#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:34:55 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296381 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572755.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572755 loop_ _publ_author_name 'Anju, Balakrishnan S.' 'Nair, Neeraja R.' 'Rajput, Janavi' 'Bertke, Jeffery A.' 'Mondal, Bhaskar' 'Kundu, Subrata' _publ_section_title ; Role of ancillary ligands in S-nitrosothiol and NO generation from nitrite-thiol interactions at mononuclear zinc(ii) sites. ; _journal_issue 43 _journal_name_full 'Chemical science' _journal_page_first 18000 _journal_page_last 18007 _journal_paper_doi 10.1039/d4sc04853a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C60 H61 N12 O Zn2, 3(Cl O4), 2(C2 H3 N)' _chemical_formula_sum 'C64 H67 Cl3 N14 O13 Zn2' _chemical_formula_weight 1477.40 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary intrinsic _audit_creation_method SHELXL-2019/3 _audit_update_record ; 2024-07-19 deposited with the CCDC. 2024-10-03 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 128.178(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 32.352(6) _cell_length_b 11.149(2) _cell_length_c 23.519(7) _cell_measurement_reflns_used 4572 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 22.43 _cell_measurement_theta_min 2.20 _cell_volume 6669(3) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELX-2018-3 (Sheldrick, 2015)' _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker APEX DUO/ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1515 _diffrn_reflns_av_unetI/netI 0.0801 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 38 _diffrn_reflns_limit_h_min -38 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 88359 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.475 _diffrn_reflns_theta_min 1.994 _exptl_absorpt_coefficient_mu 0.913 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.6757 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.472 _exptl_crystal_density_method 'not measured' _exptl_crystal_description needle _exptl_crystal_F_000 3056 _exptl_crystal_size_max 0.100 _exptl_crystal_size_mid 0.050 _exptl_crystal_size_min 0.030 _refine_diff_density_max 0.624 _refine_diff_density_min -0.412 _refine_diff_density_rms 0.071 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.010 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 515 _refine_ls_number_reflns 6190 _refine_ls_number_restraints 785 _refine_ls_restrained_S_all 1.013 _refine_ls_R_factor_all 0.1492 _refine_ls_R_factor_gt 0.0605 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0715P)^2^+16.2645P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1366 _refine_ls_wR_factor_ref 0.1799 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3074 _reflns_number_total 6190 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04853a2.cif _cod_data_source_block monoC_a _cod_depositor_comments 'Adding full bibliography for 1572750--1572760.cif.' _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 1572755 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.914 _shelx_estimated_absorpt_t_max 0.973 _shelx_res_file ; TITL monoC_a.res in C2/c monoC_a.res created by SHELXL-2019/3 at 09:40:11 on 17-Jul-2024 REM Old TITL monoC in C2/c REM SHELXT solution in C2/c: R1 0.497, Rweak 0.129, Alpha 0.102 REM 0.449 for 341 systematic absences, Orientation as input REM Formula found by SHELXT: C66 Cl3 N14 O5 P2 CELL 0.71073 32.3516 11.1490 23.5194 90.000 128.178 90.000 ZERR 4.000 0.0057 0.0020 0.0072 0.000 0.005 0.000 LATT 7 SYMM -X, Y, 1/2-Z SFAC C H Cl N O Zn UNIT 256 268 12 56 52 8 LIST 4 TEMP -123.15 SIZE 0.030 0.050 0.100 L.S. 20 FMAP 2 PLAN 20 SIMU 0.01 0.02 CL1 > O5' ISOR 0.01 0.01 CL1 > C32 SIMU 0.01 0.02 CL2 > O7' EXYZ CL2 CL2' EADP CL2 CL2' SIMU 0.01 0.02 ZN1 ZN1' RIGU ACTA OMIT 2 0 0 CONF BOND $H WGHT 0.071500 16.264500 FVAR 0.15017 0.51486 0.62274 0.53083 PART 1 41 ZN1 6 0.526700 0.025541 0.347550 41.00000 0.05635 0.04385 = 0.03554 -0.00047 0.02234 0.00461 PART 2 -41 ZN1' 6 0.551255 0.043224 0.353528 -41.00000 0.04199 0.03977 = 0.03468 -0.00326 0.02121 0.00360 PART 0 O1 5 0.500000 0.033134 0.250000 10.50000 0.03262 0.04977 = 0.03743 0.00000 0.02126 0.00000 AFIX 4 H1 2 0.471573 0.036830 0.240135 10.50000 -1.20000 AFIX 0 N1 4 0.561885 -0.114673 0.410751 11.00000 0.05518 0.06001 = 0.03590 0.00954 0.02470 0.02054 N2 4 0.588878 -0.201002 0.404569 11.00000 0.04972 0.04336 = 0.04985 0.00724 0.03186 0.01110 N3 4 0.616517 0.017881 0.361245 11.00000 0.03855 0.04467 = 0.03890 -0.00183 0.02125 0.00588 N4 4 0.555119 0.176837 0.411684 11.00000 0.03985 0.05991 = 0.04764 -0.01537 0.02462 -0.00217 N5 4 0.520088 0.266413 0.388879 11.00000 0.04837 0.04289 = 0.05748 -0.01693 0.03601 -0.00991 N6 4 0.448066 0.057080 0.318201 11.00000 0.03845 0.04061 = 0.03907 -0.00079 0.02394 -0.00120 C1 1 0.564397 -0.148461 0.467372 11.00000 0.04618 0.07655 = 0.03455 0.00273 0.01947 0.01022 C2 1 0.591815 -0.253392 0.495601 11.00000 0.05116 0.06958 = 0.04034 0.01541 0.02268 0.00340 AFIX 43 H2 2 0.598776 -0.295946 0.535695 11.00000 -1.20000 AFIX 0 C3 1 0.607325 -0.285558 0.455302 11.00000 0.04339 0.04612 = 0.04898 0.00562 0.02215 -0.00137 C4 1 0.539161 -0.075792 0.491273 11.00000 0.06551 0.12270 = 0.04728 0.00817 0.03449 0.03114 AFIX 137 H4A 2 0.563895 -0.064984 0.543840 11.00000 -1.50000 H4B 2 0.507638 -0.117209 0.478215 11.00000 -1.50000 H4C 2 0.529300 0.002764 0.467531 11.00000 -1.50000 AFIX 0 C5 1 0.637748 -0.391028 0.460723 11.00000 0.07163 0.05142 = 0.07250 0.01339 0.03852 0.01657 AFIX 137 H5A 2 0.648245 -0.440416 0.502194 11.00000 -1.50000 H5B 2 0.669191 -0.363447 0.467224 11.00000 -1.50000 H5C 2 0.615854 -0.438709 0.416323 11.00000 -1.50000 AFIX 0 C6 1 0.593239 -0.191768 0.346875 11.00000 0.06292 0.04272 = 0.05587 0.00157 0.04342 0.00747 AFIX 23 H6A 2 0.558036 -0.175794 0.300649 11.00000 -1.20000 H6B 2 0.605845 -0.269173 0.342112 11.00000 -1.20000 AFIX 0 C7 1 0.630310 -0.093702 0.360623 11.00000 0.04862 0.04831 = 0.03616 0.00525 0.02401 0.01449 C8 1 0.676040 -0.123081 0.370611 11.00000 0.05360 0.05095 = 0.06212 0.01166 0.03709 0.02058 AFIX 43 H8 2 0.684451 -0.204572 0.370240 11.00000 -1.20000 AFIX 0 C9 1 0.708624 -0.034067 0.380918 11.00000 0.04549 0.07157 = 0.06747 0.00487 0.03340 0.01712 AFIX 43 H9 2 0.740053 -0.053016 0.387742 11.00000 -1.20000 AFIX 0 C10 1 0.695978 0.085462 0.381502 11.00000 0.03746 0.06111 = 0.05142 -0.00672 0.02411 0.00253 C11 1 0.726893 0.182784 0.389275 11.00000 0.05037 0.07763 = 0.11158 -0.01692 0.05028 -0.01200 AFIX 43 H11 2 0.758715 0.168090 0.396356 11.00000 -1.20000 AFIX 0 C12 1 0.711764 0.296321 0.386762 11.00000 0.06946 0.06451 = 0.13865 -0.02701 0.06944 -0.02321 AFIX 43 H12 2 0.732965 0.361031 0.391939 11.00000 -1.20000 AFIX 0 C13 1 0.665066 0.320145 0.376590 11.00000 0.06856 0.05578 = 0.11269 -0.02630 0.05776 -0.01309 AFIX 43 H13 2 0.655074 0.400655 0.375728 11.00000 -1.20000 AFIX 0 C14 1 0.633991 0.228014 0.367938 11.00000 0.05087 0.05486 = 0.06362 -0.01313 0.03466 -0.00206 AFIX 43 H14 2 0.602104 0.244822 0.360301 11.00000 -1.20000 AFIX 0 C15 1 0.648400 0.109792 0.370155 11.00000 0.03587 0.05069 = 0.03885 -0.00455 0.01809 0.00239 C16 1 0.596338 0.203655 0.480277 11.00000 0.04769 0.09128 = 0.04783 -0.02636 0.02655 -0.02123 C17 1 0.586441 0.310240 0.499102 11.00000 0.07582 0.08397 = 0.05917 -0.03734 0.04697 -0.03901 AFIX 43 H17 2 0.609221 0.349669 0.544460 11.00000 -1.20000 AFIX 0 C18 1 0.538137 0.349405 0.441162 11.00000 0.07691 0.05254 = 0.07423 -0.02503 0.06046 -0.02433 C19 1 0.644080 0.127529 0.523515 11.00000 0.04248 0.15414 = 0.05256 -0.01761 0.01570 0.00143 AFIX 137 H19A 2 0.668756 0.161156 0.572247 11.00000 -1.50000 H19B 2 0.660780 0.125029 0.500181 11.00000 -1.50000 H19C 2 0.634261 0.046084 0.526696 11.00000 -1.50000 AFIX 0 C20 1 0.507970 0.458074 0.430383 11.00000 0.13420 0.05454 = 0.10812 -0.02455 0.09441 -0.01271 AFIX 137 H20A 2 0.474148 0.434785 0.418266 11.00000 -1.50000 H20B 2 0.501834 0.505824 0.390817 11.00000 -1.50000 H20C 2 0.527900 0.505762 0.474910 11.00000 -1.50000 AFIX 0 C21 1 0.470033 0.261843 0.317616 11.00000 0.04788 0.03463 = 0.05641 -0.00184 0.03366 0.00431 AFIX 23 H21A 2 0.475817 0.242693 0.281911 11.00000 -1.20000 H21B 2 0.453117 0.341695 0.305351 11.00000 -1.20000 AFIX 0 C22 1 0.434072 0.170282 0.312370 11.00000 0.04050 0.04228 = 0.04069 -0.00290 0.02758 0.00012 C23 1 0.388328 0.205784 0.301422 11.00000 0.05107 0.04823 = 0.05683 -0.00231 0.03732 0.00626 AFIX 43 H23 2 0.379782 0.288429 0.297524 11.00000 -1.20000 AFIX 0 C24 1 0.356254 0.121263 0.296414 11.00000 0.04660 0.06977 = 0.06206 -0.00279 0.04020 0.00298 AFIX 43 H24 2 0.324892 0.144489 0.288731 11.00000 -1.20000 AFIX 0 C25 1 0.368993 0.000842 0.302455 11.00000 0.04382 0.06108 = 0.04143 -0.00132 0.02815 -0.00421 C26 1 0.337908 -0.094794 0.297261 11.00000 0.05118 0.08140 = 0.06003 0.00057 0.03809 -0.01596 AFIX 43 H26 2 0.306101 -0.076744 0.289595 11.00000 -1.20000 AFIX 0 C27 1 0.351947 -0.209427 0.302810 11.00000 0.06654 0.06800 = 0.07600 0.00737 0.04381 -0.01989 AFIX 43 H27 2 0.330617 -0.271140 0.300289 11.00000 -1.20000 AFIX 0 C28 1 0.397470 -0.238921 0.312229 11.00000 0.06553 0.04630 = 0.06907 0.01043 0.03550 -0.00503 AFIX 43 H28 2 0.406699 -0.320791 0.314996 11.00000 -1.20000 AFIX 0 C29 1 0.429047 -0.151307 0.317540 11.00000 0.04836 0.04259 = 0.05187 0.00594 0.02437 -0.00306 AFIX 43 H29 2 0.460377 -0.172475 0.324601 11.00000 -1.20000 AFIX 0 C30 1 0.415618 -0.029943 0.312654 11.00000 0.04017 0.04482 = 0.03358 0.00065 0.02177 -0.00350 PART 1 21 CL1 3 0.679498 0.537528 0.676023 21.00000 0.05884 0.03588 = 0.05995 -0.00261 0.03076 0.00122 O2 5 0.691735 0.523355 0.742538 21.00000 0.14332 0.11715 = 0.07091 0.00263 0.05490 0.01661 O3 5 0.624648 0.536618 0.621154 21.00000 0.04747 0.06747 = 0.06478 -0.00117 0.01786 0.00806 O4 5 0.701290 0.446407 0.660670 21.00000 0.07255 0.08073 = 0.10198 -0.01882 0.05907 0.01259 O5 5 0.697347 0.652149 0.673675 21.00000 0.07249 0.05016 = 0.11222 0.00433 0.02895 -0.01495 PART 2 -21 SAME 0.01 CL1 > O5 CL1' 3 0.687417 0.536997 0.679057 -21.00000 0.04404 0.04359 = 0.07036 0.00581 0.03425 0.00155 O2' 5 0.711037 0.612597 0.737592 -21.00000 0.06348 0.08854 = 0.09006 -0.03890 0.03728 0.00626 O3' 5 0.635741 0.510239 0.651632 -21.00000 0.05044 0.07238 = 0.10972 -0.00349 0.04135 -0.00122 O4' 5 0.717782 0.432061 0.699149 -21.00000 0.06485 0.05455 = 0.08856 0.01107 0.04504 0.01019 O5' 5 0.688062 0.594177 0.625802 -21.00000 0.10871 0.12607 = 0.09141 0.02896 0.05989 0.01482 PART 0 PART 1 CL2 3 0.500000 0.461379 0.750000 30.50000 0.07745 0.05026 = 0.06580 0.00000 0.03951 0.00000 O6 5 0.546484 0.526308 0.798585 31.00000 0.07414 0.08989 = 0.09840 0.00431 0.03058 -0.02501 O7 5 0.501973 0.374454 0.706616 31.00000 0.08675 0.07713 = 0.09551 -0.00350 0.05295 0.01166 PART 2 SAME 0.01 CL2 > O7 CL2' 3 0.500000 0.461379 0.750000 -30.50000 0.07745 0.05026 = 0.06580 0.00000 0.03951 0.00000 O6' 5 0.533346 0.549076 0.804291 -31.00000 0.05755 0.06886 = 0.07526 -0.00834 0.04549 -0.00035 O7' 5 0.528482 0.410021 0.726913 -31.00000 0.09711 0.08716 = 0.08915 -0.00282 0.06310 0.02415 PART 0 N7 4 0.755448 0.902457 0.555824 11.00000 0.23639 0.16786 = 0.18240 0.00725 0.15673 0.02624 C31 1 0.742072 0.882192 0.589551 11.00000 0.12906 0.07113 = 0.11196 0.00937 0.07624 0.02903 C32 1 0.727247 0.861989 0.631381 11.00000 0.10589 0.12993 = 0.10791 -0.00191 0.06285 -0.00664 AFIX 137 H32A 2 0.738960 0.781996 0.653082 11.00000 -1.50000 H32B 2 0.688861 0.866810 0.601606 11.00000 -1.50000 H32C 2 0.743185 0.922535 0.669740 11.00000 -1.50000 AFIX 0 HKLF 4 REM monoC_a.res in C2/c REM wR2 = 0.1799, GooF = S = 1.010, Restrained GooF = 1.013 for all data REM R1 = 0.0605 for 3074 Fo > 4sig(Fo) and 0.1492 for all 6190 data REM 515 parameters refined using 785 restraints END WGHT 0.0715 16.2643 REM Highest difference peak 0.624, deepest hole -0.412, 1-sigma level 0.071 Q1 1 0.6567 0.4942 0.7183 11.00000 0.05 0.62 Q2 1 0.7182 0.4649 0.7509 11.00000 0.05 0.53 Q3 1 0.8042 0.8993 0.6322 11.00000 0.05 0.44 Q4 1 0.5539 0.4652 0.7587 11.00000 0.05 0.38 Q5 1 0.6876 0.5107 0.6187 11.00000 0.05 0.35 Q6 1 0.7028 0.6565 0.7083 11.00000 0.05 0.32 Q7 1 0.6416 0.5932 0.6111 11.00000 0.05 0.32 Q8 1 0.7070 0.6399 0.6459 11.00000 0.05 0.31 Q9 1 0.5340 0.4588 0.8185 11.00000 0.05 0.29 Q10 1 0.6567 0.5905 0.3296 11.00000 0.05 0.29 Q11 1 0.7091 0.5634 0.7493 11.00000 0.05 0.28 Q12 1 0.6080 -0.4641 0.4787 11.00000 0.05 0.27 Q13 1 0.6080 -0.3817 0.4432 11.00000 0.05 0.25 Q14 1 0.6355 0.4813 0.6084 11.00000 0.05 0.23 Q15 1 0.5369 0.3015 0.4732 11.00000 0.05 0.22 Q16 1 0.5585 0.4802 0.5084 11.00000 0.05 0.22 Q17 1 0.6365 -0.3315 0.3910 11.00000 0.05 0.22 Q18 1 0.6028 -0.4712 0.4196 11.00000 0.05 0.22 Q19 1 0.6741 -0.3215 0.4182 11.00000 0.05 0.21 Q20 1 0.6367 0.2888 0.4503 11.00000 0.05 0.21 ; _shelx_res_checksum 75542 _shelx_hkl_file ; 4 0 -4 35.60 5.40 4 0 -4 45.30 6.20 -4 0 4 36.90 4.60 -4 0 4 46.50 6.10 -4 0 4 30.20 4.90 -4 0 4 49.70 4.80 -4 0 4 49.90 5.30 4 0 -4 54.29 6.10 -4 0 4 59.59 6.00 -4 0 4 44.90 5.70 -4 0 4 45.50 5.90 4 0 -4 47.20 5.20 -4 0 4 46.90 6.00 4 0 -4 50.69 6.40 4 0 -4 45.20 5.00 4 0 -4 46.80 4.40 6 0 -6 5.40 3.30 -6 0 6 7.00 4.50 6 0 -6 2.20 4.80 -6 0 6 7.50 3.80 6 0 -6 0.40 4.60 -6 0 6 4.80 3.40 -6 0 6 3.50 5.30 6 0 -6 11.80 5.70 6 0 -6 7.60 4.50 -6 0 6 8.20 5.50 -6 0 6 -0.80 4.80 -6 0 6 9.70 5.30 -6 0 6 19.70 5.90 8 0 -8 2.80 6.00 8 0 -8 5.30 6.70 8 0 -8 10.40 5.30 8 0 -8 5.60 5.00 -8 0 8 6.10 4.50 -8 0 8 21.80 7.40 -8 0 8 1.60 5.10 8 0 -8 16.20 6.20 8 0 -8 17.70 6.00 8 0 -8 17.70 4.70 -8 0 8 25.20 7.20 -8 0 8 23.00 6.90 -8 0 8 13.00 4.80 -8 0 8 0.70 4.80 -8 0 8 5.20 6.00 8 0 -8 11.90 6.50 -10 0 10 111.29 12.90 10 0 -10 74.99 12.70 -10 0 10 77.79 12.30 -10 0 10 57.59 11.20 -10 0 10 88.09 11.10 -10 0 10 97.09 11.20 10 0 -10 92.59 10.60 -10 0 10 78.09 12.00 10 0 -10 90.99 9.50 10 0 -10 73.09 11.50 10 0 -10 96.29 12.40 10 0 -10 80.59 12.80 -10 0 10 94.89 14.50 -12 0 12 340.67 26.70 12 0 -12 301.07 25.30 -12 0 12 339.87 24.00 -12 0 12 287.17 25.00 12 0 -12 304.57 24.80 -12 0 12 307.47 26.20 12 0 -12 314.87 23.40 -12 0 12 325.37 23.40 -12 0 12 306.97 28.40 12 0 -12 266.87 28.10 12 0 -12 328.17 27.30 -14 0 14 224.08 23.90 -14 0 14 222.88 23.90 14 0 -14 225.08 24.60 14 0 -14 191.88 23.20 -14 0 14 235.88 20.50 -14 0 14 203.58 19.20 14 0 -14 209.68 21.30 14 0 -14 237.68 22.80 14 0 -14 240.38 20.70 -14 0 14 196.78 24.30 -16 0 16 332.67 32.60 16 0 -16 340.17 27.90 16 0 -16 317.17 26.10 -16 0 16 313.57 26.30 -16 0 16 384.96 35.40 -16 0 16 338.77 32.90 16 0 -16 330.77 33.70 16 0 -16 295.47 32.70 -16 0 16 290.27 30.00 -18 0 18 34.80 14.70 18 0 -18 37.80 15.70 -18 0 18 56.09 14.00 -18 0 18 79.39 17.30 -18 0 18 45.80 17.00 18 0 -18 84.59 13.10 18 0 -18 85.89 16.40 18 0 -18 46.60 17.40 20 0 -20 135.79 17.10 -20 0 20 141.69 20.60 20 0 -20 166.68 26.60 20 0 -20 98.69 23.70 -20 0 20 104.79 24.60 20 0 -20 114.49 22.30 -20 0 20 125.39 21.80 -20 0 20 114.39 22.30 22 0 -22 15.00 17.90 -22 0 22 39.20 20.30 22 0 -22 42.60 19.30 -22 0 22 20.60 14.30 22 0 -22 13.80 15.10 -22 0 22 83.39 19.10 22 0 -22 7.30 11.00 -22 0 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9.40 8 -4 -8 16.40 12.10 8 -4 -8 48.90 15.10 -8 -4 8 42.30 9.30 -8 -4 8 33.90 6.00 -8 -4 8 60.59 13.50 8 -4 -8 26.60 9.10 -8 -4 8 25.80 13.70 -8 -4 8 39.90 12.70 -8 -4 8 52.99 15.70 8 -4 -8 46.20 13.10 10 4 -10 5.40 7.20 10 4 -10 -3.40 4.50 10 4 -10 10.40 8.20 -10 4 10 6.20 5.60 10 4 -10 9.80 8.80 -10 4 10 2.90 6.40 10 4 -10 -2.20 3.90 -10 4 10 17.10 8.50 10 4 -10 7.60 3.30 -10 4 10 -11.90 7.20 -10 4 10 24.20 10.20 10 -4 -10 -4.30 5.80 -10 -4 10 10.10 8.50 -10 -4 10 -14.40 10.60 10 -4 -10 5.90 12.10 -10 -4 10 4.10 9.60 10 -4 -10 0.60 10.80 10 -4 -10 8.50 10.90 10 -4 -10 38.40 9.10 -10 -4 10 -5.70 4.60 -10 -4 10 2.40 11.90 -10 -4 10 2.10 10.00 -12 4 12 545.45 37.30 12 4 -12 492.25 29.20 12 4 -12 521.85 38.10 -12 4 12 538.15 40.00 -12 4 12 506.65 35.70 -12 4 12 426.66 36.60 12 4 -12 461.15 32.20 12 4 -12 513.85 36.90 12 4 -12 486.55 36.90 12 -4 -12 486.85 41.40 12 -4 -12 494.35 39.50 -12 -4 12 483.35 37.30 12 -4 -12 453.35 34.50 -12 -4 12 504.05 31.70 -12 -4 12 417.66 43.80 -12 -4 12 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7 36.50 14.80 -9 9 7 39.50 14.00 9 9 -7 37.30 10.00 -9 9 7 50.79 10.00 9 9 -7 61.49 15.20 9 -9 -7 47.00 24.20 9 -9 -7 8.00 16.60 9 -9 -7 25.90 23.40 -9 -9 7 60.89 23.60 -9 -9 7 49.00 26.20 -9 -9 7 14.10 25.40 9 -9 -7 40.10 24.10 -9 -9 7 37.90 22.30 -7 9 5 29.80 13.30 7 9 -5 43.80 10.80 7 9 -5 27.30 11.90 -7 9 5 43.10 10.00 7 9 -5 26.80 12.40 7 9 -5 50.89 11.40 -7 9 5 20.90 8.80 7 9 -5 27.50 11.80 -7 9 5 46.90 12.20 -7 9 5 33.90 12.50 7 -9 -5 6.50 20.50 7 -9 -5 5.90 20.30 -7 -9 5 40.50 26.70 7 -9 -5 43.50 23.80 -7 -9 5 51.99 26.40 7 -9 -5 70.99 22.00 7 -9 -5 -11.30 21.60 -7 -9 5 21.60 24.50 -7 -9 5 -2.80 18.90 -5 9 3 278.87 25.00 -5 9 3 249.08 24.20 -5 9 3 247.08 25.90 5 9 -3 260.37 27.40 -5 9 3 237.88 25.20 5 9 -3 293.37 28.10 5 9 -3 223.68 24.00 5 9 -3 275.17 27.00 -5 9 3 323.37 30.00 5 9 -3 344.17 30.20 5 -9 -3 251.87 34.60 5 -9 -3 303.97 38.00 5 -9 -3 202.88 36.50 -5 -9 3 234.18 36.00 -5 -9 3 291.07 38.70 -5 -9 3 222.58 39.10 5 -9 -3 306.27 42.10 5 -9 -3 280.97 38.10 -5 -9 3 373.16 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27.70 2 6 3 337.67 24.20 2 6 3 399.56 28.40 -2 6 -3 381.36 27.60 -2 -6 -3 359.96 37.90 -2 -6 -3 443.26 37.90 2 -6 3 278.67 37.00 2 -6 3 357.36 38.20 -2 -6 -3 305.67 35.10 2 -6 3 333.77 32.70 2 -6 3 380.56 41.90 2 -6 3 345.77 34.40 -2 -6 -3 409.46 36.00 0 6 -5 28.20 9.00 0 6 -5 2.70 7.90 0 6 5 11.80 7.90 0 6 -5 12.90 6.30 0 6 5 4.70 5.90 0 6 5 6.40 4.80 0 6 -5 22.80 6.50 0 6 5 28.00 9.40 0 -6 -5 19.90 14.20 0 -6 5 9.00 6.30 0 -6 5 -0.70 13.70 0 -6 5 6.60 13.80 0 -6 5 -8.00 13.00 0 -6 5 5.70 12.80 0 -6 -5 4.90 13.00 0 -6 -5 16.90 13.10 0 -6 -5 19.40 13.80 -2 6 7 42.80 11.90 -2 6 7 81.79 13.00 2 6 -7 89.19 8.70 -2 6 7 77.99 10.60 2 6 -7 89.29 11.80 -2 6 7 77.89 9.70 2 6 -7 93.89 13.80 2 6 -7 66.89 10.70 2 6 -7 96.69 14.20 -2 6 7 91.99 16.80 -2 -6 7 51.69 19.60 2 -6 -7 91.29 17.80 -2 -6 7 82.49 11.50 2 -6 -7 86.09 19.50 -2 -6 7 81.99 22.40 -2 -6 7 71.29 15.80 2 -6 -7 67.69 18.80 2 -6 -7 72.09 18.20 2 -6 -7 109.49 18.20 -2 -6 7 90.29 22.20 4 6 -9 25.70 10.70 4 6 -9 46.40 11.50 -4 6 9 48.40 10.70 -4 6 9 33.30 11.10 4 6 -9 20.90 7.80 -4 6 9 24.30 6.10 -4 6 9 28.70 7.10 4 6 -9 27.80 4.70 4 6 -9 40.10 9.50 -4 6 9 22.50 10.80 -4 -6 9 24.70 8.90 -4 -6 9 36.90 19.00 4 -6 -9 48.50 17.00 4 -6 -9 26.00 15.40 4 -6 -9 24.10 13.40 -4 -6 9 35.90 13.00 4 -6 -9 28.30 17.10 -4 -6 9 15.30 15.40 -4 -6 9 7.10 15.80 6 6 -11 114.79 15.90 6 6 -11 106.29 17.00 6 6 -11 126.69 18.70 -6 6 11 136.19 8.90 -6 6 11 124.39 9.30 -6 6 11 156.18 19.90 6 6 -11 100.39 15.50 -6 6 11 126.19 15.00 -6 6 11 135.79 20.00 -6 6 11 142.49 14.10 6 -6 -11 86.09 23.00 6 -6 -11 109.19 24.60 -6 -6 11 110.19 17.20 -6 -6 11 103.89 23.30 6 -6 -11 110.89 18.90 6 -6 -11 136.19 24.70 -6 -6 11 99.49 25.40 -6 -6 11 109.99 15.20 -6 -6 11 166.08 29.60 8 6 -13 477.05 35.30 8 6 -13 358.56 36.10 -8 6 13 432.66 36.90 -8 6 13 468.25 30.40 -8 6 13 467.85 36.90 8 6 -13 393.76 33.80 8 6 -13 435.06 36.00 -8 6 13 441.16 31.60 -8 -6 13 308.37 45.10 8 -6 -13 410.26 43.80 8 -6 -13 465.05 46.10 -8 -6 13 462.05 33.90 -8 -6 13 472.25 49.50 -8 -6 13 479.55 47.30 8 -6 -13 429.06 46.80 8 -6 -13 476.15 37.10 -10 6 15 54.29 16.30 -10 6 15 6.80 8.60 -10 6 15 4.80 11.60 10 6 -15 11.20 13.00 10 6 -15 17.60 10.80 10 6 -15 -3.70 11.90 10 6 -15 15.10 10.70 -10 -6 15 11.80 20.40 -10 -6 15 -13.30 16.20 -10 -6 15 23.60 13.10 -10 -6 15 35.60 20.90 10 -6 -15 17.40 13.20 10 -6 -15 10.90 17.60 10 -6 -15 7.00 19.00 12 6 -17 117.59 21.40 12 6 -17 132.59 21.70 -12 6 17 126.09 23.30 -12 6 17 129.99 22.90 12 6 -17 107.89 21.00 12 6 -17 131.99 22.80 -12 6 17 108.39 16.70 12 -6 -17 129.39 28.20 12 -6 -17 141.79 29.70 -12 -6 17 167.58 30.80 -12 -6 17 143.89 31.60 -12 -6 17 127.39 31.60 -14 6 19 -9.20 14.50 14 6 -19 2.30 15.30 14 6 -19 -7.40 11.80 14 6 -19 31.50 16.00 14 6 -19 -0.20 13.80 -14 6 19 6.90 11.20 -14 6 19 -1.40 15.40 14 -6 -19 -8.10 17.10 -14 -6 19 -8.80 18.50 14 -6 -19 25.40 20.30 -14 -6 19 12.30 20.60 -14 -6 19 -18.30 17.40 16 6 -21 40.00 17.50 16 6 -21 32.40 20.70 -16 6 21 0.00 17.90 16 6 -21 15.50 15.80 -16 6 21 -1.50 16.50 -16 6 21 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57.79 14.00 -10 6 -3 14.10 11.20 -10 6 -3 54.69 13.10 10 6 3 55.09 14.40 10 6 3 41.60 6.80 10 6 3 55.19 14.70 -10 6 -3 44.50 10.80 10 6 3 52.89 8.70 10 6 3 60.49 10.40 -10 -6 -3 51.49 18.10 10 -6 3 35.10 13.00 10 -6 3 53.19 21.20 -10 -6 -3 77.09 22.20 10 -6 3 22.00 19.10 10 -6 3 44.30 21.40 -10 -6 -3 42.00 18.50 -8 6 -5 36.50 13.50 8 6 5 18.70 11.60 -8 6 -5 30.20 11.80 8 6 5 19.90 12.20 8 6 5 24.00 8.60 8 6 5 17.20 8.60 -8 6 -5 9.60 9.00 8 6 5 41.90 13.40 -8 -6 -5 1.50 14.70 -8 -6 -5 7.20 14.10 8 -6 5 22.60 17.90 8 -6 5 26.70 16.80 8 -6 5 -14.20 10.60 -8 -6 -5 28.80 16.90 8 -6 5 30.40 10.80 -8 -6 -5 10.10 15.20 6 6 7 318.87 27.40 6 6 7 395.06 34.40 -6 6 -7 290.67 25.10 6 6 7 363.16 34.10 6 6 7 382.26 28.40 -6 6 -7 346.77 32.30 -6 6 -7 405.26 31.70 -6 6 -7 317.07 30.20 6 6 7 295.77 32.50 -6 -6 -7 390.66 36.20 -6 -6 -7 322.37 37.10 6 -6 7 319.97 43.00 -6 -6 -7 299.07 38.50 6 -6 7 277.77 36.20 -6 -6 -7 323.37 39.10 6 -6 7 342.57 42.80 -4 6 -9 54.39 7.70 4 6 9 34.00 14.90 -4 6 -9 34.10 13.50 4 6 9 50.79 15.50 4 6 9 32.60 11.60 -4 6 -9 20.50 13.10 -4 6 -9 50.19 14.20 -4 -6 -9 25.20 19.50 -4 -6 -9 187.88 28.80 4 -6 9 33.90 20.00 4 -6 9 57.69 19.50 4 -6 9 30.60 21.50 -4 -6 -9 64.09 17.40 4 -6 9 44.90 6.60 -4 -6 -9 28.80 19.40 -2 6 -11 56.09 16.10 2 6 11 56.39 17.50 -2 6 -11 86.79 11.60 2 6 11 86.89 17.10 -2 6 -11 71.19 17.10 2 6 11 66.79 18.40 -2 -6 -11 51.59 20.40 -2 -6 -11 100.19 22.60 2 -6 11 52.99 13.40 2 -6 11 41.30 19.40 2 -6 11 43.20 22.90 2 -6 11 87.09 26.40 -2 -6 -11 64.39 21.70 0 6 -13 -2.90 10.80 0 6 -13 12.50 8.90 0 6 13 -3.50 12.30 0 6 13 -5.40 12.90 0 6 -13 9.30 8.90 0 6 13 15.00 14.40 0 6 -13 -0.50 12.90 0 -6 13 9.90 19.40 0 -6 13 -2.20 15.70 0 -6 -13 -7.40 15.70 0 -6 13 -20.40 18.20 0 -6 -13 1.20 15.30 0 -6 -13 -10.40 15.90 -2 6 15 3.60 14.10 2 6 -15 -5.00 8.90 2 6 -15 9.50 10.30 -2 6 15 4.50 16.00 2 6 -15 22.20 14.10 -2 6 15 -5.60 14.30 2 6 -15 20.80 15.20 -2 -6 15 -16.10 17.70 2 -6 -15 31.80 19.00 -2 -6 15 15.10 21.10 2 -6 -15 7.10 17.90 2 -6 -15 8.10 17.20 4 6 -17 139.19 21.00 -4 6 17 153.18 24.70 4 6 -17 126.49 23.60 -4 6 17 133.29 26.20 4 6 -17 125.89 21.50 4 6 -17 95.49 22.30 4 -6 -17 183.58 28.30 -4 -6 17 151.58 33.00 4 -6 -17 165.08 31.40 -4 -6 17 112.99 31.00 4 -6 -17 80.19 26.50 6 6 -19 -15.80 13.80 -6 6 19 -1.60 16.70 6 6 -19 8.90 16.60 6 6 -19 -19.90 10.50 -6 6 19 14.10 19.90 -6 6 19 11.50 16.40 6 -6 -19 -3.50 18.90 -6 -6 19 19.40 24.60 -6 -6 19 9.50 19.20 6 -6 -19 -11.80 16.50 6 -6 -19 2.30 18.10 -6 -6 19 -12.50 19.00 -8 6 21 15.20 22.00 -8 6 21 13.70 20.00 8 6 -21 39.40 26.50 -8 6 21 -3.90 17.60 8 6 -21 -1.60 18.40 8 6 -21 49.40 20.30 8 -6 -21 -15.00 19.20 8 -6 -21 29.00 25.20 -8 -6 21 45.80 29.70 -8 -6 21 5.90 26.10 -10 6 23 14.40 21.90 10 6 -23 28.00 20.20 -10 6 23 47.60 24.60 10 6 -23 48.50 23.40 -10 6 23 44.20 21.00 -10 -6 23 129.69 34.60 10 -6 -23 -5.50 24.90 -10 -6 23 34.20 31.70 10 -6 -23 27.90 21.10 10 -6 -23 59.19 26.80 31 7 -18 -20.60 19.90 -31 7 18 11.10 20.40 31 7 -18 18.40 20.60 -31 7 18 -26.30 14.90 31 7 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4 8 86.89 18.20 24 4 -8 32.20 13.90 24 4 -8 21.70 15.50 -24 4 8 76.79 19.10 -24 4 8 86.99 13.20 24 4 -8 46.70 17.60 -24 4 8 67.09 15.60 24 4 -8 85.79 19.80 -24 -4 8 67.19 17.70 -24 -4 8 61.79 18.90 -24 -4 8 27.40 18.60 24 -4 -8 61.49 22.30 24 -4 -8 44.70 20.50 24 -4 -8 42.80 20.60 24 -4 -8 40.00 15.70 24 -4 -8 43.70 17.10 -24 -4 8 72.09 24.60 22 4 -6 23.20 14.40 22 4 -6 -11.10 11.30 22 4 -6 23.40 14.40 22 4 -6 0.20 10.80 -22 4 6 0.70 12.60 -22 4 6 5.50 10.60 -22 4 6 -10.30 5.70 -22 4 6 22.50 12.70 22 -4 -6 9.20 10.90 -22 -4 6 -16.40 12.00 -22 -4 6 26.00 21.90 -22 -4 6 -3.80 12.70 22 -4 -6 -7.20 11.10 -22 -4 6 -28.10 13.40 22 -4 -6 -7.40 14.60 22 -4 -6 -7.90 13.50 22 -4 -6 12.50 16.50 -20 4 4 200.48 17.10 20 4 -4 220.68 25.10 20 4 -4 205.98 25.10 -20 4 4 208.28 16.60 -20 4 4 168.78 22.60 -20 4 4 178.58 24.30 -20 4 4 201.98 24.40 20 4 -4 195.78 24.90 20 4 -4 175.68 24.50 -20 -4 4 182.38 27.00 -20 -4 4 215.48 25.70 -20 -4 4 202.08 22.20 20 -4 -4 163.98 27.10 20 -4 -4 110.99 24.90 20 -4 -4 247.78 18.40 20 -4 -4 194.08 20.00 -20 -4 4 238.78 34.60 -20 -4 4 183.88 26.90 20 -4 -4 153.98 27.80 -18 4 2 38.90 5.90 -18 4 2 29.90 5.50 -18 4 2 36.80 12.10 18 4 -2 28.20 13.40 -18 4 2 42.60 9.80 18 4 -2 38.00 14.20 18 4 -2 23.30 12.00 -18 4 2 31.20 13.50 18 4 -2 41.00 14.80 18 -4 -2 38.90 9.90 18 -4 -2 59.19 18.80 -18 -4 2 32.70 13.00 -18 -4 2 57.59 22.00 18 -4 -2 20.40 13.40 -18 -4 2 49.80 16.10 18 -4 -2 22.60 15.50 -18 -4 2 25.00 15.10 18 -4 -2 39.50 17.80 18 -4 -2 20.70 8.20 -18 -4 2 47.60 10.70 16 4 0 9.10 13.50 16 4 0 30.90 13.70 16 4 0 49.60 15.70 -16 4 0 29.40 10.20 -16 4 0 40.10 12.80 -16 4 0 45.60 13.30 16 4 0 93.99 17.50 16 -4 0 34.10 16.20 16 -4 0 35.20 17.00 -16 -4 0 16.30 13.70 -16 -4 0 14.60 18.80 16 -4 0 33.70 12.40 -16 -4 0 30.30 11.70 -16 -4 0 22.00 13.30 16 -4 0 32.20 16.00 -16 -4 0 25.80 14.90 14 4 2 116.19 19.50 14 4 2 85.49 16.40 -14 4 -2 95.19 16.50 -14 4 -2 72.99 9.00 -14 4 -2 64.99 13.40 14 4 2 69.29 15.50 14 4 2 120.79 19.00 -14 4 -2 81.09 15.90 14 4 2 90.89 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18 0 11 -15.00 18.40 -16 0 -13 9.60 18.30 16 0 13 1.60 25.60 -16 0 -13 15.80 22.90 16 0 13 22.20 25.50 16 0 13 -3.40 20.60 -35 1 6 -27.40 13.80 -35 -1 6 -19.40 13.90 -33 1 4 -16.40 21.40 -33 1 4 9.00 13.80 -33 1 4 15.40 17.20 33 1 -4 -8.60 20.10 -33 -1 4 -4.40 11.00 33 -1 -4 -30.30 21.60 -33 -1 4 -14.40 14.70 -33 -1 4 -33.80 19.50 -31 1 2 32.90 19.60 31 1 -2 56.59 25.00 31 1 -2 8.50 20.70 -31 1 2 4.90 12.60 -31 1 2 9.30 19.00 -31 -1 2 22.00 13.60 -31 -1 2 15.40 17.70 31 -1 -2 62.79 30.20 -29 1 0 5.20 17.90 29 1 0 -5.60 22.40 -29 1 0 -10.90 8.50 29 1 0 -27.60 19.10 29 -1 0 -36.10 19.20 -29 -1 0 -1.90 7.60 -29 -1 0 -13.30 17.90 29 -1 0 15.10 21.20 27 1 2 -16.20 21.20 -27 1 -2 -2.50 7.60 27 1 2 -6.90 19.60 -27 1 -2 0.00 19.40 27 1 2 9.70 17.90 -27 -1 -2 -9.10 7.30 27 -1 2 5.60 19.60 -27 -1 -2 -0.70 18.30 27 -1 2 -2.70 23.10 27 -1 2 -51.19 19.20 25 1 4 7.30 17.80 -25 1 -4 4.30 10.50 25 1 4 12.00 22.00 25 1 4 61.99 25.70 -25 1 -4 4.20 17.20 25 -1 4 10.40 22.00 -25 -1 -4 -1.80 7.10 -25 -1 -4 9.70 18.30 25 -1 4 3.30 20.40 25 -1 4 -1.90 21.70 23 1 6 -0.10 21.50 23 1 6 15.90 19.60 23 1 6 -12.80 23.70 -23 1 -6 2.10 7.50 -23 -1 -6 -28.90 14.40 23 -1 6 -23.00 21.10 23 -1 6 2.80 22.10 23 -1 6 -22.70 18.90 -21 1 -8 -15.70 15.50 21 1 8 -32.10 18.00 21 1 8 -25.30 20.50 21 1 8 5.10 21.50 21 -1 8 -3.20 16.70 -21 -1 -8 26.90 19.30 21 -1 8 13.60 20.80 21 -1 8 -19.50 20.50 19 1 10 30.70 23.40 -19 1 -10 -34.70 17.20 -19 1 -10 28.20 22.30 19 1 10 4.20 21.30 19 -1 10 -13.10 18.50 19 -1 10 -25.00 22.60 19 -1 10 -27.60 16.30 -19 -1 -10 -6.00 17.50 17 1 12 -5.70 20.80 17 1 12 34.40 26.10 -17 1 -12 8.20 21.70 -17 1 -12 -24.20 18.90 17 -1 12 -7.80 21.30 -17 -1 -12 -5.10 17.00 17 -1 12 -44.50 15.40 -34 2 5 -7.30 15.00 -34 2 5 8.30 17.90 34 2 -5 -22.20 18.80 -34 2 5 -40.20 17.80 -34 -2 5 -12.90 9.30 -34 -2 5 27.80 23.80 -34 -2 5 -3.40 18.20 34 -2 -5 15.80 25.30 32 2 -3 50.19 26.10 32 2 -3 4.10 22.90 -32 2 3 -9.40 21.40 -32 2 3 -7.80 12.70 -32 2 3 7.80 14.50 -32 -2 3 3.80 19.70 -32 -2 3 -6.30 7.60 32 -2 -3 -21.50 22.20 -30 2 1 13.10 19.50 30 2 -1 -22.40 17.00 -30 2 1 -9.90 11.30 30 2 -1 19.50 26.80 30 -2 -1 -30.70 21.70 30 -2 -1 -31.20 18.10 -30 -2 1 0.80 16.60 -30 -2 1 -0.80 10.10 28 2 1 7.40 21.70 -28 2 -1 0.70 10.70 28 2 1 25.20 24.50 -28 2 -1 10.00 20.60 -28 -2 -1 11.90 10.90 28 -2 1 -6.30 20.60 28 -2 1 10.90 24.40 -28 -2 -1 34.10 20.20 -26 2 -3 19.30 18.80 26 2 3 9.70 20.40 -26 2 -3 -5.10 8.00 26 2 3 14.90 18.30 26 2 3 11.50 23.20 -26 -2 -3 -26.60 16.20 26 -2 3 17.80 23.30 -26 -2 -3 15.00 19.50 26 -2 3 3.00 23.30 24 2 5 -7.80 15.30 -24 2 -5 20.80 19.40 24 2 5 17.20 22.70 -24 2 -5 13.00 11.70 24 2 5 14.00 22.60 24 -2 5 -18.40 22.60 24 -2 5 -17.80 21.00 -24 -2 -5 14.40 19.70 -24 -2 -5 9.30 17.40 24 -2 5 5.30 23.10 22 2 7 52.99 23.70 -22 2 -7 11.40 19.00 -22 2 -7 12.00 18.90 22 2 7 59.09 23.60 22 2 7 9.20 19.80 -22 -2 -7 -6.00 18.60 22 -2 7 8.30 22.30 -22 -2 -7 33.20 20.90 22 -2 7 52.59 27.20 22 -2 7 26.90 23.50 -20 2 -9 -18.00 18.30 20 2 9 -14.70 20.00 20 2 9 35.40 24.70 -20 2 -9 -13.10 15.50 20 -2 9 -0.30 22.60 20 -2 9 10.50 22.40 20 -2 9 -3.10 22.40 -20 -2 -9 -6.40 18.40 18 2 11 20.00 23.70 -18 2 -11 -1.30 19.60 -18 2 -11 7.80 17.60 18 2 11 33.50 23.80 18 -2 11 43.10 28.40 -18 -2 -11 8.30 19.70 -18 -2 -11 30.20 22.60 18 -2 11 9.10 21.80 -33 3 4 26.20 18.90 -33 -3 4 0.30 18.40 33 -3 -4 -8.50 23.10 -31 3 2 -13.40 13.00 31 3 -2 33.70 22.30 31 3 -2 -5.30 20.00 31 3 -2 16.70 21.60 -31 3 2 21.60 20.00 -31 -3 2 -3.30 8.40 31 -3 -2 -4.40 22.50 31 -3 -2 3.60 22.40 31 -3 -2 1.90 25.20 -31 -3 2 -24.50 19.70 -29 3 0 30.20 19.10 29 3 0 1.80 21.30 -29 3 0 -8.80 12.50 29 3 0 26.30 21.50 -29 3 0 -6.90 20.50 29 3 0 7.90 19.10 -29 -3 0 18.20 19.20 29 -3 0 -3.70 22.20 29 -3 0 -20.00 22.20 -29 -3 0 6.50 19.30 27 3 2 -11.50 21.50 27 3 2 -22.20 17.40 -27 3 -2 -11.50 10.30 -27 3 -2 3.60 18.20 27 3 2 35.40 25.00 27 -3 2 18.90 23.30 -27 -3 -2 14.00 21.90 27 -3 2 4.30 26.30 -27 -3 -2 -17.30 17.10 -25 3 -4 2.80 9.40 -25 3 -4 0.40 20.40 25 3 4 -1.00 17.50 25 3 4 1.90 23.20 25 3 4 3.70 22.80 -25 -3 -4 19.10 20.70 25 -3 4 9.00 25.60 -25 -3 -4 33.10 21.10 25 -3 4 21.00 22.40 -23 3 -6 5.30 17.10 -23 3 -6 1.40 19.50 23 3 6 9.70 23.10 23 3 6 0.00 17.60 23 3 6 46.70 23.00 23 -3 6 20.70 26.00 23 -3 6 28.80 23.40 23 -3 6 11.80 21.30 -23 -3 -6 -32.50 16.40 -23 -3 -6 1.80 18.90 -21 3 -8 27.50 20.50 -21 3 -8 1.70 20.10 21 3 8 19.00 25.60 -21 3 -8 10.10 20.00 21 3 8 -17.20 19.30 21 -3 8 8.30 21.50 21 -3 8 10.00 26.70 21 -3 8 -5.00 26.80 -21 -3 -8 7.70 19.40 -21 -3 -8 51.29 23.90 -21 -3 -8 -10.80 18.40 -19 3 -10 -17.80 17.90 19 3 10 13.50 20.70 19 3 10 22.30 26.30 -19 3 -10 -5.40 19.90 -19 3 -10 7.40 17.50 19 -3 10 -10.00 19.40 -19 -3 -10 -3.70 19.60 -19 -3 -10 13.50 19.60 -19 -3 -10 123.49 31.10 19 -3 10 26.40 27.80 30 4 -1 47.10 26.40 30 4 -1 9.50 21.10 -30 4 1 -3.00 20.70 -30 4 1 15.30 16.30 -30 4 1 31.20 19.60 30 4 -1 19.20 24.00 -30 -4 1 17.60 20.70 30 -4 -1 7.30 27.10 -30 -4 1 6.10 20.00 30 -4 -1 13.60 25.00 28 4 1 -8.40 24.20 28 4 1 7.20 21.00 -28 4 -1 4.20 19.00 28 4 1 15.30 20.60 -28 4 -1 1.20 10.50 28 -4 1 -19.50 19.10 28 -4 1 -33.20 25.10 -28 -4 -1 34.30 24.30 28 -4 1 -18.40 27.50 -28 -4 -1 50.39 24.30 26 4 3 -18.30 20.90 26 4 3 24.10 24.80 -26 4 -3 -14.60 17.80 -26 4 -3 15.60 20.60 26 4 3 -13.30 17.70 26 -4 3 -10.10 23.70 26 -4 3 5.60 27.00 -26 -4 -3 61.79 24.60 -26 -4 -3 -23.30 19.00 26 -4 3 -46.90 20.50 -24 4 -5 -15.80 19.00 -24 4 -5 -7.10 17.50 24 4 5 16.80 20.40 24 4 5 -2.70 22.10 24 4 5 -19.40 14.80 -24 -4 -5 124.09 28.40 -24 -4 -5 31.90 23.00 24 -4 5 7.00 24.50 -24 -4 -5 0.20 20.10 24 -4 5 37.00 26.70 24 -4 5 5.00 24.90 -22 4 -7 12.30 19.60 22 4 7 22.30 25.10 -22 4 -7 9.40 20.00 -22 4 -7 15.50 19.70 22 4 7 -21.20 20.70 22 4 7 5.60 16.80 -22 -4 -7 -6.50 20.20 -22 -4 -7 28.00 21.60 -22 -4 -7 -3.50 20.70 22 -4 7 44.00 26.50 -20 4 -9 7.80 21.30 20 -4 9 49.60 27.60 -20 -4 -9 -22.60 18.80 -32 0 2 0.50 9.70 32 0 -2 16.20 24.00 -32 0 2 0.50 15.00 -32 0 2 17.00 22.20 -30 0 0 7.50 8.50 30 0 0 2.80 22.50 -30 0 0 -20.60 19.30 -30 0 0 13.20 18.90 30 0 0 -21.30 20.90 28 0 2 80.69 30.70 -28 0 -2 -3.40 8.60 28 0 2 18.30 22.60 28 0 2 -12.30 25.60 26 0 4 -7.30 18.90 -26 0 -4 -7.40 5.20 26 0 4 1.10 23.30 26 0 4 -11.90 20.00 -24 0 -6 30.60 19.50 24 0 6 33.20 24.90 24 0 6 2.10 20.30 24 0 6 22.80 24.10 22 0 8 -20.20 19.20 22 0 8 10.60 22.40 -22 0 -8 -23.10 14.50 22 0 8 8.00 23.00 20 0 10 -22.70 20.30 -20 0 -10 1.60 18.30 20 0 10 26.40 26.20 20 0 10 -11.70 17.20 -33 1 3 -11.10 16.20 -33 -1 3 7.70 19.00 31 1 -1 32.30 25.20 -31 1 1 -8.50 20.90 -31 1 1 -8.40 7.90 -31 1 1 2.40 17.20 31 1 -1 5.40 23.70 -31 -1 1 2.20 8.00 31 -1 -1 4.80 23.70 -31 -1 1 10.80 17.50 29 1 1 6.80 22.50 29 1 1 11.50 22.00 -29 1 -1 45.10 22.40 -29 1 -1 6.20 11.70 29 -1 1 -17.50 22.60 29 -1 1 10.80 21.80 -29 -1 -1 18.00 18.40 -29 -1 -1 -10.50 7.50 -27 1 -3 -0.80 8.90 27 1 3 -2.20 19.80 -27 1 -3 -2.50 19.80 27 1 3 17.30 19.80 27 1 3 -3.40 23.20 -27 -1 -3 13.60 21.80 27 -1 3 18.80 24.60 27 -1 3 22.80 23.20 27 -1 3 -1.10 19.70 -27 -1 -3 7.20 17.80 -25 1 -5 24.40 12.80 25 1 5 4.30 23.40 25 1 5 -25.40 18.10 25 1 5 6.10 24.30 25 -1 5 -58.09 18.90 -25 -1 -5 -4.10 17.20 25 -1 5 9.70 22.10 25 -1 5 -21.10 18.90 23 1 7 -6.40 20.50 23 1 7 105.99 29.10 -23 1 -7 10.00 18.90 23 1 7 -8.20 21.90 23 -1 7 23.00 21.30 -23 -1 -7 20.60 19.30 23 -1 7 5.90 23.20 23 -1 7 -34.70 19.00 21 1 9 5.60 23.00 21 1 9 -14.60 20.10 21 1 9 16.50 25.40 -21 1 -9 -17.60 17.10 21 -1 9 -3.20 25.80 21 -1 9 -24.20 17.90 -21 -1 -9 -21.40 18.80 21 -1 9 -16.90 19.00 -32 2 2 11.10 14.70 -32 -2 2 -12.00 19.50 -30 2 0 6.50 13.30 30 2 0 19.60 22.70 30 2 0 43.20 26.70 -30 2 0 34.10 20.40 30 -2 0 8.60 25.60 30 -2 0 -1.20 21.20 -30 -2 0 8.10 19.20 -30 -2 0 40.20 20.60 28 2 2 29.50 24.50 28 2 2 -15.30 18.70 -28 2 -2 -18.70 18.90 -28 2 -2 -7.30 8.60 -28 -2 -2 2.90 19.90 28 -2 2 -7.80 17.90 28 -2 2 -23.10 21.70 -28 -2 -2 3.80 18.20 26 2 4 33.20 24.90 -26 2 -4 5.00 8.90 26 2 4 10.80 21.80 26 2 4 20.40 23.60 -26 2 -4 15.70 17.80 26 -2 4 8.40 24.40 26 -2 4 2.60 23.00 26 -2 4 2.50 22.10 -26 -2 -4 5.80 18.70 -26 -2 -4 28.10 21.80 -24 2 -6 3.10 8.40 24 2 6 19.00 21.50 24 2 6 22.60 25.40 24 2 6 18.60 24.40 -24 2 -6 4.30 19.70 -24 -2 -6 -8.00 22.20 24 -2 6 -1.30 25.60 24 -2 6 -10.30 22.40 -24 -2 -6 -0.70 19.90 24 -2 6 3.10 21.40 22 2 8 31.90 25.00 22 2 8 -8.50 20.50 22 2 8 39.60 25.90 -22 2 -8 35.20 20.30 -22 -2 -8 6.70 19.80 22 -2 8 22.60 24.40 22 -2 8 50.69 24.10 -22 -2 -8 41.70 23.40 22 -2 8 -7.60 19.50 -29 3 -1 -2.50 22.10 -29 3 -1 -1.70 9.00 29 3 1 54.99 26.30 29 -3 1 -2.50 27.10 29 -3 1 4.00 22.30 -29 -3 -1 40.10 24.20 -27 3 -3 -5.70 9.50 27 3 3 8.40 21.50 -27 3 -3 5.70 18.50 27 3 3 8.20 23.60 27 -3 3 2.80 20.10 -27 -3 -3 7.20 20.20 27 -3 3 21.30 25.50 -27 -3 -3 9.10 20.70 -25 3 -5 -23.50 18.70 25 3 5 -24.50 22.60 -25 3 -5 -6.20 6.10 25 3 5 26.90 24.70 -25 -3 -5 -10.20 19.10 25 -3 5 33.70 23.90 25 -3 5 3.90 25.60 -25 -3 -5 -21.80 18.10 -23 3 -7 1.90 21.10 -23 -3 -7 -13.90 19.10 23 -3 7 37.10 26.60 -28 0 -3 6.80 18.50 -26 0 -5 -14.40 15.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 674 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.5267(3) 0.0255(2) 0.34755(11) 0.0493(12) Uani 0.531(13) 1 d . U P A 1 Zn1' Zn 0.5513(3) 0.0432(3) 0.35353(13) 0.0405(11) Uani 0.469(13) 1 d . U P A 2 O1 O 0.500000 0.0331(4) 0.250000 0.0402(12) Uani 1 2 d S T P . . H1 H 0.472(3) 0.0368(6) 0.2401(11) 0.048 Uiso 0.5 1 d R U P A . N1 N 0.56188(16) -0.1147(4) 0.4108(2) 0.0527(11) Uani 1 1 d . . . . . N2 N 0.58888(16) -0.2010(3) 0.4046(2) 0.0469(10) Uani 1 1 d . . . . . N3 N 0.61652(14) 0.0179(3) 0.3612(2) 0.0425(10) Uani 1 1 d . . . . . N4 N 0.55512(16) 0.1768(4) 0.4117(2) 0.0507(11) Uani 1 1 d . . . . . N5 N 0.52009(16) 0.2664(4) 0.3889(2) 0.0474(10) Uani 1 1 d . . . . . N6 N 0.44807(14) 0.0571(3) 0.31820(19) 0.0394(9) Uani 1 1 d . . . . . C1 C 0.5644(2) -0.1485(5) 0.4674(3) 0.0561(14) Uani 1 1 d . . . . . C2 C 0.5918(2) -0.2534(5) 0.4956(3) 0.0574(14) Uani 1 1 d . . . . . H2 H 0.598776 -0.295946 0.535695 0.069 Uiso 1 1 calc R U . . . C3 C 0.60733(19) -0.2856(5) 0.4553(3) 0.0504(13) Uani 1 1 d . . . . . C4 C 0.5392(2) -0.0758(6) 0.4913(3) 0.079(2) Uani 1 1 d . . . . . H4A H 0.563895 -0.064984 0.543840 0.118 Uiso 1 1 calc R U . . . H4B H 0.507638 -0.117209 0.478215 0.118 Uiso 1 1 calc R U . . . H4C H 0.529300 0.002764 0.467531 0.118 Uiso 1 1 calc R U . . . C5 C 0.6377(2) -0.3910(5) 0.4607(3) 0.0692(17) Uani 1 1 d . . . . . H5A H 0.648245 -0.440416 0.502194 0.104 Uiso 1 1 calc R U . . . H5B H 0.669191 -0.363447 0.467224 0.104 Uiso 1 1 calc R U . . . H5C H 0.615854 -0.438709 0.416323 0.104 Uiso 1 1 calc R U . . . C6 C 0.5932(2) -0.1918(4) 0.3469(3) 0.0494(13) Uani 1 1 d . . . . . H6A H 0.558036 -0.175794 0.300649 0.059 Uiso 1 1 calc R U . . . H6B H 0.605845 -0.269173 0.342112 0.059 Uiso 1 1 calc R U . . . C7 C 0.63031(19) -0.0937(5) 0.3606(2) 0.0458(12) Uani 1 1 d . . . . . C8 C 0.6760(2) -0.1231(5) 0.3706(3) 0.0547(14) Uani 1 1 d . . . . . H8 H 0.684451 -0.204572 0.370240 0.066 Uiso 1 1 calc R U . . . C9 C 0.7086(2) -0.0341(5) 0.3809(3) 0.0625(15) Uani 1 1 d . . . . . H9 H 0.740053 -0.053016 0.387742 0.075 Uiso 1 1 calc R U . . . C10 C 0.69598(19) 0.0855(5) 0.3815(3) 0.0522(13) Uani 1 1 d . . . . . C11 C 0.7269(2) 0.1828(6) 0.3893(4) 0.0797(19) Uani 1 1 d . . . . . H11 H 0.758715 0.168090 0.396356 0.096 Uiso 1 1 calc R U . . . C12 C 0.7118(3) 0.2963(6) 0.3868(4) 0.087(2) Uani 1 1 d . . . . . H12 H 0.732965 0.361031 0.391939 0.105 Uiso 1 1 calc R U . . . C13 C 0.6651(2) 0.3201(5) 0.3766(4) 0.0778(19) Uani 1 1 d . . . . . H13 H 0.655074 0.400655 0.375728 0.093 Uiso 1 1 calc R U . . . C14 C 0.6340(2) 0.2280(5) 0.3679(3) 0.0569(14) Uani 1 1 d . . . . . H14 H 0.602104 0.244822 0.360301 0.068 Uiso 1 1 calc R U . . . C15 C 0.64840(18) 0.1098(5) 0.3702(2) 0.0451(12) Uani 1 1 d . . . . . C16 C 0.5963(2) 0.2037(6) 0.4803(3) 0.0642(15) Uani 1 1 d . . . . . C17 C 0.5864(3) 0.3102(6) 0.4991(3) 0.0695(17) Uani 1 1 d . . . . . H17 H 0.609221 0.349669 0.544460 0.083 Uiso 1 1 calc R U . . . C18 C 0.5381(2) 0.3494(5) 0.4412(3) 0.0587(14) Uani 1 1 d . . . . . C19 C 0.6441(2) 0.1275(7) 0.5235(3) 0.092(2) Uani 1 1 d . . . . . H19A H 0.668756 0.161156 0.572247 0.138 Uiso 1 1 calc R U . . . H19B H 0.660780 0.125029 0.500181 0.138 Uiso 1 1 calc R U . . . H19C H 0.634261 0.046084 0.526696 0.138 Uiso 1 1 calc R U . . . C20 C 0.5080(3) 0.4581(5) 0.4304(4) 0.086(2) Uani 1 1 d . . . . . H20A H 0.474148 0.434785 0.418266 0.129 Uiso 1 1 calc R U . . . H20B H 0.501834 0.505824 0.390817 0.129 Uiso 1 1 calc R U . . . H20C H 0.527900 0.505762 0.474910 0.129 Uiso 1 1 calc R U . . . C21 C 0.47003(18) 0.2618(4) 0.3176(3) 0.0454(12) Uani 1 1 d . . . . . H21A H 0.475817 0.242693 0.281911 0.054 Uiso 1 1 calc R U . . . H21B H 0.453117 0.341695 0.305351 0.054 Uiso 1 1 calc R U . . . C22 C 0.43407(18) 0.1703(4) 0.3124(2) 0.0395(11) Uani 1 1 d . . . . . C23 C 0.3883(2) 0.2058(5) 0.3014(3) 0.0494(13) Uani 1 1 d . . . . . H23 H 0.379782 0.288429 0.297524 0.059 Uiso 1 1 calc R U . . . C24 C 0.3563(2) 0.1213(5) 0.2964(3) 0.0551(14) Uani 1 1 d . . . . . H24 H 0.324892 0.144489 0.288731 0.066 Uiso 1 1 calc R U . . . C25 C 0.36899(19) 0.0008(5) 0.3025(3) 0.0476(12) Uani 1 1 d . . . . . C26 C 0.3379(2) -0.0948(6) 0.2973(3) 0.0617(15) Uani 1 1 d . . . . . H26 H 0.306101 -0.076744 0.289595 0.074 Uiso 1 1 calc R U . . . C27 C 0.3519(2) -0.2094(6) 0.3028(3) 0.0703(17) Uani 1 1 d . . . . . H27 H 0.330617 -0.271140 0.300289 0.084 Uiso 1 1 calc R U . . . C28 C 0.3975(2) -0.2389(5) 0.3122(3) 0.0644(15) Uani 1 1 d . . . . . H28 H 0.406699 -0.320791 0.314996 0.077 Uiso 1 1 calc R U . . . C29 C 0.4290(2) -0.1513(4) 0.3175(3) 0.0520(13) Uani 1 1 d . . . . . H29 H 0.460377 -0.172475 0.324601 0.062 Uiso 1 1 calc R U . . . C30 C 0.41562(18) -0.0299(4) 0.3127(2) 0.0402(11) Uani 1 1 d . . . . . Cl1 Cl 0.6795(3) 0.5375(6) 0.6760(4) 0.056(2) Uani 0.515(8) 1 d D U P B 1 O2 O 0.6917(5) 0.5234(11) 0.7425(5) 0.118(3) Uani 0.515(8) 1 d D U P B 1 O3 O 0.6246(3) 0.5366(10) 0.6212(5) 0.071(3) Uani 0.515(8) 1 d D U P B 1 O4 O 0.7013(4) 0.4464(9) 0.6607(6) 0.082(3) Uani 0.515(8) 1 d D U P B 1 O5 O 0.6973(3) 0.6521(7) 0.6737(7) 0.097(3) Uani 0.515(8) 1 d D U P B 1 Cl1' Cl 0.6874(3) 0.5370(7) 0.6791(4) 0.0534(19) Uani 0.485(8) 1 d D U P B 2 O2' O 0.7110(3) 0.6126(10) 0.7376(5) 0.087(3) Uani 0.485(8) 1 d D U P B 2 O3' O 0.6357(4) 0.5102(10) 0.6516(8) 0.083(3) Uani 0.485(8) 1 d D U P B 2 O4' O 0.7178(4) 0.4321(8) 0.6991(6) 0.071(3) Uani 0.485(8) 1 d D U P B 2 O5' O 0.6881(4) 0.5942(12) 0.6258(6) 0.110(3) Uani 0.485(8) 1 d D U P B 2 Cl2 Cl 0.500000 0.46138(19) 0.750000 0.0677(6) Uani 0.62(2) 2 d DS TU P C 1 O6 O 0.5465(4) 0.5263(12) 0.7986(7) 0.103(4) Uani 0.62(2) 1 d D U P C 1 O7 O 0.5020(6) 0.3745(8) 0.7066(5) 0.089(3) Uani 0.62(2) 1 d D U P C 1 Cl2' Cl 0.500000 0.46138(19) 0.750000 0.0677(6) Uani 0.38(2) 2 d DS TU P C 2 O6' O 0.5333(6) 0.5491(15) 0.8043(9) 0.064(4) Uani 0.38(2) 1 d D U P C 2 O7' O 0.5285(8) 0.4100(17) 0.7269(10) 0.087(4) Uani 0.38(2) 1 d D U P C 2 N7 N 0.7554(4) 0.9025(9) 0.5558(6) 0.177(4) Uani 1 1 d . U . . . C31 C 0.7421(4) 0.8822(7) 0.5896(5) 0.103(3) Uani 1 1 d . U . . . C32 C 0.7272(3) 0.8620(8) 0.6314(4) 0.117(3) Uani 1 1 d . U . . . H32A H 0.738960 0.781996 0.653082 0.175 Uiso 1 1 calc R U . . . H32B H 0.688861 0.866810 0.601606 0.175 Uiso 1 1 calc R U . . . H32C H 0.743185 0.922535 0.669740 0.175 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.056(3) 0.0438(9) 0.0355(8) -0.0005(6) 0.0223(10) 0.0046(11) Zn1' 0.042(2) 0.0398(9) 0.0347(8) -0.0033(7) 0.0212(10) 0.0036(11) O1 0.033(2) 0.050(3) 0.037(3) 0.000 0.021(2) 0.000 N1 0.055(3) 0.060(3) 0.036(2) 0.010(2) 0.025(2) 0.021(2) N2 0.050(3) 0.043(2) 0.050(3) 0.0072(19) 0.032(2) 0.011(2) N3 0.039(2) 0.045(2) 0.039(2) -0.0018(19) 0.021(2) 0.0059(19) N4 0.040(2) 0.060(3) 0.048(2) -0.015(2) 0.025(2) -0.002(2) N5 0.048(2) 0.043(2) 0.057(3) -0.017(2) 0.036(2) -0.010(2) N6 0.038(2) 0.041(2) 0.039(2) -0.0008(18) 0.0239(19) -0.0012(18) C1 0.046(3) 0.077(4) 0.035(3) 0.003(3) 0.019(3) 0.010(3) C2 0.051(3) 0.070(4) 0.040(3) 0.015(3) 0.023(3) 0.003(3) C3 0.043(3) 0.046(3) 0.049(3) 0.006(2) 0.022(3) -0.001(2) C4 0.066(4) 0.123(6) 0.047(3) 0.008(4) 0.034(3) 0.031(4) C5 0.072(4) 0.051(3) 0.072(4) 0.013(3) 0.039(4) 0.017(3) C6 0.063(3) 0.043(3) 0.056(3) 0.002(2) 0.043(3) 0.007(2) C7 0.049(3) 0.048(3) 0.036(3) 0.005(2) 0.024(3) 0.014(2) C8 0.054(3) 0.051(3) 0.062(4) 0.012(3) 0.037(3) 0.021(3) C9 0.045(3) 0.072(4) 0.067(4) 0.005(3) 0.033(3) 0.017(3) C10 0.037(3) 0.061(3) 0.051(3) -0.007(3) 0.024(3) 0.003(2) C11 0.050(4) 0.078(4) 0.112(5) -0.017(4) 0.050(4) -0.012(3) C12 0.069(4) 0.065(4) 0.139(6) -0.027(4) 0.069(5) -0.023(3) C13 0.069(4) 0.056(4) 0.113(5) -0.026(4) 0.058(4) -0.013(3) C14 0.051(3) 0.055(3) 0.064(4) -0.013(3) 0.035(3) -0.002(3) C15 0.036(3) 0.051(3) 0.039(3) -0.005(2) 0.018(2) 0.002(2) C16 0.048(3) 0.091(4) 0.048(3) -0.026(3) 0.027(3) -0.021(3) C17 0.076(4) 0.084(4) 0.059(4) -0.037(3) 0.047(3) -0.039(3) C18 0.077(4) 0.053(3) 0.074(4) -0.025(3) 0.060(3) -0.024(3) C19 0.042(3) 0.154(7) 0.053(4) -0.018(4) 0.016(3) 0.001(4) C20 0.134(6) 0.055(4) 0.108(5) -0.025(4) 0.094(5) -0.013(4) C21 0.048(3) 0.035(3) 0.056(3) -0.002(2) 0.034(3) 0.004(2) C22 0.041(3) 0.042(3) 0.041(3) -0.003(2) 0.028(2) 0.000(2) C23 0.051(3) 0.048(3) 0.057(3) -0.002(3) 0.037(3) 0.006(2) C24 0.047(3) 0.070(3) 0.062(4) -0.003(3) 0.040(3) 0.003(3) C25 0.044(3) 0.061(3) 0.041(3) -0.001(2) 0.028(3) -0.004(2) C26 0.051(3) 0.081(4) 0.060(4) 0.001(3) 0.038(3) -0.016(3) C27 0.067(4) 0.068(4) 0.076(4) 0.007(3) 0.044(4) -0.020(3) C28 0.066(4) 0.046(3) 0.069(4) 0.010(3) 0.035(3) -0.005(3) C29 0.048(3) 0.043(3) 0.052(3) 0.006(2) 0.024(3) -0.003(2) C30 0.040(3) 0.045(3) 0.034(3) 0.001(2) 0.022(2) -0.003(2) Cl1 0.059(3) 0.036(3) 0.060(3) -0.003(2) 0.031(2) 0.001(2) O2 0.143(6) 0.117(6) 0.071(4) 0.003(4) 0.055(4) 0.017(5) O3 0.047(4) 0.067(5) 0.065(5) -0.001(4) 0.018(4) 0.008(4) O4 0.073(5) 0.081(5) 0.102(6) -0.019(5) 0.059(4) 0.013(4) O5 0.072(5) 0.050(4) 0.112(6) 0.004(4) 0.029(4) -0.015(4) Cl1' 0.044(2) 0.044(3) 0.070(3) 0.006(2) 0.034(2) 0.002(2) O2' 0.063(5) 0.089(5) 0.090(5) -0.039(5) 0.037(4) 0.006(4) O3' 0.050(5) 0.072(6) 0.110(7) -0.003(5) 0.041(4) -0.001(4) O4' 0.065(5) 0.055(4) 0.089(6) 0.011(4) 0.045(4) 0.010(4) O5' 0.109(6) 0.126(6) 0.091(5) 0.029(5) 0.060(4) 0.015(5) Cl2 0.0775(14) 0.0503(11) 0.0658(13) 0.000 0.0395(12) 0.000 O6 0.074(5) 0.090(6) 0.098(5) 0.004(4) 0.031(4) -0.025(5) O7 0.087(6) 0.077(5) 0.096(5) -0.004(4) 0.053(4) 0.012(4) Cl2' 0.0775(14) 0.0503(11) 0.0658(13) 0.000 0.0395(12) 0.000 O6' 0.058(6) 0.069(6) 0.075(6) -0.008(5) 0.045(5) 0.000(5) O7' 0.097(7) 0.087(7) 0.089(6) -0.003(5) 0.063(5) 0.024(5) N7 0.236(8) 0.168(7) 0.182(7) 0.007(6) 0.157(6) 0.026(6) C31 0.129(6) 0.071(4) 0.112(6) 0.009(4) 0.076(5) 0.029(4) C32 0.106(5) 0.130(6) 0.108(6) -0.002(5) 0.063(5) -0.007(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Zn1 N1 124.8(2) . . ? O1 Zn1 N4 121.0(3) . . ? N1 Zn1 N4 108.0(2) . . ? O1 Zn1 N6 92.3(2) . . ? N1 Zn1 N6 112.3(4) . . ? N4 Zn1 N6 90.3(2) . . ? O1 Zn1 H1 23.4 . . ? N1 Zn1 H1 130.7 . . ? N4 Zn1 H1 121.2 . . ? N6 Zn1 H1 69.0 . . ? O1 Zn1 H1 22(2) . 2_655 ? N1 Zn1 H1 115.8(13) . 2_655 ? N4 Zn1 H1 113.5(7) . 2_655 ? N6 Zn1 H1 114(2) . 2_655 ? H1 Zn1 H1 45.7 . 2_655 ? O1 Zn1' N4 123.9(2) . . ? O1 Zn1' N3 98.1(2) . . ? N4 Zn1' N3 115.3(4) . . ? O1 Zn1' N1 115.6(3) . . ? N4 Zn1' N1 105.8(2) . . ? N3 Zn1' N1 94.4(2) . . ? O1 Zn1' H1 24(3) . 2_655 ? N4 Zn1' H1 131.7(7) . 2_655 ? N3 Zn1' H1 74(3) . 2_655 ? N1 Zn1' H1 121.1(2) . 2_655 ? Zn1 O1 Zn1 174.9(3) 2_655 . ? Zn1 O1 Zn1' 22.44(6) 2_655 2_655 ? Zn1 O1 Zn1' 158.36(6) . 2_655 ? Zn1 O1 H1 94.0 2_655 . ? Zn1 O1 H1 86.3 . . ? Zn1' O1 H1 107.6 . . ? Zn1' O1 H1 72.1 2_655 . ? Zn1 O1 H1 86.3(3) 2_655 2_655 ? Zn1 O1 H1 94.0(3) . 2_655 ? H1 O1 H1 174.1 . 2_655 ? C1 N1 N2 105.0(4) . . ? C1 N1 Zn1 128.9(4) . . ? N2 N1 Zn1 126.1(4) . . ? C1 N1 Zn1' 139.1(4) . . ? N2 N1 Zn1' 112.5(3) . . ? C3 N2 N1 111.3(4) . . ? C3 N2 C6 129.5(4) . . ? N1 N2 C6 119.2(4) . . ? C7 N3 C15 118.4(4) . . ? C7 N3 Zn1' 118.0(4) . . ? C15 N3 Zn1' 123.5(3) . . ? C16 N4 N5 106.2(4) . . ? C16 N4 Zn1' 126.2(4) . . ? N5 N4 Zn1' 127.3(3) . . ? C16 N4 Zn1 136.2(4) . . ? N5 N4 Zn1 115.5(3) . . ? N4 N5 C18 111.2(4) . . ? N4 N5 C21 120.0(4) . . ? C18 N5 C21 128.7(5) . . ? C22 N6 C30 118.2(4) . . ? C22 N6 Zn1 116.0(3) . . ? C30 N6 Zn1 125.5(3) . . ? N1 C1 C2 110.3(5) . . ? N1 C1 C4 120.9(5) . . ? C2 C1 C4 128.8(5) . . ? C3 C2 C1 107.1(5) . . ? C3 C2 H2 126.5 . . ? C1 C2 H2 126.5 . . ? N2 C3 C2 106.3(5) . . ? N2 C3 C5 122.7(5) . . ? C2 C3 C5 130.9(5) . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? N2 C6 C7 112.1(4) . . ? N2 C6 H6A 109.2 . . ? C7 C6 H6A 109.2 . . ? N2 C6 H6B 109.2 . . ? C7 C6 H6B 109.2 . . ? H6A C6 H6B 107.9 . . ? N3 C7 C8 123.5(5) . . ? N3 C7 C6 117.1(4) . . ? C8 C7 C6 119.4(5) . . ? C9 C8 C7 119.2(5) . . ? C9 C8 H8 120.4 . . ? C7 C8 H8 120.4 . . ? C8 C9 C10 120.0(5) . . ? C8 C9 H9 120.0 . . ? C10 C9 H9 120.0 . . ? C9 C10 C11 123.2(5) . . ? C9 C10 C15 118.1(5) . . ? C11 C10 C15 118.6(5) . . ? C12 C11 C10 120.6(6) . . ? C12 C11 H11 119.7 . . ? C10 C11 H11 119.7 . . ? C11 C12 C13 120.7(6) . . ? C11 C12 H12 119.7 . . ? C13 C12 H12 119.7 . . ? C14 C13 C12 120.1(6) . . ? C14 C13 H13 120.0 . . ? C12 C13 H13 120.0 . . ? C13 C14 C15 120.7(5) . . ? C13 C14 H14 119.6 . . ? C15 C14 H14 119.6 . . ? N3 C15 C14 119.9(4) . . ? N3 C15 C10 120.8(4) . . ? C14 C15 C10 119.3(5) . . ? N4 C16 C17 108.8(5) . . ? N4 C16 C19 122.4(5) . . ? C17 C16 C19 128.7(6) . . ? C18 C17 C16 107.9(5) . . ? C18 C17 H17 126.1 . . ? C16 C17 H17 126.1 . . ? N5 C18 C17 105.9(5) . . ? N5 C18 C20 122.6(6) . . ? C17 C18 C20 131.5(6) . . ? C16 C19 H19A 109.5 . . ? C16 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C16 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C18 C20 H20A 109.5 . . ? C18 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C18 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N5 C21 C22 112.2(4) . . ? N5 C21 H21A 109.2 . . ? C22 C21 H21A 109.2 . . ? N5 C21 H21B 109.2 . . ? C22 C21 H21B 109.2 . . ? H21A C21 H21B 107.9 . . ? N6 C22 C23 123.2(4) . . ? N6 C22 C21 116.4(4) . . ? C23 C22 C21 120.3(4) . . ? C24 C23 C22 119.2(5) . . ? C24 C23 H23 120.4 . . ? C22 C23 H23 120.4 . . ? C23 C24 C25 120.2(5) . . ? C23 C24 H24 119.9 . . ? C25 C24 H24 119.9 . . ? C24 C25 C30 118.1(5) . . ? C24 C25 C26 124.7(5) . . ? C30 C25 C26 117.2(5) . . ? C27 C26 C25 122.1(5) . . ? C27 C26 H26 119.0 . . ? C25 C26 H26 119.0 . . ? C26 C27 C28 120.4(5) . . ? C26 C27 H27 119.8 . . ? C28 C27 H27 119.8 . . ? C29 C28 C27 120.5(5) . . ? C29 C28 H28 119.8 . . ? C27 C28 H28 119.8 . . ? C28 C29 C30 120.5(5) . . ? C28 C29 H29 119.8 . . ? C30 C29 H29 119.8 . . ? N6 C30 C29 119.5(4) . . ? N6 C30 C25 121.1(4) . . ? C29 C30 C25 119.4(5) . . ? O2 Cl1 O4 112.0(8) . . ? O2 Cl1 O3 111.0(8) . . ? O4 Cl1 O3 107.9(7) . . ? O2 Cl1 O5 108.2(8) . . ? O4 Cl1 O5 111.1(8) . . ? O3 Cl1 O5 106.5(7) . . ? O2' Cl1' O3' 111.0(8) . . ? O2' Cl1' O4' 109.4(8) . . ? O3' Cl1' O4' 111.3(7) . . ? O2' Cl1' O5' 107.9(9) . . ? O3' Cl1' O5' 110.7(8) . . ? O4' Cl1' O5' 106.4(7) . . ? O6 Cl2 O6 117.9(13) . 2_656 ? O6 Cl2 O7 115.5(6) . . ? O6 Cl2 O7 105.4(7) 2_656 . ? O6 Cl2 O7 105.4(7) . 2_656 ? O6 Cl2 O7 115.5(6) 2_656 2_656 ? O7 Cl2 O7 95.2(9) . 2_656 ? O6' Cl2' O6' 93.8(17) 2_656 . ? O6' Cl2' O7' 107.6(9) 2_656 2_656 ? O6' Cl2' O7' 103.9(10) . 2_656 ? O6' Cl2' O7' 103.9(10) 2_656 . ? O6' Cl2' O7' 107.6(9) . . ? O7' Cl2' O7' 133.3(17) 2_656 . ? N7 C31 C32 177.7(12) . . ? C31 C32 H32A 109.5 . . ? C31 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C31 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 O1 1.889(2) . ? Zn1 N1 1.964(4) . ? Zn1 N4 2.062(5) . ? Zn1 N6 2.214(9) . ? Zn1 H1 2.00(3) . ? Zn1 H1 2.10(4) 2_655 ? Zn1' O1 1.923(3) . ? Zn1' N4 1.973(4) . ? Zn1' N3 2.024(8) . ? Zn1' N1 2.111(6) . ? Zn1' H1 1.842(10) 2_655 ? O1 H1 0.80(9) . ? O1 H1 0.80(9) 2_655 ? N1 C1 1.337(6) . ? N1 N2 1.366(5) . ? N2 C3 1.337(6) . ? N2 C6 1.452(6) . ? N3 C7 1.325(6) . ? N3 C15 1.375(6) . ? N4 C16 1.346(6) . ? N4 N5 1.348(5) . ? N5 C18 1.350(6) . ? N5 C21 1.442(6) . ? N6 C22 1.319(6) . ? N6 C30 1.375(6) . ? C1 C2 1.367(7) . ? C1 C4 1.485(7) . ? C2 C3 1.366(7) . ? C2 H2 0.9500 . ? C3 C5 1.487(7) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.503(7) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C8 1.386(7) . ? C8 C9 1.356(7) . ? C8 H8 0.9500 . ? C9 C10 1.397(7) . ? C9 H9 0.9500 . ? C10 C11 1.409(8) . ? C10 C15 1.416(7) . ? C11 C12 1.345(8) . ? C11 H11 0.9500 . ? C12 C13 1.401(8) . ? C12 H12 0.9500 . ? C13 C14 1.362(8) . ? C13 H13 0.9500 . ? C14 C15 1.388(7) . ? C14 H14 0.9500 . ? C16 C17 1.373(8) . ? C16 C19 1.483(8) . ? C17 C18 1.363(8) . ? C17 H17 0.9500 . ? C18 C20 1.476(8) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C22 1.494(6) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C22 C23 1.394(6) . ? C23 C24 1.352(7) . ? C23 H23 0.9500 . ? C24 C25 1.386(7) . ? C24 H24 0.9500 . ? C25 C30 1.415(7) . ? C25 C26 1.418(7) . ? C26 C27 1.335(8) . ? C26 H26 0.9500 . ? C27 C28 1.387(8) . ? C27 H27 0.9500 . ? C28 C29 1.362(7) . ? C28 H28 0.9500 . ? C29 C30 1.404(6) . ? C29 H29 0.9500 . ? Cl1 O2 1.365(8) . ? Cl1 O4 1.405(7) . ? Cl1 O3 1.408(7) . ? Cl1 O5 1.417(8) . ? Cl1' O2' 1.374(8) . ? Cl1' O3' 1.402(7) . ? Cl1' O4' 1.408(7) . ? Cl1' O5' 1.417(8) . ? Cl2 O6 1.402(6) . ? Cl2 O6 1.402(6) 2_656 ? Cl2 O7 1.437(6) . ? Cl2 O7 1.437(6) 2_656 ? Cl2' O6' 1.431(8) 2_656 ? Cl2' O6' 1.431(8) . ? Cl2' O7' 1.446(8) 2_656 ? Cl2' O7' 1.446(8) . ? N7 C31 1.137(10) . ? C31 C32 1.353(10) . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 N1 N2 C3 0.2(6) . . . . ? Zn1 N1 N2 C3 -178.9(4) . . . . ? Zn1' N1 N2 C3 163.3(4) . . . . ? C1 N1 N2 C6 179.4(4) . . . . ? Zn1 N1 N2 C6 0.3(7) . . . . ? Zn1' N1 N2 C6 -17.5(5) . . . . ? C16 N4 N5 C18 0.2(6) . . . . ? Zn1' N4 N5 C18 -173.1(4) . . . . ? Zn1 N4 N5 C18 166.4(4) . . . . ? C16 N4 N5 C21 -177.4(4) . . . . ? Zn1' N4 N5 C21 9.3(7) . . . . ? Zn1 N4 N5 C21 -11.2(6) . . . . ? N2 N1 C1 C2 -0.4(6) . . . . ? Zn1 N1 C1 C2 178.6(5) . . . . ? Zn1' N1 C1 C2 -156.3(5) . . . . ? N2 N1 C1 C4 180.0(5) . . . . ? Zn1 N1 C1 C4 -1.0(8) . . . . ? Zn1' N1 C1 C4 24.1(9) . . . . ? N1 C1 C2 C3 0.5(6) . . . . ? C4 C1 C2 C3 -179.9(6) . . . . ? N1 N2 C3 C2 0.1(6) . . . . ? C6 N2 C3 C2 -179.0(5) . . . . ? N1 N2 C3 C5 179.4(5) . . . . ? C6 N2 C3 C5 0.3(8) . . . . ? C1 C2 C3 N2 -0.4(6) . . . . ? C1 C2 C3 C5 -179.5(5) . . . . ? C3 N2 C6 C7 -108.3(6) . . . . ? N1 N2 C6 C7 72.7(6) . . . . ? C15 N3 C7 C8 2.0(7) . . . . ? Zn1' N3 C7 C8 -175.3(4) . . . . ? C15 N3 C7 C6 -176.9(4) . . . . ? Zn1' N3 C7 C6 5.8(6) . . . . ? N2 C6 C7 N3 -65.4(6) . . . . ? N2 C6 C7 C8 115.7(5) . . . . ? N3 C7 C8 C9 -0.7(8) . . . . ? C6 C7 C8 C9 178.1(5) . . . . ? C7 C8 C9 C10 0.1(8) . . . . ? C8 C9 C10 C11 -177.6(6) . . . . ? C8 C9 C10 C15 -0.8(8) . . . . ? C9 C10 C11 C12 177.5(6) . . . . ? C15 C10 C11 C12 0.7(10) . . . . ? C10 C11 C12 C13 0.2(11) . . . . ? C11 C12 C13 C14 -1.1(11) . . . . ? C12 C13 C14 C15 1.0(9) . . . . ? C7 N3 C15 C14 177.2(5) . . . . ? Zn1' N3 C15 C14 -5.7(6) . . . . ? C7 N3 C15 C10 -2.7(7) . . . . ? Zn1' N3 C15 C10 174.5(4) . . . . ? C13 C14 C15 N3 -179.9(5) . . . . ? C13 C14 C15 C10 -0.1(8) . . . . ? C9 C10 C15 N3 2.1(7) . . . . ? C11 C10 C15 N3 179.1(5) . . . . ? C9 C10 C15 C14 -177.8(5) . . . . ? C11 C10 C15 C14 -0.8(8) . . . . ? N5 N4 C16 C17 -0.3(6) . . . . ? Zn1' N4 C16 C17 173.1(4) . . . . ? Zn1 N4 C16 C17 -162.1(5) . . . . ? N5 N4 C16 C19 -178.1(6) . . . . ? Zn1' N4 C16 C19 -4.7(9) . . . . ? Zn1 N4 C16 C19 20.1(9) . . . . ? N4 C16 C17 C18 0.3(7) . . . . ? C19 C16 C17 C18 177.9(6) . . . . ? N4 N5 C18 C17 0.0(6) . . . . ? C21 N5 C18 C17 177.3(5) . . . . ? N4 N5 C18 C20 179.2(5) . . . . ? C21 N5 C18 C20 -3.5(8) . . . . ? C16 C17 C18 N5 -0.2(6) . . . . ? C16 C17 C18 C20 -179.2(6) . . . . ? N4 N5 C21 C22 72.4(5) . . . . ? C18 N5 C21 C22 -104.7(5) . . . . ? C30 N6 C22 C23 0.5(7) . . . . ? Zn1 N6 C22 C23 -173.4(4) . . . . ? C30 N6 C22 C21 -179.1(4) . . . . ? Zn1 N6 C22 C21 7.0(5) . . . . ? N5 C21 C22 N6 -67.1(5) . . . . ? N5 C21 C22 C23 113.2(5) . . . . ? N6 C22 C23 C24 0.0(8) . . . . ? C21 C22 C23 C24 179.6(5) . . . . ? C22 C23 C24 C25 0.3(8) . . . . ? C23 C24 C25 C30 -1.0(7) . . . . ? C23 C24 C25 C26 -179.3(5) . . . . ? C24 C25 C26 C27 179.3(6) . . . . ? C30 C25 C26 C27 1.0(8) . . . . ? C25 C26 C27 C28 -1.6(9) . . . . ? C26 C27 C28 C29 1.5(9) . . . . ? C27 C28 C29 C30 -0.8(8) . . . . ? C22 N6 C30 C29 179.0(4) . . . . ? Zn1 N6 C30 C29 -7.7(6) . . . . ? C22 N6 C30 C25 -1.3(6) . . . . ? Zn1 N6 C30 C25 172.0(3) . . . . ? C28 C29 C30 N6 180.0(5) . . . . ? C28 C29 C30 C25 0.3(7) . . . . ? C24 C25 C30 N6 1.6(7) . . . . ? C26 C25 C30 N6 179.9(4) . . . . ? C24 C25 C30 C29 -178.8(5) . . . . ? C26 C25 C30 C29 -0.4(7) . . . . ?