#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:41:39 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296393 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572744.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572744 loop_ _publ_author_name 'Valdés, Hugo' 'Alpuente, Nora' 'Salvador, Pedro' 'Hashmi, A Stephen K' 'Ribas, Xavi' _publ_section_title ; CCC-NHC Au(iii) pincer complexes as a reliable platform for isolating elusive species. ; _journal_issue 42 _journal_name_full 'Chemical science' _journal_page_first 17618 _journal_page_last 17628 _journal_paper_doi 10.1039/d4sc02999b _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C56 H60 Au2 N8, 2(B F4), 6(C H2 Cl2)' _chemical_formula_sum 'C62 H72 Au2 B2 Cl12 F8 N8' _chemical_formula_weight 1922.22 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_update_record ; 2024-02-20 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 87.440(4) _cell_angle_beta 88.406(4) _cell_angle_gamma 74.202(4) _cell_formula_units_Z 1 _cell_length_a 10.5400(13) _cell_length_b 13.2869(19) _cell_length_c 13.5269(18) _cell_measurement_reflns_used 9765 _cell_measurement_temperature 100.(2) _cell_measurement_theta_max 28.1725 _cell_measurement_theta_min 2.6129 _cell_volume 1820.7(4) _computing_cell_refinement 'SAINT V8.40B (Bruker AXS LLC, 2019)' _computing_data_collection 'Bruker Instrument Service vV6.2.16' _computing_data_reduction 'SAINT V8.40B (Bruker AXS LLC, 2019)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 1365)' _computing_structure_refinement 'SHELXL-2019/1 (Sheldrick, 2019)' _computing_structure_solution 'XT, VERSION 2018/2' _diffrn_ambient_temperature 100.(2) _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'D8 QUEST ECO' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'doubly curved silicon crystal Bruker Triumph' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0720 _diffrn_reflns_av_unetI/netI 0.0418 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 81153 _diffrn_reflns_theta_full 25.24 _diffrn_reflns_theta_max 28.38 _diffrn_reflns_theta_min 2.20 _diffrn_source_current 20.0 _diffrn_source_power 1.00 _diffrn_source_type 'Ceramic x-ray tube' _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 4.530 _exptl_absorpt_correction_T_max 0.81 _exptl_absorpt_correction_T_min 0.56 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Krause, L., Herbst-Irmer, R., Sheldrick, G. M., Stalke, D. (2015). "Comparison of silver and molybdenum microfocus X-ray sources for single-crystal structure determination" J. Appl. Cryst. 48, 3-10. doi:10.1107/S1600576714022985 ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.753 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 944 _exptl_crystal_size_max 0.240 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.050 _refine_diff_density_max 2.072 _refine_diff_density_min -2.660 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.059 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 442 _refine_ls_number_reflns 9086 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.059 _refine_ls_R_factor_all 0.0562 _refine_ls_R_factor_gt 0.0417 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0431P)^2^+9.8439P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0946 _refine_ls_wR_factor_ref 0.1025 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7751 _reflns_number_total 9086 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc02999b3.cif _cod_data_source_block HV2_105 _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'Multi-Scan' was changed to 'multi-scan' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas Adding full bibliography for 1572736--1572746.cif. ; _cod_database_code 1572744 _shelx_res_file ; TITL HV2_105_0m_a.res in P-1 HV2_105_0m_a.res created by SHELXL-2019/1 at 12:26:16 on 24-Oct-2023 REM Old TITL HV2_105_0m in P1 REM SHELXT solution in P-1: R1 0.105, Rweak 0.012, Alpha 0.032 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C30 Au B3 F7 N5 CELL 0.71073 10.5400 13.2869 13.5269 87.440 88.406 74.202 ZERR 1.000 0.0013 0.0019 0.0018 0.004 0.004 0.004 LATT 1 SFAC C H AU B F N Cl UNIT 62 72 2 2 8 8 12 OMIT 1 1 1 OMIT 0 1 1 OMIT -1 -1 1 OMIT 0 -1 1 OMIT 1 0 1 TEMP -173.150 SIZE 0.05 0.12 0.24 L.S. 10 BOND $h conf acta LIST 6 FMAP 2 PLAN 20 eadp c1' c1n WGHT 0.043100 9.843901 FVAR 0.37237 0.41826 0.59517 CL2L 7 0.379725 0.497813 0.690654 11.00000 0.02865 0.08839 = 0.04837 -0.02793 -0.00201 -0.01260 CL3L 7 0.576250 0.538569 0.817959 11.00000 0.03508 0.08053 = 0.04905 -0.02306 -0.01314 -0.01038 part 1 31 C1L 1 0.536667 0.516069 0.698152 31.00000 0.03655 0.10082 = 0.04248 -0.01096 -0.00367 -0.02656 AFIX 23 H1LA 2 0.542015 0.576354 0.654089 31.00000 -1.20000 H1LB 2 0.602480 0.453218 0.674166 31.00000 -1.20000 AFIX 0 part 2 -31 C1" 1 0.537961 0.446102 0.737277 -31.00000 0.03060 0.03972 = 0.03011 -0.01110 -0.00911 -0.00464 AFIX 23 H1"A 2 0.603075 0.431599 0.681972 -31.00000 -1.20000 H1"B 2 0.542789 0.379395 0.774610 -31.00000 -1.20000 AFIX 0 part 0 AU1 3 0.015104 0.243469 0.273414 11.00000 0.02094 0.02059 = 0.01878 -0.00507 -0.00008 -0.00492 N3 6 0.168960 0.319127 0.101321 11.00000 0.01880 0.02123 = 0.01981 -0.00477 -0.00126 -0.00382 N10 6 0.039281 0.445536 0.181611 11.00000 0.01777 0.02227 = 0.01699 -0.00507 -0.00120 -0.00646 N19 6 0.040035 0.840553 0.526689 11.00000 0.02368 0.01585 = 0.01762 -0.00454 -0.00116 -0.00514 N26 6 0.158531 0.889463 0.634426 11.00000 0.02379 0.01744 = 0.02363 -0.00611 -0.00146 -0.00653 C2 1 0.082598 0.340416 0.178550 11.00000 0.01558 0.02565 = 0.01781 -0.00624 -0.00183 -0.00375 C4 1 0.178912 0.411754 0.054382 11.00000 0.01892 0.02757 = 0.01655 -0.00354 -0.00298 -0.00836 C5 1 0.251726 0.432844 -0.028574 11.00000 0.02147 0.03604 = 0.02139 -0.00648 -0.00092 -0.00694 AFIX 43 H5 2 0.307735 0.378331 -0.065269 11.00000 -1.20000 AFIX 0 C6 1 0.237723 0.536539 -0.053921 11.00000 0.02715 0.03962 = 0.02098 0.00173 -0.00247 -0.01309 AFIX 43 H6 2 0.285662 0.553865 -0.109614 11.00000 -1.20000 AFIX 0 C7 1 0.155757 0.617122 -0.000870 11.00000 0.03096 0.03104 = 0.02517 0.00012 -0.00879 -0.01402 AFIX 43 H7 2 0.149738 0.687632 -0.021131 11.00000 -1.20000 AFIX 0 C8 1 0.083569 0.597306 0.079803 11.00000 0.02634 0.02700 = 0.02425 -0.00329 -0.00848 -0.00861 AFIX 43 H8 2 0.027233 0.652269 0.115796 11.00000 -1.20000 AFIX 0 C9 1 0.096900 0.492890 0.106288 11.00000 0.01827 0.03054 = 0.01534 -0.00481 -0.00456 -0.00987 C11 1 -0.052803 0.504030 0.254903 11.00000 0.01389 0.02744 = 0.01876 -0.00635 -0.00062 -0.00585 AFIX 23 H11A 2 -0.103320 0.457920 0.286213 11.00000 -1.20000 H11B 2 -0.116251 0.563554 0.220968 11.00000 -1.20000 AFIX 0 C12 1 0.015295 0.545386 0.334606 11.00000 0.01676 0.02039 = 0.01753 -0.00100 -0.00247 -0.00739 C13 1 0.128718 0.483066 0.378257 11.00000 0.02638 0.01839 = 0.02523 -0.00380 -0.00230 -0.00402 AFIX 43 H13 2 0.167777 0.414886 0.355193 11.00000 -1.20000 AFIX 0 C14 1 0.185486 0.519624 0.455350 11.00000 0.01996 0.02019 = 0.02908 -0.00373 -0.00822 0.00045 AFIX 43 H14 2 0.262511 0.476122 0.485603 11.00000 -1.20000 AFIX 0 C15 1 0.130421 0.618896 0.488165 11.00000 0.02122 0.02261 = 0.01620 -0.00572 -0.00383 -0.00586 AFIX 43 H15 2 0.169944 0.643543 0.540960 11.00000 -1.20000 AFIX 0 C16 1 0.018269 0.683049 0.445104 11.00000 0.02035 0.01693 = 0.01800 -0.00306 0.00068 -0.00731 C17 1 -0.039453 0.646062 0.367218 11.00000 0.01479 0.01810 = 0.01611 -0.00173 0.00072 -0.00406 AFIX 43 H17 2 -0.116074 0.689830 0.336672 11.00000 -1.20000 AFIX 0 C18 1 -0.049718 0.790598 0.482301 11.00000 0.01991 0.02096 = 0.02263 -0.00542 -0.00509 -0.00372 AFIX 23 H18A 2 -0.094342 0.835741 0.426317 11.00000 -1.20000 H18B 2 -0.118254 0.784213 0.531880 11.00000 -1.20000 AFIX 0 C20 1 0.123019 0.889756 0.473001 11.00000 0.02282 0.01532 = 0.02489 -0.00394 0.00054 -0.00110 C21 1 0.139247 0.904558 0.371955 11.00000 0.03224 0.02441 = 0.02264 -0.00042 -0.00024 -0.00500 AFIX 43 H21 2 0.087853 0.882033 0.325465 11.00000 -1.20000 AFIX 0 C22 1 0.234597 0.954028 0.342585 11.00000 0.04021 0.02511 = 0.02666 0.00001 0.00572 -0.00544 AFIX 43 H22 2 0.250292 0.964867 0.273952 11.00000 -1.20000 AFIX 0 C23 1 0.307710 0.988129 0.410791 11.00000 0.03301 0.02194 = 0.04072 -0.00251 0.00596 -0.01039 AFIX 43 H23 2 0.371065 1.022993 0.387627 11.00000 -1.20000 AFIX 0 C24 1 0.291279 0.972970 0.511474 11.00000 0.02714 0.01660 = 0.03589 -0.00712 -0.00135 -0.00534 AFIX 43 H24 2 0.341570 0.996662 0.557957 11.00000 -1.20000 AFIX 0 C25 1 0.197824 0.921495 0.541429 11.00000 0.02259 0.01671 = 0.02364 -0.00604 0.00049 -0.00195 C27 1 0.064042 0.839529 0.624385 11.00000 0.02035 0.01867 = 0.01986 -0.00332 -0.00134 -0.00308 C28 1 0.246853 0.213184 0.072188 11.00000 0.02758 0.02410 = 0.02545 -0.00665 0.00284 -0.00277 AFIX 13 H28 2 0.301036 0.222527 0.012380 11.00000 -1.20000 AFIX 0 C29 1 0.341648 0.162623 0.154198 11.00000 0.03179 0.03220 = 0.04171 -0.00717 -0.00421 0.00302 AFIX 137 H29A 2 0.398955 0.095845 0.132433 11.00000 -1.50000 H29B 2 0.291475 0.150218 0.213408 11.00000 -1.50000 H29C 2 0.395640 0.209202 0.169635 11.00000 -1.50000 AFIX 0 C30 1 0.159378 0.146583 0.043968 11.00000 0.03758 0.03827 = 0.03979 -0.02078 0.00690 -0.01166 AFIX 137 H30A 2 0.212869 0.083718 0.012364 11.00000 -1.50000 H30B 2 0.092598 0.186601 -0.002274 11.00000 -1.50000 H30C 2 0.115804 0.126137 0.103470 11.00000 -1.50000 AFIX 0 C31 1 0.225668 0.898467 0.727040 11.00000 0.02756 0.03484 = 0.02615 -0.00833 -0.00438 -0.01463 AFIX 13 H31 2 0.288302 0.941492 0.710200 11.00000 -1.20000 AFIX 0 C32 1 0.307836 0.791551 0.762789 11.00000 0.04230 0.05267 = 0.04556 -0.00435 -0.01577 -0.00682 AFIX 137 H32A 2 0.358982 0.799005 0.820092 11.00000 -1.50000 H32B 2 0.368042 0.759078 0.709567 11.00000 -1.50000 H32C 2 0.249650 0.747393 0.781840 11.00000 -1.50000 AFIX 0 C33 1 0.131639 0.955148 0.803563 11.00000 0.04049 0.08096 = 0.03354 -0.03195 -0.00843 0.00050 AFIX 137 H33A 2 0.180768 0.964616 0.861287 11.00000 -1.50000 H33B 2 0.069898 0.914320 0.823584 11.00000 -1.50000 H33C 2 0.082502 1.023731 0.776069 11.00000 -1.50000 AFIX 0 CL2M 7 0.385258 0.234111 0.427628 11.00000 0.03164 0.03801 = 0.09403 -0.00958 -0.01104 -0.00790 CL3M 7 0.576536 0.316978 0.521789 11.00000 0.03691 0.05685 = 0.07220 -0.03217 0.01724 -0.02134 C1M 1 0.447552 0.256474 0.539086 11.00000 0.03095 0.03681 = 0.06239 -0.00085 0.01602 -0.00521 AFIX 23 H1MA 2 0.480653 0.189036 0.576520 11.00000 -1.20000 H1MB 2 0.375838 0.301679 0.578826 11.00000 -1.20000 AFIX 0 CL2N 7 0.827207 0.136383 0.900783 11.00000 0.05260 0.06371 = 0.08405 -0.03747 -0.02117 0.01112 CL3N 7 0.577804 0.265202 0.977615 11.00000 0.04672 0.12831 = 0.06533 -0.01800 0.00127 -0.02097 part 1 21 C1N 1 0.678116 0.234362 0.872797 21.00000 0.07975 0.04629 = 0.05770 0.02133 -0.05496 -0.03348 AFIX 23 H1NA 2 0.699544 0.298193 0.845301 21.00000 -1.20000 H1NB 2 0.629906 0.208952 0.821886 21.00000 -1.20000 AFIX 0 part 2 -21 C1' 1 0.633247 0.156021 0.954990 -21.00000 0.07975 0.04629 = 0.05770 0.02133 -0.05496 -0.03348 AFIX 23 H1'A 2 0.579358 0.135677 0.904692 -21.00000 -1.20000 H1'B 2 0.633590 0.111026 1.015380 -21.00000 -1.20000 AFIX 0 part 0 F2S 5 0.306846 0.131366 0.690518 11.00000 0.07366 0.04383 = 0.03776 -0.01296 -0.00818 -0.01941 F3S 5 0.448717 0.200907 0.760936 11.00000 0.16981 0.36986 = 0.06363 0.02714 -0.03839 -0.20198 F4S 5 0.248457 0.232991 0.819116 11.00000 0.17723 0.06268 = 0.04468 -0.02010 -0.02399 0.05199 F5S 5 0.378307 0.075580 0.847016 11.00000 0.10666 0.06231 = 0.05967 0.00727 -0.02440 0.02657 B1S 4 0.345175 0.156395 0.780036 11.00000 0.04824 0.05227 = 0.02999 -0.00402 -0.00990 -0.01373 HKLF 4 REM HV2_105_0m_a.res in P-1 REM wR2 = 0.1025, GooF = S = 1.059, Restrained GooF = 1.059 for all data REM R1 = 0.0417 for 7751 Fo > 4sig(Fo) and 0.0562 for all 9086 data REM 442 parameters refined using 0 restraints END WGHT 0.0432 9.8440 REM Highest difference peak 2.072, deepest hole -2.660, 1-sigma level 0.171 Q1 1 0.5878 0.1821 0.9808 11.00000 0.05 2.07 Q2 1 0.7122 0.2808 0.7802 11.00000 0.05 2.00 Q3 1 0.4176 0.4298 0.7327 11.00000 0.05 1.47 Q4 1 0.3860 0.2388 0.4880 11.00000 0.05 1.38 Q5 1 0.5389 0.3606 0.4750 11.00000 0.05 1.33 Q6 1 0.6508 0.1422 0.9260 11.00000 0.05 1.21 Q7 1 0.3356 0.2533 0.7705 11.00000 0.05 1.05 Q8 1 0.0791 0.8002 0.7039 11.00000 0.05 0.97 Q9 1 0.0370 0.3025 0.2023 11.00000 0.05 0.96 Q10 1 0.4009 0.0923 0.7058 11.00000 0.05 0.93 Q11 1 -0.0586 0.2750 0.2622 11.00000 0.05 0.92 Q12 1 0.0514 0.7942 0.6595 11.00000 0.05 0.89 Q13 1 0.0133 0.2829 0.2382 11.00000 0.05 0.82 Q14 1 0.3442 0.8439 0.7462 11.00000 0.05 0.80 Q15 1 0.1806 0.1740 0.7926 11.00000 0.05 0.80 Q16 1 0.1166 0.2760 0.2522 11.00000 0.05 0.79 Q17 1 0.1191 0.1953 0.3090 11.00000 0.05 0.78 Q18 1 -0.0485 0.2770 0.1890 11.00000 0.05 0.77 Q19 1 0.4781 0.1149 0.7595 11.00000 0.05 0.74 Q20 1 -0.0976 0.2445 0.2361 11.00000 0.05 0.64 ; _shelx_res_checksum 43788 _shelx_hkl_file ; -2 0 0 2362.96 53.79 -3 0 0 2180.88 56.09 -4 0 0 172.08 16.50 -4 0 0 142.89 15.80 -4 0 0 149.99 17.70 -4 0 0 149.49 15.80 -5 0 0 3781.62 96.59 -5 0 0 3829.12 95.49 -5 0 0 3758.22 96.39 -5 0 0 3868.41 97.39 5 0 0 3972.70 71.49 -6 0 0 511.35 33.20 -6 0 0 520.45 33.10 -6 0 0 535.45 34.30 -6 0 0 459.95 32.80 -6 0 0 492.65 31.00 6 0 0 516.75 13.80 6 0 0 520.25 13.40 -7 0 0 1562.14 61.09 -7 0 0 1457.45 59.59 -7 0 0 1550.54 60.39 -7 0 0 1582.14 62.59 -7 0 0 1533.05 59.39 -8 0 0 216.68 31.10 -8 0 0 246.18 31.50 -8 0 0 271.87 34.30 -8 0 0 209.08 30.40 -8 0 0 217.38 30.50 -9 0 0 133.39 28.50 -9 0 0 128.29 31.40 -9 0 0 116.19 25.40 -9 0 0 73.79 27.50 -9 0 0 74.89 24.80 -9 0 0 78.49 29.90 -10 0 0 118.69 38.50 -10 0 0 85.59 30.20 -10 0 0 186.28 37.90 -11 0 0 35.20 24.50 -11 0 0 68.49 29.70 -12 0 0 98.99 33.80 -12 0 0 63.79 33.00 -13 0 0 -13.30 36.70 -13 0 0 73.09 37.50 -13 1 0 271.87 48.90 -13 1 0 146.69 40.50 -12 1 0 226.28 44.80 -12 1 0 211.18 44.30 -11 1 0 380.96 48.00 -11 1 0 433.16 54.19 -10 1 0 155.68 34.10 -10 1 0 128.19 33.70 -9 1 0 551.54 48.00 -9 1 0 708.53 52.99 -9 1 0 602.44 45.90 -9 1 0 720.13 51.49 -9 1 0 655.13 47.50 -8 1 0 271.07 34.00 -8 1 0 292.97 35.00 -8 1 0 231.88 32.80 -8 1 0 228.68 33.90 -8 1 0 199.18 31.90 -7 1 0 237.08 30.10 -7 1 0 208.48 29.90 -7 1 0 213.88 28.50 -7 1 0 183.18 28.80 -7 1 0 225.28 28.60 -6 1 0 1667.03 60.59 -6 1 0 1711.53 62.59 -6 1 0 1649.33 57.99 5 -1 0 68.69 6.40 5 -1 0 55.59 5.80 -5 1 0 73.49 16.40 -5 1 0 111.99 20.50 -5 1 0 71.79 17.50 4 -1 0 740.73 17.70 4 -1 0 737.23 18.20 -4 1 0 760.52 19.10 -4 1 0 813.92 31.90 -4 1 0 766.42 33.20 -4 1 0 759.42 19.20 3 -1 0 106.59 6.20 3 -1 0 103.19 6.00 -3 1 0 122.29 14.70 -3 1 0 109.19 7.10 -3 1 0 134.99 13.10 -3 1 0 106.19 6.80 2 -1 0 1840.52 38.80 2 -1 0 1917.81 45.00 2 -1 0 1964.30 47.60 2 -1 0 1852.21 38.60 -2 1 0 2023.10 40.10 -2 1 0 1817.12 39.50 -2 1 0 1853.41 46.70 -2 1 0 1898.61 44.90 1 -1 0 19.40 3.20 1 1 0 -1.70 1.40 1 1 0 0.00 0.60 -2 -1 0 879.81 26.00 -2 -1 0 956.60 27.00 -2 -1 0 943.11 25.00 -2 -1 0 928.81 23.40 -2 -1 0 922.71 25.20 -2 -1 0 962.80 26.90 -2 -1 0 949.60 24.10 -2 -1 0 915.21 22.30 2 1 0 874.21 23.60 2 1 0 926.91 23.00 2 1 0 946.51 27.00 2 1 0 918.51 24.90 2 1 0 953.60 25.60 2 1 0 942.31 26.60 -3 -1 0 61.19 4.70 -3 -1 0 48.60 7.80 -3 -1 0 68.19 10.80 -3 -1 0 51.59 6.90 -3 -1 0 39.60 9.20 -3 -1 0 49.70 4.30 -3 -1 0 47.80 8.90 3 1 0 57.09 6.70 3 1 0 49.70 10.20 3 1 0 52.99 10.80 3 1 0 64.79 9.50 3 1 0 53.99 5.50 3 1 0 53.49 5.10 3 1 0 50.49 7.30 -4 -1 0 609.24 21.70 -4 -1 0 636.34 27.70 -4 -1 0 622.24 28.10 -4 -1 0 612.34 28.70 -4 -1 0 645.64 21.10 4 1 0 599.24 19.50 4 1 0 608.74 28.00 4 1 0 642.54 21.80 -5 -1 0 982.90 28.90 -5 -1 0 989.40 41.20 -5 -1 0 886.71 38.00 -5 -1 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51.29 -3 -6 -17 228.58 44.80 -3 -6 -17 167.88 45.50 3 6 17 249.38 57.59 3 6 17 228.68 59.99 3 6 17 183.08 47.10 0 1 -18 -17.20 46.00 1 0 -18 89.69 48.70 0 0 -18 27.50 36.90 0 0 -18 62.69 49.90 0 0 -18 131.19 34.30 0 0 18 70.49 40.00 0 0 18 1.20 47.50 -1 0 -18 120.29 51.49 -1 0 -18 143.49 39.90 1 0 18 213.68 59.19 1 0 18 195.58 44.00 0 -1 -18 29.50 42.10 0 -1 -18 26.70 39.00 0 -1 -18 34.60 31.50 0 1 18 18.50 48.60 0 1 18 37.70 37.20 -1 -1 -18 19.30 44.90 -1 -1 -18 -15.60 30.90 -1 -1 -18 21.80 41.90 1 1 18 75.89 39.50 1 1 18 22.10 49.30 0 -2 -18 90.29 51.49 0 2 18 128.09 59.39 -1 -2 -18 128.29 52.69 -1 -2 -18 212.08 37.40 1 2 18 111.29 53.69 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 11103 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl Cl2L 0.37973(16) 0.49781(18) 0.69065(14) 0.0550(5) Uani d . . . 1.000000 . . Cl Cl3L 0.57625(17) 0.53857(18) 0.81796(14) 0.0550(5) Uani d . . . 1.000000 . . C C1L 0.5367(13) 0.5161(18) 0.6982(11) 0.058(6) Uani d . P . 0.60(3) A 1 H H1LA 0.542015 0.576354 0.654089 0.070000 Uiso calc U P R 0.60(3) A 1 H H1LB 0.602480 0.453218 0.674166 0.070000 Uiso calc U P R 0.60(3) A 1 C C1" 0.5380(15) 0.4461(16) 0.7373(13) 0.034(5) Uani d . P . 0.40(3) A 2 H H1"A 0.603075 0.431599 0.681972 0.041000 Uiso calc U P R 0.40(3) A 2 H H1"B 0.542789 0.379395 0.774610 0.041000 Uiso calc U P R 0.40(3) A 2 Au Au1 0.01510(2) 0.24347(2) 0.27341(2) 0.02012(6) Uani d . . . 1.000000 . . N N3 0.1690(4) 0.3191(3) 0.1013(3) 0.0201(8) Uani d . . . 1.000000 . . N N10 0.0393(4) 0.4455(3) 0.1816(3) 0.0187(8) Uani d . . . 1.000000 . . N N19 0.0400(4) 0.8406(3) 0.5267(3) 0.0190(8) Uani d . . . 1.000000 . . N N26 0.1585(4) 0.8895(3) 0.6344(3) 0.0212(9) Uani d . . . 1.000000 . . C C2 0.0826(5) 0.3404(4) 0.1786(4) 0.0198(10) Uani d . . . 1.000000 . . C C4 0.1789(5) 0.4118(4) 0.0544(4) 0.0205(10) Uani d . . . 1.000000 . . C C5 0.2517(5) 0.4328(5) -0.0286(4) 0.0263(11) Uani d . . . 1.000000 . . H H5 0.307735 0.378331 -0.065269 0.032000 Uiso calc U . R 1.000000 . . C C6 0.2377(5) 0.5365(5) -0.0539(4) 0.0285(12) Uani d . . . 1.000000 . . H H6 0.285662 0.553865 -0.109614 0.034000 Uiso calc U . R 1.000000 . . C C7 0.1558(5) 0.6171(5) -0.0009(4) 0.0278(11) Uani d . . . 1.000000 . . H H7 0.149738 0.687632 -0.021131 0.033000 Uiso calc U . R 1.000000 . . C C8 0.0836(5) 0.5973(4) 0.0798(4) 0.0254(11) Uani d . . . 1.000000 . . H H8 0.027233 0.652269 0.115796 0.030000 Uiso calc U . R 1.000000 . . C C9 0.0969(5) 0.4929(4) 0.1063(3) 0.0205(10) Uani d . . . 1.000000 . . C C11 -0.0528(5) 0.5040(4) 0.2549(4) 0.0198(10) Uani d . . . 1.000000 . . H H11A -0.103320 0.457920 0.286213 0.024000 Uiso calc U . R 1.000000 . . H H11B -0.116251 0.563554 0.220968 0.024000 Uiso calc U . R 1.000000 . . C C12 0.0153(5) 0.5454(4) 0.3346(3) 0.0177(9) Uani d . . . 1.000000 . . C C13 0.1287(5) 0.4831(4) 0.3783(4) 0.0236(10) Uani d . . . 1.000000 . . H H13 0.167777 0.414886 0.355193 0.028000 Uiso calc U . R 1.000000 . . C C14 0.1855(5) 0.5196(4) 0.4554(4) 0.0240(11) Uani d . . . 1.000000 . . H H14 0.262511 0.476122 0.485603 0.029000 Uiso calc U . R 1.000000 . . C C15 0.1304(5) 0.6189(4) 0.4882(3) 0.0198(10) Uani d . . . 1.000000 . . H H15 0.169944 0.643543 0.540960 0.024000 Uiso calc U . R 1.000000 . . C C16 0.0183(5) 0.6830(4) 0.4451(3) 0.0179(9) Uani d . . . 1.000000 . . C C17 -0.0395(5) 0.6461(4) 0.3672(3) 0.0164(9) Uani d . . . 1.000000 . . H H17 -0.116074 0.689830 0.336672 0.020000 Uiso calc U . R 1.000000 . . C C18 -0.0497(5) 0.7906(4) 0.4823(4) 0.0213(10) Uani d . . . 1.000000 . . H H18A -0.094342 0.835741 0.426317 0.026000 Uiso calc U . R 1.000000 . . H H18B -0.118254 0.784213 0.531880 0.026000 Uiso calc U . R 1.000000 . . C C20 0.1230(5) 0.8898(4) 0.4730(4) 0.0217(10) Uani d . . . 1.000000 . . C C21 0.1392(6) 0.9046(4) 0.3720(4) 0.0270(11) Uani d . . . 1.000000 . . H H21 0.087853 0.882033 0.325465 0.032000 Uiso calc U . R 1.000000 . . C C22 0.2346(6) 0.9540(4) 0.3426(4) 0.0315(12) Uani d . . . 1.000000 . . H H22 0.250292 0.964867 0.273952 0.038000 Uiso calc U . R 1.000000 . . C C23 0.3077(6) 0.9881(4) 0.4108(5) 0.0314(12) Uani d . . . 1.000000 . . H H23 0.371065 1.022993 0.387627 0.038000 Uiso calc U . R 1.000000 . . C C24 0.2913(5) 0.9730(4) 0.5115(4) 0.0265(11) Uani d . . . 1.000000 . . H H24 0.341570 0.996662 0.557957 0.032000 Uiso calc U . R 1.000000 . . C C25 0.1978(5) 0.9215(4) 0.5414(4) 0.0215(10) Uani d . . . 1.000000 . . C C27 0.0640(5) 0.8395(4) 0.6244(4) 0.0200(10) Uani d . . . 1.000000 . . C C28 0.2469(5) 0.2132(4) 0.0722(4) 0.0264(11) Uani d . . . 1.000000 . . H H28 0.301036 0.222527 0.012380 0.032000 Uiso calc U . R 1.000000 . . C C29 0.3416(6) 0.1626(5) 0.1542(5) 0.0373(14) Uani d . . . 1.000000 . . H H29A 0.398955 0.095845 0.132433 0.056000 Uiso calc U . R 1.000000 . . H H29B 0.291475 0.150218 0.213408 0.056000 Uiso calc U . R 1.000000 . . H H29C 0.395640 0.209202 0.169635 0.056000 Uiso calc U . R 1.000000 . . C C30 0.1594(6) 0.1466(5) 0.0440(5) 0.0378(14) Uani d . . . 1.000000 . . H H30A 0.212869 0.083718 0.012364 0.057000 Uiso calc U . R 1.000000 . . H H30B 0.092598 0.186601 -0.002274 0.057000 Uiso calc U . R 1.000000 . . H H30C 0.115804 0.126137 0.103470 0.057000 Uiso calc U . R 1.000000 . . C C31 0.2257(5) 0.8985(5) 0.7270(4) 0.0280(12) Uani d . . . 1.000000 . . H H31 0.288302 0.941492 0.710200 0.034000 Uiso calc U . R 1.000000 . . C C32 0.3078(7) 0.7916(6) 0.7628(5) 0.0477(17) Uani d . . . 1.000000 . . H H32A 0.358982 0.799005 0.820092 0.071000 Uiso calc U . R 1.000000 . . H H32B 0.368042 0.759078 0.709567 0.071000 Uiso calc U . R 1.000000 . . H H32C 0.249650 0.747393 0.781840 0.071000 Uiso calc U . R 1.000000 . . C C33 0.1316(7) 0.9551(7) 0.8036(5) 0.054(2) Uani d . . . 1.000000 . . H H33A 0.180768 0.964616 0.861287 0.081000 Uiso calc U . R 1.000000 . . H H33B 0.069898 0.914320 0.823584 0.081000 Uiso calc U . R 1.000000 . . H H33C 0.082502 1.023731 0.776069 0.081000 Uiso calc U . R 1.000000 . . Cl Cl2M 0.38526(17) 0.23411(14) 0.42763(17) 0.0545(5) Uani d . . . 1.000000 . . Cl Cl3M 0.57654(17) 0.31698(16) 0.52179(16) 0.0531(5) Uani d . . . 1.000000 . . C C1M 0.4476(6) 0.2565(5) 0.5391(6) 0.0445(17) Uani d . . . 1.000000 . . H H1MA 0.480653 0.189036 0.576520 0.053000 Uiso calc U . R 1.000000 . . H H1MB 0.375838 0.301679 0.578826 0.053000 Uiso calc U . R 1.000000 . . Cl Cl2N 0.8272(2) 0.13638(18) 0.90078(18) 0.0706(7) Uani d . . . 1.000000 . . Cl Cl3N 0.5778(2) 0.2652(3) 0.97762(18) 0.0803(8) Uani d . . . 1.000000 . . C C1N 0.678(2) 0.2344(14) 0.8728(14) 0.058(3) Uani d . P . 0.418(12) B 1 H H1NA 0.699544 0.298193 0.845301 0.069000 Uiso calc U P R 0.418(12) B 1 H H1NB 0.629906 0.208952 0.821886 0.069000 Uiso calc U P R 0.418(12) B 1 C C1' 0.6332(14) 0.1560(10) 0.9550(10) 0.058(3) Uani d . P . 0.582(12) B 2 H H1'A 0.579358 0.135677 0.904692 0.069000 Uiso calc U P R 0.582(12) B 2 H H1'B 0.633590 0.111026 1.015380 0.069000 Uiso calc U P R 0.582(12) B 2 F F2S 0.3068(5) 0.1314(3) 0.6905(3) 0.0506(10) Uani d . . . 1.000000 . . F F3S 0.4487(9) 0.2009(10) 0.7609(5) 0.176(5) Uani d . . . 1.000000 . . F F4S 0.2485(8) 0.2330(4) 0.8191(4) 0.110(3) Uani d . . . 1.000000 . . F F5S 0.3783(6) 0.0756(4) 0.8470(4) 0.0858(18) Uani d . . . 1.000000 . . B B1S 0.3452(8) 0.1564(7) 0.7800(6) 0.0432(18) Uani d . . . 1.000000 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl2L 0.0287(8) 0.0884(15) 0.0484(10) -0.0126(8) -0.0020(7) -0.0279(10) Cl3L 0.0351(8) 0.0805(14) 0.0490(10) -0.0104(8) -0.0131(7) -0.0231(9) C1L 0.037(7) 0.101(16) 0.042(7) -0.027(8) -0.004(5) -0.011(8) C1" 0.031(8) 0.040(11) 0.030(9) -0.005(7) -0.009(6) -0.011(7) Au1 0.02094(10) 0.02059(10) 0.01878(10) -0.00492(7) -0.00008(6) -0.00507(6) N3 0.019(2) 0.021(2) 0.020(2) -0.0038(16) -0.0013(16) -0.0048(16) N10 0.0178(19) 0.022(2) 0.0170(19) -0.0065(16) -0.0012(15) -0.0051(16) N19 0.024(2) 0.016(2) 0.0176(19) -0.0051(16) -0.0012(16) -0.0045(16) N26 0.024(2) 0.017(2) 0.024(2) -0.0065(17) -0.0015(17) -0.0061(17) C2 0.016(2) 0.026(3) 0.018(2) -0.0038(19) -0.0018(17) -0.0062(19) C4 0.019(2) 0.028(3) 0.017(2) -0.008(2) -0.0030(18) -0.0035(19) C5 0.021(3) 0.036(3) 0.021(2) -0.007(2) -0.0009(19) -0.006(2) C6 0.027(3) 0.040(3) 0.021(2) -0.013(2) -0.002(2) 0.002(2) C7 0.031(3) 0.031(3) 0.025(3) -0.014(2) -0.009(2) 0.000(2) C8 0.026(3) 0.027(3) 0.024(3) -0.009(2) -0.008(2) -0.003(2) C9 0.018(2) 0.031(3) 0.015(2) -0.010(2) -0.0046(17) -0.0048(19) C11 0.014(2) 0.027(3) 0.019(2) -0.0058(19) -0.0006(17) -0.0063(19) C12 0.017(2) 0.020(2) 0.018(2) -0.0074(18) -0.0025(17) -0.0010(18) C13 0.026(3) 0.018(2) 0.025(3) -0.004(2) -0.002(2) -0.004(2) C14 0.020(2) 0.020(3) 0.029(3) 0.0005(19) -0.008(2) -0.004(2) C15 0.021(2) 0.023(3) 0.016(2) -0.0059(19) -0.0038(18) -0.0057(19) C16 0.020(2) 0.017(2) 0.018(2) -0.0073(18) 0.0007(18) -0.0031(18) C17 0.015(2) 0.018(2) 0.016(2) -0.0041(17) 0.0007(16) -0.0017(17) C18 0.020(2) 0.021(3) 0.023(2) -0.0037(19) -0.0051(19) -0.0054(19) C20 0.023(2) 0.015(2) 0.025(2) -0.0011(19) 0.0005(19) -0.0039(19) C21 0.032(3) 0.024(3) 0.023(3) -0.005(2) 0.000(2) 0.000(2) C22 0.040(3) 0.025(3) 0.027(3) -0.005(2) 0.006(2) 0.000(2) C23 0.033(3) 0.022(3) 0.041(3) -0.010(2) 0.006(2) -0.003(2) C24 0.027(3) 0.017(2) 0.036(3) -0.005(2) -0.001(2) -0.007(2) C25 0.023(2) 0.017(2) 0.024(2) -0.0019(19) 0.0005(19) -0.0060(19) C27 0.020(2) 0.019(2) 0.020(2) -0.0031(19) -0.0013(18) -0.0033(19) C28 0.028(3) 0.024(3) 0.025(3) -0.003(2) 0.003(2) -0.007(2) C29 0.032(3) 0.032(3) 0.042(3) 0.003(2) -0.004(3) -0.007(3) C30 0.038(3) 0.038(4) 0.040(3) -0.012(3) 0.007(3) -0.021(3) C31 0.028(3) 0.035(3) 0.026(3) -0.015(2) -0.004(2) -0.008(2) C32 0.042(4) 0.053(4) 0.046(4) -0.007(3) -0.016(3) -0.004(3) C33 0.040(4) 0.081(6) 0.034(3) 0.000(4) -0.008(3) -0.032(4) Cl2M 0.0316(8) 0.0380(9) 0.0940(15) -0.0079(7) -0.0110(9) -0.0096(9) Cl3M 0.0369(9) 0.0569(11) 0.0722(12) -0.0213(8) 0.0172(8) -0.0322(10) C1M 0.031(3) 0.037(4) 0.062(5) -0.005(3) 0.016(3) -0.001(3) Cl2N 0.0526(11) 0.0637(13) 0.0841(15) 0.0111(10) -0.0212(10) -0.0375(12) Cl3N 0.0467(12) 0.128(2) 0.0653(14) -0.0210(13) 0.0013(10) -0.0180(14) C1N 0.080(8) 0.046(6) 0.058(6) -0.033(6) -0.055(6) 0.021(5) C1' 0.080(8) 0.046(6) 0.058(6) -0.033(6) -0.055(6) 0.021(5) F2S 0.074(3) 0.044(2) 0.038(2) -0.019(2) -0.008(2) -0.0130(18) F3S 0.170(8) 0.370(15) 0.064(4) -0.202(10) -0.038(5) 0.027(6) F4S 0.177(7) 0.063(3) 0.045(3) 0.052(4) -0.024(3) -0.020(3) F5S 0.107(4) 0.062(3) 0.060(3) 0.027(3) -0.024(3) 0.007(3) B1S 0.048(4) 0.052(5) 0.030(4) -0.014(4) -0.010(3) -0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag Cl2L C1L Cl3L . . 112.9(8) ? Cl2L C1L H1LA . . 109.000000 ? Cl3L C1L H1LA . . 109.000000 ? Cl2L C1L H1LB . . 109.000000 ? Cl3L C1L H1LB . . 109.000000 ? H1LA C1L H1LB . . 107.800000 ? Cl2L C1" Cl3L . . 109.6(9) ? Cl2L C1" H1"A . . 109.800000 ? Cl3L C1" H1"A . . 109.800000 ? Cl2L C1" H1"B . . 109.800000 ? Cl3L C1" H1"B . . 109.800000 ? H1"A C1" H1"B . . 108.200000 ? C2 Au1 C27 . 2_566 173.82(19) ? C2 N3 C4 . . 109.9(4) ? C2 N3 C28 . . 125.9(4) ? C4 N3 C28 . . 124.1(4) ? C2 N10 C9 . . 110.8(4) ? C2 N10 C11 . . 125.9(4) ? C9 N10 C11 . . 123.3(4) ? C27 N19 C20 . . 109.8(4) ? C27 N19 C18 . . 125.7(4) ? C20 N19 C18 . . 124.3(4) ? C27 N26 C25 . . 110.0(4) ? C27 N26 C31 . . 126.5(4) ? C25 N26 C31 . . 123.1(4) ? N10 C2 N3 . . 106.7(4) ? N10 C2 Au1 . . 122.5(3) ? N3 C2 Au1 . . 130.7(4) ? N3 C4 C9 . . 106.8(4) ? N3 C4 C5 . . 132.6(5) ? C9 C4 C5 . . 120.6(5) ? C6 C5 C4 . . 116.4(5) ? C6 C5 H5 . . 121.800000 ? C4 C5 H5 . . 121.800000 ? C5 C6 C7 . . 122.3(5) ? C5 C6 H6 . . 118.800000 ? C7 C6 H6 . . 118.800000 ? C8 C7 C6 . . 121.7(5) ? C8 C7 H7 . . 119.200000 ? C6 C7 H7 . . 119.200000 ? C7 C8 C9 . . 116.6(5) ? C7 C8 H8 . . 121.700000 ? C9 C8 H8 . . 121.700000 ? N10 C9 C8 . . 131.9(5) ? N10 C9 C4 . . 105.8(4) ? C8 C9 C4 . . 122.3(5) ? N10 C11 C12 . . 112.9(4) ? N10 C11 H11A . . 109.000000 ? C12 C11 H11A . . 109.000000 ? N10 C11 H11B . . 109.000000 ? C12 C11 H11B . . 109.000000 ? H11A C11 H11B . . 107.800000 ? C13 C12 C17 . . 119.4(4) ? C13 C12 C11 . . 121.0(4) ? C17 C12 C11 . . 119.6(4) ? C14 C13 C12 . . 120.4(5) ? C14 C13 H13 . . 119.800000 ? C12 C13 H13 . . 119.800000 ? C15 C14 C13 . . 120.1(5) ? C15 C14 H14 . . 120.000000 ? C13 C14 H14 . . 120.000000 ? C14 C15 C16 . . 120.7(4) ? C14 C15 H15 . . 119.700000 ? C16 C15 H15 . . 119.700000 ? C15 C16 C17 . . 119.3(4) ? C15 C16 C18 . . 122.4(4) ? C17 C16 C18 . . 118.2(4) ? C12 C17 C16 . . 120.1(4) ? C12 C17 H17 . . 119.900000 ? C16 C17 H17 . . 119.900000 ? N19 C18 C16 . . 113.2(4) ? N19 C18 H18A . . 108.900000 ? C16 C18 H18A . . 108.900000 ? N19 C18 H18B . . 108.900000 ? C16 C18 H18B . . 108.900000 ? H18A C18 H18B . . 107.800000 ? C25 C20 C21 . . 122.5(5) ? C25 C20 N19 . . 106.6(4) ? C21 C20 N19 . . 130.8(5) ? C22 C21 C20 . . 116.2(5) ? C22 C21 H21 . . 121.900000 ? C20 C21 H21 . . 121.900000 ? C21 C22 C23 . . 121.6(5) ? C21 C22 H22 . . 119.200000 ? C23 C22 H22 . . 119.200000 ? C24 C23 C22 . . 122.0(5) ? C24 C23 H23 . . 119.000000 ? C22 C23 H23 . . 119.000000 ? C23 C24 C25 . . 116.8(5) ? C23 C24 H24 . . 121.600000 ? C25 C24 H24 . . 121.600000 ? C20 C25 C24 . . 121.0(5) ? C20 C25 N26 . . 106.3(4) ? C24 C25 N26 . . 132.7(5) ? N19 C27 N26 . . 107.2(4) ? N19 C27 Au1 . 2_566 122.4(4) ? N26 C27 Au1 . 2_566 129.8(4) ? N3 C28 C30 . . 111.9(5) ? N3 C28 C29 . . 109.4(4) ? C30 C28 C29 . . 113.0(5) ? N3 C28 H28 . . 107.400000 ? C30 C28 H28 . . 107.400000 ? C29 C28 H28 . . 107.400000 ? C28 C29 H29A . . 109.500000 ? C28 C29 H29B . . 109.500000 ? H29A C29 H29B . . 109.500000 ? C28 C29 H29C . . 109.500000 ? H29A C29 H29C . . 109.500000 ? H29B C29 H29C . . 109.500000 ? C28 C30 H30A . . 109.500000 ? C28 C30 H30B . . 109.500000 ? H30A C30 H30B . . 109.500000 ? C28 C30 H30C . . 109.500000 ? H30A C30 H30C . . 109.500000 ? H30B C30 H30C . . 109.500000 ? N26 C31 C33 . . 112.1(5) ? N26 C31 C32 . . 110.0(5) ? C33 C31 C32 . . 113.6(6) ? N26 C31 H31 . . 106.900000 ? C33 C31 H31 . . 106.900000 ? C32 C31 H31 . . 106.900000 ? C31 C32 H32A . . 109.500000 ? C31 C32 H32B . . 109.500000 ? H32A C32 H32B . . 109.500000 ? C31 C32 H32C . . 109.500000 ? H32A C32 H32C . . 109.500000 ? H32B C32 H32C . . 109.500000 ? C31 C33 H33A . . 109.500000 ? C31 C33 H33B . . 109.500000 ? H33A C33 H33B . . 109.500000 ? C31 C33 H33C . . 109.500000 ? H33A C33 H33C . . 109.500000 ? H33B C33 H33C . . 109.500000 ? Cl2M C1M Cl3M . . 111.9(4) ? Cl2M C1M H1MA . . 109.200000 ? Cl3M C1M H1MA . . 109.200000 ? Cl2M C1M H1MB . . 109.200000 ? Cl3M C1M H1MB . . 109.200000 ? H1MA C1M H1MB . . 107.900000 ? Cl3N C1N Cl2N . . 111.4(9) ? Cl3N C1N H1NA . . 109.300000 ? Cl2N C1N H1NA . . 109.300000 ? Cl3N C1N H1NB . . 109.300000 ? Cl2N C1N H1NB . . 109.300000 ? H1NA C1N H1NB . . 108.000000 ? Cl3N C1' Cl2N . . 108.5(7) ? Cl3N C1' H1'A . . 110.000000 ? Cl2N C1' H1'A . . 110.000000 ? Cl3N C1' H1'B . . 110.000000 ? Cl2N C1' H1'B . . 110.000000 ? H1'A C1' H1'B . . 108.400000 ? F4S B1S F5S . . 108.6(7) ? F4S B1S F2S . . 109.7(6) ? F5S B1S F2S . . 114.7(7) ? F4S B1S F3S . . 105.0(9) ? F5S B1S F3S . . 111.6(8) ? F2S B1S F3S . . 106.8(6) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Cl2L C1L . 1.742(13) ? Cl2L C1" . 1.746(15) ? Cl3L C1L . 1.743(13) ? Cl3L C1" . 1.810(15) ? C1L H1LA . 0.990000 ? C1L H1LB . 0.990000 ? C1" H1"A . 0.990000 ? C1" H1"B . 0.990000 ? Au1 C2 . 2.028(5) ? Au1 C27 2_566 2.031(5) ? N3 C2 . 1.354(6) ? N3 C4 . 1.388(7) ? N3 C28 . 1.488(7) ? N10 C2 . 1.348(7) ? N10 C9 . 1.385(6) ? N10 C11 . 1.461(6) ? N19 C27 . 1.351(6) ? N19 C20 . 1.398(7) ? N19 C18 . 1.451(6) ? N26 C27 . 1.351(6) ? N26 C25 . 1.398(7) ? N26 C31 . 1.481(6) ? C4 C9 . 1.389(7) ? C4 C5 . 1.403(7) ? C5 C6 . 1.374(8) ? C5 H5 . 0.950000 ? C6 C7 . 1.392(8) ? C6 H6 . 0.950000 ? C7 C8 . 1.370(8) ? C7 H7 . 0.950000 ? C8 C9 . 1.387(8) ? C8 H8 . 0.950000 ? C11 C12 . 1.513(6) ? C11 H11A . 0.990000 ? C11 H11B . 0.990000 ? C12 C13 . 1.386(7) ? C12 C17 . 1.391(7) ? C13 C14 . 1.386(7) ? C13 H13 . 0.950000 ? C14 C15 . 1.377(7) ? C14 H14 . 0.950000 ? C15 C16 . 1.381(7) ? C15 H15 . 0.950000 ? C16 C17 . 1.402(6) ? C16 C18 . 1.515(7) ? C17 H17 . 0.950000 ? C18 H18A . 0.990000 ? C18 H18B . 0.990000 ? C20 C25 . 1.383(7) ? C20 C21 . 1.385(7) ? C21 C22 . 1.383(8) ? C21 H21 . 0.950000 ? C22 C23 . 1.385(9) ? C22 H22 . 0.950000 ? C23 C24 . 1.381(8) ? C23 H23 . 0.950000 ? C24 C25 . 1.386(7) ? C24 H24 . 0.950000 ? C28 C30 . 1.508(8) ? C28 C29 . 1.520(8) ? C28 H28 . 1.000000 ? C29 H29A . 0.980000 ? C29 H29B . 0.980000 ? C29 H29C . 0.980000 ? C30 H30A . 0.980000 ? C30 H30B . 0.980000 ? C30 H30C . 0.980000 ? C31 C33 . 1.492(8) ? C31 C32 . 1.515(9) ? C31 H31 . 1.000000 ? C32 H32A . 0.980000 ? C32 H32B . 0.980000 ? C32 H32C . 0.980000 ? C33 H33A . 0.980000 ? C33 H33B . 0.980000 ? C33 H33C . 0.980000 ? Cl2M C1M . 1.730(8) ? Cl3M C1M . 1.763(7) ? C1M H1MA . 0.990000 ? C1M H1MB . 0.990000 ? Cl2N C1N . 1.784(18) ? Cl2N C1' . 2.104(16) ? Cl3N C1' . 1.452(14) ? Cl3N C1N . 1.74(2) ? C1N H1NA . 0.990000 ? C1N H1NB . 0.990000 ? C1' H1'A . 0.990000 ? C1' H1'B . 0.990000 ? F2S B1S . 1.370(8) ? F3S B1S . 1.389(11) ? F4S B1S . 1.344(10) ? F5S B1S . 1.350(10) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C9 N10 C2 N3 . . . . 0.2(5) ? C11 N10 C2 N3 . . . . -178.2(4) ? C9 N10 C2 Au1 . . . . -177.4(3) ? C11 N10 C2 Au1 . . . . 4.2(6) ? C4 N3 C2 N10 . . . . -0.8(5) ? C28 N3 C2 N10 . . . . 176.9(4) ? C4 N3 C2 Au1 . . . . 176.5(4) ? C28 N3 C2 Au1 . . . . -5.8(7) ? C2 N3 C4 C9 . . . . 1.1(5) ? C28 N3 C4 C9 . . . . -176.6(4) ? C2 N3 C4 C5 . . . . -179.0(5) ? C28 N3 C4 C5 . . . . 3.3(8) ? N3 C4 C5 C6 . . . . -179.4(5) ? C9 C4 C5 C6 . . . . 0.5(7) ? C4 C5 C6 C7 . . . . -0.1(8) ? C5 C6 C7 C8 . . . . -0.3(8) ? C6 C7 C8 C9 . . . . 0.4(8) ? C2 N10 C9 C8 . . . . 180.0(5) ? C11 N10 C9 C8 . . . . -1.6(8) ? C2 N10 C9 C4 . . . . 0.4(5) ? C11 N10 C9 C4 . . . . 178.9(4) ? C7 C8 C9 N10 . . . . -179.5(5) ? C7 C8 C9 C4 . . . . 0.0(7) ? N3 C4 C9 N10 . . . . -0.9(5) ? C5 C4 C9 N10 . . . . 179.1(4) ? N3 C4 C9 C8 . . . . 179.5(4) ? C5 C4 C9 C8 . . . . -0.5(7) ? C2 N10 C11 C12 . . . . 100.6(5) ? C9 N10 C11 C12 . . . . -77.6(6) ? N10 C11 C12 C13 . . . . -44.0(7) ? N10 C11 C12 C17 . . . . 138.5(5) ? C17 C12 C13 C14 . . . . 1.6(8) ? C11 C12 C13 C14 . . . . -176.0(5) ? C12 C13 C14 C15 . . . . -0.9(8) ? C13 C14 C15 C16 . . . . 0.1(8) ? C14 C15 C16 C17 . . . . 0.0(7) ? C14 C15 C16 C18 . . . . 176.7(5) ? C13 C12 C17 C16 . . . . -1.4(7) ? C11 C12 C17 C16 . . . . 176.2(4) ? C15 C16 C17 C12 . . . . 0.6(7) ? C18 C16 C17 C12 . . . . -176.2(4) ? C27 N19 C18 C16 . . . . -95.9(6) ? C20 N19 C18 C16 . . . . 78.5(6) ? C15 C16 C18 N19 . . . . 29.8(7) ? C17 C16 C18 N19 . . . . -153.5(4) ? C27 N19 C20 C25 . . . . -1.3(5) ? C18 N19 C20 C25 . . . . -176.4(4) ? C27 N19 C20 C21 . . . . 176.3(5) ? C18 N19 C20 C21 . . . . 1.2(8) ? C25 C20 C21 C22 . . . . -0.5(8) ? N19 C20 C21 C22 . . . . -177.8(5) ? C20 C21 C22 C23 . . . . -1.0(8) ? C21 C22 C23 C24 . . . . 1.2(9) ? C22 C23 C24 C25 . . . . 0.1(8) ? C21 C20 C25 C24 . . . . 1.9(8) ? N19 C20 C25 C24 . . . . 179.7(4) ? C21 C20 C25 N26 . . . . -177.3(5) ? N19 C20 C25 N26 . . . . 0.6(5) ? C23 C24 C25 C20 . . . . -1.6(8) ? C23 C24 C25 N26 . . . . 177.2(5) ? C27 N26 C25 C20 . . . . 0.3(6) ? C31 N26 C25 C20 . . . . 173.1(5) ? C27 N26 C25 C24 . . . . -178.7(5) ? C31 N26 C25 C24 . . . . -5.9(9) ? C20 N19 C27 N26 . . . . 1.5(5) ? C18 N19 C27 N26 . . . . 176.6(4) ? C20 N19 C27 Au1 . . . 2_566 -170.6(3) ? C18 N19 C27 Au1 . . . 2_566 4.5(7) ? C25 N26 C27 N19 . . . . -1.1(6) ? C31 N26 C27 N19 . . . . -173.6(5) ? C25 N26 C27 Au1 . . . 2_566 170.2(4) ? C31 N26 C27 Au1 . . . 2_566 -2.3(7) ? C2 N3 C28 C30 . . . . 61.9(7) ? C4 N3 C28 C30 . . . . -120.7(5) ? C2 N3 C28 C29 . . . . -64.0(7) ? C4 N3 C28 C29 . . . . 113.3(5) ? C27 N26 C31 C33 . . . . -61.7(8) ? C25 N26 C31 C33 . . . . 126.8(6) ? C27 N26 C31 C32 . . . . 65.7(7) ? C25 N26 C31 C32 . . . . -105.8(6) ?