#------------------------------------------------------------------------------ #$Date: 2024-10-03 01:13:11 +0300 (Thu, 03 Oct 2024) $ #$Revision: 294991 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572745.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572745 loop_ _publ_author_name 'Vald\'es, Hugo' 'Alpuente, Nora' 'Salvador Sedano, Pedro' 'Hashmi, Stephen' 'Ribas, Xavi' _publ_section_title ; CCC--NHC Au(III) Pincer Complexes as a Reliable Platform for Isolating Elusive Species ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC02999B _journal_year 2024 _chemical_formula_moiety 'C29 H30 Au N4 O2, B F4' _chemical_formula_sum 'C29 H30 Au B F4 N4 O2' _chemical_formula_weight 750.34 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_update_record ; 2024-02-20 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90.397(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.4261(12) _cell_length_b 12.5589(9) _cell_length_c 16.0123(13) _cell_measurement_reflns_used 9992 _cell_measurement_temperature 100.(2) _cell_measurement_theta_max 27.1582 _cell_measurement_theta_min 2.5442 _cell_volume 2699.9(4) _computing_cell_refinement 'SAINT V8.40B (Bruker AXS LLC, 2019)' _computing_data_collection 'Bruker Instrument Service vV6.2.16' _computing_data_reduction 'SAINT V8.40B (Bruker AXS LLC, 2019)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 1365)' _computing_structure_refinement 'SHELXL-2019/1 (Sheldrick, 2019)' _computing_structure_solution 'XT, VERSION 2018/2' _diffrn_ambient_temperature 100.(2) _diffrn_detector_area_resol_mean 7.3910 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'D8 QUEST ECO' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'doubly curved silicon crystal Bruker Triumph' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1370 _diffrn_reflns_av_unetI/netI 0.0453 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 129169 _diffrn_reflns_theta_full 25.24 _diffrn_reflns_theta_max 27.59 _diffrn_reflns_theta_min 2.22 _diffrn_source_current 20.0 _diffrn_source_power 1.00 _diffrn_source_type 'Ceramic x-ray tube' _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 5.513 _exptl_absorpt_correction_T_max 0.73 _exptl_absorpt_correction_T_min 0.55 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Krause, L., Herbst-Irmer, R., Sheldrick, G. M., Stalke, D. (2015). "Comparison of silver and molybdenum microfocus X-ray sources for single-crystal structure determination" J. Appl. Cryst. 48, 3-10. doi:10.1107/S1600576714022985 ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.846 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1472 _exptl_crystal_size_max 0.220 _exptl_crystal_size_mid 0.080 _exptl_crystal_size_min 0.060 _refine_diff_density_max 0.963 _refine_diff_density_min -1.229 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 374 _refine_ls_number_reflns 6241 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.047 _refine_ls_R_factor_all 0.0575 _refine_ls_R_factor_gt 0.0303 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0222P)^2^+6.9793P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0565 _refine_ls_wR_factor_ref 0.0646 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4746 _reflns_number_total 6241 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc02999b3.cif _cod_data_source_block HV2_106R _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'Multi-Scan' was changed to 'multi-scan' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas ; _cod_database_code 1572745 _shelx_res_file ; TITL HV2_106R_0m_a.res in P2(1)/n HV2_106R_0m_a.res created by SHELXL-2019/1 at 14:15:32 on 10-Oct-2023 REM Old TITL HV2_106R_0m in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.080, Rweak 0.006, Alpha 0.050 REM 0.403 for 268 systematic absences, Orientation as input REM Formula found by SHELXT: C31 Au F4 N3 O2 CELL 0.71073 13.4261 12.5589 16.0123 90.000 90.397 90.000 ZERR 4.000 0.0012 0.0009 0.0013 0.000 0.003 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H AU B F N O UNIT 116 120 4 4 16 16 8 OMIT 0 0 2 OMIT 0 1 1 OMIT 1 1 1 OMIT -1 1 1 TEMP -173.150 SIZE 0.06 0.08 0.22 L.S. 10 BOND $h conf acta LIST 6 FMAP 2 PLAN 20 WGHT 0.022200 6.979300 FVAR 0.24072 AU1 3 0.224316 0.336800 0.541940 11.00000 0.01641 0.01545 = 0.01566 -0.00041 -0.00382 0.00168 O34 7 0.355373 0.303405 0.607018 11.00000 0.02317 0.02544 = 0.02461 0.00023 -0.00845 0.00292 O36 7 0.272679 0.333012 0.725456 11.00000 0.04408 0.03752 = 0.01990 0.00232 -0.00181 -0.00698 N3 6 0.334867 0.555105 0.531960 11.00000 0.02135 0.01860 = 0.01837 -0.00377 -0.00150 0.00125 N10 6 0.266923 0.501449 0.415483 11.00000 0.01593 0.01833 = 0.01483 0.00091 -0.00205 0.00151 N19 6 0.056389 0.201841 0.595858 11.00000 0.02139 0.01712 = 0.02250 0.00276 -0.00243 0.00210 N26 6 0.186492 0.098814 0.584873 11.00000 0.01835 0.01776 = 0.01755 0.00156 -0.00496 0.00038 C2 1 0.282176 0.475647 0.495874 11.00000 0.01458 0.01678 = 0.02028 -0.00178 0.00024 0.00363 C4 1 0.355293 0.632990 0.471036 11.00000 0.01581 0.01859 = 0.02398 0.00150 0.00234 0.00193 C5 1 0.411452 0.726687 0.473332 11.00000 0.02127 0.02382 = 0.03462 -0.00715 0.00669 -0.00433 AFIX 43 H5 2 0.445070 0.749624 0.522535 11.00000 -1.20000 AFIX 0 C6 1 0.415120 0.783954 0.399689 11.00000 0.03285 0.02479 = 0.03971 0.00454 0.01110 -0.00429 AFIX 43 H6 2 0.452576 0.848100 0.398349 11.00000 -1.20000 AFIX 0 C7 1 0.365774 0.750873 0.327306 11.00000 0.03847 0.03126 = 0.02825 0.01008 0.00846 -0.00300 AFIX 43 H7 2 0.369226 0.794156 0.278755 11.00000 -1.20000 AFIX 0 C8 1 0.312523 0.658025 0.323983 11.00000 0.02433 0.03355 = 0.02338 0.00772 0.00468 0.00590 AFIX 43 H8 2 0.279422 0.635421 0.274442 11.00000 -1.20000 AFIX 0 C9 1 0.309588 0.598187 0.397797 11.00000 0.01801 0.01911 = 0.02420 0.00061 0.00082 0.00322 C11 1 0.210597 0.432774 0.357095 11.00000 0.02029 0.02000 = 0.01453 -0.00396 -0.00471 0.00352 AFIX 23 H11A 2 0.247480 0.365549 0.348028 11.00000 -1.20000 H11B 2 0.203197 0.469182 0.302566 11.00000 -1.20000 AFIX 0 C12 1 0.108901 0.408477 0.392274 11.00000 0.01923 0.01783 = 0.01694 -0.00591 -0.00310 0.00408 C13 1 0.023089 0.431641 0.345388 11.00000 0.02627 0.01570 = 0.01759 -0.00540 -0.00373 0.00457 AFIX 43 H13 2 0.028809 0.459958 0.290615 11.00000 -1.20000 AFIX 0 C14 1 -0.069308 0.413331 0.378765 11.00000 0.02150 0.02076 = 0.02536 -0.00518 -0.01014 0.00619 AFIX 43 H14 2 -0.127382 0.430230 0.347230 11.00000 -1.20000 AFIX 0 C15 1 -0.078513 0.370353 0.458168 11.00000 0.01262 0.01999 = 0.02878 -0.00439 0.00182 0.00226 AFIX 43 H15 2 -0.142756 0.356274 0.480077 11.00000 -1.20000 AFIX 0 C16 1 0.006050 0.347739 0.505939 11.00000 0.01810 0.01311 = 0.02230 -0.00355 -0.00140 0.00457 C17 1 0.100120 0.367474 0.472173 11.00000 0.01610 0.01324 = 0.01891 -0.00345 -0.00024 -0.00043 C18 1 -0.003544 0.298871 0.591035 11.00000 0.02326 0.01977 = 0.02245 -0.00119 0.00329 0.00323 AFIX 23 H18A 2 0.019335 0.350139 0.634036 11.00000 -1.20000 H18B 2 -0.074243 0.281717 0.601924 11.00000 -1.20000 AFIX 0 C20 1 0.021996 0.098711 0.610826 11.00000 0.02685 0.01959 = 0.01362 0.00154 -0.00388 -0.00281 C21 1 -0.072588 0.060181 0.626635 11.00000 0.02064 0.03250 = 0.02015 0.00453 -0.00360 -0.00211 AFIX 43 H21 2 -0.128479 0.106067 0.631663 11.00000 -1.20000 AFIX 0 C22 1 -0.080900 -0.049041 0.634675 11.00000 0.03110 0.03666 = 0.01830 0.00630 -0.00723 -0.01452 AFIX 43 H22 2 -0.144647 -0.079743 0.643429 11.00000 -1.20000 AFIX 0 C23 1 0.002011 -0.114762 0.630217 11.00000 0.04329 0.02136 = 0.01989 0.00236 -0.00725 -0.00863 AFIX 43 H23 2 -0.006951 -0.189330 0.636714 11.00000 -1.20000 AFIX 0 C24 1 0.096298 -0.076719 0.616841 11.00000 0.03444 0.01637 = 0.02138 0.00151 -0.01233 0.00017 AFIX 43 H24 2 0.152443 -0.122715 0.615621 11.00000 -1.20000 AFIX 0 C25 1 0.105668 0.032791 0.605122 11.00000 0.02423 0.02197 = 0.01765 0.00180 -0.00593 -0.00216 C27 1 0.153860 0.199914 0.579094 11.00000 0.02283 0.01827 = 0.01244 0.00156 -0.00326 0.00132 C28 1 0.364388 0.559716 0.621347 11.00000 0.02136 0.02422 = 0.01889 -0.00379 -0.00210 -0.00114 AFIX 13 H28 2 0.326640 0.502632 0.651027 11.00000 -1.20000 AFIX 0 C29 1 0.335543 0.666071 0.661079 11.00000 0.02780 0.02443 = 0.02371 -0.00470 0.00057 -0.00304 AFIX 137 H29A 2 0.339393 0.659912 0.722028 11.00000 -1.50000 H29B 2 0.267379 0.684691 0.644375 11.00000 -1.50000 H29C 2 0.381388 0.721712 0.642275 11.00000 -1.50000 AFIX 0 C30 1 0.474562 0.535022 0.631784 11.00000 0.02034 0.03609 = 0.03291 -0.00832 -0.00894 0.00507 AFIX 137 H30A 2 0.492016 0.534904 0.691313 11.00000 -1.50000 H30B 2 0.513883 0.589327 0.602949 11.00000 -1.50000 H30C 2 0.488846 0.464908 0.607822 11.00000 -1.50000 AFIX 0 C31 1 0.291792 0.064864 0.575262 11.00000 0.02072 0.02306 = 0.02522 0.00287 0.00025 0.00837 AFIX 13 H31 2 0.330139 0.128472 0.556056 11.00000 -1.20000 AFIX 0 C32 1 0.303419 -0.020290 0.509407 11.00000 0.03012 0.02844 = 0.03529 -0.00051 0.00553 0.00648 AFIX 137 H32A 2 0.374371 -0.032284 0.498949 11.00000 -1.50000 H32B 2 0.270556 0.002745 0.457639 11.00000 -1.50000 H32C 2 0.272872 -0.086570 0.528911 11.00000 -1.50000 AFIX 0 C33 1 0.334837 0.032197 0.659187 11.00000 0.02445 0.03208 = 0.03038 0.00432 -0.00411 0.00610 AFIX 137 H33A 2 0.405133 0.013121 0.652670 11.00000 -1.50000 H33B 2 0.298009 -0.029268 0.680611 11.00000 -1.50000 H33C 2 0.329202 0.091618 0.698543 11.00000 -1.50000 AFIX 0 C35 1 0.346648 0.306700 0.686883 11.00000 0.03074 0.02252 = 0.02640 -0.00134 -0.00700 0.00011 AFIX 43 H35 2 0.403405 0.286666 0.718968 11.00000 -1.20000 AFIX 0 F2S 5 0.643378 0.940380 0.688672 11.00000 0.06839 0.05113 = 0.04071 -0.01851 -0.01678 -0.00768 F3S 5 0.690426 0.799852 0.612737 11.00000 0.07591 0.04248 = 0.06533 0.00893 0.03290 0.02731 F4S 5 0.586676 0.773267 0.721221 11.00000 0.09318 0.08412 = 0.04974 -0.00064 0.02201 -0.03785 F5S 5 0.535273 0.860777 0.602650 11.00000 0.04713 0.08383 = 0.10328 -0.01686 -0.03988 -0.00337 B1S 4 0.612343 0.843357 0.656930 11.00000 0.02384 0.04590 = 0.03333 -0.00973 -0.00364 -0.00397 HKLF 4 REM HV2_106R_0m_a.res in P2(1)/n REM wR2 = 0.0646, GooF = S = 1.047, Restrained GooF = 1.047 for all data REM R1 = 0.0303 for 4746 Fo > 4sig(Fo) and 0.0575 for all 6241 data REM 374 parameters refined using 0 restraints END WGHT 0.0222 6.9790 REM Highest difference peak 0.963, deepest hole -1.229, 1-sigma level 0.156 Q1 1 0.3228 0.3352 0.3730 11.00000 0.05 0.96 Q2 1 0.6313 0.7722 0.5924 11.00000 0.05 0.79 Q3 1 0.5262 0.8223 0.6717 11.00000 0.05 0.78 Q4 1 0.5576 0.9194 0.5659 11.00000 0.05 0.72 Q5 1 0.2236 -0.0073 0.5434 11.00000 0.05 0.68 Q6 1 0.1951 0.2355 0.5803 11.00000 0.05 0.68 Q7 1 0.2123 0.3062 0.6195 11.00000 0.05 0.64 Q8 1 0.1511 0.3414 0.4834 11.00000 0.05 0.62 Q9 1 0.2401 0.3915 0.4697 11.00000 0.05 0.62 Q10 1 0.4024 0.6642 0.3065 11.00000 0.05 0.60 Q11 1 0.2043 0.2915 0.4673 11.00000 0.05 0.57 Q12 1 0.4038 0.0471 0.4839 11.00000 0.05 0.57 Q13 1 0.1822 0.3966 0.6023 11.00000 0.05 0.57 Q14 1 0.3024 0.3528 0.3139 11.00000 0.05 0.56 Q15 1 0.1462 0.3277 0.6799 11.00000 0.05 0.56 Q16 1 0.3123 0.3994 0.5423 11.00000 0.05 0.56 Q17 1 0.1796 0.1688 0.6046 11.00000 0.05 0.55 Q18 1 0.6359 0.6781 0.6872 11.00000 0.05 0.55 Q19 1 0.1025 0.3576 0.7318 11.00000 0.05 0.55 Q20 1 0.6219 0.6701 0.5808 11.00000 0.05 0.54 ; _shelx_res_checksum 16392 _shelx_hkl_file ; 2 0 0 2713.63 99.59 -3 0 0 -1.20 12.30 -3 0 0 -6.70 11.90 3 0 0 4.70 12.60 3 0 0 -2.50 11.20 3 0 0 7.60 13.10 3 0 0 -18.40 10.60 -3 0 0 -9.40 7.90 -3 0 0 5.60 14.40 -3 0 0 -17.80 10.10 3 0 0 -1.30 12.70 3 0 0 -2.80 8.60 -3 0 0 0.40 12.30 4 0 0 936.51 57.49 -4 0 0 1014.90 58.49 -4 0 0 1033.60 58.69 -4 0 0 1052.19 60.09 -4 0 0 1078.59 61.59 4 0 0 975.50 59.29 4 0 0 1045.30 61.19 4 0 0 991.20 58.79 4 0 0 968.60 58.19 -4 0 0 919.61 55.09 -4 0 0 1028.90 61.99 -4 0 0 976.70 58.29 5 0 0 2.20 17.40 5 0 0 11.90 16.70 5 0 0 -9.20 17.50 -5 0 0 -11.10 15.50 -5 0 0 1.10 16.80 -5 0 0 23.10 20.10 -5 0 0 22.90 18.70 -5 0 0 5.80 16.50 -5 0 0 0.70 13.00 5 0 0 -4.80 14.80 -5 0 0 -10.70 11.00 5 0 0 -2.70 15.60 -6 0 0 292.17 44.20 6 0 0 456.75 49.80 6 0 0 370.36 41.30 6 0 0 421.86 50.29 -6 0 0 347.47 47.10 -6 0 0 386.06 48.30 -6 0 0 351.56 45.80 -6 0 0 334.47 37.10 6 0 0 355.16 49.90 6 0 0 418.76 52.69 -6 0 0 415.56 51.69 -7 0 0 3.40 17.30 7 0 0 -6.60 23.80 -7 0 0 -10.60 22.10 -7 0 0 2.50 21.20 -7 0 0 3.70 24.20 7 0 0 -7.20 21.90 -7 0 0 -13.10 17.50 7 0 0 40.90 29.30 7 0 0 5.50 18.10 -7 0 0 24.90 25.50 7 0 0 -18.70 22.80 -8 0 0 128.89 38.80 8 0 0 132.29 38.40 8 0 0 109.49 37.20 8 0 0 168.68 40.80 -8 0 0 117.69 36.40 -8 0 0 135.89 36.20 -8 0 0 133.49 38.10 8 0 0 121.09 39.80 -8 0 0 145.69 36.30 8 0 0 158.68 39.80 -8 0 0 141.09 38.80 8 0 0 197.68 46.40 -8 0 0 204.98 45.50 -9 0 0 -1.80 32.50 9 0 0 -16.00 32.00 9 0 0 16.30 32.60 9 0 0 -0.70 28.60 9 0 0 0.00 34.60 -9 0 0 34.40 31.00 -9 0 0 13.80 31.70 -9 0 0 47.80 33.30 -9 0 0 1.80 29.00 9 0 0 24.40 32.10 -9 0 0 -1.70 23.80 -9 0 0 9.40 23.80 9 0 0 39.90 29.20 -9 0 0 0.80 26.50 10 0 0 191.98 57.39 -10 0 0 119.29 45.40 10 0 0 73.69 46.50 10 0 0 64.29 37.10 10 0 0 59.59 40.10 -10 0 0 63.39 43.40 -10 0 0 68.39 39.50 -10 0 0 47.80 40.80 10 0 0 51.29 41.10 -10 0 0 43.60 38.80 -10 0 0 47.90 41.20 -10 0 0 82.39 35.60 10 0 0 77.19 41.40 -10 0 0 85.69 38.60 -11 0 0 -59.69 35.70 11 0 0 -20.40 44.50 11 0 0 -15.60 47.60 11 0 0 11.40 29.50 -11 0 0 35.80 40.00 -11 0 0 59.89 47.80 11 0 0 -19.90 43.20 -11 0 0 -20.80 32.80 -11 0 0 -4.90 25.00 11 0 0 -37.40 40.40 -11 0 0 -27.10 43.00 -11 0 0 -34.40 43.60 11 0 0 14.00 37.70 -11 0 0 -15.70 36.20 -12 0 0 -42.90 52.69 -12 0 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83.89 -16 -3 0 -80.69 52.79 -16 -3 0 -55.39 91.69 -16 3 0 -32.80 65.89 -16 3 0 77.19 67.89 -16 3 0 -70.79 87.49 16 3 0 12.20 82.19 16 3 0 278.57 119.39 -16 3 0 -58.29 82.59 -16 3 0 -188.08 63.69 16 3 0 -143.49 80.79 -17 -3 0 247.48 100.19 17 -3 0 141.79 97.89 -17 -3 0 -75.09 122.49 -17 -3 0 135.49 74.39 17 -3 0 -192.18 107.69 17 3 0 153.48 124.09 -17 3 0 127.99 81.69 17 3 0 137.89 104.69 -17 3 0 184.58 110.09 -17 3 0 104.19 97.49 0 -4 0 1791.12 60.79 0 -4 0 1770.52 60.69 0 4 0 1728.43 60.89 0 4 0 1874.71 87.49 0 4 0 1837.42 61.69 0 4 0 1779.52 86.49 0 4 0 1773.52 82.99 1 -4 0 3249.18 135.69 1 -4 0 3371.16 112.69 1 -4 0 3300.67 115.29 1 -4 0 3495.35 115.59 -1 -4 0 3457.45 110.39 1 -4 0 3304.37 136.49 -1 -4 0 3202.78 109.89 1 4 0 3551.74 145.19 1 4 0 3291.07 111.69 1 4 0 3227.08 111.89 -1 4 0 3458.65 113.79 1 4 0 3377.86 132.89 -1 4 0 3276.57 110.89 -1 4 0 3403.26 123.49 -1 4 0 3263.57 115.89 -1 4 0 3324.67 117.39 1 4 0 3538.45 141.19 -1 4 0 3352.66 135.49 -1 4 0 3361.96 136.59 2 -4 0 530.55 32.40 2 -4 0 529.45 42.10 -2 -4 0 469.35 43.90 2 -4 0 526.35 32.50 2 -4 0 507.55 33.50 2 -4 0 500.65 42.40 2 -4 0 504.15 34.10 -2 -4 0 493.25 25.00 -2 -4 0 513.45 40.90 -2 -4 0 513.05 26.40 -2 -4 0 479.95 43.80 -2 -4 0 501.65 30.00 -2 -4 0 511.15 29.10 -2 4 0 578.94 35.30 2 4 0 545.05 23.40 2 4 0 535.85 30.50 -2 4 0 544.85 31.50 2 4 0 561.74 37.60 2 4 0 519.25 29.90 -2 4 0 519.05 42.20 -2 4 0 428.16 38.70 2 4 0 529.05 22.70 2 4 0 537.25 49.50 2 4 0 541.75 47.60 -2 4 0 591.64 34.20 2 4 0 568.04 41.70 -2 4 0 530.45 33.30 -3 -4 0 1996.10 91.79 -3 -4 0 1988.00 85.69 -3 -4 0 2046.50 83.09 -3 -4 0 1986.30 81.69 3 -4 0 1854.11 94.49 -3 -4 0 1902.61 80.39 3 -4 0 1918.01 79.39 3 -4 0 2010.90 95.49 -3 -4 0 1921.01 79.09 -3 -4 0 1942.61 99.59 3 -4 0 1875.41 85.59 -3 -4 0 1908.81 101.29 3 -4 0 1880.81 87.49 3 -4 0 1886.71 85.39 3 4 0 2021.00 83.79 3 4 0 1904.71 100.09 -3 4 0 1901.71 97.29 3 4 0 2005.40 91.69 -3 4 0 2054.09 84.89 -3 4 0 1956.70 86.49 3 4 0 1863.91 82.29 3 4 0 1899.21 75.99 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2 -10 477.55 75.59 5 -2 -10 1808.42 96.29 -5 -2 10 1974.40 148.79 -5 -2 10 1663.83 136.89 5 -2 -10 1681.63 143.69 5 -2 -10 1880.81 85.09 -5 -2 10 1965.70 121.39 -5 -2 10 1676.83 84.59 -5 -2 10 1755.92 131.69 5 -2 -10 1884.61 143.19 5 -2 -10 1924.31 126.09 5 -2 -10 1696.53 127.29 -5 -2 10 1727.63 119.49 5 -2 -10 1917.11 140.69 5 -2 -10 1769.62 114.09 -5 -2 10 1715.13 131.19 -5 2 10 1834.02 135.29 5 2 -10 1915.41 133.19 5 2 -10 1795.62 143.59 -5 2 10 1796.42 99.49 5 2 -10 1898.81 119.99 -5 2 10 1818.82 114.19 5 2 -10 1742.13 136.79 -5 2 10 1915.21 117.79 5 2 -10 1861.21 148.49 5 2 -10 1875.51 126.59 5 2 -10 1861.71 124.59 -5 2 10 1731.93 123.79 -5 2 10 1641.04 133.19 -5 2 10 1660.23 137.89 5 2 -10 1807.72 114.19 5 2 -10 1869.91 117.39 4 -2 -10 308.07 49.80 4 -2 -10 299.07 71.39 -4 -2 10 285.37 57.69 4 -2 -10 309.87 30.20 4 -2 -10 322.77 40.40 -4 -2 10 332.07 37.20 -4 -2 10 375.56 76.09 -4 -2 10 288.07 70.89 -4 -2 10 278.57 54.29 4 -2 -10 291.57 70.39 4 -2 -10 242.48 60.69 4 -2 -10 402.06 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126.29 -2 -1 -20 314.27 99.79 2 -1 20 401.46 91.59 -2 -1 -20 474.95 95.89 -2 -1 -20 299.07 65.89 -2 -1 -20 464.05 84.29 -2 -1 -20 386.26 116.59 -2 1 -20 366.76 114.59 -2 1 -20 439.96 134.49 2 1 20 138.49 84.09 2 1 20 461.15 126.89 2 1 20 205.38 109.39 -2 1 -20 351.66 87.29 -2 1 -20 353.16 67.39 -2 1 -20 366.26 82.09 -2 1 -20 474.35 99.89 -2 1 -20 196.18 84.99 3 -1 20 126.49 81.19 3 -1 20 129.39 103.59 -3 -1 -20 112.09 81.29 3 -1 20 65.19 107.99 -3 -1 -20 154.38 101.29 -3 -1 -20 65.09 71.19 -3 -1 -20 -1.80 107.89 -3 -1 -20 15.80 63.29 -3 1 -20 187.88 91.79 -3 1 -20 153.28 84.09 -3 1 -20 18.00 108.79 3 1 20 74.99 89.29 -3 1 -20 178.78 83.69 -3 1 -20 54.39 57.59 3 1 20 -60.99 93.69 -3 1 -20 -47.70 105.69 -3 1 -20 26.00 72.79 3 1 20 42.50 98.39 -4 -1 -20 202.98 73.19 4 -1 20 197.58 116.19 -4 -1 -20 393.46 111.09 4 -1 20 423.76 96.99 -4 -1 -20 89.39 124.89 4 -1 20 467.55 121.09 -4 -1 -20 129.29 93.79 -4 1 -20 257.27 71.39 -4 1 -20 267.07 92.89 -4 1 -20 276.87 83.89 -4 1 -20 310.17 137.29 -4 1 -20 206.68 100.19 4 1 20 243.08 94.59 4 1 20 443.86 125.69 4 1 20 147.69 106.89 4 -2 -20 157.68 129.99 -4 -2 20 127.29 74.89 -4 -2 20 40.90 109.69 -4 -2 20 43.70 121.59 4 -2 -20 291.17 113.49 4 -2 -20 52.89 87.49 4 -2 -20 90.39 92.79 -4 -2 20 45.20 71.79 -4 2 20 203.58 78.69 4 2 -20 -55.29 91.69 4 2 -20 -173.68 73.39 -4 2 20 -18.00 80.79 4 2 -20 -17.60 127.99 4 2 -20 15.20 92.99 4 2 -20 8.40 77.79 4 2 -20 -35.70 95.59 -4 2 20 174.68 119.79 4 2 -20 -2.60 95.79 -4 2 20 7.80 107.69 4 2 -20 87.39 164.08 3 -2 -20 176.58 122.79 -3 -2 20 237.68 92.39 3 -2 -20 48.70 112.79 3 -2 -20 211.28 89.79 3 -2 -20 212.78 96.89 -3 -2 20 138.29 119.49 -3 -2 20 323.37 76.29 -3 -2 20 380.36 121.09 3 2 -20 141.79 104.79 -3 2 20 92.99 110.49 -3 2 20 72.29 120.09 3 2 -20 129.09 81.69 -3 2 20 64.89 74.19 3 2 -20 210.98 95.09 3 2 -20 164.48 88.59 3 2 -20 210.88 125.19 3 2 -20 155.88 87.99 3 2 -20 136.09 97.39 3 2 -20 120.79 75.79 -3 2 20 1.40 85.49 -2 -2 20 -51.99 94.69 2 -2 -20 113.29 111.59 2 -2 -20 -112.49 88.29 2 -2 -20 -14.60 87.49 -2 -2 20 -88.19 70.39 -2 -2 20 44.80 72.29 -2 -2 20 -35.10 106.29 2 -2 -20 170.38 84.99 2 2 -20 -94.49 116.59 -2 2 20 223.38 78.89 -2 2 20 42.10 61.39 2 2 -20 40.60 74.99 2 2 -20 129.29 88.29 2 2 -20 -51.39 86.09 -2 2 20 -124.59 92.29 2 2 -20 -71.49 86.79 2 2 -20 25.90 79.19 2 2 -20 5.30 76.99 2 2 -20 103.79 76.19 -2 2 20 81.29 100.19 1 -2 -20 362.66 140.49 1 -2 -20 230.68 90.79 -1 -2 20 342.97 73.39 1 -2 -20 114.69 89.99 -1 -2 20 254.07 124.49 -1 -2 20 134.39 67.89 1 -2 -20 292.77 107.29 -1 -2 20 77.49 108.29 1 2 -20 219.18 80.19 1 2 -20 187.98 79.29 -1 2 20 234.58 70.59 -1 2 20 132.89 107.59 1 2 -20 215.88 107.39 1 2 -20 183.78 84.19 -1 2 20 275.47 79.89 1 2 -20 297.47 97.69 1 2 -20 104.99 89.09 -1 2 20 201.38 119.79 1 2 -20 223.08 123.59 1 2 -20 264.27 88.49 0 -2 20 -35.50 64.59 0 -2 -20 114.69 85.99 0 -2 20 -121.69 96.99 0 -2 -20 -2.60 88.69 0 -2 20 70.49 105.39 0 -2 -20 377.66 270.57 0 -2 -20 -145.19 114.09 0 -2 -20 84.49 81.19 0 2 20 107.49 60.89 0 2 -20 -42.70 77.39 0 2 -20 146.29 81.59 0 2 -20 -20.80 74.29 0 2 -20 6.60 108.59 0 2 -20 128.39 74.29 0 2 -20 -17.20 86.39 0 2 20 39.30 102.69 0 2 -20 38.90 68.19 0 2 -20 -184.28 88.09 0 2 20 88.09 76.39 0 2 20 145.69 103.79 -1 -2 -20 42.90 38.40 1 -2 20 63.89 107.39 -1 -2 -20 80.09 114.99 -1 -2 -20 41.60 75.39 -1 -2 -20 87.79 29.20 -1 -2 -20 196.48 84.29 -1 -2 -20 27.80 88.99 1 -2 20 37.30 65.29 1 -2 20 -102.59 84.99 -1 2 -20 72.09 77.29 1 2 20 37.00 96.89 -1 2 -20 181.28 81.39 -1 2 -20 -24.40 115.79 -1 2 -20 149.88 78.39 1 2 20 322.87 104.29 -1 2 -20 106.29 82.79 1 2 20 338.97 91.09 -1 2 -20 -236.18 88.89 -1 2 -20 94.09 70.19 -1 2 -20 -87.09 93.99 -2 -2 -20 -208.98 82.99 2 -2 20 106.99 70.99 -2 -2 -20 -56.39 54.79 -2 -2 -20 -23.60 43.20 -2 -2 -20 -44.40 69.49 2 -2 20 -72.99 88.59 -2 -2 -20 63.89 119.59 -2 -2 -20 18.40 82.69 2 -2 20 -147.09 97.79 -2 2 -20 33.90 74.79 -2 2 -20 -134.49 80.49 -2 2 -20 -32.80 79.59 2 2 20 -70.59 69.99 -2 2 -20 14.80 68.19 2 2 20 25.70 87.59 -2 2 -20 -38.40 93.39 2 2 20 190.38 99.59 -2 2 -20 91.79 120.99 -2 2 -20 -98.89 72.09 -3 -2 -20 28.40 73.59 -3 -2 -20 15.70 86.39 -3 -2 -20 -70.59 52.59 3 -2 20 -59.39 93.59 3 -2 20 92.39 107.29 -3 -2 -20 -166.38 106.89 -3 2 -20 49.90 90.29 3 2 20 95.39 98.89 -3 2 -20 1.60 66.99 3 2 20 12.00 76.69 -3 2 -20 -46.80 102.19 -3 2 -20 -84.89 110.49 -3 2 -20 -17.40 70.89 -3 2 -20 106.09 80.09 3 2 20 94.49 94.89 -3 2 -20 29.20 66.69 4 -2 20 -23.00 97.49 -4 -2 -20 36.60 86.19 -4 -2 -20 -129.09 108.49 -4 -2 -20 3.70 81.29 -4 -2 -20 37.40 61.89 4 -2 20 -14.60 102.79 4 2 20 -36.10 97.89 -4 2 -20 -103.49 70.59 -4 2 -20 88.39 100.69 -4 2 -20 102.39 152.78 4 2 20 161.88 147.39 -4 2 -20 68.89 83.09 4 2 20 -67.19 73.39 -4 2 -20 -47.40 76.39 -4 2 -20 -69.39 103.09 3 -3 -20 212.58 110.49 3 -3 -20 -45.90 80.69 3 -3 -20 8.80 134.09 -3 -3 20 208.38 77.69 -3 -3 20 127.29 109.39 3 -3 -20 254.07 97.39 -3 -3 20 18.60 109.19 3 3 -20 -2.90 91.49 3 3 -20 140.49 75.09 -3 3 20 162.48 72.89 -3 3 20 -85.09 110.49 3 3 -20 147.69 98.69 3 3 -20 240.78 117.29 3 3 -20 157.28 108.29 -3 3 20 144.09 78.39 3 3 -20 92.39 116.59 3 3 -20 294.57 110.19 3 3 -20 146.79 96.09 -3 3 20 145.39 112.59 -2 -3 20 24.10 81.49 -2 -3 20 162.38 119.39 2 -3 -20 -131.69 77.09 -2 -3 20 60.79 95.29 2 -3 -20 -51.79 130.19 2 -3 -20 79.09 100.89 2 -3 -20 3.70 72.89 2 3 -20 -26.50 93.99 2 3 -20 63.29 88.49 2 3 -20 -11.00 91.99 2 3 -20 -158.68 104.69 -2 3 20 -74.79 106.29 2 3 -20 -65.49 82.09 2 3 -20 96.99 84.69 -2 3 20 16.50 67.19 -2 3 20 24.80 73.39 2 3 -20 -187.38 96.49 2 3 -20 2.00 99.99 -2 3 20 -24.80 93.49 -1 -3 20 257.57 119.09 1 -3 -20 401.56 136.99 1 -3 -20 194.28 92.29 -1 -3 20 41.20 109.09 1 -3 -20 146.79 105.99 1 -3 -20 288.57 88.99 -1 -3 20 209.68 82.89 1 3 -20 165.38 88.29 1 3 -20 167.98 95.19 -1 3 20 283.07 71.19 1 3 -20 141.69 72.69 1 3 -20 193.38 89.89 1 3 -20 251.77 126.59 1 3 -20 122.39 111.29 -1 3 20 242.78 91.19 -1 3 20 361.06 116.09 -1 3 20 77.59 107.19 1 3 -20 215.58 100.59 1 3 -20 -65.79 89.69 0 -3 20 62.89 117.09 0 -3 -20 152.08 116.89 0 -3 -20 -84.49 75.09 0 -3 -20 1.30 95.69 0 -3 20 -192.78 92.99 0 -3 -20 -5.70 72.39 0 3 -20 111.89 80.09 0 3 -20 34.70 98.19 0 3 -20 -44.40 79.89 0 3 -20 -9.20 78.69 0 3 20 210.88 97.29 0 3 -20 -148.29 96.49 0 3 -20 -9.30 82.89 0 3 20 17.10 54.09 0 3 -20 -73.89 91.19 0 3 20 59.99 75.19 0 3 -20 -55.29 93.79 0 3 20 -214.18 85.99 -1 -3 -20 377.86 121.69 1 -3 20 436.56 127.89 1 -3 20 339.87 123.29 -1 -3 -20 403.96 114.09 -1 -3 -20 418.66 123.49 -1 -3 -20 335.27 106.19 1 3 20 309.47 116.19 -1 3 -20 394.46 106.69 -1 3 -20 270.77 120.19 -1 3 -20 67.39 107.89 -1 3 -20 341.37 104.89 1 3 20 675.63 133.29 1 3 20 359.26 102.89 -1 3 -20 254.57 93.59 -1 3 -20 303.57 91.19 -1 3 -20 211.38 128.09 -1 3 -20 432.36 95.59 2 -3 20 -39.30 103.09 -2 -3 -20 -142.49 70.29 -2 -3 -20 62.49 83.39 -2 -3 -20 -87.49 85.39 -2 -3 -20 -1.60 112.29 2 -3 20 -119.49 100.79 -2 3 -20 88.29 83.89 -2 3 -20 -2.30 79.39 -2 3 -20 134.29 121.59 -2 3 -20 -17.80 84.39 2 3 20 47.10 88.49 -2 3 -20 -82.39 84.79 -2 3 -20 52.39 100.59 2 3 20 -98.69 71.99 -2 3 -20 138.69 78.69 2 3 20 -122.39 106.49 -3 -3 -20 732.63 132.59 -3 -3 -20 590.94 137.99 -3 -3 -20 632.64 160.28 3 -3 20 613.44 154.38 3 -3 20 627.04 139.09 3 3 20 616.04 137.69 -3 3 -20 597.24 100.29 -3 3 -20 595.24 131.59 -3 3 -20 726.33 111.89 -3 3 -20 394.96 115.69 -3 3 -20 439.26 106.89 3 3 20 702.53 131.59 -3 3 -20 879.41 172.18 -3 3 -20 619.54 119.99 2 -4 -20 213.08 112.49 2 -4 -20 71.89 87.29 -2 -4 20 124.59 120.49 -2 -4 20 85.69 74.89 2 -4 -20 165.58 87.59 -2 -4 20 -49.80 87.69 -2 4 20 -113.99 96.29 -2 4 20 124.29 70.39 2 4 -20 75.69 100.59 2 4 -20 160.08 118.49 2 4 -20 100.09 94.59 2 4 -20 -113.49 114.09 2 4 -20 -95.79 87.99 2 4 -20 285.37 102.99 2 4 -20 299.37 106.79 -2 4 20 67.19 78.39 -1 -4 20 -237.38 106.29 -1 -4 20 101.59 97.09 1 -4 -20 99.39 79.09 1 -4 -20 12.00 101.19 1 -4 -20 -95.49 142.29 1 -4 -20 212.28 95.79 -1 -4 20 12.10 71.29 1 4 -20 14.20 95.69 -1 4 20 95.59 63.79 1 4 -20 85.69 109.29 1 4 -20 109.49 93.29 1 4 -20 -134.69 91.39 1 4 -20 57.69 74.39 -1 4 20 -79.49 98.09 1 4 -20 -50.09 92.59 1 4 -20 46.20 123.69 -1 4 20 114.59 80.19 0 -4 -20 9.20 97.79 0 -4 20 148.69 106.99 0 -4 -20 113.29 88.99 0 -4 20 49.40 118.59 0 -4 -20 -140.69 166.08 0 4 20 -3.30 81.69 0 4 -20 146.99 87.59 0 4 -20 301.77 112.69 0 4 -20 -135.99 85.59 0 4 -20 43.60 114.59 0 4 20 127.49 100.59 0 4 -20 114.49 97.49 0 4 -20 114.59 80.99 0 4 -20 10.60 86.69 -1 -4 -20 49.40 93.99 -1 -4 -20 -8.30 81.59 -1 -4 -20 -12.10 174.68 -1 -4 -20 -30.00 76.69 1 -4 20 247.08 111.29 1 -4 20 19.50 106.69 1 4 20 58.69 78.49 -1 4 -20 208.18 111.99 -1 4 -20 146.59 110.79 -1 4 -20 109.69 83.89 1 4 20 36.20 99.09 -1 4 -20 108.29 110.19 -1 4 -20 62.59 87.59 -1 4 -20 150.58 94.09 -1 4 -20 19.30 82.39 -2 -4 -20 -85.09 79.49 -2 -4 -20 -125.49 82.79 2 -4 20 -19.50 112.29 2 -4 20 -14.40 91.99 -2 4 -20 90.49 84.79 -2 4 -20 -27.30 74.79 2 4 20 12.10 90.89 -2 4 -20 125.49 104.19 -2 4 -20 101.89 117.89 -2 4 -20 56.69 91.79 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 66051 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au Au1 0.22432(2) 0.33680(2) 0.54194(2) 0.01586(5) Uani d . . . 1 . . O O34 0.3554(2) 0.3034(2) 0.6070(2) 0.0244(7) Uani d . . . 1 . . O O36 0.2727(3) 0.3330(3) 0.7255(2) 0.0338(8) Uani d . . . 1 . . N N3 0.3349(3) 0.5551(3) 0.5320(2) 0.0194(8) Uani d . . . 1 . . N N10 0.2669(3) 0.5014(3) 0.4155(2) 0.0164(8) Uani d . . . 1 . . N N19 0.0564(3) 0.2018(3) 0.5959(2) 0.0203(8) Uani d . . . 1 . . N N26 0.1865(3) 0.0988(3) 0.5849(2) 0.0179(8) Uani d . . . 1 . . C C2 0.2822(3) 0.4756(3) 0.4959(3) 0.0172(9) Uani d . . . 1 . . C C4 0.3553(3) 0.6330(3) 0.4710(3) 0.0195(10) Uani d . . . 1 . . C C5 0.4115(4) 0.7267(4) 0.4733(3) 0.0265(11) Uani d . . . 1 . . H H5 0.445070 0.749624 0.522535 0.032000 Uiso calc U . R 1 . . C C6 0.4151(4) 0.7840(4) 0.3997(3) 0.0324(12) Uani d . . . 1 . . H H6 0.452576 0.848100 0.398349 0.039000 Uiso calc U . R 1 . . C C7 0.3658(4) 0.7509(4) 0.3273(3) 0.0326(12) Uani d . . . 1 . . H H7 0.369226 0.794156 0.278755 0.039000 Uiso calc U . R 1 . . C C8 0.3125(4) 0.6580(4) 0.3240(3) 0.0271(10) Uani d . . . 1 . . H H8 0.279422 0.635421 0.274442 0.032000 Uiso calc U . R 1 . . C C9 0.3096(3) 0.5982(4) 0.3978(3) 0.0204(10) Uani d . . . 1 . . C C11 0.2106(3) 0.4328(3) 0.3571(3) 0.0183(9) Uani d . . . 1 . . H H11A 0.247480 0.365549 0.348028 0.022000 Uiso calc U . R 1 . . H H11B 0.203197 0.469182 0.302566 0.022000 Uiso calc U . R 1 . . C C12 0.1089(3) 0.4085(3) 0.3923(3) 0.0180(9) Uani d . . . 1 . . C C13 0.0231(3) 0.4316(3) 0.3454(3) 0.0199(10) Uani d . . . 1 . . H H13 0.028809 0.459958 0.290615 0.024000 Uiso calc U . R 1 . . C C14 -0.0693(4) 0.4133(4) 0.3788(3) 0.0226(10) Uani d . . . 1 . . H H14 -0.127382 0.430230 0.347230 0.027000 Uiso calc U . R 1 . . C C15 -0.0785(3) 0.3704(3) 0.4582(3) 0.0205(10) Uani d . . . 1 . . H H15 -0.142756 0.356274 0.480077 0.025000 Uiso calc U . R 1 . . C C16 0.0061(3) 0.3477(3) 0.5059(3) 0.0178(9) Uani d . . . 1 . . C C17 0.1001(3) 0.3675(3) 0.4722(3) 0.0161(9) Uani d . . . 1 . . C C18 -0.0035(4) 0.2989(4) 0.5910(3) 0.0218(10) Uani d . . . 1 . . H H18A 0.019335 0.350139 0.634036 0.026000 Uiso calc U . R 1 . . H H18B -0.074243 0.281717 0.601924 0.026000 Uiso calc U . R 1 . . C C20 0.0220(4) 0.0987(4) 0.6108(3) 0.0200(10) Uani d . . . 1 . . C C21 -0.0726(4) 0.0602(4) 0.6266(3) 0.0244(11) Uani d . . . 1 . . H H21 -0.128479 0.106067 0.631663 0.029000 Uiso calc U . R 1 . . C C22 -0.0809(4) -0.0490(4) 0.6347(3) 0.0287(12) Uani d . . . 1 . . H H22 -0.144647 -0.079743 0.643429 0.034000 Uiso calc U . R 1 . . C C23 0.0020(4) -0.1148(4) 0.6302(3) 0.0282(12) Uani d . . . 1 . . H H23 -0.006951 -0.189330 0.636714 0.034000 Uiso calc U . R 1 . . C C24 0.0963(4) -0.0767(4) 0.6168(3) 0.0241(11) Uani d . . . 1 . . H H24 0.152443 -0.122715 0.615621 0.029000 Uiso calc U . R 1 . . C C25 0.1057(4) 0.0328(4) 0.6051(3) 0.0213(10) Uani d . . . 1 . . C C27 0.1539(3) 0.1999(3) 0.5791(3) 0.0179(9) Uani d . . . 1 . . C C28 0.3644(3) 0.5597(4) 0.6213(3) 0.0215(10) Uani d . . . 1 . . H H28 0.326640 0.502632 0.651027 0.026000 Uiso calc U . R 1 . . C C29 0.3355(4) 0.6661(4) 0.6611(3) 0.0253(10) Uani d . . . 1 . . H H29A 0.339393 0.659912 0.722028 0.038000 Uiso calc U . R 1 . . H H29B 0.267379 0.684691 0.644375 0.038000 Uiso calc U . R 1 . . H H29C 0.381388 0.721712 0.642275 0.038000 Uiso calc U . R 1 . . C C30 0.4746(4) 0.5350(4) 0.6318(3) 0.0298(12) Uani d . . . 1 . . H H30A 0.492016 0.534904 0.691313 0.045000 Uiso calc U . R 1 . . H H30B 0.513883 0.589327 0.602949 0.045000 Uiso calc U . R 1 . . H H30C 0.488846 0.464908 0.607822 0.045000 Uiso calc U . R 1 . . C C31 0.2918(3) 0.0649(4) 0.5753(3) 0.0230(10) Uani d . . . 1 . . H H31 0.330139 0.128472 0.556056 0.028000 Uiso calc U . R 1 . . C C32 0.3034(4) -0.0203(4) 0.5094(3) 0.0313(12) Uani d . . . 1 . . H H32A 0.374371 -0.032284 0.498949 0.047000 Uiso calc U . R 1 . . H H32B 0.270556 0.002745 0.457639 0.047000 Uiso calc U . R 1 . . H H32C 0.272872 -0.086570 0.528911 0.047000 Uiso calc U . R 1 . . C C33 0.3348(4) 0.0322(4) 0.6592(3) 0.0290(12) Uani d . . . 1 . . H H33A 0.405133 0.013121 0.652670 0.043000 Uiso calc U . R 1 . . H H33B 0.298009 -0.029268 0.680611 0.043000 Uiso calc U . R 1 . . H H33C 0.329202 0.091618 0.698543 0.043000 Uiso calc U . R 1 . . C C35 0.3466(4) 0.3067(4) 0.6869(3) 0.0266(11) Uani d . . . 1 . . H H35 0.403405 0.286666 0.718968 0.032000 Uiso calc U . R 1 . . F F2S 0.6434(3) 0.9404(3) 0.6887(2) 0.0535(10) Uani d . . . 1 . . F F3S 0.6904(3) 0.7999(3) 0.6127(2) 0.0611(11) Uani d . . . 1 . . F F4S 0.5867(3) 0.7733(3) 0.7212(2) 0.0756(13) Uani d . . . 1 . . F F5S 0.5353(3) 0.8608(3) 0.6027(3) 0.0783(13) Uani d . . . 1 . . B B1S 0.6123(4) 0.8434(6) 0.6569(4) 0.0344(14) Uani d . . . 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.01641(9) 0.01545(8) 0.01566(8) 0.00168(8) -0.00382(5) -0.00041(8) O34 0.0232(18) 0.0254(17) 0.0246(18) 0.0029(14) -0.0085(14) 0.0002(14) O36 0.044(2) 0.038(2) 0.0199(17) -0.0070(19) -0.0018(16) 0.0023(16) N3 0.021(2) 0.0186(19) 0.0184(19) 0.0013(16) -0.0015(16) -0.0038(15) N10 0.0159(19) 0.0183(19) 0.0148(18) 0.0015(15) -0.0020(14) 0.0009(15) N19 0.021(2) 0.0171(18) 0.022(2) 0.0021(16) -0.0024(16) 0.0028(16) N26 0.018(2) 0.0178(19) 0.0175(19) 0.0004(16) -0.0050(16) 0.0016(15) C2 0.015(2) 0.017(2) 0.020(2) 0.0036(18) 0.0002(18) -0.0018(18) C4 0.016(2) 0.019(2) 0.024(2) 0.0019(18) 0.0023(19) 0.0015(18) C5 0.021(3) 0.024(3) 0.035(3) -0.004(2) 0.007(2) -0.007(2) C6 0.033(3) 0.025(3) 0.040(3) -0.004(2) 0.011(2) 0.005(2) C7 0.038(3) 0.031(3) 0.028(3) -0.003(2) 0.008(2) 0.010(2) C8 0.024(3) 0.034(3) 0.023(2) 0.006(2) 0.0047(19) 0.008(2) C9 0.018(2) 0.019(2) 0.024(2) 0.0032(19) 0.0008(19) 0.0006(18) C11 0.020(2) 0.020(2) 0.015(2) 0.0035(18) -0.0047(18) -0.0040(17) C12 0.019(2) 0.018(2) 0.017(2) 0.0041(18) -0.0031(18) -0.0059(18) C13 0.026(3) 0.016(2) 0.018(2) 0.0046(19) -0.0037(19) -0.0054(18) C14 0.022(3) 0.021(2) 0.025(3) 0.006(2) -0.010(2) -0.0052(19) C15 0.013(2) 0.020(2) 0.029(3) 0.0023(18) 0.0018(19) -0.0044(19) C16 0.018(2) 0.013(2) 0.022(2) 0.0046(18) -0.0014(17) -0.0035(18) C17 0.016(2) 0.013(2) 0.019(2) -0.0004(17) -0.0002(18) -0.0035(16) C18 0.023(3) 0.020(2) 0.022(2) 0.0032(19) 0.003(2) -0.0012(19) C20 0.027(3) 0.020(2) 0.014(2) -0.003(2) -0.0039(19) 0.0015(17) C21 0.021(3) 0.033(3) 0.020(2) -0.002(2) -0.004(2) 0.005(2) C22 0.031(3) 0.037(3) 0.018(2) -0.015(2) -0.007(2) 0.006(2) C23 0.043(3) 0.021(2) 0.020(2) -0.009(2) -0.007(2) 0.002(2) C24 0.034(3) 0.016(2) 0.021(2) 0.000(2) -0.012(2) 0.0015(18) C25 0.024(3) 0.022(2) 0.018(2) -0.002(2) -0.0059(19) 0.0018(18) C27 0.023(3) 0.018(2) 0.012(2) 0.0013(19) -0.0033(18) 0.0016(17) C28 0.021(3) 0.024(2) 0.019(2) -0.001(2) -0.0021(19) -0.0038(19) C29 0.028(3) 0.024(2) 0.024(2) -0.003(2) 0.0006(19) -0.005(2) C30 0.020(3) 0.036(3) 0.033(3) 0.005(2) -0.009(2) -0.008(2) C31 0.021(3) 0.023(2) 0.025(2) 0.008(2) 0.000(2) 0.0029(19) C32 0.030(3) 0.028(3) 0.035(3) 0.006(2) 0.006(2) -0.001(2) C33 0.024(3) 0.032(3) 0.030(3) 0.006(2) -0.004(2) 0.004(2) C35 0.031(3) 0.023(2) 0.026(3) 0.000(2) -0.007(2) -0.001(2) F2S 0.068(3) 0.051(2) 0.041(2) -0.0077(19) -0.0168(18) -0.0185(16) F3S 0.076(3) 0.042(2) 0.065(2) 0.0273(19) 0.033(2) 0.0089(18) F4S 0.093(3) 0.084(3) 0.050(2) -0.038(3) 0.022(2) -0.001(2) F5S 0.047(2) 0.084(3) 0.103(3) -0.003(2) -0.040(2) -0.017(3) B1S 0.024(3) 0.046(4) 0.033(3) -0.004(3) -0.004(2) -0.010(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C17 Au1 C2 . . 87.28(17) ? C17 Au1 C27 . . 86.57(17) ? C2 Au1 C27 . . 173.80(17) ? C17 Au1 O34 . . 176.77(15) ? C2 Au1 O34 . . 91.74(15) ? C27 Au1 O34 . . 94.35(15) ? C35 O34 Au1 . . 114.1(3) ? C2 N3 C4 . . 108.7(4) ? C2 N3 C28 . . 125.3(4) ? C4 N3 C28 . . 126.1(4) ? C2 N10 C9 . . 110.5(4) ? C2 N10 C11 . . 122.7(4) ? C9 N10 C11 . . 126.8(4) ? C27 N19 C20 . . 110.0(4) ? C27 N19 C18 . . 122.9(4) ? C20 N19 C18 . . 126.8(4) ? C27 N26 C25 . . 108.7(4) ? C27 N26 C31 . . 125.0(4) ? C25 N26 C31 . . 126.3(4) ? N10 C2 N3 . . 107.9(4) ? N10 C2 Au1 . . 119.7(3) ? N3 C2 Au1 . . 132.3(3) ? C9 C4 C5 . . 121.4(4) ? C9 C4 N3 . . 106.2(4) ? C5 C4 N3 . . 132.3(4) ? C6 C5 C4 . . 116.0(5) ? C6 C5 H5 . . 122.000000 ? C4 C5 H5 . . 122.000000 ? C5 C6 C7 . . 122.3(5) ? C5 C6 H6 . . 118.800000 ? C7 C6 H6 . . 118.800000 ? C8 C7 C6 . . 122.1(5) ? C8 C7 H7 . . 119.000000 ? C6 C7 H7 . . 119.000000 ? C7 C8 C9 . . 116.2(5) ? C7 C8 H8 . . 121.900000 ? C9 C8 H8 . . 121.900000 ? N10 C9 C4 . . 106.6(4) ? N10 C9 C8 . . 131.5(4) ? C4 C9 C8 . . 121.9(4) ? N10 C11 C12 . . 110.0(3) ? N10 C11 H11A . . 109.700000 ? C12 C11 H11A . . 109.700000 ? N10 C11 H11B . . 109.700000 ? C12 C11 H11B . . 109.700000 ? H11A C11 H11B . . 108.200000 ? C17 C12 C13 . . 119.8(4) ? C17 C12 C11 . . 120.1(4) ? C13 C12 C11 . . 120.0(4) ? C14 C13 C12 . . 119.9(4) ? C14 C13 H13 . . 120.100000 ? C12 C13 H13 . . 120.100000 ? C13 C14 C15 . . 120.5(4) ? C13 C14 H14 . . 119.700000 ? C15 C14 H14 . . 119.700000 ? C14 C15 C16 . . 120.3(4) ? C14 C15 H15 . . 119.800000 ? C16 C15 H15 . . 119.800000 ? C15 C16 C17 . . 119.1(4) ? C15 C16 C18 . . 120.5(4) ? C17 C16 C18 . . 120.4(4) ? C12 C17 C16 . . 120.4(4) ? C12 C17 Au1 . . 120.1(3) ? C16 C17 Au1 . . 119.5(3) ? N19 C18 C16 . . 109.8(4) ? N19 C18 H18A . . 109.700000 ? C16 C18 H18A . . 109.700000 ? N19 C18 H18B . . 109.700000 ? C16 C18 H18B . . 109.700000 ? H18A C18 H18B . . 108.200000 ? C21 C20 N19 . . 131.4(4) ? C21 C20 C25 . . 122.9(4) ? N19 C20 C25 . . 105.7(4) ? C22 C21 C20 . . 116.0(5) ? C22 C21 H21 . . 122.000000 ? C20 C21 H21 . . 122.000000 ? C21 C22 C23 . . 121.3(5) ? C21 C22 H22 . . 119.300000 ? C23 C22 H22 . . 119.300000 ? C24 C23 C22 . . 122.8(5) ? C24 C23 H23 . . 118.600000 ? C22 C23 H23 . . 118.600000 ? C23 C24 C25 . . 116.7(5) ? C23 C24 H24 . . 121.700000 ? C25 C24 H24 . . 121.700000 ? C24 C25 C20 . . 120.1(4) ? C24 C25 N26 . . 133.1(5) ? C20 C25 N26 . . 106.7(4) ? N19 C27 N26 . . 108.8(4) ? N19 C27 Au1 . . 119.8(3) ? N26 C27 Au1 . . 131.3(3) ? N3 C28 C30 . . 110.6(4) ? N3 C28 C29 . . 111.6(4) ? C30 C28 C29 . . 112.4(4) ? N3 C28 H28 . . 107.300000 ? C30 C28 H28 . . 107.300000 ? C29 C28 H28 . . 107.300000 ? C28 C29 H29A . . 109.500000 ? C28 C29 H29B . . 109.500000 ? H29A C29 H29B . . 109.500000 ? C28 C29 H29C . . 109.500000 ? H29A C29 H29C . . 109.500000 ? H29B C29 H29C . . 109.500000 ? C28 C30 H30A . . 109.500000 ? C28 C30 H30B . . 109.500000 ? H30A C30 H30B . . 109.500000 ? C28 C30 H30C . . 109.500000 ? H30A C30 H30C . . 109.500000 ? H30B C30 H30C . . 109.500000 ? N26 C31 C32 . . 112.2(4) ? N26 C31 C33 . . 110.1(4) ? C32 C31 C33 . . 112.7(4) ? N26 C31 H31 . . 107.200000 ? C32 C31 H31 . . 107.200000 ? C33 C31 H31 . . 107.200000 ? C31 C32 H32A . . 109.500000 ? C31 C32 H32B . . 109.500000 ? H32A C32 H32B . . 109.500000 ? C31 C32 H32C . . 109.500000 ? H32A C32 H32C . . 109.500000 ? H32B C32 H32C . . 109.500000 ? C31 C33 H33A . . 109.500000 ? C31 C33 H33B . . 109.500000 ? H33A C33 H33B . . 109.500000 ? C31 C33 H33C . . 109.500000 ? H33A C33 H33C . . 109.500000 ? H33B C33 H33C . . 109.500000 ? O36 C35 O34 . . 126.4(5) ? O36 C35 H35 . . 116.800000 ? O34 C35 H35 . . 116.800000 ? F5S B1S F3S . . 108.2(5) ? F5S B1S F2S . . 108.5(5) ? F3S B1S F2S . . 108.0(5) ? F5S B1S F4S . . 112.3(5) ? F3S B1S F4S . . 108.6(5) ? F2S B1S F4S . . 111.0(5) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Au1 C17 . 2.037(4) ? Au1 C2 . 2.048(4) ? Au1 C27 . 2.052(4) ? Au1 O34 . 2.081(3) ? O34 C35 . 1.286(6) ? O36 C35 . 1.219(6) ? N3 C2 . 1.351(5) ? N3 C4 . 1.410(6) ? N3 C28 . 1.484(5) ? N10 C2 . 1.342(5) ? N10 C9 . 1.374(6) ? N10 C11 . 1.477(5) ? N19 C27 . 1.338(6) ? N19 C20 . 1.396(6) ? N19 C18 . 1.462(6) ? N26 C27 . 1.346(6) ? N26 C25 . 1.405(6) ? N26 C31 . 1.486(6) ? C4 C9 . 1.390(6) ? C4 C5 . 1.398(6) ? C5 C6 . 1.382(7) ? C5 H5 . 0.950000 ? C6 C7 . 1.394(7) ? C6 H6 . 0.950000 ? C7 C8 . 1.369(7) ? C7 H7 . 0.950000 ? C8 C9 . 1.401(6) ? C8 H8 . 0.950000 ? C11 C12 . 1.512(6) ? C11 H11A . 0.990000 ? C11 H11B . 0.990000 ? C12 C17 . 1.385(6) ? C12 C13 . 1.401(6) ? C13 C14 . 1.374(7) ? C13 H13 . 0.950000 ? C14 C15 . 1.388(6) ? C14 H14 . 0.950000 ? C15 C16 . 1.394(6) ? C15 H15 . 0.950000 ? C16 C17 . 1.399(6) ? C16 C18 . 1.501(6) ? C18 H18A . 0.990000 ? C18 H18B . 0.990000 ? C20 C21 . 1.384(7) ? C20 C25 . 1.399(6) ? C21 C22 . 1.382(7) ? C21 H21 . 0.950000 ? C22 C23 . 1.388(7) ? C22 H22 . 0.950000 ? C23 C24 . 1.371(7) ? C23 H23 . 0.950000 ? C24 C25 . 1.394(6) ? C24 H24 . 0.950000 ? C28 C30 . 1.519(6) ? C28 C29 . 1.530(6) ? C28 H28 . 1.000000 ? C29 H29A . 0.980000 ? C29 H29B . 0.980000 ? C29 H29C . 0.980000 ? C30 H30A . 0.980000 ? C30 H30B . 0.980000 ? C30 H30C . 0.980000 ? C31 C32 . 1.511(6) ? C31 C33 . 1.516(6) ? C31 H31 . 1.000000 ? C32 H32A . 0.980000 ? C32 H32B . 0.980000 ? C32 H32C . 0.980000 ? C33 H33A . 0.980000 ? C33 H33B . 0.980000 ? C33 H33C . 0.980000 ? C35 H35 . 0.950000 ? F2S B1S . 1.383(7) ? F3S B1S . 1.382(7) ? F4S B1S . 1.399(8) ? F5S B1S . 1.364(7) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C9 N10 C2 N3 . . . . 0.1(5) ? C11 N10 C2 N3 . . . . -179.4(4) ? C9 N10 C2 Au1 . . . . 178.6(3) ? C11 N10 C2 Au1 . . . . -0.9(5) ? C4 N3 C2 N10 . . . . -1.3(5) ? C28 N3 C2 N10 . . . . 177.7(4) ? C4 N3 C2 Au1 . . . . -179.5(3) ? C28 N3 C2 Au1 . . . . -0.5(7) ? C2 N3 C4 C9 . . . . 2.0(5) ? C28 N3 C4 C9 . . . . -177.0(4) ? C2 N3 C4 C5 . . . . -175.5(5) ? C28 N3 C4 C5 . . . . 5.5(8) ? C9 C4 C5 C6 . . . . 2.5(7) ? N3 C4 C5 C6 . . . . 179.6(5) ? C4 C5 C6 C7 . . . . 0.1(7) ? C5 C6 C7 C8 . . . . -1.7(8) ? C6 C7 C8 C9 . . . . 0.5(8) ? C2 N10 C9 C4 . . . . 1.2(5) ? C11 N10 C9 C4 . . . . -179.4(4) ? C2 N10 C9 C8 . . . . -179.2(5) ? C11 N10 C9 C8 . . . . 0.2(8) ? C5 C4 C9 N10 . . . . 175.9(4) ? N3 C4 C9 N10 . . . . -1.9(5) ? C5 C4 C9 C8 . . . . -3.8(7) ? N3 C4 C9 C8 . . . . 178.4(4) ? C7 C8 C9 N10 . . . . -177.5(5) ? C7 C8 C9 C4 . . . . 2.2(7) ? C2 N10 C11 C12 . . . . 54.5(5) ? C9 N10 C11 C12 . . . . -124.8(4) ? N10 C11 C12 C17 . . . . -52.7(5) ? N10 C11 C12 C13 . . . . 124.6(4) ? C17 C12 C13 C14 . . . . -0.2(6) ? C11 C12 C13 C14 . . . . -177.5(4) ? C12 C13 C14 C15 . . . . -1.1(7) ? C13 C14 C15 C16 . . . . 1.6(7) ? C14 C15 C16 C17 . . . . -1.0(6) ? C14 C15 C16 C18 . . . . -178.6(4) ? C13 C12 C17 C16 . . . . 0.8(6) ? C11 C12 C17 C16 . . . . 178.1(4) ? C13 C12 C17 Au1 . . . . -178.5(3) ? C11 C12 C17 Au1 . . . . -1.2(5) ? C15 C16 C17 C12 . . . . -0.3(6) ? C18 C16 C17 C12 . . . . 177.3(4) ? C15 C16 C17 Au1 . . . . 179.1(3) ? C18 C16 C17 Au1 . . . . -3.3(5) ? C27 N19 C18 C16 . . . . 55.4(6) ? C20 N19 C18 C16 . . . . -118.8(5) ? C15 C16 C18 N19 . . . . 125.7(4) ? C17 C16 C18 N19 . . . . -51.9(5) ? C27 N19 C20 C21 . . . . -176.6(5) ? C18 N19 C20 C21 . . . . -1.8(8) ? C27 N19 C20 C25 . . . . 2.0(5) ? C18 N19 C20 C25 . . . . 176.9(4) ? N19 C20 C21 C22 . . . . 176.9(4) ? C25 C20 C21 C22 . . . . -1.5(7) ? C20 C21 C22 C23 . . . . 2.4(7) ? C21 C22 C23 C24 . . . . -0.7(7) ? C22 C23 C24 C25 . . . . -1.9(7) ? C23 C24 C25 C20 . . . . 2.7(7) ? C23 C24 C25 N26 . . . . -175.2(4) ? C21 C20 C25 C24 . . . . -1.0(7) ? N19 C20 C25 C24 . . . . -179.8(4) ? C21 C20 C25 N26 . . . . 177.3(4) ? N19 C20 C25 N26 . . . . -1.4(5) ? C27 N26 C25 C24 . . . . 178.5(5) ? C31 N26 C25 C24 . . . . -4.3(8) ? C27 N26 C25 C20 . . . . 0.4(5) ? C31 N26 C25 C20 . . . . 177.7(4) ? C20 N19 C27 N26 . . . . -1.8(5) ? C18 N19 C27 N26 . . . . -176.9(4) ? C20 N19 C27 Au1 . . . . 173.5(3) ? C18 N19 C27 Au1 . . . . -1.6(6) ? C25 N26 C27 N19 . . . . 0.9(5) ? C31 N26 C27 N19 . . . . -176.4(4) ? C25 N26 C27 Au1 . . . . -173.7(3) ? C31 N26 C27 Au1 . . . . 9.0(6) ? C2 N3 C28 C30 . . . . 105.2(5) ? C4 N3 C28 C30 . . . . -76.0(5) ? C2 N3 C28 C29 . . . . -128.9(4) ? C4 N3 C28 C29 . . . . 49.9(6) ? C27 N26 C31 C32 . . . . -125.3(5) ? C25 N26 C31 C32 . . . . 57.9(6) ? C27 N26 C31 C33 . . . . 108.3(5) ? C25 N26 C31 C33 . . . . -68.6(5) ? Au1 O34 C35 O36 . . . . -4.6(6) ?