3) 0.021(3) -0.015(3) -0.002(2) -0.002(2) C34 0.031(4) 0.087(6) 0.086(6) -0.012(4) -0.003(4) 0.065(6) C35 0.043(5) 0.030(4) 0.033(4) -0.014(4) -0.003(4) 0.003(3) C36 0.059(7) 0.033(4) 0.045(5) -0.011(5) 0.002(6) -0.006(4) C35' 0.043(5) 0.030(4) 0.033(4) -0.014(4) -0.003(4) 0.003(3) C36' 0.059(7) 0.033(4) 0.045(5) -0.011(5) 0.002(6) -0.006(4) Cl2S 0.0336(8) 0.0307(8) 0.0855(13) -0.0118(6) -0.0117(8) -0.0045(8) Cl3S 0.0346(8) 0.0434(9) 0.0519(10) -0.0050(7) 0.0108(7) 0.0060(7) C1S 0.074(6) 0.028(3) 0.075(6) -0.008(3) 0.037(5) 0.006(3) F2R 0.0391(19) 0.0347(18) 0.0288(17) -0.0095(15) -0.0022(14) 0.0033(14) F3R 0.0259(18) 0.041(2) 0.052(2) -0.0087(15) 0.0005(16) 0.0068(17) F4R 0.077(3) 0.045(2) 0.043(2) -0.043(2) 0.027(2) -0.0243(17) F5R 0.050(2) 0.0314(17) 0.0253(16) -0.0241(16) 0.0060(15) -0.0077(13) B1R 0.027(3) 0.023(3) 0.028(3) -0.015(2) 0.002(2) -0.003(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C3 Au1 C21 . . 172.44(18) ? C3 Au1 C14 . . 86.24(17) ? C21 Au1 C14 . . 86.20(17) ? C3 Au1 Cl2 . . 93.76(13) ? C21 Au1 Cl2 . . 93.80(13) ? C14 Au1 Cl2 . . 179.58(13) ? C3 N4 C5 . . 109.3(4) ? C3 N4 C29 . . 127.7(4) ? C5 N4 C29 . . 123.0(4) ? C3 N11 C10 . . 109.4(4) ? C3 N11 C12 . . 123.1(4) ? C10 N11 C12 . . 127.1(4) ? C21 N20 C28 . . 109.8(4) ? C21 N20 C19 . . 123.0(4) ? C28 N20 C19 . . 126.8(4) ? C21 N22 C23 . . 109.7(4) ? C21 N22 C33 . . 126.3(4) ? C23 N22 C33 . . 123.7(4) ? N4 C3 N11 . . 108.3(4) ? N4 C3 Au1 . . 132.3(3) ? N11 C3 Au1 . . 119.2(3) ? C10 C5 N4 . . 107.0(4) ? C10 C5 C6 . . 121.3(4) ? N4 C5 C6 . . 131.6(4) ? C7 C6 C5 . . 116.1(5) ? C7 C6 H6 . . 121.9 ? C5 C6 H6 . . 121.9 ? C6 C7 C8 . . 122.3(5) ? C6 C7 H7 . . 118.9 ? C8 C7 H7 . . 118.9 ? C9 C8 C7 . . 121.6(5) ? C9 C8 H8 . . 119.2 ? C7 C8 H8 . . 119.2 ? C8 C9 C10 . . 116.0(5) ? C8 C9 H9 . . 122.0 ? C10 C9 H9 . . 122.0 ? C5 C10 C9 . . 122.7(4) ? C5 C10 N11 . . 105.9(4) ? C9 C10 N11 . . 131.3(4) ? N11 C12 C13 . . 109.8(4) ? N11 C12 H12A . . 109.7 ? C13 C12 H12A . . 109.7 ? N11 C12 H12B . . 109.7 ? C13 C12 H12B . . 109.7 ? H12A C12 H12B . . 108.2 ? C14 C13 C18 . . 117.9(4) ? C14 C13 C12 . . 121.4(4) ? C18 C13 C12 . . 120.6(4) ? C13 C14 C15 . . 123.2(4) ? C13 C14 Au1 . . 118.6(3) ? C15 C14 Au1 . . 118.2(3) ? C14 C15 C16 . . 118.1(4) ? C14 C15 C19 . . 121.7(4) ? C16 C15 C19 . . 120.2(4) ? C15 C16 C17 . . 120.3(4) ? C15 C16 H16 . . 119.8 ? C17 C16 H16 . . 119.8 ? C18 C17 C16 . . 120.4(5) ? C18 C17 H17 . . 119.8 ? C16 C17 H17 . . 119.8 ? C17 C18 C13 . . 120.1(4) ? C17 C18 H18 . . 120.0 ? C13 C18 H18 . . 120.0 ? N20 C19 C15 . . 110.1(4) ? N20 C19 H19A . . 109.6 ? C15 C19 H19A . . 109.6 ? N20 C19 H19B . . 109.6 ? C15 C19 H19B . . 109.6 ? H19A C19 H19B . . 108.1 ? N22 C21 N20 . . 108.0(4) ? N22 C21 Au1 . . 132.9(4) ? N20 C21 Au1 . . 119.2(3) ? N22 C23 C28 . . 106.7(4) ? N22 C23 C24 . . 132.2(5) ? C28 C23 C24 . . 121.1(5) ? C25 C24 C23 . . 117.3(6) ? C25 C24 H24 . . 121.4 ? C23 C24 H24 . . 121.4 ? C24 C25 C26 . . 121.5(5) ? C24 C25 H25 . . 119.3 ? C26 C25 H25 . . 119.3 ? C27 C26 C25 . . 121.5(5) ? C27 C26 H26 . . 119.2 ? C25 C26 H26 . . 119.2 ? C26 C27 C28 . . 116.7(6) ? C26 C27 H27 . . 121.7 ? C28 C27 H27 . . 121.7 ? C27 C28 N20 . . 132.3(5) ? C27 C28 C23 . . 121.9(5) ? N20 C28 C23 . . 105.8(4) ? N4 C29 C30 . . 111.1(4) ? N4 C29 H29A . . 109.4 ? C30 C29 H29A . . 109.4 ? N4 C29 H29B . . 109.4 ? C30 C29 H29B . . 109.4 ? H29A C29 H29B . . 108.0 ? C31 C30 C29 . . 112.7(5) ? C31 C30 H30A . . 109.0 ? C29 C30 H30A . . 109.0 ? C31 C30 H30B . . 109.0 ? C29 C30 H30B . . 109.0 ? H30A C30 H30B . . 107.8 ? C32 C31 C30 . . 113.6(5) ? C32 C31 H31A . . 108.8 ? C30 C31 H31A . . 108.8 ? C32 C31 H31B . . 108.8 ? C30 C31 H31B . . 108.8 ? H31A C31 H31B . . 107.7 ? C31 C32 H32A . . 109.5 ? C31 C32 H32B . . 109.5 ? H32A C32 H32B . . 109.5 ? C31 C32 H32C . . 109.5 ? H32A C32 H32C . . 109.5 ? H32B C32 H32C . . 109.5 ? N22 C33 C34 . . 112.5(5) ? N22 C33 H33A . . 109.1 ? C34 C33 H33A . . 109.1 ? N22 C33 H33B . . 109.1 ? C34 C33 H33B . . 109.1 ? H33A C33 H33B . . 107.8 ? C35 C34 C33 . . 120.9(8) ? C33 C34 C35' . . 115.9(8) ? C35 C34 H31C . . 107.1 ? C33 C34 H31C . . 107.1 ? C35 C34 H31D . . 107.1 ? C33 C34 H31D . . 107.1 ? H31C C34 H31D . . 106.8 ? C33 C34 H31E . . 108.3 ? C35' C34 H31E . . 108.3 ? C33 C34 H31F . . 108.3 ? C35' C34 H31F . . 108.3 ? H31E C34 H31F . . 107.4 ? C34 C35 C36 . . 112.7(9) ? C34 C35 H35A . . 109.1 ? C36 C35 H35A . . 109.1 ? C34 C35 H35B . . 109.1 ? C36 C35 H35B . . 109.1 ? H35A C35 H35B . . 107.8 ? C35 C36 H36A . . 109.5 ? C35 C36 H36B . . 109.5 ? H36A C36 H36B . . 109.5 ? C35 C36 H36C . . 109.5 ? H36A C36 H36C . . 109.5 ? H36B C36 H36C . . 109.5 ? C36' C35' C34 . . 123.1(14) ? C36' C35' H35C . . 106.6 ? C34 C35' H35C . . 106.6 ? C36' C35' H35D . . 106.6 ? C34 C35' H35D . . 106.6 ? H35C C35' H35D . . 106.5 ? C35' C36' H36D . . 109.5 ? C35' C36' H36E . . 109.5 ? H36D C36' H36E . . 109.5 ? C35' C36' H36F . . 109.5 ? H36D C36' H36F . . 109.5 ? H36E C36' H36F . . 109.5 ? Cl2S C1S Cl3S . . 113.8(4) ? Cl2S C1S H1SA . . 108.8 ? Cl3S C1S H1SA . . 108.8 ? Cl2S C1S H1SB . . 108.8 ? Cl3S C1S H1SB . . 108.8 ? H1SA C1S H1SB . . 107.7 ? F3R B1R F4R . . 111.6(5) ? F3R B1R F2R . . 109.8(4) ? F4R B1R F2R . . 110.8(5) ? F3R B1R F5R . . 108.6(5) ? F4R B1R F5R . . 108.4(4) ? F2R B1R F5R . . 107.5(4) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Au1 C3 . 2.041(5) ? Au1 C21 . 2.043(5) ? Au1 C14 . 2.068(5) ? Au1 Cl2 . 2.3519(11) ? N4 C3 . 1.337(6) ? N4 C5 . 1.393(6) ? N4 C29 . 1.490(6) ? N11 C3 . 1.351(6) ? N11 C10 . 1.396(6) ? N11 C12 . 1.463(6) ? N20 C21 . 1.350(6) ? N20 C28 . 1.392(6) ? N20 C19 . 1.466(6) ? N22 C21 . 1.334(6) ? N22 C23 . 1.391(6) ? N22 C33 . 1.466(7) ? C5 C10 . 1.388(7) ? C5 C6 . 1.398(7) ? C6 C7 . 1.384(7) ? C6 H6 . 0.95 ? C7 C8 . 1.400(7) ? C7 H7 . 0.95 ? C8 C9 . 1.388(7) ? C8 H8 . 0.95 ? C9 C10 . 1.389(6) ? C9 H9 . 0.95 ? C12 C13 . 1.510(6) ? C12 H12A . 0.99 ? C12 H12B . 0.99 ? C13 C14 . 1.375(6) ? C13 C18 . 1.398(7) ? C14 C15 . 1.377(6) ? C15 C16 . 1.382(7) ? C15 C19 . 1.515(6) ? C16 C17 . 1.389(7) ? C16 H16 . 0.95 ? C17 C18 . 1.379(7) ? C17 H17 . 0.95 ? C18 H18 . 0.95 ? C19 H19A . 0.99 ? C19 H19B . 0.99 ? C23 C28 . 1.392(7) ? C23 C24 . 1.393(7) ? C24 C25 . 1.376(8) ? C24 H24 . 0.95 ? C25 C26 . 1.401(9) ? C25 H25 . 0.95 ? C26 C27 . 1.386(8) ? C26 H26 . 0.95 ? C27 C28 . 1.387(7) ? C27 H27 . 0.95 ? C29 C30 . 1.528(8) ? C29 H29A . 0.99 ? C29 H29B . 0.99 ? C30 C31 . 1.522(8) ? C30 H30A . 0.99 ? C30 H30B . 0.99 ? C31 C32 . 1.491(9) ? C31 H31A . 0.99 ? C31 H31B . 0.99 ? C32 H32A . 0.98 ? C32 H32B . 0.98 ? C32 H32C . 0.98 ? C33 C34 . 1.489(9) ? C33 H33A . 0.99 ? C33 H33B . 0.99 ? C34 C35 . 1.339(13) ? C34 C35' . 1.741(19) ? C34 H31C . 0.99 ? C34 H31D . 0.99 ? C34 H31E . 0.99 ? C34 H31F . 0.99 ? C35 C36 . 1.514(14) ? C35 H35A . 0.99 ? C35 H35B . 0.99 ? C36 H36A . 0.98 ? C36 H36B . 0.98 ? C36 H36C . 0.98 ? C35' C36' . 1.47(3) ? C35' H35C . 0.99 ? C35' H35D . 0.99 ? C36' H36D . 0.98 ? C36' H36E . 0.98 ? C36' H36F . 0.98 ? Cl2S C1S . 1.722(7) ? Cl3S C1S . 1.750(7) ? C1S H1SA . 0.99 ? C1S H1SB . 0.99 ? F2R B1R . 1.388(7) ? F3R B1R . 1.372(7) ? F4R B1R . 1.374(6) ? F5R B1R . 1.421(7) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C5 N4 C3 N11 . . . . -0.3(5) ? C29 N4 C3 N11 . . . . 179.6(4) ? C5 N4 C3 Au1 . . . . -176.8(3) ? C29 N4 C3 Au1 . . . . 3.1(7) ? C10 N11 C3 N4 . . . . 0.3(5) ? C12 N11 C3 N4 . . . . -173.0(4) ? C10 N11 C3 Au1 . . . . 177.4(3) ? C12 N11 C3 Au1 . . . . 4.0(6) ? C3 N4 C5 C10 . . . . 0.1(5) ? C29 N4 C5 C10 . . . . -179.8(4) ? C3 N4 C5 C6 . . . . 178.7(5) ? C29 N4 C5 C6 . . . . -1.2(8) ? C10 C5 C6 C7 . . . . -1.3(7) ? N4 C5 C6 C7 . . . . -179.8(5) ? C5 C6 C7 C8 . . . . 1.2(7) ? C6 C7 C8 C9 . . . . -0.7(8) ? C7 C8 C9 C10 . . . . 0.4(7) ? N4 C5 C10 C9 . . . . 179.8(4) ? C6 C5 C10 C9 . . . . 1.1(7) ? N4 C5 C10 N11 . . . . 0.1(5) ? C6 C5 C10 N11 . . . . -178.7(4) ? C8 C9 C10 C5 . . . . -0.6(7) ? C8 C9 C10 N11 . . . . 179.2(5) ? C3 N11 C10 C5 . . . . -0.2(5) ? C12 N11 C10 C5 . . . . 172.7(4) ? C3 N11 C10 C9 . . . . -180.0(5) ? C12 N11 C10 C9 . . . . -7.0(8) ? C3 N11 C12 C13 . . . . 51.7(6) ? C10 N11 C12 C13 . . . . -120.4(5) ? N11 C12 C13 C14 . . . . -52.4(6) ? N11 C12 C13 C18 . . . . 124.0(5) ? C18 C13 C14 C15 . . . . 1.1(7) ? C12 C13 C14 C15 . . . . 177.5(4) ? C18 C13 C14 Au1 . . . . -178.1(3) ? C12 C13 C14 Au1 . . . . -1.7(6) ? C13 C14 C15 C16 . . . . -2.8(7) ? Au1 C14 C15 C16 . . . . 176.4(3) ? C13 C14 C15 C19 . . . . 178.8(4) ? Au1 C14 C15 C19 . . . . -2.0(6) ? C14 C15 C16 C17 . . . . 2.5(7) ? C19 C15 C16 C17 . . . . -179.0(5) ? C15 C16 C17 C18 . . . . -0.6(8) ? C16 C17 C18 C13 . . . . -1.1(7) ? C14 C13 C18 C17 . . . . 0.9(7) ? C12 C13 C18 C17 . . . . -175.6(4) ? C21 N20 C19 C15 . . . . 50.0(6) ? C28 N20 C19 C15 . . . . -122.7(5) ? C14 C15 C19 N20 . . . . -51.8(6) ? C16 C15 C19 N20 . . . . 129.7(5) ? C23 N22 C21 N20 . . . . -0.6(5) ? C33 N22 C21 N20 . . . . 173.7(5) ? C23 N22 C21 Au1 . . . . -179.0(4) ? C33 N22 C21 Au1 . . . . -4.7(8) ? C28 N20 C21 N22 . . . . 1.2(5) ? C19 N20 C21 N22 . . . . -172.6(4) ? C28 N20 C21 Au1 . . . . 179.8(3) ? C19 N20 C21 Au1 . . . . 6.0(6) ? C21 N22 C23 C28 . . . . -0.2(6) ? C33 N22 C23 C28 . . . . -174.6(5) ? C21 N22 C23 C24 . . . . -179.7(5) ? C33 N22 C23 C24 . . . . 5.8(9) ? N22 C23 C24 C25 . . . . 178.8(5) ? C28 C23 C24 C25 . . . . -0.7(8) ? C23 C24 C25 C26 . . . . 0.0(8) ? C24 C25 C26 C27 . . . . 0.6(9) ? C25 C26 C27 C28 . . . . -0.4(8) ? C26 C27 C28 N20 . . . . -179.8(5) ? C26 C27 C28 C23 . . . . -0.4(8) ? C21 N20 C28 C27 . . . . 178.2(5) ? C19 N20 C28 C27 . . . . -8.3(9) ? C21 N20 C28 C23 . . . . -1.2(5) ? C19 N20 C28 C23 . . . . 172.3(4) ? N22 C23 C28 C27 . . . . -178.7(5) ? C24 C23 C28 C27 . . . . 0.9(8) ? N22 C23 C28 N20 . . . . 0.8(5) ? C24 C23 C28 N20 . . . . -179.5(5) ? C3 N4 C29 C30 . . . . 110.9(5) ? C5 N4 C29 C30 . . . . -69.2(6) ? N4 C29 C30 C31 . . . . 175.8(4) ? C29 C30 C31 C32 . . . . 78.7(6) ? C21 N22 C33 C34 . . . . -90.5(7) ? C23 N22 C33 C34 . . . . 83.0(7) ? N22 C33 C34 C35 . . . . 70.8(9) ? N22 C33 C34 C35' . . . . 143.4(8) ? C33 C34 C35 C36 . . . . 74.5(10) ? C33 C34 C35' C36' . . . . -48.(2) ?