#------------------------------------------------------------------------------ #$Date: 2024-10-04 01:08:23 +0300 (Fri, 04 Oct 2024) $ #$Revision: 295020 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572748.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572748 loop_ _publ_author_name 'Guo, Jia-Dong' 'Alemu Korsaye, Feven' 'Schutz, Dorian' 'Ciofini, Ilaria' 'Miesch, Laurence' _publ_section_title ; Photocatalyst-free, visible-light-induced regio- and stereoselective synthesis of phosphorylated enamines from N-allenamides via [1,3]-sulfonyl shift at room temperature ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC05190D _journal_year 2024 _chemical_formula_moiety 'C18 H18 F3 N O2 S' _chemical_formula_sum 'C18 H18 F3 N O2 S' _chemical_formula_weight 369.39 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2023-07-13 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 92.821(7) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 17.628(2) _cell_length_b 7.0992(10) _cell_length_c 13.6449(16) _cell_measurement_reflns_used 1462 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 27.77 _cell_measurement_theta_min 2.99 _cell_volume 1705.5(4) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014 (Sheldrick 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator triumph _diffrn_radiation_source 'sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0662 _diffrn_reflns_av_unetI/netI 0.0531 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 19385 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.962 _diffrn_reflns_theta_min 1.157 _exptl_absorpt_coefficient_mu 0.232 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6067 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.439 _exptl_crystal_density_meas ? _exptl_crystal_description block _exptl_crystal_F_000 768 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.372 _refine_diff_density_min -0.292 _refine_diff_density_rms 0.055 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.856 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 227 _refine_ls_number_reflns 4081 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.856 _refine_ls_R_factor_all 0.0796 _refine_ls_R_factor_gt 0.0443 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.2495P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1183 _refine_ls_wR_factor_ref 0.1459 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2773 _reflns_number_total 4081 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05190d2.cif _cod_data_source_block elmjdg230207 _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_crystal_density_meas' value 'none' was changed to '?' -- the value is perceived as not measured. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas ; _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 1572748 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.955 _shelx_estimated_absorpt_t_max 0.977 _shelx_res_file ; TITL elmjdg_a.res in P2(1)/c elmjdg_a.res created by SHELXL-2018/3 at 11:32:43 on 06-Mar-2023 CELL 0.71073 17.6281 7.0992 13.6449 90.000 92.821 90.000 ZERR 4.000 0.0023 0.0010 0.0016 0.000 0.007 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H F O S N UNIT 72 72 12 8 4 4 L.S. 10 ACTA BOND $H FMAP 2 PLAN 5 SIZE 0.10 0.15 0.20 TEMP 23.000 WGHT 0.100000 0.249460 FVAR 0.36248 S1 5 0.216601 0.637956 0.635763 11.00000 0.02529 0.03104 = 0.01890 0.00259 0.00230 0.00170 O1 4 0.194314 0.446694 0.653743 11.00000 0.03838 0.03227 = 0.03351 0.00904 0.00839 0.00512 O2 4 0.271127 0.727727 0.703441 11.00000 0.03121 0.04926 = 0.01818 0.00136 -0.00250 -0.00083 C1 1 0.132469 0.774101 0.635705 11.00000 0.02661 0.02906 = 0.01803 0.00158 0.00537 0.00027 C2 1 0.062224 0.685151 0.621743 11.00000 0.03121 0.03138 = 0.03347 0.00142 0.00446 0.00065 AFIX 43 H2 2 0.059653 0.555172 0.613755 11.00000 -1.20000 AFIX 0 C3 1 -0.003604 0.791459 0.619848 11.00000 0.02479 0.04891 = 0.03829 0.00206 0.00338 -0.00143 AFIX 43 H3 2 -0.050347 0.731843 0.610130 11.00000 -1.20000 AFIX 0 C4 1 -0.001144 0.986597 0.632257 11.00000 0.03838 0.04567 = 0.01982 0.00344 0.00593 0.01209 C5 1 0.069912 1.071342 0.646533 11.00000 0.04726 0.02962 = 0.03277 0.00116 0.00710 0.00836 AFIX 43 H5 2 0.072839 1.201001 0.655688 11.00000 -1.20000 AFIX 0 C6 1 0.135890 0.967084 0.647366 11.00000 0.03510 0.03276 = 0.02778 -0.00145 0.00310 -0.00229 AFIX 43 H6 2 0.182720 1.026768 0.655787 11.00000 -1.20000 AFIX 0 C7 1 -0.073086 1.101140 0.627887 11.00000 0.04817 0.06714 = 0.03340 0.00433 0.00522 0.02571 AFIX 137 H7A 2 -0.090821 1.116495 0.560711 11.00000 -1.50000 H7B 2 -0.063202 1.222576 0.656720 11.00000 -1.50000 H7C 2 -0.111117 1.037403 0.663443 11.00000 -1.50000 AFIX 0 C8 1 0.248432 0.655825 0.518323 11.00000 0.02335 0.03054 = 0.01824 -0.00129 0.00244 0.00400 C9 1 0.206289 0.543680 0.439305 11.00000 0.02651 0.03175 = 0.02213 -0.00035 -0.00018 0.00299 AFIX 23 H9A 2 0.156096 0.514066 0.461042 11.00000 -1.20000 H9B 2 0.199878 0.621246 0.380961 11.00000 -1.20000 AFIX 0 C10 1 0.244945 0.363489 0.412680 11.00000 0.03900 0.03073 = 0.02633 -0.00267 0.00278 -0.00006 F1 3 0.316327 0.393103 0.386574 11.00000 0.04906 0.04326 = 0.06938 -0.00686 0.02656 0.00883 F2 3 0.249517 0.237557 0.484791 11.00000 0.06986 0.03296 = 0.04160 0.00429 0.00848 0.00968 F3 3 0.208367 0.279115 0.336876 11.00000 0.08272 0.05063 = 0.04252 -0.02402 -0.01312 0.00264 N1 6 0.332756 0.826329 0.415642 11.00000 0.02843 0.03783 = 0.01858 -0.00282 0.00380 -0.00348 AFIX 43 H1 2 0.315212 0.768464 0.363993 11.00000 -1.20000 AFIX 0 C11 1 0.304027 0.782658 0.501764 11.00000 0.02450 0.02982 = 0.01944 -0.00096 0.00031 0.00529 AFIX 43 H11 2 0.324458 0.846407 0.556451 11.00000 -1.20000 AFIX 0 C12 1 0.391956 0.966132 0.404608 11.00000 0.03227 0.03137 = 0.02545 0.00156 0.00577 -0.00012 AFIX 23 H12A 2 0.397751 1.038216 0.464903 11.00000 -1.20000 H12B 2 0.375639 1.052468 0.352654 11.00000 -1.20000 AFIX 0 C13 1 0.468655 0.886139 0.381226 11.00000 0.02658 0.03316 = 0.01844 0.00013 0.00107 -0.00108 C14 1 0.491579 0.705255 0.407436 11.00000 0.03697 0.03857 = 0.02695 0.00718 0.00485 0.00182 AFIX 43 H14 2 0.458481 0.626045 0.438843 11.00000 -1.20000 AFIX 0 C15 1 0.564098 0.641393 0.386925 11.00000 0.04164 0.04507 = 0.03568 0.00169 -0.00007 0.01339 AFIX 43 H15 2 0.579069 0.520128 0.404954 11.00000 -1.20000 AFIX 0 C16 1 0.613570 0.757427 0.340057 11.00000 0.02954 0.06302 = 0.02865 -0.00869 0.00130 0.00475 AFIX 43 H16 2 0.661873 0.714772 0.326752 11.00000 -1.20000 AFIX 0 C17 1 0.591280 0.935757 0.313179 11.00000 0.02898 0.05894 = 0.02670 -0.00741 0.00712 -0.01229 AFIX 43 H17 2 0.624389 1.013570 0.280915 11.00000 -1.20000 AFIX 0 C18 1 0.519203 1.001268 0.333933 11.00000 0.03541 0.03658 = 0.02412 -0.00065 0.00079 -0.00486 AFIX 43 H18 2 0.504821 1.122996 0.315991 11.00000 -1.20000 AFIX 0 HKLF 4 REM elmjdg_a.res in P2(1)/c REM wR2 = 0.145948, GooF = S = 0.85625, Restrained GooF = 0.85625 for all data REM R1 = 0.044291 for 2773 Fo > 4sig(Fo) and 0.079624 for all 4081 data REM 227 parameters refined using 0 restraints END WGHT 0.0504 0.1966 REM Highest difference peak 0.372, deepest hole -0.292, 1-sigma level 0.055 Q1 1 0.1683 0.7105 0.6337 11.00000 0.05 0.37 Q2 1 0.4799 0.7814 0.3675 11.00000 0.05 0.30 Q3 1 0.2186 0.5018 0.6355 11.00000 0.05 0.29 Q4 1 0.1056 0.7356 0.6243 11.00000 0.05 0.28 Q5 1 0.2306 0.4686 0.4255 11.00000 0.05 0.27 ; _shelx_res_checksum 11601 _shelx_hkl_file ; 0 0 -1 -0.10 0.40 0 0 -1 -0.10 0.30 0 0 1 -0.20 0.40 0 0 2 160.98 4.00 0 0 -2 150.98 4.00 0 0 -2 148.09 4.80 0 0 -3 3.40 1.70 0 0 -3 -6.00 1.90 0 0 -3 1.10 1.30 0 0 3 0.20 1.30 0 0 -4 9841.32 190.78 0 0 4 9698.03 189.18 0 0 -4 9518.55 190.68 0 0 -4 9999.00 189.78 0 0 -5 0.20 1.70 0 0 -5 -1.40 2.30 0 0 -5 0.50 1.50 0 0 5 -0.70 1.40 0 0 -6 974.50 23.80 0 0 -6 974.60 21.30 0 0 -6 985.20 22.40 0 0 -7 2.70 1.80 0 0 7 -1.60 1.60 0 0 -7 1.70 2.00 0 0 -7 -2.50 2.70 0 0 -8 873.81 21.90 0 0 -8 900.81 20.50 0 0 -8 922.01 23.80 0 0 -9 -0.60 2.00 0 0 -9 -1.80 2.70 0 0 -9 3.20 1.80 0 0 -10 -0.10 2.50 0 0 -10 -0.60 3.00 0 0 -10 2.70 1.90 0 0 -11 0.20 3.30 0 0 -11 0.40 1.80 0 0 -11 3.30 3.00 0 0 -12 10.10 4.00 0 0 -12 5.90 2.30 0 0 -12 9.30 4.40 0 0 -13 1.50 3.60 0 0 -13 5.10 3.40 0 0 -13 0.30 2.00 0 0 -14 103.39 9.50 0 0 -14 89.69 5.50 0 0 -14 101.59 8.70 0 0 -15 -1.50 1.90 0 0 -15 0.10 4.10 0 0 -15 0.30 3.70 0 0 -16 15.20 5.10 0 0 -16 14.50 5.50 0 0 -17 3.20 4.70 0 0 -17 -2.40 4.00 0 1 0 2.60 1.10 0 -1 0 -0.50 1.20 0 -1 0 0.90 1.10 0 1 -1 5.10 1.30 0 1 -1 4.20 1.30 0 1 1 5.90 1.30 0 -1 -1 4.70 1.30 0 -1 1 4.90 1.00 0 -1 -1 1.70 1.70 0 1 -2 444.16 10.10 0 1 2 441.16 9.90 0 1 -2 437.16 10.00 0 -1 2 443.26 10.10 0 -1 -2 420.96 11.50 0 -1 -2 421.16 9.80 0 -1 -2 432.96 10.10 0 -1 2 448.86 10.00 0 1 -3 235.08 6.80 0 1 -3 246.18 6.70 0 1 -3 235.88 5.90 0 1 3 245.58 6.40 0 -1 -3 247.18 6.90 0 -1 -3 238.48 8.60 0 -1 3 252.47 6.90 0 -1 3 249.68 6.60 0 -1 -3 239.98 6.40 0 1 4 141.29 4.70 0 1 -4 137.59 5.10 0 1 -4 142.59 4.80 0 1 -4 140.29 4.90 0 -1 4 149.29 5.00 0 -1 -4 141.99 4.70 0 -1 -4 147.49 7.10 0 -1 -4 142.09 5.30 0 -1 4 147.49 5.40 0 1 -5 67.09 4.10 0 1 -5 66.79 3.70 0 1 -5 66.89 4.00 0 1 5 73.79 3.70 0 -1 -5 62.79 5.80 0 -1 -5 63.09 3.50 0 -1 5 60.49 3.60 0 -1 -5 68.59 4.10 0 1 -6 2.40 1.80 0 1 -6 4.30 2.20 0 1 -6 0.20 2.20 0 1 6 3.30 1.90 0 -1 6 1.80 1.80 0 -1 6 2.30 1.90 0 -1 -6 2.00 1.70 0 -1 -6 4.40 2.30 0 -1 -6 -4.10 3.30 0 1 -7 1.10 2.10 0 1 -7 2.60 2.40 0 1 -7 5.40 1.90 0 -1 7 3.80 2.10 0 -1 -7 -0.10 1.70 0 -1 -7 7.70 2.60 0 -1 -7 2.50 3.60 0 1 -8 140.89 5.80 0 1 -8 135.09 6.70 0 1 -8 138.59 6.60 0 -1 -8 133.39 5.50 0 -1 -8 142.89 8.80 0 -1 -8 128.29 6.50 0 1 -9 5.40 2.60 0 1 -9 5.10 2.50 0 1 -9 4.90 2.10 0 -1 -9 3.20 1.90 0 -1 -9 0.20 3.20 0 -1 -9 1.60 2.30 0 1 -10 276.07 10.70 0 1 -10 283.27 9.30 0 1 -10 291.17 11.00 0 -1 -10 281.37 13.50 0 -1 -10 292.57 11.00 0 -1 -10 277.27 8.90 0 1 -11 15.60 3.80 0 1 -11 21.00 4.20 0 1 -11 22.10 3.20 0 -1 -11 14.50 3.80 0 -1 -11 19.40 3.00 0 -1 -11 14.50 5.20 0 1 -12 2.60 2.30 0 1 -12 2.90 3.00 0 1 -12 -3.20 2.40 0 -1 -12 -3.00 3.00 0 -1 -12 0.00 3.90 0 -1 -12 -2.80 1.80 0 1 -13 -2.20 2.00 0 1 -13 3.50 3.20 0 1 -13 2.50 3.10 0 -1 -13 -1.80 3.90 0 -1 -13 1.00 2.00 0 -1 -13 -2.60 3.00 0 1 -14 18.90 5.00 0 1 -14 20.30 4.90 0 1 -14 16.50 3.10 0 -1 -14 17.90 4.70 0 -1 -14 19.00 3.20 0 -1 -14 19.50 6.40 0 1 -15 8.80 4.30 0 1 -15 5.80 2.40 0 1 -15 14.90 4.70 0 -1 -15 5.20 2.80 0 -1 -15 15.70 6.10 0 -1 -15 2.20 4.20 0 1 -16 64.09 8.00 0 -1 -16 60.59 7.50 0 -1 -16 71.29 10.50 0 1 -17 2.50 4.30 0 -1 -17 0.30 5.00 0 -1 -17 0.00 4.30 0 2 0 449.26 11.00 0 -2 0 447.16 10.90 0 -2 0 454.15 11.80 0 2 -1 1081.59 23.50 0 2 1 1115.29 23.50 0 -2 1 1112.29 23.60 0 -2 -1 1099.49 25.10 0 2 2 139.89 5.10 0 2 -2 139.09 5.20 0 2 -2 129.79 5.20 0 -2 2 145.09 4.40 0 -2 -2 143.29 5.10 0 -2 -2 143.79 7.00 0 2 -3 496.95 12.50 0 2 -3 508.05 12.70 0 2 3 517.55 12.40 0 -2 -3 526.85 15.30 0 -2 3 519.55 12.60 0 -2 -3 497.15 12.20 0 -2 -3 515.45 12.70 0 -2 3 515.65 12.60 0 2 -4 167.18 6.20 0 2 4 167.18 5.80 0 2 -4 158.48 6.00 0 -2 -4 163.38 6.20 0 -2 -4 152.28 8.50 0 -2 -4 157.18 5.60 0 -2 4 155.68 5.80 0 2 -5 275.37 8.40 0 2 -5 260.67 6.40 0 2 5 284.27 8.20 0 2 -5 280.87 8.70 0 -2 -5 253.97 11.40 0 -2 -5 268.27 8.00 0 -2 -5 271.97 8.80 0 -2 5 271.47 9.40 0 -2 5 269.17 8.50 0 2 -6 55.19 4.00 0 2 -6 60.39 4.20 0 2 -6 45.50 2.80 0 2 -6 59.69 4.70 0 -2 6 48.50 3.90 0 -2 -6 52.29 6.60 0 -2 -6 52.79 3.80 0 -2 -6 55.19 4.50 0 2 -7 98.39 5.10 0 2 -7 83.19 5.30 0 2 -7 84.19 3.90 0 -2 -7 80.89 7.70 0 -2 -7 91.39 4.60 0 -2 -7 87.09 5.60 0 -2 7 91.59 6.00 0 2 -8 53.59 4.30 0 2 -8 55.79 4.70 0 2 -8 57.39 3.50 0 -2 -8 54.99 4.90 0 -2 -8 53.29 3.90 0 -2 -8 69.29 7.90 0 2 -9 24.10 3.70 0 2 -9 30.00 3.30 0 2 -9 35.90 3.80 0 -2 -9 27.20 3.10 0 -2 -9 26.30 5.80 0 -2 -9 24.10 3.90 0 2 -10 117.39 7.10 0 2 -10 105.19 5.80 0 2 -10 96.99 5.40 0 -2 -10 106.19 7.10 0 -2 -10 106.59 9.80 0 -2 -10 117.79 5.60 0 2 -11 29.70 4.40 0 2 -11 39.90 4.10 0 2 -11 35.80 4.00 0 -2 -11 29.00 3.50 0 -2 -11 30.40 6.80 0 -2 -11 37.60 5.00 0 2 -12 0.50 3.00 0 2 -12 1.50 2.40 0 2 -12 2.10 2.20 0 -2 -12 1.90 2.00 0 -2 -12 4.00 4.90 0 -2 -12 -1.00 3.10 0 2 -13 15.50 3.20 0 2 -13 2.70 3.20 0 -2 -13 4.90 5.20 0 -2 -13 14.60 4.50 0 -2 -13 16.20 3.00 0 2 -14 7.80 4.10 0 2 -14 5.50 2.60 0 -2 -14 -0.90 3.90 0 -2 -14 12.90 6.20 0 -2 -14 6.10 2.50 0 2 -15 2.50 3.70 0 2 -15 3.50 2.50 0 -2 -15 7.40 4.30 0 -2 -15 7.40 5.40 0 2 -16 1.20 3.70 0 -2 -16 2.50 4.20 0 -2 -16 6.30 5.90 0 2 -17 52.59 7.50 0 -2 -17 36.90 6.90 0 -2 -17 52.19 10.30 0 3 0 0.00 0.80 0 3 0 2.50 2.00 0 -3 0 -1.40 2.20 0 3 -1 391.76 10.90 0 3 1 388.16 10.80 0 -3 1 397.26 10.70 0 -3 -1 372.26 12.50 0 -3 1 392.06 11.20 0 3 -2 332.37 9.60 0 3 2 332.17 10.50 0 -3 2 309.87 9.00 0 -3 -2 301.67 11.60 0 3 -3 738.83 17.80 0 3 -3 755.02 18.00 0 -3 -3 736.13 17.90 0 -3 -3 739.23 21.00 0 -3 3 701.23 16.20 0 3 -4 85.59 5.20 0 3 -4 89.89 5.00 0 -3 -4 81.99 4.90 0 -3 -4 74.79 6.80 0 3 -5 33.90 4.00 0 3 -5 42.80 4.10 0 -3 -5 32.20 6.00 0 -3 -5 31.50 3.30 0 -3 -5 30.60 3.60 0 -3 5 43.30 4.30 0 3 -6 30.80 3.60 0 3 -6 23.30 3.30 0 -3 -6 23.90 3.40 0 -3 -6 24.40 3.10 0 -3 -6 22.60 5.30 0 3 -7 130.69 6.40 0 3 -7 123.09 6.60 0 3 -7 136.69 6.80 0 -3 -7 136.19 9.80 0 -3 -7 130.69 5.90 0 -3 -7 130.19 6.80 0 3 -8 26.60 3.90 0 3 -8 34.20 3.90 0 -3 -8 24.40 5.80 0 -3 -8 29.70 3.50 0 -3 -8 19.30 3.60 0 3 -9 12.10 3.60 0 3 -9 16.40 3.30 0 -3 -9 11.90 5.10 0 -3 -9 10.30 3.60 0 -3 -9 17.50 3.00 0 3 -10 7.90 2.80 0 3 -10 10.50 3.60 0 -3 -10 2.10 3.30 0 -3 -10 8.40 2.60 0 -3 -10 9.30 5.30 0 3 -11 23.10 3.80 0 3 -11 6.90 3.40 0 -3 -11 17.50 4.40 0 -3 -11 12.70 2.90 0 -3 -11 14.30 6.20 0 3 -12 5.20 3.60 0 3 -12 4.60 2.90 0 -3 -12 3.30 3.50 0 -3 -12 7.10 5.90 0 -3 -12 2.30 2.30 0 3 -13 -0.50 2.50 0 3 -13 1.50 3.20 0 -3 -13 1.80 3.70 0 -3 -13 1.80 2.10 0 -3 -13 1.00 5.10 0 3 -14 5.40 2.80 0 3 -14 4.90 3.80 0 -3 -14 1.90 2.30 0 -3 -14 8.70 4.50 0 -3 -14 4.90 5.80 0 3 -15 -0.10 3.80 0 3 -15 0.50 2.50 0 -3 -15 1.20 5.30 0 -3 -15 3.20 4.10 0 3 -16 -4.50 3.60 0 -3 -16 6.80 6.20 0 -3 -16 3.10 4.50 0 -3 -17 16.60 7.60 0 4 0 56.49 4.50 0 -4 0 55.79 5.20 0 4 1 45.50 4.40 0 4 -1 45.20 4.30 0 -4 1 36.80 4.30 0 -4 -1 43.50 5.50 0 4 -2 6.90 2.60 0 4 2 7.90 2.30 0 -4 -2 7.90 3.80 0 -4 2 11.20 2.70 0 4 -3 -1.90 1.90 0 4 -3 0.00 2.10 0 -4 3 0.70 1.70 0 -4 -3 -2.80 3.00 0 4 -4 162.48 7.20 0 4 -4 165.88 7.30 0 -4 4 164.78 5.50 0 -4 -4 165.08 10.10 0 4 -5 1.50 2.30 0 4 -5 3.00 2.40 0 -4 -5 0.50 4.10 0 -4 -5 5.30 2.60 0 4 -6 205.88 8.50 0 4 -6 194.88 8.60 0 -4 -6 195.58 8.80 0 -4 -6 200.18 12.10 0 4 -7 63.79 6.00 0 4 -7 58.09 5.30 0 -4 -7 59.99 8.90 0 -4 -7 61.59 5.90 0 4 -8 77.89 6.10 0 4 -8 71.19 5.50 0 -4 -8 85.09 7.20 0 -4 -8 78.69 10.10 0 4 -9 0.70 2.60 0 4 -9 1.00 2.40 0 4 -9 4.00 3.10 0 -4 -9 5.80 3.60 0 -4 -9 3.30 5.10 0 4 -10 -1.00 2.50 0 4 -10 -2.70 2.80 0 -4 -10 0.70 2.80 0 -4 -10 2.00 5.20 0 4 -11 45.30 6.20 0 4 -11 41.80 5.00 0 -4 -11 36.20 8.20 0 -4 -11 38.60 6.00 0 4 -12 74.39 6.60 0 4 -12 52.39 6.50 0 -4 -12 57.29 7.10 0 -4 -12 71.29 11.30 0 4 -13 3.40 3.70 0 4 -13 9.20 3.30 0 -4 -13 19.20 6.70 0 -4 -13 1.20 4.00 0 4 -14 -0.40 2.60 0 4 -14 1.20 3.60 0 -4 -14 -2.40 3.90 0 -4 -14 5.80 5.80 0 4 -15 7.20 4.50 0 4 -15 10.70 3.60 0 -4 -15 9.60 6.90 0 -4 -15 6.10 4.80 0 4 -16 24.20 5.80 0 -4 -16 -1.50 5.50 0 -4 -16 3.10 4.50 0 5 0 1.40 2.30 0 -5 0 -2.40 2.70 0 5 -1 71.99 5.50 0 5 1 86.19 5.80 0 -5 -1 68.89 6.50 0 -5 1 71.09 6.00 0 5 2 107.59 6.40 0 5 -2 111.79 6.60 0 -5 2 119.79 6.70 0 -5 -2 109.79 8.30 0 5 -3 3.40 2.50 0 5 -3 -0.90 2.20 0 5 3 2.40 2.60 0 -5 -3 2.40 3.60 0 -5 3 -0.50 2.00 0 5 -4 -1.20 2.30 0 5 4 -1.30 2.10 0 5 -4 -3.00 2.00 0 -5 -4 -1.50 3.60 0 -5 4 -1.60 1.60 0 5 -5 21.90 4.00 0 5 -5 17.20 3.60 0 -5 5 21.60 3.10 0 -5 -5 19.80 6.00 0 5 -6 19.20 3.80 0 5 -6 17.40 3.70 0 -5 -6 18.30 6.10 0 5 -7 48.60 5.50 0 5 -7 38.80 5.10 0 -5 -7 60.49 6.40 0 -5 -7 57.89 9.00 0 5 -8 14.30 3.80 0 5 -8 13.10 3.70 0 -5 -8 20.00 6.70 0 -5 -8 20.30 4.60 0 5 -9 13.20 3.90 0 5 -9 15.70 3.80 0 -5 -9 11.50 4.20 0 -5 -9 1.00 5.00 0 5 -10 3.20 3.00 0 5 -10 1.50 2.90 0 5 -10 -7.00 2.60 0 -5 -10 2.60 5.30 0 -5 -10 1.10 3.70 0 5 -11 7.60 3.40 0 5 -11 4.30 3.80 0 -5 -11 -0.20 3.70 0 -5 -11 11.20 6.40 0 5 -12 6.40 4.10 0 5 -12 16.70 4.00 0 -5 -12 12.20 7.10 0 -5 -12 15.20 5.00 0 5 -13 10.80 4.60 0 5 -13 11.90 3.80 0 -5 -13 7.00 4.80 0 -5 -13 3.50 6.30 0 5 -14 -3.30 3.50 0 5 -14 -1.30 2.90 0 -5 -14 -2.60 4.20 0 -5 -14 -1.80 5.30 0 5 -15 2.30 3.10 0 5 -15 -1.90 3.60 0 -5 -15 4.30 6.80 0 -5 -15 6.10 4.80 0 6 0 1.60 2.90 0 -6 0 0.00 3.30 0 6 1 45.50 5.20 0 6 -1 55.09 5.80 0 -6 1 57.09 6.50 0 -6 -1 59.39 7.40 0 6 -2 2.90 2.90 0 6 2 4.40 2.90 0 -6 2 -2.10 2.60 0 -6 -2 5.90 4.20 0 6 3 132.99 7.90 0 6 -3 137.49 8.10 0 6 -3 144.19 8.20 0 -6 -3 141.19 10.60 0 -6 3 139.59 7.50 0 6 -4 13.20 3.70 0 6 4 9.10 3.40 0 6 -4 8.60 3.30 0 -6 -4 3.10 4.80 0 6 -5 28.30 4.70 0 6 5 25.40 4.60 0 6 -5 30.60 4.80 0 -6 -5 37.40 7.50 0 6 -6 25.40 4.60 0 6 -6 19.40 4.20 0 -6 -6 18.40 6.50 0 6 -7 25.80 4.70 0 6 -7 19.50 4.00 0 -6 -7 30.30 7.90 0 6 -8 -1.10 2.70 0 6 -8 -0.30 2.50 0 -6 -8 -3.20 5.10 0 6 -9 111.99 8.20 0 6 -9 115.89 7.80 0 -6 -9 96.99 12.50 0 6 -10 2.90 3.20 0 6 -10 -2.30 3.40 0 6 -10 -2.00 2.70 0 -6 -10 3.40 4.10 0 -6 -10 -4.80 5.40 0 6 -11 0.10 2.90 0 6 -11 0.40 3.30 0 6 -11 -2.40 2.80 0 -6 -11 1.20 4.10 0 -6 -11 3.70 6.10 0 6 -12 3.80 3.80 0 6 -12 -1.90 2.90 0 -6 -12 -0.20 5.50 0 -6 -12 1.00 4.30 0 6 -13 17.70 5.00 0 6 -13 30.70 5.50 0 -6 -13 28.20 8.60 0 -6 -13 36.40 7.10 0 7 0 -4.30 2.40 0 -7 0 -0.40 3.70 0 7 -1 47.40 6.10 0 7 1 50.69 6.10 0 -7 -1 48.70 7.40 0 -7 1 55.09 6.90 0 7 -2 14.30 4.00 0 7 2 17.10 4.30 0 7 -2 11.80 4.10 0 -7 2 18.30 4.50 0 -7 -2 20.70 6.00 0 7 3 -1.00 2.80 0 7 -3 0.20 3.00 0 7 -3 -0.50 3.00 0 -7 -3 -0.90 4.40 0 7 -4 8.60 3.70 0 7 -4 7.80 3.60 0 7 4 5.80 3.40 0 -7 -4 12.00 5.60 0 7 5 3.90 3.20 0 7 -5 -0.50 2.70 0 7 -5 2.90 3.30 0 -7 -5 4.30 5.30 0 7 -6 1.10 2.80 0 7 6 -0.90 3.20 0 7 -6 1.50 3.20 0 -7 -6 8.10 5.50 0 7 -7 55.29 6.30 0 7 7 60.89 7.10 0 7 -7 50.09 6.50 0 -7 -7 52.49 9.60 0 7 8 14.10 4.40 0 7 -8 5.10 3.50 0 7 -8 8.80 3.80 0 -7 -8 12.70 6.40 0 7 -9 21.90 5.00 0 7 -9 19.60 4.80 0 -7 -9 28.50 7.90 0 7 -10 4.10 3.50 0 7 -10 9.00 3.70 0 -7 -10 7.10 6.60 0 7 -11 10.80 4.80 0 7 -11 7.30 4.00 0 7 -11 9.30 3.80 0 -7 -11 11.90 7.10 0 8 0 24.00 5.20 0 -8 0 26.40 6.10 0 8 1 4.10 3.60 0 8 -1 0.70 3.30 0 -8 -1 9.80 3.80 0 8 -2 0.20 3.30 0 8 2 7.90 4.00 0 8 -2 -1.20 3.40 0 -8 -2 -1.80 4.40 0 8 -3 4.90 3.60 0 8 -3 9.40 4.10 0 8 3 12.90 4.30 0 -8 -3 12.10 6.00 0 8 4 9.00 4.00 0 8 -4 6.70 3.50 0 8 -4 2.80 3.30 0 -8 -4 7.90 5.80 0 8 5 -0.70 3.10 0 8 -5 -2.30 3.00 0 8 -5 2.70 3.40 0 -8 -5 9.20 6.00 0 8 -6 4.40 4.00 0 8 -6 3.40 3.40 0 8 6 4.30 3.60 0 -8 -6 4.60 5.80 0 8 -7 10.70 4.30 0 8 -7 4.40 3.90 0 8 7 11.40 4.40 0 -8 -7 10.80 6.40 0 8 8 22.50 5.30 0 8 -8 22.10 4.90 0 8 -8 23.00 5.20 0 -8 -8 22.10 8.30 0 8 9 -4.90 3.30 0 8 -9 1.70 3.40 0 8 -9 -1.60 3.10 0 -8 -9 0.50 6.00 0 9 0 -1.80 3.40 0 9 -1 -0.40 4.40 0 9 1 8.20 4.40 0 9 -1 5.50 3.90 0 -9 -1 12.60 6.30 0 9 -2 23.00 5.80 0 9 2 31.80 6.10 0 9 -2 30.60 6.20 0 -9 -2 20.70 6.60 0 9 -3 -3.30 3.10 0 9 -3 0.10 3.60 0 9 3 -0.20 3.60 0 9 4 1.00 3.80 0 9 -4 1.50 3.70 0 9 -4 4.50 3.60 0 -9 -4 0.40 5.40 1 0 -17 -1.90 4.00 1 0 -17 2.40 4.50 1 0 -16 137.09 10.40 1 0 -16 161.78 11.90 1 0 -15 1.60 4.00 1 0 -15 2.80 4.00 1 0 -14 2.20 1.90 1 0 -14 4.10 4.10 1 0 -14 0.80 3.70 1 0 -13 3.00 2.00 1 0 -13 -2.80 3.00 1 0 -13 2.80 3.80 1 0 -12 383.66 10.90 1 0 -12 398.86 15.70 1 0 -12 388.56 13.90 1 0 -11 -1.40 2.90 1 0 -11 -1.10 1.60 1 0 -11 -3.10 2.40 1 0 -10 11.40 2.10 1 0 -10 15.80 3.60 1 0 -10 24.20 4.60 1 0 -9 -0.20 1.40 1 0 -9 -0.10 2.40 1 0 -9 3.40 2.40 1 0 -8 1062.69 26.80 1 0 -8 1084.19 25.10 1 0 -8 1041.20 23.00 1 0 -7 0.80 2.70 1 0 -7 1.20 1.50 1 0 -7 2.10 2.00 -1 0 7 2.20 1.70 -1 0 6 20.60 2.40 1 0 -6 18.20 3.50 1 0 -6 23.20 2.20 -1 0 5 -1.70 1.30 1 0 -5 -2.80 2.00 1 0 -5 -1.10 1.20 1 0 -5 -0.90 1.50 1 0 -4 4156.28 82.79 1 0 -4 4214.48 81.79 1 0 -4 4205.68 83.89 -1 0 4 4209.68 81.99 1 0 -3 -1.00 1.80 1 0 -3 3.50 1.50 1 0 -3 -0.20 1.00 -1 0 3 3.60 1.10 1 0 -2 44.30 1.50 -1 0 2 46.10 1.60 1 0 -2 44.20 2.60 1 0 -1 0.30 0.70 -1 0 0 -0.10 0.20 1 0 0 0.40 0.30 1 0 0 0.10 0.30 -1 0 -1 1.50 0.70 1 0 1 0.30 0.20 -1 0 -2 353.46 8.30 1 0 2 375.66 8.30 1 0 3 -0.10 1.40 -1 0 -3 0.30 1.60 -1 0 -3 1.30 1.50 1 0 4 889.41 18.80 -1 0 -4 825.62 18.50 -1 0 -4 859.21 19.00 -1 0 -4 845.42 20.00 -1 0 -5 0.40 1.70 -1 0 -5 0.80 1.70 1 0 5 2.00 1.60 -1 0 -5 -0.50 2.80 -1 0 -6 516.95 15.30 -1 0 -6 507.65 12.90 1 0 6 528.45 13.20 -1 0 -6 523.35 13.50 -1 0 -7 0.20 1.70 -1 0 -7 0.10 2.00 -1 0 -7 -0.40 3.20 -1 0 -8 2.10 3.10 -1 0 -8 -1.30 2.00 -1 0 -8 1.20 1.80 -1 0 -9 0.50 1.80 -1 0 -9 0.00 2.30 -1 0 -9 1.30 3.00 1 0 10 839.72 18.50 -1 0 -10 828.82 23.90 -1 0 -10 799.92 21.70 -1 0 -10 815.52 20.00 1 0 11 1.00 2.00 -1 0 -11 -1.40 2.70 -1 0 -11 0.00 2.00 -1 0 -11 0.30 3.60 -1 0 -12 1.40 2.20 -1 0 -12 5.20 3.20 -1 0 -12 -1.20 3.90 -1 0 -13 -0.40 2.20 -1 0 -13 11.80 4.70 -1 0 -13 -0.90 3.10 -1 0 -14 234.08 11.80 -1 0 -14 226.38 9.00 -1 0 -14 235.68 13.70 -1 0 -15 1.70 3.90 -1 0 -15 3.70 4.50 -1 0 -15 0.20 2.40 -1 0 -16 14.00 4.90 -1 0 -16 19.60 6.20 -1 0 -17 3.20 4.60 -1 0 -17 3.00 4.60 1 1 -17 8.60 5.00 1 -1 -17 19.60 5.40 1 -1 -17 23.30 7.10 1 1 -16 26.10 6.00 1 -1 -16 39.00 8.10 1 -1 -16 24.30 5.70 1 1 -15 3.50 4.70 1 1 -15 5.90 4.00 1 -1 -15 5.80 4.80 1 -1 -15 6.60 3.90 1 1 -14 85.09 7.70 1 1 -14 97.69 8.50 1 1 -14 87.69 5.00 1 -1 -14 92.39 10.70 1 -1 -14 98.29 8.60 1 -1 -14 85.09 4.70 1 1 -13 7.70 3.50 1 1 -13 0.70 3.20 1 1 -13 4.80 2.20 1 -1 -13 0.60 4.20 1 -1 -13 3.10 1.90 1 -1 -13 5.80 3.50 1 1 -12 136.09 6.10 1 1 -12 149.88 8.40 1 1 -12 132.89 8.20 1 -1 -12 137.59 10.60 1 -1 -12 137.39 8.20 1 -1 -12 135.29 5.70 1 1 -11 81.89 6.40 1 1 -11 94.09 6.60 1 1 -11 83.29 4.80 1 -1 -11 88.29 6.70 1 -1 -11 90.39 4.60 1 -1 -11 89.69 8.50 1 1 -10 4.80 2.60 1 1 -10 3.40 2.70 1 1 -10 3.70 2.00 1 -1 -10 5.80 3.80 1 -1 -10 3.00 1.70 1 -1 -10 3.60 2.90 1 1 -9 19.50 3.40 1 1 -9 19.30 2.60 1 1 -9 14.00 3.10 1 -1 -9 19.00 4.70 1 -1 -9 20.30 2.40 1 -1 -9 14.40 3.10 1 1 -8 96.39 4.60 1 1 -8 101.59 5.50 1 1 -8 96.29 5.60 1 -1 -8 90.39 4.20 1 -1 -8 101.29 7.70 1 -1 -8 98.69 5.70 1 1 -7 131.19 5.10 1 1 -7 124.69 5.80 1 1 -7 128.39 6.00 -1 1 7 127.59 5.20 -1 -1 7 121.39 6.00 1 -1 -7 122.99 7.90 1 -1 -7 133.09 4.80 1 -1 -7 122.39 6.00 1 1 -6 103.39 5.10 -1 1 6 104.49 4.40 1 1 -6 107.19 4.50 1 1 -6 103.99 4.90 -1 -1 6 105.79 5.30 1 -1 -6 101.39 7.00 1 -1 -6 100.19 4.10 -1 -1 6 100.39 4.60 1 -1 -6 105.79 5.20 1 1 -5 0.30 1.50 1 1 -5 -0.40 1.50 1 1 -5 -0.80 1.70 -1 1 5 -0.60 1.30 -1 -1 5 1.50 1.40 1 -1 -5 1.70 1.80 1 -1 -5 0.50 1.30 1 -1 -5 -3.60 2.50 -1 -1 5 -0.40 1.50 1 1 -4 35.10 2.40 1 1 -4 36.10 3.00 -1 1 4 38.80 2.60 1 1 -4 33.20 2.50 -1 -1 4 37.10 2.80 1 -1 -4 44.20 3.20 1 -1 -4 33.80 2.40 1 -1 -4 35.50 4.30 -1 -1 4 31.80 2.90 1 1 -3 27.20 1.60 1 1 -3 31.50 2.40 1 1 -3 25.30 2.60 -1 1 3 30.20 2.30 1 -1 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13.30 3.20 4 5 -6 14.10 3.30 4 -5 -6 15.90 5.70 -4 5 5 68.99 5.50 4 5 -5 66.39 5.60 4 5 -5 78.19 7.10 4 -5 -5 79.49 9.70 4 5 -4 -2.80 2.00 -4 5 4 0.40 2.10 4 5 -4 0.60 2.50 -4 -5 4 1.10 1.90 4 -5 -4 5.50 4.40 -4 5 3 37.30 4.40 4 5 -3 48.50 5.10 4 5 -3 39.00 4.70 4 -5 -3 47.60 7.30 -4 -5 3 45.40 4.50 -4 5 2 0.40 2.40 4 5 -2 -1.30 2.30 4 5 -2 -1.00 2.30 4 -5 -2 -0.30 3.30 -4 -5 2 1.00 2.60 4 5 -1 123.09 6.90 -4 5 1 121.59 7.00 4 -5 -1 112.49 8.40 -4 -5 1 120.79 7.80 4 5 0 64.99 5.70 -4 5 0 46.10 4.80 4 -5 0 53.99 6.80 -4 -5 0 56.89 6.50 -4 5 -1 133.59 7.20 4 5 1 138.49 7.30 -4 -5 -1 126.69 9.10 4 -5 1 134.59 8.30 4 5 2 101.89 6.50 -4 5 -2 95.19 6.50 4 -5 2 106.99 7.20 -4 -5 -2 96.09 8.50 -4 5 -3 75.09 6.40 -4 5 -3 59.19 4.90 -4 -5 -3 50.79 5.10 -4 -5 -3 66.99 8.40 4 -5 3 57.69 5.60 -4 5 -4 43.70 4.50 -4 5 -4 34.90 4.80 -4 -5 -4 31.70 7.00 -4 -5 -4 26.80 4.30 4 -5 4 39.40 4.80 -4 5 -5 45.30 5.20 -4 5 -5 49.90 4.90 -4 -5 -5 38.60 4.80 -4 -5 -5 40.20 7.70 -4 5 -6 233.88 10.40 -4 5 -6 233.88 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6 58.89 4.60 -6 4 -6 42.50 4.80 -6 -4 -6 47.90 5.30 -6 -4 -6 51.79 9.00 -6 -4 -6 56.99 5.70 -6 4 -7 83.39 5.00 6 4 7 76.09 4.90 -6 4 -7 69.89 6.40 -6 -4 -7 70.79 6.40 -6 -4 -7 72.49 10.10 -6 -4 -7 90.29 6.80 -6 4 -8 47.40 5.60 6 4 8 73.09 4.70 -6 4 -8 55.19 5.70 -6 -4 -8 60.29 6.20 -6 -4 -8 64.49 6.40 -6 -4 -8 34.90 8.00 -6 4 -9 11.40 4.00 -6 4 -9 8.70 3.50 -6 -4 -9 7.40 3.70 -6 -4 -9 10.70 6.60 -6 -4 -9 9.00 3.70 -6 4 -10 6.90 3.40 -6 4 -10 2.50 3.60 -6 -4 -10 -0.80 3.30 -6 -4 -10 0.50 3.20 -6 -4 -10 6.10 6.60 -6 4 -11 24.10 5.50 -6 4 -11 27.40 5.00 -6 -4 -11 40.40 9.50 -6 -4 -11 28.20 5.40 -6 -4 -11 29.40 5.20 -6 4 -12 25.70 5.40 -6 4 -12 22.60 5.10 -6 -4 -12 25.80 5.70 -6 -4 -12 23.50 4.90 -6 -4 -12 39.90 9.80 -6 4 -13 -2.50 3.60 -6 4 -13 4.80 3.60 6 -4 13 0.80 3.40 -6 -4 -13 -1.20 3.80 -6 -4 -13 7.90 6.60 -6 -4 -13 6.00 3.80 -6 4 -14 3.20 4.10 -6 4 -14 -2.30 3.20 -6 -4 -14 8.10 3.80 -6 -4 -14 6.50 4.90 -6 -4 -14 13.10 7.30 6 -4 14 0.80 3.50 -6 4 -15 1.20 3.50 -6 4 -15 2.80 4.50 -6 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18.30 7.60 -8 -2 -9 14.90 3.90 -8 2 -10 10.20 3.80 8 2 10 9.60 2.60 -8 2 -10 10.50 3.90 -8 -2 -10 9.40 3.70 -8 -2 -10 12.60 7.90 8 -2 10 10.50 3.40 -8 -2 -10 12.70 3.90 -8 2 -11 49.90 5.80 -8 2 -11 56.49 6.40 8 -2 11 68.89 6.50 -8 -2 -11 67.59 11.40 -8 -2 -11 64.29 6.80 -8 -2 -11 55.89 6.30 -8 2 -12 10.70 4.10 -8 2 -12 5.80 3.70 -8 -2 -12 7.50 4.20 -8 -2 -12 17.00 4.30 8 -2 12 8.00 3.50 -8 -2 -12 6.00 7.60 -8 2 -13 -0.20 3.10 -8 2 -13 -19.40 8.00 -8 2 -13 7.30 3.80 -8 -2 -13 6.70 7.20 -8 -2 -13 4.90 3.80 -8 -2 -13 1.60 3.60 8 -2 13 0.60 2.90 -8 2 -14 12.40 4.60 -8 2 -14 38.20 10.60 -8 2 -14 5.20 3.80 8 -2 14 13.60 3.80 -8 -2 -14 27.40 9.50 -8 -2 -14 16.10 4.60 -8 -2 -14 18.80 5.20 -8 2 -15 13.80 4.50 -8 2 -15 6.80 4.50 -8 -2 -15 5.90 4.10 -8 -2 -15 21.40 9.60 -8 -2 -15 8.50 5.00 -8 2 -16 -4.50 3.00 -8 2 -16 -3.60 3.50 -8 -2 -16 1.40 3.60 -8 -2 -16 -4.30 3.80 -8 -2 -16 15.20 8.50 8 3 -16 22.10 5.10 8 -3 -16 27.40 8.10 8 -3 -16 33.70 5.90 8 3 -15 2.90 3.30 8 -3 -15 10.90 6.40 8 -3 -15 16.60 4.60 8 3 -14 29.00 5.00 8 -3 -14 25.90 4.90 8 -3 -14 30.30 8.30 8 3 -13 97.09 7.30 8 -3 -13 93.39 8.00 8 -3 -13 96.79 12.20 8 3 -12 110.49 7.30 8 -3 -12 127.19 12.10 8 -3 -12 94.69 7.40 8 3 -11 26.60 4.20 8 -3 -11 17.60 4.00 8 -3 -11 19.20 6.30 8 3 -10 30.70 4.10 8 -3 -10 35.70 7.80 8 -3 -10 25.60 4.20 8 3 -9 85.39 5.50 8 -3 -9 76.79 5.80 8 -3 -9 72.09 9.30 8 3 -8 44.30 5.60 8 3 -8 44.90 4.20 8 3 -8 40.30 2.20 8 3 -8 44.40 2.30 8 -3 -8 41.50 3.20 8 -3 -8 45.30 7.40 8 -3 -8 51.99 4.90 8 3 -7 8.90 2.40 8 3 -7 8.10 1.50 8 3 -7 11.00 3.70 8 3 -7 6.30 1.50 8 -3 -7 8.20 2.10 8 -3 -7 3.90 2.30 8 -3 -7 9.50 5.20 8 3 -6 10.50 3.70 8 3 -6 8.20 1.80 8 3 -6 8.30 1.70 -8 3 6 5.90 1.90 8 -3 -6 11.30 5.10 8 -3 -6 3.80 2.00 8 3 -5 65.49 6.10 8 3 -5 54.09 5.10 8 3 -5 51.89 3.40 8 3 -5 55.19 3.30 -8 3 5 55.19 3.70 8 -3 -5 51.59 4.00 8 -3 -5 54.89 7.40 -8 3 4 48.80 3.50 8 3 -4 46.40 3.20 8 3 -4 45.50 4.80 8 3 -4 43.70 3.30 8 3 -4 47.30 4.80 8 -3 -4 34.70 6.30 -8 -3 4 49.60 4.10 8 -3 -4 49.90 4.20 8 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-6 0.60 4.90 8 -4 -6 6.40 2.30 -8 4 5 -0.40 1.90 8 4 -5 1.10 3.10 8 4 -5 1.70 1.90 8 -4 -5 1.80 4.40 8 -4 -5 -1.00 2.00 8 4 -4 330.07 12.40 8 4 -4 327.67 10.20 -8 4 4 315.97 10.30 8 -4 -4 319.77 10.60 8 -4 -4 343.77 16.00 -8 4 3 55.39 4.70 8 4 -3 49.40 5.50 8 4 -3 51.49 4.40 8 4 -3 62.09 5.90 8 -4 -3 57.99 7.70 -8 -4 3 45.70 4.60 8 -4 -3 48.70 4.70 8 4 -2 35.10 3.90 8 4 -2 33.40 4.40 8 4 -2 43.60 5.00 -8 4 2 36.10 4.00 8 -4 -2 44.50 4.50 8 -4 -2 38.10 6.20 -8 -4 2 36.70 4.50 -8 4 1 4.30 2.40 8 4 -1 9.70 2.60 8 4 -1 10.80 3.40 8 4 -1 4.90 3.00 8 -4 -1 6.70 4.00 8 -4 -1 1.30 2.50 -8 -4 1 8.70 3.00 8 4 0 237.68 9.00 -8 4 0 238.38 9.10 -8 -4 0 228.48 9.50 8 -4 0 239.48 11.90 8 -4 0 230.98 9.50 8 4 1 8.50 3.00 -8 4 -1 8.70 2.80 -8 -4 -1 10.80 3.10 8 -4 1 7.70 3.30 8 -4 1 6.60 3.80 8 4 2 64.99 5.40 -8 4 -2 71.79 5.60 8 -4 2 61.99 6.90 -8 -4 -2 73.09 6.20 8 -4 2 66.89 5.80 -8 4 -3 12.20 3.50 -8 4 -3 13.60 2.10 8 4 3 5.80 2.70 -8 -4 -3 4.40 5.80 8 -4 3 7.00 3.70 -8 -4 -3 14.70 3.70 -8 4 -4 21.80 2.50 8 4 4 20.60 3.50 -8 4 -4 19.40 3.90 -8 -4 -4 27.50 7.70 -8 -4 -4 22.00 4.10 -8 -4 -4 15.10 3.10 -8 4 -5 0.20 2.60 -8 4 -5 0.50 1.60 8 4 5 -3.20 2.10 -8 -4 -5 -0.30 2.90 -8 -4 -5 -2.60 2.40 -8 -4 -5 5.00 6.50 8 4 6 16.10 3.30 -8 4 -6 19.50 4.10 -8 -4 -6 23.60 4.00 -8 -4 -6 26.00 4.80 -8 -4 -6 25.50 8.10 -8 4 -7 7.20 3.40 8 4 7 8.00 2.70 -8 4 -7 10.30 3.70 -8 -4 -7 11.80 3.50 -8 -4 -7 11.40 7.50 -8 -4 -7 15.60 4.30 -8 4 -8 0.90 3.00 8 4 8 -1.00 2.10 -8 4 -8 -1.70 2.90 -8 -4 -8 3.20 6.70 -8 -4 -8 -1.90 2.80 8 -4 8 -0.20 3.30 -8 -4 -8 1.20 3.50 -8 4 -9 6.00 3.40 -8 4 -9 -2.10 3.20 8 -4 9 -3.60 3.10 -8 -4 -9 -4.40 2.90 -8 -4 -9 0.40 3.40 -8 -4 -9 -5.10 6.20 -8 4 -10 17.90 5.00 -8 4 -10 18.90 4.70 -8 -4 -10 28.90 9.10 8 -4 10 15.90 4.50 -8 -4 -10 21.50 4.70 -8 -4 -10 25.00 5.20 -8 4 -11 18.60 4.80 -8 4 -11 11.80 4.30 -8 -4 -11 17.10 5.10 -8 -4 -11 14.50 4.50 -8 -4 -11 4.70 7.30 8 -4 11 10.50 4.50 -8 4 -12 6.70 4.40 -8 -4 -12 4.20 6.40 -8 -4 -12 1.50 3.70 8 -4 12 -1.00 3.40 -8 -4 -12 5.00 4.10 -8 4 -13 1.90 3.90 -8 4 -13 5.40 3.80 -8 -4 -13 0.10 4.10 -8 -4 -13 -0.50 3.80 8 -4 13 6.80 4.10 -8 -4 -13 9.50 7.30 -8 4 -14 13.90 5.20 -8 4 -14 13.90 4.60 -8 -4 -14 26.10 8.90 -8 -4 -14 6.10 4.20 -8 -4 -14 19.80 5.70 8 -4 14 10.00 4.60 8 5 -14 56.69 6.80 8 -5 -14 52.89 11.40 8 -5 -14 64.49 7.70 8 5 -13 6.80 3.60 8 -5 -13 5.70 6.00 8 -5 -13 1.10 3.60 8 5 -12 6.30 3.40 8 -5 -12 2.70 6.00 8 5 -11 35.40 5.10 8 -5 -11 20.80 7.60 8 5 -10 29.40 6.10 8 5 -10 30.50 3.60 8 5 -10 29.20 4.70 8 -5 -10 35.80 9.00 8 5 -9 11.90 3.90 8 5 -9 11.60 2.70 -8 5 9 11.20 3.20 8 5 -9 8.10 3.30 8 -5 -9 11.50 6.70 8 5 -8 4.70 3.70 -8 5 8 1.70 2.40 8 5 -8 5.30 2.50 8 -5 -8 4.30 5.60 8 5 -7 20.20 3.40 8 5 -7 18.10 4.70 -8 5 7 26.80 3.90 8 -5 -7 23.20 3.40 8 -5 -7 28.10 7.40 8 5 -6 24.70 5.00 8 5 -6 26.10 3.70 -8 5 6 33.80 4.20 8 -5 -6 27.10 3.70 8 -5 -6 27.90 7.50 8 5 -5 16.20 4.50 -8 5 5 14.70 3.40 8 5 -5 12.30 3.10 8 -5 -5 11.70 3.10 8 -5 -5 18.80 6.60 8 5 -4 21.20 4.70 -8 5 4 20.60 3.70 8 5 -4 18.30 3.40 8 -5 -4 27.10 4.00 -8 -5 4 22.10 4.70 8 -5 -4 22.70 6.30 -8 5 3 49.90 5.10 8 5 -3 55.59 6.00 8 5 -3 46.70 5.00 8 -5 -3 53.89 5.40 8 -5 -3 56.29 8.50 -8 -5 3 52.79 6.60 8 5 -2 26.60 4.60 -8 5 2 26.10 4.10 8 5 -2 31.30 4.20 8 -5 -2 32.60 4.50 -8 -5 2 29.50 6.10 8 -5 -2 39.40 7.10 8 5 -1 14.10 3.40 -8 5 1 17.60 3.70 8 5 -1 21.40 4.70 -8 -5 1 25.00 4.00 8 -5 -1 21.30 5.50 -8 -5 1 20.40 5.90 8 -5 -1 14.80 3.80 8 5 0 140.49 7.50 -8 5 0 137.69 7.70 -8 -5 0 122.79 7.70 8 -5 0 140.29 9.80 -8 -5 0 126.39 10.50 -8 5 -1 70.99 6.40 8 5 1 72.29 6.40 -8 -5 -1 76.09 9.50 -8 -5 -1 71.19 6.60 8 -5 1 86.19 8.30 -8 5 -2 -0.50 2.80 8 5 2 3.60 2.80 -8 -5 -2 1.80 3.20 -8 -5 -2 5.40 5.80 8 -5 2 3.90 3.70 8 5 3 18.00 4.00 -8 5 -3 14.50 3.90 -8 5 -3 17.90 2.90 -8 -5 -3 14.00 4.30 -8 -5 -3 20.40 7.00 8 -5 3 15.20 4.50 -8 5 -4 184.38 7.00 8 5 4 176.78 8.60 -8 5 -4 171.48 9.10 -8 -5 -4 169.38 9.50 -8 -5 -4 168.68 13.40 8 -5 4 173.98 10.30 -8 5 -5 40.30 3.80 8 5 5 39.50 4.90 -8 5 -5 36.40 5.40 -8 -5 -5 40.20 8.70 -8 -5 -5 37.80 5.40 -8 5 -6 3.40 2.10 -8 5 -6 3.00 3.10 -8 -5 -6 5.80 6.50 -8 -5 -6 -1.10 2.90 -8 -5 -6 5.80 3.80 -8 5 -7 19.70 3.10 -8 5 -7 21.30 4.60 -8 -5 -7 17.00 4.60 -8 -5 -7 21.10 8.40 -8 -5 -7 25.00 5.00 -8 5 -8 136.59 9.10 -8 5 -8 144.09 9.20 -8 -5 -8 150.78 13.40 -8 -5 -8 137.89 9.10 -8 -5 -8 124.99 9.00 -8 5 -9 1.30 3.20 -8 5 -9 3.80 3.60 -8 -5 -9 6.60 4.00 -8 -5 -9 -2.50 3.30 -8 -5 -9 5.70 6.90 -8 5 -10 1.60 3.40 -8 5 -10 3.30 3.60 -8 -5 -10 0.70 3.90 -8 -5 -10 5.30 6.60 -8 -5 -10 0.00 3.40 -8 5 -11 3.40 3.70 -8 5 -11 11.70 4.60 -8 -5 -11 3.70 4.00 -8 -5 -11 5.60 4.10 8 -5 11 6.40 4.30 -8 -5 -11 12.70 7.80 -8 5 -12 36.10 6.50 -8 5 -12 44.50 6.80 -8 -5 -12 39.90 6.50 -8 -5 -12 48.90 7.40 -8 -5 -12 51.59 10.40 8 -5 12 30.80 6.40 -8 5 -13 1.70 3.90 -8 5 -13 2.40 4.00 -8 -5 -13 2.30 4.20 8 -5 13 1.80 4.20 -8 -5 -13 8.00 4.50 -8 -5 -13 8.70 6.50 8 6 -12 2.90 3.50 8 -6 -12 4.50 6.80 8 6 -11 4.20 4.10 8 6 -11 1.80 3.30 8 -6 -11 3.50 6.60 8 6 -10 8.10 3.60 8 6 -10 5.20 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3.30 10 2 8 2.60 2.60 10 -2 8 1.40 1.60 10 -2 8 3.70 2.80 -10 -2 -8 0.80 2.80 -10 -2 -8 5.20 3.30 -10 2 -9 3.70 3.30 10 2 9 10.50 3.10 -10 2 -9 5.80 3.40 -10 -2 -9 2.00 3.40 10 -2 9 4.50 3.20 -10 -2 -9 7.50 3.40 -10 2 -10 -1.30 3.00 10 2 10 0.80 2.50 -10 2 -10 2.10 3.40 10 -2 10 3.70 3.30 -10 -2 -10 5.50 3.30 -10 -2 -10 0.20 7.70 -10 -2 -10 1.80 3.10 -10 2 -11 60.09 6.60 -10 2 -11 50.19 6.40 10 -2 11 49.10 5.90 -10 -2 -11 64.89 7.30 -10 -2 -11 46.40 6.10 -10 -2 -11 45.60 10.70 -10 2 -12 22.40 5.10 -10 2 -12 22.80 5.00 -10 -2 -12 15.20 9.20 10 -2 12 32.60 5.10 -10 -2 -12 21.90 5.20 -10 -2 -12 26.60 5.40 -10 2 -13 16.10 4.70 -10 2 -13 16.50 5.20 10 -2 13 11.90 4.00 -10 -2 -13 12.50 4.70 -10 -2 -13 11.40 4.40 -10 -2 -13 13.30 9.30 -10 2 -14 -0.90 3.30 -10 2 -14 3.30 3.40 10 -2 14 0.50 2.90 -10 -2 -14 4.00 8.30 -10 -2 -14 5.20 4.00 -10 -2 -14 4.90 4.30 -10 2 -15 9.90 4.50 -10 2 -15 2.70 4.30 -10 -2 -15 0.50 4.40 10 -2 15 11.30 4.70 -10 -2 -15 6.00 4.50 10 3 -15 12.90 3.70 10 -3 -15 8.20 6.70 10 -3 -15 7.80 3.90 10 3 -14 36.00 5.00 10 -3 -14 39.50 8.90 10 -3 -14 33.70 5.30 10 3 -13 6.00 3.00 10 -3 -13 13.60 6.30 10 -3 -13 4.30 3.40 10 3 -12 1.70 2.70 10 -3 -12 3.00 5.40 10 -3 -12 0.50 2.70 10 3 -11 9.90 3.00 10 -3 -11 13.60 6.50 10 -3 -11 12.90 3.60 10 3 -10 100.89 6.10 10 -3 -10 112.39 11.50 10 -3 -10 109.69 6.70 10 3 -9 12.80 2.80 10 -3 -9 6.50 5.10 10 -3 -9 6.10 2.60 10 3 -8 9.20 3.50 10 3 -8 8.80 2.40 -10 3 8 8.70 2.10 10 -3 -8 8.00 5.60 10 -3 -8 8.00 2.40 -10 3 7 0.30 1.60 10 3 -7 5.00 3.30 10 3 -7 3.60 1.80 10 3 -7 2.90 3.40 10 -3 -7 2.80 4.70 10 -3 -7 4.40 2.20 -10 3 6 65.19 3.90 10 3 -6 72.29 6.30 10 3 -6 57.49 3.80 10 3 -6 58.79 2.60 10 3 -6 60.69 2.70 10 3 -6 50.89 5.60 10 -3 -6 62.79 8.80 10 -3 -6 59.19 4.90 10 3 -5 39.90 2.80 10 3 -5 36.40 2.80 10 3 -5 41.50 5.10 -10 3 5 46.40 3.60 10 3 -5 51.29 5.50 10 -3 -5 49.10 4.60 10 -3 -5 34.70 6.50 -10 -3 5 48.40 4.40 10 3 -4 2.00 1.40 10 3 -4 -2.60 2.60 10 3 -4 -0.60 2.70 10 3 -4 -0.80 1.40 -10 3 4 0.30 1.70 10 -3 -4 0.60 2.20 -10 -3 4 -1.60 1.90 10 -3 -4 -3.80 3.60 10 3 -3 -0.10 2.50 10 3 -3 -0.50 1.50 10 3 -3 3.10 2.60 -10 3 3 0.70 1.80 10 3 -3 -0.70 1.30 -10 -3 3 -2.20 1.80 10 -3 -3 1.90 4.10 10 -3 -3 -1.70 2.00 10 3 -2 14.40 3.30 10 3 -2 19.30 3.80 -10 3 2 11.80 2.50 10 3 -2 14.70 2.50 10 3 -2 17.50 2.60 -10 -3 2 15.00 3.00 10 -3 -2 14.70 3.20 10 -3 -2 15.00 4.70 10 3 -1 10.20 2.40 -10 3 1 9.50 2.60 10 3 -1 6.90 2.60 10 3 -1 8.60 2.90 10 -3 -1 10.90 1.90 10 -3 -1 10.40 4.70 10 -3 -1 11.90 3.10 -10 -3 1 4.40 2.50 10 3 0 -0.50 2.20 -10 3 0 -3.40 1.90 10 3 0 6.10 3.00 10 -3 0 1.90 3.70 -10 -3 0 0.90 2.30 10 -3 0 4.60 2.90 10 -3 0 1.90 1.50 -10 3 -1 5.20 2.50 10 3 1 6.80 2.90 10 3 1 3.60 2.80 10 -3 1 3.70 2.90 10 -3 1 7.00 4.10 -10 -3 -1 8.80 2.90 -10 3 -2 16.50 3.40 10 3 2 11.00 3.10 -10 3 -2 15.20 1.30 10 -3 2 12.80 3.50 10 -3 2 11.30 4.50 -10 -3 -2 12.30 2.40 -10 -3 -2 14.60 3.20 10 3 3 170.38 7.90 -10 3 -3 164.48 7.90 10 -3 3 165.38 8.30 -10 -3 -3 154.98 6.80 -10 -3 -3 153.48 8.00 10 3 4 2.90 2.50 -10 3 -4 8.60 3.20 -10 -3 -4 4.20 2.40 -10 -3 -4 10.90 3.50 10 -3 4 4.00 3.10 10 3 5 3.60 2.70 -10 3 -5 7.20 3.10 -10 3 -5 3.40 2.70 -10 -3 -5 -0.40 2.20 10 -3 5 0.30 2.90 -10 -3 -5 5.10 3.40 10 3 6 -0.40 2.30 -10 3 -6 0.50 2.70 -10 3 -6 -4.40 2.40 -10 -3 -6 0.40 2.30 10 -3 6 1.20 3.10 -10 -3 -6 -2.20 2.70 -10 3 -7 25.60 4.40 -10 3 -7 15.50 4.00 10 3 7 16.10 3.40 10 -3 7 12.30 3.80 -10 -3 -7 14.10 4.20 -10 -3 -7 12.90 3.40 -10 3 -8 7.40 3.70 -10 3 -8 1.60 3.10 10 3 8 3.80 2.70 -10 -3 -8 6.40 3.20 10 -3 8 3.30 3.30 -10 -3 -8 5.40 7.80 -10 -3 -8 3.80 3.70 -10 3 -9 5.50 3.70 -10 3 -9 6.90 3.50 10 3 9 7.00 2.80 -10 -3 -9 9.00 8.20 10 -3 9 -1.80 3.00 -10 -3 -9 7.10 3.70 -10 -3 -9 7.80 3.80 -10 3 -10 4.70 3.60 -10 3 -10 12.60 3.20 10 -3 10 4.00 3.50 -10 -3 -10 4.20 3.80 -10 -3 -10 2.30 7.80 -10 -3 -10 10.10 4.00 -10 3 -11 -2.30 3.00 -10 3 -11 -0.60 3.10 -10 -3 -11 0.70 3.50 -10 -3 -11 3.10 4.00 -10 -3 -11 -8.40 7.00 10 -3 11 1.30 3.40 -10 3 -12 -4.40 3.10 -10 3 -12 -1.10 3.10 -10 -3 -12 -0.40 3.60 10 -3 12 1.20 3.40 -10 -3 -12 3.80 7.20 -10 -3 -12 -1.00 3.50 -10 3 -13 1.50 3.70 -10 3 -13 4.40 3.70 -10 -3 -13 1.90 3.80 -10 -3 -13 1.30 4.20 -10 -3 -13 0.30 7.70 10 -3 13 3.40 3.90 -10 3 -14 7.00 4.20 -10 3 -14 1.60 3.60 10 -3 14 -0.80 3.40 -10 -3 -14 7.30 4.40 -10 -3 -14 2.10 4.20 -10 -3 -14 31.80 8.90 10 4 -14 3.90 3.30 10 -4 -14 11.10 5.70 10 -4 -14 3.60 3.50 10 4 -13 19.80 4.20 10 -4 -13 20.70 7.40 10 -4 -13 15.00 4.40 10 4 -12 34.10 4.70 10 -4 -12 39.60 5.50 10 -4 -12 44.90 9.70 10 4 -11 -0.70 2.40 10 -4 -11 14.50 5.60 10 4 -10 0.40 2.40 10 -4 -10 9.40 4.70 10 4 -9 23.60 5.40 10 4 -9 28.20 3.90 10 -4 -9 34.90 8.50 10 4 -8 42.30 2.90 10 4 -8 39.60 5.70 -10 4 8 47.20 4.30 10 4 -8 42.70 4.50 10 -4 -8 48.70 4.40 10 -4 -8 45.80 8.90 10 4 -7 1.60 1.60 10 4 -7 1.30 3.20 -10 4 7 -2.20 1.90 10 4 -7 0.60 2.10 10 -4 -7 -1.90 2.00 10 -4 -7 -3.30 4.60 10 4 -6 -0.80 1.60 -10 4 6 -2.40 1.90 10 4 -6 0.70 2.70 10 -4 -6 1.10 4.70 10 -4 -6 2.60 2.50 10 4 -5 10.70 2.40 10 4 -5 11.10 4.00 10 4 -5 9.40 2.40 -10 4 5 11.10 2.80 10 4 -5 12.20 4.00 10 -4 -5 7.80 2.80 10 -4 -5 3.60 5.00 10 4 -4 23.30 4.70 10 4 -4 24.10 4.80 10 4 -4 19.30 2.90 -10 4 4 16.00 3.10 -10 -4 4 22.20 3.70 10 -4 -4 22.40 6.60 10 -4 -4 21.20 3.70 -10 4 3 17.70 3.20 10 4 -3 14.10 3.60 10 4 -3 13.50 2.70 10 4 -3 18.20 4.00 -10 -4 3 16.90 3.50 10 -4 -3 12.90 5.30 10 -4 -3 11.80 3.30 10 4 -2 51.29 4.50 -10 4 2 34.10 4.20 10 4 -2 41.60 5.30 10 4 -2 46.80 5.60 10 -4 -2 37.40 6.80 10 -4 -2 39.60 4.70 -10 -4 2 41.70 4.80 10 4 -1 13.00 3.50 10 4 -1 13.80 3.70 10 4 -1 18.50 3.30 -10 4 1 15.00 3.20 10 -4 -1 19.40 3.80 10 -4 -1 12.00 5.00 -10 -4 1 20.60 3.90 -10 4 0 32.30 4.20 10 4 0 31.30 4.20 10 4 0 26.50 4.40 10 4 0 25.10 4.20 10 -4 0 26.50 4.30 10 -4 0 21.20 5.40 -10 -4 0 23.40 3.90 -10 4 -1 22.00 3.80 10 4 1 33.30 4.80 10 -4 1 28.80 4.80 -10 -4 -1 23.30 4.20 10 -4 1 23.20 5.40 -10 4 -2 100.19 4.30 10 4 2 117.49 7.20 -10 4 -2 117.39 7.00 10 -4 2 99.79 7.00 -10 -4 -2 119.39 7.50 10 -4 2 111.89 8.90 -10 4 -3 0.10 2.70 -10 4 -3 2.00 1.30 10 4 3 3.20 2.80 10 -4 3 -1.50 3.40 10 -4 3 1.30 3.30 -10 -4 -3 -1.10 2.80 10 4 4 60.49 5.60 -10 4 -4 72.59 6.60 -10 4 -4 75.09 3.30 -10 -4 -4 75.59 7.00 10 -4 4 66.19 6.60 -10 -4 -4 77.99 5.80 -10 4 -5 3.80 3.10 10 4 5 3.00 2.80 10 -4 5 2.10 3.60 -10 -4 -5 2.50 6.80 -10 -4 -5 5.90 3.80 -10 -4 -5 4.30 2.90 10 4 6 37.20 4.50 -10 4 -6 34.70 5.10 -10 4 -6 34.20 5.10 -10 -4 -6 39.00 5.70 10 -4 6 36.20 5.80 -10 -4 -6 45.30 5.40 -10 -4 -6 37.70 9.40 10 4 7 65.89 5.80 -10 4 -7 68.69 6.70 -10 4 -7 53.69 6.30 -10 -4 -7 65.89 7.00 -10 -4 -7 56.99 6.30 -10 -4 -7 87.39 12.40 10 -4 7 56.99 6.60 -10 4 -8 -0.30 2.90 10 4 8 8.40 2.90 -10 4 -8 0.20 3.20 -10 -4 -8 6.90 4.00 10 -4 8 9.30 4.20 -10 -4 -8 4.60 3.30 -10 -4 -8 9.00 7.80 10 4 9 3.30 2.80 -10 4 -9 1.90 3.40 -10 4 -9 5.50 3.80 10 -4 9 6.30 4.00 -10 -4 -9 1.10 7.40 -10 -4 -9 4.30 3.70 -10 -4 -9 6.00 3.80 -10 4 -10 25.50 5.10 -10 4 -10 35.10 5.60 -10 -4 -10 46.80 10.80 10 -4 10 38.60 6.00 -10 -4 -10 37.80 6.10 -10 -4 -10 32.20 5.70 -10 4 -11 64.79 7.60 -10 4 -11 70.49 8.10 -10 -4 -11 71.69 7.80 -10 -4 -11 52.09 6.70 10 -4 11 55.29 7.30 -10 -4 -11 52.09 10.50 -10 4 -12 6.10 4.20 -10 4 -12 2.40 3.80 10 -4 12 -2.20 3.40 -10 -4 -12 3.80 4.10 -10 -4 -12 12.60 7.20 -10 -4 -12 6.80 4.30 -10 4 -13 0.00 3.50 -10 4 -13 2.40 3.60 -10 -4 -13 -0.90 3.80 10 -4 13 -3.60 3.40 -10 -4 -13 -0.20 3.90 -10 -4 -13 1.90 6.90 10 5 -13 19.10 4.30 10 -5 -13 22.70 9.00 10 5 -12 -2.10 2.70 10 -5 -12 4.10 6.50 10 5 -11 13.40 3.60 10 -5 -11 20.80 7.40 10 5 -10 -0.50 2.50 10 5 -10 -0.50 3.50 10 -5 -10 11.40 4.70 10 5 -9 53.79 7.20 10 5 -9 44.80 5.10 10 -5 -9 54.99 10.10 -10 5 8 2.70 2.80 10 5 -8 8.00 4.10 10 5 -8 4.00 2.10 10 5 -8 1.00 2.50 10 -5 -8 -1.80 5.20 10 5 -7 51.59 4.40 10 5 -7 49.40 6.60 -10 5 7 55.09 5.20 10 -5 -7 52.49 9.20 10 -5 -7 56.89 5.40 -10 5 6 11.60 3.10 10 5 -6 2.50 3.60 10 5 -6 3.80 2.30 10 -5 -6 9.50 3.00 10 -5 -6 7.50 5.50 10 5 -5 14.80 4.30 10 5 -5 10.00 2.80 -10 5 5 18.30 3.50 10 -5 -5 14.90 3.50 10 -5 -5 18.20 6.20 -10 5 4 1.70 2.50 10 5 -4 5.00 3.50 10 5 -4 -0.60 2.20 10 -5 -4 0.80 4.70 10 -5 -4 2.50 2.80 -10 5 3 26.50 4.20 10 5 -3 24.30 3.70 10 5 -3 20.40 4.70 10 -5 -3 26.20 4.40 10 -5 -3 36.30 7.60 10 5 -2 100.79 6.50 10 5 -2 111.99 8.10 -10 5 2 106.19 6.80 10 -5 -2 101.49 7.10 10 -5 -2 102.19 9.90 -10 -5 2 101.09 7.20 -10 5 1 10.40 3.40 10 5 -1 7.30 3.10 10 5 -1 4.70 3.80 10 5 -1 8.20 3.80 10 -5 -1 10.10 3.80 10 -5 -1 5.00 4.90 -10 -5 1 2.50 3.10 10 5 0 7.50 3.50 10 5 0 6.60 3.00 10 5 0 11.40 4.20 -10 5 0 4.40 3.10 10 -5 0 0.00 3.20 -10 -5 0 -3.60 5.80 10 -5 0 5.90 4.70 -10 -5 0 3.10 3.30 10 5 1 9.00 3.40 -10 5 -1 7.80 3.40 10 5 1 3.10 3.40 10 -5 1 5.10 3.40 -10 -5 -1 0.50 3.30 -10 -5 -1 5.80 6.60 10 -5 1 2.10 4.30 10 5 2 43.60 5.40 -10 5 -2 46.20 5.70 10 5 2 47.40 5.40 -10 5 -2 41.80 3.90 -10 -5 -2 53.29 6.30 10 -5 2 56.19 7.80 10 -5 2 41.10 5.50 -10 -5 -2 37.60 8.60 10 5 3 1.40 3.00 -10 5 -3 4.00 3.20 -10 5 -3 2.50 1.70 10 -5 3 -2.60 3.30 10 -5 3 -0.90 3.70 -10 -5 -3 8.20 3.80 -10 -5 -3 -1.80 6.60 10 5 4 6.40 3.40 -10 5 -4 2.30 3.20 -10 5 -4 3.40 2.00 -10 -5 -4 -2.30 6.80 -10 -5 -4 -2.90 3.20 10 -5 4 3.20 4.00 10 5 5 1.50 2.90 -10 5 -5 -0.10 2.80 10 -5 5 -0.20 3.50 -10 -5 -5 0.20 3.40 -10 -5 -5 -6.70 6.30 10 5 6 5.90 3.40 -10 5 -6 7.60 3.70 10 -5 6 2.10 4.40 -10 -5 -6 9.10 3.60 -10 -5 -6 7.80 4.10 -10 -5 -6 -0.80 6.70 -10 5 -7 7.60 3.80 10 5 7 10.20 3.50 -10 5 -7 11.60 4.00 10 -5 7 6.30 4.10 -10 -5 -7 15.60 4.70 -10 -5 -7 11.60 3.90 -10 -5 -7 10.40 7.60 10 5 8 0.60 2.90 -10 5 -8 -1.60 3.00 -10 5 -8 6.10 3.70 -10 -5 -8 5.80 3.70 10 -5 8 -3.20 4.10 -10 -5 -8 5.20 4.10 -10 -5 -8 -6.50 6.40 -10 5 -9 7.70 3.80 -10 5 -9 0.00 3.50 -10 -5 -9 5.90 4.10 -10 -5 -9 5.20 6.90 10 -5 9 6.10 4.80 -10 -5 -9 4.30 3.70 -10 5 -10 3.20 3.90 -10 5 -10 -2.20 3.40 -10 -5 -10 14.80 5.80 -10 -5 -10 -0.70 3.50 -10 -5 -10 2.60 3.80 10 -5 10 2.20 4.10 -10 5 -11 7.80 4.30 -10 5 -11 7.10 4.20 -10 -5 -11 1.90 4.10 10 -5 11 11.10 4.90 -10 -5 -11 8.20 7.30 -10 -5 -11 12.20 4.80 -10 5 -12 21.20 5.30 -10 5 -12 18.70 5.50 10 -5 12 26.80 6.60 -10 -5 -12 23.50 6.10 -10 -5 -12 28.50 6.00 -10 -5 -12 25.10 8.80 10 6 -11 11.90 3.70 10 6 -11 13.00 5.10 10 -6 -11 21.00 6.10 10 6 -10 5.90 4.40 10 6 -10 3.20 3.00 10 -6 -10 12.20 5.20 10 6 -9 3.40 3.00 10 6 -9 3.40 3.90 10 -6 -9 3.10 6.50 10 6 -8 10.10 3.00 10 6 -8 9.50 4.40 10 -6 -8 3.10 6.00 10 6 -7 78.19 5.80 10 6 -7 83.49 8.90 -10 6 7 67.59 6.40 10 -6 -7 61.79 8.70 10 -6 -7 91.39 12.70 10 6 -6 -0.30 2.30 -10 6 6 1.00 2.80 10 6 -6 3.20 3.70 10 -6 -6 2.20 2.80 10 -6 -6 -2.70 4.90 10 6 -5 5.10 4.10 10 6 -5 4.40 2.70 -10 6 5 1.10 3.00 10 -6 -5 2.20 3.00 10 -6 -5 10.00 5.80 -10 6 4 6.90 3.30 10 6 -4 -0.80 3.30 10 6 -4 1.60 2.60 10 -6 -4 2.00 4.70 10 -6 -4 0.20 2.90 10 6 -3 109.29 8.70 10 6 -3 96.69 6.90 -10 6 3 102.89 7.40 -10 -6 3 111.09 9.60 10 -6 -3 89.79 10.90 10 -6 -3 99.09 7.30 10 6 -2 11.80 4.20 -10 6 2 7.10 3.50 10 6 -2 5.60 3.10 -10 -6 2 6.30 4.90 10 -6 -2 1.00 4.80 10 -6 -2 -1.60 3.30 10 6 -1 1.70 3.60 10 6 -1 3.50 2.80 -10 6 1 4.00 3.20 -10 -6 1 -2.50 4.70 10 -6 -1 1.20 4.40 10 -6 -1 1.20 3.40 -10 6 0 -0.70 2.90 10 6 0 3.40 3.10 10 6 0 0.10 3.70 10 -6 0 4.50 4.80 -10 -6 0 4.40 5.70 10 -6 0 0.00 3.50 -10 -6 0 -1.50 3.20 10 6 1 60.39 6.60 -10 6 -1 53.69 6.30 -10 -6 -1 65.49 9.60 10 -6 1 60.79 7.10 -10 -6 -1 46.50 6.00 10 -6 1 65.39 9.20 10 6 2 10.90 3.70 -10 6 -2 4.50 2.70 -10 6 -2 6.10 3.60 10 -6 2 4.90 3.90 -10 -6 -2 7.30 4.00 -10 -6 -2 10.90 6.50 10 -6 2 2.90 4.50 -10 6 -3 11.00 4.00 10 6 3 14.30 4.20 -10 -6 -3 12.60 4.30 10 -6 3 11.60 4.60 10 -6 3 3.50 4.60 -10 -6 -3 10.90 6.60 -10 6 -4 1.50 3.20 -10 -6 -4 0.80 6.30 10 -6 4 0.80 3.80 -10 -6 -4 7.40 4.00 10 -6 4 5.00 4.40 -10 6 -5 5.50 3.80 10 -6 5 9.10 5.10 -10 -6 -5 12.10 4.70 -10 -6 -5 10.10 7.10 -10 6 -6 0.10 3.40 10 -6 6 -1.70 4.10 -10 -6 -6 -0.90 3.80 -10 -6 -6 11.00 5.70 -10 6 -7 15.50 4.80 -10 -6 -7 22.70 8.30 10 -6 7 7.90 5.10 -10 -6 -7 13.70 4.90 -10 6 -8 -2.20 3.40 -10 6 -8 -0.20 3.40 -10 -6 -8 3.40 4.10 -10 -6 -8 2.60 6.50 10 -6 8 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38.70 11.10 -11 -3 -11 39.80 6.20 -11 -3 -11 13.00 4.70 -11 3 -12 1.00 3.50 -11 3 -12 -5.90 2.50 -11 -3 -12 -5.80 7.10 -11 -3 -12 -2.50 3.50 11 -3 12 4.00 3.50 -11 -3 -12 -0.60 3.50 -11 3 -13 23.60 5.30 -11 3 -13 29.80 5.90 -11 -3 -13 34.20 10.40 -11 -3 -13 29.50 6.10 11 -3 13 28.00 5.50 -11 -3 -13 31.70 6.00 -11 3 -14 1.50 3.50 -11 3 -14 2.70 3.90 11 -3 14 7.30 4.20 -11 -3 -14 4.20 4.30 -11 -3 -14 6.70 4.20 -11 -3 -14 2.20 7.70 11 -4 -14 31.90 5.50 11 -4 -14 12.60 7.30 11 4 -13 2.80 2.90 11 -4 -13 -1.60 5.10 11 -4 -13 -4.40 2.70 11 4 -12 0.50 2.70 11 -4 -12 -5.90 5.20 11 4 -11 0.40 2.40 11 -4 -11 -4.00 4.80 11 4 -10 -0.40 2.30 11 -4 -10 2.60 5.70 11 4 -9 8.70 2.70 11 4 -9 4.80 3.80 11 -4 -9 5.40 5.60 11 4 -8 38.70 6.20 11 4 -8 38.80 4.20 11 -4 -8 34.10 4.00 11 -4 -8 42.90 8.80 11 4 -7 9.40 3.80 11 4 -7 8.20 1.70 -11 4 7 9.00 2.60 11 4 -7 4.50 2.30 11 -4 -7 11.50 5.30 11 -4 -7 5.40 2.60 11 4 -6 18.10 2.40 11 4 -6 14.80 4.40 11 4 -6 18.10 4.70 -11 4 6 13.70 2.90 11 -4 -6 20.90 6.80 11 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3.20 11 -4 2 0.90 3.90 -11 4 -3 86.69 7.30 11 4 3 62.79 6.10 -11 4 -3 66.19 2.80 11 -4 3 72.19 7.00 -11 -4 -3 70.29 6.90 11 4 4 3.50 2.90 -11 4 -4 6.70 3.20 11 -4 4 3.30 3.30 -11 -4 -4 5.80 3.50 -11 -4 -4 8.40 3.10 11 4 5 14.60 3.60 -11 4 -5 26.30 4.80 -11 -4 -5 17.20 4.40 -11 -4 -5 20.50 4.10 11 -4 5 11.40 4.60 11 4 6 10.40 3.40 -11 4 -6 14.70 4.10 -11 4 -6 9.60 3.60 -11 -4 -6 15.70 3.90 -11 -4 -6 8.10 3.70 11 -4 6 11.70 4.40 -11 -4 -6 11.40 8.20 -11 4 -7 -0.70 2.70 11 4 7 0.40 2.60 -11 4 -7 -2.40 3.00 -11 -4 -7 -1.40 2.80 -11 -4 -7 -0.10 3.30 11 -4 7 -0.90 3.60 -11 -4 -7 -6.40 6.90 -11 4 -8 -0.70 3.00 11 4 8 2.00 2.70 -11 4 -8 3.10 3.40 -11 -4 -8 3.10 3.80 11 -4 8 -1.60 3.40 -11 -4 -8 1.60 8.50 -11 -4 -8 3.50 3.40 -11 4 -9 8.00 4.00 11 4 9 9.40 3.20 -11 4 -9 7.40 3.90 -11 -4 -9 11.80 4.10 -11 -4 -9 12.20 4.50 -11 -4 -9 11.40 8.50 11 -4 9 13.90 4.80 -11 4 -10 0.00 3.40 -11 4 -10 6.30 3.80 -11 -4 -10 -1.00 3.60 11 -4 10 6.40 4.00 -11 -4 -10 3.40 7.80 -11 -4 -10 4.50 3.50 -11 4 -11 5.00 4.00 -11 4 -11 -4.20 3.10 11 -4 11 -4.20 3.50 -11 -4 -11 4.00 7.60 -11 -4 -11 2.10 3.50 -11 -4 -11 3.40 3.90 -11 4 -12 51.79 7.20 -11 4 -12 50.29 6.90 -11 -4 -12 67.49 12.60 -11 -4 -12 52.59 7.30 -11 -4 -12 69.89 8.30 11 -4 12 54.69 7.70 -11 4 -13 6.00 4.40 -11 4 -13 7.20 4.30 -11 -4 -13 30.60 7.40 11 -4 13 2.90 4.10 -11 -4 -13 5.90 4.50 -11 -4 -13 3.70 4.50 11 5 -12 -0.70 2.70 11 -5 -12 -1.10 5.90 11 5 -11 1.00 2.80 11 -5 -11 -0.20 5.60 11 5 -10 8.10 4.20 11 5 -10 5.10 2.90 11 -5 -10 -6.90 5.30 11 5 -9 -0.20 2.20 11 5 -9 4.10 4.10 11 -5 -9 -3.70 4.90 11 5 -8 3.20 2.50 11 5 -8 -1.20 3.60 11 -5 -8 -3.20 5.10 11 5 -7 5.40 2.10 11 5 -7 4.40 3.70 -11 5 7 4.30 2.80 11 -5 -7 4.60 6.00 11 -5 -7 6.20 2.90 11 5 -6 0.80 3.50 -11 5 6 -1.10 2.30 11 5 -6 1.70 2.10 11 -5 -6 2.70 5.20 11 -5 -6 3.50 2.70 11 5 -5 12.90 4.30 11 5 -5 12.60 2.90 -11 5 5 10.90 3.20 11 -5 -5 8.30 3.00 11 -5 -5 10.50 6.00 -11 5 4 82.09 6.00 11 5 -4 88.39 8.20 11 5 -4 75.49 5.50 11 -5 -4 85.69 10.70 11 -5 -4 71.49 6.40 -11 5 3 27.50 4.20 11 5 -3 34.40 5.70 11 5 -3 26.40 3.90 11 -5 -3 29.10 6.80 11 -5 -3 28.30 4.70 -11 -5 3 24.80 4.40 11 5 -2 -0.30 3.30 11 5 -2 -0.50 2.40 11 5 -2 2.10 3.60 -11 5 2 7.90 3.10 11 -5 -2 -1.30 4.00 11 -5 -2 7.20 3.30 -11 -5 2 4.20 3.30 11 5 -1 1.30 3.40 11 5 -1 3.60 2.70 -11 5 1 1.90 2.90 11 5 -1 0.50 3.00 11 -5 -1 4.20 3.30 11 -5 -1 1.60 4.70 -11 -5 1 8.50 3.70 11 5 0 2.40 3.30 -11 5 0 2.40 3.00 11 5 0 -3.90 3.20 11 5 0 -1.40 2.40 11 -5 0 0.50 3.00 -11 -5 0 -1.20 3.20 11 -5 0 -4.10 3.80 11 5 1 85.59 6.70 -11 5 -1 83.49 6.70 11 5 1 69.89 6.80 11 5 1 86.59 8.00 -11 -5 -1 95.89 7.60 11 -5 1 92.49 10.60 11 -5 1 69.89 7.00 -11 5 -2 130.09 5.60 11 5 2 142.39 8.50 -11 5 -2 123.99 8.20 11 5 2 143.59 8.20 -11 -5 -2 113.09 8.40 -11 -5 -2 114.09 12.70 11 -5 2 147.79 10.70 11 -5 2 129.49 8.80 -11 5 -3 6.80 3.50 11 5 3 4.70 3.40 11 -5 3 12.40 4.40 -11 -5 -3 3.30 3.60 11 -5 3 1.90 4.10 -11 -5 -3 8.50 7.40 11 5 4 53.39 5.90 -11 5 -4 48.10 5.90 -11 -5 -4 70.69 7.50 11 -5 4 57.09 7.20 -11 -5 -4 67.09 11.00 -11 5 -5 4.50 3.50 11 5 5 8.40 3.50 11 -5 5 11.60 4.40 -11 -5 -5 2.40 3.70 -11 -5 -5 8.30 7.90 -11 5 -6 6.80 3.60 11 5 6 7.90 3.40 -11 -5 -6 9.30 3.70 -11 -5 -6 2.90 3.80 11 -5 6 8.90 4.70 -11 -5 -6 8.20 7.80 -11 5 -7 5.80 3.50 11 5 7 0.30 2.90 -11 5 -7 -0.60 3.20 -11 -5 -7 6.20 3.60 -11 -5 -7 3.50 4.00 11 -5 7 9.90 4.70 -11 -5 -7 4.70 7.60 11 5 8 12.00 3.60 -11 5 -8 13.20 4.50 -11 5 -8 14.50 4.20 11 -5 8 11.70 5.10 -11 -5 -8 18.80 8.60 -11 -5 -8 9.40 4.40 -11 -5 -8 12.40 4.30 -11 5 -9 0.50 3.50 -11 5 -9 2.70 3.70 -11 -5 -9 -0.10 3.90 -11 -5 -9 7.00 7.80 11 -5 9 1.10 4.30 -11 -5 -9 12.50 4.40 -11 5 -10 35.90 5.90 -11 5 -10 44.00 6.50 -11 -5 -10 29.50 5.80 -11 -5 -10 44.30 11.30 11 -5 10 33.70 6.60 -11 -5 -10 45.30 6.90 -11 5 -11 5.60 4.20 -11 5 -11 -3.00 3.30 11 -5 11 7.70 4.90 -11 -5 -11 0.80 3.90 -11 -5 -11 5.10 4.40 -11 -5 -11 26.50 7.80 -11 5 -12 5.40 4.20 -11 5 -12 5.50 4.20 -11 -5 -12 8.80 4.90 11 -5 12 6.40 4.80 -11 -5 -12 7.60 4.50 -11 -5 -12 27.10 8.70 11 6 -11 -0.90 2.70 11 -6 -11 -0.20 5.60 11 6 -10 11.00 5.00 11 6 -10 2.90 3.00 11 -6 -10 3.70 6.70 11 6 -9 10.80 5.00 11 6 -9 19.20 4.00 11 -6 -9 23.00 8.00 11 6 -8 -0.60 3.90 11 -6 -8 5.10 5.90 11 6 -7 9.70 2.90 11 6 -7 16.20 5.30 11 -6 -7 23.40 5.20 11 -6 -7 19.60 7.50 11 6 -6 3.30 2.50 -11 6 6 0.20 2.80 11 6 -6 -2.30 3.50 11 -6 -6 -1.40 5.00 11 -6 -6 1.60 2.80 -11 6 5 0.80 2.90 11 6 -5 15.70 4.70 11 6 -5 12.30 3.30 11 -6 -5 9.00 3.40 11 -6 -5 8.70 6.00 -11 6 4 -1.10 2.80 11 6 -4 -1.10 2.30 11 6 -4 0.90 3.60 11 -6 -4 3.30 5.40 11 -6 -4 5.50 3.30 11 6 -3 4.10 3.80 11 6 -3 3.80 2.80 -11 6 3 3.60 3.20 11 -6 -3 4.80 3.50 11 -6 -3 6.40 5.40 -11 -6 3 3.60 5.30 11 6 -2 2.90 2.70 -11 6 2 -2.10 2.70 11 6 -2 5.00 4.00 11 -6 -2 -2.50 3.00 -11 -6 2 5.60 5.50 11 -6 -2 3.70 4.80 11 6 -1 77.49 7.00 -11 6 1 58.59 6.30 11 6 -1 64.09 7.40 -11 -6 1 62.39 9.30 11 -6 -1 71.99 7.50 -11 -6 1 60.39 6.90 11 -6 -1 64.49 9.50 11 6 0 13.80 4.60 11 6 0 13.60 3.90 -11 6 0 12.10 4.10 -11 -6 0 6.90 6.30 11 -6 0 10.20 5.40 11 -6 0 8.90 4.40 -11 -6 0 11.80 4.30 11 6 1 3.70 3.10 11 6 1 1.10 4.00 -11 6 -1 -0.70 3.00 11 -6 1 -1.00 4.20 11 -6 1 -0.50 3.50 -11 -6 -1 -1.20 6.00 -11 -6 -1 3.50 3.60 -11 6 -2 1.80 3.20 11 6 2 0.10 2.80 -11 -6 -2 7.90 4.10 11 -6 2 4.90 4.20 11 -6 2 2.30 4.50 -11 -6 -2 -8.50 5.70 11 6 3 56.69 6.70 -11 6 -3 57.39 6.90 -11 -6 -3 49.50 6.60 11 -6 3 56.89 7.20 -11 -6 -3 56.59 10.20 11 -6 3 59.39 8.70 -11 6 -4 4.90 3.60 -11 -6 -4 17.30 4.90 11 -6 4 13.60 5.10 -11 -6 -4 8.80 7.00 -11 6 -5 3.90 3.70 -11 -6 -5 -4.50 6.10 11 -6 5 1.40 4.00 -11 -6 -5 -3.40 3.50 -11 6 -6 0.10 3.20 -11 -6 -6 -1.20 6.80 11 -6 6 5.30 4.60 -11 -6 -6 -0.60 3.60 -11 6 -7 36.30 5.90 -11 -6 -7 35.50 6.30 11 -6 7 40.00 7.50 -11 -6 -7 47.10 10.40 -11 6 -8 1.40 3.40 -11 6 -8 4.60 3.80 11 -6 8 4.90 4.90 -11 -6 -8 10.00 6.50 -11 -6 -8 -2.30 3.80 -11 6 -9 0.40 3.70 -11 6 -9 2.50 3.80 11 -6 9 2.80 4.80 -11 -6 -9 8.70 4.40 -11 -6 -9 7.80 7.30 -11 -6 -9 -0.50 3.60 -11 6 -10 5.70 4.20 -11 6 -10 9.00 4.60 11 -6 10 0.50 4.70 -11 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4.90 -12 4 -12 19.10 5.20 12 -4 12 16.40 5.30 -12 -4 -12 25.80 10.00 -12 -4 -12 17.40 5.30 -12 -4 -12 15.70 4.80 12 -5 -12 -2.00 5.90 12 -5 -11 7.20 6.40 12 5 -10 2.40 3.70 12 -5 -10 -2.70 5.50 12 5 -9 -2.70 3.40 12 -5 -9 -7.50 4.50 12 5 -8 -4.80 3.30 12 5 -8 2.10 2.40 12 -5 -8 1.30 5.40 12 5 -7 18.30 5.10 12 -5 -7 19.40 3.80 12 -5 -7 17.90 7.10 12 5 -6 12.80 4.40 -12 5 6 13.80 3.30 12 5 -6 15.80 2.90 12 -5 -6 18.60 3.70 12 -5 -6 22.00 7.30 12 5 -5 4.40 3.80 12 5 -5 0.80 1.90 -12 5 5 -1.20 2.40 12 -5 -5 2.00 5.00 12 -5 -5 3.70 2.80 12 5 -4 9.00 2.80 12 5 -4 9.90 4.40 -12 5 4 9.40 3.20 12 -5 -4 5.80 3.30 12 -5 -4 8.10 5.30 12 5 -3 6.00 2.70 12 5 -3 -0.40 3.10 -12 5 3 6.10 3.00 12 5 -3 4.60 3.90 12 -5 -3 0.20 4.70 -12 -5 3 4.60 3.20 12 -5 -3 7.00 3.50 12 5 -2 35.10 4.50 -12 5 2 38.90 5.00 12 5 -2 40.40 6.20 12 5 -2 31.40 5.20 -12 -5 2 36.30 5.30 12 -5 -2 31.90 7.40 12 -5 -2 34.40 5.50 12 5 -1 -0.70 2.40 -12 5 1 7.80 3.20 12 5 -1 3.20 3.20 12 5 -1 9.30 4.30 -12 -5 1 2.10 3.20 12 -5 -1 8.20 3.70 12 -5 -1 2.20 4.70 12 5 0 4.60 3.70 -12 5 0 9.00 3.50 12 5 0 13.20 3.60 12 5 0 23.10 4.80 12 -5 0 10.40 4.00 -12 -5 0 11.00 3.90 12 -5 0 13.00 5.60 12 5 1 6.50 3.90 12 5 1 4.30 3.70 12 5 1 3.70 3.00 -12 5 -1 5.60 3.20 -12 -5 -1 -2.20 3.10 12 -5 1 0.50 4.40 12 -5 1 4.00 3.50 -12 5 -2 5.30 3.50 12 5 2 4.60 3.50 12 5 2 4.70 3.20 12 -5 2 9.80 5.00 -12 -5 -2 6.10 3.80 12 -5 2 10.70 4.30 -12 5 -3 4.00 3.20 12 5 3 -2.90 3.00 -12 -5 -3 -7.50 7.00 12 -5 3 1.60 3.30 -12 -5 -3 5.20 3.80 12 5 4 -1.50 3.00 -12 5 -4 2.90 3.40 -12 -5 -4 -2.20 7.30 12 -5 4 0.50 3.70 -12 -5 -4 3.60 3.80 -12 5 -5 3.60 3.60 12 5 5 7.30 3.50 -12 -5 -5 3.90 4.00 12 -5 5 6.40 4.50 -12 -5 -5 3.80 7.90 -12 5 -6 6.50 3.60 12 5 6 5.80 3.30 -12 5 -6 1.10 3.20 -12 -5 -6 -5.10 7.00 -12 -5 -6 3.70 3.20 -12 -5 -6 6.60 4.10 12 -5 6 1.40 4.30 -12 5 -7 1.80 3.50 12 5 7 2.50 3.00 -12 5 -7 -1.60 3.20 -12 -5 -7 -1.50 7.40 -12 -5 -7 -0.10 3.10 12 -5 7 1.30 4.30 -12 -5 -7 -1.00 3.70 12 5 8 1.70 2.90 -12 5 -8 6.00 4.10 -12 5 -8 8.60 3.80 -12 -5 -8 2.10 3.70 -12 -5 -8 6.20 4.10 12 -5 8 12.60 5.20 -12 -5 -8 2.30 7.40 -12 5 -9 -1.50 3.50 -12 5 -9 5.00 3.90 -12 -5 -9 -0.80 3.70 -12 -5 -9 -1.00 3.50 -12 -5 -9 8.20 8.30 12 -5 9 -1.70 4.00 -12 5 -10 -2.20 3.40 -12 5 -10 -2.50 3.40 -12 -5 -10 0.50 3.70 -12 -5 -10 3.20 4.20 -12 -5 -10 6.30 7.60 12 -5 10 -7.60 3.60 -12 5 -11 0.50 3.80 -12 5 -11 1.90 3.70 12 -5 11 -0.60 4.30 -12 -5 -11 3.20 4.00 -12 -5 -11 0.80 4.10 -12 -5 -11 12.50 8.20 12 6 -10 3.50 4.70 12 -6 -10 0.40 6.20 12 6 -9 11.70 4.90 12 -6 -9 10.30 6.80 12 6 -8 4.00 2.80 12 6 -8 3.40 4.30 12 -6 -8 1.40 5.60 12 6 -7 1.00 4.00 12 -6 -7 3.20 5.90 12 -6 -7 4.20 3.60 12 6 -6 2.70 4.00 12 6 -6 -1.90 2.10 12 -6 -6 0.10 5.20 12 -6 -6 4.60 3.20 -12 6 5 23.00 4.30 12 6 -5 27.40 6.00 12 6 -5 28.30 4.20 12 -6 -5 26.10 4.60 12 -6 -5 18.90 6.80 12 6 -4 5.10 2.80 12 6 -4 7.10 4.40 -12 6 4 2.40 3.20 12 -6 -4 0.50 3.00 12 -6 -4 0.00 4.70 12 6 -3 1.20 2.70 -12 6 3 -1.00 2.80 12 6 -3 0.20 3.60 12 -6 -3 2.90 4.60 12 -6 -3 -2.00 3.00 -12 -6 3 -2.00 7.30 -12 6 2 1.00 2.90 12 6 -2 3.70 3.00 12 6 -2 1.40 3.30 12 -6 -2 5.90 3.60 12 -6 -2 9.20 5.80 -12 -6 2 1.20 5.90 -12 6 1 -3.00 2.80 12 6 -1 -0.40 2.80 12 6 -1 1.40 3.40 12 -6 -1 -3.50 3.20 -12 -6 1 1.10 3.70 -12 -6 1 -4.80 6.00 12 -6 -1 0.00 4.50 12 6 0 -1.10 2.90 -12 6 0 5.50 3.40 12 6 0 3.70 3.80 -12 -6 0 5.60 3.80 12 -6 0 -1.40 3.50 -12 -6 0 -5.60 6.00 12 -6 0 1.60 4.70 12 6 1 22.40 5.50 -12 6 -1 22.10 4.70 12 6 1 22.50 4.60 -12 -6 -1 28.30 8.70 -12 -6 -1 10.70 4.50 12 -6 1 13.50 4.70 12 -6 1 20.80 6.20 12 6 2 15.60 4.20 -12 6 -2 20.00 4.60 12 6 2 11.80 5.40 -12 -6 -2 19.20 5.00 12 -6 2 14.00 5.80 -12 -6 -2 15.70 7.90 12 -6 2 19.10 5.20 12 6 3 1.60 3.30 -12 6 -3 -4.10 2.90 12 6 3 -0.90 3.60 -12 -6 -3 1.70 3.80 -12 -6 -3 -2.00 6.60 12 -6 3 0.80 4.40 12 -6 3 -0.50 4.00 -12 6 -4 0.20 3.20 12 6 4 3.90 3.90 -12 -6 -4 4.60 3.90 12 -6 4 10.60 5.00 -12 -6 -4 -3.80 6.60 -12 6 -5 11.50 4.40 12 6 5 13.60 4.60 -12 -6 -5 8.90 4.40 -12 -6 -5 6.40 7.10 12 -6 5 4.10 4.60 -12 6 -6 8.90 4.10 -12 -6 -6 5.20 4.40 12 -6 6 12.50 5.20 -12 -6 -6 2.90 6.80 -12 6 -7 2.10 3.80 -12 6 -7 0.50 3.40 12 -6 7 5.10 4.90 -12 -6 -7 -1.30 7.00 -12 -6 -7 3.10 4.40 -12 6 -8 -1.50 3.30 -12 6 -8 -2.30 3.20 -12 -6 -8 7.90 4.60 -12 -6 -8 4.00 6.80 12 -6 8 2.70 5.00 -12 6 -9 18.80 5.30 -12 6 -9 20.60 5.20 12 -6 9 7.50 5.20 -12 -6 -9 16.60 5.20 -12 -6 -9 26.20 6.20 -12 -6 -9 42.80 9.60 12 7 -7 3.40 4.40 12 -7 -7 7.60 6.60 12 7 -6 1.80 2.80 12 7 -6 0.80 4.00 12 -7 -6 -5.60 5.10 12 -7 -6 2.10 3.10 -12 7 5 30.80 5.30 12 7 -5 31.20 6.50 12 7 -5 30.10 4.70 12 -7 -5 24.60 7.50 12 -7 -5 33.90 5.40 -12 7 4 5.10 3.80 12 7 -4 11.30 3.50 12 7 -4 5.70 4.50 12 -7 -4 6.60 5.90 12 -7 -4 5.30 3.70 -12 7 3 5.80 3.80 12 7 -3 -0.80 2.90 12 7 -3 -0.90 3.90 12 -7 -3 3.50 3.70 12 -7 -3 0.80 5.30 12 7 -2 1.80 3.10 12 7 -2 1.00 3.60 -12 7 2 0.70 3.30 12 -7 -2 -1.30 5.10 12 -7 -2 4.00 3.90 12 7 -1 25.80 4.80 12 7 -1 13.50 4.80 -12 7 1 15.40 4.50 12 -7 -1 7.00 4.40 12 -7 -1 12.00 6.40 12 7 0 13.50 4.40 12 7 0 8.10 4.70 -12 7 0 5.80 3.90 12 -7 0 18.40 6.50 12 -7 0 8.60 4.70 12 7 1 7.10 3.80 12 7 1 9.40 4.80 -12 7 -1 10.50 4.20 12 -7 1 12.80 5.90 12 -7 1 10.30 5.00 -12 7 -2 -1.00 3.30 12 7 2 -3.40 2.90 12 7 2 -9.00 4.30 -12 -7 -2 -5.00 3.70 12 -7 2 7.30 4.90 12 -7 2 2.10 4.80 12 7 3 10.50 4.30 -12 7 -3 12.10 4.50 -12 -7 -3 44.90 8.60 12 -7 3 14.60 5.60 -12 -7 -3 17.10 5.30 12 -7 3 11.80 5.80 12 7 4 5.60 4.10 -12 7 -4 1.50 3.70 -12 -7 -4 12.20 7.60 -12 -7 -4 -5.40 3.60 12 -7 4 -3.40 4.40 12 7 5 1.40 3.70 -12 7 -5 0.20 3.50 -12 -7 -5 16.80 7.90 -12 -7 -5 2.40 4.10 12 -7 5 4.80 4.80 -12 7 -6 2.80 3.90 12 7 6 -0.70 3.20 -12 -7 -6 0.00 4.10 12 -7 6 2.40 4.90 -12 -7 -6 14.30 7.50 -12 -7 -7 5.70 4.70 -12 -7 -7 18.40 8.10 13 0 -15 -4.30 3.90 13 0 -14 11.90 5.40 13 0 -13 -0.80 3.80 13 0 -12 -3.60 3.40 13 0 -12 -2.50 2.40 13 0 -11 6.10 2.70 13 0 -11 -0.20 4.00 13 0 -10 145.89 11.00 13 0 -10 163.88 8.20 13 0 -9 5.60 2.90 13 0 -9 -1.60 3.70 13 0 -8 356.06 12.30 13 0 -8 340.27 16.00 13 0 -7 -5.10 3.30 13 0 -7 -2.60 2.50 13 0 -6 458.95 14.60 -13 0 6 474.35 11.10 13 0 -6 485.25 19.00 13 0 -5 -0.20 3.70 -13 0 5 0.20 1.40 13 0 -5 -0.30 2.60 -13 0 4 285.87 8.20 13 0 -4 259.97 10.50 13 0 -4 293.87 14.20 13 0 -3 4.10 2.80 -13 0 3 -0.20 2.00 -13 0 3 -1.40 1.60 -13 0 2 214.28 7.80 -13 0 2 221.68 7.60 13 0 -2 225.38 9.50 -13 0 1 0.30 1.90 13 0 -1 -1.70 2.40 13 0 -1 1.60 1.20 13 0 0 130.49 5.10 13 0 0 138.09 7.60 -13 0 0 140.29 6.50 -13 0 -1 -1.40 1.10 -13 0 -1 -1.50 2.20 13 0 1 0.20 1.50 13 0 1 2.00 2.90 -13 0 -2 610.84 17.00 13 0 2 605.34 17.80 -13 0 -2 590.24 14.10 -13 0 -3 -0.40 2.40 -13 0 -3 2.60 1.80 13 0 3 4.70 3.20 13 0 3 1.10 1.10 -13 0 -4 22.50 4.10 13 0 4 18.40 3.90 -13 0 -4 27.70 3.20 13 0 4 26.30 2.00 -13 0 -5 0.90 2.10 13 0 5 2.20 1.10 13 0 5 0.60 2.90 -13 0 -5 -4.80 2.30 -13 0 -6 204.58 8.40 -13 0 -6 201.48 9.90 13 0 6 190.18 9.40 13 0 6 192.28 5.60 13 0 7 5.90 3.20 -13 0 -7 5.80 2.90 -13 0 -7 -5.30 2.50 -13 0 -8 69.89 6.20 13 0 8 66.49 6.60 -13 0 -8 71.09 7.00 -13 0 -9 0.30 3.20 13 0 9 1.20 3.00 -13 0 -9 2.80 3.10 -13 0 -10 51.09 6.70 13 0 10 63.49 6.60 -13 0 -10 48.10 6.30 13 0 11 2.40 3.30 -13 0 -11 -3.60 3.00 -13 0 -11 -0.80 3.20 -13 0 -12 24.50 5.40 -13 0 -12 17.80 4.90 13 0 12 28.70 5.00 -13 0 -13 -5.20 3.10 -13 0 -13 5.30 4.00 13 0 13 -1.20 2.90 -13 0 -14 -3.20 3.40 -13 0 -14 2.40 3.90 -13 0 -14 -31.60 11.50 13 -1 -15 8.10 5.60 13 -1 -14 21.90 6.70 13 1 -13 -3.60 3.50 13 -1 -13 -3.90 4.10 13 1 -12 27.30 6.10 13 -1 -12 34.60 7.50 13 1 -11 0.60 3.60 13 1 -11 3.30 3.00 13 -1 -11 -5.20 3.80 13 -1 -11 -4.70 1.90 13 1 -10 2.20 3.90 13 1 -10 0.10 2.70 13 -1 -10 1.60 4.40 13 -1 -10 0.70 2.30 13 1 -9 5.00 4.10 13 1 -9 1.80 2.80 13 -1 -9 1.10 4.40 13 -1 -9 0.20 2.40 13 1 -8 33.90 4.70 13 1 -8 31.80 6.10 13 -1 -8 35.70 7.40 13 -1 -8 26.50 3.90 13 1 -7 3.50 3.10 13 1 -7 3.20 3.70 13 -1 -7 5.00 4.50 13 -1 -7 1.50 2.50 -13 -1 7 2.70 1.50 13 1 -6 4.10 3.10 -13 1 6 1.20 1.20 13 -1 -6 -0.10 4.10 -13 -1 6 2.20 1.60 13 -1 -6 1.90 2.60 -13 1 5 90.79 3.90 13 1 -5 83.29 6.30 13 -1 -5 86.49 8.90 13 -1 -5 100.19 6.30 -13 -1 5 95.19 4.50 -13 1 4 0.30 1.50 13 1 -4 2.40 2.70 -13 -1 4 1.00 1.70 13 -1 -4 2.70 3.90 13 -1 -4 0.20 2.60 13 1 -3 22.40 4.00 -13 1 3 10.60 2.30 -13 1 3 11.50 2.60 -13 -1 3 13.70 2.60 13 -1 -3 11.50 5.10 13 -1 -3 12.70 3.40 -13 1 2 12.80 2.70 13 1 -2 16.00 3.80 13 1 -2 12.40 2.90 13 1 -2 15.00 1.50 -13 1 2 18.50 2.50 13 1 -2 14.40 1.40 -13 -1 2 20.00 3.00 13 -1 -2 27.20 6.40 13 -1 -2 18.90 3.90 13 1 -1 114.99 4.50 -13 1 1 110.19 5.70 13 1 -1 110.79 7.00 13 1 -1 109.09 5.70 -13 1 1 107.29 4.60 13 -1 -1 111.19 3.90 -13 -1 1 109.79 5.70 13 -1 -1 121.09 7.10 13 1 0 90.69 5.00 -13 1 0 83.39 3.50 -13 1 0 84.69 5.30 13 1 0 91.39 6.20 13 -1 0 88.49 6.50 13 -1 0 85.39 4.00 -13 -1 0 81.79 5.20 13 1 1 -1.60 2.80 -13 1 -1 -2.30 2.00 13 1 1 0.50 1.70 -13 1 -1 -2.80 1.30 13 -1 1 0.10 1.40 -13 -1 -1 -0.20 1.10 -13 -1 -1 0.90 2.30 13 -1 1 -0.30 2.70 13 1 2 16.70 2.40 13 1 2 20.10 3.90 -13 1 -2 19.80 2.60 -13 1 -2 20.30 3.80 -13 -1 -2 19.10 3.60 -13 -1 -2 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226.78 7.20 14 1 -5 9.10 3.40 -14 1 5 17.50 2.20 14 -1 -5 8.80 3.30 14 -1 -5 7.80 4.80 -14 -1 5 14.50 2.40 14 1 -4 202.78 9.60 -14 1 4 224.08 7.30 14 -1 -4 204.68 9.50 14 -1 -4 222.98 13.50 -14 -1 4 227.98 7.70 -14 1 3 0.40 2.00 14 1 -3 4.50 3.10 -14 1 3 1.70 1.90 14 -1 -3 -0.10 4.40 14 -1 -3 1.60 2.90 -14 -1 3 -0.60 1.90 14 1 -2 64.59 6.50 14 1 -2 55.69 2.30 -14 1 2 58.99 4.00 14 1 -2 65.29 4.90 -14 1 2 58.29 4.40 -14 -1 2 58.79 4.70 14 -1 -2 68.79 6.40 14 1 -1 23.20 4.60 -14 1 1 22.20 3.30 -14 1 1 21.70 2.60 14 1 -1 18.80 3.10 14 1 -1 19.80 2.30 -14 -1 1 21.90 3.40 14 -1 -1 20.40 1.80 14 -1 -1 23.30 4.30 -14 1 0 54.69 4.90 14 1 0 54.29 4.40 14 1 0 35.30 4.80 -14 -1 0 47.90 4.80 14 -1 0 51.49 5.90 14 -1 0 45.20 3.20 14 1 1 0.60 3.00 -14 1 -1 3.80 2.60 14 1 1 -0.50 1.70 -14 1 -1 1.30 1.50 -14 -1 -1 -2.60 2.20 14 -1 1 -0.10 1.50 14 -1 1 -2.70 2.90 14 1 2 126.19 7.90 -14 1 -2 119.69 5.20 14 1 2 134.69 5.60 -14 1 -2 130.29 7.40 -14 -1 -2 113.59 6.90 -14 -1 -2 118.19 4.70 14 -1 2 136.99 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109.39 6.60 14 -3 -3 103.69 7.30 14 3 -2 9.10 3.60 -14 3 2 13.40 3.20 14 3 -2 9.70 2.30 14 3 -2 7.20 3.20 -14 -3 2 9.40 3.00 14 -3 -2 9.90 3.80 14 -3 -2 7.50 5.20 14 3 -1 1.10 2.60 14 3 -1 -2.70 2.90 -14 3 1 2.20 2.50 14 3 -1 1.90 2.00 -14 -3 1 5.80 2.90 14 -3 -1 -1.50 4.30 14 -3 -1 5.50 3.50 14 3 0 15.10 4.30 14 3 0 13.00 3.40 14 3 0 13.80 3.00 -14 3 0 17.60 3.60 14 -3 0 15.80 5.70 14 -3 0 20.30 4.50 -14 -3 0 15.10 3.70 14 3 1 32.30 4.30 -14 3 -1 35.80 4.70 14 3 1 30.60 4.80 -14 -3 -1 32.90 4.80 14 -3 1 32.50 4.90 -14 3 -2 41.80 4.50 14 3 2 38.30 4.70 14 3 2 36.10 5.50 -14 3 -2 48.60 5.40 14 -3 2 28.80 5.10 -14 -3 -2 37.40 5.20 14 3 3 49.30 5.70 -14 3 -3 60.39 5.30 14 3 3 66.69 6.00 -14 3 -3 69.49 6.80 14 -3 3 47.90 5.90 -14 -3 -3 60.89 4.80 -14 -3 -3 67.79 6.90 14 3 4 2.40 3.20 -14 3 -4 6.90 3.50 -14 3 -4 1.50 2.70 -14 -3 -4 1.00 2.40 -14 -3 -4 1.70 3.40 14 -3 4 3.70 3.70 -14 3 -5 6.00 3.50 14 3 5 6.30 3.30 -14 3 -5 3.20 2.80 -14 -3 -5 3.80 2.70 -14 -3 -5 4.60 3.70 14 -3 5 12.00 4.40 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4.50 -15 -1 5 1.80 2.00 15 1 -4 32.00 5.00 -15 1 4 25.70 3.10 15 -1 -4 30.10 7.20 -15 -1 4 25.20 3.30 15 -1 -4 24.20 4.60 -15 1 3 65.89 6.30 15 1 -3 79.39 7.20 -15 1 3 65.99 4.60 -15 -1 3 70.39 4.90 15 -1 -3 72.39 6.90 15 -1 -3 70.79 9.60 15 1 -2 8.50 3.70 -15 1 2 13.30 2.80 -15 1 2 7.60 3.40 15 -1 -2 10.80 3.80 -15 -1 2 6.00 2.60 15 1 -1 23.80 4.80 15 1 -1 19.50 3.30 -15 1 1 18.40 3.30 15 1 -1 19.40 2.50 15 -1 -1 18.30 1.70 -15 -1 1 16.80 3.40 15 -1 -1 20.50 4.40 15 1 0 95.59 5.40 15 1 0 94.29 7.30 -15 1 0 95.19 6.00 15 -1 0 92.89 7.30 -15 -1 0 104.69 6.40 15 -1 0 100.59 5.10 15 1 1 45.40 5.80 -15 1 -1 28.20 4.20 15 1 1 31.40 3.40 -15 -1 -1 30.70 4.40 15 -1 1 33.10 3.70 15 -1 1 27.90 4.80 -15 1 -2 -0.40 2.00 -15 1 -2 5.90 3.10 15 1 2 3.30 3.30 15 1 2 3.40 1.90 -15 -1 -2 3.30 2.90 15 -1 2 5.40 3.40 15 1 3 10.90 4.20 15 1 3 10.50 2.20 -15 1 -3 5.20 3.20 -15 1 -3 12.40 2.50 -15 -1 -3 10.30 3.50 15 -1 3 5.10 3.70 -15 1 -4 109.79 7.50 15 1 4 104.99 4.90 -15 1 -4 116.39 5.90 15 1 4 101.79 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19 4 -7 1.20 4.50 19 -4 -7 -0.30 3.60 19 -4 -7 3.70 6.10 19 4 -6 38.40 6.20 19 4 -6 21.20 6.10 19 -4 -6 26.40 8.50 19 -4 -6 26.10 5.60 19 4 -5 -0.50 4.40 19 4 -5 -0.70 3.60 19 -4 -5 -1.30 3.50 19 -4 -5 -6.10 4.80 19 4 -4 16.80 5.90 19 4 -4 9.50 4.40 19 -4 -4 22.40 5.40 19 -4 -4 16.00 7.20 19 4 -3 2.60 4.60 19 4 -3 3.70 3.70 19 -4 -3 12.60 4.90 19 -4 -3 8.90 6.70 19 4 -2 13.80 4.60 19 4 -2 1.00 4.00 -19 -4 2 12.40 4.40 19 -4 -2 13.10 7.10 19 -4 -2 3.00 4.00 19 4 -1 1.80 3.30 19 4 -1 -0.90 4.00 19 -4 -1 -5.80 3.20 -19 -4 1 -3.90 3.40 19 4 0 5.80 3.60 -19 4 0 13.50 4.30 19 4 0 3.30 4.40 -19 -4 0 15.20 4.90 19 -4 0 3.50 4.40 19 4 1 6.90 3.10 19 4 1 7.10 3.50 19 4 1 4.50 4.60 -19 4 -1 5.50 3.90 19 -4 1 7.50 4.80 -19 -4 -1 3.80 4.20 19 4 2 14.50 4.00 -19 4 -2 9.30 4.20 19 4 2 7.70 3.50 19 4 2 2.20 4.50 -19 -4 -2 14.00 5.10 19 -4 2 5.30 4.80 -19 4 -3 8.60 4.10 19 4 3 0.10 3.90 19 -4 3 -6.50 3.80 -19 -4 -3 1.00 4.10 -19 4 -4 14.70 4.90 19 4 4 16.70 5.20 -19 -4 -4 25.00 6.10 19 -4 4 24.00 6.60 -19 4 -5 -3.80 3.40 19 4 5 2.40 4.20 19 -4 5 -4.30 4.40 -19 -4 -5 -1.90 4.00 19 4 6 18.10 5.10 -19 4 -6 14.90 5.20 19 -4 6 22.00 6.70 -19 -4 -6 23.30 6.30 19 5 -4 18.00 5.20 19 -5 -4 19.90 5.50 19 -5 -4 15.10 7.70 19 5 -3 -0.20 3.90 19 5 -3 3.80 4.60 19 -5 -3 9.50 4.70 19 -5 -3 0.70 5.80 -19 -5 3 6.20 5.20 19 5 -2 5.00 3.60 19 5 -2 2.00 4.40 -19 -5 2 9.80 4.60 19 -5 -2 3.60 6.20 19 -5 -2 -6.80 3.50 19 5 -1 -2.20 4.00 19 5 -1 2.90 3.40 19 -5 -1 0.30 4.40 -19 -5 1 2.80 4.50 19 5 0 8.60 4.90 19 5 0 4.70 3.80 -19 -5 0 8.80 4.70 19 -5 0 5.60 4.90 19 5 1 0.40 4.20 19 5 1 1.60 3.00 -19 5 -1 2.40 3.60 19 5 1 1.50 3.20 -19 -5 -1 3.60 4.30 19 -5 1 5.80 4.90 19 5 2 5.90 3.50 19 5 2 10.20 3.90 -19 5 -2 6.50 4.20 19 5 2 5.80 4.70 -19 -5 -2 5.80 4.50 19 -5 2 2.80 4.60 -19 5 -3 0.10 3.40 19 5 3 4.00 3.60 19 5 3 -0.10 4.60 -19 -5 -3 3.50 4.70 20 0 -9 0.10 3.70 20 0 -8 11.90 4.60 20 0 -7 -4.80 3.10 20 0 -6 -4.00 3.20 20 0 -5 -1.40 3.50 20 0 -4 38.30 6.20 20 0 -3 1.50 4.00 20 0 -2 35.70 6.40 20 0 -1 -0.80 3.80 -20 0 1 -1.80 3.10 20 0 0 -2.10 3.50 -20 0 0 -1.80 2.80 -20 0 -1 -1.60 2.80 20 0 1 -6.80 3.00 -20 0 -2 14.00 4.20 20 0 2 10.20 4.90 20 0 3 1.20 4.10 -20 0 -3 1.10 3.30 20 0 4 11.30 4.80 -20 0 -4 13.80 4.30 20 0 5 2.00 4.10 -20 0 -5 3.10 3.70 20 0 6 1.10 4.00 -20 0 -6 -4.00 3.10 -20 0 -7 -2.10 3.60 20 0 7 -3.50 3.90 20 0 8 1.70 4.40 -20 0 -8 -3.30 3.60 20 1 -9 -2.10 3.60 20 -1 -9 0.00 5.40 20 -1 -9 6.50 4.10 20 1 -8 12.20 4.80 20 -1 -8 8.30 4.40 20 1 -7 -0.20 3.80 20 -1 -7 2.90 3.90 20 1 -6 4.90 4.60 20 -1 -6 2.10 3.90 20 1 -5 19.70 5.40 20 -1 -5 9.90 4.80 20 1 -4 27.80 6.30 20 -1 -4 29.70 5.80 20 1 -3 2.00 3.80 20 -1 -3 0.80 4.00 20 1 -2 -1.40 3.50 20 -1 -2 6.80 4.20 20 1 -1 4.30 4.40 20 -1 -1 3.40 4.20 -20 -1 1 7.40 3.40 20 1 0 15.30 5.10 -20 1 0 10.90 3.80 -20 -1 0 12.60 4.00 20 -1 0 17.90 5.30 -20 1 -1 1.80 3.00 20 1 1 1.40 4.10 20 -1 1 0.20 4.00 -20 -1 -1 -0.10 3.10 20 1 2 -1.50 3.50 -20 1 -2 1.20 3.30 20 -1 2 1.70 4.30 -20 -1 -2 1.40 3.30 -20 1 -3 -2.20 3.20 20 1 3 1.80 3.80 20 -1 3 0.90 4.40 -20 -1 -3 2.60 3.50 20 1 4 9.40 4.80 -20 1 -4 -0.70 3.30 20 -1 4 0.20 4.20 -20 -1 -4 2.00 3.60 20 1 5 19.50 5.70 -20 1 -5 16.80 4.80 -20 -1 -5 28.40 5.80 20 -1 5 11.60 5.20 -20 1 -6 7.50 4.10 20 1 6 6.00 4.80 20 -1 6 7.90 4.80 -20 -1 -6 0.30 3.80 20 1 7 5.00 4.50 -20 1 -7 3.20 4.20 20 -1 7 1.40 4.40 -20 -1 -7 0.70 4.00 20 1 8 10.90 5.00 -20 1 -8 18.10 5.40 20 -1 8 12.30 5.40 -20 -1 -8 9.10 4.90 20 -2 -9 0.70 5.70 20 2 -8 2.60 4.20 20 -2 -8 7.40 6.40 20 -2 -8 6.50 4.20 20 2 -7 -2.00 4.00 20 -2 -7 4.70 6.20 20 -2 -7 1.80 3.50 20 2 -6 4.90 4.60 20 -2 -6 -4.20 3.40 20 -2 -6 2.10 5.80 20 2 -5 41.80 7.00 20 -2 -5 53.69 7.30 20 2 -4 4.70 4.60 20 -2 -4 6.30 4.30 20 2 -3 10.20 4.70 20 -2 -3 5.00 4.30 20 2 -2 9.30 4.90 20 -2 -2 9.80 4.80 20 2 -1 49.40 7.10 -20 -2 1 74.69 7.10 20 -2 -1 66.09 7.80 -20 2 0 -3.70 2.80 20 2 0 -0.10 3.60 -20 -2 0 0.90 3.30 20 -2 0 -3.90 3.80 20 2 1 5.40 4.50 -20 2 -1 3.60 3.30 -20 -2 -1 9.20 4.00 20 -2 1 0.10 4.20 20 2 2 -0.40 3.80 -20 2 -2 2.00 3.50 -20 -2 -2 0.20 3.40 20 -2 2 5.60 4.30 -20 2 -3 86.49 8.40 20 2 3 73.09 8.40 -20 -2 -3 80.89 8.50 20 -2 3 64.39 8.10 20 2 4 -0.40 3.90 -20 2 -4 4.50 4.00 20 -2 4 -2.40 4.30 -20 -2 -4 3.20 4.10 20 2 5 -3.10 3.90 -20 2 -5 9.30 4.20 -20 -2 -5 4.20 4.30 20 -2 5 5.70 4.60 20 2 6 4.30 4.30 -20 2 -6 0.60 3.70 20 -2 6 -3.10 4.10 -20 -2 -6 0.10 4.00 -20 2 -7 17.10 5.40 20 2 7 18.80 5.60 -20 -2 -7 24.40 6.10 20 -2 7 21.20 6.20 20 3 -7 16.50 5.50 20 -3 -7 20.10 8.40 20 -3 -7 17.20 4.80 20 3 -6 7.30 5.00 20 -3 -6 3.90 6.30 20 -3 -6 1.60 3.70 20 3 -5 12.80 4.80 20 -3 -5 21.70 8.00 20 -3 -5 23.90 5.60 20 3 -4 -3.50 3.80 20 -3 -4 1.70 4.10 20 -3 -4 11.90 6.60 20 3 -3 19.40 5.50 20 3 -3 32.40 5.40 20 -3 -3 27.70 5.90 20 3 -2 6.50 3.60 20 3 -2 -3.30 3.90 20 -3 -2 7.50 4.40 20 3 -1 10.80 3.90 20 3 -1 18.90 5.60 20 -3 -1 10.10 5.00 -20 -3 1 20.50 4.70 20 3 0 6.00 4.60 20 -3 0 2.10 4.50 -20 -3 0 4.50 3.70 20 3 1 9.90 5.00 -20 3 -1 19.80 4.90 -20 -3 -1 7.20 4.30 20 -3 1 15.90 5.40 -20 3 -2 -1.90 3.50 20 3 2 -3.50 3.90 -20 -3 -2 -3.80 3.40 20 -3 2 2.60 4.60 20 3 3 -4.00 3.80 20 -3 3 0.50 4.40 -20 -3 -3 1.30 4.20 -20 3 -4 1.00 3.80 20 3 4 13.70 5.30 20 -3 4 8.00 4.90 -20 -3 -4 8.40 5.10 -20 3 -5 -3.10 3.50 20 3 5 0.70 4.20 20 -3 5 0.50 4.20 -20 -3 -5 6.50 4.70 -20 3 -6 6.10 4.40 20 3 6 -2.90 3.70 20 -3 6 0.10 4.50 -20 -3 -6 0.20 4.50 20 4 -5 3.60 3.70 20 4 -5 7.10 4.90 20 -4 -5 3.80 6.00 20 -4 -5 4.60 4.10 20 4 -4 -1.90 3.30 20 4 -4 -0.40 4.40 20 -4 -4 4.00 4.30 20 -4 -4 -1.40 5.60 20 4 -3 -1.30 3.10 20 4 -3 -1.10 4.20 20 -4 -3 11.90 5.00 20 -4 -3 -0.50 5.50 20 4 -2 13.40 5.20 20 4 -2 4.10 3.50 20 -4 -2 8.30 5.00 -20 -4 2 8.50 7.00 20 4 -1 -0.80 4.10 20 4 -1 3.20 3.90 20 -4 -1 2.20 4.40 -20 -4 1 2.70 4.00 20 4 0 10.00 4.20 20 4 0 17.00 5.60 20 -4 0 11.90 5.20 -20 -4 0 16.80 5.20 20 4 1 -0.10 4.20 -20 4 -1 -0.40 3.50 20 -4 1 -1.50 4.40 -20 -4 -1 2.60 4.20 -20 4 -2 22.80 5.40 20 4 2 32.00 5.00 20 4 2 26.70 6.10 20 -4 2 21.70 6.40 -20 -4 -2 32.60 6.20 20 4 3 -1.70 3.90 -20 4 -3 0.20 3.90 20 -4 3 8.20 5.00 -20 -4 -3 -5.10 3.80 -20 4 -4 29.70 6.10 -20 -4 -4 36.80 7.10 20 -4 4 23.40 6.40 21 0 -8 1.80 4.00 21 0 -7 -0.40 3.80 21 0 -6 7.10 4.70 21 0 -5 -1.90 3.70 21 0 -4 -2.80 3.60 21 0 -3 -5.60 3.80 21 0 -2 5.20 4.60 21 0 -1 -0.30 4.10 21 0 0 3.40 4.30 -21 0 0 4.60 3.70 21 0 1 -0.10 3.80 -21 0 -1 -2.00 2.80 -21 0 -2 9.60 4.10 21 0 2 17.00 5.60 -21 0 -3 0.40 3.20 21 0 3 3.50 4.50 21 0 4 -0.10 3.90 -21 0 -4 -2.40 3.30 21 0 5 -4.10 4.00 -21 0 -5 0.60 3.50 -21 0 -6 8.00 4.30 21 0 6 1.30 4.40 21 1 -8 -3.00 3.80 21 -1 -8 1.50 3.80 21 1 -7 11.60 4.90 21 -1 -7 8.80 4.50 21 1 -6 20.60 5.90 21 -1 -6 18.40 5.20 21 1 -5 7.00 4.60 21 -1 -5 4.80 4.50 21 1 -4 0.80 4.20 21 -1 -4 3.50 4.50 21 1 -3 3.70 4.20 21 -1 -3 13.50 4.80 21 1 -2 48.30 7.40 21 -1 -2 54.39 7.80 21 1 -1 6.50 4.50 21 -1 -1 9.50 4.80 21 1 0 0.30 4.00 21 -1 0 6.20 4.50 -21 -1 0 5.30 3.40 21 1 1 15.80 5.60 -21 1 -1 7.40 3.60 21 -1 1 8.60 4.70 -21 -1 -1 6.10 3.70 21 1 2 4.30 4.40 -21 1 -2 3.80 3.60 -21 -1 -2 -2.00 3.10 21 -1 2 -2.10 4.20 -21 1 -3 8.20 4.00 21 1 3 16.10 5.50 -21 -1 -3 6.50 3.90 21 -1 3 7.00 5.00 -21 1 -4 16.60 4.80 21 1 4 27.40 6.30 21 -1 4 16.00 5.50 -21 -1 -4 25.80 5.60 21 1 5 8.30 4.90 -21 1 -5 9.10 4.10 -21 -1 -5 7.80 4.40 21 -1 5 8.50 5.00 -21 1 -6 4.60 3.90 21 1 6 1.20 4.30 -21 -1 -6 0.70 3.90 21 -1 6 1.30 4.60 21 2 -7 1.60 4.20 21 -2 -7 -7.40 3.10 21 2 -6 7.40 4.60 21 -2 -6 -4.70 3.50 21 2 -5 65.69 8.30 21 -2 -5 70.59 8.40 21 2 -4 5.80 4.70 21 -2 -4 3.10 4.50 21 2 -3 8.80 4.70 21 -2 -3 7.10 4.70 21 2 -2 -5.00 3.70 21 -2 -2 -5.10 4.10 21 2 -1 47.00 7.30 21 -2 -1 41.90 7.20 21 2 0 0.60 4.00 21 -2 0 6.00 4.50 -21 -2 0 5.90 3.90 21 2 1 10.80 4.80 -21 2 -1 12.40 4.10 -21 -2 -1 12.50 4.50 21 -2 1 16.60 5.50 21 2 2 1.90 4.40 -21 2 -2 0.40 3.40 -21 -2 -2 -1.00 3.50 21 -2 2 4.60 4.50 -21 2 -3 -0.80 3.20 21 2 3 2.70 4.40 -21 -2 -3 4.80 4.20 21 -2 3 -0.20 4.60 21 2 4 -1.40 4.40 -21 2 -4 6.80 4.30 -21 -2 -4 5.20 4.40 21 -2 4 -1.40 4.80 21 2 5 23.70 6.20 -21 2 -5 35.90 6.60 -21 -2 -5 26.30 6.30 21 -2 5 49.10 8.00 21 3 -5 5.70 4.80 21 -3 -5 8.10 4.70 21 3 -4 6.10 4.70 21 -3 -4 -2.30 4.00 21 3 -3 17.00 6.00 21 -3 -3 9.80 4.80 21 3 -2 -3.90 4.20 21 -3 -2 -1.80 4.00 21 3 -1 2.20 4.50 21 -3 -1 3.00 4.70 21 3 0 -5.00 4.00 -21 -3 0 0.70 3.70 21 -3 0 2.50 4.70 21 3 1 -4.00 3.80 21 -3 1 1.10 4.30 -21 -3 -1 5.70 4.30 -21 3 -2 4.40 4.00 21 3 2 7.70 4.80 21 -3 2 1.70 4.80 -21 -3 -2 1.30 4.10 21 3 3 7.80 4.80 -21 3 -3 11.30 4.60 21 -3 3 10.00 5.10 -21 -3 -3 6.90 4.60 21 3 4 0.10 4.20 -21 3 -4 -3.40 3.50 -21 -3 -4 1.50 4.40 21 -3 4 -7.80 4.00 22 0 -6 26.40 6.50 22 0 -5 -5.40 3.80 22 0 -4 -0.80 4.00 22 0 -3 -6.00 3.80 22 0 -2 91.39 9.90 22 0 -1 2.40 4.30 22 0 0 6.70 5.00 -22 0 -1 2.60 4.20 22 0 1 1.20 4.30 22 0 2 -8.30 3.80 -22 0 -2 -0.90 3.40 22 0 3 1.70 4.90 -22 0 -3 -3.20 3.30 -22 0 -4 1.30 3.70 22 0 4 8.40 5.00 22 1 -6 5.10 4.70 22 -1 -6 -7.60 3.30 22 1 -5 3.70 4.50 22 -1 -5 -2.20 3.90 22 1 -4 11.10 5.20 22 -1 -4 11.10 5.00 22 1 -3 0.80 4.10 22 -1 -3 -1.00 4.00 22 1 -2 22.50 5.80 22 -1 -2 16.30 5.80 22 1 -1 6.50 4.90 22 -1 -1 -1.90 3.90 22 1 0 16.70 5.50 22 -1 0 20.90 5.40 22 1 1 6.10 4.80 -22 -1 -1 4.10 3.60 22 -1 1 -4.20 4.10 -22 1 -2 12.80 4.50 22 1 2 7.10 5.20 22 -1 2 12.10 5.20 -22 -1 -2 16.80 4.70 22 1 3 -0.10 4.40 -22 1 -3 -2.10 3.40 22 -1 3 -2.60 4.20 -22 -1 -3 -2.50 3.60 22 1 4 -7.40 3.50 -22 1 -4 1.90 3.90 22 -1 4 3.50 4.60 -22 -1 -4 3.10 3.90 22 -2 -5 6.10 4.60 22 2 -4 -0.20 4.30 22 -2 -4 -4.70 3.60 22 2 -3 24.90 6.20 22 -2 -3 31.30 6.80 22 2 -2 8.70 5.10 22 -2 -2 4.30 4.80 22 2 -1 6.40 5.10 22 -2 -1 5.30 4.30 22 2 0 -1.80 4.20 22 -2 0 -0.50 4.30 22 2 1 13.80 5.70 22 -2 1 14.10 5.60 -22 -2 -1 7.70 4.40 22 2 2 6.90 4.80 -22 2 -2 2.50 3.80 22 -2 2 5.50 4.50 -22 -2 -2 -2.10 3.90 -22 2 -3 4.20 4.10 22 2 3 0.80 4.50 -22 -2 -3 0.50 3.80 22 -2 3 4.80 4.40 23 0 -3 -4.80 4.00 23 0 -2 1.30 4.70 23 0 -1 4.70 4.90 23 0 0 41.40 7.40 23 0 1 -6.90 3.90 23 1 -2 21.40 6.10 23 -1 -2 26.50 6.70 23 1 -1 8.40 4.90 23 -1 -1 1.00 4.60 23 1 0 0.30 4.70 23 -1 0 0.00 4.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 3701 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.21660(3) 0.63796(8) 0.63576(4) 0.02504(16) Uani 1 1 d . . . . . O1 O 0.19431(10) 0.4467(2) 0.65374(12) 0.0345(4) Uani 1 1 d . . . . . O2 O 0.27113(9) 0.7277(3) 0.70344(11) 0.0330(4) Uani 1 1 d . . . . . C1 C 0.13247(12) 0.7741(3) 0.63570(15) 0.0244(5) Uani 1 1 d . . . . . C2 C 0.06222(13) 0.6852(4) 0.62174(17) 0.0319(5) Uani 1 1 d . . . . . H2 H 0.059653 0.555172 0.613755 0.038 Uiso 1 1 calc R U . . . C3 C -0.00360(13) 0.7915(4) 0.61985(19) 0.0373(6) Uani 1 1 d . . . . . H3 H -0.050347 0.731843 0.610130 0.045 Uiso 1 1 calc R U . . . C4 C -0.00114(14) 0.9866(4) 0.63226(17) 0.0345(6) Uani 1 1 d . . . . . C5 C 0.06991(15) 1.0713(4) 0.64653(18) 0.0364(6) Uani 1 1 d . . . . . H5 H 0.072839 1.201001 0.655688 0.044 Uiso 1 1 calc R U . . . C6 C 0.13589(14) 0.9671(4) 0.64737(17) 0.0318(5) Uani 1 1 d . . . . . H6 H 0.182720 1.026768 0.655787 0.038 Uiso 1 1 calc R U . . . C7 C -0.07309(17) 1.1011(5) 0.6279(2) 0.0495(8) Uani 1 1 d . . . . . H7A H -0.090821 1.116495 0.560711 0.074 Uiso 1 1 calc R U . . . H7B H -0.063202 1.222576 0.656720 0.074 Uiso 1 1 calc R U . . . H7C H -0.111117 1.037403 0.663443 0.074 Uiso 1 1 calc R U . . . C8 C 0.24843(11) 0.6558(3) 0.51832(15) 0.0240(5) Uani 1 1 d . . . . . C9 C 0.20629(12) 0.5437(3) 0.43930(16) 0.0268(5) Uani 1 1 d . . . . . H9A H 0.156096 0.514066 0.461042 0.032 Uiso 1 1 calc R U . . . H9B H 0.199878 0.621246 0.380961 0.032 Uiso 1 1 calc R U . . . C10 C 0.24494(14) 0.3635(3) 0.41268(17) 0.0320(5) Uani 1 1 d . . . . . F1 F 0.31633(9) 0.3931(2) 0.38657(14) 0.0531(5) Uani 1 1 d . . . . . F2 F 0.24952(10) 0.2376(2) 0.48479(11) 0.0480(4) Uani 1 1 d . . . . . F3 F 0.20837(11) 0.2791(3) 0.33688(12) 0.0592(5) Uani 1 1 d . . . . . N1 N 0.33276(10) 0.8263(3) 0.41564(13) 0.0282(4) Uani 1 1 d . . . . . H1 H 0.315212 0.768464 0.363993 0.034 Uiso 1 1 calc R U . . . C11 C 0.30403(11) 0.7827(3) 0.50176(15) 0.0246(5) Uani 1 1 d . . . . . H11 H 0.324458 0.846407 0.556451 0.030 Uiso 1 1 calc R U . . . C12 C 0.39196(13) 0.9661(3) 0.40461(17) 0.0296(5) Uani 1 1 d . . . . . H12A H 0.397751 1.038216 0.464903 0.035 Uiso 1 1 calc R U . . . H12B H 0.375639 1.052468 0.352654 0.035 Uiso 1 1 calc R U . . . C13 C 0.46865(12) 0.8861(3) 0.38123(15) 0.0261(5) Uani 1 1 d . . . . . C14 C 0.49158(14) 0.7053(4) 0.40744(17) 0.0341(6) Uani 1 1 d . . . . . H14 H 0.458481 0.626045 0.438843 0.041 Uiso 1 1 calc R U . . . C15 C 0.56410(15) 0.6414(4) 0.38692(19) 0.0409(6) Uani 1 1 d . . . . . H15 H 0.579069 0.520128 0.404954 0.049 Uiso 1 1 calc R U . . . C16 C 0.61357(14) 0.7574(4) 0.34006(18) 0.0404(6) Uani 1 1 d . . . . . H16 H 0.661873 0.714772 0.326752 0.048 Uiso 1 1 calc R U . . . C17 C 0.59128(14) 0.9358(4) 0.31318(18) 0.0380(6) Uani 1 1 d . . . . . H17 H 0.624389 1.013570 0.280915 0.046 Uiso 1 1 calc R U . . . C18 C 0.51920(13) 1.0013(4) 0.33393(17) 0.0321(5) Uani 1 1 d . . . . . H18 H 0.504821 1.122996 0.315991 0.038 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0253(3) 0.0310(3) 0.0189(3) 0.0026(2) 0.00230(19) 0.0017(2) O1 0.0384(9) 0.0323(10) 0.0335(9) 0.0090(7) 0.0084(7) 0.0051(7) O2 0.0312(8) 0.0493(11) 0.0182(8) 0.0014(7) -0.0025(6) -0.0008(7) C1 0.0266(11) 0.0291(12) 0.0180(10) 0.0016(8) 0.0054(8) 0.0003(8) C2 0.0312(12) 0.0314(13) 0.0335(13) 0.0014(10) 0.0045(10) 0.0006(9) C3 0.0248(12) 0.0489(16) 0.0383(14) 0.0021(12) 0.0034(10) -0.0014(10) C4 0.0384(14) 0.0457(16) 0.0198(11) 0.0034(10) 0.0059(9) 0.0121(11) C5 0.0473(15) 0.0296(13) 0.0328(13) 0.0012(10) 0.0071(11) 0.0084(11) C6 0.0351(13) 0.0328(13) 0.0278(12) -0.0015(10) 0.0031(9) -0.0023(10) C7 0.0482(16) 0.067(2) 0.0334(15) 0.0043(13) 0.0052(12) 0.0257(14) C8 0.0234(10) 0.0305(12) 0.0182(10) -0.0013(9) 0.0024(8) 0.0040(8) C9 0.0265(11) 0.0317(13) 0.0221(11) -0.0004(9) -0.0002(8) 0.0030(9) C10 0.0390(13) 0.0307(13) 0.0263(12) -0.0027(10) 0.0028(9) -0.0001(10) F1 0.0491(9) 0.0433(10) 0.0694(12) -0.0069(8) 0.0266(8) 0.0088(7) F2 0.0699(11) 0.0330(9) 0.0416(9) 0.0043(7) 0.0085(8) 0.0097(7) F3 0.0827(13) 0.0506(11) 0.0425(10) -0.0240(8) -0.0131(9) 0.0026(9) N1 0.0284(10) 0.0378(12) 0.0186(9) -0.0028(8) 0.0038(7) -0.0035(8) C11 0.0245(11) 0.0298(12) 0.0194(10) -0.0010(9) 0.0003(8) 0.0053(9) C12 0.0323(12) 0.0314(13) 0.0254(12) 0.0016(9) 0.0058(9) -0.0001(9) C13 0.0266(11) 0.0332(13) 0.0184(10) 0.0001(9) 0.0011(8) -0.0011(9) C14 0.0370(13) 0.0386(14) 0.0269(12) 0.0072(11) 0.0048(10) 0.0018(10) C15 0.0416(14) 0.0451(16) 0.0357(14) 0.0017(12) -0.0001(11) 0.0134(12) C16 0.0295(13) 0.0630(19) 0.0287(13) -0.0087(12) 0.0013(10) 0.0047(12) C17 0.0290(13) 0.0589(18) 0.0267(12) -0.0074(12) 0.0071(10) -0.0123(11) C18 0.0354(12) 0.0366(14) 0.0241(12) -0.0007(10) 0.0008(9) -0.0049(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 S1 O2 119.03(10) . . ? O1 S1 C8 109.35(11) . . ? O2 S1 C8 108.87(10) . . ? O1 S1 C1 106.24(10) . . ? O2 S1 C1 106.85(10) . . ? C8 S1 C1 105.65(10) . . ? C6 C1 C2 119.9(2) . . ? C6 C1 S1 120.67(18) . . ? C2 C1 S1 119.41(18) . . ? C3 C2 C1 119.6(2) . . ? C3 C2 H2 120.2 . . ? C1 C2 H2 120.2 . . ? C2 C3 C4 121.2(2) . . ? C2 C3 H3 119.4 . . ? C4 C3 H3 119.4 . . ? C5 C4 C3 117.9(2) . . ? C5 C4 C7 121.4(3) . . ? C3 C4 C7 120.7(2) . . ? C6 C5 C4 121.4(2) . . ? C6 C5 H5 119.3 . . ? C4 C5 H5 119.3 . . ? C5 C6 C1 120.0(2) . . ? C5 C6 H6 120.0 . . ? C1 C6 H6 120.0 . . ? C4 C7 H7A 109.5 . . ? C4 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C4 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C11 C8 C9 124.46(19) . . ? C11 C8 S1 118.22(16) . . ? C9 C8 S1 116.98(16) . . ? C10 C9 C8 114.17(19) . . ? C10 C9 H9A 108.7 . . ? C8 C9 H9A 108.7 . . ? C10 C9 H9B 108.7 . . ? C8 C9 H9B 108.7 . . ? H9A C9 H9B 107.6 . . ? F2 C10 F3 106.3(2) . . ? F2 C10 F1 106.2(2) . . ? F3 C10 F1 106.8(2) . . ? F2 C10 C9 113.92(19) . . ? F3 C10 C9 111.2(2) . . ? F1 C10 C9 111.9(2) . . ? C11 N1 C12 123.62(19) . . ? C11 N1 H1 118.2 . . ? C12 N1 H1 118.2 . . ? N1 C11 C8 127.4(2) . . ? N1 C11 H11 116.3 . . ? C8 C11 H11 116.3 . . ? N1 C12 C13 114.8(2) . . ? N1 C12 H12A 108.6 . . ? C13 C12 H12A 108.6 . . ? N1 C12 H12B 108.6 . . ? C13 C12 H12B 108.6 . . ? H12A C12 H12B 107.6 . . ? C14 C13 C18 118.6(2) . . ? C14 C13 C12 123.0(2) . . ? C18 C13 C12 118.4(2) . . ? C13 C14 C15 120.4(2) . . ? C13 C14 H14 119.8 . . ? C15 C14 H14 119.8 . . ? C16 C15 C14 120.3(3) . . ? C16 C15 H15 119.9 . . ? C14 C15 H15 119.9 . . ? C17 C16 C15 119.8(2) . . ? C17 C16 H16 120.1 . . ? C15 C16 H16 120.1 . . ? C16 C17 C18 120.4(2) . . ? C16 C17 H17 119.8 . . ? C18 C17 H17 119.8 . . ? C13 C18 C17 120.6(2) . . ? C13 C18 H18 119.7 . . ? C17 C18 H18 119.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O1 1.4379(18) . ? S1 O2 1.4476(17) . ? S1 C8 1.728(2) . ? S1 C1 1.770(2) . ? C1 C6 1.380(3) . ? C1 C2 1.395(3) . ? C2 C3 1.383(3) . ? C2 H2 0.9300 . ? C3 C4 1.396(4) . ? C3 H3 0.9300 . ? C4 C5 1.395(4) . ? C4 C7 1.505(3) . ? C5 C6 1.378(3) . ? C5 H5 0.9300 . ? C6 H6 0.9300 . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 C11 1.358(3) . ? C8 C9 1.506(3) . ? C9 C10 1.502(3) . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C10 F2 1.329(3) . ? C10 F3 1.334(3) . ? C10 F1 1.341(3) . ? N1 C11 1.339(3) . ? N1 C12 1.453(3) . ? N1 H1 0.8600 . ? C11 H11 0.9300 . ? C12 C13 1.515(3) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C13 C14 1.388(3) . ? C13 C18 1.391(3) . ? C14 C15 1.398(4) . ? C14 H14 0.9300 . ? C15 C16 1.379(4) . ? C15 H15 0.9300 . ? C16 C17 1.370(4) . ? C16 H16 0.9300 . ? C17 C18 1.395(4) . ? C17 H17 0.9300 . ? C18 H18 0.9300 . ?