#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:32:25 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296377 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572747.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572747 loop_ _publ_author_name 'Guo, Jia-Dong' 'Korsaye, Feven-Alemu' 'Schutz, Dorian' 'Ciofini, Ilaria' 'Miesch, Laurence' _publ_section_title ; Photocatalyst-free, visible-light-induced regio- and stereoselective synthesis of phosphorylated enamines from N-allenamides via [1,3]-sulfonyl shift at room temperature. ; _journal_issue 43 _journal_name_full 'Chemical science' _journal_page_first 17962 _journal_page_last 17970 _journal_paper_doi 10.1039/d4sc05190d _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C30 H26 Br F3 N O3 P S' _chemical_formula_sum 'C30 H26 Br F3 N O3 P S' _chemical_formula_weight 648.46 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2023-07-13 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 112.2560(10) _cell_angle_beta 111.385(2) _cell_angle_gamma 90.4840(10) _cell_formula_units_Z 2 _cell_length_a 10.2345(4) _cell_length_b 12.0047(4) _cell_length_c 13.9944(6) _cell_measurement_reflns_used 9944 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 29.93 _cell_measurement_theta_min 2.16 _cell_volume 1460.15(10) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2019/3(Sheldrick, 2019)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 120(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker PHOTON-III CPAD' _diffrn_measurement_method '\f and \w shuterless scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0478 _diffrn_reflns_av_unetI/netI 0.0243 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 79769 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.122 _diffrn_reflns_theta_min 1.945 _diffrn_source 'Mo-ImuS 3.0 microfocus tube' _exptl_absorpt_coefficient_mu 1.585 _exptl_absorpt_correction_T_max 0.7460 _exptl_absorpt_correction_T_min 0.6389 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.475 _exptl_crystal_density_meas ? _exptl_crystal_description needle _exptl_crystal_F_000 660 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.120 _refine_diff_density_max 1.611 _refine_diff_density_min -1.708 _refine_diff_density_rms 0.069 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.012 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 362 _refine_ls_number_reflns 8606 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.012 _refine_ls_R_factor_all 0.0513 _refine_ls_R_factor_gt 0.0379 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0367P)^2^+1.5957P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0870 _refine_ls_wR_factor_ref 0.0961 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7140 _reflns_number_total 8606 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05190d2.cif _cod_data_source_block elmjd230705 _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_crystal_density_meas' value 'none' was changed to '?' -- the value is perceived as not measured. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas Adding full bibliography for 1572747--1572749.cif. ; _cod_database_code 1572747 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.742 _shelx_estimated_absorpt_t_max 0.833 _shelx_res_file ; TITL elmjd_a.res in P-1 elmjd_a.res created by SHELXL-2018/3 at 14:13:06 on 13-Jul-2023 CELL 0.71073 10.2345 12.0047 13.9944 112.256 111.385 90.484 ZERR 2.000 0.0004 0.0004 0.0006 0.001 0.002 0.001 LATT 1 SFAC C H Br F N O P S UNIT 60 52 2 6 2 6 2 2 L.S. 10 ACTA BOND $H FMAP 2 PLAN 5 CONF SIZE 0.12 0.12 0.20 TEMP -153.150 WGHT 0.036700 1.595700 FVAR 0.58618 S1 8 0.636067 0.164197 0.723855 11.00000 0.01962 0.01836 = 0.01570 0.00790 0.00575 0.00366 O1 6 0.548548 0.052230 0.632678 11.00000 0.02930 0.01847 = 0.01995 0.00714 0.00815 0.00027 O2 6 0.772086 0.156811 0.800736 11.00000 0.02368 0.02757 = 0.02217 0.01328 0.00532 0.00876 C1 1 0.539044 0.231963 0.806846 11.00000 0.02188 0.02020 = 0.01863 0.00822 0.00849 0.00182 C2 1 0.407766 0.261089 0.757776 11.00000 0.02829 0.03657 = 0.02591 0.01759 0.01308 0.01197 AFIX 43 H2 2 0.370232 0.245921 0.680271 11.00000 -1.20000 AFIX 0 C3 1 0.331706 0.312640 0.823020 11.00000 0.03315 0.03967 = 0.04026 0.02416 0.02291 0.01513 AFIX 43 H3 2 0.241350 0.332360 0.789536 11.00000 -1.20000 AFIX 0 C4 1 0.385595 0.335992 0.936852 11.00000 0.03957 0.03448 = 0.03736 0.01380 0.02635 0.00676 C5 1 0.514612 0.302452 0.982541 11.00000 0.04221 0.07360 = 0.02088 0.01664 0.01651 0.01290 AFIX 43 H5 2 0.550707 0.314494 1.059266 11.00000 -1.20000 AFIX 0 C6 1 0.592803 0.251485 0.918790 11.00000 0.02918 0.05987 = 0.02158 0.01873 0.01005 0.01208 AFIX 43 H6 2 0.682331 0.230282 0.951868 11.00000 -1.20000 AFIX 0 C7 1 0.306593 0.397973 1.009328 11.00000 0.06222 0.05529 = 0.05464 0.02149 0.04531 0.01802 AFIX 137 H7A 2 0.328589 0.370829 1.070448 11.00000 -1.50000 H7B 2 0.203931 0.376696 0.963517 11.00000 -1.50000 H7C 2 0.335901 0.486685 1.041134 11.00000 -1.50000 AFIX 0 C8 1 0.659865 0.267317 0.670324 11.00000 0.01717 0.01821 = 0.01741 0.00762 0.00742 0.00339 C9 1 0.583293 0.234583 0.558519 11.00000 0.01842 0.01808 = 0.01745 0.00709 0.00795 0.00400 AFIX 43 H9 2 0.529068 0.154512 0.516636 11.00000 -1.20000 AFIX 0 N1 5 0.576564 0.303994 0.501310 11.00000 0.02313 0.01697 = 0.01373 0.00532 0.00532 0.00159 AFIX 43 H1 2 0.612839 0.382268 0.538491 11.00000 -1.20000 AFIX 0 C10 1 0.510130 0.251820 0.378558 11.00000 0.01943 0.01705 = 0.01485 0.00606 0.00599 0.00132 AFIX 13 H10 2 0.493823 0.160984 0.352072 11.00000 -1.20000 AFIX 0 P1 7 0.333807 0.297403 0.331052 11.00000 0.02111 0.01718 = 0.01698 0.00684 0.00586 0.00415 O3 6 0.338234 0.431772 0.365974 11.00000 0.03329 0.01788 = 0.02603 0.00861 0.00840 0.00652 C11 1 0.251968 0.210144 0.180893 11.00000 0.02315 0.02557 = 0.01811 0.00878 0.00466 0.00086 C12 1 0.122990 0.238032 0.123849 11.00000 0.02735 0.04277 = 0.02789 0.01629 0.00338 0.00671 AFIX 43 H12 2 0.083091 0.300601 0.164254 11.00000 -1.20000 AFIX 0 C13 1 0.052388 0.175004 0.008364 11.00000 0.03441 0.06215 = 0.03002 0.02100 -0.00468 0.00048 AFIX 43 H13 2 -0.036073 0.194070 -0.030011 11.00000 -1.20000 AFIX 0 C14 1 0.109845 0.085031 -0.050856 11.00000 0.04829 0.05934 = 0.01982 0.00733 -0.00341 -0.00890 AFIX 43 H14 2 0.061876 0.043032 -0.130207 11.00000 -1.20000 AFIX 0 C15 1 0.236677 0.055659 0.004530 11.00000 0.05358 0.05978 = 0.02284 -0.00518 0.00603 0.00753 AFIX 43 H15 2 0.275799 -0.006904 -0.036691 11.00000 -1.20000 AFIX 0 C16 1 0.308170 0.117316 0.120985 11.00000 0.03638 0.04495 = 0.02253 0.00072 0.00233 0.01099 AFIX 43 H16 2 0.394964 0.095903 0.159177 11.00000 -1.20000 AFIX 0 C17 1 0.232139 0.239190 0.388474 11.00000 0.01864 0.02604 = 0.02278 0.01053 0.00772 0.00607 C18 1 0.203260 0.114563 0.360297 11.00000 0.03167 0.02907 = 0.04576 0.01865 0.02235 0.00935 AFIX 43 H18 2 0.235792 0.058255 0.308461 11.00000 -1.20000 AFIX 0 C19 1 0.127326 0.072445 0.407549 11.00000 0.03914 0.04503 = 0.05998 0.03139 0.02504 0.00524 AFIX 43 H19 2 0.110380 -0.012291 0.390111 11.00000 -1.20000 AFIX 0 C20 1 0.076218 0.154448 0.480341 11.00000 0.03055 0.07170 = 0.04181 0.02701 0.01748 -0.00304 AFIX 43 H20 2 0.024150 0.125808 0.512903 11.00000 -1.20000 AFIX 0 C21 1 0.100471 0.276929 0.505644 11.00000 0.03696 0.05958 = 0.03567 0.00722 0.02349 0.00378 AFIX 43 H21 2 0.063242 0.332323 0.554362 11.00000 -1.20000 AFIX 0 C22 1 0.179303 0.320727 0.460433 11.00000 0.03033 0.03440 = 0.02895 0.00492 0.01511 0.00570 AFIX 43 H22 2 0.196666 0.405657 0.478756 11.00000 -1.20000 AFIX 0 C23 1 0.610889 0.283397 0.331489 11.00000 0.02210 0.02101 = 0.01475 0.00518 0.00573 -0.00178 C24 1 0.702843 0.205493 0.299777 11.00000 0.02479 0.02247 = 0.02816 0.00657 0.01194 -0.00147 C25 1 0.800724 0.237975 0.263474 11.00000 0.03044 0.03278 = 0.03562 0.00561 0.01879 -0.00284 AFIX 43 H25 2 0.862336 0.183637 0.242982 11.00000 -1.20000 AFIX 0 C26 1 0.807796 0.350040 0.257391 11.00000 0.03917 0.03973 = 0.03178 0.01170 0.01930 -0.00757 AFIX 43 H26 2 0.874600 0.373064 0.232812 11.00000 -1.20000 AFIX 0 C27 1 0.717805 0.428382 0.287028 11.00000 0.04805 0.03073 = 0.03253 0.01525 0.01916 -0.00291 AFIX 43 H27 2 0.722006 0.504936 0.281951 11.00000 -1.20000 AFIX 0 C28 1 0.620970 0.395746 0.324304 11.00000 0.03570 0.02500 = 0.02588 0.01252 0.01394 0.00217 AFIX 43 H28 2 0.560450 0.451035 0.345305 11.00000 -1.20000 AFIX 0 BR1 3 0.695703 0.049357 0.302571 11.00000 0.03339 0.02730 = 0.07947 0.02390 0.03458 0.01051 C29 1 0.760293 0.385109 0.753062 11.00000 0.01812 0.01914 = 0.01873 0.00698 0.00698 0.00229 AFIX 23 H29A 2 0.773514 0.397059 0.830202 11.00000 -1.20000 H29B 2 0.717247 0.453787 0.738824 11.00000 -1.20000 AFIX 0 C30 1 0.903376 0.387630 0.745874 11.00000 0.01930 0.03050 = 0.03907 0.01451 0.01001 0.00202 F1 4 0.896061 0.390227 0.649282 11.00000 0.03514 0.07306 = 0.05025 0.02724 0.02945 0.00779 F2 4 0.995432 0.488427 0.828632 11.00000 0.02378 0.03842 = 0.05520 0.01757 0.00305 -0.00931 F3 4 0.965359 0.292429 0.754439 11.00000 0.02241 0.04071 = 0.08939 0.03079 0.02269 0.01330 HKLF 4 REM elmjd_a.res in P-1 REM wR2 = 0.096134, GooF = S = 1.01232, Restrained GooF = 1.01232 for all data REM R1 = 0.037887 for 7140 Fo > 4sig(Fo) and 0.051292 for all 8606 data REM 362 parameters refined using 0 restraints END WGHT 0.0323 1.6447 REM Highest difference peak 1.611, deepest hole -1.708, 1-sigma level 0.069 Q1 1 0.7196 0.0783 0.3685 11.00000 0.05 1.61 Q2 1 0.8269 0.3843 0.7425 11.00000 0.05 0.44 Q3 1 0.6162 0.2599 0.6217 11.00000 0.05 0.39 Q4 1 0.2036 0.2821 0.4159 11.00000 0.05 0.37 Q5 1 0.2748 0.2661 0.3687 11.00000 0.05 0.35 ; _shelx_res_checksum 52685 _shelx_hkl_file ; -1 0 0 1530.35 30.40 -1 0 0 1694.53 29.00 -1 0 0 1750.92 29.30 1 0 0 1639.24 30.00 1 0 0 1613.44 29.70 1 0 0 1702.63 29.50 1 0 0 1443.36 28.70 -2 0 0 1962.60 38.00 -2 0 0 1934.91 38.90 -2 0 0 1952.30 38.30 -2 0 0 1967.70 36.70 -2 0 0 1995.10 37.90 -2 0 0 1955.30 37.10 2 0 0 1980.20 37.90 2 0 0 2007.00 39.30 2 0 0 1954.30 38.20 2 0 0 1995.00 37.00 2 0 0 1969.00 36.80 2 0 0 2020.80 38.20 -3 0 0 3027.50 59.89 -3 0 0 2926.21 58.39 -3 0 0 3036.10 58.29 -3 0 0 3017.80 57.89 -3 0 0 3042.60 56.89 -3 0 0 3018.10 56.09 3 0 0 3008.40 56.89 3 0 0 3020.90 59.79 3 0 0 3049.99 58.59 3 0 0 3083.89 58.19 3 0 0 3081.29 56.69 3 0 0 2949.51 56.79 3 0 0 3073.89 58.29 3 0 0 3045.70 56.29 -4 0 0 98.49 7.40 -4 0 0 97.69 8.10 -4 0 0 100.39 7.80 -4 0 0 92.19 6.80 -4 0 0 92.49 6.50 4 0 0 95.59 7.50 4 0 0 100.69 6.70 4 0 0 101.89 7.00 4 0 0 96.49 7.30 4 0 0 103.09 6.90 4 0 0 96.79 8.20 -5 0 0 442.86 16.80 -5 0 0 439.16 15.90 -5 0 0 444.56 18.50 -5 0 0 455.45 18.10 -5 0 0 472.35 19.70 -5 0 0 475.45 18.10 -5 0 0 416.26 18.40 5 0 0 425.26 16.00 5 0 0 444.66 16.80 5 0 0 463.55 16.50 5 0 0 406.66 18.40 5 0 0 434.76 17.80 5 0 0 434.56 19.60 5 0 0 421.36 16.50 5 0 0 403.36 17.10 -6 0 0 81.39 8.30 -6 0 0 97.49 8.80 -6 0 0 94.19 8.90 -6 0 0 91.89 10.00 -6 0 0 91.59 9.70 -6 0 0 84.79 8.90 6 0 0 113.59 8.80 6 0 0 79.29 7.70 6 0 0 89.29 9.00 6 0 0 97.79 9.50 6 0 0 92.19 9.70 6 0 0 87.79 8.90 6 0 0 103.29 8.60 -7 0 0 10.00 4.90 -7 0 0 7.30 3.90 -7 0 0 13.10 5.10 -7 0 0 13.20 5.40 -7 0 0 9.30 5.00 -7 0 0 9.10 4.70 -7 0 0 8.80 3.80 7 0 0 19.50 5.60 7 0 0 12.60 4.20 7 0 0 14.80 5.00 7 0 0 9.20 4.20 7 0 0 15.50 4.80 7 0 0 9.40 4.80 7 0 0 15.70 6.10 -8 0 0 63.69 10.50 -8 0 0 69.99 12.00 -8 0 0 58.69 11.20 -8 0 0 48.90 9.70 -8 0 0 57.09 9.90 -8 0 0 68.69 10.20 -8 0 0 58.29 9.40 8 0 0 95.79 12.90 8 0 0 49.10 10.00 8 0 0 78.09 11.50 8 0 0 57.39 9.00 8 0 0 50.29 9.70 8 0 0 61.19 10.70 8 0 0 49.10 8.20 8 0 0 55.99 8.70 -9 0 0 178.78 14.70 -9 0 0 151.78 13.10 -9 0 0 117.09 15.50 -9 0 0 118.29 12.60 -9 0 0 153.08 15.90 -9 0 0 155.48 15.10 9 0 0 160.48 14.80 9 0 0 159.48 13.60 9 0 0 163.48 15.00 9 0 0 123.89 13.00 9 0 0 164.48 15.10 9 0 0 151.58 13.10 9 0 0 179.38 16.60 9 0 0 170.98 13.70 -10 0 0 129.39 18.10 -10 0 0 105.09 14.10 -10 0 0 113.29 14.10 -10 0 0 97.99 15.80 -10 0 0 90.29 13.40 -10 0 0 78.79 12.70 10 0 0 130.89 14.70 10 0 0 120.09 12.10 10 0 0 84.99 11.90 10 0 0 105.09 13.00 10 0 0 112.19 12.80 10 0 0 89.49 15.10 10 0 0 92.39 15.60 10 0 0 106.49 14.70 -11 0 0 18.70 7.70 -11 0 0 13.70 7.40 -11 0 0 41.30 11.30 -11 0 0 24.30 9.90 11 0 0 29.10 9.90 11 0 0 26.30 9.30 11 0 0 27.30 7.60 11 0 0 29.40 7.90 11 0 0 46.30 11.30 11 0 0 18.10 8.00 -12 0 0 -6.70 4.70 -12 0 0 -11.00 5.30 12 0 0 6.20 7.20 12 0 0 5.20 6.80 12 0 0 -4.00 6.00 12 0 0 3.40 5.20 -13 0 0 -8.00 7.70 -13 0 0 7.60 7.60 -13 0 0 5.90 5.80 13 0 0 5.20 6.30 13 0 0 24.10 10.00 13 0 0 -0.50 7.40 13 0 0 1.00 7.40 13 -1 0 91.99 12.80 13 -1 0 128.89 18.80 13 -1 0 132.09 21.00 -13 1 0 106.89 16.70 -13 1 0 91.99 18.20 -13 1 0 85.59 14.50 12 -1 0 136.09 20.60 12 -1 0 119.79 12.30 12 -1 0 122.69 17.00 12 -1 0 142.69 20.70 -12 1 0 93.19 16.80 -12 1 0 124.19 17.00 -12 1 0 161.98 16.20 -12 1 0 121.99 18.90 11 -1 0 182.28 14.50 11 -1 0 216.48 19.40 11 -1 0 178.08 16.80 11 -1 0 190.88 18.50 11 -1 0 208.88 19.20 11 -1 0 239.08 22.30 -11 1 0 195.68 19.40 -11 1 0 212.78 18.10 -11 1 0 170.08 19.10 -11 1 0 199.38 18.00 10 -1 0 124.29 16.00 10 -1 0 119.79 15.90 10 -1 0 109.19 12.00 10 -1 0 154.58 16.00 10 -1 0 111.39 10.90 10 -1 0 87.79 14.00 10 -1 0 124.79 18.60 10 -1 0 120.09 17.30 -10 1 0 128.19 17.40 -10 1 0 107.79 15.50 -10 1 0 134.39 17.70 -10 1 0 106.69 13.10 -10 1 0 129.49 14.20 -10 1 0 103.29 14.90 9 -1 0 28.20 7.40 9 -1 0 26.30 6.50 9 -1 0 21.80 6.40 9 -1 0 27.50 7.30 9 -1 0 13.50 5.30 9 -1 0 30.10 8.90 9 -1 0 34.10 8.80 9 -1 0 20.00 7.80 -9 1 0 19.60 7.40 -9 1 0 25.30 6.30 -9 1 0 28.00 8.40 -9 1 0 19.40 7.20 -9 1 0 25.60 7.40 -9 1 0 27.50 6.20 8 -1 0 379.06 22.90 8 -1 0 360.66 26.50 8 -1 0 394.16 18.90 8 -1 0 428.26 22.00 8 -1 0 357.06 18.70 8 -1 0 394.46 20.60 8 -1 0 381.66 19.50 8 -1 0 372.26 20.30 -8 1 0 399.96 21.30 -8 1 0 418.56 23.50 -8 1 0 388.96 20.60 -8 1 0 365.26 19.90 -8 1 0 398.06 19.40 -8 1 0 374.16 19.60 -8 1 0 421.96 22.80 7 -1 0 52.79 9.60 7 -1 0 42.80 7.00 7 -1 0 46.80 7.90 7 -1 0 36.50 8.20 7 -1 0 34.90 6.50 7 -1 0 50.29 7.30 7 -1 0 49.90 7.60 7 -1 0 58.89 8.90 -7 1 0 58.09 9.50 -7 1 0 47.70 8.60 -7 1 0 54.29 8.70 -7 1 0 52.79 8.30 -7 1 0 61.49 10.00 -7 1 0 32.70 6.70 6 -1 0 4.70 3.80 6 -1 0 5.90 3.60 6 -1 0 9.50 4.00 6 -1 0 15.20 4.00 6 -1 0 10.30 4.30 6 -1 0 5.10 3.60 6 -1 0 10.90 3.80 6 -1 0 21.00 5.50 -6 1 0 9.90 3.50 -6 1 0 7.50 3.70 -6 1 0 8.10 4.10 -6 1 0 10.90 4.70 -6 1 0 14.90 4.60 -6 1 0 17.20 5.10 5 -1 0 1466.85 37.50 5 -1 0 1483.95 33.60 5 -1 0 1479.45 36.00 5 -1 0 1445.36 36.40 5 -1 0 1456.75 38.80 5 -1 0 1408.06 36.30 5 -1 0 1396.16 34.10 5 -1 0 1439.56 35.00 -5 1 0 1402.36 35.00 -5 1 0 1493.05 37.10 -5 1 0 1461.35 38.00 -5 1 0 1474.25 39.30 -5 1 0 1427.16 35.20 -5 1 0 1455.75 35.60 -5 1 0 1448.06 36.90 4 -1 0 803.02 22.90 4 -1 0 768.12 19.60 4 -1 0 743.33 20.70 4 -1 0 752.02 23.30 4 -1 0 778.42 20.90 4 -1 0 755.62 22.00 4 -1 0 796.32 22.20 4 -1 0 782.62 21.80 -4 1 0 803.42 21.60 -4 1 0 737.53 22.60 -4 1 0 779.12 22.30 -4 1 0 773.82 21.50 -4 1 0 772.92 23.70 -4 1 0 775.92 22.20 3 -1 0 289.17 9.90 3 -1 0 279.07 10.50 3 -1 0 286.67 8.90 3 -1 0 276.27 10.50 3 -1 0 290.67 10.70 3 -1 0 291.67 10.10 -3 1 0 309.17 11.10 -3 1 0 284.87 10.70 -3 1 0 284.07 11.10 -3 1 0 281.47 11.60 -3 1 0 288.17 10.10 -3 1 0 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152.38 10.00 -4 -3 0 140.99 8.80 -4 -3 0 141.19 10.10 4 3 0 148.29 9.80 4 3 0 139.89 9.50 4 3 0 144.09 8.70 4 3 0 151.88 10.80 4 3 0 143.79 9.60 4 3 0 166.08 9.40 4 3 0 140.89 6.90 -5 -3 0 328.27 12.10 -5 -3 0 340.37 15.20 -5 -3 0 324.77 14.40 -5 -3 0 346.97 17.60 -5 -3 0 330.07 20.30 -5 -3 0 333.97 14.50 -5 -3 0 346.37 16.80 5 3 0 341.37 16.40 5 3 0 337.87 17.10 5 3 0 347.17 12.60 5 3 0 338.37 17.60 5 3 0 305.07 15.20 5 3 0 310.87 17.00 5 3 0 297.37 17.10 5 3 0 316.77 15.80 -6 -3 0 109.99 11.10 -6 -3 0 112.59 9.50 -6 -3 0 118.29 9.90 -6 -3 0 124.69 10.40 -6 -3 0 105.29 10.60 -6 -3 0 124.09 11.60 -6 -3 0 110.29 8.00 6 3 0 116.99 10.90 6 3 0 129.39 10.90 6 3 0 119.29 11.30 6 3 0 124.49 8.40 6 3 0 123.49 11.90 6 3 0 120.29 9.90 6 3 0 109.39 11.60 6 3 0 100.59 10.40 -7 -3 0 28.40 6.30 -7 -3 0 37.50 7.50 -7 -3 0 44.70 8.40 -7 -3 0 40.40 8.60 -7 -3 0 32.90 8.40 -7 -3 0 35.40 8.40 7 3 0 53.69 9.70 7 3 0 32.40 7.30 7 3 0 35.60 7.90 7 3 0 41.00 6.30 7 3 0 39.70 9.10 7 3 0 34.50 7.00 7 3 0 37.40 9.00 7 3 0 32.90 7.30 -8 -3 0 275.57 14.70 -8 -3 0 273.17 17.30 -8 -3 0 315.17 18.00 -8 -3 0 238.98 15.90 -8 -3 0 284.37 20.20 -8 -3 0 274.17 19.30 8 3 0 249.97 18.70 8 3 0 282.37 19.10 8 3 0 297.97 15.30 8 3 0 297.97 20.70 8 3 0 266.47 19.30 8 3 0 307.77 19.60 8 3 0 270.67 16.80 -9 -3 0 5.60 10.70 -9 -3 0 13.20 6.30 -9 -3 0 11.00 4.70 -9 -3 0 9.70 6.40 -9 -3 0 12.60 5.70 9 3 0 13.60 10.40 9 3 0 11.80 6.00 9 3 0 6.30 4.10 9 3 0 6.80 5.70 9 3 0 11.00 6.90 9 3 0 11.50 5.80 -10 -3 0 56.59 10.30 -10 -3 0 26.90 14.20 -10 -3 0 66.19 9.70 -10 -3 0 30.70 9.90 -10 -3 0 72.19 12.50 10 3 0 61.79 12.10 10 3 0 59.49 9.90 10 3 0 62.49 11.90 10 3 0 44.40 13.00 10 3 0 46.70 11.20 10 3 0 77.99 15.00 -11 -3 0 38.80 8.80 -11 -3 0 39.40 12.10 -11 -3 0 50.29 11.30 11 3 0 44.90 11.50 11 3 0 18.90 8.70 11 3 0 44.90 10.10 11 3 0 57.89 12.20 11 3 0 37.30 11.90 11 3 0 20.40 7.00 -12 -3 0 6.90 8.20 -12 -3 0 1.70 6.40 12 3 0 -2.00 7.50 12 3 0 5.50 8.40 12 3 0 9.30 10.10 12 3 0 6.70 5.80 12 3 0 -3.00 5.70 13 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3 -4 0 259.67 11.70 3 -4 0 300.07 9.90 3 -4 0 280.47 7.50 3 -4 0 286.07 7.70 3 -4 0 293.37 12.70 3 -4 0 282.07 10.20 -3 4 0 315.17 9.80 -3 4 0 289.37 12.30 -3 4 0 282.27 9.60 -3 4 0 290.07 10.90 -3 4 0 293.97 10.00 -3 4 0 300.47 7.20 -3 4 0 309.57 11.60 2 -4 0 1022.20 21.50 2 -4 0 1020.00 24.90 2 -4 0 1001.00 20.60 2 -4 0 1007.60 20.70 -2 4 0 1018.90 21.90 -2 4 0 1022.60 21.70 -2 4 0 996.90 19.80 -2 4 0 996.20 19.70 -2 4 0 983.20 24.40 -2 4 0 1022.20 21.00 1 -4 0 199.88 8.00 -1 4 0 200.68 5.80 -1 4 0 196.58 5.70 -1 4 0 191.58 6.90 -1 4 0 199.48 8.00 -1 4 0 188.48 8.90 0 -4 0 344.17 7.60 0 -4 0 357.26 7.70 0 -4 0 322.67 11.60 0 4 0 336.27 11.70 0 4 0 339.67 8.20 0 4 0 338.27 8.80 0 4 0 324.87 12.80 0 4 0 334.37 9.40 -1 -4 0 708.03 18.60 -1 -4 0 684.53 16.00 -1 -4 0 671.13 20.60 -1 -4 0 672.43 16.30 1 4 0 695.63 18.20 1 4 0 673.73 15.00 1 4 0 669.93 17.10 1 4 0 693.73 15.80 1 4 0 695.43 20.80 -2 -4 0 34.70 4.60 -2 -4 0 37.20 3.30 -2 -4 0 43.60 4.50 -2 -4 0 41.30 5.10 -2 -4 0 35.00 4.80 -2 -4 0 33.20 3.00 2 4 0 34.30 3.60 2 4 0 27.30 4.10 2 4 0 33.70 4.40 2 4 0 22.80 3.80 2 4 0 29.20 3.90 2 4 0 41.50 4.60 -3 -4 0 28.90 5.00 -3 -4 0 25.70 4.60 -3 -4 0 29.00 4.70 -3 -4 0 24.20 3.70 -3 -4 0 19.10 3.50 3 4 0 22.20 3.90 3 4 0 19.90 4.20 3 4 0 28.50 4.70 3 4 0 25.40 2.60 3 4 0 26.80 4.60 3 4 0 28.90 5.20 3 4 0 28.50 4.80 -4 -4 0 574.94 20.80 -4 -4 0 570.24 21.40 -4 -4 0 580.84 22.90 -4 -4 0 591.84 19.60 -4 -4 0 636.24 18.70 -4 -4 0 578.34 18.80 -4 -4 0 592.24 15.10 4 4 0 587.64 21.10 4 4 0 598.44 20.80 4 4 0 597.14 15.10 4 4 0 593.14 23.10 4 4 0 590.24 19.40 4 4 0 594.04 19.40 4 4 0 593.94 22.50 4 4 0 617.44 21.30 -5 -4 0 325.17 14.80 -5 -4 0 318.97 16.50 -5 -4 0 330.47 14.90 -5 -4 0 314.07 11.50 -5 -4 0 353.26 16.50 -5 -4 0 324.77 17.20 -5 -4 0 325.87 17.80 5 4 0 321.77 11.70 5 4 0 341.67 15.30 5 4 0 343.07 15.20 5 4 0 305.87 16.00 5 4 0 308.07 17.40 5 4 0 334.87 16.70 5 4 0 350.16 16.70 5 4 0 316.77 17.70 -6 -4 0 53.09 8.30 -6 -4 0 75.39 12.00 -6 -4 0 61.69 9.00 -6 -4 0 53.19 6.40 -6 -4 0 43.40 8.40 -6 -4 0 57.79 9.50 -6 -4 0 43.20 7.10 6 4 0 62.39 5.90 6 4 0 50.99 8.40 6 4 0 35.90 6.40 6 4 0 73.49 10.90 6 4 0 60.09 8.10 6 4 0 43.30 8.70 6 4 0 63.49 9.60 6 4 0 52.39 9.50 -7 -4 0 738.73 31.10 -7 -4 0 708.03 22.30 -7 -4 0 722.73 27.40 -7 -4 0 739.03 26.90 -7 -4 0 766.12 27.00 -7 -4 0 715.63 29.80 7 4 0 719.43 32.20 7 4 0 672.33 28.90 7 4 0 728.83 27.30 7 4 0 724.43 29.40 7 4 0 718.83 31.00 7 4 0 742.93 22.90 7 4 0 763.92 32.60 7 4 0 759.42 29.40 -8 -4 0 86.49 8.50 -8 -4 0 72.59 10.60 -8 -4 0 80.39 12.60 -8 -4 0 71.99 10.50 -8 -4 0 84.29 13.00 -8 -4 0 71.59 10.30 8 4 0 69.49 16.00 8 4 0 45.00 9.50 8 4 0 54.19 10.50 8 4 0 79.49 13.40 8 4 0 87.39 13.90 8 4 0 64.19 8.80 8 4 0 58.49 10.70 -9 -4 0 45.40 9.00 -9 -4 0 53.29 11.10 -9 -4 0 52.99 10.20 -9 -4 0 66.39 9.20 -9 -4 0 67.79 13.10 9 4 0 51.29 8.10 9 4 0 50.49 16.20 9 4 0 63.89 13.90 9 4 0 60.79 11.40 9 4 0 89.89 14.90 -10 -4 0 37.80 9.30 -10 -4 0 19.30 8.50 -10 -4 0 29.30 8.90 -10 -4 0 28.00 8.40 -10 -4 0 23.50 6.60 10 4 0 46.40 11.80 10 4 0 14.30 7.90 10 4 0 25.70 10.00 10 4 0 22.60 8.50 10 4 0 25.10 10.50 10 4 0 31.20 7.30 -11 -4 0 9.30 6.60 -11 -4 0 9.20 5.50 -11 -4 0 9.70 8.70 11 4 0 15.10 8.40 11 4 0 13.50 8.10 11 4 0 15.20 8.70 11 4 0 12.60 5.60 11 4 0 2.30 7.00 11 4 0 11.20 7.30 -12 -4 0 4.70 8.40 -12 -4 0 -10.70 5.90 -12 -4 0 -4.30 4.60 12 4 0 1.40 7.70 12 4 0 6.10 8.00 12 4 0 -2.70 6.70 12 4 0 13.30 8.60 13 -5 0 13.00 6.80 13 -5 0 10.60 9.30 -13 5 0 -1.90 9.60 -13 5 0 0.80 13.40 -13 5 0 -13.10 8.00 -13 5 0 16.70 9.30 12 -5 0 -1.40 8.50 12 -5 0 -1.10 5.70 -12 5 0 -3.60 5.70 -12 5 0 0.80 7.40 -12 5 0 10.70 8.50 -12 5 0 6.50 7.80 11 -5 0 12.30 5.00 11 -5 0 15.80 8.20 11 -5 0 10.90 5.60 -11 5 0 11.30 7.10 -11 5 0 10.00 6.30 -11 5 0 4.80 5.80 10 -5 0 4.70 4.90 10 -5 0 -6.20 3.30 10 -5 0 -0.80 4.30 10 -5 0 6.70 4.80 10 -5 0 5.00 3.90 -10 5 0 4.60 6.30 -10 5 0 -6.20 5.40 -10 5 0 -5.20 4.50 -10 5 0 -0.70 4.50 -10 5 0 4.00 4.90 9 -5 0 268.77 15.20 9 -5 0 239.58 15.50 9 -5 0 237.08 15.80 9 -5 0 278.97 19.40 9 -5 0 273.67 19.10 9 -5 0 291.37 20.60 -9 5 0 290.77 18.80 -9 5 0 260.57 19.20 -9 5 0 282.97 21.10 -9 5 0 264.27 17.60 -9 5 0 257.07 19.60 -9 5 0 271.67 18.80 8 -5 0 75.39 8.20 8 -5 0 79.69 8.90 8 -5 0 87.89 11.70 8 -5 0 60.99 9.50 8 -5 0 63.59 8.40 -8 5 0 56.19 8.90 -8 5 0 69.39 9.60 -8 5 0 62.59 9.90 -8 5 0 72.49 11.70 -8 5 0 48.40 7.60 -8 5 0 75.39 11.50 -8 5 0 50.29 8.10 7 -5 0 961.30 28.30 7 -5 0 969.50 32.60 7 -5 0 976.10 31.70 7 -5 0 966.60 29.90 7 -5 0 982.70 27.10 -7 5 0 967.80 33.20 -7 5 0 954.90 32.70 -7 5 0 957.90 30.40 -7 5 0 993.90 34.50 -7 5 0 1044.90 33.40 -7 5 0 1046.20 29.80 -7 5 0 987.90 32.40 6 -5 0 60.49 8.30 6 -5 0 69.09 6.90 6 -5 0 73.79 7.90 6 -5 0 69.39 9.80 6 -5 0 71.89 6.20 -6 5 0 101.49 12.30 -6 5 0 84.69 11.50 -6 5 0 61.69 8.70 -6 5 0 69.69 7.00 -6 5 0 58.19 8.50 -6 5 0 63.99 7.80 5 -5 0 371.16 15.10 5 -5 0 347.57 11.80 5 -5 0 339.77 11.50 5 -5 0 357.46 13.70 5 -5 0 342.77 17.00 -5 5 0 357.86 14.20 -5 5 0 353.66 15.70 -5 5 0 358.16 16.80 -5 5 0 343.27 16.10 -5 5 0 398.16 14.00 -5 5 0 364.66 16.00 -5 5 0 353.16 14.90 4 -5 0 374.66 12.70 4 -5 0 352.86 9.50 4 -5 0 341.17 13.00 4 -5 0 339.27 15.50 4 -5 0 351.06 15.90 4 -5 0 365.16 9.50 -4 5 0 358.56 12.70 -4 5 0 365.66 14.20 -4 5 0 368.26 14.70 -4 5 0 388.96 12.50 -4 5 0 344.77 13.10 -4 5 0 419.36 21.50 3 -5 0 34.60 3.60 3 -5 0 31.80 5.00 3 -5 0 34.90 3.60 3 -5 0 39.80 3.80 -3 5 0 45.70 4.50 -3 5 0 31.60 5.10 -3 5 0 40.10 4.30 -3 5 0 36.50 3.60 -3 5 0 37.40 3.60 -3 5 0 46.50 4.10 2 -5 0 100.19 4.30 2 -5 0 103.89 7.10 2 -5 0 109.49 4.30 -2 5 0 100.29 5.30 -2 5 0 115.59 7.30 -2 5 0 108.99 5.40 -2 5 0 114.09 4.20 -2 5 0 104.99 5.20 -2 5 0 107.79 4.20 -1 5 0 153.38 7.50 -1 5 0 156.18 5.20 -1 5 0 156.78 6.90 -1 5 0 155.08 8.90 -1 5 0 159.28 5.40 0 5 0 119.79 8.50 0 5 0 125.99 5.30 0 5 0 122.19 4.80 0 5 0 118.19 3.70 0 5 0 115.79 5.60 0 5 0 110.39 7.40 -1 -5 0 126.99 5.80 -1 -5 0 131.19 6.10 -1 -5 0 141.19 8.20 1 5 0 124.89 5.40 1 5 0 130.19 9.30 1 5 0 129.99 6.20 1 5 0 136.59 7.00 1 5 0 131.69 5.00 1 5 0 139.69 8.00 1 5 0 140.59 6.20 -2 -5 0 1523.55 34.40 -2 -5 0 1567.24 40.30 -2 -5 0 1660.23 28.90 -2 -5 0 1569.04 35.80 -2 -5 0 1572.84 34.10 2 5 0 1573.14 34.10 2 5 0 1570.74 32.70 2 5 0 1570.14 40.10 2 5 0 1491.05 36.30 2 5 0 1528.05 33.90 2 5 0 1601.34 35.50 -3 -5 0 139.69 7.00 -3 -5 0 134.19 8.80 -3 -5 0 137.19 10.70 -3 -5 0 150.58 9.20 -3 -5 0 125.09 6.40 -3 -5 0 142.49 9.20 3 5 0 134.79 9.60 3 5 0 145.69 8.90 3 5 0 132.49 10.60 3 5 0 148.19 8.30 3 5 0 154.48 9.20 3 5 0 146.39 8.90 -4 -5 0 221.88 12.00 -4 -5 0 229.28 13.00 -4 -5 0 228.08 10.70 -4 -5 0 222.28 14.50 -4 -5 0 244.08 10.50 -4 -5 0 202.78 14.40 4 5 0 230.58 14.60 4 5 0 223.58 13.20 4 5 0 215.18 14.40 4 5 0 232.18 7.70 4 5 0 227.88 14.00 4 5 0 238.18 11.80 4 5 0 240.08 12.10 -5 -5 0 9.20 4.80 -5 -5 0 -0.90 2.80 -5 -5 0 7.20 4.10 -5 -5 0 1.50 3.30 -5 -5 0 13.50 4.00 -5 -5 0 6.70 4.00 5 5 0 6.30 4.10 5 5 0 20.50 6.60 5 5 0 8.60 3.70 5 5 0 7.50 3.90 5 5 0 18.20 4.90 5 5 0 9.70 2.70 5 5 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22.20 9 5 0 394.56 26.90 9 5 0 357.36 16.80 9 5 0 424.86 26.80 9 5 0 401.76 26.90 9 5 0 413.16 24.50 9 5 0 410.86 25.20 -10 -5 0 5.70 5.00 -10 -5 0 1.20 7.00 -10 -5 0 9.90 6.50 -10 -5 0 13.80 6.30 -10 -5 0 4.60 4.60 10 5 0 4.60 4.10 10 5 0 4.90 6.40 10 5 0 5.10 7.10 10 5 0 10.00 6.70 10 5 0 -0.30 5.50 10 5 0 8.00 7.50 -11 -5 0 85.69 10.90 -11 -5 0 85.99 16.10 -11 -5 0 58.99 12.30 11 5 0 62.59 13.70 11 5 0 64.39 15.10 11 5 0 52.39 13.60 11 5 0 87.59 16.30 13 -6 0 -8.00 6.40 -13 6 0 -3.00 6.70 -13 6 0 7.90 12.00 -13 6 0 -1.90 7.20 12 -6 0 1.50 5.90 12 -6 0 16.00 6.20 12 -6 0 6.50 6.40 -12 6 0 15.10 8.90 -12 6 0 5.10 6.70 -12 6 0 33.10 9.80 -12 6 0 8.10 7.50 11 -6 0 13.00 5.70 11 -6 0 19.40 7.30 11 -6 0 3.60 4.90 11 -6 0 21.70 8.30 -11 6 0 6.90 6.10 -11 6 0 20.90 8.70 -11 6 0 17.40 8.90 10 -6 0 169.18 12.80 10 -6 0 179.58 16.50 10 -6 0 147.19 12.40 10 -6 0 152.88 13.80 -10 6 0 158.08 15.70 -10 6 0 159.58 16.80 -10 6 0 189.78 17.50 -10 6 0 159.08 17.10 -10 6 0 146.89 14.80 9 -6 0 298.57 18.40 9 -6 0 262.47 16.20 9 -6 0 298.57 19.50 9 -6 0 290.17 15.00 -9 6 0 243.38 19.20 -9 6 0 279.77 19.70 -9 6 0 317.07 19.80 -9 6 0 264.87 19.20 -9 6 0 284.87 17.90 8 -6 0 171.18 12.30 8 -6 0 209.48 15.00 8 -6 0 188.48 10.90 -8 6 0 170.68 15.20 -8 6 0 182.98 13.90 -8 6 0 180.48 14.30 -8 6 0 173.58 14.60 -8 6 0 217.28 16.40 -8 6 0 172.58 13.50 -8 6 0 155.98 12.00 7 -6 0 954.40 25.70 7 -6 0 960.70 34.50 7 -6 0 958.60 30.70 7 -6 0 922.01 28.40 7 -6 0 926.61 25.00 7 -6 0 849.81 32.80 -7 6 0 954.90 32.60 -7 6 0 1032.10 28.80 -7 6 0 942.01 31.60 -7 6 0 948.71 30.10 -7 6 0 997.50 32.90 -7 6 0 966.60 33.40 -7 6 0 955.40 33.60 6 -6 0 1011.10 23.70 6 -6 0 987.90 29.30 6 -6 0 959.70 29.80 6 -6 0 1006.80 27.80 6 -6 0 961.50 23.70 6 -6 0 984.20 33.30 -6 6 0 1119.59 28.20 -6 6 0 964.20 31.80 -6 6 0 1022.80 31.90 -6 6 0 977.20 30.80 -6 6 0 978.20 28.50 -6 6 0 1026.00 33.10 5 -6 0 1124.69 30.20 5 -6 0 1106.49 22.60 5 -6 0 1120.69 29.50 5 -6 0 1117.59 22.70 5 -6 0 1145.89 34.70 5 -6 0 1180.68 28.70 -5 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2297.47 43.70 1 6 0 2286.57 42.50 1 6 0 2244.28 43.70 1 6 0 2270.67 41.60 -2 -6 0 84.19 6.10 -2 -6 0 74.29 6.90 -2 -6 0 91.39 6.30 -2 -6 0 82.89 8.60 2 6 0 86.79 5.90 2 6 0 74.99 8.40 2 6 0 79.29 6.20 2 6 0 77.69 6.00 2 6 0 81.59 7.20 2 6 0 88.49 7.10 -3 -6 0 11.70 4.30 -3 -6 0 18.30 2.40 -3 -6 0 23.00 5.00 -3 -6 0 18.10 4.20 -3 -6 0 21.70 5.00 -3 -6 0 18.70 2.60 3 6 0 16.70 4.30 3 6 0 16.10 3.60 3 6 0 15.60 4.10 3 6 0 14.90 3.90 -4 -6 0 454.85 21.90 -4 -6 0 462.25 14.70 -4 -6 0 437.46 18.30 -4 -6 0 445.26 14.00 -4 -6 0 454.75 18.90 -4 -6 0 450.55 18.30 4 6 0 451.65 18.70 4 6 0 441.76 20.10 4 6 0 433.96 21.60 4 6 0 483.75 18.80 4 6 0 428.46 17.50 4 6 0 443.56 17.30 4 6 0 414.36 18.80 -5 -6 0 22.20 7.40 -5 -6 0 15.60 4.20 -5 -6 0 7.30 4.30 -5 -6 0 18.10 5.30 -5 -6 0 19.60 4.30 -5 -6 0 13.10 5.20 5 6 0 15.80 4.50 5 6 0 14.10 4.80 5 6 0 13.60 5.90 5 6 0 6.90 5.10 5 6 0 12.20 4.60 5 6 0 20.30 5.10 5 6 0 14.90 5.60 5 6 0 18.40 5.70 -6 -6 0 111.69 9.10 -6 -6 0 98.99 9.00 -6 -6 0 92.09 14.70 -6 -6 0 87.39 11.70 -6 -6 0 73.09 10.50 6 6 0 84.49 13.10 6 6 0 95.19 9.60 6 6 0 102.99 6.20 6 6 0 100.69 11.10 6 6 0 82.89 10.90 6 6 0 104.39 13.80 6 6 0 64.59 9.60 6 6 0 102.69 11.20 -7 -6 0 41.80 9.00 -7 -6 0 51.29 8.20 -7 -6 0 53.69 10.10 -7 -6 0 38.30 8.60 -7 -6 0 38.30 7.10 7 6 0 45.00 5.50 7 6 0 39.70 9.80 7 6 0 33.40 8.40 7 6 0 32.70 9.10 7 6 0 39.50 7.90 7 6 0 51.99 10.40 7 6 0 51.69 10.70 -8 -6 0 11.50 5.80 -8 -6 0 19.80 6.10 -8 -6 0 4.70 5.10 -8 -6 0 3.80 4.90 8 6 0 14.50 3.80 8 6 0 12.00 7.30 8 6 0 13.50 7.80 8 6 0 10.70 5.40 8 6 0 16.20 7.80 8 6 0 15.50 7.50 8 6 0 4.70 5.00 -9 -6 0 227.48 16.50 -9 -6 0 192.28 15.80 -9 -6 0 259.17 21.10 -9 -6 0 205.28 15.90 9 6 0 235.68 21.10 9 6 0 292.07 24.10 9 6 0 243.98 20.60 9 6 0 265.67 22.30 -10 -6 0 12.10 5.70 -10 -6 0 4.20 5.80 -10 -6 0 9.20 8.00 -10 -6 0 4.60 6.30 10 6 0 14.60 8.30 10 6 0 10.80 6.80 10 6 0 6.10 7.10 10 6 0 -0.80 5.20 -11 -6 0 67.99 11.20 11 6 0 60.09 14.60 11 6 0 68.29 16.80 11 6 0 66.09 13.90 11 6 0 74.29 14.10 12 -7 0 80.59 11.00 12 -7 0 36.90 14.30 -12 7 0 89.19 17.20 -12 7 0 86.49 15.80 -12 7 0 77.59 13.80 -12 7 0 69.09 14.90 11 -7 0 96.59 11.30 11 -7 0 91.19 14.10 11 -7 0 82.69 10.50 11 -7 0 56.89 11.20 -11 7 0 102.49 14.60 -11 7 0 83.09 12.30 -11 7 0 99.39 16.40 -11 7 0 115.49 16.50 10 -7 0 109.19 11.20 10 -7 0 128.99 10.80 10 -7 0 116.19 10.40 10 -7 0 133.29 16.80 -10 7 0 112.39 15.70 -10 7 0 125.09 15.10 -10 7 0 146.09 19.50 -10 7 0 141.09 14.40 -10 7 0 123.49 16.10 9 -7 0 56.99 14.90 9 -7 0 72.09 8.20 9 -7 0 83.39 16.90 9 -7 0 57.29 9.90 9 -7 0 89.89 10.00 9 -7 0 88.79 8.40 -9 7 0 76.89 11.10 -9 7 0 83.59 13.00 -9 7 0 43.70 10.70 -9 7 0 90.59 13.40 -9 7 0 66.59 11.60 8 -7 0 17.30 5.10 8 -7 0 28.40 4.90 8 -7 0 15.30 3.90 -8 7 0 11.80 5.80 -8 7 0 9.60 5.30 -8 7 0 20.10 5.90 -8 7 0 18.50 7.00 -8 7 0 18.80 5.90 -8 7 0 31.50 7.80 -8 7 0 16.90 6.30 7 -7 0 778.12 25.20 7 -7 0 824.42 32.00 7 -7 0 745.43 19.60 7 -7 0 743.63 26.10 7 -7 0 686.23 36.80 7 -7 0 754.22 19.30 -7 7 0 864.01 25.60 -7 7 0 789.62 30.40 -7 7 0 747.03 27.50 -7 7 0 740.43 28.20 -7 7 0 809.22 30.20 -7 7 0 767.22 28.80 -7 7 0 781.32 26.80 6 -7 0 311.77 14.70 6 -7 0 319.17 18.40 6 -7 0 342.67 14.60 6 -7 0 346.57 15.80 -6 7 0 333.47 18.00 -6 7 0 354.76 17.70 -6 7 0 401.56 20.00 -6 7 0 379.46 14.80 -6 7 0 327.37 15.20 -6 7 0 331.67 16.70 -6 7 0 334.57 17.30 5 -7 0 63.79 6.20 5 -7 0 63.09 6.20 5 -7 0 52.99 7.70 5 -7 0 70.79 6.30 -5 7 0 71.09 6.30 -5 7 0 54.89 6.90 -5 7 0 67.59 8.30 -5 7 0 76.69 10.50 -5 7 0 67.59 6.50 -5 7 0 61.09 7.60 4 -7 0 708.33 18.70 4 -7 0 692.43 18.40 4 -7 0 697.73 25.60 4 -7 0 707.93 19.60 -4 7 0 746.63 21.30 -4 7 0 722.83 19.00 -4 7 0 720.83 21.60 -4 7 0 751.42 17.10 -4 7 0 726.83 19.50 -4 7 0 719.43 24.80 -4 7 0 705.93 20.00 3 -7 0 626.14 14.20 3 -7 0 627.24 22.10 3 -7 0 673.23 14.30 -3 7 0 649.43 17.80 -3 7 0 651.63 17.30 -3 7 0 641.24 16.00 -3 7 0 621.04 15.80 -3 7 0 617.24 25.10 -3 7 0 636.64 16.90 -2 7 0 463.15 12.40 -2 7 0 465.45 11.00 -2 7 0 467.55 10.80 -2 7 0 478.15 19.30 -2 7 0 444.46 16.50 -2 7 0 477.85 12.40 -2 7 0 473.85 14.20 -1 7 0 568.14 16.70 -1 7 0 528.45 19.90 -1 7 0 549.85 16.90 -1 7 0 552.94 12.80 -1 7 0 532.65 11.20 0 7 0 3.80 2.10 0 7 0 5.50 1.70 0 7 0 6.00 3.20 0 7 0 3.30 1.40 0 7 0 5.60 3.10 0 7 0 4.90 1.90 0 7 0 4.80 1.70 -1 -7 0 32.10 5.40 -1 -7 0 29.90 3.30 -1 -7 0 26.40 3.10 1 7 0 31.80 3.30 1 7 0 30.90 3.60 1 7 0 35.30 4.30 1 7 0 32.60 4.00 1 7 0 54.59 9.40 1 7 0 40.00 5.00 1 7 0 29.10 5.50 -2 -7 0 58.99 8.10 -2 -7 0 57.29 5.30 -2 -7 0 57.79 5.50 2 7 0 51.29 5.60 2 7 0 33.80 7.20 2 7 0 53.49 5.50 2 7 0 47.90 5.50 2 7 0 60.69 7.50 2 7 0 46.60 6.30 -3 -7 0 2.20 2.60 -3 -7 0 7.40 4.40 -3 -7 0 9.70 3.70 -3 -7 0 1.60 2.80 3 7 0 5.00 3.30 3 7 0 2.50 2.50 3 7 0 4.00 3.40 3 7 0 5.00 3.30 3 7 0 7.70 3.20 3 7 0 -2.70 2.40 -4 -7 0 30.40 5.70 -4 -7 0 30.50 3.40 -4 -7 0 27.40 6.40 -4 -7 0 24.90 5.70 -4 -7 0 24.60 6.60 -4 -7 0 26.80 3.10 4 7 0 32.90 5.90 4 7 0 28.50 5.80 4 7 0 29.10 6.70 4 7 0 25.70 7.40 4 7 0 33.30 6.30 4 7 0 21.10 5.40 4 7 0 29.00 6.30 -5 -7 0 9.40 3.30 -5 -7 0 19.90 7.30 -5 -7 0 11.30 7.30 -5 -7 0 10.10 3.20 -5 -7 0 22.70 6.30 -5 -7 0 18.00 5.70 5 7 0 9.20 4.90 5 7 0 16.00 5.30 5 7 0 14.60 6.00 5 7 0 9.60 4.30 5 7 0 12.10 5.30 5 7 0 16.80 6.80 5 7 0 17.80 5.10 -6 -7 0 22.80 5.40 -6 -7 0 14.80 5.40 -6 -7 0 25.30 5.40 -6 -7 0 13.80 10.00 6 7 0 23.80 6.10 6 7 0 9.50 5.20 6 7 0 18.70 6.80 6 7 0 13.00 5.50 6 7 0 14.80 6.10 6 7 0 16.20 6.00 6 7 0 15.30 5.30 -7 -7 0 74.19 11.40 -7 -7 0 89.29 13.40 -7 -7 0 90.09 9.00 -7 -7 0 91.19 12.70 -7 -7 0 83.89 12.60 7 7 0 94.39 13.80 7 7 0 130.19 19.80 7 7 0 110.29 14.50 7 7 0 98.19 15.60 7 7 0 127.19 12.10 7 7 0 108.29 15.20 -8 -7 0 43.80 7.90 -8 -7 0 39.90 9.40 -8 -7 0 42.20 8.20 -8 -7 0 68.49 9.50 8 7 0 40.00 9.40 8 7 0 42.40 9.90 8 7 0 35.80 10.70 8 7 0 53.29 11.40 -9 -7 0 -5.50 5.50 -9 -7 0 13.90 5.40 9 7 0 14.40 6.80 9 7 0 9.50 7.00 9 7 0 9.80 7.50 9 7 0 9.90 7.30 9 7 0 19.50 7.00 10 7 0 23.30 9.90 10 7 0 33.30 10.20 10 7 0 34.80 12.50 10 7 0 28.80 9.30 12 -8 0 16.80 5.80 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0 306.17 18.20 -6 8 0 301.77 15.30 -6 8 0 303.97 16.00 -6 8 0 289.37 15.30 -6 8 0 335.87 13.90 -6 8 0 301.17 14.70 5 -8 0 369.96 13.70 5 -8 0 423.16 14.50 5 -8 0 390.36 14.60 5 -8 0 429.16 21.00 -5 8 0 423.16 14.50 -5 8 0 429.86 20.10 -5 8 0 404.46 17.20 -5 8 0 436.36 16.60 -5 8 0 415.66 16.70 -5 8 0 427.96 15.80 4 -8 0 20.30 3.00 4 -8 0 20.90 3.10 -4 8 0 18.80 3.60 -4 8 0 19.30 4.30 -4 8 0 23.90 4.00 -4 8 0 20.30 3.80 -4 8 0 19.50 3.70 -4 8 0 11.90 4.60 -4 8 0 25.20 4.50 -3 8 0 643.84 16.40 -3 8 0 648.64 25.30 -3 8 0 627.84 17.00 -3 8 0 660.43 16.50 -3 8 0 683.33 23.00 -3 8 0 659.53 17.90 -3 8 0 661.43 17.80 -2 8 0 636.44 14.50 -2 8 0 622.54 15.40 -2 8 0 659.53 24.40 -2 8 0 649.14 15.50 -2 8 0 639.74 14.30 -2 8 0 654.13 18.40 -2 8 0 674.33 21.30 -1 8 0 89.99 9.60 -1 8 0 78.49 3.70 -1 8 0 79.49 4.50 -1 8 0 80.99 3.90 -1 8 0 86.29 6.70 -1 8 0 87.09 8.70 -1 8 0 82.59 4.30 -1 8 0 79.49 6.70 0 8 0 423.76 11.20 0 8 0 428.56 18.10 0 8 0 414.06 13.50 0 8 0 421.86 11.80 0 8 0 428.26 12.70 0 8 0 441.46 20.70 0 8 0 426.06 11.90 1 8 0 1084.39 24.70 1 8 0 1136.09 36.60 1 8 0 1084.49 27.20 1 8 0 1098.19 23.40 1 8 0 1134.99 25.60 1 8 0 1105.49 31.60 1 8 0 1125.49 26.40 -2 -8 0 27.60 5.80 -2 -8 0 26.40 4.20 -2 -8 0 25.20 4.00 2 8 0 38.60 7.30 2 8 0 24.90 4.40 2 8 0 24.50 5.00 2 8 0 27.70 4.50 2 8 0 23.80 4.70 2 8 0 25.50 6.90 -3 -8 0 402.26 15.90 -3 -8 0 407.76 18.60 -3 -8 0 418.16 15.80 -3 -8 0 406.26 22.00 3 8 0 382.76 17.40 3 8 0 404.36 18.20 3 8 0 403.46 22.00 3 8 0 404.36 15.60 3 8 0 373.06 19.30 3 8 0 389.16 16.00 -4 -8 0 79.49 8.30 -4 -8 0 54.49 7.80 -4 -8 0 86.99 9.30 4 8 0 59.19 8.90 4 8 0 64.89 9.10 4 8 0 63.49 8.00 4 8 0 82.79 8.90 4 8 0 79.29 11.20 4 8 0 81.49 9.60 4 8 0 77.69 11.10 -5 -8 0 158.78 12.40 -5 -8 0 142.79 11.80 5 8 0 143.19 14.80 5 8 0 144.09 13.50 5 8 0 141.99 11.60 5 8 0 125.39 12.30 5 8 0 128.09 10.90 5 8 0 160.38 13.30 5 8 0 149.39 11.70 5 8 0 104.59 15.50 -6 -8 0 43.90 5.50 -6 -8 0 54.39 5.90 -6 -8 0 26.20 7.00 -6 -8 0 33.20 7.40 -6 -8 0 46.20 11.60 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143.49 12.20 5 11 0 147.79 21.20 -6 -11 0 13.80 6.00 6 11 0 1.80 5.50 6 11 0 18.90 6.10 6 11 0 7.50 6.80 6 11 0 12.90 6.10 6 11 0 14.40 6.00 6 11 0 1.40 7.20 7 11 0 149.39 15.60 7 11 0 267.87 42.90 7 11 0 198.28 31.30 7 11 0 163.88 17.20 7 11 0 162.08 23.50 10 -12 0 12.50 5.70 -10 12 0 4.40 7.30 -10 12 0 8.40 6.70 -10 12 0 17.20 10.20 -10 12 0 9.60 7.20 9 -12 0 80.79 8.70 -9 12 0 63.09 15.40 -9 12 0 62.79 10.20 -9 12 0 51.69 11.60 -9 12 0 55.19 11.70 -9 12 0 46.80 9.90 -8 12 0 242.08 15.80 -8 12 0 225.98 19.60 -8 12 0 234.98 21.80 -8 12 0 270.77 21.50 -8 12 0 236.48 15.60 -7 12 0 89.19 15.70 -7 12 0 79.19 6.90 -7 12 0 81.69 9.00 -7 12 0 57.19 8.50 -7 12 0 70.99 10.20 -7 12 0 58.99 8.80 -7 12 0 55.89 11.00 -6 12 0 49.90 7.00 -6 12 0 60.69 12.80 -6 12 0 58.09 7.40 -6 12 0 60.09 8.20 -6 12 0 54.29 7.60 -5 12 0 309.27 13.30 -5 12 0 366.06 13.20 -5 12 0 365.66 13.70 -5 12 0 368.46 16.20 -5 12 0 404.56 21.60 -5 12 0 401.46 24.60 -4 12 0 53.69 11.80 -4 12 0 45.40 5.80 -4 12 0 39.50 5.80 -4 12 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55.89 4 1 -3 2706.83 53.99 4 1 -3 2736.73 57.29 4 1 -3 2737.43 55.59 -4 -1 3 2681.03 54.39 -4 -1 3 2725.93 55.99 -4 -1 3 2794.52 55.79 -4 -1 3 2822.82 56.99 -4 -1 3 2734.33 56.99 -4 -1 3 2804.32 54.39 -4 -1 3 2893.21 58.29 3 1 -3 498.35 14.70 3 1 -3 504.05 15.40 3 1 -3 488.75 14.50 3 1 -3 511.35 16.00 3 1 -3 489.85 14.80 3 1 -3 512.75 14.50 3 1 -3 480.25 15.60 -3 -1 3 487.95 15.50 -3 -1 3 512.75 15.00 -3 -1 3 507.65 14.50 -3 -1 3 507.45 14.60 -3 -1 3 496.75 15.90 -3 -1 3 492.75 14.80 2 1 -3 23.30 3.20 2 1 -3 11.40 2.30 2 1 -3 21.80 3.30 2 1 -3 13.70 2.40 2 1 -3 14.80 2.70 2 1 -3 17.30 2.70 -2 -1 3 14.70 2.20 -2 -1 3 15.00 2.40 -2 -1 3 22.40 2.30 -2 -1 3 25.40 3.40 -2 -1 3 9.10 1.80 -2 -1 3 17.10 3.00 -2 -1 3 17.30 2.70 -2 -1 3 18.00 3.00 1 1 -3 1980.50 37.80 1 1 -3 1981.50 38.60 1 1 -3 1941.01 37.50 1 1 -3 1929.21 37.20 1 1 -3 1991.10 37.00 1 1 -3 1959.50 37.50 1 1 -3 2008.10 36.50 -1 -1 3 1958.40 38.50 -1 -1 3 1996.00 37.90 -1 -1 3 1954.20 37.80 -1 -1 3 1962.70 37.40 -1 -1 3 2011.40 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222.18 12.80 -7 -3 4 213.58 11.30 -7 -3 4 231.28 15.40 -7 -3 4 229.28 13.40 -7 -3 4 192.58 13.10 6 3 -4 51.29 7.90 6 3 -4 40.80 6.30 6 3 -4 32.70 6.40 6 3 -4 45.30 7.20 6 3 -4 47.30 7.10 6 3 -4 43.00 7.50 6 3 -4 48.80 8.50 -6 -3 4 56.99 8.80 -6 -3 4 40.30 6.30 -6 -3 4 45.90 6.60 -6 -3 4 35.10 6.90 -6 -3 4 36.60 6.80 -6 -3 4 50.09 8.40 5 3 -4 11.00 3.70 5 3 -4 16.30 4.40 5 3 -4 17.60 4.80 5 3 -4 9.10 3.70 5 3 -4 20.50 4.50 5 3 -4 17.10 4.50 5 3 -4 23.50 4.80 -5 -3 4 15.30 4.10 -5 -3 4 23.40 4.20 -5 -3 4 25.20 5.60 -5 -3 4 11.10 3.80 -5 -3 4 11.60 3.90 -5 -3 4 24.60 5.20 -5 -3 4 19.40 4.20 4 3 -4 2015.60 44.20 4 3 -4 2013.80 45.60 4 3 -4 2065.99 43.40 4 3 -4 2065.09 47.30 4 3 -4 1971.30 45.30 4 3 -4 2020.80 44.00 4 3 -4 2091.79 43.10 -4 -3 4 2050.99 48.30 -4 -3 4 2038.10 44.40 -4 -3 4 2062.69 45.60 -4 -3 4 2073.49 43.70 -4 -3 4 1958.80 42.10 -4 -3 4 2050.19 43.20 -4 -3 4 2031.90 46.00 3 3 -4 25.50 3.90 3 3 -4 26.00 4.70 3 3 -4 27.10 3.60 3 3 -4 34.80 4.50 3 3 -4 32.10 4.20 3 3 -4 34.40 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129.89 18.20 -4 11 -9 77.19 12.60 -4 11 -9 102.39 12.70 -4 11 -9 133.69 12.30 -4 11 -9 127.59 11.30 4 -11 9 128.59 11.10 4 -11 9 139.29 17.90 -5 11 -9 2.40 5.40 -5 11 -9 1.70 4.40 -5 11 -9 -0.60 5.40 -5 11 -9 8.50 6.40 -5 11 -9 2.70 5.00 -5 11 -9 2.10 5.40 5 -11 9 15.80 5.40 -6 11 -9 44.20 10.10 -6 11 -9 60.99 14.00 -6 11 -9 48.10 10.50 -6 11 -9 42.30 9.20 -6 11 -9 64.29 13.10 -7 11 -9 129.39 16.50 -7 11 -9 141.59 15.70 -7 11 -9 139.59 15.70 -7 11 -9 128.29 11.00 -7 11 -9 101.89 16.90 -7 11 -9 99.49 14.40 -8 11 -9 18.30 7.80 -8 11 -9 22.00 7.90 -8 11 -9 24.30 6.40 -8 11 -9 29.30 9.20 -8 11 -9 26.20 8.90 -8 11 -9 19.80 9.40 11 10 -9 23.30 11.60 11 10 -9 14.30 8.30 11 10 -9 4.50 7.40 11 10 -9 4.50 7.70 11 10 -9 9.50 6.70 -11 -10 9 -5.60 5.40 -11 -10 9 4.00 8.50 10 10 -9 3.10 6.80 10 10 -9 -4.60 5.60 10 10 -9 1.60 6.70 10 10 -9 10.50 7.70 10 10 -9 -1.70 4.70 10 10 -9 3.80 5.60 -10 -10 9 2.70 4.10 9 10 -9 183.68 16.80 9 10 -9 172.68 16.80 9 10 -9 123.29 17.90 9 10 -9 161.18 14.50 9 10 -9 172.88 16.30 9 10 -9 177.08 23.70 -9 -10 9 154.58 9.10 -9 -10 9 160.78 8.70 -9 -10 9 145.99 16.40 8 10 -9 36.80 10.00 8 10 -9 24.90 6.40 8 10 -9 18.40 6.60 8 10 -9 10.40 6.50 8 10 -9 26.40 7.50 8 10 -9 22.40 7.80 8 10 -9 22.00 7.30 -8 -10 9 31.20 7.80 -8 -10 9 21.30 8.80 7 10 -9 413.96 20.80 7 10 -9 410.76 21.80 7 10 -9 408.86 21.90 7 10 -9 374.96 20.20 7 10 -9 456.05 27.40 7 10 -9 417.36 21.80 7 10 -9 387.46 20.50 -7 -10 9 439.56 21.00 -7 -10 9 374.66 21.90 6 10 -9 845.72 30.40 6 10 -9 922.51 31.90 6 10 -9 850.71 29.30 6 10 -9 872.11 29.50 6 10 -9 879.41 33.20 6 10 -9 890.91 31.00 6 10 -9 847.62 37.10 -6 -10 9 821.52 31.00 -6 -10 9 896.11 30.80 -6 -10 9 874.31 29.50 5 10 -9 -5.00 3.00 5 10 -9 0.90 3.30 5 10 -9 7.60 4.90 5 10 -9 0.80 3.10 5 10 -9 0.70 4.50 5 10 -9 4.10 3.90 5 10 -9 2.40 3.70 -5 -10 9 -0.50 3.30 -5 -10 9 1.10 3.00 4 10 -9 646.74 29.50 4 10 -9 660.73 20.90 4 10 -9 689.73 23.70 4 10 -9 668.13 29.90 4 10 -9 684.63 23.60 4 10 -9 678.93 23.30 4 10 -9 695.33 24.80 -4 -10 9 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125.79 12.50 7 6 -9 144.39 12.20 -7 -6 9 145.39 13.00 -7 -6 9 133.99 11.10 -7 -6 9 132.59 11.30 -7 -6 9 115.79 12.00 -7 -6 9 114.99 10.90 6 6 -9 7.00 4.20 6 6 -9 5.40 3.60 6 6 -9 13.00 5.40 6 6 -9 18.90 6.00 6 6 -9 15.10 5.20 6 6 -9 15.50 5.10 -6 -6 9 9.10 4.90 -6 -6 9 14.80 4.70 -6 -6 9 9.00 4.80 -6 -6 9 4.20 3.50 -6 -6 9 8.10 4.60 -6 -6 9 7.60 4.40 5 6 -9 33.70 8.10 5 6 -9 38.00 6.90 5 6 -9 41.10 7.80 5 6 -9 44.40 8.20 5 6 -9 40.90 7.30 5 6 -9 41.00 7.00 -5 -6 9 34.30 6.80 -5 -6 9 43.40 7.00 -5 -6 9 35.00 6.40 -5 -6 9 33.60 6.10 -5 -6 9 30.30 6.60 -5 -6 9 47.50 9.90 4 6 -9 20.40 5.40 4 6 -9 22.40 5.60 4 6 -9 35.40 6.50 4 6 -9 30.10 7.10 4 6 -9 33.50 6.30 4 6 -9 26.30 6.20 4 6 -9 31.40 6.10 -4 -6 9 28.90 6.30 -4 -6 9 24.60 5.70 -4 -6 9 34.70 5.80 -4 -6 9 36.40 5.40 -4 -6 9 37.20 5.70 -4 -6 9 33.40 6.80 3 6 -9 227.38 8.90 3 6 -9 224.08 14.40 3 6 -9 215.88 12.90 3 6 -9 229.98 13.90 3 6 -9 200.08 13.00 3 6 -9 223.38 12.20 -3 -6 9 216.68 13.40 -3 -6 9 214.48 13.00 -3 -6 9 227.18 11.30 -3 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14.00 -7 -5 9 138.09 11.60 -7 -5 9 156.28 12.10 -7 -5 9 130.79 13.00 -7 -5 9 138.99 7.30 6 5 -9 105.19 10.70 6 5 -9 103.49 11.00 6 5 -9 98.99 10.30 6 5 -9 100.49 10.00 6 5 -9 103.39 10.10 6 5 -9 119.79 11.70 -6 -5 9 104.59 10.80 -6 -5 9 102.49 10.60 -6 -5 9 99.39 9.50 -6 -5 9 102.29 11.60 -6 -5 9 97.99 5.90 -6 -5 9 111.39 9.90 -6 -5 9 102.29 9.20 5 5 -9 2.70 3.40 5 5 -9 5.30 4.30 5 5 -9 5.90 3.80 5 5 -9 6.20 4.10 5 5 -9 4.70 3.70 5 5 -9 9.70 4.60 -5 -5 9 -0.60 3.10 -5 -5 9 6.80 3.00 -5 -5 9 11.50 4.60 -5 -5 9 0.90 2.80 -5 -5 9 1.90 3.30 -5 -5 9 3.50 2.20 -5 -5 9 3.70 4.10 4 5 -9 9.10 3.90 4 5 -9 10.60 2.90 4 5 -9 9.70 4.10 4 5 -9 20.80 6.00 4 5 -9 12.40 4.20 4 5 -9 15.50 5.20 4 5 -9 11.60 4.60 4 5 -9 18.50 5.50 -4 -5 9 7.30 4.20 -4 -5 9 15.30 4.20 -4 -5 9 17.60 4.00 -4 -5 9 9.10 4.00 -4 -5 9 11.60 3.00 -4 -5 9 6.80 4.10 -4 -5 9 14.50 4.70 3 5 -9 42.00 6.90 3 5 -9 43.00 6.30 3 5 -9 46.90 5.50 3 5 -9 61.59 9.20 3 5 -9 45.70 7.60 3 5 -9 41.80 7.60 3 5 -9 34.00 6.10 -3 -5 9 48.70 5.20 -3 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3.40 1 -5 9 3.30 3.90 1 -5 9 2.00 2.80 -2 5 -9 778.42 29.10 -2 5 -9 798.72 28.70 -2 5 -9 821.42 29.30 -2 5 -9 807.52 27.40 -2 5 -9 825.22 31.20 -2 5 -9 774.42 27.80 2 -5 9 770.12 27.40 2 -5 9 816.72 21.60 2 -5 9 790.32 29.80 2 -5 9 790.42 31.10 2 -5 9 795.32 28.00 2 -5 9 771.72 25.70 2 -5 9 776.62 25.10 -3 5 -9 506.85 23.20 -3 5 -9 522.05 22.50 -3 5 -9 487.15 18.10 -3 5 -9 513.75 23.80 -3 5 -9 526.05 24.70 -3 5 -9 501.85 24.10 -3 5 -9 524.85 25.50 3 -5 9 552.14 26.70 3 -5 9 510.45 23.80 3 -5 9 483.55 22.20 3 -5 9 462.35 22.00 3 -5 9 482.45 19.50 3 -5 9 528.75 20.60 3 -5 9 520.95 18.30 -4 5 -9 112.09 12.90 -4 5 -9 106.49 11.50 -4 5 -9 114.79 14.20 -4 5 -9 113.19 12.20 -4 5 -9 111.89 9.50 -4 5 -9 96.89 13.40 -4 5 -9 97.09 13.00 -4 5 -9 87.19 12.50 4 -5 9 109.19 10.30 4 -5 9 120.59 11.70 4 -5 9 127.69 12.30 4 -5 9 108.49 14.90 -5 5 -9 230.78 18.40 -5 5 -9 231.48 16.70 -5 5 -9 215.38 16.70 -5 5 -9 222.38 18.00 -5 5 -9 189.48 13.40 -5 5 -9 231.68 18.70 -5 5 -9 229.68 17.50 -5 5 -9 188.78 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399.56 29.40 -13 -4 9 410.46 25.70 -13 -4 9 417.56 22.00 -13 -4 9 380.36 21.10 -13 -4 9 396.46 29.60 -13 -4 9 412.16 25.90 12 4 -9 48.50 11.90 12 4 -9 14.80 7.10 12 4 -9 47.40 12.80 12 4 -9 33.90 9.80 -12 -4 9 36.70 9.70 -12 -4 9 56.69 9.00 -12 -4 9 36.70 7.60 -12 -4 9 33.70 11.10 -12 -4 9 27.60 8.90 11 4 -9 351.36 24.90 11 4 -9 374.96 23.90 11 4 -9 361.16 23.40 11 4 -9 392.66 26.10 -11 -4 9 365.56 23.00 -11 -4 9 402.96 23.20 -11 -4 9 350.06 25.00 -11 -4 9 382.16 31.30 -11 -4 9 402.76 27.80 -11 -4 9 348.17 22.10 -11 -4 9 338.07 17.70 10 4 -9 333.07 25.30 10 4 -9 301.47 21.90 10 4 -9 349.37 23.50 10 4 -9 348.07 20.90 10 4 -9 314.47 23.00 10 4 -9 334.07 21.70 -10 -4 9 372.86 24.10 -10 -4 9 355.96 20.70 -10 -4 9 333.87 26.60 -10 -4 9 360.96 16.80 -10 -4 9 351.56 23.80 9 4 -9 8.50 5.90 9 4 -9 7.10 5.70 9 4 -9 7.10 5.60 9 4 -9 15.40 6.30 -9 -4 9 0.50 3.00 -9 -4 9 6.30 6.60 -9 -4 9 4.40 4.40 -9 -4 9 2.80 4.40 -9 -4 9 4.40 4.60 -9 -4 9 9.10 3.90 -9 -4 9 -2.60 5.20 8 4 -9 484.55 24.80 8 4 -9 475.75 23.80 8 4 -9 526.95 23.40 8 4 -9 543.45 26.50 8 4 -9 477.35 22.60 8 4 -9 463.75 22.20 -8 -4 9 441.96 24.40 -8 -4 9 512.25 17.90 -8 -4 9 478.95 25.90 -8 -4 9 504.75 22.80 -8 -4 9 475.95 24.80 -8 -4 9 489.15 23.50 -8 -4 9 507.75 23.30 7 4 -9 115.39 10.90 7 4 -9 116.29 11.80 7 4 -9 107.49 11.80 7 4 -9 114.59 11.10 7 4 -9 128.69 12.50 7 4 -9 112.29 10.90 -7 -4 9 130.69 12.80 -7 -4 9 124.29 12.60 -7 -4 9 115.59 7.80 -7 -4 9 81.79 11.00 -7 -4 9 124.69 11.20 -7 -4 9 117.59 11.10 -7 -4 9 99.49 9.90 6 4 -9 40.50 8.20 6 4 -9 38.10 6.70 6 4 -9 37.10 6.90 6 4 -9 20.70 5.70 6 4 -9 34.10 7.00 6 4 -9 33.10 6.90 -6 -4 9 20.20 5.80 -6 -4 9 36.40 7.00 -6 -4 9 33.00 8.00 -6 -4 9 34.60 6.90 -6 -4 9 38.40 5.30 -6 -4 9 19.60 5.90 -6 -4 9 32.70 6.60 5 4 -9 155.48 11.70 5 4 -9 157.28 11.40 5 4 -9 171.68 12.70 5 4 -9 159.38 11.20 5 4 -9 162.28 12.10 5 4 -9 161.18 11.90 5 4 -9 148.29 12.30 -5 -4 9 167.68 10.50 -5 -4 9 158.98 8.60 -5 -4 9 166.28 12.70 -5 -4 9 148.29 12.60 -5 -4 9 150.58 11.30 -5 -4 9 144.39 12.30 4 4 -9 120.39 10.40 4 4 -9 133.49 10.50 4 4 -9 119.49 9.70 4 4 -9 108.09 10.30 4 4 -9 114.19 9.80 4 4 -9 112.19 9.60 4 4 -9 127.39 10.30 4 4 -9 109.79 7.40 -4 -4 9 116.89 10.60 -4 -4 9 129.39 9.70 -4 -4 9 132.99 11.30 -4 -4 9 114.19 10.20 -4 -4 9 119.29 9.70 -4 -4 9 108.69 7.40 -4 -4 9 107.99 7.70 3 4 -9 48.20 7.10 3 4 -9 55.99 5.90 3 4 -9 63.89 9.40 3 4 -9 49.90 8.00 3 4 -9 38.40 6.30 3 4 -9 45.80 7.20 3 4 -9 46.50 7.20 -3 -4 9 60.29 7.70 -3 -4 9 53.79 6.60 -3 -4 9 53.79 8.30 -3 -4 9 58.39 5.30 -3 -4 9 63.29 9.70 -3 -4 9 45.90 7.20 2 4 -9 7.70 4.00 2 4 -9 5.30 3.80 2 4 -9 2.50 3.30 2 4 -9 2.20 3.30 2 4 -9 2.10 2.40 2 4 -9 2.60 3.50 2 4 -9 5.50 3.50 -2 -4 9 1.30 3.10 -2 -4 9 1.30 3.40 -2 -4 9 6.00 3.30 -2 -4 9 7.50 3.30 1 4 -9 129.69 10.40 1 4 -9 138.39 9.80 1 4 -9 122.49 10.90 1 4 -9 118.99 9.90 1 4 -9 141.69 10.60 1 4 -9 148.59 11.00 1 4 -9 127.39 9.40 -1 -4 9 127.39 10.20 -1 -4 9 123.99 9.70 -1 -4 9 124.19 10.30 -1 -4 9 140.19 10.60 -1 -4 9 143.79 11.80 -1 -4 9 139.19 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5.00 7 -4 9 -0.80 6.40 7 -4 9 0.60 5.40 7 -4 9 -0.10 4.10 7 -4 9 3.20 4.60 -8 4 -9 -4.60 5.60 -8 4 -9 2.80 6.60 -8 4 -9 3.60 7.60 -8 4 -9 5.80 8.90 -8 4 -9 -11.10 6.80 -8 4 -9 2.30 5.50 8 -4 9 8.30 6.90 8 -4 9 -0.20 4.60 8 -4 9 13.40 8.60 8 -4 9 -1.30 5.40 -9 4 -9 35.60 13.10 -9 4 -9 62.89 12.40 -9 4 -9 35.10 11.30 -9 4 -9 22.30 13.60 -9 4 -9 21.10 12.40 9 -4 9 23.90 11.90 9 -4 9 27.50 9.70 9 -4 9 50.89 8.90 9 -4 9 27.40 9.00 14 3 -9 37.50 12.20 14 3 -9 18.70 9.20 -14 -3 9 24.90 10.20 -14 -3 9 30.80 10.00 -14 -3 9 20.10 7.70 -14 -3 9 30.20 12.50 13 3 -9 38.10 12.00 13 3 -9 24.80 8.40 13 3 -9 10.30 8.30 -13 -3 9 29.10 8.80 -13 -3 9 26.10 10.80 -13 -3 9 26.90 9.10 -13 -3 9 30.00 7.60 12 3 -9 15.00 6.50 12 3 -9 44.00 10.90 -12 -3 9 16.90 9.30 -12 -3 9 17.40 7.50 -12 -3 9 20.40 8.20 -12 -3 9 20.40 7.00 11 3 -9 151.58 19.30 11 3 -9 181.18 17.70 11 3 -9 200.98 17.20 -11 -3 9 174.68 18.30 -11 -3 9 169.18 18.00 -11 -3 9 188.18 16.90 -11 -3 9 148.59 15.10 -11 -3 9 213.18 19.70 -11 -3 9 186.18 14.00 10 3 -9 83.39 13.10 10 3 -9 86.09 13.50 10 3 -9 102.49 13.10 10 3 -9 89.59 12.20 -10 -3 9 128.09 21.00 -10 -3 9 102.89 10.20 -10 -3 9 113.69 14.60 -10 -3 9 115.09 14.50 -10 -3 9 100.49 15.20 -10 -3 9 106.59 16.10 9 3 -9 4.60 4.60 9 3 -9 -1.30 4.30 9 3 -9 -2.20 3.10 9 3 -9 -4.10 4.70 9 3 -9 3.10 4.70 -9 -3 9 2.70 5.40 -9 -3 9 0.30 4.80 -9 -3 9 -1.40 3.90 -9 -3 9 2.60 4.60 -9 -3 9 -0.10 3.80 -9 -3 9 -4.20 4.20 -9 -3 9 -0.20 3.00 -9 -3 9 5.40 4.60 8 3 -9 149.49 13.80 8 3 -9 155.38 13.70 8 3 -9 173.68 14.00 8 3 -9 178.78 15.50 8 3 -9 165.18 13.40 -8 -3 9 149.59 19.80 -8 -3 9 185.58 15.60 -8 -3 9 184.38 15.80 -8 -3 9 176.78 13.80 -8 -3 9 170.78 13.60 -8 -3 9 155.58 10.80 -8 -3 9 161.28 13.50 7 3 -9 291.97 16.80 7 3 -9 305.57 17.30 7 3 -9 295.07 18.70 7 3 -9 264.47 17.10 7 3 -9 301.77 17.40 7 3 -9 311.77 17.10 -7 -3 9 282.97 18.20 -7 -3 9 287.47 13.60 -7 -3 9 292.57 16.60 -7 -3 9 282.57 16.80 -7 -3 9 291.57 18.50 -7 -3 9 323.27 17.30 -7 -3 9 294.27 18.50 6 3 -9 32.90 7.10 6 3 -9 40.00 7.90 6 3 -9 24.20 6.50 6 3 -9 33.50 7.50 6 3 -9 28.80 6.10 6 3 -9 38.00 7.30 -6 -3 9 47.30 7.80 -6 -3 9 28.20 5.30 -6 -3 9 24.50 6.10 -6 -3 9 27.50 7.10 -6 -3 9 38.30 6.90 -6 -3 9 25.10 6.40 -6 -3 9 32.60 6.10 5 3 -9 291.97 16.00 5 3 -9 279.37 16.00 5 3 -9 279.17 14.90 5 3 -9 271.97 16.50 5 3 -9 269.17 14.90 5 3 -9 260.17 14.80 5 3 -9 307.87 15.40 -5 -3 9 278.77 13.70 -5 -3 9 309.57 15.70 -5 -3 9 282.57 16.80 -5 -3 9 278.87 12.60 -5 -3 9 292.67 15.50 -5 -3 9 280.27 19.30 -5 -3 9 281.57 16.80 4 3 -9 3.70 3.40 4 3 -9 3.20 3.40 4 3 -9 4.10 3.40 4 3 -9 7.70 4.00 4 3 -9 4.30 2.90 4 3 -9 0.80 2.60 4 3 -9 6.10 3.90 4 3 -9 4.20 3.70 -4 -3 9 -1.00 2.80 -4 -3 9 2.30 3.20 -4 -3 9 4.40 3.90 -4 -3 9 4.90 2.80 -4 -3 9 6.20 3.30 -4 -3 9 3.70 2.50 3 3 -9 580.84 21.70 3 3 -9 561.24 21.10 3 3 -9 584.94 20.70 3 3 -9 585.04 19.70 3 3 -9 578.14 21.80 3 3 -9 586.24 21.20 3 3 -9 608.34 24.00 3 3 -9 589.04 22.50 -3 -3 9 565.44 20.60 -3 -3 9 600.34 23.90 -3 -3 9 552.34 19.20 -3 -3 9 562.04 22.50 -3 -3 9 600.54 22.00 -3 -3 9 567.74 22.30 2 3 -9 9.60 4.30 2 3 -9 14.60 4.60 2 3 -9 14.70 4.50 2 3 -9 7.30 3.30 2 3 -9 11.30 4.10 2 3 -9 7.00 4.20 2 3 -9 10.10 4.40 -2 -3 9 4.80 3.50 -2 -3 9 10.10 3.90 -2 -3 9 15.30 4.90 -2 -3 9 12.60 4.70 -2 -3 9 3.70 3.20 -2 -3 9 6.60 3.30 -2 -3 9 9.80 4.60 1 3 -9 80.39 8.50 1 3 -9 70.49 8.20 1 3 -9 70.59 9.70 1 3 -9 66.89 8.40 1 3 -9 67.39 7.60 1 3 -9 63.69 8.80 1 3 -9 66.99 7.40 -1 -3 9 72.69 10.30 -1 -3 9 59.69 8.20 -1 -3 9 73.69 7.90 -1 -3 9 71.09 9.70 -1 -3 9 81.69 6.70 -1 -3 9 70.69 10.10 -1 -3 9 76.19 10.20 0 3 -9 -0.70 2.70 0 3 -9 -1.50 3.00 0 3 -9 -1.60 2.90 0 3 -9 -0.70 2.90 0 3 -9 1.70 3.40 0 -3 9 0.10 2.10 0 -3 9 0.30 2.70 0 -3 9 1.40 2.40 0 -3 9 1.00 2.70 0 -3 9 5.40 4.30 0 -3 9 1.90 2.90 0 -3 9 0.40 3.50 -1 3 -9 49.40 8.00 -1 3 -9 54.49 8.10 -1 3 -9 56.79 9.60 -1 3 -9 54.99 9.00 -1 3 -9 47.80 9.10 -1 3 -9 57.89 9.30 1 -3 9 43.80 6.80 1 -3 9 49.10 8.60 1 -3 9 61.99 9.10 1 -3 9 39.00 6.60 1 -3 9 55.79 10.00 1 -3 9 53.29 9.10 1 -3 9 56.79 6.40 1 -3 9 40.40 7.10 -2 3 -9 27.00 6.50 -2 3 -9 23.60 6.70 -2 3 -9 33.80 7.40 -2 3 -9 29.20 6.90 -2 3 -9 29.80 7.90 -2 3 -9 29.10 6.70 2 -3 9 18.50 5.60 2 -3 9 23.60 6.40 2 -3 9 28.20 6.10 2 -3 9 31.10 6.00 2 -3 9 18.00 5.00 2 -3 9 15.20 5.40 2 -3 9 37.50 6.90 2 -3 9 25.00 7.50 -3 3 -9 104.59 11.40 -3 3 -9 105.79 9.70 -3 3 -9 130.19 12.50 -3 3 -9 110.19 11.30 -3 3 -9 109.69 12.00 -3 3 -9 110.29 12.30 -3 3 -9 129.69 11.80 -3 3 -9 117.29 12.80 3 -3 9 125.69 11.80 3 -3 9 122.29 13.60 3 -3 9 122.19 12.60 3 -3 9 114.59 10.20 3 -3 9 124.99 11.70 3 -3 9 127.39 10.50 3 -3 9 131.79 11.20 -4 3 -9 12.00 6.00 -4 3 -9 6.60 4.80 -4 3 -9 18.70 6.60 -4 3 -9 7.60 7.70 -4 3 -9 6.40 5.70 -4 3 -9 3.70 3.80 -4 3 -9 9.20 5.40 4 -3 9 8.30 4.20 4 -3 9 6.30 5.40 4 -3 9 5.60 5.00 4 -3 9 18.70 7.40 4 -3 9 5.80 5.70 4 -3 9 8.60 4.40 4 -3 9 9.70 5.10 -5 3 -9 93.19 14.40 -5 3 -9 94.79 13.90 -5 3 -9 81.29 13.00 -5 3 -9 75.09 11.20 -5 3 -9 98.79 14.00 -5 3 -9 120.59 11.70 -5 3 -9 64.09 11.00 5 -3 9 101.39 14.60 5 -3 9 110.69 16.30 5 -3 9 85.09 9.80 5 -3 9 93.29 12.90 5 -3 9 83.39 12.60 5 -3 9 78.59 12.20 -6 3 -9 152.08 14.80 -6 3 -9 175.28 16.00 -6 3 -9 196.28 19.10 -6 3 -9 118.39 16.70 -6 3 -9 163.88 16.70 -6 3 -9 168.08 14.80 6 -3 9 155.28 20.40 6 -3 9 165.68 14.80 6 -3 9 154.88 16.00 6 -3 9 140.49 13.00 6 -3 9 153.38 15.50 6 -3 9 157.38 13.20 -7 3 -9 114.19 26.20 -7 3 -9 102.69 14.20 -7 3 -9 122.99 15.70 -7 3 -9 88.49 14.00 -7 3 -9 117.79 17.30 -7 3 -9 72.59 11.50 7 -3 9 101.59 17.40 7 -3 9 129.19 17.20 7 -3 9 122.69 13.70 7 -3 9 102.19 11.30 -8 3 -9 89.39 14.50 -8 3 -9 51.19 11.80 -8 3 -9 97.99 18.00 -8 3 -9 78.69 15.40 -8 3 -9 61.19 13.90 8 -3 9 94.99 16.20 8 -3 9 98.89 14.00 8 -3 9 99.59 18.80 -9 3 -9 -1.10 7.60 -9 3 -9 2.20 7.30 -9 3 -9 -2.90 4.90 -9 3 -9 6.70 7.10 9 -3 9 -2.70 7.20 9 -3 9 8.80 9.90 9 -3 9 5.00 6.70 9 -3 9 -2.00 6.40 14 2 -9 15.20 8.40 14 2 -9 -5.30 5.10 14 2 -9 -2.50 7.80 -14 -2 9 10.90 12.00 -14 -2 9 2.20 9.40 -14 -2 9 4.50 7.10 -14 -2 9 9.60 7.40 13 2 -9 2.50 6.60 13 2 -9 4.30 5.50 13 2 -9 -7.40 6.50 -13 -2 9 1.50 6.50 -13 -2 9 -5.10 5.30 -13 -2 9 11.80 8.90 -13 -2 9 10.80 7.30 12 2 -9 32.50 8.50 12 2 -9 28.60 9.60 12 2 -9 21.70 9.20 12 2 -9 49.50 11.30 -12 -2 9 31.40 11.90 -12 -2 9 42.70 9.80 -12 -2 9 36.70 9.70 -12 -2 9 28.90 7.90 -12 -2 9 41.60 10.60 -12 -2 9 18.20 10.10 11 2 -9 37.50 9.70 11 2 -9 32.60 9.60 11 2 -9 70.39 12.10 11 2 -9 62.99 11.50 -11 -2 9 65.09 12.80 -11 -2 9 45.00 11.70 -11 -2 9 41.10 17.30 -11 -2 9 39.40 10.20 -11 -2 9 48.00 10.60 -11 -2 9 46.80 8.80 10 2 -9 28.70 8.90 10 2 -9 28.40 7.30 10 2 -9 34.10 8.30 10 2 -9 36.30 9.10 10 2 -9 21.40 6.90 10 2 -9 39.80 9.80 -10 -2 9 23.30 7.40 -10 -2 9 35.00 7.50 -10 -2 9 23.40 7.30 -10 -2 9 23.60 8.00 -10 -2 9 26.70 8.60 -10 -2 9 43.70 10.50 -10 -2 9 33.30 10.70 9 2 -9 431.26 22.80 9 2 -9 532.35 24.40 9 2 -9 524.15 26.90 9 2 -9 519.95 27.10 9 2 -9 415.46 25.70 9 2 -9 472.75 23.40 -9 -2 9 511.15 27.50 -9 -2 9 462.65 24.00 -9 -2 9 497.75 26.00 -9 -2 9 509.95 27.00 -9 -2 9 479.65 24.50 -9 -2 9 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3 -10 53.39 11.90 -6 3 -10 62.09 13.00 -6 3 -10 43.40 10.10 -6 3 -10 53.39 10.20 -6 3 -10 49.80 10.90 6 -3 10 33.60 6.90 6 -3 10 21.70 8.80 6 -3 10 64.99 13.80 6 -3 10 48.10 10.60 6 -3 10 49.70 11.00 -7 3 -10 7.20 8.80 -7 3 -10 5.20 7.20 -7 3 -10 1.40 6.40 -7 3 -10 10.50 6.60 -7 3 -10 15.70 7.40 -7 3 -10 2.30 6.60 7 -3 10 -3.00 6.20 7 -3 10 -3.00 5.90 -8 3 -10 20.40 7.50 -8 3 -10 26.20 10.20 -8 3 -10 28.60 10.80 -8 3 -10 12.60 9.20 8 -3 10 19.30 7.40 8 -3 10 26.10 10.40 8 -3 10 32.20 9.30 8 -3 10 33.60 12.90 14 2 -10 165.58 16.90 14 2 -10 166.18 20.50 14 2 -10 204.98 22.80 -14 -2 10 132.49 21.00 -14 -2 10 151.18 22.30 -14 -2 10 183.38 17.50 -14 -2 10 144.29 19.40 13 2 -10 14.60 7.90 13 2 -10 15.60 6.60 13 2 -10 2.10 7.40 -13 -2 10 2.80 6.80 -13 -2 10 7.40 7.50 -13 -2 10 2.60 6.90 -13 -2 10 3.50 5.40 12 2 -10 163.18 18.40 12 2 -10 138.39 18.90 12 2 -10 173.28 17.00 12 2 -10 174.38 21.50 12 2 -10 143.79 15.10 -12 -2 10 145.79 19.90 -12 -2 10 146.89 18.00 -12 -2 10 154.18 17.30 -12 -2 10 170.38 18.80 -12 -2 10 140.19 13.90 11 2 -10 54.39 11.30 11 2 -10 65.09 12.90 11 2 -10 34.70 9.70 11 2 -10 69.39 12.10 -11 -2 10 60.89 11.30 -11 -2 10 53.29 11.60 -11 -2 10 54.99 11.00 -11 -2 10 43.30 8.40 -11 -2 10 72.39 19.50 -11 -2 10 71.99 13.90 10 2 -10 2.50 4.70 10 2 -10 11.60 6.90 10 2 -10 5.10 5.60 10 2 -10 5.40 5.00 10 2 -10 3.90 6.40 10 2 -10 8.50 5.20 -10 -2 10 8.10 5.10 -10 -2 10 16.50 6.80 -10 -2 10 2.30 5.50 -10 -2 10 1.50 6.60 -10 -2 10 5.60 5.90 -10 -2 10 -1.20 6.60 9 2 -10 163.48 14.40 9 2 -10 170.68 14.20 9 2 -10 188.48 17.20 9 2 -10 163.08 15.60 -9 -2 10 177.38 15.10 -9 -2 10 169.78 14.70 -9 -2 10 179.58 13.30 -9 -2 10 188.58 17.30 -9 -2 10 188.28 17.50 -9 -2 10 154.68 15.10 -9 -2 10 171.38 15.00 8 2 -10 29.40 8.30 8 2 -10 22.90 6.40 8 2 -10 21.50 6.70 8 2 -10 16.50 6.30 8 2 -10 42.10 9.40 -8 -2 10 23.70 7.70 -8 -2 10 31.40 6.70 -8 -2 10 19.20 7.10 -8 -2 10 23.00 7.50 -8 -2 10 22.30 6.40 -8 -2 10 30.00 7.60 -8 -2 10 23.10 6.30 7 2 -10 41.30 7.60 7 2 -10 48.80 8.40 7 2 -10 48.70 8.40 7 2 -10 53.79 9.50 7 2 -10 63.49 10.10 7 2 -10 38.00 9.00 -7 -2 10 63.09 8.50 -7 -2 10 57.19 10.50 -7 -2 10 47.10 8.60 -7 -2 10 38.50 8.80 -7 -2 10 59.79 10.90 -7 -2 10 53.09 9.20 -7 -2 10 58.59 9.70 6 2 -10 189.78 14.40 6 2 -10 188.68 13.60 6 2 -10 185.98 12.40 6 2 -10 202.68 14.20 6 2 -10 208.38 15.80 6 2 -10 209.88 14.60 6 2 -10 179.98 13.00 -6 -2 10 196.28 13.10 -6 -2 10 207.18 14.40 -6 -2 10 199.38 14.80 -6 -2 10 199.28 15.20 -6 -2 10 177.38 17.00 -6 -2 10 197.78 13.80 -6 -2 10 188.58 12.20 5 2 -10 7.60 4.30 5 2 -10 11.40 4.70 5 2 -10 4.70 4.20 5 2 -10 21.80 6.60 5 2 -10 4.10 4.40 5 2 -10 9.90 3.70 5 2 -10 13.10 5.00 -5 -2 10 12.20 4.80 -5 -2 10 8.70 4.90 -5 -2 10 3.10 4.20 -5 -2 10 7.40 3.80 -5 -2 10 6.10 4.70 -5 -2 10 11.40 5.10 4 2 -10 -0.30 3.00 4 2 -10 2.70 3.90 4 2 -10 -1.70 2.70 4 2 -10 3.40 3.90 4 2 -10 3.60 3.00 4 2 -10 -0.60 3.00 4 2 -10 0.60 2.90 4 2 -10 0.30 3.00 -4 -2 10 1.70 3.80 -4 -2 10 -0.40 2.70 -4 -2 10 0.60 2.90 -4 -2 10 -1.10 3.10 -4 -2 10 0.80 2.70 -4 -2 10 -1.40 2.90 3 2 -10 14.00 4.40 3 2 -10 22.00 5.70 3 2 -10 20.30 6.00 3 2 -10 12.40 4.80 3 2 -10 9.30 4.90 3 2 -10 15.80 4.80 3 2 -10 26.50 6.20 3 2 -10 13.50 5.00 -3 -2 10 21.40 5.30 -3 -2 10 8.70 3.60 -3 -2 10 11.70 4.40 -3 -2 10 11.50 5.00 -3 -2 10 14.90 4.90 -3 -2 10 16.70 6.00 2 2 -10 9.90 4.30 2 2 -10 8.80 4.40 2 2 -10 5.80 4.80 2 2 -10 12.50 4.60 2 2 -10 14.30 5.00 2 2 -10 16.90 5.10 2 2 -10 17.30 5.20 -2 -2 10 14.50 5.00 -2 -2 10 11.30 4.20 -2 -2 10 13.20 5.20 -2 -2 10 2.80 3.90 -2 -2 10 3.60 4.50 -2 -2 10 11.40 4.80 1 2 -10 -5.50 2.90 1 2 -10 3.50 4.20 1 2 -10 -4.90 2.60 1 2 -10 -0.10 3.10 1 2 -10 2.40 4.00 1 2 -10 -4.80 2.80 -1 -2 10 2.70 4.00 -1 -2 10 2.40 3.20 -1 -2 10 1.40 2.60 -1 -2 10 1.40 3.00 -1 -2 10 -1.80 3.20 -1 -2 10 4.00 3.10 -1 -2 10 1.10 3.50 0 2 -10 103.09 10.00 0 2 -10 105.89 12.40 0 2 -10 96.49 12.50 0 2 -10 116.59 11.60 0 2 -10 98.89 10.10 0 2 -10 86.99 11.70 0 -2 10 99.29 10.40 0 -2 10 104.69 11.10 0 -2 10 85.89 8.90 0 -2 10 100.79 9.50 0 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14.10 9.70 11 5 -14 94.29 14.30 11 5 -14 71.49 14.10 11 5 -14 48.50 12.80 11 5 -14 71.99 14.10 -11 -5 14 72.49 15.40 -11 -5 14 76.09 13.30 -11 -5 14 75.59 9.50 10 5 -14 179.08 18.90 10 5 -14 207.68 21.10 10 5 -14 213.78 19.90 10 5 -14 232.28 18.80 10 5 -14 217.48 18.50 -10 -5 14 189.68 19.40 -10 -5 14 173.98 16.70 -10 -5 14 232.08 19.10 -10 -5 14 205.58 12.90 9 5 -14 23.40 9.60 9 5 -14 20.20 7.20 9 5 -14 24.40 8.20 9 5 -14 17.10 8.40 -9 -5 14 27.20 6.00 -9 -5 14 27.40 9.80 -9 -5 14 28.20 7.90 -9 -5 14 14.90 6.90 -9 -5 14 31.30 8.10 8 5 -14 65.99 12.10 8 5 -14 65.29 13.00 8 5 -14 77.09 11.90 8 5 -14 77.49 13.20 8 5 -14 68.99 12.40 -8 -5 14 85.39 14.60 -8 -5 14 87.29 15.10 -8 -5 14 63.19 11.40 -8 -5 14 65.19 11.30 -8 -5 14 68.49 10.00 -8 -5 14 80.09 8.70 7 5 -14 30.00 8.50 7 5 -14 38.20 9.00 7 5 -14 36.30 9.10 7 5 -14 31.10 11.70 7 5 -14 25.00 8.60 7 5 -14 25.60 8.10 7 5 -14 40.70 10.20 -7 -5 14 39.80 9.50 -7 -5 14 39.60 7.20 -7 -5 14 48.30 14.90 -7 -5 14 44.30 10.60 -7 -5 14 45.50 10.20 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78.69 11.00 -11 -4 14 96.59 16.30 -11 -4 14 103.79 15.70 10 4 -14 236.78 23.90 10 4 -14 253.37 22.00 10 4 -14 246.68 19.80 10 4 -14 267.37 21.50 -10 -4 14 238.28 15.10 -10 -4 14 230.88 18.70 -10 -4 14 232.38 21.60 -10 -4 14 203.48 18.10 9 4 -14 135.69 14.10 9 4 -14 132.89 18.40 9 4 -14 120.59 16.80 9 4 -14 119.49 17.20 9 4 -14 90.09 13.00 -9 -4 14 98.49 10.70 -9 -4 14 109.19 16.50 -9 -4 14 119.59 16.90 -9 -4 14 108.99 15.40 8 4 -14 135.59 14.20 8 4 -14 149.69 14.30 8 4 -14 144.59 15.80 8 4 -14 160.08 17.20 8 4 -14 145.69 15.60 -8 -4 14 125.79 17.10 -8 -4 14 122.49 13.10 -8 -4 14 124.69 15.70 -8 -4 14 156.78 15.60 -8 -4 14 118.39 16.40 -8 -4 14 126.79 11.60 7 4 -14 212.68 18.60 7 4 -14 186.98 16.10 7 4 -14 203.08 15.80 7 4 -14 208.68 16.50 7 4 -14 202.18 17.70 7 4 -14 208.18 18.00 -7 -4 14 220.08 17.60 -7 -4 14 249.88 33.40 -7 -4 14 217.18 14.20 -7 -4 14 227.48 15.60 -7 -4 14 192.98 18.20 -7 -4 14 215.48 18.80 6 4 -14 84.59 12.70 6 4 -14 63.79 11.70 6 4 -14 69.59 12.70 6 4 -14 40.10 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10.30 4 8 -19 -6.40 7.00 4 8 -19 -1.60 7.30 -4 -8 19 -11.80 4.50 -4 -8 19 -12.20 6.10 3 8 -19 5.30 8.20 3 8 -19 17.80 10.70 3 8 -19 18.00 8.60 3 8 -19 6.80 7.70 -3 -8 19 -11.90 6.70 -3 -8 19 3.60 6.90 2 8 -19 8.00 6.40 2 8 -19 0.60 7.10 2 8 -19 2.20 10.50 -2 -8 19 5.30 8.30 -2 -8 19 -12.10 5.90 8 7 -19 47.00 11.60 8 7 -19 75.69 14.60 8 7 -19 58.59 14.60 8 7 -19 72.69 14.10 8 7 -19 70.59 14.70 -8 -7 19 73.69 10.40 -8 -7 19 52.79 13.80 -8 -7 19 76.59 14.10 7 7 -19 1.90 10.50 7 7 -19 17.40 8.90 7 7 -19 9.70 7.90 7 7 -19 12.90 8.60 7 7 -19 10.20 8.50 -7 -7 19 13.40 6.30 -7 -7 19 5.00 9.50 -7 -7 19 32.90 9.40 -7 -7 19 20.90 7.10 6 7 -19 8.90 10.90 6 7 -19 3.90 7.30 6 7 -19 -4.20 5.20 -6 -7 19 -5.50 7.60 -6 -7 19 8.50 6.80 -6 -7 19 1.20 5.40 5 7 -19 27.30 10.10 5 7 -19 34.90 10.90 5 7 -19 21.30 9.10 5 7 -19 20.70 9.40 5 7 -19 25.00 10.60 -5 -7 19 6.10 7.00 -5 -7 19 25.40 8.10 -5 -7 19 17.10 9.80 4 7 -19 21.00 10.20 4 7 -19 28.90 10.10 4 7 -19 42.70 14.10 -4 -7 19 23.40 9.40 -4 -7 19 39.00 12.90 -4 -7 19 29.20 8.50 3 7 -19 24.40 11.60 3 7 -19 19.30 9.20 3 7 -19 7.40 8.60 3 7 -19 11.00 9.10 -3 -7 19 13.90 7.80 -3 -7 19 14.40 10.90 -3 -7 19 28.20 9.40 2 7 -19 61.29 15.10 2 7 -19 40.20 11.60 2 7 -19 42.20 11.40 -2 -7 19 60.99 16.00 -2 -7 19 68.29 13.10 8 6 -19 1.90 6.10 8 6 -19 5.70 11.20 8 6 -19 -10.70 6.10 8 6 -19 -7.40 6.50 8 6 -19 21.70 8.70 -8 -6 19 5.00 8.60 -8 -6 19 4.30 5.70 -8 -6 19 -4.90 5.30 7 6 -19 2.50 10.60 7 6 -19 9.30 6.10 7 6 -19 -7.40 5.60 7 6 -19 -2.40 6.80 7 6 -19 3.60 7.00 -7 -6 19 19.80 8.40 -7 -6 19 6.10 5.80 -7 -6 19 7.40 8.90 -7 -6 19 0.20 5.30 6 6 -19 4.70 7.60 6 6 -19 10.50 10.20 6 6 -19 25.60 10.10 6 6 -19 -1.40 11.50 6 6 -19 11.20 7.40 -6 -6 19 -2.60 7.70 -6 -6 19 15.60 6.50 -6 -6 19 18.80 9.10 -6 -6 19 9.00 4.90 5 6 -19 0.90 6.40 5 6 -19 7.90 9.90 5 6 -19 4.40 7.50 -5 -6 19 -4.20 6.30 -5 -6 19 9.00 5.20 -5 -6 19 -2.00 8.80 -5 -6 19 -8.90 3.60 -5 -6 19 -4.10 5.40 4 6 -19 -7.80 10.40 4 6 -19 1.90 6.70 4 6 -19 3.10 7.60 4 6 -19 9.40 9.10 -4 -6 19 -10.10 5.80 -4 -6 19 -4.30 4.70 -4 -6 19 -1.80 7.70 3 6 -19 0.90 6.80 3 6 -19 0.70 7.30 3 6 -19 7.20 6.90 3 6 -19 11.70 11.00 -3 -6 19 5.90 6.60 -3 -6 19 3.10 9.60 -3 -6 19 2.00 5.20 2 6 -19 -3.40 7.10 2 6 -19 -9.80 6.00 2 6 -19 1.40 11.50 2 6 -19 23.20 10.30 -2 -6 19 19.50 9.30 -2 -6 19 8.20 7.00 -2 -6 19 -1.40 6.20 8 5 -19 21.60 10.70 8 5 -19 25.60 10.40 8 5 -19 13.20 9.00 8 5 -19 27.00 9.90 -8 -5 19 36.40 11.50 -8 -5 19 47.30 11.90 -8 -5 19 22.10 12.10 -8 -5 19 16.80 8.60 7 5 -19 58.69 14.00 7 5 -19 61.89 13.00 7 5 -19 55.29 13.60 7 5 -19 63.49 12.10 -7 -5 19 66.59 12.20 -7 -5 19 58.49 15.00 -7 -5 19 69.39 13.90 6 5 -19 54.09 12.10 6 5 -19 32.20 11.70 6 5 -19 43.90 12.80 -6 -5 19 49.10 10.10 -6 -5 19 46.40 9.40 -6 -5 19 33.00 9.50 -6 -5 19 53.49 12.20 -6 -5 19 41.70 13.10 5 5 -19 28.30 11.20 5 5 -19 40.40 17.00 5 5 -19 54.49 12.50 -5 -5 19 30.20 11.20 -5 -5 19 38.30 8.30 -5 -5 19 44.80 11.60 -5 -5 19 43.20 10.40 4 5 -19 48.60 12.60 4 5 -19 75.69 13.70 4 5 -19 56.09 13.20 -4 -5 19 68.19 15.40 -4 -5 19 48.50 12.30 -4 -5 19 84.99 14.40 -4 -5 19 81.59 11.50 3 5 -19 1.20 6.70 3 5 -19 18.00 9.50 3 5 -19 1.10 7.60 -3 -5 19 -0.80 9.70 -3 -5 19 2.40 5.40 -3 -5 19 4.40 7.90 -3 -5 19 5.60 6.00 2 5 -19 33.40 11.80 2 5 -19 51.79 12.20 2 5 -19 40.20 13.20 -2 -5 19 48.00 14.00 -2 -5 19 54.79 8.80 -2 -5 19 49.99 12.80 8 4 -19 -14.50 6.40 8 4 -19 -16.30 5.30 8 4 -19 1.30 5.20 8 4 -19 -10.00 7.30 -8 -4 19 0.00 8.40 -8 -4 19 3.90 7.10 -8 -4 19 -6.30 7.50 7 4 -19 -13.10 6.50 7 4 -19 2.40 7.90 7 4 -19 8.20 6.30 -7 -4 19 -4.20 5.50 -7 -4 19 7.90 10.00 -7 -4 19 21.70 14.40 -7 -4 19 7.40 7.10 6 4 -19 23.10 8.20 6 4 -19 8.60 9.20 6 4 -19 5.50 7.70 -6 -4 19 16.40 9.10 -6 -4 19 21.30 7.60 -6 -4 19 11.80 8.50 -6 -4 19 11.50 5.90 5 4 -19 -9.10 4.70 5 4 -19 -4.40 6.60 5 4 -19 -7.00 6.20 -5 -4 19 -13.10 4.90 -5 -4 19 9.80 6.80 -5 -4 19 9.60 8.00 4 4 -19 -7.40 5.40 4 4 -19 9.40 8.40 -4 -4 19 3.40 8.90 -4 -4 19 1.30 5.40 -4 -4 19 10.10 11.30 -4 -4 19 5.70 6.10 3 4 -19 11.80 8.10 3 4 -19 4.50 8.60 3 4 -19 11.70 7.90 -3 -4 19 8.80 8.10 -3 -4 19 9.50 10.10 -3 -4 19 2.60 11.80 -3 -4 19 17.50 7.00 7 3 -19 40.10 11.10 7 3 -19 50.69 12.90 7 3 -19 67.49 12.10 -7 -3 19 68.39 14.50 -7 -3 19 51.29 11.10 -7 -3 19 61.29 12.70 -7 -3 19 35.30 13.60 6 3 -19 46.50 10.00 6 3 -19 37.30 12.00 6 3 -19 27.70 10.80 -6 -3 19 49.80 12.90 -6 -3 19 54.09 15.70 -6 -3 19 58.79 12.00 -6 -3 19 75.89 14.20 5 3 -19 9.40 8.50 5 3 -19 -12.20 7.80 5 3 -19 10.80 6.50 -5 -3 19 12.20 9.40 -5 -3 19 17.10 7.90 -5 -3 19 9.00 10.90 -5 -3 19 16.20 8.50 4 3 -19 16.30 7.30 4 3 -19 2.40 8.10 4 3 -19 1.50 7.10 -4 -3 19 4.50 8.60 -4 -3 19 0.90 9.40 -4 -3 19 2.60 7.40 6 2 -19 81.19 14.10 6 2 -19 56.59 13.70 6 2 -19 62.59 11.00 -6 -2 19 76.19 14.90 -6 -2 19 59.19 14.60 -6 -2 19 50.19 13.00 -6 -2 19 61.49 12.50 5 2 -19 43.00 10.80 5 2 -19 40.00 13.20 -5 -2 19 41.80 14.50 -5 -2 19 59.69 14.90 -5 -2 19 55.49 13.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 12927 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.63607(4) 0.16420(4) 0.72385(3) 0.01798(9) Uani 1 1 d . . . . . O1 O 0.54855(14) 0.05223(12) 0.63268(11) 0.0233(3) Uani 1 1 d . . . . . O2 O 0.77209(14) 0.15681(12) 0.80074(11) 0.0246(3) Uani 1 1 d . . . . . C1 C 0.53904(19) 0.23196(16) 0.80685(14) 0.0200(3) Uani 1 1 d . . . . . C2 C 0.4078(2) 0.26109(19) 0.75778(17) 0.0279(4) Uani 1 1 d . . . . . H2 H 0.370232 0.245921 0.680271 0.034 Uiso 1 1 calc R U . . . C3 C 0.3317(2) 0.3126(2) 0.82302(19) 0.0325(4) Uani 1 1 d . . . . . H3 H 0.241350 0.332360 0.789536 0.039 Uiso 1 1 calc R U . . . C4 C 0.3856(2) 0.3360(2) 0.93685(19) 0.0340(5) Uani 1 1 d . . . . . C5 C 0.5146(3) 0.3025(3) 0.98254(19) 0.0452(6) Uani 1 1 d . . . . . H5 H 0.550707 0.314494 1.059266 0.054 Uiso 1 1 calc R U . . . C6 C 0.5928(2) 0.2515(2) 0.91879(17) 0.0362(5) Uani 1 1 d . . . . . H6 H 0.682331 0.230282 0.951868 0.043 Uiso 1 1 calc R U . . . C7 C 0.3066(3) 0.3980(3) 1.0093(2) 0.0508(7) Uani 1 1 d . . . . . H7A H 0.328589 0.370829 1.070448 0.076 Uiso 1 1 calc R U . . . H7B H 0.203931 0.376696 0.963517 0.076 Uiso 1 1 calc R U . . . H7C H 0.335901 0.486685 1.041134 0.076 Uiso 1 1 calc R U . . . C8 C 0.65987(18) 0.26732(15) 0.67032(14) 0.0173(3) Uani 1 1 d . . . . . C9 C 0.58329(18) 0.23458(15) 0.55852(14) 0.0178(3) Uani 1 1 d . . . . . H9 H 0.529068 0.154512 0.516636 0.021 Uiso 1 1 calc R U . . . N1 N 0.57656(16) 0.30399(13) 0.50131(12) 0.0189(3) Uani 1 1 d . . . . . H1 H 0.612839 0.382268 0.538491 0.023 Uiso 1 1 calc R U . . . C10 C 0.51013(18) 0.25182(15) 0.37856(14) 0.0175(3) Uani 1 1 d . . . . . H10 H 0.493823 0.160984 0.352072 0.021 Uiso 1 1 calc R U . . . P1 P 0.33381(5) 0.29740(4) 0.33105(4) 0.01900(9) Uani 1 1 d . . . . . O3 O 0.33823(15) 0.43177(12) 0.36597(12) 0.0269(3) Uani 1 1 d . . . . . C11 C 0.2520(2) 0.21014(17) 0.18089(15) 0.0235(3) Uani 1 1 d . . . . . C12 C 0.1230(2) 0.2380(2) 0.12385(18) 0.0345(5) Uani 1 1 d . . . . . H12 H 0.083091 0.300601 0.164254 0.041 Uiso 1 1 calc R U . . . C13 C 0.0524(3) 0.1750(3) 0.0084(2) 0.0470(6) Uani 1 1 d . . . . . H13 H -0.036073 0.194070 -0.030011 0.056 Uiso 1 1 calc R U . . . C14 C 0.1098(3) 0.0850(3) -0.0509(2) 0.0508(7) Uani 1 1 d . . . . . H14 H 0.061876 0.043032 -0.130207 0.061 Uiso 1 1 calc R U . . . C15 C 0.2367(3) 0.0557(3) 0.0045(2) 0.0555(8) Uani 1 1 d . . . . . H15 H 0.275799 -0.006904 -0.036691 0.067 Uiso 1 1 calc R U . . . C16 C 0.3082(3) 0.1173(2) 0.12099(18) 0.0418(6) Uani 1 1 d . . . . . H16 H 0.394964 0.095903 0.159177 0.050 Uiso 1 1 calc R U . . . C17 C 0.23214(19) 0.23919(17) 0.38847(15) 0.0225(3) Uani 1 1 d . . . . . C18 C 0.2033(2) 0.1146(2) 0.3603(2) 0.0322(4) Uani 1 1 d . . . . . H18 H 0.235792 0.058255 0.308461 0.039 Uiso 1 1 calc R U . . . C19 C 0.1273(3) 0.0724(2) 0.4075(2) 0.0432(6) Uani 1 1 d . . . . . H19 H 0.110380 -0.012291 0.390111 0.052 Uiso 1 1 calc R U . . . C20 C 0.0762(3) 0.1544(3) 0.4803(2) 0.0459(6) Uani 1 1 d . . . . . H20 H 0.024150 0.125808 0.512903 0.055 Uiso 1 1 calc R U . . . C21 C 0.1005(3) 0.2769(3) 0.5056(2) 0.0453(6) Uani 1 1 d . . . . . H21 H 0.063242 0.332323 0.554362 0.054 Uiso 1 1 calc R U . . . C22 C 0.1793(2) 0.3207(2) 0.46043(18) 0.0328(4) Uani 1 1 d . . . . . H22 H 0.196666 0.405657 0.478756 0.039 Uiso 1 1 calc R U . . . C23 C 0.61089(19) 0.28340(16) 0.33149(14) 0.0205(3) Uani 1 1 d . . . . . C24 C 0.7028(2) 0.20549(17) 0.29978(17) 0.0260(4) Uani 1 1 d . . . . . C25 C 0.8007(2) 0.2380(2) 0.26347(19) 0.0340(5) Uani 1 1 d . . . . . H25 H 0.862336 0.183637 0.242982 0.041 Uiso 1 1 calc R U . . . C26 C 0.8078(3) 0.3500(2) 0.25739(19) 0.0363(5) Uani 1 1 d . . . . . H26 H 0.874600 0.373064 0.232812 0.044 Uiso 1 1 calc R U . . . C27 C 0.7178(3) 0.4284(2) 0.28703(19) 0.0354(5) Uani 1 1 d . . . . . H27 H 0.722006 0.504936 0.281951 0.043 Uiso 1 1 calc R U . . . C28 C 0.6210(2) 0.39575(18) 0.32430(17) 0.0277(4) Uani 1 1 d . . . . . H28 H 0.560450 0.451035 0.345305 0.033 Uiso 1 1 calc R U . . . Br1 Br 0.69570(2) 0.04936(2) 0.30257(3) 0.04223(8) Uani 1 1 d . . . . . C29 C 0.76029(18) 0.38511(16) 0.75306(14) 0.0190(3) Uani 1 1 d . . . . . H29A H 0.773514 0.397059 0.830202 0.023 Uiso 1 1 calc R U . . . H29B H 0.717247 0.453787 0.738824 0.023 Uiso 1 1 calc R U . . . C30 C 0.9034(2) 0.38763(19) 0.74587(19) 0.0301(4) Uani 1 1 d . . . . . F1 F 0.89606(15) 0.39023(16) 0.64928(13) 0.0483(4) Uani 1 1 d . . . . . F2 F 0.99543(14) 0.48843(13) 0.82863(13) 0.0437(3) Uani 1 1 d . . . . . F3 F 0.96536(14) 0.29243(13) 0.75444(15) 0.0493(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.01962(19) 0.01836(18) 0.01570(18) 0.00790(15) 0.00575(15) 0.00366(14) O1 0.0293(7) 0.0185(6) 0.0199(6) 0.0071(5) 0.0081(5) 0.0003(5) O2 0.0237(6) 0.0276(7) 0.0222(6) 0.0133(5) 0.0053(5) 0.0088(5) C1 0.0219(8) 0.0202(8) 0.0186(8) 0.0082(6) 0.0085(7) 0.0018(6) C2 0.0283(9) 0.0366(10) 0.0259(9) 0.0176(8) 0.0131(8) 0.0120(8) C3 0.0332(11) 0.0397(11) 0.0403(12) 0.0242(10) 0.0229(9) 0.0151(9) C4 0.0396(12) 0.0345(11) 0.0374(11) 0.0138(9) 0.0263(10) 0.0068(9) C5 0.0422(13) 0.0736(18) 0.0209(10) 0.0166(11) 0.0165(9) 0.0129(12) C6 0.0292(10) 0.0599(15) 0.0216(9) 0.0187(10) 0.0101(8) 0.0121(10) C7 0.0622(17) 0.0553(16) 0.0546(16) 0.0215(13) 0.0453(15) 0.0180(13) C8 0.0172(7) 0.0182(7) 0.0174(7) 0.0076(6) 0.0074(6) 0.0034(6) C9 0.0184(7) 0.0181(7) 0.0174(7) 0.0071(6) 0.0080(6) 0.0040(6) N1 0.0231(7) 0.0170(6) 0.0137(6) 0.0053(5) 0.0053(5) 0.0016(5) C10 0.0194(7) 0.0170(7) 0.0149(7) 0.0061(6) 0.0060(6) 0.0013(6) P1 0.0211(2) 0.01718(19) 0.0170(2) 0.00684(16) 0.00586(16) 0.00415(16) O3 0.0333(7) 0.0179(6) 0.0260(7) 0.0086(5) 0.0084(6) 0.0065(5) C11 0.0232(8) 0.0256(9) 0.0181(8) 0.0088(7) 0.0047(7) 0.0009(7) C12 0.0274(10) 0.0428(12) 0.0279(10) 0.0163(9) 0.0034(8) 0.0067(9) C13 0.0344(12) 0.0621(17) 0.0300(11) 0.0210(12) -0.0047(10) 0.0005(11) C14 0.0483(15) 0.0593(17) 0.0198(10) 0.0073(10) -0.0034(10) -0.0089(12) C15 0.0536(16) 0.0598(17) 0.0228(11) -0.0052(11) 0.0060(11) 0.0075(13) C16 0.0364(12) 0.0449(13) 0.0225(10) 0.0007(9) 0.0023(9) 0.0110(10) C17 0.0186(8) 0.0260(9) 0.0228(8) 0.0105(7) 0.0077(7) 0.0061(7) C18 0.0317(10) 0.0291(10) 0.0458(12) 0.0187(9) 0.0224(9) 0.0094(8) C19 0.0391(12) 0.0450(13) 0.0600(16) 0.0314(12) 0.0250(12) 0.0052(10) C20 0.0306(11) 0.0717(18) 0.0418(13) 0.0270(13) 0.0175(10) -0.0030(11) C21 0.0370(12) 0.0596(16) 0.0357(12) 0.0072(11) 0.0235(10) 0.0038(11) C22 0.0303(10) 0.0344(11) 0.0289(10) 0.0049(8) 0.0151(8) 0.0057(8) C23 0.0221(8) 0.0210(8) 0.0147(7) 0.0052(6) 0.0057(6) -0.0018(6) C24 0.0248(9) 0.0225(8) 0.0282(9) 0.0066(7) 0.0119(8) -0.0015(7) C25 0.0304(10) 0.0328(11) 0.0356(11) 0.0056(9) 0.0188(9) -0.0028(8) C26 0.0392(12) 0.0397(12) 0.0318(11) 0.0117(9) 0.0193(9) -0.0076(9) C27 0.0481(13) 0.0307(10) 0.0325(11) 0.0152(9) 0.0192(10) -0.0029(9) C28 0.0357(10) 0.0250(9) 0.0259(9) 0.0125(7) 0.0139(8) 0.0022(8) Br1 0.03339(12) 0.02730(11) 0.07947(19) 0.02390(11) 0.03458(12) 0.01051(8) C29 0.0181(7) 0.0191(7) 0.0187(8) 0.0070(6) 0.0070(6) 0.0023(6) C30 0.0193(9) 0.0305(10) 0.0391(11) 0.0145(9) 0.0100(8) 0.0020(7) F1 0.0351(7) 0.0731(11) 0.0502(9) 0.0272(8) 0.0295(7) 0.0078(7) F2 0.0238(6) 0.0384(7) 0.0552(9) 0.0176(7) 0.0031(6) -0.0093(5) F3 0.0224(6) 0.0407(8) 0.0894(12) 0.0308(8) 0.0227(7) 0.0133(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 S1 O2 118.08(8) . . ? O1 S1 C8 109.41(8) . . ? O2 S1 C8 109.58(8) . . ? O1 S1 C1 107.99(8) . . ? O2 S1 C1 106.07(8) . . ? C8 S1 C1 104.86(8) . . ? C6 C1 C2 120.65(18) . . ? C6 C1 S1 119.70(15) . . ? C2 C1 S1 119.62(14) . . ? C1 C2 C3 119.24(18) . . ? C1 C2 H2 120.4 . . ? C3 C2 H2 120.4 . . ? C2 C3 C4 121.1(2) . . ? C2 C3 H3 119.5 . . ? C4 C3 H3 119.5 . . ? C5 C4 C3 118.35(19) . . ? C5 C4 C7 120.5(2) . . ? C3 C4 C7 121.2(2) . . ? C4 C5 C6 121.4(2) . . ? C4 C5 H5 119.3 . . ? C6 C5 H5 119.3 . . ? C1 C6 C5 119.2(2) . . ? C1 C6 H6 120.4 . . ? C5 C6 H6 120.4 . . ? C4 C7 H7A 109.5 . . ? C4 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C4 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C9 C8 C29 127.01(15) . . ? C9 C8 S1 116.56(13) . . ? C29 C8 S1 116.41(12) . . ? N1 C9 C8 126.63(16) . . ? N1 C9 H9 116.7 . . ? C8 C9 H9 116.7 . . ? C9 N1 C10 121.16(14) . . ? C9 N1 H1 119.4 . . ? C10 N1 H1 119.4 . . ? N1 C10 C23 110.36(14) . . ? N1 C10 P1 110.01(12) . . ? C23 C10 P1 114.48(12) . . ? N1 C10 H10 107.2 . . ? C23 C10 H10 107.2 . . ? P1 C10 H10 107.2 . . ? O3 P1 C17 110.86(9) . . ? O3 P1 C11 113.69(8) . . ? C17 P1 C11 105.89(9) . . ? O3 P1 C10 114.36(8) . . ? C17 P1 C10 105.51(8) . . ? C11 P1 C10 105.84(8) . . ? C16 C11 C12 119.25(19) . . ? C16 C11 P1 124.26(15) . . ? C12 C11 P1 116.48(16) . . ? C13 C12 C11 120.3(2) . . ? C13 C12 H12 119.8 . . ? C11 C12 H12 119.8 . . ? C14 C13 C12 120.2(2) . . ? C14 C13 H13 119.9 . . ? C12 C13 H13 119.9 . . ? C13 C14 C15 120.1(2) . . ? C13 C14 H14 119.9 . . ? C15 C14 H14 119.9 . . ? C14 C15 C16 120.3(3) . . ? C14 C15 H15 119.8 . . ? C16 C15 H15 119.8 . . ? C11 C16 C15 119.8(2) . . ? C11 C16 H16 120.1 . . ? C15 C16 H16 120.1 . . ? C22 C17 C18 119.73(19) . . ? C22 C17 P1 118.79(16) . . ? C18 C17 P1 121.47(15) . . ? C19 C18 C17 120.3(2) . . ? C19 C18 H18 119.9 . . ? C17 C18 H18 119.9 . . ? C18 C19 C20 119.7(2) . . ? C18 C19 H19 120.2 . . ? C20 C19 H19 120.2 . . ? C21 C20 C19 120.3(2) . . ? C21 C20 H20 119.9 . . ? C19 C20 H20 119.9 . . ? C20 C21 C22 120.6(2) . . ? C20 C21 H21 119.7 . . ? C22 C21 H21 119.7 . . ? C17 C22 C21 119.4(2) . . ? C17 C22 H22 120.3 . . ? C21 C22 H22 120.3 . . ? C28 C23 C24 116.99(17) . . ? C28 C23 C10 120.71(17) . . ? C24 C23 C10 122.20(16) . . ? C25 C24 C23 121.99(19) . . ? C25 C24 Br1 117.25(16) . . ? C23 C24 Br1 120.76(14) . . ? C26 C25 C24 119.5(2) . . ? C26 C25 H25 120.3 . . ? C24 C25 H25 120.3 . . ? C25 C26 C27 119.97(19) . . ? C25 C26 H26 120.0 . . ? C27 C26 H26 120.0 . . ? C26 C27 C28 120.3(2) . . ? C26 C27 H27 119.9 . . ? C28 C27 H27 119.9 . . ? C27 C28 C23 121.3(2) . . ? C27 C28 H28 119.3 . . ? C23 C28 H28 119.3 . . ? C8 C29 C30 112.70(15) . . ? C8 C29 H29A 109.1 . . ? C30 C29 H29A 109.1 . . ? C8 C29 H29B 109.1 . . ? C30 C29 H29B 109.1 . . ? H29A C29 H29B 107.8 . . ? F3 C30 F1 106.80(19) . . ? F3 C30 F2 106.34(17) . . ? F1 C30 F2 105.96(17) . . ? F3 C30 C29 113.79(17) . . ? F1 C30 C29 112.25(16) . . ? F2 C30 C29 111.20(17) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O1 1.4437(13) . ? S1 O2 1.4441(13) . ? S1 C8 1.7273(17) . ? S1 C1 1.7708(18) . ? C1 C6 1.379(3) . ? C1 C2 1.384(3) . ? C2 C3 1.386(3) . ? C2 H2 0.9500 . ? C3 C4 1.392(3) . ? C3 H3 0.9500 . ? C4 C5 1.379(3) . ? C4 C7 1.508(3) . ? C5 C6 1.388(3) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 C9 1.361(2) . ? C8 C29 1.505(2) . ? C9 N1 1.344(2) . ? C9 H9 0.9500 . ? N1 C10 1.460(2) . ? N1 H1 0.8800 . ? C10 C23 1.523(2) . ? C10 P1 1.8480(18) . ? C10 H10 1.0000 . ? P1 O3 1.4928(14) . ? P1 C17 1.7999(19) . ? P1 C11 1.8025(19) . ? C11 C16 1.389(3) . ? C11 C12 1.390(3) . ? C12 C13 1.385(3) . ? C12 H12 0.9500 . ? C13 C14 1.374(4) . ? C13 H13 0.9500 . ? C14 C15 1.375(4) . ? C14 H14 0.9500 . ? C15 C16 1.395(3) . ? C15 H15 0.9500 . ? C16 H16 0.9500 . ? C17 C22 1.387(3) . ? C17 C18 1.394(3) . ? C18 C19 1.385(3) . ? C18 H18 0.9500 . ? C19 C20 1.385(4) . ? C19 H19 0.9500 . ? C20 C21 1.373(4) . ? C20 H20 0.9500 . ? C21 C22 1.395(3) . ? C21 H21 0.9500 . ? C22 H22 0.9500 . ? C23 C28 1.396(3) . ? C23 C24 1.401(3) . ? C24 C25 1.389(3) . ? C24 Br1 1.891(2) . ? C25 C26 1.383(3) . ? C25 H25 0.9500 . ? C26 C27 1.379(3) . ? C26 H26 0.9500 . ? C27 C28 1.390(3) . ? C27 H27 0.9500 . ? C28 H28 0.9500 . ? C29 C30 1.505(3) . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C30 F3 1.335(2) . ? C30 F1 1.339(3) . ? C30 F2 1.348(2) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 S1 C1 C6 119.72(18) . . . . ? O2 S1 C1 C6 -7.77(19) . . . . ? C8 S1 C1 C6 -123.70(18) . . . . ? O1 S1 C1 C2 -58.15(17) . . . . ? O2 S1 C1 C2 174.37(15) . . . . ? C8 S1 C1 C2 58.44(17) . . . . ? C6 C1 C2 C3 1.3(3) . . . . ? S1 C1 C2 C3 179.16(16) . . . . ? C1 C2 C3 C4 0.3(3) . . . . ? C2 C3 C4 C5 -2.3(4) . . . . ? C2 C3 C4 C7 176.8(2) . . . . ? C3 C4 C5 C6 2.8(4) . . . . ? C7 C4 C5 C6 -176.4(3) . . . . ? C2 C1 C6 C5 -0.9(4) . . . . ? S1 C1 C6 C5 -178.7(2) . . . . ? C4 C5 C6 C1 -1.2(4) . . . . ? O1 S1 C8 C9 7.13(16) . . . . ? O2 S1 C8 C9 138.06(13) . . . . ? C1 S1 C8 C9 -108.47(14) . . . . ? O1 S1 C8 C29 -174.38(12) . . . . ? O2 S1 C8 C29 -43.45(15) . . . . ? C1 S1 C8 C29 70.01(14) . . . . ? C29 C8 C9 N1 -3.9(3) . . . . ? S1 C8 C9 N1 174.40(14) . . . . ? C8 C9 N1 C10 169.50(16) . . . . ? C9 N1 C10 C23 -127.70(17) . . . . ? C9 N1 C10 P1 105.04(16) . . . . ? N1 C10 P1 O3 62.42(14) . . . . ? C23 C10 P1 O3 -62.51(14) . . . . ? N1 C10 P1 C17 -59.67(13) . . . . ? C23 C10 P1 C17 175.40(12) . . . . ? N1 C10 P1 C11 -171.64(11) . . . . ? C23 C10 P1 C11 63.43(14) . . . . ? O3 P1 C11 C16 134.0(2) . . . . ? C17 P1 C11 C16 -104.1(2) . . . . ? C10 P1 C11 C16 7.6(2) . . . . ? O3 P1 C11 C12 -47.28(19) . . . . ? C17 P1 C11 C12 74.67(18) . . . . ? C10 P1 C11 C12 -173.63(16) . . . . ? C16 C11 C12 C13 -0.9(3) . . . . ? P1 C11 C12 C13 -179.68(19) . . . . ? C11 C12 C13 C14 -0.5(4) . . . . ? C12 C13 C14 C15 1.1(5) . . . . ? C13 C14 C15 C16 -0.3(5) . . . . ? C12 C11 C16 C15 1.6(4) . . . . ? P1 C11 C16 C15 -179.7(2) . . . . ? C14 C15 C16 C11 -1.0(5) . . . . ? O3 P1 C17 C22 -3.82(18) . . . . ? C11 P1 C17 C22 -127.57(16) . . . . ? C10 P1 C17 C22 120.50(16) . . . . ? O3 P1 C17 C18 174.81(16) . . . . ? C11 P1 C17 C18 51.05(18) . . . . ? C10 P1 C17 C18 -60.88(18) . . . . ? C22 C17 C18 C19 -2.8(3) . . . . ? P1 C17 C18 C19 178.63(18) . . . . ? C17 C18 C19 C20 2.0(4) . . . . ? C18 C19 C20 C21 0.0(4) . . . . ? C19 C20 C21 C22 -1.4(4) . . . . ? C18 C17 C22 C21 1.4(3) . . . . ? P1 C17 C22 C21 -179.93(18) . . . . ? C20 C21 C22 C17 0.6(4) . . . . ? N1 C10 C23 C28 -82.9(2) . . . . ? P1 C10 C23 C28 41.8(2) . . . . ? N1 C10 C23 C24 93.3(2) . . . . ? P1 C10 C23 C24 -141.92(15) . . . . ? C28 C23 C24 C25 0.5(3) . . . . ? C10 C23 C24 C25 -175.93(18) . . . . ? C28 C23 C24 Br1 -178.47(14) . . . . ? C10 C23 C24 Br1 5.1(2) . . . . ? C23 C24 C25 C26 -0.5(3) . . . . ? Br1 C24 C25 C26 178.50(17) . . . . ? C24 C25 C26 C27 -0.1(3) . . . . ? C25 C26 C27 C28 0.7(3) . . . . ? C26 C27 C28 C23 -0.8(3) . . . . ? C24 C23 C28 C27 0.2(3) . . . . ? C10 C23 C28 C27 176.60(18) . . . . ? C9 C8 C29 C30 -79.0(2) . . . . ? S1 C8 C29 C30 102.71(16) . . . . ? C8 C29 C30 F3 -53.4(2) . . . . ? C8 C29 C30 F1 68.0(2) . . . . ? C8 C29 C30 F2 -173.45(16) . . . . ?