#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:34:55 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296381 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572754.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572754 loop_ _publ_author_name 'Anju, Balakrishnan S.' 'Nair, Neeraja R.' 'Rajput, Janavi' 'Bertke, Jeffery A.' 'Mondal, Bhaskar' 'Kundu, Subrata' _publ_section_title ; Role of ancillary ligands in S-nitrosothiol and NO generation from nitrite-thiol interactions at mononuclear zinc(ii) sites. ; _journal_issue 43 _journal_name_full 'Chemical science' _journal_page_first 18000 _journal_page_last 18007 _journal_paper_doi 10.1039/d4sc04853a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C28 H41 N6 O P Zn, 2(Cl O4)' _chemical_formula_sum 'C28 H41 Cl2 N6 O9 P Zn' _chemical_formula_weight 772.91 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary intrinsic _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-05-16 deposited with the CCDC. 2024-10-03 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 104.442(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.9275(10) _cell_length_b 14.5700(12) _cell_length_c 20.8368(17) _cell_measurement_reflns_used 6398 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 22.92 _cell_measurement_theta_min 2.25 _cell_volume 3506.7(5) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELX-2018-3 (Sheldrick, 2015)' _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.981 _diffrn_measurement_device_type 'Bruker APEX DUO/ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0959 _diffrn_reflns_av_unetI/netI 0.0764 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.981 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 56975 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.981 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.611 _diffrn_reflns_theta_min 2.019 _exptl_absorpt_coefficient_mu 0.956 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.5761 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.464 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1608 _exptl_crystal_size_max 0.095 _exptl_crystal_size_mid 0.068 _exptl_crystal_size_min 0.048 _refine_diff_density_max 0.451 _refine_diff_density_min -0.448 _refine_diff_density_rms 0.078 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.026 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 523 _refine_ls_number_reflns 8815 _refine_ls_number_restraints 302 _refine_ls_restrained_S_all 1.027 _refine_ls_R_factor_all 0.0863 _refine_ls_R_factor_gt 0.0461 _refine_ls_shift/su_max 0.009 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0434P)^2^+0.3307P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0971 _refine_ls_wR_factor_ref 0.1117 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5898 _reflns_number_total 8815 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04853a2.cif _cod_data_source_block ABS1284 _cod_depositor_comments 'Adding full bibliography for 1572750--1572760.cif.' _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 1572754 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.915 _shelx_estimated_absorpt_t_max 0.956 _shelx_res_file ; TITL abs1284_a.res in P2(1)/c ABS1284.res created by SHELXL-2018/3 at 14:06:08 on 19-Jun-2023 REM Old TITL ABS1284 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.118, Rweak 0.007, Alpha 0.046 REM 0.612 for 301 systematic absences, Orientation as input REM Formula found by SHELXT: C28 Cl2 N6 O9 P Zn CELL 0.71073 11.9275 14.57 20.8368 90 104.442 90 ZERR 4 0.001 0.0012 0.0017 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cl N O P Zn UNIT 112 164 8 24 36 4 4 L.S. 20 PLAN 20 SIZE 0.048 0.068 0.095 TEMP -123.15 BOND $H LIST 4 SIMU 0.01 0.02 CL1 > O5' SIMU 0.01 0.02 CL2 > O9' OMIT 0 1 1 OMIT 1 0 0 CONF FMAP 2 ACTA WGHT 0.043400 0.330700 FVAR 0.26869 0.90891 0.85401 ZN1 7 0.276407 0.332261 0.630876 11.00000 0.02424 0.02250 = 0.01925 0.00143 0.00489 0.00036 P1 6 0.255070 0.094296 0.630335 11.00000 0.02450 0.02112 = 0.02760 0.00164 0.00529 -0.00146 O1 5 0.261491 0.196922 0.638370 11.00000 0.03080 0.01998 = 0.03919 0.00044 0.00524 -0.00132 N1 4 0.245339 0.421430 0.699943 11.00000 0.02811 0.02328 = 0.02216 0.00373 0.00639 0.00443 N2 4 0.290330 0.404647 0.765736 11.00000 0.02374 0.02355 = 0.02221 -0.00021 0.00799 0.00200 N3 4 0.447477 0.316852 0.695441 11.00000 0.02342 0.02393 = 0.02414 -0.00294 0.00606 -0.00113 N4 4 0.310974 0.398675 0.551685 11.00000 0.02715 0.02833 = 0.02270 0.00032 0.00731 -0.00218 N5 4 0.246220 0.377219 0.489193 11.00000 0.02466 0.02732 = 0.02180 0.00157 0.00824 0.00087 N6 4 0.097483 0.324529 0.573431 11.00000 0.02346 0.03210 = 0.02202 0.00408 0.00662 0.00268 C1 1 0.196625 0.504466 0.696625 11.00000 0.02923 0.02340 = 0.03569 0.00426 0.01338 0.00511 C2 1 0.208981 0.539564 0.760011 11.00000 0.03124 0.02485 = 0.04348 -0.00397 0.01746 0.00453 AFIX 43 H2 2 0.181350 0.597038 0.771198 11.00000 -1.20000 AFIX 0 C3 1 0.269021 0.474938 0.803485 11.00000 0.02380 0.03081 = 0.03069 -0.00528 0.01287 -0.00345 C4 1 0.140474 0.547491 0.631499 11.00000 0.05611 0.03624 = 0.04436 0.01165 0.01405 0.01865 AFIX 137 H4A 2 0.189672 0.538604 0.600712 11.00000 -1.50000 H4B 2 0.129985 0.613312 0.637743 11.00000 -1.50000 H4C 2 0.064913 0.518795 0.613298 11.00000 -1.50000 AFIX 0 C5 1 0.303728 0.473803 0.877490 11.00000 0.04052 0.05203 = 0.02971 -0.01388 0.01298 0.00100 AFIX 137 H5A 2 0.258333 0.427380 0.893923 11.00000 -1.50000 H5B 2 0.289359 0.534280 0.894419 11.00000 -1.50000 H5C 2 0.386265 0.459004 0.892681 11.00000 -1.50000 AFIX 0 C6 1 0.350711 0.318599 0.785637 11.00000 0.02521 0.02515 = 0.02360 0.00415 0.00752 0.00366 AFIX 23 H6A 2 0.298456 0.266896 0.767630 11.00000 -1.20000 H6B 2 0.370822 0.313993 0.834582 11.00000 -1.20000 AFIX 0 C7 1 0.459967 0.310439 0.761645 11.00000 0.02460 0.01707 = 0.02439 -0.00250 0.00521 -0.00136 C8 1 0.566415 0.294295 0.805301 11.00000 0.02819 0.03474 = 0.02829 -0.00212 0.00285 0.00264 AFIX 43 H8 2 0.572949 0.289631 0.851565 11.00000 -1.20000 AFIX 0 C9 1 0.662501 0.285130 0.780553 11.00000 0.02441 0.04562 = 0.04328 -0.00303 -0.00013 0.00457 AFIX 43 H9 2 0.736455 0.274895 0.809735 11.00000 -1.20000 AFIX 0 C10 1 0.650936 0.290859 0.713399 11.00000 0.02446 0.05179 = 0.04762 -0.00754 0.01433 0.00584 AFIX 43 H10 2 0.716309 0.284008 0.695484 11.00000 -1.20000 AFIX 0 C11 1 0.542157 0.306809 0.672387 11.00000 0.03026 0.03715 = 0.03245 -0.00591 0.01206 -0.00012 AFIX 43 H11 2 0.534220 0.310812 0.625961 11.00000 -1.20000 AFIX 0 C12 1 0.361453 0.478966 0.545704 11.00000 0.03135 0.02809 = 0.03076 -0.00026 0.01445 -0.00277 C13 1 0.330940 0.507808 0.479994 11.00000 0.03624 0.03165 = 0.03794 0.00913 0.01669 -0.00284 AFIX 43 H13 2 0.355546 0.562320 0.462538 11.00000 -1.20000 AFIX 0 C14 1 0.257865 0.441528 0.445229 11.00000 0.02868 0.03619 = 0.02635 0.00767 0.01193 0.00328 C15 1 0.438126 0.526539 0.603872 11.00000 0.04617 0.03729 = 0.03944 -0.00424 0.01197 -0.01726 AFIX 137 H15A 2 0.397960 0.531785 0.639403 11.00000 -1.50000 H15B 2 0.457221 0.587964 0.590624 11.00000 -1.50000 H15C 2 0.509481 0.491068 0.619738 11.00000 -1.50000 AFIX 0 C16 1 0.202139 0.433567 0.372790 11.00000 0.04836 0.06099 = 0.02935 0.01510 0.00942 -0.00431 AFIX 137 H16A 2 0.239304 0.384107 0.353776 11.00000 -1.50000 H16B 2 0.210916 0.491603 0.350773 11.00000 -1.50000 H16C 2 0.119652 0.419771 0.366315 11.00000 -1.50000 AFIX 0 C17 1 0.177878 0.293099 0.479553 11.00000 0.02882 0.02646 = 0.02384 0.00059 0.00775 -0.00207 AFIX 23 H17A 2 0.227860 0.241245 0.499917 11.00000 -1.20000 H17B 2 0.150385 0.280641 0.431477 11.00000 -1.20000 AFIX 0 C18 1 0.074898 0.298187 0.509286 11.00000 0.02465 0.02221 = 0.02583 0.00563 0.00681 0.00317 C19 1 -0.035502 0.274164 0.473879 11.00000 0.02812 0.03306 = 0.02761 0.00384 0.00281 0.00149 AFIX 43 H19 2 -0.048974 0.254793 0.429067 11.00000 -1.20000 AFIX 0 C20 1 -0.125994 0.278600 0.504278 11.00000 0.01907 0.04026 = 0.04293 0.00285 0.00227 0.00004 AFIX 43 H20 2 -0.202493 0.262996 0.480654 11.00000 -1.20000 AFIX 0 C21 1 -0.102963 0.306139 0.569606 11.00000 0.02839 0.04801 = 0.03693 0.00676 0.01230 0.00307 AFIX 43 H21 2 -0.163432 0.309547 0.591785 11.00000 -1.20000 AFIX 0 C22 1 0.009340 0.328718 0.602376 11.00000 0.03172 0.03872 = 0.02912 0.00513 0.01007 0.00236 AFIX 43 H22 2 0.024500 0.347991 0.647277 11.00000 -1.20000 AFIX 0 C23 1 0.396742 0.043343 0.651940 11.00000 0.03507 0.02997 = 0.03793 0.00479 0.01232 0.00561 AFIX 23 H23A 2 0.389894 -0.022656 0.640320 11.00000 -1.20000 H23B 2 0.445112 0.072571 0.625368 11.00000 -1.20000 AFIX 0 C24 1 0.456998 0.053045 0.725097 11.00000 0.03720 0.03888 = 0.04497 0.00057 -0.00397 0.00950 AFIX 137 H24A 2 0.537233 0.031836 0.732825 11.00000 -1.50000 H24B 2 0.416344 0.015951 0.751408 11.00000 -1.50000 H24C 2 0.456239 0.117599 0.738191 11.00000 -1.50000 AFIX 0 C25 1 0.189859 0.061425 0.546627 11.00000 0.03741 0.03191 = 0.03390 -0.00047 0.00433 -0.00556 AFIX 23 H25A 2 0.116546 0.095878 0.531120 11.00000 -1.20000 H25B 2 0.241893 0.080164 0.518648 11.00000 -1.20000 AFIX 0 C26 1 0.163698 -0.041536 0.535759 11.00000 0.05021 0.04020 = 0.04965 -0.01418 0.00749 -0.00830 AFIX 137 H26A 2 0.130114 -0.053140 0.488543 11.00000 -1.50000 H26B 2 0.108712 -0.060450 0.561197 11.00000 -1.50000 H26C 2 0.235592 -0.076645 0.550611 11.00000 -1.50000 AFIX 0 C27 1 0.172273 0.045277 0.682515 11.00000 0.03780 0.03828 = 0.03857 0.00212 0.01718 -0.00596 AFIX 23 H27A 2 0.170772 -0.022247 0.677072 11.00000 -1.20000 H27B 2 0.211122 0.059024 0.729308 11.00000 -1.20000 AFIX 0 C28 1 0.048796 0.080487 0.667726 11.00000 0.05063 0.05258 = 0.08834 0.00698 0.04154 0.00132 AFIX 137 H28A 2 0.009139 0.066025 0.621734 11.00000 -1.50000 H28B 2 0.049429 0.147119 0.674226 11.00000 -1.50000 H28C 2 0.008043 0.051064 0.697663 11.00000 -1.50000 AFIX 0 PART 1 21 CL1 3 0.513219 0.213245 0.491020 21.00000 0.03345 0.03386 = 0.02919 -0.00654 0.01405 -0.00609 O2 5 0.601937 0.271313 0.528984 21.00000 0.04632 0.06531 = 0.05826 -0.02046 0.01915 -0.03090 O3 5 0.444063 0.178587 0.532432 21.00000 0.04841 0.06521 = 0.04791 0.00643 0.02303 -0.01904 O4 5 0.564034 0.140601 0.462284 21.00000 0.07319 0.05871 = 0.05507 -0.01731 0.02107 0.02267 O5 5 0.440153 0.266185 0.438291 21.00000 0.06003 0.05066 = 0.04210 0.00575 0.01049 0.01092 PART 2 -21 SAME 0.01 CL1 > O5 CL1' 3 0.531340 0.200697 0.493398 -21.00000 0.04460 0.05425 = 0.04334 0.00719 0.02273 -0.01403 O2' 5 0.624785 0.224253 0.548508 -21.00000 0.02948 0.05197 = 0.03700 -0.01826 0.01456 -0.01898 O3' 5 0.433483 0.174828 0.517396 -21.00000 0.02429 0.05956 = 0.03594 -0.00106 0.01737 -0.01206 O4' 5 0.563735 0.129280 0.455210 -21.00000 0.05039 0.04601 = 0.04436 -0.00350 0.02308 0.00005 O5' 5 0.498791 0.280461 0.451790 -21.00000 0.05896 0.05102 = 0.05137 0.01594 0.01569 -0.01005 PART 0 PART 1 31 CL2 3 0.001248 0.309324 0.793751 31.00000 0.02659 0.02989 = 0.03891 0.00357 0.01530 -0.00269 O6 5 0.035133 0.360011 0.854763 31.00000 0.10768 0.05132 = 0.04808 0.00113 -0.00126 -0.02574 O7 5 -0.064429 0.231809 0.804619 31.00000 0.04407 0.05062 = 0.06219 0.00486 0.02101 -0.02085 O8 5 0.101254 0.278716 0.774673 31.00000 0.03623 0.08233 = 0.11044 0.02473 0.04141 0.01556 O9 5 -0.064956 0.366554 0.742888 31.00000 0.05617 0.05687 = 0.03862 0.01021 0.01197 0.01810 PART 2 -31 SAME 0.01 CL2 > O9 CL2' 3 0.002689 0.304921 0.793334 -31.00000 0.05359 0.04670 = 0.04612 0.01703 -0.00437 -0.00002 O6' 5 -0.039510 0.336345 0.848697 -31.00000 0.07302 0.04972 = 0.03963 -0.00309 0.03105 0.02097 O7' 5 -0.074863 0.235687 0.761134 -31.00000 0.04662 0.04844 = 0.08602 -0.00921 0.00725 -0.01295 O8' 5 0.117528 0.273886 0.815583 -31.00000 0.04238 0.06302 = 0.05017 0.03373 -0.00076 0.00314 O9' 5 -0.001734 0.382453 0.750411 -31.00000 0.03328 0.05595 = 0.04399 0.01858 0.02002 0.00966 PART 0 HKLF 4 REM abs1284_a.res in P2(1)/c REM wR2 = 0.111669, GooF = S = 1.02647, Restrained GooF = 1.02664 for all data REM R1 = 0.046067 for 5898 Fo > 4sig(Fo) and 0.086251 for all 8815 data REM 523 parameters refined using 302 restraints END WGHT 0.0436 0.3310 REM Highest difference peak 0.451, deepest hole -0.448, 1-sigma level 0.078 Q1 1 0.1967 0.0769 0.6515 11.00000 0.05 0.45 Q2 1 0.5134 0.1588 0.5325 11.00000 0.05 0.38 Q3 1 0.0969 0.3365 0.8367 11.00000 0.05 0.36 Q4 1 0.2772 0.3729 0.5831 11.00000 0.05 0.36 Q5 1 0.0380 0.2784 0.7784 11.00000 0.05 0.34 Q6 1 -0.0821 0.3083 0.8171 11.00000 0.05 0.34 Q7 1 0.2515 0.3991 0.7284 11.00000 0.05 0.33 Q8 1 0.2315 0.1788 0.6126 11.00000 0.05 0.33 Q9 1 0.2077 0.3402 0.6419 11.00000 0.05 0.33 Q10 1 0.0687 0.5761 0.6334 11.00000 0.05 0.33 Q11 1 0.2387 0.1523 0.6468 11.00000 0.05 0.32 Q12 1 0.3307 0.0647 0.6600 11.00000 0.05 0.32 Q13 1 0.3595 0.4815 0.5089 11.00000 0.05 0.32 Q14 1 0.3757 0.3140 0.6894 11.00000 0.05 0.32 Q15 1 0.0736 0.2378 0.7402 11.00000 0.05 0.32 Q16 1 0.2532 0.0577 0.5794 11.00000 0.05 0.31 Q17 1 0.5724 0.2574 0.4976 11.00000 0.05 0.31 Q18 1 0.1762 0.6053 0.6130 11.00000 0.05 0.31 Q19 1 0.4137 0.3031 0.7656 11.00000 0.05 0.30 Q20 1 -0.0659 0.2467 0.4991 11.00000 0.05 0.29 ; _shelx_res_checksum 25618 _shelx_hkl_file ; 1 0 0 4.00 1.70 -2 0 0 57.79 6.10 -2 0 0 55.69 5.70 -2 0 0 68.49 5.80 2 0 0 59.59 8.90 -2 0 0 59.69 8.90 -2 0 0 61.39 5.30 2 0 0 58.79 5.80 2 0 0 47.50 5.60 2 0 0 54.29 5.60 2 0 0 60.09 5.30 3 0 0 62.39 7.40 -3 0 0 86.29 8.20 -3 0 0 75.59 8.00 -3 0 0 67.59 11.30 -3 0 0 70.59 7.90 3 0 0 67.89 11.40 3 0 0 76.19 6.90 3 0 0 68.79 7.60 3 0 0 73.39 8.00 4 0 0 3613.74 270.97 4 0 0 3683.53 270.27 4 0 0 3606.14 276.27 -4 0 0 3858.41 276.77 -4 0 0 3467.35 271.17 -4 0 0 3546.75 271.07 -4 0 0 3659.83 271.07 4 0 0 3584.54 271.17 4 0 0 3764.92 271.27 5 0 0 253.17 20.50 -5 0 0 253.07 22.30 5 0 0 223.28 21.50 5 0 0 241.18 21.40 5 0 0 285.37 22.80 6 0 0 514.15 39.90 6 0 0 500.25 41.40 6 0 0 513.75 41.10 -6 0 0 509.15 41.60 7 0 0 710.03 56.79 -7 0 0 655.03 57.09 7 0 0 757.52 57.49 7 0 0 732.93 55.49 8 0 0 81.19 12.90 -8 0 0 68.79 12.00 8 0 0 93.49 12.80 -9 0 0 16.30 8.00 9 0 0 18.50 7.80 9 0 0 -1.20 7.10 10 0 0 19.00 8.10 10 0 0 18.60 9.40 -10 0 0 28.40 10.40 -11 0 0 661.03 59.19 11 0 0 684.43 57.79 11 0 0 717.63 59.19 12 0 0 46.30 13.20 -12 0 0 74.09 15.90 12 0 0 51.99 12.40 13 0 0 77.49 16.40 13 0 0 59.29 15.30 -13 0 0 85.69 18.70 14 0 0 8.60 10.60 -14 0 0 17.30 13.20 14 0 0 13.30 12.30 -15 0 0 55.59 18.80 15 0 0 69.69 18.80 15 0 0 62.59 16.00 0 -1 0 1.20 1.10 0 -1 0 -0.40 0.70 0 -1 0 0.20 0.80 0 -1 0 0.10 0.30 0 1 0 1.10 0.60 0 1 0 0.10 0.60 0 1 0 0.00 0.60 0 1 0 -1.00 0.40 1 -1 0 3812.82 250.87 -1 -1 0 3061.19 251.17 1 -1 0 3468.35 251.07 -1 1 0 3733.33 250.97 1 1 0 2875.51 250.97 -2 -1 0 8.80 2.20 2 -1 0 9.60 2.30 2 -1 0 7.80 2.00 2 -1 0 4.00 3.90 2 -1 0 11.30 2.30 -2 -1 0 10.40 2.30 -2 -1 0 16.90 3.10 2 -1 0 14.50 2.40 2 1 0 11.00 2.30 2 1 0 9.70 2.40 -2 1 0 14.30 2.30 -2 1 0 11.50 2.50 -2 1 0 6.90 4.10 -2 1 0 8.20 2.10 2 1 0 6.60 2.20 -2 1 0 12.00 2.40 3 -1 0 2922.71 221.68 3 -1 0 2954.90 221.48 3 -1 0 2974.10 221.88 -3 -1 0 3120.49 225.58 -3 -1 0 2957.60 221.98 3 -1 0 2916.71 221.68 -3 -1 0 2868.51 221.68 -3 -1 0 2966.60 222.18 -3 1 0 2962.90 221.48 -3 1 0 3274.97 226.98 -3 1 0 3061.59 221.88 3 1 0 3017.30 222.08 3 1 0 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14.70 9.40 -10 5 0 28.00 9.90 -10 5 0 20.40 7.60 10 5 0 9.50 8.00 11 -5 0 0.40 12.70 11 -5 0 26.00 10.40 -11 -5 0 12.10 10.60 11 -5 0 10.20 9.00 11 5 0 17.50 10.00 -11 5 0 12.30 9.80 11 5 0 12.10 8.60 12 -5 0 15.50 10.50 12 -5 0 27.70 11.60 -12 -5 0 12.90 10.50 12 5 0 17.90 10.10 12 5 0 14.60 10.70 -12 5 0 41.00 13.20 13 -5 0 16.70 11.60 13 -5 0 23.90 12.40 -13 -5 0 24.50 12.80 -13 5 0 31.40 13.20 13 5 0 35.10 14.60 13 5 0 31.80 11.40 14 -5 0 -2.40 10.40 14 -5 0 2.80 12.20 -14 -5 0 17.50 13.20 14 5 0 12.00 11.00 -14 5 0 -0.40 12.90 14 5 0 0.20 11.60 0 -6 0 602.44 47.70 0 -6 0 493.55 41.00 0 -6 0 459.65 41.20 0 6 0 485.65 41.30 0 6 0 507.95 40.80 0 6 0 591.94 46.50 0 6 0 520.65 41.20 -1 -6 0 70.29 8.30 1 -6 0 60.39 14.10 -1 -6 0 70.29 8.00 -1 -6 0 74.59 14.50 1 -6 0 63.99 9.00 -1 -6 0 62.09 8.60 -1 -6 0 65.19 8.70 1 6 0 72.69 9.10 1 6 0 65.99 8.90 -1 6 0 74.89 8.60 -1 6 0 72.09 14.00 1 6 0 61.29 11.80 -1 6 0 56.69 7.30 -1 6 0 72.09 9.30 -2 -6 0 74.19 8.70 -2 -6 0 106.49 10.90 2 -6 0 88.09 10.70 2 -6 0 85.69 8.80 -2 -6 0 91.39 10.80 -2 -6 0 71.99 14.20 2 -6 0 82.69 17.30 -2 6 0 75.29 8.10 2 6 0 93.49 9.80 2 6 0 83.49 10.20 -2 6 0 66.89 9.60 -2 6 0 55.69 13.50 3 -6 0 274.17 22.10 -3 -6 0 292.97 22.20 -3 -6 0 198.58 27.60 3 -6 0 221.78 30.00 3 -6 0 263.77 23.70 -3 -6 0 298.27 24.50 3 6 0 269.57 23.30 -3 6 0 283.37 21.50 -3 6 0 279.77 23.90 3 6 0 296.87 22.50 4 -6 0 97.29 11.80 -4 -6 0 86.99 8.60 4 -6 0 71.49 17.50 4 -6 0 79.49 8.80 4 -6 0 74.99 7.60 -4 -6 0 62.89 10.60 4 6 0 75.89 8.70 4 6 0 73.59 10.10 -4 6 0 74.39 8.50 -4 6 0 91.59 11.10 5 -6 0 32.80 6.20 -5 -6 0 33.40 8.10 5 -6 0 44.60 8.10 5 -6 0 40.20 15.20 5 -6 0 46.90 5.00 5 6 0 30.00 7.10 5 6 0 39.20 5.90 -5 6 0 46.10 6.30 -5 6 0 42.30 7.20 5 6 0 29.20 6.80 -5 6 0 42.00 8.10 6 -6 0 17.80 3.60 6 -6 0 19.70 7.30 6 -6 0 8.60 5.20 6 -6 0 8.70 11.60 -6 -6 0 12.30 7.00 -6 6 0 16.40 6.30 6 6 0 25.10 7.40 -6 6 0 15.10 5.80 6 6 0 17.70 5.80 6 6 0 19.20 4.10 7 -6 0 394.36 32.30 7 -6 0 393.66 29.50 7 -6 0 351.56 43.90 7 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11.60 13 6 0 13.40 12.30 13 6 0 20.80 11.90 14 -6 0 62.09 16.90 -14 -6 0 74.99 19.80 14 -6 0 100.29 21.90 14 6 0 92.39 19.20 -14 6 0 89.59 20.00 14 6 0 79.69 17.20 0 -7 0 13.00 4.60 0 -7 0 3.70 8.00 0 7 0 7.60 4.50 0 7 0 -1.70 3.60 0 7 0 -0.40 4.80 0 7 0 10.80 3.80 1 -7 0 220.48 27.60 -1 -7 0 249.58 22.00 1 -7 0 267.27 22.50 -1 -7 0 268.47 21.50 -1 -7 0 261.77 22.50 -1 -7 0 222.48 27.70 -1 7 0 229.68 27.40 -1 7 0 249.58 21.50 1 7 0 186.88 24.40 -1 7 0 266.27 22.50 -1 7 0 283.07 21.20 1 7 0 292.07 22.20 2 -7 0 145.39 23.30 2 -7 0 123.69 11.80 -2 -7 0 137.09 12.20 -2 -7 0 111.19 18.80 2 -7 0 122.99 14.20 -2 -7 0 112.59 13.90 -2 7 0 112.69 11.30 -2 7 0 127.79 14.60 2 7 0 131.39 12.60 2 7 0 121.19 13.50 -3 -7 0 3.30 7.30 3 -7 0 16.80 10.90 3 -7 0 10.60 3.90 -3 -7 0 23.30 4.50 -3 -7 0 15.70 5.70 3 7 0 20.60 5.30 -3 7 0 25.50 4.10 -3 7 0 23.10 6.40 3 7 0 27.80 5.30 4 -7 0 149.29 13.80 4 -7 0 142.79 16.50 -4 -7 0 138.69 13.30 -4 -7 0 107.89 15.70 4 -7 0 146.49 26.40 4 7 0 155.08 16.60 4 7 0 173.48 14.10 -4 7 0 146.29 12.60 -4 7 0 168.68 17.50 5 -7 0 86.69 21.40 5 -7 0 117.69 14.10 5 -7 0 92.99 10.60 5 -7 0 89.19 8.40 -5 -7 0 62.89 11.40 5 7 0 90.89 10.00 -5 7 0 129.29 14.40 -5 7 0 94.69 10.10 5 7 0 96.39 12.90 -5 7 0 72.39 10.70 6 -7 0 29.80 4.20 -6 -7 0 29.50 8.40 6 -7 0 11.50 6.60 6 -7 0 33.50 16.80 6 -7 0 25.40 6.60 6 7 0 43.00 8.80 6 7 0 20.30 7.40 -6 7 0 26.60 7.00 -6 7 0 34.10 7.50 6 7 0 29.10 5.60 7 -7 0 2.90 6.70 7 -7 0 1.60 2.90 7 -7 0 -2.60 5.00 7 -7 0 12.30 14.50 -7 -7 0 5.20 5.80 -7 7 0 -5.90 5.30 7 7 0 -2.40 3.40 -7 7 0 -1.30 4.90 7 7 0 -2.00 5.30 7 7 0 -0.40 5.60 8 -7 0 108.79 27.50 -8 -7 0 103.19 16.40 8 -7 0 112.39 14.70 8 -7 0 133.89 17.40 8 7 0 111.39 11.40 -8 7 0 97.89 14.60 8 7 0 101.09 15.70 -8 7 0 109.39 16.00 8 7 0 135.99 16.30 9 -7 0 -3.20 15.40 9 -7 0 -4.30 7.30 -9 -7 0 1.00 7.00 9 -7 0 -7.40 6.10 9 7 0 15.70 8.20 9 7 0 -0.30 6.30 -9 7 0 1.00 6.00 -9 7 0 2.60 7.40 10 -7 0 151.38 37.80 -10 -7 0 167.68 25.30 10 -7 0 261.77 27.50 10 -7 0 227.28 24.20 10 7 0 200.48 25.50 10 7 0 211.08 24.40 -10 7 0 251.37 26.40 -10 7 0 220.68 24.80 11 -7 0 26.40 11.70 11 -7 0 17.10 10.20 -11 -7 0 29.70 12.80 11 -7 0 24.50 22.10 11 7 0 7.60 9.40 11 7 0 16.00 9.80 -11 7 0 15.50 10.20 -11 7 0 15.10 8.30 12 -7 0 76.59 30.60 12 -7 0 93.49 18.60 12 -7 0 120.69 18.50 -12 -7 0 141.29 23.40 12 7 0 85.29 16.50 -12 7 0 101.29 18.10 12 7 0 94.29 18.00 -13 -7 0 26.20 14.00 13 -7 0 32.30 19.30 13 -7 0 41.50 14.20 -13 7 0 43.70 15.00 13 7 0 37.90 13.00 13 7 0 34.80 12.90 14 -7 0 8.80 11.70 -14 -7 0 18.50 14.10 14 7 0 20.00 12.10 0 -8 0 2097.29 164.18 0 -8 0 1984.10 156.88 0 8 0 2123.39 156.88 0 8 0 2083.99 156.08 -1 -8 0 -1.30 3.30 1 -8 0 -5.80 3.50 -1 -8 0 2.00 7.50 -1 -8 0 5.00 4.60 1 -8 0 2.80 8.40 -1 8 0 6.10 5.00 -1 8 0 -1.20 2.70 1 8 0 -3.20 3.50 1 8 0 6.10 6.50 1 8 0 3.40 4.00 2 -8 0 4.50 3.40 -2 -8 0 3.30 4.00 -2 -8 0 15.00 8.90 -2 -8 0 1.10 3.90 2 -8 0 -2.00 3.70 2 -8 0 2.60 9.20 2 8 0 4.50 4.20 -2 8 0 11.50 5.50 -2 8 0 0.60 2.40 3 -8 0 23.80 12.60 -3 -8 0 27.70 11.70 3 -8 0 18.50 6.00 3 -8 0 14.90 4.40 -3 -8 0 23.80 6.90 3 8 0 23.90 5.40 3 8 0 10.70 5.30 -3 8 0 13.80 6.10 -3 8 0 14.70 3.70 4 -8 0 314.07 25.80 4 -8 0 310.17 28.30 -4 -8 0 360.46 27.20 -4 -8 0 314.87 28.60 4 -8 0 286.57 37.50 -4 -8 0 265.87 33.70 4 8 0 343.67 26.50 -4 8 0 310.17 28.30 4 8 0 319.57 27.70 -4 8 0 298.77 24.90 5 -8 0 7.80 4.60 -5 -8 0 -0.70 2.70 -5 -8 0 -0.60 4.60 5 -8 0 2.40 11.70 5 -8 0 5.70 5.80 -5 8 0 -0.40 4.50 5 8 0 -1.00 4.50 5 8 0 -4.80 3.70 -5 8 0 -8.20 3.60 -6 -8 0 -7.10 5.10 6 -8 0 5.20 6.00 6 -8 0 -4.60 12.40 6 -8 0 -1.10 4.80 6 8 0 -0.90 4.00 -6 8 0 -0.70 5.10 6 8 0 8.40 5.50 -6 8 0 -1.90 4.90 7 -8 0 240.68 26.30 7 -8 0 180.48 36.70 7 -8 0 229.98 22.30 -7 -8 0 227.38 26.40 7 8 0 249.97 23.70 -7 8 0 293.27 27.90 7 8 0 243.18 20.60 -7 8 0 213.98 23.20 8 -8 0 48.80 20.40 8 -8 0 60.19 10.60 8 -8 0 53.39 11.70 -8 -8 0 44.70 12.30 8 8 0 42.30 10.50 -8 8 0 49.50 10.40 -8 8 0 67.49 12.40 8 8 0 57.69 7.60 9 -8 0 -3.30 6.80 9 -8 0 7.20 18.50 9 -8 0 10.60 7.30 -9 -8 0 -1.10 7.80 -9 8 0 6.60 6.70 -9 8 0 -6.00 6.70 9 8 0 13.30 7.40 10 -8 0 3.60 17.60 10 -8 0 -0.70 8.10 10 -8 0 5.20 7.80 -10 -8 0 1.10 8.20 -10 8 0 9.60 7.40 -10 8 0 4.20 8.50 10 8 0 -2.20 7.30 11 -8 0 273.37 27.80 -11 -8 0 199.88 28.80 11 -8 0 253.87 28.80 11 -8 0 175.38 43.40 -11 8 0 269.77 28.60 -11 8 0 261.57 28.40 11 8 0 236.18 28.80 12 -8 0 9.80 18.80 12 -8 0 -2.60 10.00 -12 -8 0 -11.20 10.00 12 8 0 3.20 9.70 -12 8 0 8.40 8.00 -12 8 0 9.50 10.50 13 -8 0 -11.60 16.30 13 -8 0 -3.50 10.00 -13 -8 0 13.00 13.00 13 8 0 4.80 10.60 14 -8 0 16.60 13.30 -14 -8 0 -5.50 13.40 14 8 0 28.70 12.90 0 -9 0 61.89 16.10 0 9 0 56.19 9.50 1 -9 0 414.06 36.20 1 -9 0 347.07 42.50 -1 -9 0 448.66 36.20 -1 -9 0 417.76 43.20 -1 -9 0 458.95 36.80 1 9 0 382.76 35.40 -1 9 0 453.15 34.90 -1 9 0 409.86 36.20 1 9 0 500.95 36.10 -2 -9 0 48.90 9.00 2 -9 0 43.80 15.20 2 -9 0 36.80 8.10 -2 -9 0 56.19 9.10 -2 -9 0 37.50 13.60 2 -9 0 46.70 6.90 -2 9 0 45.60 8.80 2 9 0 40.80 8.10 2 9 0 38.70 8.20 -2 9 0 36.70 6.50 3 -9 0 25.10 7.90 -3 -9 0 20.20 7.00 3 -9 0 46.50 17.30 -3 -9 0 38.60 13.70 3 -9 0 22.00 5.30 3 9 0 32.20 6.80 -3 9 0 27.40 5.10 -3 9 0 27.00 8.00 -4 -9 0 2.20 11.40 4 -9 0 3.30 12.50 4 -9 0 2.20 4.20 4 -9 0 0.30 5.00 -4 -9 0 -2.00 5.30 -4 9 0 10.50 5.90 4 9 0 1.60 5.00 -4 9 0 1.80 2.90 4 9 0 4.30 5.40 -5 -9 0 116.79 25.50 5 -9 0 203.48 21.50 -5 -9 0 130.89 18.90 5 -9 0 131.29 29.50 5 -9 0 187.78 16.20 5 9 0 174.28 19.70 -5 9 0 199.68 21.30 5 9 0 167.68 16.20 -6 -9 0 2.60 6.00 6 -9 0 -2.80 4.90 -6 -9 0 -2.10 11.70 6 -9 0 3.80 6.80 6 -9 0 4.40 13.80 -6 9 0 -1.90 5.80 6 9 0 5.60 4.90 -6 9 0 1.30 5.60 6 9 0 -8.40 4.70 7 -9 0 23.00 7.30 7 -9 0 21.00 9.70 -7 -9 0 12.40 7.70 7 -9 0 14.00 16.90 7 9 0 28.30 8.60 -7 9 0 10.00 7.00 7 9 0 14.30 5.80 -7 9 0 15.20 8.00 8 -9 0 0.00 6.40 -8 -9 0 -1.10 7.10 8 -9 0 11.80 17.70 8 -9 0 27.60 9.90 -8 9 0 3.30 7.00 -8 9 0 0.20 5.40 8 9 0 10.30 7.40 9 -9 0 -0.40 7.50 -9 -9 0 0.80 8.40 9 -9 0 6.50 16.20 9 -9 0 2.90 7.10 -9 9 0 4.50 7.60 9 9 0 7.90 7.80 -9 9 0 -0.40 5.60 -10 -9 0 -1.50 9.10 10 -9 0 0.40 8.90 10 -9 0 1.60 8.30 10 -9 0 1.70 15.20 -10 9 0 11.50 9.10 -10 9 0 -3.20 7.00 10 9 0 8.40 8.50 11 -9 0 41.80 27.00 -11 -9 0 30.10 13.20 11 -9 0 25.60 12.60 -11 9 0 31.10 12.00 -11 9 0 23.80 10.00 11 9 0 32.10 11.50 12 -9 0 7.30 10.80 -12 -9 0 20.30 12.00 12 -9 0 1.40 20.40 -12 9 0 4.30 8.30 12 9 0 9.30 9.90 -13 -9 0 -6.80 10.80 13 -9 0 12.30 24.40 13 -9 0 -3.70 11.40 13 9 0 -15.60 8.80 0 -10 0 330.07 38.30 0 -10 0 318.47 29.70 0 10 0 353.06 29.90 0 10 0 314.57 28.40 -1 -10 0 9.20 11.70 -1 -10 0 17.60 7.50 1 -10 0 24.70 13.70 1 -10 0 36.00 8.20 1 10 0 41.00 7.90 -1 10 0 37.10 8.10 1 10 0 43.70 8.40 -1 10 0 31.10 6.20 -2 -10 0 33.70 8.20 -2 -10 0 52.59 16.60 -2 -10 0 34.10 8.30 2 -10 0 34.20 8.60 2 -10 0 52.89 18.50 2 -10 0 18.40 5.90 2 10 0 33.30 7.50 -2 10 0 28.70 8.70 2 10 0 27.40 7.80 -2 10 0 33.00 6.00 3 -10 0 18.20 7.30 3 -10 0 10.50 14.00 -3 -10 0 17.20 12.20 3 -10 0 26.80 5.80 -3 -10 0 25.10 7.70 -3 -10 0 28.20 8.50 -3 10 0 18.30 4.80 3 10 0 24.50 7.10 -3 10 0 23.90 8.10 4 -10 0 158.08 15.00 -4 -10 0 114.79 24.00 4 -10 0 110.99 27.90 -4 -10 0 159.48 19.90 4 -10 0 143.19 18.70 -4 10 0 151.38 18.80 4 10 0 155.58 18.10 4 10 0 120.79 15.50 -4 10 0 144.09 13.20 -5 -10 0 -0.20 12.90 5 -10 0 21.90 9.40 5 -10 0 10.10 15.90 5 -10 0 39.60 7.20 -5 -10 0 23.10 8.80 -5 10 0 26.80 9.10 5 10 0 18.70 8.20 5 10 0 29.80 7.40 6 -10 0 35.30 10.70 -6 -10 0 47.30 10.90 6 -10 0 60.79 23.60 -6 -10 0 32.80 16.80 6 -10 0 22.30 7.20 6 10 0 34.30 7.60 6 10 0 23.90 8.40 -6 10 0 27.40 8.40 -6 10 0 23.20 8.00 -7 -10 0 2.70 13.60 7 -10 0 0.80 5.90 -7 -10 0 8.10 7.70 7 -10 0 -0.70 7.30 7 -10 0 1.40 17.00 -7 10 0 12.40 7.10 -7 10 0 14.60 8.20 7 10 0 5.60 6.60 7 10 0 0.90 5.10 8 -10 0 61.09 13.50 8 -10 0 42.40 9.70 -8 -10 0 53.49 13.40 8 -10 0 17.10 19.50 -8 10 0 54.69 11.60 8 10 0 45.40 11.20 -8 10 0 42.50 9.90 9 -10 0 92.29 14.10 -9 -10 0 89.59 18.20 9 -10 0 96.29 30.40 9 -10 0 55.09 14.00 9 10 0 85.29 15.30 -9 10 0 103.69 16.90 -9 10 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10.40 4.10 -3 11 0 4.90 6.40 3 11 0 -4.10 4.80 -4 -11 0 2.00 5.90 4 -11 0 9.40 15.00 4 -11 0 4.80 6.80 -4 -11 0 3.50 12.80 4 -11 0 8.60 5.40 -4 11 0 1.70 7.00 -4 11 0 4.80 3.70 4 11 0 -2.30 6.30 4 11 0 2.30 6.30 5 -11 0 93.99 27.40 -5 -11 0 70.79 13.60 5 -11 0 94.89 15.10 -5 -11 0 64.29 20.50 5 -11 0 76.69 11.00 -5 11 0 94.99 9.90 5 11 0 77.39 13.60 -5 11 0 106.79 15.90 5 11 0 102.69 13.10 -6 -11 0 85.99 15.60 -6 -11 0 69.59 22.20 6 -11 0 99.39 16.10 6 -11 0 101.59 30.40 6 -11 0 83.69 11.70 6 11 0 74.59 14.00 -6 11 0 79.79 12.60 6 11 0 108.59 13.10 -6 11 0 92.59 14.90 -7 -11 0 23.90 9.70 -7 -11 0 -1.90 14.40 7 -11 0 8.10 6.70 7 -11 0 18.50 19.50 7 -11 0 7.70 8.30 7 11 0 16.60 8.40 -7 11 0 15.50 9.00 -7 11 0 41.20 9.30 7 11 0 12.30 6.60 8 -11 0 5.50 8.80 8 -11 0 -7.90 17.60 -8 -11 0 -11.70 14.20 -8 -11 0 13.70 9.00 8 11 0 -10.20 6.70 -8 11 0 -1.70 7.30 -8 11 0 9.50 8.00 9 -11 0 -10.90 19.50 9 -11 0 10.40 9.60 -9 -11 0 7.10 16.10 -9 -11 0 2.80 8.90 -9 11 0 8.60 8.50 -9 11 0 -8.90 7.70 9 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8.50 8.90 6 -14 -3 0.90 8.70 -6 -14 3 6.70 18.80 6 -14 -3 4.00 20.40 -6 -14 3 14.10 9.40 -6 -14 3 5.70 8.90 -6 14 3 2.70 7.90 6 14 -3 -4.40 7.50 5 -14 -3 11.80 9.60 -5 -14 3 18.70 8.70 5 -14 -3 16.10 20.30 -5 -14 3 0.10 17.80 -5 -14 3 9.70 9.40 -5 14 3 12.90 9.60 5 14 -3 0.00 8.00 5 14 -3 11.40 8.80 -4 -14 3 17.80 18.20 -4 -14 3 25.20 11.50 4 -14 -3 28.00 10.90 4 -14 -3 31.60 20.70 -4 -14 3 18.40 8.80 4 14 -3 20.90 9.80 -4 14 3 55.49 13.30 4 14 -3 19.80 9.30 3 -14 -3 5.50 15.20 -3 -14 3 26.50 11.30 -3 -14 3 33.30 9.40 -3 -14 3 0.10 15.70 3 -14 -3 14.20 9.60 -3 14 3 11.10 5.40 3 14 -3 34.10 9.90 3 14 -3 13.00 8.50 -3 14 3 21.60 10.20 2 -14 -3 -5.40 7.00 -2 -14 3 -13.70 14.10 2 -14 -3 -1.10 15.10 -2 -14 3 3.90 7.90 2 14 -3 10.80 7.00 -2 14 3 -0.20 6.90 2 14 -3 3.30 8.30 -2 14 3 -4.90 4.20 1 -14 -3 99.39 17.00 -1 -14 3 115.19 17.70 1 -14 -3 95.09 25.80 -1 -14 3 68.39 25.90 1 14 -3 111.09 16.80 -1 14 3 111.79 14.30 -1 14 3 74.49 15.20 1 14 -3 111.19 15.70 0 -14 -3 84.19 15.30 0 -14 3 74.39 14.70 0 -14 3 84.99 27.20 0 -14 -3 61.89 22.10 0 14 3 63.89 13.10 0 14 3 57.59 11.30 0 14 -3 61.99 12.10 0 14 -3 68.69 14.10 1 -14 3 38.70 9.50 -1 -14 -3 34.20 17.70 -1 -14 -3 27.50 10.80 1 -14 3 40.90 11.20 1 -14 3 51.69 23.60 -1 14 -3 32.60 8.60 1 14 3 32.50 9.20 1 14 3 34.70 11.30 -1 14 -3 35.40 11.50 2 -14 3 5.70 7.20 2 -14 3 -2.00 16.50 -2 -14 -3 1.20 13.40 2 -14 3 7.20 8.50 -2 -14 -3 -1.90 7.30 -2 14 -3 -1.20 8.30 -2 14 -3 1.30 5.30 2 14 3 -3.70 5.80 2 14 3 1.10 8.10 3 -14 3 71.99 15.00 3 -14 3 51.39 25.10 3 -14 3 75.79 12.20 -3 -14 -3 53.49 22.50 -3 -14 -3 87.39 16.90 3 14 3 89.39 15.00 -3 14 -3 66.49 14.10 -3 14 -3 66.29 10.90 3 14 3 72.19 13.90 -4 -14 -3 -6.20 7.00 -4 -14 -3 -1.70 8.80 4 -14 3 -5.40 6.40 4 -14 3 6.00 8.60 4 -14 3 -24.00 14.20 4 14 3 13.10 8.60 -4 14 -3 -7.40 8.10 -5 -14 -3 5.40 9.40 5 -14 3 3.40 21.50 -5 -14 -3 12.10 9.70 5 -14 3 16.10 10.10 5 14 3 4.50 8.50 -5 14 -3 15.50 10.70 6 -14 3 92.89 17.10 6 -14 3 70.19 30.30 -6 -14 -3 65.39 16.50 -6 -14 -3 61.79 15.10 6 14 3 74.09 15.80 -6 14 -3 49.99 14.10 6 14 3 44.40 13.40 -7 -14 -3 9.00 10.40 7 -14 3 8.30 10.20 7 -14 3 3.30 23.60 -7 14 -3 -9.30 8.40 7 14 3 8.50 9.50 8 -14 3 14.90 12.30 -8 -14 -3 7.20 11.20 8 -14 3 6.60 21.30 8 14 3 5.60 9.40 -8 14 -3 9.30 9.80 9 -14 3 26.80 28.80 -9 -14 -3 42.20 15.10 9 -14 3 42.80 14.40 -9 14 -3 14.80 10.50 9 14 3 34.20 13.00 10 -14 3 46.70 33.40 10 -14 3 29.60 14.50 -10 -14 -3 20.60 13.90 10 14 3 39.70 13.30 -10 14 -3 42.40 14.10 10 -15 -3 -3.90 26.50 -10 -15 3 -13.40 9.20 10 -15 -3 12.90 12.00 10 15 -3 2.70 10.60 -10 15 3 7.30 11.10 -9 -15 3 8.60 11.00 9 -15 -3 10.90 12.50 9 -15 -3 -4.80 25.50 9 15 -3 2.70 10.50 -9 15 3 -2.70 9.30 8 -15 -3 -10.90 22.40 -8 -15 3 -5.50 21.50 -8 -15 3 7.40 10.00 8 -15 -3 7.70 11.20 -8 15 3 -1.90 8.00 8 15 -3 13.00 9.60 -7 -15 3 58.69 15.30 7 -15 -3 66.19 31.00 7 -15 -3 25.70 12.80 -7 -15 3 4.50 21.00 -7 -15 3 23.40 11.50 7 15 -3 61.79 14.80 -7 15 3 59.89 15.40 -6 -15 3 16.80 10.20 -6 -15 3 9.50 20.50 6 -15 -3 0.90 10.00 6 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12 5 -4 200.78 23.70 -12 5 4 226.88 26.90 -12 5 4 185.88 22.20 12 5 -4 205.38 26.40 11 -5 -4 -1.40 7.10 11 -5 -4 5.90 8.00 -11 -5 4 6.80 7.90 -11 5 4 -3.30 8.40 -11 5 4 -2.10 5.10 11 5 -4 -4.60 6.70 11 5 -4 7.90 9.40 10 -5 -4 87.89 14.60 10 -5 -4 114.59 14.90 -10 -5 4 109.39 18.00 -10 5 4 112.99 15.00 10 5 -4 116.09 15.50 -10 5 4 78.39 15.50 10 5 -4 125.09 18.00 -9 -5 4 6.80 6.90 9 -5 -4 8.60 7.00 9 -5 -4 10.10 6.60 -9 5 4 -2.80 7.50 9 5 -4 6.40 6.40 9 5 -4 7.50 7.30 -9 5 4 12.40 5.70 8 -5 -4 331.37 30.00 8 -5 -4 325.27 28.70 -8 -5 4 371.46 32.50 8 -5 -4 333.57 41.90 -8 5 4 324.77 29.50 8 5 -4 330.07 31.70 8 5 -4 366.16 29.90 -8 5 4 318.87 30.70 7 -5 -4 5.60 4.30 7 -5 -4 9.00 5.90 -7 -5 4 11.80 6.40 7 -5 -4 11.60 11.90 -7 5 4 8.00 3.60 -7 5 4 19.30 7.40 -7 5 4 10.50 5.20 7 5 -4 0.80 6.40 7 5 -4 13.40 5.50 6 -5 -4 103.99 10.90 6 -5 -4 91.79 12.10 6 -5 -4 97.49 21.60 -6 -5 4 114.99 14.10 -6 5 4 106.89 9.90 -6 5 4 93.69 12.10 6 5 -4 131.99 13.00 -6 5 4 90.29 12.80 6 5 -4 91.09 12.90 5 -5 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4 300.47 35.10 9 -9 -4 331.57 32.00 9 -9 -4 273.37 49.90 9 9 -4 349.77 34.50 -9 9 4 367.96 32.90 -9 9 4 377.46 33.20 9 9 -4 325.57 31.50 8 -9 -4 7.50 16.80 8 -9 -4 6.40 7.40 -8 -9 4 -4.90 5.10 8 -9 -4 -2.20 4.80 8 9 -4 1.50 6.60 -8 9 4 7.30 7.90 -8 9 4 0.40 6.10 8 9 -4 -19.30 5.40 7 -9 -4 -9.20 14.60 7 -9 -4 3.00 4.10 -7 -9 4 3.70 6.20 7 -9 -4 7.80 7.40 7 9 -4 -4.20 3.60 -7 9 4 5.30 7.20 7 9 -4 8.80 6.80 -7 9 4 -0.90 5.10 7 9 -4 -3.00 7.10 6 -9 -4 13.70 7.30 -6 -9 4 13.20 15.60 6 -9 -4 0.80 14.10 6 -9 -4 5.30 5.00 -6 -9 4 5.40 3.20 -6 -9 4 6.30 6.10 6 9 -4 0.70 5.80 -6 9 4 6.60 6.40 6 9 -4 8.60 4.40 5 -9 -4 143.69 28.10 -5 -9 4 90.99 24.50 5 -9 -4 143.09 12.00 5 -9 -4 163.08 18.60 -5 -9 4 133.39 13.40 -5 -9 4 141.79 17.70 5 9 -4 156.18 19.60 -5 9 4 161.28 18.90 5 9 -4 157.98 14.30 -4 -9 4 2.80 12.70 4 -9 -4 11.60 2.50 -4 -9 4 6.70 5.20 4 -9 -4 4.60 6.20 4 -9 -4 20.30 13.50 4 9 -4 3.70 4.50 -4 9 4 5.40 6.10 4 9 -4 17.00 7.10 -4 9 4 6.60 2.60 3 -9 -4 113.99 15.40 3 -9 -4 129.29 10.50 -3 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13 11 -4 3.10 13.80 12 -11 -4 30.40 13.20 -12 -11 4 43.90 15.10 12 -11 -4 19.10 27.10 -12 11 4 52.39 14.10 -12 11 4 36.10 14.90 12 11 -4 24.30 12.80 12 11 -4 17.70 11.20 11 -11 -4 1.10 10.30 -11 -11 4 12.10 10.20 11 -11 -4 -5.40 20.60 -11 11 4 16.50 11.60 11 11 -4 -2.80 9.80 11 11 -4 -10.80 7.90 -11 11 4 6.60 8.80 10 -11 -4 42.10 26.50 -10 -11 4 28.80 12.40 10 -11 -4 54.09 13.40 10 11 -4 46.30 14.70 10 11 -4 53.49 12.40 -10 11 4 48.90 12.50 -10 11 4 46.60 13.30 -9 -11 4 38.90 11.90 9 -11 -4 27.50 11.20 -9 -11 4 18.50 19.50 9 -11 -4 28.80 22.50 9 11 -4 22.90 10.00 9 11 -4 83.19 16.00 -9 11 4 13.60 10.60 -9 11 4 41.40 11.80 8 -11 -4 3.80 18.10 -8 -11 4 14.90 19.10 -8 -11 4 30.40 10.10 8 -11 -4 21.80 10.00 8 11 -4 44.40 13.20 -8 11 4 52.49 12.20 -8 11 4 35.90 10.80 7 -11 -4 100.89 16.70 7 -11 -4 123.19 30.80 -7 -11 4 83.29 15.90 -7 -11 4 103.29 28.90 7 11 -4 118.79 17.80 -7 11 4 134.89 18.90 -6 -11 4 -6.40 5.40 6 -11 -4 -6.10 6.80 6 -11 -4 -4.00 13.60 -6 -11 4 5.00 16.40 -6 11 4 10.80 8.00 6 11 -4 -6.20 6.60 6 11 -4 3.70 5.20 -5 -11 4 24.40 18.10 5 -11 -4 10.90 16.10 -5 -11 4 52.79 10.80 5 -11 -4 57.19 11.20 -5 11 4 47.80 11.70 5 11 -4 46.90 8.40 5 11 -4 31.60 10.00 4 -11 -4 5.30 14.40 -4 -11 4 11.80 6.60 -4 -11 4 5.10 15.20 4 -11 -4 5.70 3.20 4 -11 -4 9.50 7.80 4 11 -4 17.00 8.10 -4 11 4 -4.00 6.10 4 11 -4 10.80 6.40 -4 11 4 11.70 3.70 -3 -11 4 209.48 22.40 3 -11 -4 187.28 16.40 -3 -11 4 239.18 24.40 3 -11 -4 179.98 22.00 3 -11 -4 189.58 31.70 -3 -11 4 152.28 31.70 3 11 -4 219.98 21.50 3 11 -4 173.68 21.70 -3 11 4 199.08 22.60 -3 11 4 202.28 17.60 -2 -11 4 11.80 7.10 -2 -11 4 6.50 14.00 2 -11 -4 1.70 11.80 -2 -11 4 2.00 4.70 2 -11 -4 5.80 3.70 2 -11 -4 -4.20 6.30 2 11 -4 5.20 5.80 -2 11 4 9.90 7.10 2 11 -4 6.80 6.50 -2 11 4 5.90 4.00 -1 -11 4 81.09 13.20 -1 -11 4 48.40 20.10 1 -11 -4 83.69 19.10 1 -11 -4 87.09 9.60 1 -11 -4 75.49 12.70 -1 11 4 61.19 12.00 1 11 -4 86.99 12.60 1 11 -4 63.39 11.80 0 -11 -4 73.79 12.70 0 -11 -4 57.69 17.20 0 -11 4 113.69 15.20 0 -11 4 61.39 22.00 0 11 -4 106.59 13.40 0 11 4 85.99 13.20 0 11 -4 84.19 13.70 1 -11 4 122.49 16.40 -1 -11 -4 110.69 20.90 1 -11 4 84.39 24.10 1 -11 4 110.39 14.40 -1 -11 -4 129.99 17.30 1 11 4 117.99 15.50 -1 11 -4 135.79 17.10 -1 11 -4 118.99 14.60 2 -11 4 -0.60 13.10 -2 -11 -4 6.90 10.70 2 -11 4 -0.20 5.40 -2 -11 -4 14.30 7.60 2 -11 4 0.90 6.40 2 11 4 -3.90 6.00 -2 11 -4 2.40 7.30 -2 11 -4 6.70 5.30 -3 -11 -4 7.50 7.20 3 -11 4 18.50 7.90 3 -11 4 18.30 8.10 -3 -11 -4 -2.00 11.00 3 -11 4 -0.40 14.90 -3 -11 -4 10.10 6.40 3 11 4 3.20 7.00 -3 11 -4 3.80 7.30 -3 11 -4 8.90 5.20 3 11 4 6.10 5.90 -4 -11 -4 108.89 20.70 4 -11 4 130.59 17.60 -4 -11 -4 94.39 16.40 4 -11 4 100.49 28.80 4 -11 4 105.79 14.50 -4 11 -4 111.69 13.40 4 11 4 95.39 14.20 4 11 4 120.49 15.80 -4 11 -4 96.59 16.30 5 -11 4 35.90 10.10 5 -11 4 37.40 20.90 -5 -11 -4 33.30 14.40 5 -11 4 35.60 9.50 -5 -11 -4 18.30 10.40 5 11 4 15.30 7.60 5 11 4 38.20 9.20 -5 11 -4 36.10 11.20 -5 11 -4 39.50 7.20 -6 -11 -4 54.19 13.20 -6 -11 -4 28.20 15.00 6 -11 4 58.59 11.20 6 -11 4 50.09 12.40 6 -11 4 26.70 20.70 6 11 4 39.50 10.40 -6 11 -4 37.20 11.00 6 11 4 50.19 10.00 7 -11 4 -0.50 15.40 -7 -11 -4 -5.30 6.60 7 -11 4 -0.30 7.80 -7 -11 -4 13.90 18.00 7 -11 4 -1.70 7.80 7 11 4 -1.00 6.30 7 11 4 4.00 7.00 -7 11 -4 -5.40 6.10 -8 -11 -4 118.09 20.80 8 -11 4 129.19 20.40 8 -11 4 132.89 18.10 8 -11 4 81.59 32.90 -8 11 -4 123.49 18.60 8 11 4 94.19 16.70 -9 -11 -4 4.40 9.90 9 -11 4 6.50 21.50 9 -11 4 29.80 11.40 9 -11 4 0.00 9.20 9 11 4 0.10 7.70 -9 11 -4 1.90 9.00 -10 -11 -4 22.50 12.80 10 -11 4 42.40 14.50 10 -11 4 15.00 24.40 10 11 4 18.30 11.00 -10 11 -4 32.10 12.50 11 -11 4 -4.40 19.90 -11 -11 -4 22.70 13.00 11 -11 4 10.20 12.40 11 11 4 7.70 10.80 12 -12 -4 -17.20 22.30 -12 -12 4 21.60 12.60 12 -12 -4 -5.70 10.10 -12 -12 4 -7.80 20.90 12 12 -4 6.00 13.00 -12 12 4 -2.30 8.80 12 12 -4 -3.90 9.80 -11 -12 4 4.60 22.20 11 -12 -4 36.40 28.40 11 -12 -4 54.29 15.10 -11 -12 4 55.59 15.80 11 12 -4 47.10 13.30 11 12 -4 46.40 16.60 -11 12 4 52.59 15.00 -11 12 4 57.89 14.60 -10 -12 4 -5.40 8.10 -10 -12 4 18.70 22.40 10 -12 -4 -4.60 9.20 10 -12 -4 -11.80 19.70 -10 12 4 28.60 11.80 10 12 -4 23.70 12.20 -10 12 4 -2.90 9.00 -9 -12 4 3.00 20.10 9 -12 -4 40.00 12.80 9 -12 -4 66.29 29.20 -9 -12 4 38.00 13.00 -9 12 4 40.70 12.30 9 12 -4 46.60 14.40 -9 12 4 44.00 13.00 -8 -12 4 54.59 24.80 8 -12 -4 67.19 28.60 -8 -12 4 39.60 12.20 8 -12 -4 38.50 12.30 -8 12 4 23.00 11.20 -8 12 4 51.89 12.90 8 12 -4 44.80 13.20 -7 -12 4 16.80 9.70 7 -12 -4 31.30 22.30 -7 -12 4 9.40 19.70 7 -12 -4 17.50 10.00 7 12 -4 35.60 10.90 -7 12 4 15.80 8.40 6 -12 -4 24.90 10.30 -6 -12 4 14.90 17.80 6 -12 -4 -1.50 15.10 -6 -12 4 22.40 9.30 -6 12 4 19.50 9.50 6 12 -4 17.60 7.10 6 12 -4 25.40 9.70 5 -12 -4 40.00 10.80 -5 -12 4 28.70 9.70 5 -12 -4 41.20 20.30 -5 -12 4 12.80 17.30 5 12 -4 33.00 8.30 5 12 -4 32.10 10.40 -5 12 4 28.80 9.20 4 -12 -4 362.46 36.10 4 -12 -4 362.16 48.00 -4 -12 4 436.36 36.80 -4 -12 4 437.96 37.70 -4 -12 4 287.97 48.40 -4 12 4 376.66 36.80 4 12 -4 435.56 37.10 4 12 -4 429.66 34.90 -4 12 4 411.36 31.90 -3 -12 4 14.30 7.00 -3 -12 4 23.60 17.40 3 -12 -4 8.90 14.60 -3 -12 4 2.80 6.70 3 -12 -4 21.40 4.60 3 -12 -4 10.70 7.80 -3 12 4 9.50 4.30 3 12 -4 13.40 7.60 3 12 -4 9.30 7.20 -3 12 4 10.80 7.90 2 -12 -4 28.90 16.60 -2 -12 4 61.89 10.80 -2 -12 4 38.30 19.30 2 -12 -4 53.09 7.40 -2 -12 4 97.29 14.90 2 -12 -4 60.09 12.10 2 12 -4 50.19 10.90 -2 12 4 62.99 9.30 2 12 -4 43.80 10.30 -2 12 4 49.70 11.40 1 -12 -4 -6.20 6.40 -1 -12 4 -10.70 12.00 -1 -12 4 4.70 6.50 1 -12 -4 -4.10 11.30 -1 12 4 9.20 7.50 -1 12 4 0.70 4.90 1 12 -4 2.20 5.60 1 12 -4 8.30 7.10 0 -12 -4 617.84 63.39 0 -12 4 554.54 68.29 0 -12 -4 717.83 57.19 0 -12 4 704.93 57.29 0 12 4 768.32 57.39 0 12 -4 683.73 55.69 0 12 -4 717.13 56.99 1 -12 4 8.40 7.10 1 -12 4 21.70 8.00 -1 -12 -4 12.70 12.30 -1 -12 -4 10.60 7.80 1 -12 4 9.60 15.00 -1 12 -4 16.80 9.10 -1 12 -4 18.90 7.00 1 12 4 7.70 7.90 2 -12 4 49.60 20.60 2 -12 4 51.09 12.10 2 -12 4 57.69 11.00 -2 -12 -4 69.09 17.80 -2 -12 -4 106.89 15.80 -2 12 -4 55.79 12.80 2 12 4 55.19 11.40 -2 12 -4 68.49 10.80 -3 -12 -4 0.00 6.90 -3 -12 -4 23.80 12.50 3 -12 4 7.70 6.80 -3 -12 -4 28.10 10.20 3 -12 4 10.80 17.10 3 -12 4 34.10 9.80 -3 12 -4 25.00 9.20 3 12 4 2.80 7.00 -3 12 -4 1.70 4.90 4 -12 4 348.77 34.10 -4 -12 -4 288.87 32.30 -4 -12 -4 265.57 34.50 4 -12 4 272.27 48.50 -4 -12 -4 227.48 31.00 4 -12 4 301.57 27.80 4 12 4 311.17 29.20 -4 12 -4 267.47 30.80 -4 12 -4 311.47 26.60 4 12 4 332.37 28.90 5 -12 4 187.28 20.90 -5 -12 -4 230.98 27.40 5 -12 4 179.38 23.60 5 -12 4 127.89 36.20 5 12 4 213.48 24.50 -5 12 -4 157.48 18.20 5 12 4 203.58 21.60 6 -12 4 17.60 10.10 -6 -12 -4 27.40 11.30 6 -12 4 30.80 9.80 6 -12 4 29.00 22.60 6 12 4 28.20 9.80 6 12 4 41.80 9.90 -6 12 -4 34.60 11.90 7 -12 4 14.20 8.90 7 -12 4 15.70 21.40 -7 -12 -4 17.80 10.50 7 -12 4 11.90 10.30 7 12 4 19.60 9.30 7 12 4 -1.00 7.50 -7 12 -4 24.10 10.00 -8 -12 -4 17.10 11.40 8 -12 4 32.40 12.40 8 -12 4 7.80 22.10 8 -12 4 33.00 11.50 -8 12 -4 25.10 10.30 8 12 4 8.00 9.10 9 -12 4 106.19 19.70 -9 -12 -4 69.29 18.30 9 -12 4 66.09 33.20 9 12 4 62.59 14.80 -9 12 -4 84.09 16.80 -10 -12 -4 -1.70 11.60 10 -12 4 -2.50 21.40 10 -12 4 8.50 11.60 10 12 4 -4.50 8.60 -10 12 -4 -8.90 8.60 11 -12 4 20.30 28.40 11 -12 4 46.20 16.50 -11 -12 -4 56.99 18.50 11 12 4 25.60 12.80 11 -13 -4 13.70 12.20 -11 -13 4 2.10 10.70 -11 -13 4 12.60 23.60 11 -13 -4 -0.40 23.30 11 13 -4 -0.70 11.60 -11 13 4 -5.20 8.90 -10 -13 4 23.90 13.70 10 -13 -4 22.40 26.10 -10 -13 4 6.50 21.90 10 -13 -4 26.00 12.70 10 13 -4 17.20 11.40 -10 13 4 33.70 12.40 -10 13 4 40.20 14.20 -9 -13 4 -6.50 19.50 -9 -13 4 -2.70 7.90 9 -13 -4 7.70 10.60 9 -13 -4 15.60 22.90 -9 13 4 -1.10 8.70 9 13 -4 5.30 9.80 -9 13 4 1.60 8.80 -8 -13 4 71.79 29.90 8 -13 -4 150.08 38.40 8 -13 -4 169.48 22.00 -8 -13 4 133.19 21.20 -8 13 4 156.08 20.70 8 13 -4 132.69 21.90 -8 13 4 160.28 21.80 7 -13 -4 162.08 37.00 -7 -13 4 135.09 20.10 -7 -13 4 95.69 30.90 7 -13 -4 118.39 18.90 -7 13 4 149.88 21.30 7 13 -4 108.99 18.70 6 -13 -4 19.80 9.50 6 -13 -4 3.30 17.20 -6 -13 4 12.50 7.90 -6 -13 4 17.40 19.20 -6 13 4 0.00 8.40 6 13 -4 -1.70 7.30 -5 -13 4 31.20 10.00 5 -13 -4 21.60 20.30 -5 -13 4 20.50 10.30 -5 -13 4 20.00 19.20 5 -13 -4 26.70 10.40 5 13 -4 26.40 10.80 -5 13 4 38.80 11.40 5 13 -4 42.20 9.50 -4 -13 4 72.89 14.80 4 -13 -4 17.60 19.00 4 -13 -4 41.00 11.20 -4 -13 4 63.59 12.40 -4 -13 4 29.00 20.50 4 13 -4 62.49 11.10 4 13 -4 51.79 11.80 -4 13 4 31.90 10.40 3 -13 -4 248.88 27.90 -3 -13 4 239.08 26.10 -3 -13 4 259.07 29.30 3 -13 -4 218.38 37.20 -3 -13 4 168.38 38.00 -3 13 4 238.18 21.30 -3 13 4 257.27 28.70 3 13 -4 242.18 26.80 3 13 -4 233.18 25.20 -2 -13 4 17.30 7.90 -2 -13 4 -3.20 14.30 2 -13 -4 5.90 7.90 2 -13 -4 1.10 13.90 2 13 -4 -2.50 6.60 -2 13 4 1.60 4.70 2 13 -4 -6.10 5.50 -2 13 4 1.10 7.90 -1 -13 4 175.78 21.10 -1 -13 4 101.39 30.10 1 -13 -4 134.79 27.10 1 -13 -4 167.28 21.30 1 13 -4 111.99 18.10 -1 13 4 194.88 18.60 -1 13 4 188.38 21.70 1 13 -4 110.19 17.20 0 -13 4 40.80 21.20 0 -13 -4 25.70 16.70 0 -13 -4 56.09 12.80 0 -13 4 43.30 11.10 0 13 -4 73.19 11.90 0 13 -4 37.10 11.00 0 13 4 48.40 11.50 0 13 4 62.49 10.80 -1 -13 -4 151.58 27.70 1 -13 4 146.99 21.30 1 -13 4 228.28 21.60 1 -13 4 118.39 31.40 -1 -13 -4 202.88 23.40 1 13 4 191.28 22.00 -1 13 -4 170.98 22.40 -1 13 -4 183.18 20.50 -2 -13 -4 13.90 12.80 2 -13 4 9.30 7.60 2 -13 4 1.20 7.00 2 -13 4 19.70 18.50 -2 -13 -4 2.90 8.70 -2 13 -4 12.30 8.90 -2 13 -4 -4.80 4.90 2 13 4 20.20 9.30 3 -13 4 289.07 51.29 -3 -13 -4 267.27 37.20 -3 -13 -4 326.97 34.70 3 -13 4 339.67 30.20 3 -13 4 341.37 32.40 -3 13 -4 321.27 28.90 3 13 4 330.07 30.90 -3 13 -4 372.06 36.20 -4 -13 -4 49.40 12.80 4 -13 4 39.00 11.30 4 -13 4 28.40 21.10 -4 -13 -4 26.60 11.30 4 -13 4 64.29 11.40 4 13 4 51.49 11.90 -4 13 -4 62.79 10.00 -4 13 -4 45.60 11.90 5 -13 4 50.99 24.90 5 -13 4 89.39 13.30 5 -13 4 65.39 14.30 -5 -13 -4 46.90 13.40 -5 -13 -4 77.69 16.50 5 13 4 69.99 13.10 -5 13 -4 67.59 14.00 5 13 4 64.69 13.70 -6 -13 -4 109.69 18.90 6 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9.80 -7 -14 4 6.30 21.20 7 -14 -4 15.70 22.30 -7 -14 4 3.20 8.00 -7 14 4 3.30 8.80 7 14 -4 -3.20 7.10 -6 -14 4 1.50 18.90 6 -14 -4 -0.30 8.80 -6 -14 4 0.40 8.20 6 -14 -4 13.50 20.70 -6 -14 4 3.40 9.40 -6 14 4 0.90 7.50 6 14 -4 8.40 9.40 5 -14 -4 47.60 13.40 -5 -14 4 17.40 20.20 -5 -14 4 96.69 15.70 -5 -14 4 67.39 15.00 5 -14 -4 37.50 23.10 5 14 -4 52.99 13.10 5 14 -4 91.59 13.40 -5 14 4 84.49 16.20 -4 -14 4 23.00 10.80 4 -14 -4 13.20 18.80 4 -14 -4 8.50 9.30 -4 -14 4 28.40 21.40 -4 -14 4 6.90 7.20 -4 14 4 37.20 11.50 4 14 -4 11.80 8.30 4 14 -4 18.90 9.00 3 -14 -4 -10.30 13.90 3 -14 -4 -2.00 7.40 -3 -14 4 6.20 17.60 -3 -14 4 2.20 8.70 -3 -14 4 -3.20 5.70 -3 14 4 -1.60 4.20 3 14 -4 -2.40 7.30 -3 14 4 9.50 9.20 3 14 -4 6.80 8.20 -2 -14 4 2.50 8.10 2 -14 -4 4.00 8.20 -2 -14 4 23.30 20.10 2 -14 -4 13.50 15.60 -2 14 4 5.70 8.70 -2 14 4 7.00 5.40 2 14 -4 23.30 8.80 1 -14 -4 69.89 14.20 -1 -14 4 52.79 12.50 -1 -14 4 35.60 22.20 1 -14 -4 47.60 20.20 -1 14 4 82.19 14.80 -1 14 4 84.59 11.90 1 14 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14 4 10.60 9.90 -6 14 -4 8.50 9.80 6 14 4 -5.30 6.90 7 -14 4 0.90 10.20 -7 -14 -4 3.20 8.80 7 14 4 12.90 8.60 -7 14 -4 3.00 10.00 8 -14 4 15.90 25.10 8 -14 4 9.60 10.60 -8 -14 -4 20.20 12.30 8 14 4 0.00 9.00 -8 14 -4 -9.70 7.30 9 -14 4 27.20 13.70 9 -14 4 5.20 25.70 -9 -14 -4 11.20 12.30 9 14 4 34.90 12.30 -9 14 -4 26.00 12.40 10 -15 -4 -4.20 25.90 10 -15 -4 23.50 12.80 -10 -15 4 -5.20 9.90 10 15 -4 -3.90 10.50 -10 15 4 -2.00 9.80 -9 -15 4 -0.90 22.50 -9 -15 4 -6.40 9.90 9 -15 -4 12.00 26.20 9 -15 -4 17.70 12.30 9 15 -4 0.50 10.30 -9 15 4 28.80 13.00 8 -15 -4 53.69 15.00 8 -15 -4 46.00 30.30 -8 -15 4 17.80 22.30 -8 -15 4 49.60 16.10 -8 15 4 45.50 15.20 8 15 -4 37.60 13.60 7 -15 -4 6.60 10.60 -7 -15 4 -2.70 19.90 -7 -15 4 24.80 13.10 7 -15 -4 -12.20 20.50 -7 -15 4 6.90 9.10 7 15 -4 4.90 9.50 -7 15 4 -0.70 7.80 -6 -15 4 41.00 13.60 -6 -15 4 44.90 12.70 6 -15 -4 31.10 12.60 6 -15 -4 26.00 25.60 -6 -15 4 3.80 20.90 -6 15 4 54.89 15.00 6 15 -4 21.40 10.50 -5 -15 4 0.50 19.90 -5 -15 4 9.90 8.40 -5 -15 4 5.00 9.40 5 -15 -4 17.50 10.30 5 -15 -4 10.10 21.90 5 15 -4 2.40 8.00 -5 15 4 12.70 10.90 4 -15 -4 22.30 21.10 -4 -15 4 -3.50 18.00 -4 -15 4 7.40 9.20 4 -15 -4 22.00 11.00 -4 -15 4 10.30 8.90 4 15 -4 14.70 9.10 -4 15 4 4.70 10.30 4 15 -4 9.50 8.50 3 -15 -4 12.40 10.40 -3 -15 4 4.40 19.00 3 -15 -4 6.50 15.70 -3 -15 4 -7.10 8.00 3 15 -4 10.90 8.70 3 15 -4 -2.30 6.50 -3 15 4 -3.30 8.00 -2 -15 4 17.30 21.20 -2 -15 4 39.30 12.30 2 -15 -4 42.00 12.70 2 -15 -4 42.70 20.50 2 15 -4 47.10 12.60 2 15 -4 34.50 10.70 -2 15 4 60.49 10.00 -2 15 4 20.90 11.20 1 -15 -4 2.50 8.80 -1 -15 4 -10.60 15.50 -1 -15 4 -8.10 6.90 1 -15 -4 -3.90 14.50 -1 15 4 -11.30 8.20 1 15 -4 9.60 7.30 1 15 -4 -4.40 8.70 -1 15 4 -5.80 5.30 0 -15 4 -4.00 7.20 0 -15 -4 0.00 8.20 0 -15 4 -13.00 14.70 0 15 -4 13.60 9.40 0 15 4 -0.30 7.50 0 15 4 -5.60 4.80 0 15 -4 7.90 6.70 1 -15 4 82.49 16.20 1 -15 4 31.50 21.50 1 -15 4 69.99 12.90 -1 -15 -4 67.49 15.30 1 15 4 82.59 15.30 -1 15 -4 53.39 14.20 -1 15 -4 95.29 14.60 1 15 4 45.70 11.30 -2 -15 -4 -6.70 7.60 2 -15 4 2.00 7.80 2 -15 4 15.00 9.60 2 -15 4 -0.80 18.50 2 15 4 12.80 8.00 -2 15 -4 9.80 6.70 -2 15 -4 15.00 10.90 2 15 4 -1.90 8.70 3 -15 4 12.70 9.70 3 -15 4 5.70 19.70 3 -15 4 17.70 9.30 -3 -15 -4 6.80 11.20 3 15 4 10.50 8.50 -3 15 -4 25.20 12.60 3 15 4 19.90 10.80 -3 15 -4 21.10 7.50 4 -15 4 1.80 22.90 -4 -15 -4 -14.20 8.70 4 -15 4 6.80 9.80 -4 15 -4 -8.50 8.90 4 15 4 9.80 9.50 5 -15 4 14.00 24.40 -5 -15 -4 7.10 10.80 5 -15 4 13.80 10.50 5 15 4 22.50 11.00 -5 15 -4 0.50 8.70 6 -15 4 -12.10 8.70 6 -15 4 -3.30 21.40 -6 -15 -4 5.30 10.80 -6 -15 -4 10.90 11.20 -6 15 -4 4.70 10.10 7 -15 4 2.90 23.90 -7 -15 -4 -13.20 9.20 -7 -15 -4 -12.50 8.20 7 -15 4 9.30 11.30 7 15 4 -6.20 7.80 -8 -15 -4 -6.20 10.30 8 -15 4 -5.70 10.00 8 -15 4 30.00 30.40 -8 15 -4 -8.00 9.60 8 15 4 -2.50 9.00 9 -15 4 11.70 29.50 9 15 4 54.89 17.10 9 -16 -4 14.90 27.30 9 16 -4 19.70 13.30 8 -16 -4 -18.50 25.00 -8 -16 4 -5.40 10.30 8 -16 -4 -1.90 11.00 -8 -16 4 16.20 11.00 -8 16 4 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31.00 11.80 -11 12 5 40.70 14.60 11 12 -5 30.30 14.20 10 -12 -5 12.50 24.20 10 -12 -5 14.60 10.60 -10 -12 5 13.30 20.90 -10 -12 5 14.80 10.80 -10 12 5 -3.30 9.00 10 12 -5 4.60 10.60 -10 12 5 0.00 10.10 9 -12 -5 6.80 9.60 -9 -12 5 17.00 21.10 -9 -12 5 1.10 8.00 9 -12 -5 -16.20 19.40 9 12 -5 -0.20 9.90 -9 12 5 -12.70 9.50 -9 12 5 -5.50 7.40 8 -12 -5 -2.30 8.40 -8 -12 5 28.00 10.80 -8 -12 5 5.90 18.60 8 -12 -5 25.10 23.70 -8 12 5 11.00 9.70 -8 12 5 31.60 11.20 8 12 -5 18.00 10.30 -7 -12 5 15.40 8.60 7 -12 -5 11.60 19.20 7 -12 -5 6.50 8.60 -7 -12 5 -4.40 16.10 7 12 -5 0.60 8.30 -7 12 5 8.50 8.50 -6 -12 5 0.10 16.60 6 -12 -5 7.10 8.20 6 -12 -5 -5.10 15.50 -6 -12 5 1.10 5.80 6 12 -5 2.90 5.90 6 12 -5 1.60 7.70 -6 12 5 -6.50 6.30 -5 -12 5 39.80 21.70 -5 -12 5 51.79 11.10 5 -12 -5 54.49 22.00 5 12 -5 29.70 9.80 -5 12 5 52.89 12.20 5 12 -5 29.00 8.30 -4 -12 5 51.09 13.00 4 -12 -5 42.80 12.10 -4 -12 5 88.19 13.50 4 -12 -5 79.19 23.10 -4 -12 5 60.69 22.80 4 12 -5 88.49 12.70 -4 12 5 45.90 11.60 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7.30 -3 -12 -5 56.29 16.40 3 -12 5 70.79 26.40 3 -12 5 84.89 14.50 3 -12 5 76.49 12.30 -3 -12 -5 59.29 13.20 -3 12 -5 72.69 11.20 -3 12 -5 50.09 12.50 3 12 5 77.19 13.50 3 12 5 59.49 12.20 4 -12 5 22.70 8.30 4 -12 5 49.10 24.00 -4 -12 -5 34.50 10.80 4 -12 5 24.70 8.90 -4 -12 -5 11.60 8.50 4 12 5 26.60 9.30 -4 12 -5 12.10 6.20 4 12 5 13.90 7.40 -4 12 -5 23.70 10.70 -5 -12 -5 4.40 8.70 5 -12 5 7.90 8.30 5 -12 5 10.30 7.80 5 -12 5 11.30 17.20 -5 12 -5 9.20 8.30 5 12 5 5.70 6.60 -5 12 -5 11.80 6.40 5 12 5 -0.20 7.30 6 -12 5 7.10 8.30 -6 -12 -5 -9.70 7.50 6 -12 5 18.00 20.60 6 -12 5 7.30 8.30 -6 12 -5 3.40 8.40 6 12 5 -4.10 5.80 6 12 5 5.70 7.70 -7 -12 -5 13.20 10.80 7 -12 5 -1.90 8.40 7 -12 5 -0.50 8.50 7 -12 5 -7.50 18.30 -7 12 -5 5.60 8.60 7 12 5 1.00 7.60 7 12 5 -10.00 6.00 8 -12 5 4.20 18.30 8 -12 5 -2.30 9.30 8 -12 5 9.10 10.40 -8 -12 -5 22.20 12.40 -8 12 -5 17.10 10.50 8 12 5 18.20 9.00 9 -12 5 7.20 23.30 9 -12 5 8.20 10.50 -9 -12 -5 3.70 10.70 9 12 5 -9.10 8.00 -9 12 -5 2.90 9.40 10 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38.50 14.20 6 17 -5 18.30 12.30 -6 17 5 31.70 13.80 -5 -17 5 18.10 10.80 -5 -17 5 16.10 24.70 -5 -17 5 24.70 13.30 5 -17 -5 44.30 14.40 -5 17 5 23.90 11.70 5 17 -5 19.60 11.10 -4 -17 5 5.80 22.60 -4 -17 5 40.30 14.80 4 -17 -5 10.30 11.10 4 17 -5 -5.80 7.90 -4 17 5 13.30 11.30 -3 -17 5 -1.10 22.30 3 -17 -5 6.30 10.80 -3 -17 5 9.50 11.30 3 17 -5 13.50 9.10 -3 17 5 5.80 11.10 3 17 -5 7.30 11.20 -2 -17 5 109.39 20.20 2 -17 -5 78.89 16.80 -2 -17 5 27.60 24.60 2 17 -5 69.29 16.20 2 17 -5 73.79 14.90 -2 17 5 55.49 14.70 1 -17 -5 139.09 22.00 -1 -17 5 117.99 21.30 -1 -17 5 81.99 32.70 -1 17 5 151.28 22.70 1 17 -5 144.99 20.40 1 17 -5 132.59 21.50 0 -17 5 18.20 11.20 0 -17 5 4.30 10.20 0 -17 -5 -10.30 9.20 0 -17 5 3.90 21.60 0 17 -5 20.00 9.10 0 17 -5 -2.70 11.00 0 17 5 4.30 7.50 0 17 5 -6.40 10.50 1 -17 5 28.60 12.70 -1 -17 -5 36.00 13.50 1 -17 5 21.20 24.60 1 17 5 51.79 14.80 -1 17 -5 31.20 10.20 1 17 5 32.00 10.70 -1 17 -5 39.50 14.70 -2 -17 -5 0.50 10.90 2 -17 5 3.20 9.80 2 -17 5 2.90 23.30 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132.19 18.30 8 -4 -10 159.98 13.70 -8 4 10 152.58 14.80 -8 4 10 135.59 18.30 8 4 -10 153.78 19.50 -8 4 10 145.79 16.80 -7 -4 10 86.99 8.10 -7 -4 10 93.49 8.30 7 -4 -10 90.79 8.90 7 -4 -10 103.69 10.70 7 -4 -10 100.99 8.90 -7 -4 10 80.29 13.10 -7 4 10 78.79 13.00 -7 4 10 101.79 10.50 -7 4 10 91.59 9.90 7 4 -10 109.79 14.90 -7 4 10 134.99 13.90 -6 -4 10 68.09 7.30 -6 -4 10 68.79 7.50 -6 -4 10 75.99 10.80 -6 4 10 79.89 10.60 -6 4 10 65.29 7.80 6 4 -10 77.19 12.90 -6 4 10 73.19 8.40 -5 -4 10 271.67 21.80 -5 -4 10 259.07 21.20 -5 -4 10 254.17 23.10 5 4 -10 232.58 24.00 -5 4 10 250.37 20.60 -5 4 10 245.78 22.90 -5 4 10 268.47 21.70 -4 -4 10 125.39 24.40 -4 -4 10 66.99 9.70 -4 -4 10 87.39 9.50 -4 -4 10 81.39 8.50 -4 4 10 73.39 7.50 -4 4 10 86.89 9.10 -4 4 10 89.79 16.70 4 4 -10 65.99 11.00 -4 4 10 88.29 9.90 -4 4 10 67.19 10.00 -3 -4 10 185.88 17.20 -3 -4 10 254.67 29.70 -3 4 10 175.48 16.50 -3 4 10 207.58 21.70 -3 4 10 197.88 16.00 -3 4 10 193.18 16.40 3 4 -10 185.98 20.40 -3 4 10 201.08 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23.60 -9 5 10 280.47 28.60 9 5 -10 253.77 27.30 8 -5 -10 30.10 6.10 -8 -5 10 24.00 8.30 8 5 -10 38.60 10.70 -8 5 10 34.80 7.90 -8 5 10 32.00 5.60 -8 5 10 48.20 11.30 7 -5 -10 54.79 7.20 -7 -5 10 46.80 10.20 7 -5 -10 64.99 7.40 -7 -5 10 54.59 5.30 -7 -5 10 60.49 5.50 -7 5 10 64.29 6.90 7 5 -10 57.29 12.20 -7 5 10 62.79 7.00 -7 5 10 42.10 10.80 -7 5 10 40.90 8.90 6 -5 -10 0.00 2.90 -6 -5 10 4.10 4.40 -6 -5 10 1.70 2.20 6 -5 -10 0.40 2.60 6 5 -10 -2.00 5.80 -6 5 10 3.50 4.50 -6 5 10 -1.20 2.40 -6 5 10 0.80 2.20 5 -5 -10 244.58 19.00 -5 -5 10 237.68 20.10 5 -5 -10 255.57 19.10 -5 -5 10 241.98 22.10 -5 5 10 233.28 20.30 -5 5 10 223.38 18.70 -5 5 10 240.08 18.90 -5 5 10 263.07 22.60 5 5 -10 235.98 23.60 -4 -5 10 249.38 22.20 -4 -5 10 318.07 35.90 -4 -5 10 244.78 21.30 4 -5 -10 261.87 19.60 4 -5 -10 245.48 19.60 -4 5 10 257.47 29.70 4 5 -10 247.08 24.40 -4 5 10 243.38 21.50 -4 5 10 242.68 19.60 -4 5 10 254.67 23.00 3 -5 -10 147.39 12.90 -3 -5 10 159.08 29.30 -3 -5 10 154.48 14.70 3 -5 -10 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21.70 5.10 -1 -7 10 -4.10 8.70 -1 -7 10 12.60 4.90 1 -7 -10 14.60 5.50 1 -7 -10 13.80 3.90 -1 -7 10 19.70 3.60 -1 7 10 37.10 8.40 -1 7 10 16.30 5.00 1 7 -10 8.20 5.60 -1 7 10 13.70 3.70 0 -7 10 7.30 6.20 0 -7 10 8.20 4.50 0 -7 10 7.20 11.10 0 -7 -10 8.90 5.20 0 -7 -10 6.80 4.20 0 7 10 2.90 3.70 0 7 -10 1.70 5.50 0 7 10 12.10 4.00 0 7 10 9.90 5.50 1 -7 10 57.29 18.60 -1 -7 -10 58.39 9.40 1 -7 10 46.40 8.60 1 -7 10 36.00 8.80 -1 7 -10 54.99 10.30 1 7 10 62.49 8.70 1 7 10 43.10 8.30 1 7 10 62.39 10.60 -2 -7 -10 41.60 9.00 2 -7 10 68.39 10.50 2 -7 10 43.00 16.80 2 -7 10 47.10 10.50 2 7 10 53.79 10.40 2 7 10 48.90 8.50 -2 7 -10 57.69 10.40 2 7 10 33.90 7.90 3 -7 10 120.09 16.50 3 -7 10 129.59 16.10 3 -7 10 110.99 27.60 -3 7 -10 141.59 17.30 3 7 10 143.99 17.40 3 7 10 124.59 15.60 3 7 10 118.59 15.70 4 -7 10 129.59 31.60 -4 -7 -10 173.78 23.40 4 -7 10 191.18 22.50 4 -7 10 184.48 21.70 4 7 10 232.88 20.30 4 7 10 182.28 20.90 4 7 10 166.98 20.00 5 -7 10 114.29 29.90 -5 -7 -10 144.79 20.20 5 -7 10 146.29 18.30 5 -7 10 128.89 18.40 5 7 10 117.19 16.20 5 7 10 123.39 16.80 5 7 10 117.39 16.90 6 -7 10 34.80 19.70 6 -7 10 18.80 9.70 6 -7 10 6.10 7.20 -6 -7 -10 4.40 8.40 6 7 10 28.80 8.40 6 7 10 23.40 8.50 6 7 10 10.60 7.70 7 -7 10 92.39 16.50 7 -7 10 87.99 15.30 7 -7 10 117.19 32.50 -7 -7 -10 106.39 18.90 7 7 10 109.79 17.10 7 7 10 114.19 17.80 7 7 10 80.59 14.10 8 -7 10 1.40 15.50 8 -7 10 22.40 11.00 -8 -7 -10 7.50 11.10 8 -7 10 2.80 7.70 8 7 10 3.10 8.00 8 7 10 7.10 7.60 8 7 10 26.60 10.50 9 -7 10 55.99 16.50 9 -7 10 69.39 15.20 9 -7 10 103.59 32.80 -9 -7 -10 78.19 18.70 9 7 10 81.29 16.10 9 7 10 83.39 14.70 9 7 10 78.59 16.50 10 -7 10 21.20 12.80 -10 -7 -10 0.50 12.40 10 -7 10 20.90 12.30 10 -7 10 8.50 20.50 10 7 10 8.60 8.70 10 7 10 16.60 11.60 11 -7 10 -2.10 9.60 11 -7 10 -1.40 12.30 -11 -7 -10 6.20 13.00 11 -7 10 -5.00 18.40 11 7 10 -4.40 9.80 11 7 10 7.80 9.10 -14 -8 10 3.80 10.60 14 8 -10 -9.70 13.30 -14 8 10 -4.80 14.20 -13 -8 10 43.90 14.90 -13 8 10 29.60 10.90 13 8 -10 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2 -17 -11 44.30 15.50 -2 -17 11 46.90 17.00 -2 -17 11 61.19 17.70 2 17 -11 51.99 14.40 -2 17 11 31.10 13.50 1 -17 -11 -0.20 10.70 -1 -17 11 -7.80 12.10 -1 -17 11 -12.40 8.70 -1 -17 11 12.00 23.70 1 17 -11 -6.20 8.80 -1 17 11 -8.30 10.30 0 -17 -11 23.00 12.30 0 -17 11 2.30 22.90 0 -17 11 16.30 12.70 0 -17 11 15.90 11.40 0 17 11 18.80 12.80 0 17 -11 24.60 11.30 -1 -17 -11 16.20 13.20 1 -17 11 16.10 11.70 1 -17 11 42.40 15.20 1 -17 11 20.20 26.50 -1 17 -11 27.20 11.00 1 17 11 24.50 14.20 2 -17 11 111.29 20.10 2 -17 11 24.70 27.00 -2 -17 -11 46.10 16.00 2 -17 11 57.09 15.70 2 17 11 93.49 19.40 3 -17 11 11.00 26.40 -15 0 12 18.70 12.50 -14 0 12 -5.00 8.70 -13 0 12 8.90 9.10 12 0 -12 12.90 9.00 -12 0 12 23.20 11.90 -11 0 12 309.27 33.60 11 0 -12 304.37 29.80 -10 0 12 66.89 13.60 -10 0 12 78.89 9.20 10 0 -12 63.69 12.10 -9 0 12 5.60 5.60 -9 0 12 -2.50 2.80 9 0 -12 -1.50 7.10 -8 0 12 459.85 39.10 8 0 -12 460.15 38.60 -8 0 12 424.16 35.40 7 0 -12 131.49 16.90 -7 0 12 137.89 17.60 -7 0 12 160.78 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3.40 8 -3 -14 19.00 7.50 -8 3 14 4.40 6.50 -8 3 14 11.60 5.50 8 3 -14 19.30 9.40 -7 -3 14 60.59 11.00 -7 -3 14 45.20 7.10 7 -3 -14 42.50 9.30 -7 3 14 45.50 10.30 7 3 -14 78.49 13.80 -7 3 14 49.00 9.00 -6 -3 14 143.19 13.80 -6 -3 14 128.99 16.10 -6 -3 14 139.99 12.20 -6 3 14 141.09 16.10 6 3 -14 130.09 18.10 -5 -3 14 20.30 13.60 -5 -3 14 53.09 5.60 -5 -3 14 42.70 8.20 -5 3 14 52.79 6.30 5 3 -14 48.60 11.10 -5 3 14 45.00 6.80 -5 3 14 40.80 8.50 -4 -3 14 0.40 3.60 -4 -3 14 9.30 11.30 -4 3 14 2.40 4.60 -4 3 14 -2.20 2.80 4 3 -14 3.50 6.20 -4 3 14 0.90 2.30 -4 3 14 1.50 2.10 -3 -3 14 38.60 15.80 -3 -3 14 64.09 10.20 -3 -3 14 53.29 8.20 -3 3 14 43.80 9.00 -3 3 14 45.80 7.40 3 3 -14 58.39 11.00 -3 3 14 68.79 7.10 -3 3 14 61.79 6.70 -2 -3 14 75.99 19.70 -2 -3 14 93.49 8.60 -2 -3 14 81.49 10.00 -2 -3 14 101.29 13.10 -2 3 14 71.49 11.40 -2 3 14 75.69 15.00 -2 3 14 89.09 10.80 -2 3 14 82.89 9.00 2 3 -14 82.59 13.50 -1 -3 14 56.59 16.40 -1 -3 14 32.00 8.20 -1 -3 14 49.90 6.40 -1 -3 14 33.90 5.90 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154.98 29.10 -1 -4 14 127.29 13.50 -1 -4 14 126.59 16.40 -1 4 14 143.79 13.00 -1 4 14 107.89 15.50 -1 4 14 129.59 16.00 -1 4 14 131.59 14.40 1 4 -14 131.89 17.90 0 -4 14 7.40 2.90 0 -4 14 19.50 12.70 0 -4 14 11.50 5.90 0 -4 14 6.00 3.80 0 -4 14 9.60 3.40 0 4 -14 6.50 6.70 0 4 14 18.50 6.30 0 4 14 3.00 6.30 0 4 14 1.80 4.30 0 4 14 13.60 4.50 1 -4 14 256.87 25.00 -1 -4 -14 262.57 20.30 -1 -4 -14 253.07 20.50 1 -4 14 248.78 22.40 1 -4 14 251.17 20.10 1 -4 14 192.98 35.10 1 -4 14 283.17 20.50 1 4 14 267.17 23.70 1 4 14 213.78 25.50 1 4 14 257.77 22.50 1 4 14 226.28 23.20 -2 -4 -14 308.17 25.20 2 -4 14 251.37 25.60 2 -4 14 260.97 41.10 -2 -4 -14 335.87 27.60 2 -4 14 308.37 23.20 2 -4 14 267.17 28.00 2 4 14 281.87 26.80 2 4 14 235.68 28.50 2 4 14 295.17 26.10 -2 4 -14 326.77 26.10 2 4 14 300.67 27.30 3 -4 14 74.69 11.50 3 -4 14 82.59 14.10 3 -4 14 110.09 26.50 3 4 14 64.59 12.10 3 4 14 74.29 11.80 3 4 14 74.99 12.70 3 4 14 70.19 13.10 4 -4 14 85.69 13.90 4 -4 14 113.89 16.90 4 -4 14 84.29 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173.98 16.20 -2 5 14 187.78 16.50 -2 5 14 170.68 19.10 -2 5 14 185.38 16.20 -2 5 14 167.48 19.10 2 5 -14 153.58 20.30 -2 5 14 193.88 20.60 -1 -5 14 27.00 5.90 -1 -5 14 14.70 6.60 -1 -5 14 36.10 16.00 -1 5 14 15.20 5.00 -1 5 14 30.50 6.80 -1 5 14 18.60 7.50 -1 5 14 20.80 5.70 1 5 -14 24.50 8.50 -1 5 14 58.59 9.10 0 -5 14 214.18 20.50 0 -5 14 210.48 24.00 0 -5 14 235.28 18.40 0 -5 14 236.78 18.50 0 -5 14 178.58 34.50 0 5 14 193.98 23.50 0 5 14 260.57 21.10 0 5 -14 259.37 27.00 0 5 14 230.08 21.30 -1 -5 -14 170.08 15.50 1 -5 14 202.08 35.10 1 -5 14 159.68 20.50 1 -5 14 165.58 17.90 -1 -5 -14 161.88 15.20 1 5 14 160.98 18.50 1 5 14 164.08 18.10 -1 5 -14 172.48 21.30 1 5 14 182.58 20.90 2 -5 14 262.27 24.20 2 -5 14 214.58 21.40 2 -5 14 200.88 37.00 -2 -5 -14 228.58 21.00 2 5 14 199.48 24.00 2 5 14 248.38 23.10 2 5 14 220.98 21.50 3 -5 14 75.09 13.90 3 -5 14 74.19 11.60 3 5 14 62.89 10.40 3 5 14 55.09 11.60 3 5 14 63.69 12.60 4 -5 14 -4.40 10.60 4 -5 14 17.30 9.20 4 -5 14 4.90 6.10 4 5 14 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5 -3 21 45.90 23.70 5 -3 21 25.80 12.80 5 -3 21 54.79 13.50 5 3 21 62.69 15.60 5 3 21 45.10 13.10 5 3 21 80.49 14.50 6 -3 21 19.10 21.10 6 -3 21 15.80 9.10 6 -3 21 12.00 10.50 6 3 21 9.80 11.20 6 3 21 9.50 9.20 -12 -4 21 6.20 9.70 12 4 -21 14.60 13.40 -12 4 21 4.60 11.50 -11 -4 21 20.50 11.10 -11 -4 21 11.80 20.40 11 4 -21 26.50 14.10 -11 4 21 44.50 13.70 -10 -4 21 24.50 10.50 -10 -4 21 36.00 25.60 -10 4 21 24.70 9.70 -10 4 21 26.10 11.80 10 4 -21 19.20 12.50 -9 -4 21 16.30 19.10 -9 -4 21 47.20 12.40 -9 4 21 94.79 14.40 -9 4 21 61.39 15.20 9 4 -21 81.29 17.70 -8 -4 21 4.60 15.90 -8 -4 21 3.60 7.40 8 4 -21 6.70 11.00 -8 4 21 3.90 8.80 -8 4 21 8.30 7.70 -7 -4 21 21.90 20.50 -7 -4 21 61.19 11.20 -7 -4 21 80.99 13.50 -7 4 21 70.19 13.10 7 4 -21 71.69 16.30 -7 4 21 57.69 13.90 -6 -4 21 128.59 16.60 -6 -4 21 99.19 32.30 -6 -4 21 133.19 18.00 -6 -4 21 95.59 15.20 -6 4 21 97.49 23.60 6 4 -21 94.19 19.20 -6 4 21 102.39 16.00 -5 -4 21 37.60 10.50 -5 -4 21 34.20 8.60 -5 -4 21 35.30 22.40 -5 4 21 14.80 13.10 -5 4 21 45.00 11.10 5 4 -21 39.00 13.80 -5 4 21 36.90 7.90 -4 -4 21 -2.80 5.80 -4 -4 21 -3.90 12.10 -4 -4 21 12.70 6.20 -4 4 21 -4.00 9.00 -4 4 21 -9.50 6.00 4 4 -21 -3.20 9.20 -4 4 21 7.90 5.10 -3 -4 21 36.10 8.80 -3 -4 21 24.60 18.70 -3 -4 21 52.19 12.00 -3 4 21 38.50 11.00 -3 4 21 28.30 8.10 3 4 -21 44.20 13.40 -2 -4 21 373.36 62.79 -2 -4 21 542.95 47.20 -2 4 21 541.05 44.60 -2 4 21 616.14 48.40 -1 -4 21 -3.10 12.00 -1 -4 21 11.90 8.50 -1 4 21 -10.40 4.90 -1 4 21 -3.00 7.10 0 -4 21 21.90 9.40 0 -4 21 16.30 16.80 0 4 21 34.90 11.50 0 4 21 27.70 8.90 1 -4 21 -6.50 6.80 1 -4 21 -2.60 12.30 1 4 21 -4.00 6.50 1 4 21 -3.20 6.30 2 -4 21 216.38 26.90 2 -4 21 161.68 37.00 2 4 21 136.29 22.70 2 4 21 222.38 25.10 2 4 21 239.08 26.20 3 -4 21 1.20 10.00 3 -4 21 -0.50 8.40 3 -4 21 1.90 14.10 3 4 21 2.40 6.20 3 4 21 1.30 8.10 3 4 21 8.20 9.10 4 -4 21 39.20 21.60 4 -4 21 60.29 14.10 4 -4 21 46.40 11.80 4 4 21 35.00 12.40 4 4 21 49.90 14.40 4 4 21 31.60 10.40 5 -4 21 33.70 13.40 5 -4 21 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8.50 -2 -4 25 11.10 17.60 -2 -4 25 15.30 9.60 -2 4 25 32.20 12.40 -2 4 25 11.30 8.70 -1 -4 25 -0.70 15.60 -1 -4 25 3.00 8.70 -1 4 25 1.30 7.50 -1 4 25 -4.20 8.70 0 -4 25 168.18 23.40 0 -4 25 100.39 32.10 0 4 25 150.98 22.70 0 4 25 192.18 23.60 1 -4 25 -0.50 15.70 1 -4 25 -8.60 7.90 1 4 25 2.60 9.40 1 4 25 10.30 9.80 2 -4 25 19.90 24.90 2 -4 25 71.59 16.90 2 4 25 38.20 14.00 2 4 25 61.59 15.70 -9 -5 25 -14.20 16.80 -9 -5 25 2.10 8.60 9 5 -25 8.40 13.90 -8 -5 25 -5.70 17.70 -8 -5 25 36.90 12.60 -8 5 25 46.10 15.10 8 5 -25 41.70 17.80 -8 5 25 20.30 10.90 -7 -5 25 87.19 17.80 -7 -5 25 59.19 33.00 -7 5 25 109.19 19.40 -7 5 25 127.39 19.50 7 5 -25 137.59 25.30 -6 -5 25 5.80 18.30 -6 -5 25 10.30 8.30 -6 -5 25 17.30 9.70 6 5 -25 14.80 13.00 -6 5 25 -2.10 8.80 -5 -5 25 9.50 19.80 -5 -5 25 -5.00 7.60 5 5 -25 8.30 12.90 -5 5 25 -2.30 7.60 -4 -5 25 7.20 18.30 -4 -5 25 -2.60 8.00 -4 5 25 -1.20 8.20 -3 -5 25 94.49 17.20 -3 -5 25 12.10 21.10 -3 5 25 69.39 15.30 -2 -5 25 -10.30 16.30 -2 -5 25 10.70 9.00 -2 5 25 15.80 11.00 -1 -5 25 62.59 14.80 -1 -5 25 34.10 22.90 -1 5 25 32.80 14.00 0 -5 25 29.10 11.40 0 -5 25 7.30 18.30 0 5 25 8.80 10.20 0 5 25 2.30 8.30 1 -5 25 25.70 22.00 1 -5 25 58.69 15.80 1 5 25 60.89 14.60 1 5 25 46.00 15.30 2 -5 25 -6.40 17.40 -8 -6 25 3.70 18.60 -8 -6 25 35.80 12.60 -8 6 25 53.39 14.00 8 6 -25 59.69 19.00 -8 6 25 33.90 12.70 -7 -6 25 6.10 9.70 -7 -6 25 -1.40 20.70 -7 6 25 11.50 9.80 7 6 -25 -11.60 11.70 -7 6 25 14.80 9.40 -6 -6 25 -3.50 7.80 -6 -6 25 9.70 20.30 6 6 -25 2.30 14.30 -6 6 25 6.00 8.90 -5 -6 25 6.90 8.90 -5 -6 25 -3.60 18.10 5 6 -25 -0.10 12.40 -5 6 25 -12.10 7.80 -4 -6 25 22.90 24.00 -4 -6 25 42.40 14.00 4 6 -25 75.59 19.30 -4 6 25 37.60 12.70 -3 -6 25 15.50 20.30 -3 -6 25 0.00 8.50 -3 6 25 0.30 8.90 -2 -6 25 43.90 13.40 -2 -6 25 8.30 20.70 -2 6 25 25.90 12.20 -1 -6 25 10.00 8.70 -1 -6 25 7.10 19.30 -1 6 25 1.70 9.70 0 -6 25 10.20 20.60 0 -6 25 32.10 13.10 0 6 25 14.80 10.80 1 -6 25 -11.50 8.10 1 -6 25 3.10 18.90 1 6 25 -5.00 10.40 -7 -7 25 -12.40 8.10 -7 -7 25 1.60 20.30 7 7 -25 -5.60 13.30 -7 7 25 -13.20 8.30 -6 -7 25 -4.30 19.60 -6 -7 25 -1.80 8.70 -6 7 25 -1.70 9.10 6 7 -25 4.60 13.90 -5 -7 25 35.00 12.80 -5 -7 25 25.10 23.80 -5 7 25 50.09 14.20 5 7 -25 45.10 17.00 -4 -7 25 3.90 9.20 -4 -7 25 -8.10 17.30 -4 7 25 10.10 10.20 4 7 -25 0.40 12.70 -3 -7 25 6.50 20.50 -3 7 25 42.80 13.90 -2 -7 25 0.10 9.20 -2 -7 25 3.80 20.30 -2 7 25 8.20 10.10 -1 -7 25 49.80 14.20 -1 -7 25 25.90 23.90 -1 7 25 20.00 12.00 0 -7 25 39.80 26.40 0 -7 25 -3.30 9.70 0 7 25 -5.30 9.80 -6 -8 25 43.10 30.00 -5 -8 25 6.30 10.90 -5 -8 25 -17.70 17.70 -5 8 25 0.40 9.60 5 8 -25 -13.60 11.90 -4 -8 25 43.30 14.60 -4 -8 25 17.40 20.20 -4 8 25 45.10 14.00 4 8 -25 33.40 15.40 -3 -8 25 3.30 8.90 -3 -8 25 16.10 23.30 3 8 -25 8.50 12.60 -3 8 25 8.50 10.80 -2 -8 25 90.19 18.70 -2 -8 25 106.99 39.00 -2 8 25 93.69 19.30 -1 -8 25 15.40 23.50 -9 0 26 39.70 13.40 -9 0 26 21.90 22.40 -8 0 26 30.70 22.40 -8 0 26 47.60 15.40 -8 0 26 52.39 13.90 -7 0 26 17.80 19.30 -7 0 26 38.10 11.80 -7 0 26 70.89 14.90 -7 0 26 53.19 12.50 -6 0 26 0.40 16.00 -6 0 26 27.50 10.30 -6 0 26 24.70 10.00 -6 0 26 10.30 8.50 -5 0 26 -0.60 8.40 -5 0 26 -3.80 7.40 -5 0 26 8.90 8.20 -4 0 26 29.00 10.50 -4 0 26 56.59 14.20 -3 0 26 122.69 18.60 -3 0 26 99.89 19.60 -2 0 26 33.10 11.00 -2 0 26 14.90 10.30 -1 0 26 6.00 8.50 -1 0 26 10.00 10.00 0 0 26 44.20 12.80 0 0 26 53.19 14.70 1 0 26 32.10 11.90 -9 -1 26 -8.60 8.40 -9 -1 26 14.20 19.30 -9 1 26 6.50 9.60 -9 1 26 1.10 15.60 -8 -1 26 -5.90 7.50 -8 -1 26 0.30 8.00 -8 -1 26 3.10 19.50 -8 1 26 6.90 18.80 -8 1 26 12.60 8.90 -8 1 26 4.90 8.50 -7 -1 26 1.80 8.40 -7 -1 26 0.90 7.70 -7 -1 26 -13.50 14.50 -7 -1 26 2.50 8.30 -7 1 26 -10.00 7.00 -7 1 26 -2.20 7.90 -6 -1 26 95.29 16.50 -6 -1 26 98.59 17.00 -6 -1 26 68.49 14.20 -6 -1 26 62.59 26.50 -6 1 26 70.19 15.10 -6 1 26 70.69 14.90 -6 1 26 89.99 17.00 -5 -1 26 7.60 8.60 -5 -1 26 3.40 7.60 -5 -1 26 -2.60 14.10 -5 1 26 11.50 8.80 -5 1 26 -2.00 8.00 -5 1 26 -5.90 6.10 -4 -1 26 -6.50 7.40 -4 -1 26 -9.30 7.60 -4 -1 26 1.50 15.70 -4 1 26 -3.70 6.80 -4 1 26 -0.80 7.00 -4 1 26 5.40 8.70 -3 -1 26 19.00 9.60 -3 -1 26 -0.20 7.40 -3 1 26 -7.60 6.30 -3 1 26 1.00 8.80 -2 -1 26 62.39 16.20 -2 -1 26 71.09 14.70 -2 1 26 82.19 15.20 -2 1 26 95.39 18.50 -1 -1 26 87.19 16.60 -1 1 26 71.59 16.70 -1 1 26 57.99 14.10 0 -1 26 6.50 9.10 0 1 26 8.90 10.80 0 1 26 -3.00 7.00 1 -1 26 31.50 12.50 1 1 26 9.00 10.40 1 1 26 41.20 12.90 -9 -2 26 -1.60 18.10 -8 -2 26 5.80 9.10 -8 -2 26 -15.40 16.20 -8 -2 26 -0.70 7.70 -8 2 26 8.60 9.10 -8 2 26 7.90 8.90 -7 -2 26 34.40 10.90 -7 -2 26 6.20 17.60 -7 -2 26 1.20 7.80 -7 2 26 0.00 7.60 -7 2 26 9.90 9.20 -6 -2 26 58.59 13.60 -6 -2 26 39.90 12.40 -6 -2 26 16.50 21.20 -6 2 26 36.00 12.10 -6 2 26 83.99 15.80 -5 -2 26 -4.90 14.50 -5 -2 26 -3.60 7.10 -5 -2 26 -12.60 6.50 -5 2 26 6.40 9.60 -5 2 26 2.50 7.70 -4 -2 26 4.80 9.00 -4 -2 26 24.40 20.70 -4 -2 26 6.40 8.40 -4 2 26 26.70 9.50 -4 2 26 47.00 13.20 -3 -2 26 7.30 9.40 -3 -2 26 32.70 10.00 -3 -2 26 3.20 16.10 -3 2 26 17.80 10.60 -3 2 26 -2.90 7.20 -2 -2 26 20.30 25.70 -2 -2 26 2.40 8.40 -2 2 26 -4.00 7.10 -2 2 26 13.60 9.10 -1 -2 26 7.60 8.80 -1 2 26 10.70 9.00 -1 2 26 4.80 9.30 0 -2 26 17.90 9.50 0 2 26 22.40 11.30 0 2 26 25.00 10.50 1 -2 26 -4.70 8.10 1 2 26 3.80 9.30 1 2 26 11.80 11.10 -8 -3 26 0.50 20.00 -8 -3 26 11.70 9.00 -8 3 26 21.70 10.20 -8 3 26 6.90 9.20 8 3 -26 0.30 12.90 -7 -3 26 12.60 19.80 -7 3 26 -1.40 7.80 7 3 -26 -5.30 13.40 -7 3 26 16.40 9.70 -6 -3 26 13.10 9.00 -6 -3 26 1.20 7.80 -6 -3 26 4.30 18.10 -6 3 26 3.60 8.70 -6 3 26 10.90 9.50 -5 -3 26 -2.80 15.50 -5 -3 26 -7.10 6.80 -5 -3 26 8.30 8.60 -5 3 26 2.80 7.50 -5 3 26 3.00 8.90 -4 -3 26 3.40 19.20 -4 -3 26 30.50 12.10 -4 -3 26 42.40 13.20 -4 3 26 36.10 12.90 -3 -3 26 0.90 17.30 -3 -3 26 18.90 10.20 -3 3 26 24.70 11.60 -2 -3 26 4.90 7.80 -2 -3 26 5.60 16.40 -2 3 26 2.50 9.40 -2 3 26 5.50 7.70 -1 -3 26 -0.30 16.10 -1 -3 26 7.30 8.70 -1 3 26 15.80 9.10 -1 3 26 -5.70 8.30 0 -3 26 20.40 11.00 0 3 26 11.90 9.90 0 3 26 14.80 11.30 1 -3 26 5.30 9.60 1 3 26 -12.50 7.30 1 3 26 8.10 9.90 -8 -4 26 -0.20 8.00 -8 -4 26 -0.30 19.80 -8 4 26 3.10 8.30 8 4 -26 -2.40 13.00 -7 -4 26 -0.90 17.70 -7 -4 26 15.70 10.30 7 4 -26 20.00 14.70 -7 4 26 17.50 10.60 -7 4 26 -0.70 9.00 -6 -4 26 -8.20 6.60 -6 -4 26 1.80 8.50 -6 -4 26 -2.60 16.20 -6 4 26 -5.40 7.20 6 4 -26 -5.60 10.70 -6 4 26 1.60 8.30 -5 -4 26 15.50 10.20 -5 -4 26 6.40 9.10 -5 -4 26 22.80 21.20 -5 4 26 12.80 10.20 -4 -4 26 1.80 18.20 -4 -4 26 -2.90 8.20 -4 4 26 7.70 9.20 -3 -4 26 11.20 19.40 -3 -4 26 37.70 12.60 -3 4 26 4.00 9.50 -2 -4 26 19.20 20.30 -2 -4 26 -1.10 8.10 -2 4 26 31.10 12.60 -1 -4 26 -4.50 16.80 -1 -4 26 16.90 10.50 -1 4 26 4.30 13.50 -1 4 26 -3.30 9.00 0 -4 26 25.20 10.80 0 -4 26 2.80 18.50 0 4 26 8.90 9.30 0 4 26 38.50 13.70 -7 -5 26 -9.50 6.90 -7 -5 26 -7.00 18.10 -7 5 26 7.90 9.60 -7 5 26 4.80 9.50 7 5 -26 -6.70 11.50 -6 -5 26 10.80 15.00 -6 -5 26 20.50 10.90 -6 -5 26 11.60 19.80 6 5 -26 -6.30 12.20 -6 5 26 2.10 9.60 -5 -5 26 13.50 9.50 -5 -5 26 9.90 19.10 -5 5 26 27.40 11.20 -4 -5 26 13.10 20.30 -4 -5 26 38.80 12.90 -4 5 26 25.60 12.80 -3 -5 26 8.90 9.70 -3 -5 26 20.60 22.50 -3 5 26 18.70 12.00 -2 -5 26 56.59 14.70 -2 -5 26 25.10 23.10 -2 5 26 26.50 12.70 -1 -5 26 4.60 18.90 -1 -5 26 18.00 11.20 -1 5 26 18.10 12.00 0 -5 26 -4.00 16.10 -6 -6 26 -6.80 18.90 -6 -6 26 5.20 9.50 -6 6 26 -12.00 7.60 6 6 -26 3.00 12.50 -5 -6 26 -5.40 17.50 -5 -6 26 14.10 10.60 -5 6 26 0.60 10.30 5 6 -26 1.00 13.00 -4 -6 26 3.50 18.30 -4 -6 26 -2.00 8.80 -4 6 26 4.80 8.80 -3 -6 26 26.00 24.60 -3 -6 26 35.30 13.20 -3 6 26 62.09 15.60 -2 -6 26 5.90 9.70 -2 -6 26 32.20 23.90 -2 6 26 3.40 9.10 -1 -6 26 0.00 18.70 -5 -7 26 9.20 21.90 -4 -7 26 20.00 24.20 -3 -7 26 13.60 23.00 -2 -7 26 19.60 23.90 -7 0 27 -1.20 7.60 -7 0 27 -0.30 8.50 -6 0 27 16.20 8.60 -6 0 27 -9.70 7.90 -6 0 27 -4.50 7.50 -5 0 27 -2.40 8.40 -5 0 27 1.30 7.40 -4 0 27 8.40 9.10 -4 0 27 -0.90 8.40 -3 0 27 0.40 9.70 -3 0 27 -5.60 6.90 -2 0 27 -5.20 7.90 -2 0 27 13.90 8.60 -1 0 27 -1.90 9.10 -1 0 27 8.50 8.70 -7 -1 27 -2.40 7.90 -7 -1 27 7.60 18.60 -7 -1 27 4.00 8.80 -7 1 27 3.40 9.10 -7 1 27 21.40 10.60 -6 -1 27 -0.60 18.80 -6 -1 27 0.40 7.60 -6 -1 27 2.00 9.00 -6 1 27 -9.10 6.90 -6 1 27 5.70 8.90 -5 -1 27 -1.80 7.70 -5 -1 27 -6.60 7.20 -5 1 27 -6.90 7.10 -5 1 27 -2.00 8.00 -5 1 27 3.60 8.90 -4 -1 27 -4.80 7.80 -4 -1 27 18.90 8.10 -4 1 27 9.00 8.60 -4 1 27 12.10 10.20 -3 -1 27 -3.10 8.30 -3 -1 27 -4.90 7.60 -3 1 27 25.90 11.40 -3 1 27 -4.50 7.10 -2 -1 27 14.30 10.80 -2 -1 27 4.30 8.60 -2 1 27 -10.20 7.70 -2 1 27 0.50 8.80 -1 -1 27 6.90 10.40 -1 -1 27 30.60 11.70 -1 1 27 16.30 9.70 -1 1 27 15.60 11.40 -7 -2 27 -1.20 8.40 -7 -2 27 -5.90 17.20 -7 2 27 7.40 9.20 -7 2 27 -5.70 7.50 -6 -2 27 3.40 17.80 -6 -2 27 2.10 8.60 -6 -2 27 25.20 10.30 -6 2 27 18.60 10.80 -6 2 27 4.70 8.90 -5 -2 27 2.60 18.20 -5 -2 27 8.90 9.70 -5 -2 27 5.70 8.40 -5 2 27 -1.80 8.00 -5 2 27 5.20 9.50 -4 -2 27 10.40 20.60 -4 -2 27 10.80 9.70 -4 -2 27 12.80 9.20 -4 2 27 3.30 7.60 -4 2 27 -1.70 8.90 -3 -2 27 32.20 11.40 -3 -2 27 55.19 14.90 -3 2 27 76.09 14.90 -3 2 27 65.39 15.70 -2 -2 27 -2.60 7.60 -2 2 27 -8.60 9.20 -2 2 27 0.10 8.30 -1 -2 27 2.10 9.50 -1 2 27 1.20 9.30 -1 2 27 11.70 9.30 -7 -3 27 29.90 23.70 -6 -3 27 13.10 10.00 -6 -3 27 16.80 20.90 -6 -3 27 15.30 10.00 -6 3 27 -0.90 8.40 -6 3 27 18.80 11.50 -5 -3 27 52.89 14.00 -5 -3 27 4.90 18.50 -5 -3 27 43.80 12.80 -5 3 27 45.00 12.60 -5 3 27 29.60 12.00 -4 -3 27 46.90 13.40 -4 -3 27 49.60 14.10 -4 -3 27 45.40 24.90 -4 3 27 28.80 12.90 -3 -3 27 10.40 8.60 -3 -3 27 -3.50 18.20 -3 3 27 13.00 10.90 -2 -3 27 65.49 15.10 -2 3 27 27.90 13.60 -6 -4 27 7.20 21.00 -5 -4 27 9.70 10.40 -5 -4 27 -1.90 19.50 -5 -4 27 -1.00 8.10 -5 4 27 -8.90 8.60 -4 -4 27 24.30 11.50 -4 -4 27 16.60 22.50 -4 4 27 16.10 11.10 -3 -4 27 205.08 25.90 -3 -4 27 117.89 38.10 -3 4 27 189.98 26.40 -2 -4 27 10.60 21.10 -5 -5 27 8.50 22.60 -4 -5 27 -3.00 17.90 -3 -5 27 -9.10 18.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 81640 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.27641(3) 0.33226(2) 0.63088(2) 0.02209(9) Uani 1 1 d . . . . . P1 P 0.25507(6) 0.09430(5) 0.63033(3) 0.02462(16) Uani 1 1 d . . . . . O1 O 0.26149(16) 0.19692(12) 0.63837(10) 0.0306(5) Uani 1 1 d . . . . . N1 N 0.24534(18) 0.42143(14) 0.69994(10) 0.0245(5) Uani 1 1 d . . . . . N2 N 0.29033(18) 0.40465(14) 0.76574(10) 0.0228(5) Uani 1 1 d . . . . . N3 N 0.44748(18) 0.31685(14) 0.69544(11) 0.0238(5) Uani 1 1 d . . . . . N4 N 0.31097(19) 0.39868(15) 0.55168(10) 0.0259(5) Uani 1 1 d . . . . . N5 N 0.24622(18) 0.37722(15) 0.48919(10) 0.0242(5) Uani 1 1 d . . . . . N6 N 0.09748(18) 0.32453(15) 0.57343(11) 0.0257(5) Uani 1 1 d . . . . . C1 C 0.1966(2) 0.50447(18) 0.69662(14) 0.0285(6) Uani 1 1 d . . . . . C2 C 0.2090(2) 0.53956(19) 0.76001(14) 0.0317(7) Uani 1 1 d . . . . . H2 H 0.181350 0.597038 0.771198 0.038 Uiso 1 1 calc R U . . . C3 C 0.2690(2) 0.47494(19) 0.80348(13) 0.0274(6) Uani 1 1 d . . . . . C4 C 0.1405(3) 0.5475(2) 0.63150(15) 0.0453(8) Uani 1 1 d . . . . . H4A H 0.189672 0.538604 0.600712 0.068 Uiso 1 1 calc R U . . . H4B H 0.129985 0.613312 0.637743 0.068 Uiso 1 1 calc R U . . . H4C H 0.064913 0.518795 0.613298 0.068 Uiso 1 1 calc R U . . . C5 C 0.3037(3) 0.4738(2) 0.87749(14) 0.0400(8) Uani 1 1 d . . . . . H5A H 0.258333 0.427380 0.893923 0.060 Uiso 1 1 calc R U . . . H5B H 0.289359 0.534280 0.894419 0.060 Uiso 1 1 calc R U . . . H5C H 0.386265 0.459004 0.892681 0.060 Uiso 1 1 calc R U . . . C6 C 0.3507(2) 0.31860(18) 0.78564(13) 0.0244(6) Uani 1 1 d . . . . . H6A H 0.298456 0.266896 0.767630 0.029 Uiso 1 1 calc R U . . . H6B H 0.370822 0.313993 0.834582 0.029 Uiso 1 1 calc R U . . . C7 C 0.4600(2) 0.31044(16) 0.76165(13) 0.0222(6) Uani 1 1 d . . . . . C8 C 0.5664(2) 0.29430(19) 0.80530(14) 0.0311(6) Uani 1 1 d . . . . . H8 H 0.572949 0.289631 0.851565 0.037 Uiso 1 1 calc R U . . . C9 C 0.6625(3) 0.2851(2) 0.78055(16) 0.0393(8) Uani 1 1 d . . . . . H9 H 0.736455 0.274895 0.809735 0.047 Uiso 1 1 calc R U . . . C10 C 0.6509(3) 0.2909(2) 0.71340(16) 0.0403(8) Uani 1 1 d . . . . . H10 H 0.716309 0.284008 0.695484 0.048 Uiso 1 1 calc R U . . . C11 C 0.5422(2) 0.30681(19) 0.67239(15) 0.0325(7) Uani 1 1 d . . . . . H11 H 0.534220 0.310812 0.625961 0.039 Uiso 1 1 calc R U . . . C12 C 0.3615(2) 0.47897(19) 0.54570(14) 0.0289(6) Uani 1 1 d . . . . . C13 C 0.3309(2) 0.5078(2) 0.47999(14) 0.0340(7) Uani 1 1 d . . . . . H13 H 0.355546 0.562320 0.462538 0.041 Uiso 1 1 calc R U . . . C14 C 0.2579(2) 0.4415(2) 0.44523(13) 0.0295(6) Uani 1 1 d . . . . . C15 C 0.4381(3) 0.5265(2) 0.60387(15) 0.0407(8) Uani 1 1 d . . . . . H15A H 0.397960 0.531785 0.639403 0.061 Uiso 1 1 calc R U . . . H15B H 0.457221 0.587964 0.590624 0.061 Uiso 1 1 calc R U . . . H15C H 0.509481 0.491068 0.619738 0.061 Uiso 1 1 calc R U . . . C16 C 0.2021(3) 0.4336(2) 0.37279(14) 0.0463(9) Uani 1 1 d . . . . . H16A H 0.239304 0.384107 0.353776 0.069 Uiso 1 1 calc R U . . . H16B H 0.210916 0.491603 0.350773 0.069 Uiso 1 1 calc R U . . . H16C H 0.119652 0.419771 0.366315 0.069 Uiso 1 1 calc R U . . . C17 C 0.1779(2) 0.29310(18) 0.47955(13) 0.0262(6) Uani 1 1 d . . . . . H17A H 0.227860 0.241245 0.499917 0.031 Uiso 1 1 calc R U . . . H17B H 0.150385 0.280641 0.431477 0.031 Uiso 1 1 calc R U . . . C18 C 0.0749(2) 0.29819(17) 0.50929(13) 0.0241(6) Uani 1 1 d . . . . . C19 C -0.0355(2) 0.27416(19) 0.47388(14) 0.0303(6) Uani 1 1 d . . . . . H19 H -0.048974 0.254793 0.429067 0.036 Uiso 1 1 calc R U . . . C20 C -0.1260(2) 0.2786(2) 0.50428(15) 0.0351(7) Uani 1 1 d . . . . . H20 H -0.202493 0.262996 0.480654 0.042 Uiso 1 1 calc R U . . . C21 C -0.1030(3) 0.3061(2) 0.56961(15) 0.0370(7) Uani 1 1 d . . . . . H21 H -0.163432 0.309547 0.591785 0.044 Uiso 1 1 calc R U . . . C22 C 0.0093(2) 0.3287(2) 0.60238(14) 0.0327(7) Uani 1 1 d . . . . . H22 H 0.024500 0.347991 0.647277 0.039 Uiso 1 1 calc R U . . . C23 C 0.3967(2) 0.0433(2) 0.65194(14) 0.0338(7) Uani 1 1 d . . . . . H23A H 0.389894 -0.022656 0.640320 0.041 Uiso 1 1 calc R U . . . H23B H 0.445112 0.072571 0.625368 0.041 Uiso 1 1 calc R U . . . C24 C 0.4570(3) 0.0530(2) 0.72510(15) 0.0429(8) Uani 1 1 d . . . . . H24A H 0.537233 0.031836 0.732825 0.064 Uiso 1 1 calc R U . . . H24B H 0.416344 0.015951 0.751408 0.064 Uiso 1 1 calc R U . . . H24C H 0.456239 0.117599 0.738191 0.064 Uiso 1 1 calc R U . . . C25 C 0.1899(3) 0.06142(19) 0.54663(14) 0.0352(7) Uani 1 1 d . . . . . H25A H 0.116546 0.095878 0.531120 0.042 Uiso 1 1 calc R U . . . H25B H 0.241893 0.080164 0.518648 0.042 Uiso 1 1 calc R U . . . C26 C 0.1637(3) -0.0415(2) 0.53576(17) 0.0476(9) Uani 1 1 d . . . . . H26A H 0.130114 -0.053140 0.488543 0.071 Uiso 1 1 calc R U . . . H26B H 0.108712 -0.060450 0.561197 0.071 Uiso 1 1 calc R U . . . H26C H 0.235592 -0.076645 0.550611 0.071 Uiso 1 1 calc R U . . . C27 C 0.1723(2) 0.0453(2) 0.68252(15) 0.0369(7) Uani 1 1 d . . . . . H27A H 0.170772 -0.022247 0.677072 0.044 Uiso 1 1 calc R U . . . H27B H 0.211122 0.059024 0.729308 0.044 Uiso 1 1 calc R U . . . C28 C 0.0488(3) 0.0805(3) 0.6677(2) 0.0596(10) Uani 1 1 d . . . . . H28A H 0.009139 0.066025 0.621734 0.089 Uiso 1 1 calc R U . . . H28B H 0.049429 0.147119 0.674226 0.089 Uiso 1 1 calc R U . . . H28C H 0.008043 0.051064 0.697663 0.089 Uiso 1 1 calc R U . . . Cl1 Cl 0.51322(18) 0.21324(13) 0.49102(9) 0.0311(4) Uani 0.909(11) 1 d D U P A 1 O2 O 0.6019(3) 0.2713(4) 0.5290(2) 0.0555(12) Uani 0.909(11) 1 d D U P A 1 O3 O 0.4441(4) 0.1786(4) 0.5324(2) 0.0519(12) Uani 0.909(11) 1 d D U P A 1 O4 O 0.5640(5) 0.1406(3) 0.4623(3) 0.0614(11) Uani 0.909(11) 1 d D U P A 1 O5 O 0.4402(4) 0.2662(2) 0.43829(15) 0.0513(10) Uani 0.909(11) 1 d D U P A 1 Cl1' Cl 0.531(2) 0.2007(16) 0.4934(11) 0.045(3) Uani 0.091(11) 1 d D U P A 2 O2' O 0.625(2) 0.224(3) 0.5485(13) 0.038(5) Uani 0.091(11) 1 d D U P A 2 O3' O 0.433(3) 0.175(4) 0.517(2) 0.038(6) Uani 0.091(11) 1 d D U P A 2 O4' O 0.564(4) 0.129(2) 0.455(2) 0.045(6) Uani 0.091(11) 1 d D U P A 2 O5' O 0.499(4) 0.2805(19) 0.4518(16) 0.053(5) Uani 0.091(11) 1 d D U P A 2 Cl2 Cl 0.00125(15) 0.30932(13) 0.79375(10) 0.0305(4) Uani 0.854(6) 1 d D U P B 1 O6 O 0.0351(4) 0.3600(2) 0.85476(15) 0.0727(12) Uani 0.854(6) 1 d D U P B 1 O7 O -0.0644(3) 0.2318(2) 0.80462(19) 0.0509(9) Uani 0.854(6) 1 d D U P B 1 O8 O 0.1013(3) 0.2787(2) 0.7747(3) 0.0722(12) Uani 0.854(6) 1 d D U P B 1 O9 O -0.0650(3) 0.3666(2) 0.74289(14) 0.0505(9) Uani 0.854(6) 1 d D U P B 1 Cl2' Cl 0.0027(11) 0.3049(9) 0.7933(6) 0.052(3) Uani 0.146(6) 1 d D U P B 2 O6' O -0.0395(18) 0.3363(12) 0.8487(8) 0.051(4) Uani 0.146(6) 1 d D U P B 2 O7' O -0.0749(14) 0.2357(11) 0.7611(12) 0.062(4) Uani 0.146(6) 1 d D U P B 2 O8' O 0.1175(11) 0.2739(12) 0.8156(10) 0.054(4) Uani 0.146(6) 1 d D U P B 2 O9' O -0.0017(16) 0.3825(10) 0.7504(8) 0.043(4) Uani 0.146(6) 1 d D U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.02424(17) 0.02250(16) 0.01925(16) 0.00143(12) 0.00489(12) 0.00036(13) P1 0.0245(4) 0.0211(3) 0.0276(4) 0.0016(3) 0.0053(3) -0.0015(3) O1 0.0308(11) 0.0200(10) 0.0392(12) 0.0004(8) 0.0052(9) -0.0013(8) N1 0.0281(12) 0.0233(12) 0.0222(12) 0.0037(9) 0.0064(10) 0.0044(9) N2 0.0237(12) 0.0236(12) 0.0222(11) -0.0002(9) 0.0080(9) 0.0020(9) N3 0.0234(12) 0.0239(12) 0.0241(12) -0.0029(9) 0.0061(10) -0.0011(9) N4 0.0272(12) 0.0283(13) 0.0227(12) 0.0003(10) 0.0073(10) -0.0022(10) N5 0.0247(12) 0.0273(12) 0.0218(11) 0.0016(10) 0.0082(10) 0.0009(9) N6 0.0235(12) 0.0321(13) 0.0220(12) 0.0041(10) 0.0066(10) 0.0027(10) C1 0.0292(15) 0.0234(14) 0.0357(16) 0.0043(12) 0.0134(13) 0.0051(11) C2 0.0312(16) 0.0248(15) 0.0435(18) -0.0040(13) 0.0175(14) 0.0045(12) C3 0.0238(14) 0.0308(15) 0.0307(15) -0.0053(12) 0.0129(12) -0.0034(11) C4 0.056(2) 0.0362(18) 0.0444(19) 0.0117(15) 0.0140(17) 0.0187(16) C5 0.0405(18) 0.052(2) 0.0297(16) -0.0139(15) 0.0130(14) 0.0010(15) C6 0.0252(14) 0.0251(14) 0.0236(14) 0.0041(11) 0.0075(11) 0.0037(11) C7 0.0246(14) 0.0171(13) 0.0244(14) -0.0025(10) 0.0052(11) -0.0014(10) C8 0.0282(16) 0.0347(16) 0.0283(15) -0.0021(13) 0.0029(12) 0.0026(12) C9 0.0244(16) 0.0456(19) 0.0433(19) -0.0030(15) -0.0001(14) 0.0046(13) C10 0.0245(16) 0.052(2) 0.048(2) -0.0075(16) 0.0143(15) 0.0058(14) C11 0.0303(16) 0.0371(17) 0.0325(16) -0.0059(13) 0.0121(13) -0.0001(12) C12 0.0314(15) 0.0281(15) 0.0308(15) -0.0003(12) 0.0144(13) -0.0028(12) C13 0.0362(17) 0.0317(16) 0.0379(17) 0.0091(13) 0.0167(14) -0.0028(13) C14 0.0287(15) 0.0362(16) 0.0263(15) 0.0077(12) 0.0119(12) 0.0033(12) C15 0.0462(19) 0.0373(18) 0.0394(18) -0.0042(14) 0.0120(15) -0.0173(15) C16 0.048(2) 0.061(2) 0.0293(17) 0.0151(15) 0.0094(15) -0.0043(17) C17 0.0288(15) 0.0265(14) 0.0238(14) 0.0006(11) 0.0078(12) -0.0021(12) C18 0.0247(14) 0.0222(13) 0.0258(14) 0.0056(11) 0.0068(11) 0.0032(11) C19 0.0281(15) 0.0331(16) 0.0276(15) 0.0038(12) 0.0028(12) 0.0015(12) C20 0.0191(14) 0.0403(18) 0.0429(18) 0.0028(14) 0.0023(13) 0.0000(12) C21 0.0284(16) 0.0480(19) 0.0369(18) 0.0068(14) 0.0123(14) 0.0031(13) C22 0.0317(16) 0.0387(17) 0.0291(15) 0.0051(13) 0.0101(13) 0.0024(13) C23 0.0351(17) 0.0300(16) 0.0379(17) 0.0048(13) 0.0123(14) 0.0056(13) C24 0.0372(18) 0.0389(18) 0.0450(19) 0.0006(15) -0.0040(15) 0.0095(14) C25 0.0374(17) 0.0319(16) 0.0339(17) -0.0005(13) 0.0043(14) -0.0056(13) C26 0.050(2) 0.0402(19) 0.050(2) -0.0142(16) 0.0075(17) -0.0083(16) C27 0.0378(17) 0.0383(18) 0.0386(17) 0.0021(14) 0.0172(14) -0.0060(14) C28 0.051(2) 0.053(2) 0.088(3) 0.007(2) 0.042(2) 0.0013(18) Cl1 0.0335(7) 0.0339(7) 0.0292(6) -0.0065(5) 0.0140(5) -0.0061(5) O2 0.0463(18) 0.065(3) 0.058(2) -0.0205(19) 0.0192(16) -0.0309(18) O3 0.048(2) 0.065(2) 0.048(3) 0.006(2) 0.0230(17) -0.0190(17) O4 0.073(2) 0.059(2) 0.055(2) -0.0173(18) 0.0211(19) 0.023(2) O5 0.060(3) 0.0507(18) 0.0421(17) 0.0058(13) 0.0105(16) 0.0109(16) Cl1' 0.045(5) 0.054(6) 0.043(5) 0.007(5) 0.023(5) -0.014(5) O2' 0.029(9) 0.052(11) 0.037(10) -0.018(9) 0.015(8) -0.019(9) O3' 0.024(10) 0.060(11) 0.036(11) -0.001(10) 0.017(9) -0.012(10) O4' 0.050(11) 0.046(11) 0.044(11) -0.004(10) 0.023(10) 0.000(10) O5' 0.059(10) 0.051(9) 0.051(9) 0.016(8) 0.016(9) -0.010(9) Cl2 0.0266(7) 0.0299(8) 0.0389(8) 0.0036(7) 0.0153(7) -0.0027(6) O6 0.108(3) 0.051(2) 0.0481(19) 0.0011(15) -0.001(2) -0.026(2) O7 0.0441(17) 0.0506(18) 0.062(2) 0.0049(16) 0.0210(17) -0.0208(13) O8 0.0362(19) 0.082(2) 0.110(3) 0.025(2) 0.041(2) 0.0156(16) O9 0.056(2) 0.057(2) 0.0386(16) 0.0102(14) 0.0120(16) 0.0181(17) Cl2' 0.054(5) 0.047(5) 0.046(5) 0.017(5) -0.004(5) 0.000(5) O6' 0.073(8) 0.050(8) 0.040(7) -0.003(6) 0.031(7) 0.021(7) O7' 0.047(7) 0.048(8) 0.086(9) -0.009(8) 0.007(8) -0.013(6) O8' 0.042(7) 0.063(8) 0.050(8) 0.034(7) -0.001(7) 0.003(6) O9' 0.033(7) 0.056(8) 0.044(7) 0.019(6) 0.020(7) 0.010(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Zn1 N1 122.70(8) . . ? O1 Zn1 N4 124.97(8) . . ? N1 Zn1 N4 112.15(9) . . ? O1 Zn1 N3 86.39(8) . . ? N1 Zn1 N3 86.35(8) . . ? N4 Zn1 N3 101.72(9) . . ? O1 Zn1 N6 84.10(8) . . ? N1 Zn1 N6 95.47(8) . . ? N4 Zn1 N6 87.02(8) . . ? N3 Zn1 N6 169.70(8) . . ? O1 P1 C25 111.86(12) . . ? O1 P1 C27 110.46(13) . . ? C25 P1 C27 108.29(14) . . ? O1 P1 C23 111.35(13) . . ? C25 P1 C23 106.66(14) . . ? C27 P1 C23 108.05(14) . . ? P1 O1 Zn1 168.36(13) . . ? C1 N1 N2 105.7(2) . . ? C1 N1 Zn1 133.88(18) . . ? N2 N1 Zn1 119.98(15) . . ? C3 N2 N1 111.4(2) . . ? C3 N2 C6 129.7(2) . . ? N1 N2 C6 119.0(2) . . ? C11 N3 C7 118.0(2) . . ? C11 N3 Zn1 122.55(19) . . ? C7 N3 Zn1 119.30(17) . . ? C12 N4 N5 105.7(2) . . ? C12 N4 Zn1 132.62(18) . . ? N5 N4 Zn1 118.62(16) . . ? C14 N5 N4 111.0(2) . . ? C14 N5 C17 130.0(2) . . ? N4 N5 C17 119.0(2) . . ? C22 N6 C18 118.3(2) . . ? C22 N6 Zn1 121.56(18) . . ? C18 N6 Zn1 119.04(17) . . ? N1 C1 C2 110.0(2) . . ? N1 C1 C4 121.2(3) . . ? C2 C1 C4 128.8(3) . . ? C3 C2 C1 106.7(2) . . ? C3 C2 H2 126.6 . . ? C1 C2 H2 126.6 . . ? N2 C3 C2 106.1(2) . . ? N2 C3 C5 123.2(3) . . ? C2 C3 C5 130.6(3) . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? N2 C6 C7 112.3(2) . . ? N2 C6 H6A 109.1 . . ? C7 C6 H6A 109.1 . . ? N2 C6 H6B 109.1 . . ? C7 C6 H6B 109.1 . . ? H6A C6 H6B 107.9 . . ? N3 C7 C8 122.1(2) . . ? N3 C7 C6 116.5(2) . . ? C8 C7 C6 121.4(2) . . ? C9 C8 C7 118.9(3) . . ? C9 C8 H8 120.6 . . ? C7 C8 H8 120.6 . . ? C10 C9 C8 119.6(3) . . ? C10 C9 H9 120.2 . . ? C8 C9 H9 120.2 . . ? C9 C10 C11 118.7(3) . . ? C9 C10 H10 120.7 . . ? C11 C10 H10 120.7 . . ? N3 C11 C10 122.7(3) . . ? N3 C11 H11 118.6 . . ? C10 C11 H11 118.6 . . ? N4 C12 C13 110.1(2) . . ? N4 C12 C15 122.0(2) . . ? C13 C12 C15 128.0(3) . . ? C14 C13 C12 106.3(2) . . ? C14 C13 H13 126.8 . . ? C12 C13 H13 126.8 . . ? N5 C14 C13 106.9(2) . . ? N5 C14 C16 122.7(3) . . ? C13 C14 C16 130.4(3) . . ? C12 C15 H15A 109.5 . . ? C12 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C12 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C14 C16 H16A 109.5 . . ? C14 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C14 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? N5 C17 C18 112.7(2) . . ? N5 C17 H17A 109.0 . . ? C18 C17 H17A 109.0 . . ? N5 C17 H17B 109.0 . . ? C18 C17 H17B 109.0 . . ? H17A C17 H17B 107.8 . . ? N6 C18 C19 121.8(3) . . ? N6 C18 C17 116.0(2) . . ? C19 C18 C17 122.2(2) . . ? C20 C19 C18 119.4(3) . . ? C20 C19 H19 120.3 . . ? C18 C19 H19 120.3 . . ? C21 C20 C19 118.7(3) . . ? C21 C20 H20 120.7 . . ? C19 C20 H20 120.7 . . ? C20 C21 C22 119.1(3) . . ? C20 C21 H21 120.4 . . ? C22 C21 H21 120.4 . . ? N6 C22 C21 122.7(3) . . ? N6 C22 H22 118.7 . . ? C21 C22 H22 118.7 . . ? C24 C23 P1 113.1(2) . . ? C24 C23 H23A 109.0 . . ? P1 C23 H23A 109.0 . . ? C24 C23 H23B 109.0 . . ? P1 C23 H23B 109.0 . . ? H23A C23 H23B 107.8 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C26 C25 P1 115.3(2) . . ? C26 C25 H25A 108.4 . . ? P1 C25 H25A 108.4 . . ? C26 C25 H25B 108.4 . . ? P1 C25 H25B 108.4 . . ? H25A C25 H25B 107.5 . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C28 C27 P1 113.4(2) . . ? C28 C27 H27A 108.9 . . ? P1 C27 H27A 108.9 . . ? C28 C27 H27B 108.9 . . ? P1 C27 H27B 108.9 . . ? H27A C27 H27B 107.7 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? O4 Cl1 O3 111.2(2) . . ? O4 Cl1 O2 109.8(2) . . ? O3 Cl1 O2 109.6(2) . . ? O4 Cl1 O5 108.5(2) . . ? O3 Cl1 O5 108.6(2) . . ? O2 Cl1 O5 109.1(2) . . ? O4' Cl1' O2' 111.1(13) . . ? O4' Cl1' O3' 111.3(13) . . ? O2' Cl1' O3' 108.9(13) . . ? O4' Cl1' O5' 108.9(13) . . ? O2' Cl1' O5' 109.2(13) . . ? O3' Cl1' O5' 107.5(13) . . ? O8 Cl2 O9 108.9(2) . . ? O8 Cl2 O7 109.2(2) . . ? O9 Cl2 O7 111.0(2) . . ? O8 Cl2 O6 109.8(3) . . ? O9 Cl2 O6 109.8(2) . . ? O7 Cl2 O6 108.1(2) . . ? O8' Cl2' O7' 113.2(11) . . ? O8' Cl2' O9' 109.9(10) . . ? O7' Cl2' O9' 110.3(11) . . ? O8' Cl2' O6' 110.1(11) . . ? O7' Cl2' O6' 106.7(11) . . ? O9' Cl2' O6' 106.4(10) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 O1 1.9895(18) . ? Zn1 N1 2.040(2) . ? Zn1 N4 2.042(2) . ? Zn1 N3 2.157(2) . ? Zn1 N6 2.174(2) . ? P1 O1 1.5044(19) . ? P1 C25 1.789(3) . ? P1 C27 1.790(3) . ? P1 C23 1.797(3) . ? N1 C1 1.336(3) . ? N1 N2 1.364(3) . ? N2 C3 1.353(3) . ? N2 C6 1.454(3) . ? N3 C11 1.341(3) . ? N3 C7 1.353(3) . ? N4 C12 1.336(3) . ? N4 N5 1.374(3) . ? N5 C14 1.342(3) . ? N5 C17 1.458(3) . ? N6 C22 1.338(3) . ? N6 C18 1.352(3) . ? C1 C2 1.389(4) . ? C1 C4 1.493(4) . ? C2 C3 1.377(4) . ? C2 H2 0.9500 . ? C3 C5 1.494(4) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.512(3) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C8 1.385(4) . ? C8 C9 1.375(4) . ? C8 H8 0.9500 . ? C9 C10 1.374(4) . ? C9 H9 0.9500 . ? C10 C11 1.384(4) . ? C10 H10 0.9500 . ? C11 H11 0.9500 . ? C12 C13 1.391(4) . ? C12 C15 1.494(4) . ? C13 C14 1.379(4) . ? C13 H13 0.9500 . ? C14 C16 1.494(4) . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 C18 1.509(4) . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C18 C19 1.384(4) . ? C19 C20 1.383(4) . ? C19 H19 0.9500 . ? C20 C21 1.379(4) . ? C20 H20 0.9500 . ? C21 C22 1.383(4) . ? C21 H21 0.9500 . ? C22 H22 0.9500 . ? C23 C24 1.521(4) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 C26 1.537(4) . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 C28 1.517(4) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? Cl1 O4 1.424(3) . ? Cl1 O3 1.427(3) . ? Cl1 O2 1.430(3) . ? Cl1 O5 1.444(3) . ? Cl1' O4' 1.421(9) . ? Cl1' O2' 1.428(9) . ? Cl1' O3' 1.430(9) . ? Cl1' O5' 1.444(9) . ? Cl2 O8 1.420(3) . ? Cl2 O9 1.423(3) . ? Cl2 O7 1.424(3) . ? Cl2 O6 1.438(3) . ? Cl2' O8' 1.407(9) . ? Cl2' O7' 1.419(9) . ? Cl2' O9' 1.434(9) . ? Cl2' O6' 1.443(9) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C25 P1 O1 Zn1 -36.7(7) . . . . ? C27 P1 O1 Zn1 -157.4(6) . . . . ? C23 P1 O1 Zn1 82.5(6) . . . . ? C1 N1 N2 C3 1.0(3) . . . . ? Zn1 N1 N2 C3 174.66(16) . . . . ? C1 N1 N2 C6 -179.5(2) . . . . ? Zn1 N1 N2 C6 -5.8(3) . . . . ? C12 N4 N5 C14 1.2(3) . . . . ? Zn1 N4 N5 C14 163.89(17) . . . . ? C12 N4 N5 C17 -178.7(2) . . . . ? Zn1 N4 N5 C17 -16.1(3) . . . . ? N2 N1 C1 C2 -1.0(3) . . . . ? Zn1 N1 C1 C2 -173.38(19) . . . . ? N2 N1 C1 C4 178.4(3) . . . . ? Zn1 N1 C1 C4 6.0(4) . . . . ? N1 C1 C2 C3 0.6(3) . . . . ? C4 C1 C2 C3 -178.7(3) . . . . ? N1 N2 C3 C2 -0.6(3) . . . . ? C6 N2 C3 C2 179.9(2) . . . . ? N1 N2 C3 C5 177.3(2) . . . . ? C6 N2 C3 C5 -2.1(4) . . . . ? C1 C2 C3 N2 0.0(3) . . . . ? C1 C2 C3 C5 -177.7(3) . . . . ? C3 N2 C6 C7 -115.9(3) . . . . ? N1 N2 C6 C7 64.6(3) . . . . ? C11 N3 C7 C8 0.2(4) . . . . ? Zn1 N3 C7 C8 175.57(19) . . . . ? C11 N3 C7 C6 -177.8(2) . . . . ? Zn1 N3 C7 C6 -2.4(3) . . . . ? N2 C6 C7 N3 -57.8(3) . . . . ? N2 C6 C7 C8 124.2(3) . . . . ? N3 C7 C8 C9 0.5(4) . . . . ? C6 C7 C8 C9 178.3(3) . . . . ? C7 C8 C9 C10 -0.9(4) . . . . ? C8 C9 C10 C11 0.7(5) . . . . ? C7 N3 C11 C10 -0.4(4) . . . . ? Zn1 N3 C11 C10 -175.6(2) . . . . ? C9 C10 C11 N3 0.0(5) . . . . ? N5 N4 C12 C13 -1.0(3) . . . . ? Zn1 N4 C12 C13 -160.2(2) . . . . ? N5 N4 C12 C15 178.8(2) . . . . ? Zn1 N4 C12 C15 19.6(4) . . . . ? N4 C12 C13 C14 0.5(3) . . . . ? C15 C12 C13 C14 -179.3(3) . . . . ? N4 N5 C14 C13 -0.9(3) . . . . ? C17 N5 C14 C13 179.0(2) . . . . ? N4 N5 C14 C16 176.7(3) . . . . ? C17 N5 C14 C16 -3.4(4) . . . . ? C12 C13 C14 N5 0.3(3) . . . . ? C12 C13 C14 C16 -177.1(3) . . . . ? C14 N5 C17 C18 -109.1(3) . . . . ? N4 N5 C17 C18 70.8(3) . . . . ? C22 N6 C18 C19 -1.2(4) . . . . ? Zn1 N6 C18 C19 166.8(2) . . . . ? C22 N6 C18 C17 -179.0(2) . . . . ? Zn1 N6 C18 C17 -10.9(3) . . . . ? N5 C17 C18 N6 -52.0(3) . . . . ? N5 C17 C18 C19 130.3(3) . . . . ? N6 C18 C19 C20 1.2(4) . . . . ? C17 C18 C19 C20 178.8(2) . . . . ? C18 C19 C20 C21 -0.7(4) . . . . ? C19 C20 C21 C22 0.3(4) . . . . ? C18 N6 C22 C21 0.8(4) . . . . ? Zn1 N6 C22 C21 -166.9(2) . . . . ? C20 C21 C22 N6 -0.4(5) . . . . ? O1 P1 C23 C24 66.3(2) . . . . ? C25 P1 C23 C24 -171.5(2) . . . . ? C27 P1 C23 C24 -55.2(3) . . . . ? O1 P1 C25 C26 -171.5(2) . . . . ? C27 P1 C25 C26 -49.6(3) . . . . ? C23 P1 C25 C26 66.5(3) . . . . ? O1 P1 C27 C28 59.8(3) . . . . ? C25 P1 C27 C28 -63.0(3) . . . . ? C23 P1 C27 C28 -178.1(2) . . . . ?