#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:34:55 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296381 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572756.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572756 loop_ _publ_author_name 'Anju, Balakrishnan S.' 'Nair, Neeraja R.' 'Rajput, Janavi' 'Bertke, Jeffery A.' 'Mondal, Bhaskar' 'Kundu, Subrata' _publ_section_title ; Role of ancillary ligands in S-nitrosothiol and NO generation from nitrite-thiol interactions at mononuclear zinc(ii) sites. ; _journal_issue 43 _journal_name_full 'Chemical science' _journal_page_first 18000 _journal_page_last 18007 _journal_paper_doi 10.1039/d4sc04853a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C22 H26 N7 O2 Zn, Cl O4' _chemical_formula_sum 'C22 H26 Cl N7 O6 Zn' _chemical_formula_weight 585.32 _space_group_crystal_system orthorhombic _space_group_IT_number 52 _space_group_name_Hall '-P 2a 2bc' _space_group_name_H-M_alt 'P n n a' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary intrinsic _audit_creation_method SHELXL-2019/1 _audit_update_record ; 2024-05-16 deposited with the CCDC. 2024-10-03 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.0967(9) _cell_length_b 11.9311(8) _cell_length_c 14.7941(9) _cell_measurement_reflns_used 9938 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 27.92 _cell_measurement_theta_min 2.19 _cell_volume 2488.2(3) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELX-2018-3 (Sheldrick, 2015)' _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_device_type 'Bruker ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0461 _diffrn_reflns_av_unetI/netI 0.0239 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 40384 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.543 _diffrn_reflns_theta_min 2.626 _exptl_absorpt_coefficient_mu 1.148 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.5001 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.562 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1208 _exptl_crystal_size_max 0.095 _exptl_crystal_size_mid 0.078 _exptl_crystal_size_min 0.048 _refine_diff_density_max 0.371 _refine_diff_density_min -0.445 _refine_diff_density_rms 0.066 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.025 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 171 _refine_ls_number_reflns 3140 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.025 _refine_ls_R_factor_all 0.0408 _refine_ls_R_factor_gt 0.0304 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0422P)^2^+1.6276P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0781 _refine_ls_wR_factor_ref 0.0846 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2556 _reflns_number_total 3140 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04853a2.cif _cod_data_source_block ABS1238 _cod_depositor_comments 'Adding full bibliography for 1572750--1572760.cif.' _cod_database_code 1572756 _shelx_shelxl_version_number 2019/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.899 _shelx_estimated_absorpt_t_max 0.947 _shelx_res_file ; TITL abs1238_a.res in Pnna ABS1238.res created by SHELXL-2019/1 at 09:42:19 on 10-Aug-2023 REM Old TITL abs1238_a.res in Pnna REM SHELXT solution in Pnna: R1 0.111, Rweak 0.002, Alpha 0.026 REM 0.995 for 336 systematic absences, Orientation as input REM Formula found by SHELXT: C27 Cl N6 O2 Zn CELL 0.71073 14.0967 11.9311 14.7941 90 90 90 ZERR 4 0.0009 0.0008 0.0009 0 0 0 LATT 1 SYMM 0.5-X,-Y,+Z SYMM 0.5-X,0.5+Y,0.5-Z SYMM +X,0.5-Y,0.5-Z SFAC C H Cl N O Zn UNIT 88 104 4 28 24 4 L.S. 20 PLAN 20 SIZE 0.048 0.078 0.095 TEMP -123.15 BOND $H LIST 4 FMAP 2 CONF ACTA OMIT 11 0 11 WGHT 0.042200 1.627600 FVAR 0.29731 ZN1 6 0.407781 0.250000 0.250000 10.50000 0.01881 0.02346 = 0.01132 0.00012 0.00000 0.00000 O1 5 0.268407 0.183492 0.296728 11.00000 0.02901 0.04242 = 0.02218 -0.00649 0.00403 -0.00629 N1 4 0.497646 0.162249 0.336739 11.00000 0.02235 0.02204 = 0.01295 -0.00084 0.00166 0.00239 N2 4 0.484987 0.171137 0.428644 11.00000 0.02226 0.01947 = 0.01289 0.00037 0.00011 0.00244 N3 4 0.393493 0.373422 0.355529 11.00000 0.02047 0.02227 = 0.01400 0.00143 -0.00099 0.00060 N4 4 0.219003 0.250000 0.250000 10.50000 0.02249 0.05329 = 0.02747 -0.01710 0.00000 0.00000 C1 1 0.584647 0.119775 0.325797 11.00000 0.02269 0.01860 = 0.02000 -0.00168 0.00077 0.00041 C2 1 0.626530 0.101203 0.409853 11.00000 0.02291 0.02331 = 0.02419 -0.00065 -0.00355 0.00388 AFIX 43 H2 2 0.688069 0.071662 0.420697 11.00000 -1.20000 AFIX 0 C3 1 0.561480 0.133945 0.474170 11.00000 0.02454 0.01665 = 0.01873 -0.00043 -0.00450 0.00013 C4 1 0.625617 0.098529 0.234528 11.00000 0.02470 0.02820 = 0.02269 -0.00454 0.00392 0.00333 AFIX 137 H4A 2 0.578320 0.116420 0.188172 11.00000 -1.50000 H4B 2 0.643688 0.019461 0.229494 11.00000 -1.50000 H4C 2 0.681783 0.145736 0.225902 11.00000 -1.50000 AFIX 0 C5 1 0.565240 0.128230 0.574986 11.00000 0.03205 0.02657 = 0.01787 -0.00037 -0.00683 -0.00030 AFIX 137 H5A 2 0.546512 0.200777 0.600413 11.00000 -1.50000 H5B 2 0.629979 0.110182 0.594247 11.00000 -1.50000 H5C 2 0.521696 0.069983 0.596431 11.00000 -1.50000 AFIX 0 C6 1 0.398002 0.220164 0.464310 11.00000 0.02454 0.02554 = 0.01280 0.00251 0.00228 0.00319 AFIX 23 H6A 2 0.396174 0.209238 0.530623 11.00000 -1.20000 H6B 2 0.342785 0.180630 0.437978 11.00000 -1.20000 AFIX 0 C7 1 0.390143 0.344061 0.443539 11.00000 0.01612 0.02415 = 0.01450 0.00139 -0.00026 0.00270 C8 1 0.377644 0.422382 0.511089 11.00000 0.03049 0.02949 = 0.01533 -0.00129 -0.00296 0.00605 AFIX 43 H8 2 0.376096 0.399810 0.572652 11.00000 -1.20000 AFIX 0 C9 1 0.367368 0.534385 0.488163 11.00000 0.03543 0.02666 = 0.02327 -0.00648 -0.00642 0.00474 AFIX 43 H9 2 0.358931 0.589563 0.533756 11.00000 -1.20000 AFIX 0 C10 1 0.369572 0.564522 0.398203 11.00000 0.02865 0.02094 = 0.02735 0.00036 -0.00543 0.00004 AFIX 43 H10 2 0.361790 0.640550 0.380622 11.00000 -1.20000 AFIX 0 C11 1 0.383327 0.481878 0.334239 11.00000 0.02476 0.02419 = 0.01918 0.00352 -0.00153 -0.00127 AFIX 43 H11 2 0.385689 0.502863 0.272336 11.00000 -1.20000 AFIX 0 CL1 3 0.606976 0.750000 0.250000 10.50000 0.02669 0.03255 = 0.01481 0.00322 0.00000 0.00000 O2 5 0.547644 0.664024 0.287339 11.00000 0.04863 0.03141 = 0.03380 0.01173 -0.00135 -0.00565 O3 5 0.665537 0.795969 0.320249 11.00000 0.04074 0.07805 = 0.02023 -0.00582 -0.00208 -0.01787 HKLF 4 REM abs1238_a.res in Pnna REM wR2 = 0.0846, GooF = S = 1.025, Restrained GooF = 1.025 for all data REM R1 = 0.0304 for 2556 Fo > 4sig(Fo) and 0.0408 for all 3140 data REM 171 parameters refined using 0 restraints END WGHT 0.0422 1.6279 REM Highest difference peak 0.371, deepest hole -0.445, 1-sigma level 0.066 Q1 1 0.3713 0.5425 0.4437 11.00000 0.05 0.37 Q2 1 0.6131 0.1133 0.3623 11.00000 0.05 0.34 Q3 1 0.5638 0.1364 0.5214 11.00000 0.05 0.32 Q4 1 0.5918 0.1057 0.4441 11.00000 0.05 0.31 Q5 1 0.3833 0.5225 0.3710 11.00000 0.05 0.31 Q6 1 0.6062 0.1085 0.2845 11.00000 0.05 0.31 Q7 1 0.4865 0.1660 0.3859 11.00000 0.05 0.31 Q8 1 0.3895 0.2831 0.4525 11.00000 0.05 0.31 Q9 1 0.3623 0.4771 0.4887 11.00000 0.05 0.30 Q10 1 0.3948 0.4318 0.3523 11.00000 0.05 0.29 Q11 1 0.3900 0.3603 0.4001 11.00000 0.05 0.29 Q12 1 0.6914 0.0700 0.2470 11.00000 0.05 0.28 Q13 1 0.5975 0.6429 0.2648 11.00000 0.05 0.27 Q14 1 0.5837 0.0486 0.2110 11.00000 0.05 0.26 Q15 1 0.5268 0.1619 0.4502 11.00000 0.05 0.25 Q16 1 0.4068 0.3355 0.3227 11.00000 0.05 0.25 Q17 1 0.2385 0.1578 0.3438 11.00000 0.05 0.24 Q18 1 0.3887 0.3873 0.4749 11.00000 0.05 0.24 Q19 1 0.3645 0.3826 0.4759 11.00000 0.05 0.24 Q20 1 0.5623 0.1614 0.3287 11.00000 0.05 0.23 ; _shelx_res_checksum 10479 _shelx_hkl_file ; 0 1 0 0.10 0.20 0 1 0 0.20 0.10 0 -1 0 -0.10 0.10 0 2 0 5680.43 258.97 0 2 0 5247.97 258.77 0 -2 0 5349.16 259.67 0 -2 0 5122.49 258.97 0 -2 0 5414.96 258.67 0 -2 0 5688.43 260.17 0 -2 0 4577.44 258.87 0 3 0 -0.70 0.80 0 3 0 -0.30 0.70 0 -3 0 0.60 1.00 0 -3 0 0.10 0.40 0 -3 0 0.60 0.60 0 -3 0 1.70 0.70 0 -3 0 0.00 0.70 0 3 0 -0.50 0.60 0 4 0 249.18 12.70 0 4 0 254.37 13.60 0 4 0 263.27 13.00 0 -4 0 252.37 12.80 0 -4 0 248.58 12.70 0 -4 0 247.98 12.50 0 -4 0 240.88 12.90 0 -4 0 242.78 13.60 0 5 0 -1.20 0.90 0 -5 0 0.90 1.60 0 -5 0 -0.10 0.60 0 -5 0 0.30 0.90 0 5 0 -0.10 1.20 0 -5 0 0.40 0.90 0 6 0 133.59 7.70 0 -6 0 138.29 8.00 0 -6 0 143.79 7.30 0 -6 0 139.69 7.80 0 -6 0 141.59 9.20 0 -7 0 0.20 2.10 0 7 0 0.40 1.20 0 -7 0 0.60 1.20 0 -7 0 2.10 1.40 0 -7 0 0.20 0.80 0 -8 0 798.12 41.10 0 -8 0 822.02 40.00 0 -8 0 827.92 42.60 0 -8 0 785.32 40.60 0 -10 0 527.65 27.00 0 -10 0 521.65 25.90 0 -10 0 520.95 29.40 0 -10 0 497.25 27.40 0 -11 0 15.80 4.90 0 -11 0 18.80 2.90 0 -11 0 19.90 3.40 0 -12 0 285.77 19.50 0 -12 0 296.27 16.50 0 -13 0 11.50 3.00 0 -13 0 8.40 5.00 0 -14 0 168.68 15.50 0 -14 0 182.18 11.50 0 -15 0 8.80 6.40 0 -15 0 8.40 3.40 0 0 -1 0.00 0.10 0 0 -1 0.00 0.10 0 0 -1 0.20 0.10 0 0 -1 -0.10 0.10 0 -3 -1 3148.49 153.28 0 3 -1 3199.68 153.18 0 3 -1 3230.28 152.68 0 3 -1 3129.79 152.68 0 3 -1 3212.68 152.78 0 -3 -1 3030.00 152.48 0 -3 -1 3074.99 152.78 0 3 1 3162.68 153.28 0 3 1 3213.18 152.78 0 -3 1 3041.40 152.68 0 3 1 3125.09 152.38 0 -3 1 3054.39 152.78 0 -3 1 3043.00 153.18 0 -3 1 3099.59 152.68 0 4 -1 0.80 0.70 0 4 -1 0.70 1.00 0 4 -1 0.70 0.90 0 4 -1 0.60 0.90 0 -4 -1 0.30 0.80 0 -4 -1 0.20 0.60 0 -4 -1 0.60 1.20 0 -4 1 1.20 0.80 0 4 1 0.50 1.10 0 -4 1 -1.00 0.80 0 -4 1 1.00 0.90 0 -4 1 0.00 0.30 0 -4 1 -0.60 1.00 0 4 1 -0.20 0.60 0 4 1 1.40 0.90 0 5 -1 104.89 7.00 0 -5 -1 115.59 6.30 0 -5 -1 106.99 5.80 0 -5 -1 107.19 7.30 0 5 -1 108.39 6.20 0 -5 1 101.39 5.50 0 -5 1 104.69 6.10 0 5 1 109.39 7.30 0 5 1 105.89 5.80 0 -5 1 98.59 6.00 0 -5 1 109.69 6.30 0 -5 1 113.29 7.30 0 -6 -1 1.10 1.00 0 6 -1 2.30 1.30 0 -6 -1 -0.50 0.80 0 -6 -1 0.10 1.80 0 6 -1 -0.70 1.40 0 -6 -1 0.60 1.10 0 -6 1 1.30 1.10 0 -6 1 0.60 0.60 0 6 1 -1.20 1.00 0 -6 1 -0.50 1.70 0 -6 1 -0.80 1.20 0 -7 -1 5.60 1.40 0 -7 -1 4.90 1.60 0 -7 -1 2.80 1.00 0 -7 -1 1.80 2.40 0 -7 1 4.40 1.70 0 7 1 3.10 1.20 0 -7 1 2.80 0.70 0 -7 1 2.00 1.40 0 -7 1 1.20 2.30 0 -8 -1 -1.40 1.40 0 -8 -1 -0.50 1.20 0 -8 -1 2.70 2.90 0 -8 -1 -0.10 1.10 0 -8 1 1.60 0.80 0 8 1 -0.50 1.30 0 -8 1 1.80 1.70 0 -8 1 2.10 2.80 0 -8 1 -0.60 1.30 0 -9 -1 96.39 6.60 0 -9 -1 89.79 6.20 0 -9 -1 89.69 8.60 0 -9 -1 92.59 5.50 0 -9 1 94.49 6.40 0 9 1 100.69 6.20 0 -9 1 91.49 5.10 0 -9 1 81.99 8.30 0 -9 1 98.09 6.80 0 -10 -1 3.50 3.80 0 -10 -1 1.40 1.80 0 -10 -1 1.80 2.10 0 -10 -1 1.40 1.40 0 -10 1 4.40 3.70 0 -10 1 0.20 1.00 0 -10 1 2.30 2.00 0 -11 -1 -0.20 1.40 0 -11 -1 1.50 2.60 0 -11 -1 -1.90 3.40 0 -11 -1 -1.90 1.80 0 -11 1 1.60 3.90 0 -11 1 -3.40 1.80 0 -12 -1 -2.20 2.40 0 -12 -1 2.00 4.40 0 -12 -1 1.70 2.30 0 -12 1 3.10 4.40 0 -12 1 -1.60 2.20 0 -13 -1 14.30 3.10 0 -13 -1 14.10 4.10 0 -13 -1 3.20 4.70 0 -13 1 9.70 5.60 0 -13 1 6.20 2.80 0 -14 -1 -0.10 2.50 0 -14 -1 8.40 5.80 0 -14 1 1.40 2.70 0 -14 1 0.10 5.50 0 -15 -1 1.70 6.30 0 -15 -1 0.10 2.90 0 -15 1 -1.10 3.40 0 -15 1 -4.00 5.90 0 -15 1 1.20 2.80 0 0 2 2794.82 137.89 0 0 2 2919.21 137.99 0 0 2 2744.53 137.79 0 0 2 2827.02 138.19 0 -1 2 -0.10 0.10 0 2 -2 5354.96 253.47 0 2 -2 5497.45 253.07 0 2 -2 5279.77 253.77 0 -2 -2 5225.18 254.77 0 -2 -2 5077.99 254.47 0 2 -2 5148.49 252.97 0 -2 2 5034.70 253.27 0 2 2 5169.78 253.37 0 -2 2 4893.11 253.87 0 -2 2 5159.18 253.87 0 -2 2 5072.19 255.07 0 2 2 5382.26 254.87 0 2 2 5092.69 253.97 0 3 -2 2.00 1.10 0 3 -2 1.20 0.70 0 3 -2 0.70 0.80 0 3 -2 0.90 0.80 0 -3 -2 0.00 0.70 0 -3 -2 1.70 1.10 0 -3 2 1.80 0.80 0 -3 2 3.00 0.90 0 3 2 0.50 0.30 0 -3 2 0.80 0.90 0 3 2 1.20 0.80 0 -3 2 1.60 0.90 0 3 2 1.80 1.00 0 4 -2 2243.98 108.69 0 4 -2 2212.18 108.59 0 4 -2 2222.68 108.69 0 4 -2 2280.57 109.29 0 -4 -2 2175.68 108.69 0 -4 -2 2182.68 109.49 0 -4 -2 2180.48 108.49 0 4 2 2255.87 108.69 0 4 2 2203.98 108.09 0 -4 2 2248.18 109.29 0 -4 2 2199.68 108.59 0 4 2 2177.38 109.39 0 -4 2 2228.38 108.69 0 5 -2 0.70 1.20 0 -5 -2 0.60 1.70 0 -5 -2 0.50 0.90 0 5 -2 1.30 1.40 0 -5 -2 0.50 1.00 0 -5 2 -1.70 1.00 0 5 2 0.10 0.70 0 -5 2 1.00 1.00 0 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46.20 3.30 2 -2 2 33.50 2.30 2 -2 2 35.30 2.10 -2 2 2 32.10 2.50 2 -2 2 34.20 2.70 2 -2 2 30.60 2.20 2 -2 2 44.40 2.90 2 -2 2 31.60 2.40 2 -2 2 32.60 2.60 2 -1 -2 2218.28 102.59 -2 1 -2 2033.60 101.89 2 -1 -2 2152.18 102.19 -2 1 -2 2014.20 101.99 2 -1 -2 1973.00 102.19 -2 1 -2 2045.50 102.29 -2 1 -2 2032.70 101.89 -2 1 -2 2255.47 102.49 -2 1 -2 2065.39 102.29 2 -1 2 2228.18 102.49 2 -1 2 1997.10 102.19 2 -1 2 2017.50 102.09 -2 1 2 2288.07 102.69 -2 1 2 2092.09 102.19 2 -1 2 1947.21 101.99 2 -1 2 2061.39 101.99 -2 0 -2 124.99 6.90 2 0 -2 123.39 6.80 -2 0 -2 147.69 7.20 2 0 -2 137.49 6.90 2 0 -2 145.59 7.30 -2 0 -2 112.19 6.60 -2 0 -2 124.29 6.80 -2 0 -2 122.89 6.60 -2 0 -2 132.29 7.00 2 0 2 141.89 7.10 -2 0 2 127.89 6.80 2 0 2 129.29 7.00 -2 0 2 152.98 7.40 2 0 2 132.69 6.80 2 0 2 126.79 6.90 -2 0 2 129.39 6.90 2 0 2 126.99 6.60 -2 0 2 124.09 6.60 -2 -1 -2 2038.00 100.19 2 1 -2 2106.29 100.19 -2 -1 -2 2015.90 99.79 2 1 -2 2034.80 99.89 -2 -1 -2 2025.60 99.69 -2 -1 -2 2020.80 99.49 2 1 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6.10 -2 -4 -2 82.79 5.00 -2 -4 2 87.09 5.00 2 4 2 92.59 5.10 -2 -4 2 86.29 4.80 2 4 2 93.49 6.00 2 4 2 89.89 5.40 2 4 2 84.49 4.90 -2 -4 2 88.89 5.30 -2 -4 2 92.49 6.00 2 5 -2 867.31 42.20 2 5 -2 913.21 43.70 2 5 -2 874.41 42.70 -2 -5 -2 846.92 42.30 2 5 -2 910.31 43.40 -2 -5 -2 840.82 42.70 -2 -5 -2 836.72 42.50 -2 -5 -2 825.32 43.80 -2 -5 2 840.32 42.90 2 5 2 860.61 42.80 2 5 2 863.71 42.50 -2 -5 2 836.52 42.60 -2 -5 2 826.22 42.30 -2 -5 2 876.61 43.80 2 6 -2 107.39 5.70 -2 -6 -2 116.19 6.00 -2 -6 -2 103.49 7.80 -2 -6 -2 105.49 6.20 2 6 -2 108.09 7.50 -2 -6 -2 107.99 6.40 -2 -6 2 104.59 5.80 -2 -6 2 99.29 6.30 -2 -6 2 110.69 7.70 -2 -6 2 93.69 6.60 -2 -7 -2 185.58 10.80 -2 -7 -2 187.88 10.30 -2 -7 -2 208.88 12.60 -2 -7 -2 191.28 10.40 2 7 -2 190.68 9.90 -2 -7 2 205.38 12.40 -2 -7 2 184.08 10.00 2 7 2 199.28 10.30 -2 -7 2 186.08 11.00 -2 -7 2 198.08 10.70 -2 -8 -2 94.59 5.60 -2 -8 -2 87.89 8.10 -2 -8 -2 90.59 6.20 -2 -8 -2 85.99 5.60 2 8 2 89.09 5.40 -2 -8 2 86.69 7.60 -2 -8 2 82.99 5.10 -2 -8 2 91.69 6.40 -2 -8 2 92.99 6.00 -2 -9 -2 902.21 47.80 -2 -9 -2 914.61 45.20 -2 -9 -2 910.51 45.10 -2 -9 -2 912.51 45.80 -2 -9 2 875.71 44.60 -2 -9 2 928.91 47.70 -2 -9 2 863.21 45.90 2 9 2 918.41 44.90 -2 -9 2 895.01 45.50 -2 -10 -2 68.19 7.90 -2 -10 -2 80.99 5.40 -2 -10 -2 90.89 5.50 -2 -10 -2 97.29 6.60 -2 -10 2 66.79 6.30 -2 -10 2 72.59 5.70 -2 -10 2 62.79 7.80 -2 -10 2 63.79 4.40 -2 -11 -2 159.48 10.30 -2 -11 -2 177.78 13.20 -2 -11 -2 149.79 9.30 -2 -11 -2 159.78 9.20 -2 -11 2 150.58 10.30 -2 -11 2 150.08 12.60 -2 -11 2 150.58 9.70 -2 -12 -2 62.89 8.70 -2 -12 -2 64.89 5.40 -2 -12 2 39.50 7.30 -2 -12 2 61.69 6.60 -2 -12 2 67.39 5.80 -2 -13 -2 136.59 13.00 -2 -13 -2 122.29 8.40 -2 -13 2 119.99 8.70 -2 -13 2 127.89 12.80 -2 -13 2 122.99 9.90 -2 -14 -2 14.60 3.60 -2 -14 -2 16.70 6.60 -2 -14 2 14.80 3.60 -2 -14 2 18.10 6.60 -2 -14 2 27.50 5.00 -2 -15 -2 129.59 14.80 -2 -15 2 132.09 17.10 2 15 2 141.19 11.30 -2 -15 2 157.58 11.80 -2 -15 2 143.89 10.20 2 -15 -3 1.60 3.90 2 -15 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7.00 2 -15 4 44.60 6.20 2 -14 -4 0.00 2.60 2 -14 -4 0.50 3.50 2 -14 -4 2.70 5.70 2 -14 4 -0.20 3.30 2 -14 4 -0.40 2.90 2 -13 -4 95.39 11.50 2 -13 -4 104.89 7.60 2 -13 4 117.19 8.20 2 -13 4 73.59 7.90 2 -12 -4 11.10 2.90 2 -12 -4 10.60 3.70 2 -12 -4 15.30 3.20 2 -12 -4 6.60 5.30 2 -12 4 12.60 3.50 2 -12 4 16.70 3.90 2 -12 4 9.40 4.80 2 -11 -4 548.85 29.10 2 -11 -4 561.64 32.30 2 -11 -4 570.14 28.60 2 -11 -4 557.94 29.80 2 -11 4 565.14 29.50 2 -11 4 564.94 31.60 2 -11 4 513.15 29.60 2 -11 4 563.74 29.60 2 -10 -4 43.70 4.10 2 -10 -4 50.19 7.00 2 -10 -4 48.30 5.30 2 -10 4 50.09 6.40 2 -10 4 46.60 4.90 2 -10 4 43.90 4.80 2 -10 4 35.80 4.50 2 -9 -4 76.89 8.40 2 -9 -4 84.29 6.40 2 -9 -4 89.69 5.80 2 -9 4 82.59 6.50 2 -9 4 82.89 6.30 2 -9 4 79.09 7.80 2 -9 4 85.29 6.30 2 -8 -4 91.59 8.30 2 -8 -4 89.59 6.40 2 -8 4 86.29 7.60 2 -8 4 88.59 6.50 2 -8 4 92.79 6.60 2 -8 4 93.79 6.60 2 -7 -4 661.83 35.40 -2 7 -4 678.73 34.90 2 -7 -4 658.83 34.00 2 -7 4 655.83 34.80 2 -7 4 654.53 33.90 2 -7 4 664.23 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1 -3 51.99 4.20 8 1 3 54.99 3.00 -8 -1 3 55.69 3.10 -8 -1 3 60.49 6.80 -8 -1 3 58.39 5.10 -8 -1 3 62.89 4.20 8 2 -3 25.80 2.80 -8 -2 -3 23.30 3.00 -8 -2 -3 29.20 2.10 -8 -2 -3 25.20 4.30 8 2 3 25.80 3.00 8 2 3 25.10 1.70 -8 -2 3 28.20 4.40 -8 -2 3 31.90 3.00 8 2 3 25.80 1.80 -8 -2 3 24.40 3.20 -8 -3 -3 132.19 8.20 -8 -3 -3 132.09 9.90 -8 -3 3 128.49 8.40 -8 -3 3 128.69 7.90 8 3 3 132.19 6.90 -8 -3 3 134.49 10.00 8 3 3 134.69 6.90 8 3 3 126.89 7.90 -8 -4 -3 0.60 1.70 -8 -4 -3 2.00 2.70 -8 -4 3 0.90 1.90 8 4 3 -1.00 1.50 8 4 3 -0.40 0.90 -8 -4 3 1.70 2.80 -8 -4 3 3.60 1.60 -8 -5 -3 0.20 2.80 -8 -5 -3 1.30 2.10 8 5 3 -0.20 1.70 -8 -5 3 1.10 3.10 -8 -5 3 -0.20 1.60 -8 -5 3 -0.10 1.80 8 5 3 1.00 1.20 -8 -6 -3 10.20 4.00 8 6 -3 5.90 1.10 -8 -6 -3 4.30 2.10 -8 -6 3 11.20 2.60 -8 -6 3 4.90 3.60 8 6 3 7.90 2.20 -8 -6 3 11.00 2.60 -8 -7 -3 6.90 4.10 8 7 -3 9.60 1.60 -8 -7 -3 9.90 2.50 -8 -7 3 13.10 4.60 -8 -7 3 13.90 2.70 8 7 3 4.70 2.30 -8 -7 3 8.70 2.60 -8 -8 -3 41.20 6.50 -8 -8 -3 38.20 4.40 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14.30 1.80 -10 2 -1 15.70 5.00 10 -2 -1 17.00 2.40 -10 2 1 16.20 4.80 -10 2 1 13.70 2.70 10 -2 1 10.30 2.00 10 -1 -1 3.70 1.30 -10 1 -1 3.50 1.30 -10 1 1 5.40 2.30 10 -1 1 5.40 1.50 -10 1 1 11.50 4.10 10 0 -1 0.50 1.50 10 0 -1 2.40 1.10 -10 0 -1 2.10 1.90 -10 0 -1 3.00 3.10 10 0 1 3.20 1.20 -10 0 1 1.40 1.50 -10 0 1 3.30 2.10 -10 0 1 7.10 3.60 -10 0 1 1.50 1.10 -10 -1 -1 4.90 3.20 -10 -1 -1 3.40 2.20 10 1 -1 5.10 1.70 -10 -1 1 17.00 4.30 -10 -1 1 5.00 1.40 -10 -1 1 3.80 1.50 -10 -2 -1 13.10 2.30 -10 -2 -1 12.90 1.70 10 2 -1 16.30 2.20 -10 -2 -1 17.40 4.50 -10 -2 -1 16.60 3.20 -10 -2 1 12.90 2.00 -10 -2 1 14.30 2.90 -10 -2 1 17.20 4.40 -10 -2 1 16.60 1.90 10 2 1 13.70 1.90 -10 -3 -1 6.50 2.50 -10 -3 -1 7.80 1.50 -10 -3 -1 5.30 2.00 -10 -3 -1 5.90 3.70 10 3 -1 8.00 1.90 10 3 1 3.90 1.50 -10 -3 1 12.30 2.00 -10 -3 1 2.10 3.40 10 3 1 7.40 1.90 -10 -3 1 6.10 2.60 -10 -4 -1 9.00 2.60 -10 -4 -1 7.50 4.10 -10 -4 -1 9.40 2.10 -10 -4 -1 9.10 1.80 10 4 1 9.40 1.90 -10 -4 1 6.10 4.00 -10 -4 1 6.90 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9.90 -10 2 2 131.59 11.90 -10 2 2 169.28 10.00 10 -1 -2 149.19 9.00 -10 1 -2 160.38 9.70 -10 1 -2 156.48 8.30 10 -1 -2 158.48 8.50 -10 1 -2 131.79 11.20 -10 1 2 139.89 12.00 10 -1 2 153.68 8.30 -10 1 2 151.88 9.60 10 0 -2 393.26 20.60 10 0 -2 434.16 20.70 -10 0 -2 372.56 21.20 -10 0 -2 398.56 23.60 10 0 2 380.66 19.90 -10 0 2 409.46 20.30 -10 0 2 403.26 21.50 -10 0 2 395.36 20.30 -10 0 2 361.66 23.40 -10 -1 -2 140.09 11.50 -10 -1 -2 156.78 9.80 -10 -1 -2 157.28 7.90 10 1 -2 150.88 9.00 -10 -1 2 157.18 8.70 -10 -1 2 155.88 8.20 10 1 2 150.48 8.10 -10 -1 2 153.88 9.70 -10 -1 2 143.39 11.90 -10 -2 -2 154.38 8.40 10 2 -2 169.48 9.20 -10 -2 -2 140.39 11.90 -10 -2 -2 142.19 9.70 10 2 2 156.08 8.40 -10 -2 2 166.48 8.10 -10 -2 2 158.58 9.00 -10 -2 2 163.98 10.20 -10 -2 2 148.09 12.10 -10 -3 -2 23.90 2.40 10 3 -2 27.70 3.00 -10 -3 -2 17.70 4.40 -10 -3 -2 20.10 3.30 -10 -3 2 21.30 3.50 10 3 2 25.90 2.30 10 3 2 25.60 3.00 -10 -3 2 28.30 3.00 -10 -3 2 28.00 5.70 10 4 -2 316.97 17.20 -10 -4 -2 284.87 19.80 -10 -4 -2 324.17 17.00 -10 -4 -2 347.57 18.20 -10 -4 2 314.77 17.40 -10 -4 2 284.97 19.80 10 4 2 337.37 16.70 10 4 2 332.57 16.60 10 4 2 343.77 16.60 10 4 2 327.37 17.20 -10 -4 2 322.47 18.20 -10 -5 -2 6.20 1.80 -10 -5 -2 7.30 2.70 -10 -5 -2 6.70 4.00 -10 -5 2 1.60 3.90 -10 -5 2 9.50 2.40 -10 -5 2 4.40 2.60 10 5 2 6.70 2.10 10 6 -2 470.25 23.10 -10 -6 -2 479.15 24.80 -10 -6 -2 459.25 23.80 -10 -6 -2 408.16 26.70 -10 -6 2 413.86 26.90 -10 -6 2 478.55 24.80 -10 -6 2 466.65 24.20 10 6 2 456.15 23.60 -10 -7 -2 122.39 7.80 -10 -7 -2 108.49 8.50 -10 -7 -2 102.69 10.70 -10 -7 2 128.69 8.60 10 7 2 112.39 7.40 -10 -7 2 121.79 8.10 -10 -7 2 104.69 11.30 -10 -8 -2 549.45 27.60 -10 -8 -2 493.65 30.70 -10 -8 -2 525.35 28.00 -10 -8 2 523.15 27.90 10 8 2 522.85 27.10 -10 -8 2 487.05 30.60 -10 -8 2 535.65 27.90 -10 -9 -2 5.50 5.00 -10 -9 -2 6.30 2.80 -10 -9 -2 0.80 2.80 -10 -9 2 1.70 2.60 -10 -9 2 3.10 2.40 -10 -9 2 0.60 4.80 10 9 2 0.80 2.20 -10 -10 -2 181.88 11.50 -10 -10 -2 146.49 15.10 -10 -10 -2 188.08 11.90 -10 -10 2 164.18 15.20 -10 -10 2 184.28 11.70 -10 -10 2 190.68 12.00 10 10 2 166.88 11.60 -10 -11 -2 38.80 5.50 -10 -11 -2 36.20 5.00 -10 -11 -2 44.80 9.20 -10 -11 2 36.80 8.50 -10 -11 2 50.89 5.90 -10 -12 -2 42.80 5.40 -10 -12 -2 39.30 8.90 -10 -12 -2 43.50 5.90 -10 -12 2 37.70 5.60 -10 -12 2 24.70 7.60 -10 -13 -2 0.40 3.40 -10 -13 -2 2.10 6.50 -10 -13 2 -0.80 3.30 -10 -13 2 -2.30 6.10 10 -13 -3 14.90 7.20 10 -13 -3 14.60 4.70 10 -13 3 12.90 4.70 10 -13 3 14.00 4.60 10 -12 -3 0.90 5.40 10 -12 -3 -0.70 3.20 10 -12 3 -1.40 3.30 10 -12 3 4.50 3.80 10 -12 3 3.00 3.40 10 -11 -3 -0.80 3.30 10 -11 -3 6.00 5.40 -10 11 -3 0.20 6.00 10 -11 3 -3.00 2.70 10 -11 3 0.00 3.20 10 -11 3 -3.20 4.70 10 -11 3 -1.00 2.80 -10 11 3 0.60 6.60 10 -10 -3 70.09 9.70 10 -10 -3 62.09 6.60 -10 10 -3 29.10 8.20 -10 10 3 26.20 8.80 10 -10 3 47.10 5.70 10 -10 3 57.79 8.70 10 -10 3 44.70 5.50 10 -10 3 42.90 5.40 10 -9 -3 46.90 8.10 -10 9 -3 35.30 7.70 10 -9 -3 44.40 4.80 10 -9 -3 43.50 5.30 10 -9 3 38.00 5.30 10 -9 3 53.59 5.90 10 -9 3 43.10 7.20 -10 9 3 35.80 9.10 10 -9 3 49.30 5.50 10 -8 -3 20.40 5.60 10 -8 -3 21.70 3.40 -10 8 -3 17.00 6.30 10 -8 -3 19.00 3.70 10 -8 3 11.00 3.10 -10 8 3 16.50 6.40 10 -8 3 8.10 4.50 10 -8 3 10.70 3.40 10 -8 3 21.70 3.70 -10 7 -3 26.20 6.60 -10 7 -3 46.70 4.40 10 -7 -3 43.90 7.10 10 -7 -3 42.70 4.80 10 -7 -3 37.40 4.90 10 -7 3 40.30 4.90 10 -7 3 46.00 6.70 10 -7 3 50.59 5.60 -10 7 3 19.30 6.60 10 -7 3 47.90 4.70 10 -7 3 54.09 4.80 -10 6 -3 17.50 2.90 -10 6 -3 10.00 5.10 10 -6 -3 15.20 3.20 10 -6 -3 13.10 4.50 10 -6 -3 15.30 3.30 -10 6 3 8.80 5.50 10 -6 3 15.20 2.70 10 -6 3 20.30 3.80 10 -6 3 15.20 1.90 10 -6 3 11.10 4.40 -10 5 -3 21.70 5.70 -10 5 -3 26.00 3.40 10 -5 -3 26.30 3.80 10 -5 3 33.20 4.40 -10 5 3 20.80 6.10 10 -5 3 33.90 3.50 10 -5 3 32.10 2.40 10 -4 -3 1.60 2.20 -10 4 -3 3.10 3.70 -10 4 -3 -0.30 1.70 -10 4 3 0.80 4.20 10 -4 3 0.70 1.60 10 -4 3 -0.90 2.60 -10 3 -3 47.30 4.60 10 -3 -3 43.40 4.20 -10 3 -3 41.60 6.70 10 -3 3 36.70 3.30 -10 3 3 38.00 6.60 10 -3 3 29.20 4.40 10 -2 -3 2.90 1.90 -10 2 -3 4.60 2.20 -10 2 -3 1.00 1.10 -10 2 -3 6.10 3.50 10 -2 3 1.90 1.30 10 -2 3 3.90 2.60 -10 2 3 3.20 2.40 -10 2 3 8.60 4.20 -10 1 -3 -0.10 0.80 -10 1 -3 -1.30 2.50 10 -1 -3 2.70 1.90 -10 1 -3 -1.20 1.50 10 -1 3 0.30 2.20 10 -1 3 -0.60 0.90 -10 1 3 -1.70 3.10 -10 1 3 -1.40 1.70 -10 0 -3 -0.80 1.70 -10 0 -3 -0.10 2.90 10 0 -3 -1.70 1.60 -10 0 3 1.10 3.40 -10 0 3 -0.80 1.30 -10 0 3 -0.90 1.80 10 0 3 -1.10 0.80 -10 0 3 0.30 1.30 -10 -1 -3 -2.00 1.90 -10 -1 -3 -1.50 2.60 10 1 -3 -1.30 1.60 -10 -1 3 2.40 2.30 -10 -1 3 -0.30 1.30 10 1 3 0.00 0.70 -10 -1 3 0.60 0.90 -10 -1 3 -1.60 2.90 -10 -2 -3 3.70 1.00 10 2 -3 3.10 1.80 -10 -2 -3 3.90 3.50 -10 -2 -3 2.60 2.00 -10 -2 3 6.40 3.50 -10 -2 3 3.40 2.20 -10 -2 3 5.30 1.70 10 2 3 5.00 0.90 -10 -3 -3 41.10 3.10 10 3 -3 30.40 3.60 -10 -3 -3 38.70 4.40 -10 -3 -3 33.20 5.50 10 3 3 41.60 2.70 10 3 3 44.00 2.80 10 3 3 37.90 3.80 -10 -3 3 33.70 6.20 -10 -3 3 38.60 4.40 -10 -3 3 36.10 3.80 -10 -4 -3 -0.50 3.10 -10 -4 -3 -2.10 1.90 10 4 -3 2.30 1.90 -10 -4 -3 2.20 1.30 -10 -4 3 1.90 2.50 -10 -4 3 2.60 1.80 10 4 3 -0.20 1.10 -10 -4 3 2.70 3.60 10 4 3 4.60 2.10 -10 -5 -3 20.50 5.10 -10 -5 -3 29.90 4.30 -10 -5 -3 33.60 3.20 10 5 3 35.60 3.70 -10 -5 3 24.30 5.80 -10 -5 3 27.30 3.50 -10 -5 3 37.20 4.60 -10 -6 -3 11.30 2.40 -10 -6 -3 9.30 4.30 -10 -6 -3 15.90 3.30 -10 -6 3 9.80 2.80 -10 -6 3 16.50 3.50 -10 -6 3 16.50 5.30 10 6 3 16.10 2.80 -10 -7 -3 39.80 4.70 -10 -7 -3 32.80 6.60 -10 -7 -3 45.20 4.20 10 7 3 37.20 4.10 -10 -7 3 30.00 6.30 -10 -7 3 32.50 4.40 -10 -7 3 42.70 4.60 -10 -8 -3 17.50 3.20 -10 -8 -3 17.60 3.90 -10 -8 -3 20.40 5.80 -10 -8 3 19.50 5.90 10 8 3 20.00 3.20 -10 -8 3 12.70 3.30 -10 -8 3 15.30 3.50 -10 -9 -3 53.89 5.30 -10 -9 -3 58.69 6.10 -10 -9 -3 42.60 7.70 -10 -9 3 43.80 7.90 -10 -9 3 47.60 5.30 10 9 3 43.80 4.70 -10 -9 3 50.19 5.70 -10 -10 -3 54.49 6.10 -10 -10 -3 61.39 6.10 -10 -10 -3 55.89 9.30 -10 -10 3 47.00 5.80 -10 -10 3 42.50 8.20 -10 -10 3 55.39 5.90 10 10 3 55.49 5.40 -10 -11 -3 1.50 5.30 -10 -11 -3 2.30 2.80 -10 -11 -3 -3.10 3.10 -10 -11 3 1.80 5.60 -10 -11 3 4.20 3.30 -10 -12 -3 -0.50 3.30 -10 -12 -3 -0.30 6.00 -10 -12 -3 0.20 3.00 -10 -12 3 3.90 5.90 -10 -12 3 -1.60 2.60 -10 -13 -3 7.10 6.40 -10 -13 -3 10.10 3.90 -10 -13 3 11.90 4.00 10 -13 -4 18.40 7.60 10 -13 -4 17.20 5.40 10 -13 4 26.20 5.70 10 -13 4 23.40 5.00 10 -12 -4 103.19 12.40 10 -12 -4 78.59 8.70 10 -12 4 106.59 8.80 10 -12 4 107.09 9.50 10 -11 -4 6.70 5.40 10 -11 -4 3.10 3.30 -10 11 -4 -5.90 5.30 10 -11 4 4.70 3.50 10 -11 4 1.80 3.20 10 -11 4 -1.40 3.00 -10 11 4 3.80 7.40 10 -10 -4 110.69 11.80 -10 10 -4 73.89 11.60 10 -10 -4 88.99 8.30 10 -10 4 98.89 11.50 10 -10 4 112.69 8.50 -10 10 4 61.79 11.80 10 -10 4 104.49 8.30 10 -10 4 102.39 8.20 10 -9 -4 86.69 6.60 -10 9 -4 49.30 9.70 10 -9 -4 90.19 10.40 10 -9 -4 115.09 8.30 -10 9 4 62.59 10.70 10 -9 4 98.69 8.00 10 -9 4 93.09 8.10 10 -9 4 99.49 10.70 10 -9 4 87.69 7.40 10 -8 -4 139.89 12.40 -10 8 -4 107.29 13.00 10 -8 -4 152.18 9.90 10 -8 -4 132.89 8.70 -10 8 4 97.99 13.20 10 -8 4 137.89 11.80 10 -8 4 135.39 9.50 10 -8 4 125.69 9.40 10 -8 4 131.39 8.90 10 -7 -4 18.10 3.20 -10 7 -4 15.10 5.90 10 -7 -4 18.50 5.20 10 -7 -4 15.10 3.60 -10 7 -4 21.50 3.10 10 -7 4 14.80 5.10 -10 7 4 10.80 5.70 10 -7 4 13.90 3.50 10 -7 4 21.60 4.20 10 -7 4 19.10 3.20 10 -6 -4 696.93 33.70 10 -6 -4 660.33 33.40 -10 6 -4 533.65 35.80 10 -6 -4 681.63 36.40 -10 6 -4 654.53 33.00 10 -6 4 653.63 34.00 -10 6 4 515.15 36.30 10 -6 4 670.23 32.80 10 -6 4 643.44 33.30 10 -6 4 660.03 35.60 -10 5 -4 21.20 5.60 -10 5 -4 20.90 3.10 10 -5 -4 25.30 3.80 10 -5 4 17.60 3.40 -10 5 4 13.00 5.40 10 -5 4 19.80 3.70 10 -5 4 19.90 2.80 10 -4 -4 815.22 40.70 -10 4 -4 848.22 40.70 -10 4 -4 712.83 43.20 -10 4 4 707.73 43.40 10 -4 4 811.52 40.50 10 -4 4 824.22 39.90 10 -4 4 818.52 41.30 10 -3 -4 45.40 4.70 -10 3 -4 49.50 4.80 -10 3 -4 54.99 3.70 -10 3 -4 50.89 7.30 -10 3 4 53.29 7.70 10 -3 4 48.30 3.80 10 -3 4 49.60 5.50 10 -2 -4 563.84 28.20 -10 2 -4 534.85 28.30 -10 2 -4 509.35 30.60 -10 2 -4 563.64 27.00 -10 2 4 489.45 30.60 10 -2 4 527.95 28.90 10 -2 4 561.84 27.00 -10 1 -4 16.00 2.80 10 -1 -4 15.20 2.80 -10 1 -4 19.50 4.50 10 -1 4 19.20 1.70 -10 1 4 24.00 5.70 10 -1 4 16.50 3.40 -10 1 4 15.30 3.00 -10 0 -4 179.58 10.60 -10 0 -4 164.18 12.50 10 0 -4 179.88 10.20 10 0 4 162.28 10.90 -10 0 4 168.08 12.90 -10 0 4 172.68 9.90 -10 0 4 166.98 10.70 -10 -1 -4 18.00 4.10 10 1 -4 14.40 2.50 -10 -1 -4 16.30 3.00 -10 -1 4 11.70 3.00 -10 -1 4 16.60 2.60 -10 -1 4 25.90 5.40 -10 -2 -4 512.05 30.40 -10 -2 -4 534.85 28.50 10 2 -4 563.44 28.10 -10 -2 -4 552.74 26.90 -10 -2 4 556.94 28.00 10 2 4 554.04 28.20 -10 -2 4 501.95 30.50 -10 -2 4 536.95 28.70 10 3 -4 51.49 4.60 -10 -3 -4 38.60 6.20 -10 -3 -4 46.60 3.40 -10 -3 -4 48.10 5.00 -10 -3 4 46.10 6.80 10 3 4 44.20 4.50 10 3 4 56.29 3.40 -10 -3 4 49.60 4.50 -10 -3 4 41.60 5.10 -10 -4 -4 832.72 40.70 -10 -4 -4 785.12 41.80 -10 -4 -4 809.52 44.20 10 4 -4 803.72 41.40 -10 -4 4 767.02 44.00 10 4 4 850.91 40.10 -10 -4 4 823.82 41.60 10 4 4 814.12 41.40 -10 -4 4 816.22 42.00 -10 -5 -4 21.40 5.20 -10 -5 -4 19.80 2.60 -10 -5 -4 20.10 3.70 -10 -5 4 18.80 3.70 -10 -5 4 14.10 5.00 10 5 4 25.20 3.30 -10 -5 4 16.70 3.10 -10 -6 -4 644.14 36.40 -10 -6 -4 669.63 33.90 -10 -6 4 650.03 33.80 -10 -6 4 686.93 33.80 -10 -6 4 600.74 36.20 10 6 4 617.04 33.20 -10 -7 -4 19.10 5.80 -10 -7 -4 16.60 3.40 -10 -7 4 21.70 3.70 -10 -7 4 16.80 3.40 10 7 4 18.70 3.30 -10 -7 4 21.70 6.00 -10 -8 -4 146.29 9.80 -10 -8 -4 127.09 12.50 10 8 4 135.99 9.00 -10 -8 4 129.29 9.20 -10 -8 4 132.79 9.50 -10 -8 4 135.39 12.70 -10 -9 -4 93.79 11.30 -10 -9 -4 99.69 8.00 -10 -9 4 99.59 7.90 -10 -9 4 82.79 10.70 10 9 4 83.19 7.10 -10 -9 4 87.09 7.60 -10 -10 -4 87.39 11.30 -10 -10 -4 105.99 8.70 -10 -10 4 109.69 8.20 -10 -10 4 106.79 8.60 -10 -10 4 94.09 11.70 10 10 4 103.39 7.90 -10 -11 -4 2.10 5.60 -10 -11 -4 1.50 3.20 -10 -11 -4 2.00 3.00 10 11 4 4.00 2.90 -10 -11 4 4.20 3.50 -10 -11 4 1.70 6.00 -10 -12 -4 110.69 8.70 -10 -12 -4 103.19 9.00 -10 -12 -4 71.89 11.30 -10 -12 4 105.49 9.20 -10 -13 -4 26.90 4.90 -10 -13 -4 23.00 8.50 -10 -13 4 26.20 5.60 10 -12 -5 19.80 6.80 10 -12 -5 26.00 5.40 10 -12 5 16.90 4.60 10 -12 5 21.10 5.30 10 -11 -5 5.80 3.90 -10 11 -5 -1.30 5.80 10 -11 -5 10.10 5.70 10 -11 5 3.50 3.50 -10 11 5 5.90 8.00 10 -11 5 8.10 3.90 10 -10 -5 18.10 6.20 -10 10 -5 7.30 6.30 10 -10 -5 16.40 4.10 -10 10 5 5.20 7.10 10 -10 5 18.50 4.30 10 -10 5 15.30 4.40 10 -9 -5 3.00 4.80 10 -9 -5 -0.30 3.10 -10 9 -5 5.30 5.40 -10 9 5 -4.10 6.00 10 -9 5 0.00 2.60 10 -9 5 1.40 2.90 10 -9 5 3.50 3.20 10 -8 -5 1.50 2.00 10 -8 -5 -1.70 2.70 10 -8 -5 1.40 4.00 -10 8 -5 0.00 1.70 -10 8 -5 3.00 4.70 10 -8 5 -2.00 2.30 10 -8 5 -2.30 3.60 10 -8 5 3.10 3.00 10 -8 5 1.30 2.40 -10 8 5 0.20 5.90 -10 7 -5 9.80 5.30 -10 7 -5 12.60 2.60 10 -7 -5 20.00 5.50 10 -7 -5 10.90 2.90 10 -7 -5 13.00 3.30 -10 7 5 8.00 5.80 10 -7 5 20.80 5.20 10 -7 5 2.60 2.90 10 -7 5 16.00 3.10 10 -7 5 11.50 3.50 10 -6 -5 37.20 6.30 10 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3.90 -10 -8 -5 -1.40 2.80 -10 -8 5 -1.10 2.20 -10 -8 5 -5.40 3.80 -10 -8 5 -0.70 2.50 10 8 5 -0.70 2.40 -10 -9 -5 -1.10 2.90 -10 -9 -5 0.40 5.00 -10 -9 5 3.40 4.80 -10 -9 5 1.20 2.80 -10 -9 5 3.70 2.90 10 9 5 0.20 2.70 -10 -10 -5 14.10 4.00 -10 -10 -5 14.60 6.10 -10 -10 5 19.10 4.30 -10 -10 5 19.10 6.80 10 10 5 23.60 4.10 -10 -11 -5 3.90 5.80 -10 -11 -5 7.90 4.00 -10 -11 5 8.30 3.80 10 11 5 8.50 3.40 -10 -12 -5 22.30 7.10 -10 -12 -5 19.40 4.70 -10 -12 5 29.20 5.20 10 -12 -6 111.79 12.80 10 -12 -6 87.89 9.40 10 -12 6 100.59 9.70 10 -12 6 112.49 10.00 10 -11 -6 -0.90 3.10 10 -11 -6 -0.50 4.70 -10 11 -6 1.60 6.30 10 -11 6 -2.30 3.40 10 -11 6 -1.90 3.20 10 -10 -6 127.69 12.70 10 -10 -6 128.19 9.60 -10 10 -6 69.29 11.50 10 -10 6 119.09 9.50 -10 10 6 72.69 12.60 10 -10 6 118.59 9.00 -10 9 -6 2.10 4.90 10 -9 -6 1.00 2.90 10 -9 -6 2.40 4.70 10 -9 6 1.80 2.80 10 -9 6 -0.30 2.70 -10 9 6 -3.10 6.30 10 -8 -6 93.09 6.60 10 -8 -6 103.59 7.90 -10 8 -6 70.39 10.20 10 -8 -6 93.29 10.70 10 -8 6 88.79 7.70 10 -8 6 85.09 8.20 -10 8 6 75.69 11.40 -10 7 -6 166.98 9.40 10 -7 -6 156.78 10.60 -10 7 -6 126.29 13.10 10 -7 -6 154.08 9.60 10 -7 -6 154.88 13.00 10 -7 6 144.59 10.00 -10 7 6 137.19 15.10 10 -7 6 159.88 12.30 10 -7 6 137.09 10.40 10 -6 -6 245.48 14.80 10 -6 -6 260.07 17.40 -10 6 -6 210.88 17.20 -10 6 -6 256.37 14.00 -10 6 6 217.28 18.20 10 -6 6 261.77 16.60 10 -6 6 254.97 14.60 10 -6 6 257.17 15.30 -10 5 -6 71.09 5.70 10 -5 -6 63.69 6.10 -10 5 -6 75.69 9.10 -10 5 6 70.09 9.60 10 -5 6 64.99 5.90 10 -5 6 66.89 6.90 -10 4 -6 599.24 28.90 10 -4 -6 591.34 29.20 -10 4 -6 487.65 31.20 10 -4 6 578.84 29.80 -10 4 6 462.75 31.70 10 -4 6 569.64 28.80 10 -3 -6 59.59 5.50 -10 3 -6 47.80 4.80 -10 3 -6 43.60 6.90 10 -3 6 57.09 4.90 -10 3 6 50.09 7.90 10 -3 6 52.29 6.00 -10 2 -6 452.65 28.90 -10 2 -6 539.85 27.00 10 -2 -6 549.95 27.10 10 -2 6 523.75 26.40 10 -2 6 514.85 27.50 -10 2 6 467.95 29.50 -10 1 -6 74.19 8.00 10 -1 -6 73.49 6.00 -10 1 -6 75.19 6.40 10 -1 6 77.09 5.40 -10 1 6 68.89 8.40 10 -1 6 77.39 7.10 -10 1 6 73.99 5.20 10 0 -6 245.08 13.60 -10 0 -6 216.08 15.50 -10 0 -6 229.48 13.50 -10 0 6 246.68 13.40 10 0 6 237.98 12.60 -10 0 6 235.98 12.10 -10 0 6 223.08 16.10 10 0 6 220.78 14.00 -10 -1 -6 73.79 5.90 10 1 -6 63.39 5.80 -10 -1 -6 67.79 7.80 10 1 6 73.29 6.80 10 1 6 73.99 4.70 -10 -1 6 70.09 5.60 -10 -1 6 69.79 8.20 10 2 -6 552.34 27.70 -10 -2 -6 489.75 29.70 -10 -2 -6 546.45 27.90 10 2 6 546.15 27.90 -10 -2 6 489.45 29.90 10 2 6 514.25 28.10 -10 -2 6 523.05 27.60 10 2 6 530.85 26.20 10 3 -6 48.10 4.80 -10 -3 -6 44.80 5.00 -10 -3 -6 49.50 7.10 -10 -3 6 56.49 5.20 10 3 6 58.39 5.60 10 3 6 46.40 5.60 -10 -3 6 54.59 7.50 -10 -3 6 70.39 6.30 -10 -4 -6 585.64 30.70 -10 -4 -6 567.84 32.80 10 4 -6 615.74 30.40 10 4 6 580.94 30.70 -10 -4 6 604.64 30.70 10 4 6 556.44 30.30 -10 -4 6 521.85 32.40 -10 -4 6 586.84 30.40 -10 -5 -6 74.59 6.70 -10 -5 -6 66.79 8.50 -10 -5 6 62.09 6.00 -10 -5 6 69.49 6.40 -10 -5 6 62.79 8.60 10 5 6 72.39 6.30 -10 -6 -6 212.08 16.70 -10 -6 -6 270.97 14.90 -10 -6 6 225.78 16.90 -10 -6 6 263.87 14.70 -10 -6 6 244.88 14.70 10 6 6 253.37 14.50 -10 -7 -6 158.38 10.80 -10 -7 -6 156.68 13.30 -10 -7 6 141.49 13.00 10 7 6 155.78 10.40 -10 -7 6 162.38 10.50 -10 -7 6 151.68 10.60 -10 -8 -6 94.49 10.90 -10 -8 -6 97.49 7.80 -10 -8 6 89.59 7.40 10 8 6 94.69 7.60 -10 -8 6 90.89 10.80 -10 -8 6 100.09 8.50 -10 -9 -6 1.60 4.90 -10 -9 -6 -5.50 2.70 -10 -9 6 -1.10 2.70 10 9 6 0.50 2.80 -10 -9 6 -1.00 2.70 -10 -10 -6 108.79 12.60 -10 -10 -6 117.29 9.20 10 10 6 125.99 9.10 -10 -10 6 122.09 9.80 -10 -11 -6 2.40 3.20 -10 -11 -6 2.90 5.70 -10 -11 6 -1.60 3.10 10 11 6 1.90 3.20 -10 -12 -6 108.79 9.50 -10 -12 -6 72.89 11.80 10 12 6 116.79 9.70 -10 -12 6 115.49 10.40 10 -12 -7 3.90 6.00 10 -12 -7 -0.80 4.00 10 -12 7 -0.50 4.00 10 -12 7 7.70 4.20 10 -11 -7 -5.60 3.00 10 -11 -7 -5.10 4.70 10 -11 7 1.80 3.30 10 -11 7 -1.80 3.50 10 -10 -7 5.00 5.10 -10 10 -7 4.10 5.80 10 -10 -7 9.90 4.10 -10 10 7 5.10 7.80 10 -10 7 10.40 4.20 10 -10 7 5.00 3.20 10 -9 -7 -0.50 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6.40 2.60 -10 0 -9 3.40 3.20 10 0 9 -4.90 2.70 -10 0 9 3.50 4.00 10 0 9 1.90 1.90 -10 0 9 -0.30 2.20 -10 -1 -9 7.10 2.90 -10 -1 -9 3.20 3.30 10 1 -9 4.40 2.80 -10 -1 9 2.70 3.90 10 1 9 8.10 3.40 10 1 9 7.70 2.70 -10 -1 9 2.90 2.50 10 1 9 0.90 2.70 -10 -2 -9 1.30 3.10 -10 -2 -9 -0.30 2.20 10 2 -9 -0.50 2.20 10 2 9 4.10 3.10 -10 -2 9 5.20 2.60 -10 -2 9 0.20 3.60 10 2 9 -4.60 2.60 10 3 -9 0.30 2.70 -10 -3 -9 0.60 3.20 -10 -3 -9 4.60 2.90 10 3 9 4.40 3.10 -10 -3 9 6.70 2.90 10 3 9 2.90 3.00 -10 -4 -9 0.30 3.40 10 4 -9 1.10 2.70 -10 -4 -9 0.30 2.50 10 4 9 2.40 3.10 10 4 9 1.10 2.70 -10 -4 9 4.30 2.90 -10 -5 -9 0.40 3.60 10 5 -9 -0.10 2.40 -10 -5 -9 -0.40 2.80 -10 -5 9 -2.80 2.40 10 5 9 -0.60 2.50 10 5 9 1.10 2.90 -10 -6 -9 37.30 5.50 -10 -6 -9 40.20 7.20 -10 -6 9 39.70 5.30 10 6 9 44.10 5.70 10 6 9 49.70 5.50 -10 -7 -9 1.80 4.30 -10 -7 -9 3.30 3.20 -10 -7 9 4.50 3.00 10 7 9 10.50 3.50 10 7 9 0.00 3.00 -10 -8 -9 6.00 3.70 -10 -8 -9 6.50 4.90 10 8 9 8.30 3.70 -10 -8 9 8.60 3.80 -10 -9 -9 2.10 4.60 -10 -9 -9 -4.30 2.90 10 9 9 4.80 3.40 -10 -9 9 3.70 3.50 -10 -10 -9 0.80 5.20 -10 -10 -9 6.50 3.90 10 10 9 2.30 3.70 -10 -10 9 2.80 3.80 -10 -11 -9 5.90 6.10 -10 -11 -9 -1.60 3.50 -10 -11 9 3.30 4.00 10 11 9 -1.50 3.40 10 -10 -10 147.89 14.70 10 -10 -10 150.08 12.20 10 -10 10 193.88 13.30 -10 10 10 172.88 13.30 10 -10 10 147.99 11.70 -10 9 -10 2.60 5.40 10 -9 -10 0.30 4.60 10 -9 -10 9.30 3.90 -10 9 10 10.90 4.90 10 -9 10 -2.20 3.20 10 -9 10 9.20 4.10 10 -8 -10 153.78 13.70 -10 8 -10 123.29 13.60 10 -8 -10 160.28 11.40 10 -8 10 161.58 11.30 10 -8 10 164.58 12.10 -10 8 10 154.18 11.80 10 -7 -10 18.30 4.50 -10 7 -10 14.40 5.60 10 -7 -10 20.10 5.70 -10 7 10 20.30 4.80 10 -7 10 8.60 3.80 -10 6 -10 44.80 8.00 10 -6 -10 73.29 7.10 10 -6 -10 63.49 8.40 -10 6 -10 70.69 5.70 10 -6 10 75.99 7.00 10 -6 10 60.69 7.20 -10 6 10 70.29 7.10 10 -5 -10 12.70 4.80 10 -5 -10 11.50 3.80 -10 5 -10 14.40 3.00 -10 5 -10 13.30 5.10 10 -5 10 13.50 3.60 10 -5 10 11.10 3.90 -10 5 10 18.70 4.10 10 -4 -10 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6.10 11 -6 9 6.00 3.30 11 -6 9 8.10 4.10 11 -5 -9 148.69 12.90 -11 5 -9 150.38 13.60 11 -5 -9 160.28 10.80 -11 5 -9 165.08 10.10 11 -5 9 152.38 10.30 -11 5 9 141.89 10.30 11 -5 9 158.28 11.50 -11 5 9 128.89 14.40 -11 4 -9 48.30 5.00 -11 4 -9 30.80 6.50 11 -4 -9 32.20 4.80 -11 4 9 47.60 5.20 11 -4 9 41.60 4.90 -11 4 9 37.70 8.00 11 -4 9 36.90 5.50 -11 3 -9 176.78 14.30 11 -3 -9 187.18 12.10 -11 3 -9 187.08 11.80 11 -3 9 206.58 11.50 -11 3 9 196.38 15.90 11 -3 9 159.98 12.60 -11 3 9 191.68 11.50 -11 2 -9 15.50 5.00 11 -2 -9 9.80 3.50 -11 2 -9 9.70 3.00 11 -2 9 14.50 3.90 11 -2 9 12.50 2.90 -11 2 9 15.10 5.50 11 -1 -9 210.18 13.70 -11 1 -9 210.48 15.70 -11 1 -9 221.78 13.50 11 -1 9 228.58 12.50 11 -1 9 222.98 14.10 -11 1 9 228.28 16.90 -11 0 -9 4.60 2.80 -11 0 -9 4.20 3.50 11 0 -9 7.70 2.90 11 0 9 8.90 3.50 11 0 9 5.80 3.50 -11 0 9 2.00 4.50 11 1 -9 223.78 13.20 -11 -1 -9 215.08 15.40 -11 -1 -9 201.98 13.00 -11 -1 9 224.98 13.30 11 1 9 210.68 13.70 -11 -1 9 195.88 16.50 -11 -2 -9 15.60 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45.30 6.00 11 6 11 62.29 7.20 -11 -6 11 56.89 7.00 11 6 11 59.79 7.80 -11 -7 -11 43.70 5.90 -11 -7 -11 31.30 6.80 11 7 -11 32.70 5.40 -11 -7 11 34.30 5.50 11 7 11 25.80 5.40 -11 -8 -11 16.90 6.20 -11 -8 -11 15.00 4.40 11 8 -11 11.00 4.50 11 8 11 14.80 4.70 -11 -8 11 19.80 4.70 -11 -9 -11 52.69 7.10 -11 -9 -11 63.49 10.10 11 9 11 74.99 8.20 -11 -9 11 61.49 8.00 11 -8 -12 -3.30 4.10 11 -8 -12 0.00 3.40 -11 8 -12 -2.10 5.10 11 -8 12 -1.00 3.60 11 -8 12 -0.10 4.00 -11 8 12 1.20 4.50 11 -7 -12 13.50 5.50 -11 7 -12 15.40 6.00 11 -7 -12 9.80 4.20 11 -7 12 12.30 4.50 11 -7 12 16.90 5.40 11 -6 -12 7.10 3.80 11 -6 -12 8.30 4.80 -11 6 -12 6.40 5.10 11 -6 12 10.60 4.80 11 -6 12 12.10 4.10 -11 5 -12 2.70 4.30 11 -5 -12 -1.40 3.00 -11 5 -12 1.90 2.50 11 -5 -12 2.20 3.80 11 -5 12 -0.10 3.20 11 -5 12 -3.10 3.80 11 -4 -12 13.30 3.90 11 -4 -12 6.00 4.20 -11 4 -12 11.90 4.90 -11 4 -12 7.10 3.00 11 -4 12 4.80 3.90 11 -4 12 8.00 3.50 11 -3 -12 36.60 6.40 -11 3 -12 42.90 5.10 11 -3 -12 36.50 5.60 -11 3 -12 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5.60 -11 -7 -12 18.70 5.00 11 7 -12 12.20 4.40 11 7 12 22.00 5.40 -11 -8 -12 -3.30 4.50 11 8 -12 -2.00 3.60 -11 -8 -12 -1.30 3.80 11 8 12 3.50 4.10 -11 -8 12 5.90 4.10 -11 7 -13 15.50 6.20 11 -7 -13 18.40 5.80 11 -7 -13 19.10 5.40 11 -7 13 26.10 6.10 11 -7 13 23.30 5.00 11 -6 -13 17.20 4.80 -11 6 -13 5.50 5.10 11 -6 -13 11.00 5.10 11 -6 13 9.00 4.20 11 -6 13 9.60 5.00 11 -5 -13 102.59 10.80 -11 5 -13 93.09 10.80 11 -5 -13 112.59 10.00 11 -5 13 101.69 8.80 11 -5 13 99.09 9.90 11 -4 -13 5.30 3.80 -11 4 -13 -0.60 3.80 -11 4 -13 2.50 2.80 11 -4 -13 2.20 3.80 11 -4 13 8.90 4.60 11 -4 13 0.90 3.20 -11 3 -13 61.59 6.40 11 -3 -13 65.59 7.40 -11 3 -13 69.79 8.70 11 -3 -13 56.69 7.90 11 -3 13 54.49 7.50 -11 2 -13 6.50 3.20 11 -2 -13 14.70 4.40 -11 2 -13 13.00 4.70 11 -2 13 6.30 4.50 -11 1 -13 102.79 10.20 -11 1 -13 100.49 8.80 11 -1 -13 99.59 9.30 11 -1 13 94.99 9.30 11 0 -13 10.60 3.50 -11 0 -13 9.60 4.20 -11 0 -13 11.30 3.40 11 0 13 14.10 4.70 -11 -1 -13 101.69 9.00 11 1 -13 108.79 8.80 -11 -1 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6.80 4.10 12 -12 0 1.20 3.70 12 -11 0 48.80 6.30 12 -11 0 66.59 7.10 -12 11 0 25.30 9.40 12 -11 0 57.19 6.90 12 -11 0 52.99 9.40 12 -10 0 33.60 5.00 -12 10 0 21.10 8.30 12 -10 0 39.30 8.10 12 -10 0 36.20 5.40 12 -9 0 385.86 20.80 12 -9 0 396.56 24.60 -12 9 0 263.37 24.90 12 -9 0 372.26 20.50 -12 8 0 33.60 8.70 12 -8 0 62.69 9.00 12 -8 0 61.89 6.20 12 -8 0 52.09 5.70 12 -7 0 219.28 13.50 12 -7 0 226.78 14.10 12 -7 0 236.18 17.10 12 -6 0 -0.10 2.30 12 -6 0 1.70 2.30 -12 6 0 1.60 5.00 -12 5 0 107.99 7.80 12 -5 0 93.49 7.70 -12 5 0 62.99 9.90 12 -5 0 121.59 7.30 -12 4 0 68.59 10.10 -12 4 0 116.89 8.10 12 -4 0 114.29 8.20 12 -4 0 115.59 7.30 -12 3 0 75.59 9.80 12 -3 0 72.99 5.40 -12 3 0 72.79 6.60 -12 2 0 484.25 30.80 12 -2 0 534.65 26.80 -12 2 0 538.45 28.00 12 -1 0 880.41 43.20 -12 1 0 784.22 46.90 -12 1 0 912.01 44.60 -12 0 0 10.70 5.20 12 0 0 0.40 1.70 -12 0 0 -0.10 2.10 -12 -1 0 864.21 45.20 12 1 0 900.41 43.90 -12 -1 0 909.81 43.50 -12 -1 0 812.22 47.80 -12 -2 0 599.74 29.50 -12 -2 0 567.24 27.70 12 2 0 547.95 27.80 -12 -2 0 465.65 31.20 -12 -3 0 83.59 9.70 12 3 0 84.99 5.70 -12 -3 0 92.79 7.20 -12 -3 0 78.29 5.50 -12 -4 0 80.59 9.90 12 4 0 103.09 6.60 -12 -4 0 110.39 6.70 -12 -4 0 106.99 8.10 -12 -5 0 117.69 9.10 -12 -5 0 104.39 12.00 12 5 0 122.39 7.40 -12 -5 0 119.29 7.70 -12 -6 0 0.00 1.90 -12 -6 0 3.30 4.30 -12 -6 0 0.20 2.90 -12 -7 0 231.78 13.10 -12 -7 0 194.78 17.00 -12 -7 0 235.58 14.30 -12 -8 0 73.09 7.20 -12 -8 0 56.09 9.10 -12 -8 0 66.29 6.20 -12 -9 0 388.46 22.00 -12 -9 0 401.96 21.50 -12 -9 0 349.17 25.60 -12 -10 0 48.00 6.20 -12 -10 0 47.90 5.70 -12 -10 0 25.50 8.10 -12 -11 0 39.40 9.50 -12 -11 0 50.29 6.20 -12 -11 0 60.89 7.10 -12 -12 0 9.10 6.90 -12 -12 0 6.60 3.50 12 -12 -1 16.00 7.00 12 -12 -1 7.20 4.10 12 -12 -1 -0.80 3.90 -12 12 -1 2.20 7.90 -12 12 1 3.10 8.10 12 -12 1 3.80 5.90 12 -12 1 3.50 3.40 12 -12 1 4.00 3.90 12 -11 -1 -3.10 5.60 12 -11 -1 -1.90 3.40 -12 11 -1 -6.20 6.50 12 -11 1 16.30 6.70 -12 11 1 4.90 7.70 12 -11 1 0.00 3.10 12 -11 1 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9 8 33.80 10.50 -12 8 -8 32.20 8.30 12 -8 -8 46.30 6.40 12 -8 -8 47.20 8.60 12 -8 8 44.50 6.00 12 -8 8 47.40 6.70 -12 8 8 30.20 9.60 12 -7 -8 137.89 10.30 -12 7 -8 113.89 13.70 12 -7 -8 144.19 13.20 -12 7 8 100.19 14.20 12 -7 8 127.79 9.80 12 -7 8 133.19 10.50 12 -6 -8 12.50 3.70 12 -6 -8 9.00 5.30 -12 6 -8 13.30 3.20 -12 6 -8 8.50 5.60 12 -6 8 12.00 4.10 -12 6 8 13.40 7.40 12 -6 8 13.00 3.80 -12 6 8 22.10 4.50 12 -5 -8 225.38 13.40 -12 5 -8 219.58 12.60 -12 5 -8 147.79 15.40 -12 5 8 211.38 12.80 -12 5 8 152.08 16.80 12 -5 8 221.28 13.80 12 -5 8 210.48 12.70 12 -4 -8 113.39 9.00 -12 4 -8 113.89 11.80 -12 4 -8 127.99 8.60 -12 4 8 100.79 12.60 12 -4 8 112.99 9.40 12 -4 8 110.39 8.30 -12 4 8 119.69 9.00 12 -3 -8 158.78 10.30 -12 3 -8 144.19 9.80 -12 3 -8 111.29 11.90 12 -3 8 143.49 10.50 12 -3 8 168.08 9.50 -12 3 8 113.39 13.30 -12 2 -8 49.20 7.70 -12 2 -8 65.69 6.40 12 -2 -8 47.00 5.80 12 -2 8 57.19 6.90 12 -2 8 67.69 5.50 -12 2 8 68.39 9.90 -12 1 -8 123.29 12.20 -12 1 -8 157.78 10.30 12 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6 9 13.20 4.20 -12 -6 9 10.20 3.60 12 6 9 9.40 3.60 -12 -7 -9 35.40 7.50 -12 -7 -9 35.20 5.80 12 7 -9 36.10 5.30 12 7 9 30.90 5.20 12 7 9 33.40 5.60 -12 -7 9 38.40 5.70 -12 -8 -9 -0.70 3.80 -12 -8 -9 0.80 5.10 12 8 9 3.50 3.50 -12 -8 9 11.30 4.30 -12 -9 -9 -1.90 5.40 -12 -9 -9 9.20 4.50 -12 -9 9 5.70 3.60 12 9 9 9.30 4.00 12 -9 -10 79.89 11.20 12 -9 -10 92.59 9.10 -12 9 10 81.49 9.40 12 -9 10 100.49 9.30 12 -9 10 91.59 9.70 12 -8 -10 4.20 4.00 12 -8 -10 5.20 5.40 -12 8 -10 4.20 5.80 -12 8 10 9.50 4.80 12 -8 10 3.10 4.00 12 -8 10 2.80 4.00 -12 7 -10 51.19 9.40 12 -7 -10 65.79 9.40 12 -7 -10 83.99 8.30 -12 7 10 65.39 10.00 12 -7 10 66.09 7.00 12 -7 10 66.29 8.00 -12 6 -10 42.10 8.50 12 -6 -10 47.10 6.70 12 -6 -10 63.79 9.10 12 -6 10 61.29 7.60 12 -6 10 58.39 6.50 12 -5 -10 23.70 6.20 12 -5 -10 20.70 4.60 -12 5 -10 21.40 6.40 -12 5 -10 31.80 4.40 12 -5 10 29.30 5.40 12 -5 10 25.30 4.50 -12 4 -10 11.30 5.30 -12 4 -10 16.90 3.50 12 -4 -10 12.40 3.80 12 -4 10 15.10 4.50 12 -4 10 21.00 4.00 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9.10 -15 5 -9 52.59 6.10 15 -5 -9 40.30 6.30 -15 5 -9 25.70 8.30 15 -5 -9 29.20 7.60 15 -5 9 35.70 6.80 -15 4 -9 56.09 10.00 15 -4 -9 67.59 7.40 -15 4 -9 86.29 7.90 15 -4 9 54.49 7.80 -15 3 -9 24.90 7.70 -15 3 -9 22.50 4.60 15 -3 -9 23.10 4.70 15 -3 9 19.70 5.50 -15 2 -9 44.30 6.20 15 -2 -9 50.29 6.30 -15 2 -9 43.10 8.60 15 -2 9 66.49 7.90 -15 1 -9 7.00 3.80 15 -1 -9 12.70 4.30 -15 1 -9 14.70 6.40 15 -1 9 13.30 4.70 15 0 -9 64.09 6.90 -15 0 -9 51.59 9.10 -15 0 -9 49.00 6.50 15 0 9 47.40 7.20 15 1 -9 16.90 4.50 -15 -1 -9 16.40 4.30 -15 -1 -9 11.60 5.70 15 1 9 12.00 4.90 -15 -2 -9 52.59 9.30 15 2 -9 50.29 6.30 -15 -2 -9 65.39 7.50 -15 -2 9 67.49 6.70 15 2 9 48.00 6.80 15 3 -9 22.50 4.90 -15 -3 -9 24.30 7.30 -15 -3 -9 34.00 5.90 -15 -3 9 30.20 4.90 15 3 9 27.00 5.90 -15 -4 -9 61.79 10.20 15 4 -9 72.09 7.60 -15 -4 -9 87.49 8.90 15 4 9 73.99 8.50 -15 -4 9 90.19 8.30 15 5 -9 35.90 5.80 -15 -5 -9 48.80 7.00 -15 -5 -9 25.90 7.90 -15 -5 9 49.10 6.20 15 5 9 34.40 6.10 -15 -6 -9 95.29 10.10 15 6 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-5 10 8.20 4.00 15 5 10 1.30 4.20 -15 4 -11 63.69 10.90 -15 3 -11 8.00 3.80 -15 3 -11 1.60 5.30 15 -3 -11 2.90 4.00 15 -3 11 2.20 4.20 -15 2 -11 97.99 9.10 -15 2 -11 70.79 11.10 15 -2 -11 113.29 9.80 15 -2 11 102.19 10.30 15 -1 -11 3.50 4.00 -15 1 -11 7.10 3.80 -15 1 -11 4.70 5.00 15 -1 11 -4.50 4.40 -15 0 -11 37.40 6.10 -15 0 -11 32.50 7.70 15 0 -11 24.20 5.00 15 0 11 38.20 6.70 15 1 -11 21.70 5.00 -15 -1 -11 3.40 3.90 -15 -1 -11 2.40 5.00 15 1 11 -4.70 3.90 15 2 -11 97.09 9.10 -15 -2 -11 66.79 10.50 -15 -2 -11 109.69 9.90 15 2 11 106.29 10.20 -15 -3 -11 1.00 3.80 15 3 -11 -0.50 3.40 -15 -3 -11 1.70 5.10 -15 -3 11 1.80 3.50 15 3 11 -3.40 3.50 -15 -4 -11 55.19 10.20 -15 1 -12 4.10 5.30 -15 0 -12 -0.20 4.80 -15 -1 -12 -1.90 4.80 16 -8 0 77.09 8.30 16 -8 0 63.39 10.70 -16 8 0 55.69 12.00 16 -7 0 6.20 3.90 16 -7 0 3.90 6.00 -16 7 0 -1.30 6.80 -16 6 0 42.20 10.50 16 -6 0 89.99 8.60 -16 5 0 -0.40 3.10 16 -5 0 3.30 3.60 -16 5 0 2.00 6.50 16 -4 0 273.97 16.70 -16 4 0 196.48 20.30 -16 4 0 296.77 16.80 -16 3 0 2.40 6.00 -16 3 0 -1.30 3.20 16 -3 0 4.70 3.80 -16 2 0 226.18 18.90 -16 1 0 91.79 12.40 -16 0 0 1.00 3.40 -16 0 0 -0.90 5.70 -16 -1 0 102.89 12.60 -16 -2 0 242.78 21.20 -16 -2 0 330.27 18.20 -16 -3 0 -4.90 3.30 -16 -3 0 -2.30 5.90 -16 -4 0 219.28 20.00 -16 -4 0 310.37 17.30 -16 -5 0 -0.50 3.50 -16 -5 0 0.70 6.00 -16 -6 0 64.29 7.30 -16 -6 0 43.70 9.30 -16 -7 0 -2.10 6.40 -16 -7 0 4.00 4.20 -16 -8 0 55.29 7.40 -16 -8 0 49.00 10.20 16 -8 -1 45.10 9.30 -16 8 -1 15.70 9.10 16 -8 -1 44.40 6.50 16 -8 1 37.10 8.70 16 -8 1 59.69 7.30 -16 8 1 25.40 9.80 16 -7 -1 34.90 8.30 16 -7 -1 29.70 5.50 -16 7 -1 24.80 9.00 -16 7 1 12.80 8.00 16 -7 1 40.10 6.20 16 -7 1 30.70 8.10 16 -6 -1 -3.00 3.10 -16 6 -1 -4.50 3.00 -16 6 -1 1.80 7.30 -16 6 1 3.60 6.90 16 -6 1 -5.40 3.00 -16 5 -1 5.10 6.70 -16 5 -1 10.80 3.90 16 -5 -1 8.40 4.10 -16 5 1 2.10 6.60 16 -5 1 6.50 3.70 -16 4 -1 -3.10 2.80 -16 4 -1 7.70 6.40 16 -4 -1 -1.10 3.20 -16 4 1 8.90 7.30 16 -4 1 4.00 3.50 -16 4 1 -1.40 3.20 -16 3 -1 19.60 4.60 -16 3 -1 17.30 7.30 -16 3 1 24.30 8.00 -16 3 1 19.30 4.80 16 -3 1 26.00 5.40 -16 2 -1 16.30 6.70 -16 2 -1 23.10 4.50 16 -2 1 20.60 4.90 -16 2 1 24.50 7.60 -16 2 1 30.40 5.00 -16 1 -1 -1.20 2.80 -16 1 -1 2.30 5.80 -16 1 1 5.20 5.90 -16 1 1 -1.70 2.80 -16 0 -1 3.30 5.80 -16 0 -1 2.50 3.40 -16 0 1 5.00 5.60 -16 0 1 -1.20 3.40 -16 -1 -1 0.90 3.30 -16 -1 -1 1.10 5.10 -16 -1 1 4.20 3.80 -16 -1 1 6.00 6.20 -16 -2 -1 28.80 8.20 -16 -2 -1 23.30 4.80 -16 -2 1 25.10 4.90 -16 -2 1 21.40 7.00 -16 -3 -1 17.20 7.40 -16 -3 -1 28.30 5.30 -16 -3 1 25.60 5.00 -16 -3 1 26.10 7.40 -16 -4 -1 2.40 3.50 -16 -4 -1 -3.70 5.40 -16 -4 1 -0.10 5.40 -16 -4 1 -1.30 3.60 -16 -5 -1 12.30 7.20 -16 -5 -1 12.60 4.60 -16 -5 1 4.10 6.20 -16 -5 1 15.10 4.30 -16 -6 -1 -0.30 5.90 -16 -6 -1 -2.20 3.40 -16 -6 1 -3.20 3.70 -16 -6 1 0.60 6.20 -16 -7 -1 38.20 6.50 -16 -7 -1 22.80 8.70 -16 -7 1 26.80 5.40 -16 -7 1 18.40 8.00 -16 -8 -1 44.40 6.80 -16 -8 -1 29.10 8.70 -16 -8 1 43.40 6.60 -16 -8 1 32.60 9.60 16 -8 -2 67.19 7.70 16 -8 -2 92.59 12.40 16 -8 -2 75.19 7.40 -16 8 -2 45.40 11.90 -16 8 2 37.70 11.60 16 -8 2 62.79 7.40 16 -8 2 85.79 8.70 16 -7 -2 1.30 3.40 -16 7 -2 1.90 6.90 16 -7 -2 3.90 3.40 16 -7 -2 -2.90 5.50 16 -7 2 0.70 3.80 16 -7 2 1.60 5.50 -16 7 2 4.80 7.20 -16 6 -2 100.29 8.80 16 -6 -2 104.99 9.50 16 -6 -2 100.19 8.10 -16 6 2 56.49 11.50 16 -6 2 86.69 8.90 16 -5 -2 -2.30 3.10 -16 5 -2 1.40 6.60 16 -5 -2 -2.40 2.90 -16 5 -2 2.20 3.00 16 -5 2 0.30 3.00 -16 5 2 2.10 6.10 -16 4 -2 53.59 6.50 16 -4 -2 49.00 6.80 16 -4 -2 65.89 7.80 -16 4 -2 38.90 9.50 16 -4 2 48.50 6.70 -16 4 2 35.10 8.90 -16 3 -2 6.10 3.20 -16 3 -2 1.30 5.70 -16 3 2 13.80 4.50 16 -3 2 7.30 3.70 -16 3 2 6.80 6.70 -16 2 -2 62.69 10.80 -16 2 -2 94.29 8.80 -16 2 2 115.39 8.80 -16 2 2 74.79 12.00 16 -2 2 92.79 8.90 -16 1 -2 34.70 5.30 -16 1 -2 10.60 6.40 -16 1 2 17.90 7.50 16 -1 2 22.20 4.90 -16 1 2 37.40 5.80 -16 0 -2 280.57 15.50 -16 0 -2 180.08 17.90 -16 0 2 268.67 15.40 -16 0 2 181.48 18.30 -16 -1 -2 12.20 6.50 -16 -1 -2 30.80 5.30 -16 -1 2 15.60 6.70 -16 -1 2 27.60 5.10 -16 -2 -2 74.49 11.60 -16 -2 -2 100.69 9.00 -16 -2 2 123.09 10.10 -16 -2 2 63.79 11.10 -16 -3 -2 11.90 6.90 -16 -3 -2 7.40 3.80 -16 -3 2 4.50 6.30 -16 -3 2 6.40 4.20 -16 -4 -2 35.40 8.80 -16 -4 -2 62.99 7.00 -16 -4 2 55.39 7.00 -16 -4 2 34.40 8.40 -16 -5 -2 0.40 3.40 -16 -5 -2 5.00 6.40 -16 -5 2 2.50 3.90 -16 -5 2 -0.10 5.70 -16 -6 -2 52.99 10.60 -16 -6 -2 95.89 9.30 -16 -6 2 67.69 11.10 -16 -6 2 96.59 9.10 -16 -7 -2 3.10 3.90 -16 -7 -2 -2.10 6.40 -16 -7 2 -0.50 4.00 -16 -7 2 2.70 6.40 -16 -8 -2 82.79 8.50 -16 -8 -2 47.20 10.00 -16 -8 2 65.99 8.00 -16 -8 2 52.59 10.90 16 -8 -3 2.20 5.90 16 -8 -3 -3.00 3.20 -16 8 -3 2.80 7.60 -16 8 3 -8.50 6.60 16 -8 3 0.10 3.60 -16 7 -3 6.20 3.60 16 -7 -3 8.20 3.70 -16 7 -3 -1.10 6.70 16 -7 -3 2.10 5.80 16 -7 -3 -0.10 3.20 -16 7 3 6.60 7.90 16 -7 3 5.10 4.20 16 -7 3 10.10 4.10 16 -6 -3 -5.00 3.00 -16 6 -3 2.30 6.50 16 -6 -3 -3.00 3.30 -16 6 -3 -0.60 3.10 16 -6 3 4.60 3.20 16 -6 3 1.90 3.60 -16 6 3 0.00 7.40 -16 5 -3 7.80 6.80 -16 5 -3 1.00 3.20 16 -5 -3 -2.60 3.20 16 -5 -3 -3.40 2.80 -16 5 3 -6.40 6.70 16 -5 3 -3.30 2.90 -16 4 -3 2.30 5.90 16 -4 -3 -2.60 2.80 -16 4 -3 0.80 3.10 16 -4 3 1.00 3.80 -16 4 3 7.30 6.90 -16 3 -3 -3.40 5.40 16 -3 -3 -3.00 2.60 -16 3 -3 2.30 3.20 -16 3 3 -6.90 5.60 16 -3 3 -2.40 3.50 16 -2 -3 2.50 2.80 -16 2 -3 1.10 5.20 -16 2 -3 3.40 3.30 -16 2 3 2.70 3.80 -16 2 3 5.80 6.50 16 -2 3 0.70 3.70 -16 1 -3 0.20 3.20 16 -1 -3 0.20 2.60 -16 1 -3 3.30 5.70 -16 1 3 2.40 6.30 16 -1 3 -0.70 3.20 -16 1 3 -1.50 3.40 -16 0 -3 3.30 3.10 -16 0 -3 -0.30 5.50 16 0 3 8.40 4.20 -16 0 3 11.30 6.50 -16 0 3 -1.70 3.50 -16 -1 -3 -1.70 2.90 -16 -1 -3 1.60 5.60 -16 -1 3 -4.10 5.00 -16 -1 3 1.20 3.70 -16 -2 -3 -4.50 4.80 -16 -2 -3 6.70 4.20 -16 -2 3 0.30 3.30 -16 -2 3 1.10 5.90 -16 -3 -3 1.10 5.50 -16 -3 -3 1.70 3.70 -16 -3 3 1.10 6.00 -16 -3 3 -0.30 3.40 -16 -4 -3 6.00 5.80 -16 -4 -3 -2.80 3.70 -16 -4 3 1.70 6.10 -16 -4 3 1.50 3.90 -16 -5 -3 0.70 3.90 -16 -5 -3 -3.30 5.10 -16 -5 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-0.80 4.30 -17 -6 -3 3.60 6.40 -17 -6 3 9.30 7.40 -17 -6 3 3.50 4.40 -17 6 -4 -3.10 6.60 -17 6 -4 0.30 3.30 -17 6 4 1.50 7.90 17 -5 -4 -1.80 4.80 -17 5 -4 -6.70 2.90 17 -5 -4 6.70 4.00 -17 5 -4 6.80 7.20 17 -5 4 6.10 3.50 17 -5 4 4.70 4.20 -17 5 4 -4.90 7.40 -17 4 -4 26.20 8.80 -17 4 -4 26.40 5.30 17 -4 4 32.90 6.10 17 -4 4 22.70 4.60 -17 4 4 29.90 9.10 -17 3 -4 10.10 6.50 -17 3 -4 7.20 3.80 -17 3 4 13.30 7.90 17 -3 4 11.90 4.90 -17 2 -4 4.60 3.40 -17 2 -4 -0.50 5.30 17 -2 4 -1.00 3.50 -17 2 4 2.50 6.30 -17 1 -4 1.20 5.70 -17 1 -4 -1.50 2.90 -17 1 4 -3.00 3.20 -17 1 4 3.60 6.90 17 -1 4 -1.90 3.30 -17 0 -4 3.00 5.70 -17 0 -4 1.60 3.60 -17 0 4 3.60 6.40 -17 0 4 0.60 3.30 17 0 4 5.60 3.90 -17 -1 -4 -1.60 5.60 -17 -1 -4 -2.60 3.50 -17 -1 4 -2.50 3.70 17 1 4 4.20 4.40 -17 -1 4 0.70 6.00 -17 -2 -4 -1.50 5.70 -17 -2 -4 -0.40 3.20 17 2 4 1.40 4.30 -17 -2 4 -0.80 3.50 -17 -2 4 2.90 6.50 -17 -3 -4 8.40 4.20 -17 -3 -4 3.70 6.70 -17 -3 4 14.00 5.00 -17 -3 4 11.60 7.40 -17 -4 -4 36.70 6.30 -17 -4 -4 23.60 7.50 -17 -4 4 15.00 7.60 -17 -4 4 20.40 5.30 -17 -5 -4 1.30 4.40 -17 -5 -4 7.40 6.70 -17 -5 4 1.00 6.50 -17 -5 4 -4.70 3.70 -17 -6 -4 3.80 7.00 -17 -6 4 1.50 4.60 -17 -6 4 -1.40 7.00 -17 5 -5 59.39 11.30 -17 5 -5 74.09 7.90 17 -5 -5 72.59 7.70 17 -5 -5 84.39 8.80 17 -5 5 63.59 8.30 17 -5 5 85.89 7.80 -17 5 5 62.89 13.00 -17 4 -5 7.90 6.90 -17 4 -5 3.40 3.70 17 -4 -5 9.30 4.00 -17 4 5 6.30 7.20 17 -4 5 4.80 4.20 -17 3 -5 69.29 11.70 -17 3 -5 109.69 9.30 -17 3 5 71.79 12.90 17 -3 5 70.49 8.30 -17 2 -5 6.70 3.50 -17 2 -5 9.00 6.40 17 -2 -5 1.60 3.40 -17 2 5 3.10 6.80 17 -2 5 5.90 4.40 -17 1 -5 48.40 9.60 17 -1 -5 75.99 9.10 -17 1 -5 71.49 7.40 17 -1 5 52.19 7.70 -17 1 5 52.19 11.00 -17 0 -5 3.30 3.90 -17 0 -5 -2.90 5.30 17 0 5 3.10 3.80 -17 0 5 3.30 6.90 -17 -1 -5 51.19 10.10 -17 -1 -5 76.89 8.00 17 1 5 67.29 8.30 -17 -1 5 41.80 10.00 -17 -1 5 59.79 8.10 -17 -2 -5 9.20 6.70 -17 -2 -5 3.40 3.70 -17 -2 5 12.30 7.60 -17 -2 5 7.60 4.60 17 2 5 4.60 4.50 -17 -3 -5 67.39 11.70 -17 -3 -5 97.79 9.30 17 3 5 74.39 8.70 -17 -3 5 91.99 9.50 -17 -3 5 64.29 11.60 -17 -4 -5 8.90 6.50 -17 -4 -5 7.60 4.70 -17 -4 5 7.60 7.40 17 4 5 9.30 5.10 -17 -4 5 9.10 4.90 -17 -5 -5 58.79 10.70 -17 -5 -5 87.19 9.30 17 5 5 76.49 9.10 -17 -5 5 63.79 8.50 -17 5 -6 3.10 7.10 -17 5 6 3.90 8.10 -17 4 -6 -2.70 5.70 17 -4 -6 6.50 3.90 -17 4 -6 -3.20 2.90 -17 4 6 4.70 7.70 17 -4 6 1.10 3.80 -17 3 -6 0.00 3.30 17 -3 -6 0.60 3.80 -17 3 -6 4.40 5.70 17 -3 6 0.80 4.00 -17 3 6 9.80 7.50 -17 2 -6 -0.30 3.10 17 -2 -6 -3.40 3.30 -17 2 -6 4.70 6.00 17 -2 6 -5.40 3.60 -17 2 6 -3.50 6.80 -17 1 -6 6.30 3.90 17 -1 -6 -0.90 3.40 -17 1 -6 2.00 6.00 -17 1 6 -4.60 6.20 17 -1 6 4.40 4.40 -17 0 -6 0.70 5.70 -17 0 -6 -2.50 3.00 17 0 -6 1.70 3.40 -17 0 6 2.40 6.50 17 0 6 -0.70 3.60 17 1 -6 1.50 3.50 -17 -1 -6 6.90 5.90 -17 -1 -6 2.80 3.50 17 1 6 -2.00 4.00 -17 -1 6 2.70 6.40 -17 -2 -6 -2.00 5.50 -17 -2 -6 -1.90 3.80 17 2 6 2.20 4.50 -17 -3 -6 5.40 6.10 -17 -3 -6 1.10 4.10 17 3 6 15.90 5.00 -17 -4 -6 3.10 3.90 -17 -4 -6 2.60 6.10 -17 -4 6 -0.30 4.10 17 4 6 1.10 4.00 -17 -5 -6 7.90 7.70 -17 4 -7 1.20 6.10 17 -3 -7 92.59 8.00 -17 3 -7 68.19 7.70 -17 3 -7 47.70 9.90 17 -3 7 63.89 8.10 17 -2 -7 -2.10 3.40 -17 2 -7 -1.30 3.50 -17 2 -7 2.20 6.00 17 -2 7 9.40 4.40 17 -1 -7 94.69 8.50 -17 1 -7 75.19 8.40 -17 1 -7 80.59 12.30 17 -1 7 96.69 9.90 17 0 -7 -5.50 3.20 -17 0 -7 -0.50 5.60 -17 0 -7 -4.20 3.40 17 0 7 0.60 3.70 -17 -1 -7 102.09 9.70 17 1 -7 82.09 8.00 -17 -1 -7 77.99 11.80 17 1 7 82.39 9.40 17 2 -7 0.00 3.50 -17 -2 -7 -3.90 3.70 -17 -2 -7 1.20 5.70 17 2 7 0.40 3.70 -17 -3 -7 73.29 8.50 17 3 -7 75.39 8.00 -17 -3 -7 54.89 10.80 17 3 7 89.19 9.50 -17 -4 -7 0.30 6.20 -17 2 -8 0.30 3.50 -17 2 -8 -4.60 5.40 17 -2 8 2.50 4.90 -17 1 -8 9.90 4.30 17 -1 -8 7.90 4.00 -17 1 -8 9.60 6.40 17 -1 8 8.70 4.40 -17 0 -8 6.10 4.10 -17 0 -8 4.40 5.90 17 0 -8 -0.90 3.50 17 0 8 3.20 4.00 17 1 -8 5.00 3.80 -17 -1 -8 1.40 5.70 -17 -1 -8 6.40 4.20 17 1 8 0.60 4.00 -17 -2 -8 -2.50 5.20 -17 -2 -8 -2.10 3.70 17 2 8 2.00 4.70 -18 5 0 27.80 11.10 18 -4 0 8.80 4.60 -18 4 0 8.40 7.70 -18 4 0 13.30 4.60 -18 3 0 9.70 4.30 -18 3 0 10.30 7.50 18 -3 0 4.80 3.70 -18 2 0 19.30 5.00 18 -2 0 24.00 5.70 -18 2 0 6.90 7.80 -18 1 0 144.69 10.60 -18 1 0 81.89 12.80 -18 0 0 63.79 7.60 -18 0 0 43.10 9.70 -18 -1 0 76.69 12.50 -18 -1 0 141.89 10.50 -18 -2 0 10.70 7.60 -18 -2 0 20.40 5.20 -18 -3 0 -0.20 3.70 -18 -3 0 5.70 6.90 -18 -4 0 13.40 7.90 -18 -4 0 7.70 4.80 -18 -5 0 26.90 10.10 -18 4 -1 11.90 4.40 18 -4 -1 4.30 4.00 -18 4 -1 8.00 7.30 -18 4 1 5.40 7.50 18 -4 1 -2.00 3.30 -18 4 1 -1.30 3.90 18 -3 -1 11.10 4.90 -18 3 -1 -1.50 3.50 -18 3 -1 8.70 7.60 18 -3 1 4.70 3.90 -18 3 1 -0.50 3.60 -18 3 1 4.40 7.00 -18 2 -1 3.50 6.60 -18 2 -1 -0.80 3.80 -18 2 1 -2.00 6.80 -18 2 1 -5.30 3.00 18 -2 1 -2.20 3.40 -18 1 -1 -2.20 6.40 -18 1 -1 -2.70 3.60 -18 1 1 6.70 7.10 -18 1 1 -2.50 3.70 18 -1 1 2.70 3.90 -18 0 -1 1.70 6.40 -18 0 -1 -1.40 3.70 -18 0 1 1.40 6.70 -18 0 1 -5.50 3.70 -18 -1 -1 4.10 4.10 -18 -1 -1 0.80 6.10 -18 -1 1 -1.10 6.10 -18 -1 1 -4.40 3.70 -18 -2 -1 -0.50 3.70 -18 -2 -1 -1.10 6.40 -18 -2 1 -1.70 4.00 -18 -2 1 2.80 6.90 -18 -3 -1 -0.50 6.30 -18 -3 -1 -1.50 3.90 -18 -3 1 6.40 7.00 -18 -3 1 -1.00 4.00 -18 -4 -1 7.20 4.60 -18 -4 -1 4.60 7.20 -18 -4 1 3.90 4.00 -18 -4 1 4.00 6.60 -18 4 -2 9.00 4.10 18 -4 -2 11.60 4.90 -18 4 -2 6.60 7.70 -18 4 2 -0.20 6.50 18 -4 2 12.10 4.90 -18 3 -2 17.60 8.00 18 -3 -2 37.30 6.10 -18 3 -2 49.30 6.80 18 -3 2 35.60 6.40 -18 3 2 29.10 6.20 -18 3 2 22.90 9.50 -18 2 -2 3.70 3.80 -18 2 -2 8.60 7.20 -18 2 2 2.60 4.00 18 -2 2 -1.80 3.60 -18 2 2 3.70 6.70 -18 1 -2 48.30 6.80 -18 1 -2 19.30 8.20 -18 1 2 36.40 6.30 18 -1 2 42.90 6.50 -18 1 2 13.50 8.00 -18 0 -2 1.90 6.70 -18 0 -2 1.30 3.30 18 0 2 -0.40 3.70 -18 0 2 4.70 7.10 -18 0 2 -3.80 3.20 -18 -1 -2 27.90 8.70 -18 -1 -2 54.09 7.10 -18 -1 2 25.70 8.70 -18 -1 2 40.70 6.70 -18 -2 -2 -2.30 3.20 -18 -2 -2 4.40 6.80 -18 -2 2 6.10 6.70 -18 -2 2 -3.80 3.30 -18 -3 -2 20.50 8.00 -18 -3 -2 33.10 5.90 -18 -3 2 17.60 8.30 -18 -3 2 38.00 6.70 -18 -4 -2 -2.10 6.30 -18 -4 -2 10.20 4.80 -18 -4 2 9.90 4.50 -18 -4 2 -0.90 7.00 -18 4 -3 -2.60 6.80 -18 4 3 4.00 7.50 -18 3 -3 17.20 4.70 -18 3 -3 3.50 7.00 -18 3 3 7.60 7.40 18 -3 3 4.30 4.40 -18 2 -3 14.90 7.30 -18 2 -3 33.30 5.60 18 -2 3 16.30 5.20 -18 2 3 8.60 7.70 -18 1 -3 7.40 7.00 -18 1 -3 10.70 4.40 -18 1 3 9.00 4.20 -18 1 3 3.40 7.30 18 -1 3 4.00 3.90 -18 0 -3 3.80 3.50 -18 0 -3 -5.60 5.20 -18 0 3 -3.80 3.20 18 0 3 1.10 4.40 -18 0 3 -2.90 6.80 -18 -1 -3 2.70 6.10 -18 -1 -3 -0.60 3.60 -18 -1 3 6.20 4.50 -18 -1 3 11.10 7.90 18 1 3 4.80 4.40 -18 -2 -3 29.00 5.50 -18 -2 -3 7.70 6.90 -18 -2 3 11.30 7.80 -18 -2 3 21.80 5.20 18 2 3 16.20 5.20 -18 -3 -3 3.70 6.70 -18 -3 -3 0.80 3.70 -18 -3 3 8.40 7.80 -18 -3 3 -2.30 4.30 -18 -4 -3 3.20 7.20 -18 -4 3 -0.90 7.00 -18 3 -4 96.69 9.00 -18 3 -4 49.50 10.60 18 -3 4 63.19 8.10 -18 3 4 47.70 11.30 -18 2 -4 -2.10 3.20 -18 2 -4 -0.50 6.10 -18 2 4 2.80 7.20 18 -2 4 9.70 4.70 -18 1 -4 70.79 8.10 -18 1 -4 56.59 11.20 18 -1 4 69.89 8.40 -18 1 4 41.60 10.30 -18 0 -4 -0.90 3.60 -18 0 -4 2.10 6.10 18 0 4 3.60 4.00 -18 0 4 1.20 4.10 -18 0 4 9.50 7.50 -18 -1 -4 58.29 11.10 -18 -1 -4 89.69 9.00 18 1 4 73.29 8.90 -18 -1 4 42.90 10.70 -18 -1 4 68.49 8.20 -18 -2 -4 0.90 6.00 -18 -2 -4 3.50 3.70 -18 -2 4 -0.70 3.70 18 2 4 5.80 4.70 -18 -2 4 2.10 6.50 -18 -3 -4 72.99 8.60 -18 -3 -4 54.29 11.20 18 3 4 90.99 9.60 -18 -3 4 89.69 9.50 -18 -3 4 59.79 11.90 -18 3 5 3.50 8.10 -18 2 -5 3.70 6.70 -18 2 -5 -2.90 3.30 18 -2 5 0.70 4.10 -18 2 5 -1.50 7.20 -18 1 -5 -2.20 6.30 -18 1 -5 1.40 3.60 -18 1 5 3.20 7.40 18 -1 5 1.90 3.80 -18 0 -5 4.90 3.90 -18 0 -5 1.70 6.10 18 0 5 -5.90 4.00 -18 0 5 2.00 7.30 -18 -1 -5 2.20 6.40 -18 -1 -5 -1.10 3.80 18 1 5 0.80 4.30 -18 -1 5 4.70 7.00 -18 -2 -5 6.70 4.50 -18 -2 -5 -0.10 6.10 -18 -2 5 -8.80 3.60 -18 -2 5 -2.10 6.60 18 2 5 -5.30 4.20 -18 -3 5 0.40 8.30 -18 1 6 27.20 12.70 -18 0 -6 10.80 8.00 -18 -1 -6 22.90 9.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 22606 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x, y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.40778(2) 0.250000 0.250000 0.01786(9) Uani 1 2 d S T P . . O1 O 0.26841(10) 0.18349(12) 0.29673(8) 0.0312(3) Uani 1 1 d . . . . . N1 N 0.49765(10) 0.16225(12) 0.33674(9) 0.0191(3) Uani 1 1 d . . . . . N2 N 0.48499(10) 0.17114(11) 0.42864(9) 0.0182(3) Uani 1 1 d . . . . . N3 N 0.39349(10) 0.37342(12) 0.35553(9) 0.0189(3) Uani 1 1 d . . . . . N4 N 0.21900(17) 0.250000 0.250000 0.0344(6) Uani 1 2 d S T P . . C1 C 0.58465(12) 0.11977(14) 0.32580(11) 0.0204(3) Uani 1 1 d . . . . . C2 C 0.62653(13) 0.10120(15) 0.40985(12) 0.0235(4) Uani 1 1 d . . . . . H2 H 0.688069 0.071662 0.420697 0.028 Uiso 1 1 calc R U . . . C3 C 0.56148(12) 0.13395(13) 0.47417(11) 0.0200(3) Uani 1 1 d . . . . . C4 C 0.62562(14) 0.09853(16) 0.23453(12) 0.0252(4) Uani 1 1 d . . . . . H4A H 0.578320 0.116420 0.188172 0.038 Uiso 1 1 calc R U . . . H4B H 0.643688 0.019461 0.229494 0.038 Uiso 1 1 calc R U . . . H4C H 0.681783 0.145736 0.225902 0.038 Uiso 1 1 calc R U . . . C5 C 0.56524(14) 0.12823(15) 0.57499(11) 0.0255(4) Uani 1 1 d . . . . . H5A H 0.546512 0.200777 0.600413 0.038 Uiso 1 1 calc R U . . . H5B H 0.629979 0.110182 0.594247 0.038 Uiso 1 1 calc R U . . . H5C H 0.521696 0.069983 0.596431 0.038 Uiso 1 1 calc R U . . . C6 C 0.39800(12) 0.22016(15) 0.46431(11) 0.0210(3) Uani 1 1 d . . . . . H6A H 0.396174 0.209238 0.530623 0.025 Uiso 1 1 calc R U . . . H6B H 0.342785 0.180630 0.437978 0.025 Uiso 1 1 calc R U . . . C7 C 0.39014(12) 0.34406(14) 0.44354(10) 0.0183(3) Uani 1 1 d . . . . . C8 C 0.37764(14) 0.42238(16) 0.51109(11) 0.0251(4) Uani 1 1 d . . . . . H8 H 0.376096 0.399810 0.572652 0.030 Uiso 1 1 calc R U . . . C9 C 0.36737(15) 0.53439(16) 0.48816(12) 0.0285(4) Uani 1 1 d . . . . . H9 H 0.358931 0.589563 0.533756 0.034 Uiso 1 1 calc R U . . . C10 C 0.36957(14) 0.56452(15) 0.39820(12) 0.0256(4) Uani 1 1 d . . . . . H10 H 0.361790 0.640550 0.380622 0.031 Uiso 1 1 calc R U . . . C11 C 0.38333(13) 0.48188(15) 0.33424(11) 0.0227(3) Uani 1 1 d . . . . . H11 H 0.385689 0.502863 0.272336 0.027 Uiso 1 1 calc R U . . . Cl1 Cl 0.60698(5) 0.750000 0.250000 0.02468(14) Uani 1 2 d S T P . . O2 O 0.54764(11) 0.66402(12) 0.28734(10) 0.0379(4) Uani 1 1 d . . . . . O3 O 0.66554(11) 0.79597(16) 0.32025(10) 0.0463(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.01881(15) 0.02346(15) 0.01132(13) 0.00012(10) 0.000 0.000 O1 0.0290(7) 0.0424(8) 0.0222(6) -0.0065(6) 0.0040(5) -0.0063(6) N1 0.0224(7) 0.0220(7) 0.0130(6) -0.0008(5) 0.0017(5) 0.0024(6) N2 0.0223(7) 0.0195(7) 0.0129(6) 0.0004(5) 0.0001(5) 0.0024(5) N3 0.0205(7) 0.0223(7) 0.0140(6) 0.0014(5) -0.0010(5) 0.0006(5) N4 0.0225(12) 0.0533(16) 0.0275(12) -0.0171(11) 0.000 0.000 C1 0.0227(8) 0.0186(8) 0.0200(8) -0.0017(6) 0.0008(6) 0.0004(6) C2 0.0229(9) 0.0233(8) 0.0242(8) -0.0006(7) -0.0036(7) 0.0039(7) C3 0.0245(9) 0.0167(8) 0.0187(8) -0.0004(6) -0.0045(7) 0.0001(6) C4 0.0247(9) 0.0282(9) 0.0227(8) -0.0045(7) 0.0039(7) 0.0033(7) C5 0.0321(10) 0.0266(9) 0.0179(8) -0.0004(7) -0.0068(7) -0.0003(7) C6 0.0245(9) 0.0255(8) 0.0128(7) 0.0025(6) 0.0023(6) 0.0032(7) C7 0.0161(8) 0.0241(8) 0.0145(7) 0.0014(6) -0.0003(6) 0.0027(6) C8 0.0305(9) 0.0295(9) 0.0153(7) -0.0013(7) -0.0030(7) 0.0061(8) C9 0.0354(10) 0.0267(9) 0.0233(8) -0.0065(7) -0.0064(8) 0.0047(8) C10 0.0286(9) 0.0209(8) 0.0273(9) 0.0004(7) -0.0054(7) 0.0000(7) C11 0.0248(9) 0.0242(9) 0.0192(8) 0.0035(6) -0.0015(7) -0.0013(7) Cl1 0.0267(3) 0.0325(3) 0.0148(3) 0.0032(2) 0.000 0.000 O2 0.0486(9) 0.0314(7) 0.0338(8) 0.0117(6) -0.0014(7) -0.0057(7) O3 0.0407(9) 0.0781(12) 0.0202(7) -0.0058(8) -0.0021(6) -0.0179(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Zn1 N1 105.18(8) 4 . ? N1 Zn1 N3 87.37(5) 4 4 ? N1 Zn1 N3 99.18(5) . 4 ? N1 Zn1 N3 99.18(5) 4 . ? N1 Zn1 N3 87.37(5) . . ? N3 Zn1 N3 169.28(8) 4 . ? N1 Zn1 O1 99.55(5) 4 4 ? N1 Zn1 O1 154.85(5) . 4 ? N3 Zn1 O1 86.34(5) 4 4 ? N3 Zn1 O1 84.21(5) . 4 ? N1 Zn1 O1 154.85(5) 4 . ? N1 Zn1 O1 99.55(5) . . ? N3 Zn1 O1 84.21(5) 4 . ? N3 Zn1 O1 86.34(5) . . ? O1 Zn1 O1 56.35(8) 4 . ? N4 O1 Zn1 95.32(12) . . ? C1 N1 N2 105.54(13) . . ? C1 N1 Zn1 132.31(11) . . ? N2 N1 Zn1 119.40(10) . . ? C3 N2 N1 111.42(13) . . ? C3 N2 C6 128.67(14) . . ? N1 N2 C6 119.87(13) . . ? C11 N3 C7 118.30(14) . . ? C11 N3 Zn1 119.98(11) . . ? C7 N3 Zn1 121.66(11) . . ? O1 N4 O1 113.0(2) . 4 ? N1 C1 C2 109.92(15) . . ? N1 C1 C4 121.99(15) . . ? C2 C1 C4 128.09(16) . . ? C3 C2 C1 106.80(15) . . ? C3 C2 H2 126.6 . . ? C1 C2 H2 126.6 . . ? N2 C3 C2 106.32(14) . . ? N2 C3 C5 122.87(16) . . ? C2 C3 C5 130.75(16) . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? N2 C6 C7 112.33(14) . . ? N2 C6 H6A 109.1 . . ? C7 C6 H6A 109.1 . . ? N2 C6 H6B 109.1 . . ? C7 C6 H6B 109.1 . . ? H6A C6 H6B 107.9 . . ? N3 C7 C8 121.85(16) . . ? N3 C7 C6 116.54(14) . . ? C8 C7 C6 121.58(15) . . ? C7 C8 C9 119.28(16) . . ? C7 C8 H8 120.4 . . ? C9 C8 H8 120.4 . . ? C10 C9 C8 119.02(17) . . ? C10 C9 H9 120.5 . . ? C8 C9 H9 120.5 . . ? C9 C10 C11 118.59(17) . . ? C9 C10 H10 120.7 . . ? C11 C10 H10 120.7 . . ? N3 C11 C10 122.95(16) . . ? N3 C11 H11 118.5 . . ? C10 C11 H11 118.5 . . ? O2 Cl1 O2 108.65(13) 4_565 . ? O2 Cl1 O3 109.25(9) 4_565 4_565 ? O2 Cl1 O3 109.93(10) . 4_565 ? O2 Cl1 O3 109.93(10) 4_565 . ? O2 Cl1 O3 109.25(9) . . ? O3 Cl1 O3 109.83(14) 4_565 . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 N1 2.0851(14) 4 ? Zn1 N1 2.0851(14) . ? Zn1 N3 2.1555(14) 4 ? Zn1 N3 2.1555(14) . ? Zn1 O1 2.2288(13) 4 ? Zn1 O1 2.2288(13) . ? O1 N4 1.2620(19) . ? N1 C1 1.337(2) . ? N1 N2 1.3754(18) . ? N2 C3 1.347(2) . ? N2 C6 1.457(2) . ? N3 C11 1.339(2) . ? N3 C7 1.349(2) . ? C1 C2 1.394(2) . ? C1 C4 1.490(2) . ? C2 C3 1.378(2) . ? C2 H2 0.9500 . ? C3 C5 1.494(2) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.514(2) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C8 1.379(2) . ? C8 C9 1.386(3) . ? C8 H8 0.9500 . ? C9 C10 1.379(3) . ? C9 H9 0.9500 . ? C10 C11 1.380(2) . ? C10 H10 0.9500 . ? C11 H11 0.9500 . ? Cl1 O2 1.4342(14) 4_565 ? Cl1 O2 1.4342(14) . ? Cl1 O3 1.4361(15) 4_565 ? Cl1 O3 1.4361(15) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 N1 N2 C3 -0.76(18) . . . . ? Zn1 N1 N2 C3 -164.23(11) . . . . ? C1 N1 N2 C6 177.09(15) . . . . ? Zn1 N1 N2 C6 13.61(19) . . . . ? Zn1 O1 N4 O1 0.002(0) . . . 4 ? N2 N1 C1 C2 0.39(19) . . . . ? Zn1 N1 C1 C2 160.81(12) . . . . ? N2 N1 C1 C4 -179.33(15) . . . . ? Zn1 N1 C1 C4 -18.9(3) . . . . ? N1 C1 C2 C3 0.1(2) . . . . ? C4 C1 C2 C3 179.79(17) . . . . ? N1 N2 C3 C2 0.82(19) . . . . ? C6 N2 C3 C2 -176.79(16) . . . . ? N1 N2 C3 C5 -176.69(15) . . . . ? C6 N2 C3 C5 5.7(3) . . . . ? C1 C2 C3 N2 -0.55(19) . . . . ? C1 C2 C3 C5 176.69(17) . . . . ? C3 N2 C6 C7 109.79(18) . . . . ? N1 N2 C6 C7 -67.64(19) . . . . ? C11 N3 C7 C8 -0.7(3) . . . . ? Zn1 N3 C7 C8 -177.67(13) . . . . ? C11 N3 C7 C6 177.63(15) . . . . ? Zn1 N3 C7 C6 0.6(2) . . . . ? N2 C6 C7 N3 57.5(2) . . . . ? N2 C6 C7 C8 -124.17(17) . . . . ? N3 C7 C8 C9 0.6(3) . . . . ? C6 C7 C8 C9 -177.64(18) . . . . ? C7 C8 C9 C10 0.2(3) . . . . ? C8 C9 C10 C11 -0.9(3) . . . . ? C7 N3 C11 C10 0.0(3) . . . . ? Zn1 N3 C11 C10 177.00(14) . . . . ? C9 C10 C11 N3 0.8(3) . . . . ?