#------------------------------------------------------------------------------ #$Date: 2024-10-04 01:09:57 +0300 (Fri, 04 Oct 2024) $ #$Revision: 295021 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572759.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572759 loop_ _publ_author_name 'Anju, B. S.' 'Nair, Neeraja R.' 'Rajput, Janavi' 'Bertke, Jeffery A.' 'Mondal, Bhaskar' 'Kundu, Subrata' _publ_section_title ; Role of Ancillary Ligands in S-nitrosothiol and NO Generation from Nitrite-Thiol Interactions at Mononuclear Zinc(II) Sites ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC04853A _journal_year 2024 _chemical_formula_moiety 'C30 H30 N7 O2 Zn, Cl O4' _chemical_formula_sum 'C30 H30 Cl N7 O6 Zn' _chemical_formula_weight 685.43 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary intrinsic _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-05-16 deposited with the CCDC. 2024-10-03 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 111.897(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 19.739(3) _cell_length_b 8.1896(12) _cell_length_c 23.969(4) _cell_measurement_reflns_used 5977 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 27.18 _cell_measurement_theta_min 2.55 _cell_volume 3595.2(10) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELX-2018-3 (Sheldrick, 2015)' _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEX DUO/ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1010 _diffrn_reflns_av_unetI/netI 0.0847 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_h_min -26 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 57867 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.360 _diffrn_reflns_theta_min 2.294 _exptl_absorpt_coefficient_mu 0.805 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6589 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.266 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1416 _exptl_crystal_size_max 0.110 _exptl_crystal_size_mid 0.068 _exptl_crystal_size_min 0.048 _refine_diff_density_max 0.483 _refine_diff_density_min -0.650 _refine_diff_density_rms 0.070 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 503 _refine_ls_number_reflns 8940 _refine_ls_number_restraints 844 _refine_ls_restrained_S_all 1.027 _refine_ls_R_factor_all 0.1239 _refine_ls_R_factor_gt 0.0637 _refine_ls_shift/su_max 0.006 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0807P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1529 _refine_ls_wR_factor_ref 0.1755 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4756 _reflns_number_total 8940 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04853a2.cif _cod_data_source_block abs1097_sq _cod_original_cell_volume 3595.1(10) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1572759 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.917 _shelx_estimated_absorpt_t_max 0.962 _shelx_res_file ; TITL abs1097_a.res in P2(1)/n abs1097_sq.res created by SHELXL-2018/3 at 16:00:15 on 19-Jun-2023 REM Old TITL abs1097_a.res in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.183, Rweak 0.025, Alpha 0.057 REM 0.838 for 541 systematic absences, Orientation as input REM Formula found by SHELXT: C36 Cl N5 O5 Zn CELL 0.71073 19.7391 8.1896 23.9687 90 111.897 90 ZERR 4 0.0031 0.0012 0.0039 0 0.005 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl N O Zn UNIT 120 120 4 28 24 4 LIST 4 L.S. 20 0 54 PLAN 20 SIZE 0.048 0.068 0.11 TEMP -123.15 BOND $H FMAP 2 RIGU SIMU 0.01 0.02 CL1 > O6" SUMP 1.00 0.00001 1 2 1 3 1 4 CONF OMIT 1 0 1 OMIT -1 0 1 OMIT 2 0 0 ACTA ABIN WGHT 0.080700 FVAR 0.40473 0.63119 0.21169 0.15712 ZN1 6 0.712827 0.469297 0.467931 11.00000 0.04708 0.03655 = 0.04144 0.00357 0.01287 0.00480 N1 4 0.795406 0.583044 0.537230 11.00000 0.05785 0.03549 = 0.04625 -0.00154 0.01466 0.00714 N2 4 0.858193 0.500278 0.566752 11.00000 0.04933 0.03769 = 0.04003 0.00158 0.00428 0.00089 N3 4 0.803283 0.311728 0.453227 11.00000 0.04464 0.03152 = 0.04506 0.00274 0.01557 0.00627 N4 4 0.704547 0.636765 0.401345 11.00000 0.04946 0.03664 = 0.04764 0.00386 0.01882 0.00395 N5 4 0.638620 0.707724 0.372209 11.00000 0.05360 0.03992 = 0.03675 0.00353 0.01220 0.00897 N6 4 0.616109 0.590000 0.481503 11.00000 0.04614 0.04420 = 0.03798 -0.00201 0.01036 0.00253 N7 4 0.646665 0.186882 0.462676 11.00000 0.05149 0.04846 = 0.08011 0.00630 0.02567 0.00068 O1 5 0.637322 0.273468 0.417932 11.00000 0.05808 0.05699 = 0.06326 0.00160 0.01866 0.00654 O2 5 0.691162 0.249243 0.510202 11.00000 0.05786 0.05869 = 0.06334 0.00680 0.02440 0.00953 C1 1 0.810969 0.740466 0.550091 11.00000 0.07273 0.04142 = 0.04860 -0.01208 0.01720 -0.00181 C2 1 0.883042 0.756712 0.587153 11.00000 0.08275 0.05005 = 0.05454 -0.01332 0.01355 -0.02008 AFIX 43 H2 2 0.907858 0.855804 0.602837 11.00000 -1.20000 AFIX 0 C3 1 0.912317 0.602646 0.597185 11.00000 0.06101 0.06096 = 0.04374 -0.00140 0.00697 -0.01000 C4 1 0.755323 0.871225 0.526108 11.00000 0.09164 0.03702 = 0.07576 -0.01202 0.02186 0.01135 AFIX 137 H4A 2 0.754006 0.939033 0.559377 11.00000 -1.50000 H4B 2 0.707261 0.821635 0.505358 11.00000 -1.50000 H4C 2 0.768043 0.939154 0.497788 11.00000 -1.50000 AFIX 0 C5 1 0.987470 0.544867 0.633336 11.00000 0.06461 0.09045 = 0.07940 0.00241 -0.00580 -0.01644 AFIX 137 H5A 2 1.017687 0.637888 0.653948 11.00000 -1.50000 H5B 2 1.008757 0.493578 0.606707 11.00000 -1.50000 H5C 2 0.985434 0.465100 0.663150 11.00000 -1.50000 AFIX 0 C6 1 0.859157 0.325302 0.561411 11.00000 0.04112 0.04938 = 0.04177 0.01085 0.00191 0.00591 AFIX 23 H6A 2 0.815287 0.278879 0.566122 11.00000 -1.20000 H6B 2 0.902718 0.281007 0.594000 11.00000 -1.20000 AFIX 0 C7 1 0.860609 0.274646 0.501821 11.00000 0.04602 0.03327 = 0.05483 0.00580 0.01376 0.00965 C8 1 0.920712 0.191539 0.499159 11.00000 0.04838 0.05908 = 0.07715 0.00391 0.01109 0.01796 AFIX 43 H8 2 0.960549 0.165078 0.535113 11.00000 -1.20000 AFIX 0 C9 1 0.922270 0.148178 0.444784 11.00000 0.05941 0.06379 = 0.09624 0.00198 0.03771 0.02239 AFIX 43 H9 2 0.963637 0.093924 0.442384 11.00000 -1.20000 AFIX 0 C10 1 0.860312 0.140819 0.335461 11.00000 0.09986 0.06299 = 0.08609 -0.00175 0.06388 0.00464 AFIX 43 H10 2 0.900053 0.082656 0.331734 11.00000 -1.20000 AFIX 0 C11 1 0.803477 0.179669 0.286247 11.00000 0.13007 0.04701 = 0.07033 -0.00051 0.06908 -0.00259 AFIX 43 H11 2 0.803494 0.152272 0.247738 11.00000 -1.20000 AFIX 0 C12 1 0.743292 0.261344 0.291150 11.00000 0.10867 0.04051 = 0.04948 0.00579 0.03326 0.00311 AFIX 43 H12 2 0.702534 0.287976 0.255869 11.00000 -1.20000 AFIX 0 C13 1 0.742994 0.302241 0.345673 11.00000 0.06954 0.03757 = 0.04643 0.00104 0.02361 0.00623 AFIX 43 H13 2 0.701550 0.355547 0.348318 11.00000 -1.20000 AFIX 0 C14 1 0.802664 0.267305 0.398120 11.00000 0.05654 0.03138 = 0.04806 0.00482 0.02490 0.00665 C15 1 0.862817 0.184176 0.393085 11.00000 0.06814 0.04074 = 0.06989 0.00142 0.04075 0.00398 C16 1 0.752794 0.732245 0.389809 11.00000 0.06458 0.03646 = 0.04519 0.00013 0.02354 -0.00316 C17 1 0.717196 0.862170 0.354560 11.00000 0.08528 0.03978 = 0.04195 0.00312 0.02126 -0.00520 AFIX 43 H17 2 0.739201 0.947465 0.340368 11.00000 -1.20000 AFIX 0 C18 1 0.644289 0.846041 0.343684 11.00000 0.08523 0.03587 = 0.04052 0.00541 0.01454 0.00685 C19 1 0.832807 0.695981 0.413364 11.00000 0.06376 0.05620 = 0.08270 0.00728 0.03463 -0.00283 AFIX 137 H19A 2 0.859977 0.796746 0.414271 11.00000 -1.50000 H19B 2 0.843128 0.616102 0.387129 11.00000 -1.50000 H19C 2 0.847751 0.651331 0.454128 11.00000 -1.50000 AFIX 0 C20 1 0.580935 0.947724 0.309014 11.00000 0.09217 0.07147 = 0.06133 0.02764 -0.00193 0.01462 AFIX 137 H20A 2 0.597419 1.041316 0.291930 11.00000 -1.50000 H20B 2 0.556848 0.986814 0.335595 11.00000 -1.50000 H20C 2 0.546418 0.882647 0.276467 11.00000 -1.50000 AFIX 0 C21 1 0.573598 0.631183 0.374673 11.00000 0.04880 0.04457 = 0.03722 0.00286 0.00376 0.01067 AFIX 23 H21A 2 0.575110 0.512785 0.366882 11.00000 -1.20000 H21B 2 0.530132 0.677402 0.342521 11.00000 -1.20000 AFIX 0 C22 1 0.566121 0.654799 0.434025 11.00000 0.04265 0.04150 = 0.03973 -0.00113 0.00784 0.00418 C23 1 0.506293 0.743934 0.436831 11.00000 0.04945 0.05644 = 0.06340 0.00808 0.01791 0.01520 AFIX 43 H23 2 0.471204 0.789910 0.401452 11.00000 -1.20000 AFIX 0 C24 1 0.499661 0.762840 0.490171 11.00000 0.04637 0.06267 = 0.07564 -0.00210 0.02623 0.01048 AFIX 43 H24 2 0.460023 0.824145 0.492654 11.00000 -1.20000 AFIX 0 C25 1 0.550405 0.693330 0.541914 11.00000 0.04114 0.05413 = 0.06288 -0.01412 0.02252 -0.00725 C26 1 0.544964 0.703496 0.599261 11.00000 0.06067 0.08321 = 0.07100 -0.02483 0.03644 -0.01022 AFIX 43 H26 2 0.506026 0.763175 0.603729 11.00000 -1.20000 AFIX 0 C27 1 0.594456 0.629373 0.647295 11.00000 0.06969 0.10782 = 0.05213 -0.02257 0.02916 -0.02164 AFIX 43 H27 2 0.589793 0.635495 0.685282 11.00000 -1.20000 AFIX 0 C28 1 0.652808 0.543244 0.641589 11.00000 0.06409 0.11364 = 0.04831 -0.00245 0.01817 0.00162 AFIX 43 H28 2 0.687824 0.492835 0.675973 11.00000 -1.20000 AFIX 0 C29 1 0.660004 0.530831 0.587868 11.00000 0.05406 0.09094 = 0.03954 0.00546 0.01430 0.00829 AFIX 43 H29 2 0.699803 0.471097 0.584941 11.00000 -1.20000 AFIX 0 C30 1 0.609371 0.605149 0.536176 11.00000 0.04265 0.04970 = 0.04299 -0.00637 0.01600 -0.00257 PART 1 21 CL1 3 0.503470 0.410227 0.216399 21.00000 0.05389 0.05910 = 0.04788 0.00727 0.01513 -0.00346 O3 5 0.579414 0.396390 0.254605 21.00000 0.06271 0.14349 = 0.06737 0.01978 0.00621 0.00295 O4 5 0.463687 0.277564 0.227610 21.00000 0.09922 0.09899 = 0.10334 0.01721 0.04851 -0.03151 O5 5 0.474735 0.560372 0.227869 21.00000 0.12694 0.08417 = 0.08553 -0.00892 0.01861 0.03501 O6 5 0.495534 0.404798 0.154172 21.00000 0.05641 0.07608 = 0.05422 -0.00605 0.01315 -0.00678 PART 2 31 SAME 0.01 CL1 > O6 CL1' 3 0.499484 0.406467 0.214061 31.00000 0.07137 0.07402 = 0.06546 0.00501 0.00881 -0.00769 O3' 5 0.521601 0.354210 0.165947 31.00000 0.07777 0.07464 = 0.06002 -0.01241 0.01269 -0.00950 O4' 5 0.541715 0.314852 0.265429 31.00000 0.09620 0.09430 = 0.07561 0.03234 -0.00059 0.00678 O5' 5 0.513378 0.575632 0.225820 31.00000 0.05025 0.06767 = 0.06135 0.00183 0.02753 0.00909 O6' 5 0.423414 0.375186 0.199123 31.00000 0.07556 0.10948 = 0.08980 0.00887 0.01673 -0.01451 PART 3 41 SAME 0.01 CL1 > O6 CL1" 3 0.517315 0.389526 0.218812 41.00000 0.07010 0.07728 = 0.06784 0.01486 0.00975 -0.01047 O3" 5 0.577311 0.289895 0.217869 41.00000 0.07206 0.08250 = 0.08090 0.01324 0.00957 0.00338 O4" 5 0.486633 0.301201 0.254673 41.00000 0.07432 0.09272 = 0.07118 0.02359 0.01362 -0.02082 O5" 5 0.547056 0.539302 0.247581 41.00000 0.08180 0.07784 = 0.05510 0.00161 0.01585 -0.01299 O6" 5 0.468553 0.414544 0.158172 41.00000 0.06751 0.08203 = 0.06058 0.01358 0.01076 -0.00881 PART 0 HKLF 4 REM abs1097_a.res in P2(1)/n REM wR2 = 0.175471, GooF = S = 1.04526, Restrained GooF = 1.02718 for all data REM R1 = 0.063703 for 4756 Fo > 4sig(Fo) and 0.123872 for all 8940 data REM 503 parameters refined using 844 restraints END WGHT 0.0800 0.0000 REM Highest difference peak 0.483, deepest hole -0.650, 1-sigma level 0.070 Q1 1 0.7198 0.4660 0.5108 11.00000 0.05 0.48 Q2 1 0.7146 0.3065 0.4700 11.00000 0.05 0.39 Q3 1 0.6970 0.4696 0.4196 11.00000 0.05 0.38 Q4 1 0.5785 0.4888 0.2547 11.00000 0.05 0.37 Q5 1 0.6801 0.5826 0.4986 11.00000 0.05 0.37 Q6 1 0.4388 0.5014 0.1873 11.00000 0.05 0.33 Q7 1 0.6567 0.6003 0.4771 11.00000 0.05 0.32 Q8 1 0.7628 0.3719 0.4416 11.00000 0.05 0.32 Q9 1 0.6674 0.5893 0.4270 11.00000 0.05 0.32 Q10 1 0.4353 0.4766 0.2233 11.00000 0.05 0.32 Q11 1 0.7149 0.6238 0.4713 11.00000 0.05 0.29 Q12 1 0.8568 0.7755 0.4593 11.00000 0.05 0.29 Q13 1 0.5051 0.2571 0.2164 11.00000 0.05 0.29 Q14 1 0.8425 0.7284 0.3830 11.00000 0.05 0.28 Q15 1 0.5715 0.3181 0.2412 11.00000 0.05 0.28 Q16 1 0.6407 0.4605 0.5008 11.00000 0.05 0.27 Q17 1 0.5182 0.4402 0.2683 11.00000 0.05 0.27 Q18 1 0.7239 0.8496 0.4747 11.00000 0.05 0.27 Q19 1 0.7817 0.9651 0.5323 11.00000 0.05 0.24 Q20 1 0.6612 0.7177 0.6899 11.00000 0.05 0.24 ; _shelx_res_checksum 5426 _shelx_hkl_file ; -1 0 0 0.50 1.10 -1 0 0 0.00 1.50 -1 0 0 -0.60 0.70 1 0 0 0.00 0.90 1 0 0 -0.20 1.00 1 0 0 -1.00 1.20 2 0 0 1025.60 49.10 -3 0 0 -0.10 2.80 -3 0 0 -0.60 2.50 3 0 0 5.70 2.80 3 0 0 -1.90 2.80 3 0 0 4.90 2.80 -3 0 0 0.50 2.90 -4 0 0 288.17 17.40 4 0 0 306.07 17.90 4 0 0 293.57 17.70 4 0 0 339.37 18.80 -4 0 0 276.67 17.70 -4 0 0 303.67 18.40 -5 0 0 1.40 4.60 -5 0 0 2.40 4.00 5 0 0 11.10 5.20 5 0 0 1.00 4.30 5 0 0 -4.50 4.30 -5 0 0 10.20 4.90 6 0 0 1365.46 65.79 -6 0 0 1410.96 68.79 -6 0 0 1351.96 68.49 6 0 0 1377.46 68.29 6 0 0 1342.67 68.79 6 0 0 1410.36 69.89 -6 0 0 1342.37 69.49 -7 0 0 -5.70 4.90 7 0 0 -4.00 5.90 7 0 0 8.10 3.80 7 0 0 7.80 6.10 -7 0 0 10.00 7.00 -7 0 0 25.50 6.80 7 0 0 3.30 5.50 8 0 0 324.47 22.80 -8 0 0 327.27 23.50 8 0 0 348.97 24.20 -8 0 0 329.97 24.70 8 0 0 379.96 20.50 9 0 0 9.10 8.60 -9 0 0 14.70 7.20 -9 0 0 42.50 10.80 9 0 0 6.70 5.10 -10 0 0 748.43 43.90 10 0 0 794.42 45.10 10 0 0 736.73 39.50 -10 0 0 742.13 45.80 10 0 0 785.72 43.90 -11 0 0 32.70 9.70 11 0 0 51.89 12.40 11 0 0 30.40 9.30 11 0 0 32.60 7.10 -11 0 0 48.00 13.20 -12 0 0 209.78 24.20 12 0 0 182.18 21.60 12 0 0 174.68 14.90 12 0 0 185.88 19.80 -13 0 0 15.70 13.10 13 0 0 0.70 10.40 13 0 0 -3.20 7.50 13 0 0 10.00 7.40 14 0 0 1975.20 107.49 14 0 0 2038.80 101.79 -14 0 0 2222.88 112.49 14 0 0 2101.59 110.79 15 0 0 100.39 12.90 15 0 0 107.69 21.40 -15 0 0 164.78 24.70 15 0 0 104.69 17.60 16 0 0 23.80 8.90 16 0 0 30.40 12.00 -16 0 0 15.60 16.10 16 0 0 15.40 15.70 17 0 0 -2.60 8.50 17 0 0 13.40 13.10 17 0 0 20.60 17.30 -17 0 0 -16.10 15.20 18 0 0 11.30 10.20 18 0 0 3.50 19.00 -18 0 0 15.30 19.20 18 0 0 0.10 12.90 19 0 0 -4.00 18.30 19 0 0 4.40 13.30 -19 0 0 24.00 19.10 20 0 0 94.99 21.60 20 0 0 104.19 28.60 -20 0 0 109.39 27.30 21 0 0 -2.10 15.00 -21 0 0 19.50 22.90 21 0 0 -22.50 21.70 22 0 0 1.30 23.00 -22 0 0 -8.80 20.40 22 0 0 -10.00 15.50 -23 0 0 -12.30 22.20 23 0 0 9.20 17.20 23 0 0 29.90 27.20 24 0 0 16.50 20.10 24 0 0 -13.70 27.10 -24 0 0 35.90 29.40 0 -1 0 4.40 2.90 0 -1 0 7.80 3.80 0 1 0 2.20 2.10 0 1 0 -0.90 2.50 -1 -1 0 4492.35 196.78 1 -1 0 3605.54 196.38 1 -1 0 4498.95 194.98 2 -1 0 1758.42 85.69 -2 -1 0 1796.92 83.79 -2 -1 0 1812.62 84.29 2 -1 0 1824.02 83.89 2 -1 0 1735.33 83.89 -3 -1 0 339.07 18.50 3 -1 0 348.77 20.00 3 -1 0 348.97 17.90 3 -1 0 330.27 18.60 3 -1 0 356.86 19.00 -3 -1 0 346.97 19.20 -3 1 0 334.27 19.80 -3 1 0 324.67 19.00 3 1 0 340.47 19.20 -3 1 0 350.76 18.70 3 1 0 353.76 18.90 -3 1 0 344.37 18.00 -4 -1 0 1980.20 93.49 4 -1 0 1914.61 92.39 4 -1 0 1988.70 93.99 4 -1 0 1948.11 94.79 -4 -1 0 1936.51 94.19 4 -1 0 1955.70 93.59 4 1 0 1989.20 94.39 -4 1 0 1916.81 94.39 4 1 0 1981.70 93.69 -4 1 0 1941.31 93.49 -4 1 0 1910.71 92.59 -4 1 0 1953.30 94.29 5 -1 0 1020.50 49.70 5 -1 0 933.61 49.80 -5 -1 0 958.10 48.70 -5 -1 0 924.91 49.50 5 -1 0 967.70 48.90 5 -1 0 911.21 47.40 -5 1 0 992.90 49.10 -5 1 0 981.50 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36.90 9 1 -3 660.03 40.40 -9 1 3 707.13 36.80 8 -1 -3 825.22 42.40 -8 -1 3 863.91 46.30 8 -1 -3 842.02 46.10 -8 -1 3 853.41 46.80 8 -1 -3 725.43 45.30 8 -1 -3 920.41 47.00 8 -1 -3 813.22 41.20 8 1 -3 857.21 43.90 -8 1 3 838.32 46.50 -8 1 3 836.02 42.90 -8 1 3 816.62 45.10 8 1 -3 748.03 45.90 -8 1 3 864.81 40.80 7 -1 -3 1132.69 58.39 7 -1 -3 1139.79 54.39 -7 -1 3 1072.89 55.39 7 -1 -3 1125.09 57.89 -7 -1 3 1078.29 58.19 -7 -1 3 1103.29 57.39 7 -1 -3 1157.38 53.79 7 -1 -3 1135.49 58.09 -7 1 3 1067.39 54.59 -7 1 3 1100.09 53.29 -7 1 3 1103.79 57.69 -7 1 3 1039.40 56.99 7 1 -3 1167.18 58.39 -7 1 3 1089.79 57.99 7 1 -3 1110.19 55.89 7 1 -3 1113.09 58.59 -6 -1 3 156.88 14.90 6 -1 -3 114.59 8.30 -6 -1 3 115.59 10.50 6 -1 -3 102.29 8.00 6 -1 -3 103.89 12.10 -6 -1 3 106.49 11.60 6 -1 -3 101.59 12.50 6 -1 -3 114.69 12.80 -6 1 3 100.89 7.50 -6 1 3 150.48 14.10 -6 1 3 95.79 11.20 6 1 -3 121.99 13.30 6 1 -3 123.09 11.10 -6 1 3 116.39 13.40 6 1 -3 122.39 13.20 -6 1 3 104.49 8.80 -5 -1 3 1224.08 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0.00 -8 2 31 1.08 0.00 -7 2 31 0.00 0.00 -6 2 31 -1.54 0.00 19 7 0 -0.82 0.00 14 9 0 -1.66 0.00 10 10 0 -0.28 0.00 1 11 0 0.60 0.00 -24 3 1 0.67 0.00 -17 8 1 -2.00 0.00 10 10 1 0.06 0.00 -1 11 1 0.64 0.00 0 11 1 -0.09 0.00 1 11 1 -0.26 0.00 0 0 2 -134.98 0.00 24 0 2 -0.24 0.00 -25 1 2 -0.31 0.00 23 3 2 0.31 0.00 20 6 2 0.78 0.00 16 8 2 0.92 0.00 -1 11 2 0.13 0.00 0 11 2 -1.00 0.00 -1 0 3 -82.87 0.00 -25 2 3 -1.00 0.00 13 9 3 0.81 0.00 -11 10 3 -1.87 0.00 9 10 3 3.31 0.00 23 1 4 0.15 0.00 -24 4 4 0.32 0.00 -20 7 4 0.28 0.00 -15 9 4 -0.38 0.00 -11 10 4 -0.15 0.00 -24 4 5 -0.53 0.00 21 4 5 1.50 0.00 -23 5 5 -0.42 0.00 20 5 5 0.47 0.00 -20 7 5 0.31 0.00 17 7 5 0.85 0.00 -18 8 5 0.65 0.00 15 8 5 -0.46 0.00 -15 9 5 0.10 0.00 12 9 5 -2.16 0.00 -11 10 5 0.04 0.00 8 10 5 1.39 0.00 -26 0 6 0.32 0.00 -25 3 6 -0.78 0.00 -22 6 6 0.33 0.00 -18 8 6 -0.52 0.00 -15 9 6 -0.07 0.00 -11 10 6 0.38 0.00 7 10 6 1.73 0.00 -26 1 7 0.58 0.00 19 5 7 -0.30 0.00 -22 6 7 -2.78 0.00 16 7 7 0.01 0.00 -18 8 7 -0.48 0.00 -15 9 7 0.90 0.00 11 9 7 0.75 0.00 -11 10 7 0.18 0.00 21 2 8 0.55 0.00 -22 6 8 0.42 0.00 -18 8 8 0.67 0.00 -15 9 8 -1.10 0.00 10 9 8 1.09 0.00 -26 2 9 -1.20 0.00 19 4 9 0.22 0.00 18 5 9 -0.96 0.00 15 7 9 0.70 0.00 -18 8 9 2.10 0.00 -15 9 9 -0.95 0.00 -10 10 9 1.35 0.00 5 10 9 -0.71 0.00 -26 2 10 -0.48 0.00 16 6 10 0.05 0.00 -18 8 10 -0.61 0.00 12 8 10 -0.18 0.00 -15 9 10 1.18 0.00 -10 10 10 -0.48 0.00 -9 10 10 -1.15 0.00 -26 2 11 0.07 0.00 18 4 11 -0.54 0.00 -18 8 11 -1.71 0.00 11 8 11 -0.49 0.00 8 9 11 -1.46 0.00 -9 10 11 1.58 0.00 -8 10 11 0.99 0.00 1 10 11 -0.40 0.00 2 10 11 -0.22 0.00 19 1 12 0.49 0.00 -26 2 12 0.79 0.00 -22 6 12 -0.96 0.00 13 7 12 -0.35 0.00 7 9 12 0.03 0.00 -8 10 12 -1.53 0.00 -7 10 12 -0.20 0.00 0 10 12 -0.84 0.00 1 10 12 1.68 0.00 -26 2 13 0.75 0.00 18 2 13 -0.33 0.00 -22 6 13 -1.29 0.00 14 6 13 -1.06 0.00 -20 7 13 -2.71 0.00 12 7 13 -1.78 0.00 -14 9 13 -2.10 0.00 6 9 13 0.93 0.00 -7 10 13 0.97 0.00 -6 10 13 -0.94 0.00 -5 10 13 -1.41 0.00 -4 10 13 0.32 0.00 -3 10 13 1.70 0.00 -2 10 13 -0.58 0.00 -1 10 13 -1.15 0.00 -26 2 14 -0.07 0.00 16 4 14 0.22 0.00 -22 6 14 0.89 0.00 -20 7 14 -0.28 0.00 -13 9 14 2.14 0.00 5 9 14 2.32 0.00 17 1 15 -1.06 0.00 16 3 15 1.19 0.00 14 5 15 -2.26 0.00 -17 8 15 1.09 0.00 -13 9 15 0.05 0.00 16 2 16 0.54 0.00 -23 5 16 0.81 0.00 -12 9 16 0.40 0.00 2 9 16 -1.36 0.00 -26 1 17 -0.30 0.00 -25 3 17 1.22 0.00 -24 4 17 -1.49 0.00 -19 7 17 0.39 0.00 -16 8 17 -0.35 0.00 -11 9 17 -0.40 0.00 -10 9 17 0.50 0.00 0 9 17 0.64 0.00 -26 0 18 -0.42 0.00 -15 8 18 -0.93 0.00 4 8 18 -0.91 0.00 -9 9 18 -0.17 0.00 -8 9 18 -0.86 0.00 -7 9 18 -0.75 0.00 -6 9 18 0.17 0.00 -5 9 18 0.90 0.00 -4 9 18 0.54 0.00 -3 9 18 -2.25 0.00 -2 9 18 0.04 0.00 -18 7 19 -0.80 0.00 -14 8 19 1.62 0.00 13 1 20 -0.26 0.00 12 3 20 0.47 0.00 11 4 20 -0.56 0.00 -20 6 20 0.75 0.00 5 7 20 -0.12 0.00 -13 8 20 -0.26 0.00 1 8 20 -0.47 0.00 -25 0 21 -0.28 0.00 -25 1 21 -1.61 0.00 12 1 21 -0.90 0.00 11 3 21 0.84 0.00 10 4 21 -1.37 0.00 -11 8 21 -0.76 0.00 -2 8 21 0.54 0.00 -1 8 21 0.13 0.00 11 1 22 -0.58 0.00 -24 2 22 0.71 0.00 5 6 22 -0.40 0.00 2 7 22 -0.66 0.00 -9 8 22 0.93 0.00 -8 8 22 -0.71 0.00 -7 8 22 -0.08 0.00 -6 8 22 1.04 0.00 -5 8 22 -1.09 0.00 -24 1 23 -0.81 0.00 10 1 23 -0.36 0.00 -23 3 23 -0.51 0.00 -20 5 23 -0.55 0.00 6 5 23 0.65 0.00 -14 7 23 1.83 0.00 0 7 23 -1.44 0.00 -23 2 24 -1.94 0.00 -21 4 24 -0.97 0.00 2 6 24 -0.97 0.00 -12 7 24 0.30 0.00 -3 7 24 0.64 0.00 -23 0 25 -0.34 0.00 -23 1 25 -0.02 0.00 7 2 25 -1.00 0.00 5 4 25 -1.13 0.00 3 5 25 -1.16 0.00 -15 6 25 1.70 0.00 0 6 25 -0.52 0.00 5 3 26 0.69 0.00 -17 5 26 0.97 0.00 1 5 26 0.25 0.00 -13 6 26 -0.75 0.00 -3 6 26 0.14 0.00 5 0 27 0.25 0.00 5 1 27 1.02 0.00 -21 2 27 0.62 0.00 -20 3 27 0.86 0.00 3 3 27 -0.01 0.00 -18 4 27 -0.28 0.00 -1 5 27 0.17 0.00 -9 6 27 1.58 0.00 -8 6 27 1.68 0.00 -7 6 27 0.78 0.00 -20 2 28 0.05 0.00 -13 5 28 0.11 0.00 -4 5 28 0.65 0.00 -17 3 29 0.76 0.00 -1 3 29 1.12 0.00 -15 4 29 -1.08 0.00 -3 4 29 -1.01 0.00 -18 0 30 -0.12 0.00 -18 1 30 -0.69 0.00 -1 1 30 -0.37 0.00 -17 2 30 1.54 0.00 -2 2 30 -0.68 0.00 -15 3 30 -0.97 0.00 -4 3 30 -0.63 0.00 -10 4 30 0.02 0.00 -9 4 30 0.68 0.00 -8 4 30 -0.06 0.00 -3 0 31 -0.50 0.00 -16 1 31 0.35 0.00 -14 2 31 -0.20 0.00 -5 2 31 -0.68 0.00 -11 3 31 0.76 0.00 -10 3 31 -0.79 0.00 -9 3 31 -2.25 0.00 -12 0 32 -0.30 0.00 -10 0 32 1.18 0.00 -8 0 32 -0.04 0.00 -12 1 32 2.05 0.00 -11 1 32 -0.13 0.00 -10 1 32 -1.39 0.00 -9 1 32 -1.09 0.00 -8 1 32 -0.23 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 130720) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.250 -0.015 0.250 306 95 ' ' 2 0.500 0.000 0.000 13 1 ' ' 3 0.750 -0.018 0.750 306 95 ' ' 4 0.000 0.500 0.500 13 1 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 0 2 1.831 -1 0 3 2.551 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) A total of approximately 7.25 highly disordered methanol solvent molecules per unit cell were removed from the model. TITL ABS1097 P 21/n R = 0.10 CELL 19.7390 8.1896 23.9690 90.00 111.90 90.00 SPGR P21/n # Solvent Accessible Volume = 639 # Electrons Found in S.A.V. = 192 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.804 0.590 0.781 ! 2.75 eA-3 C102 0.858 0.533 0.777 ! 2.74 eA-3 C103 0.771 0.093 0.673 ! 2.63 eA-3 C104 0.790 0.563 0.834 ! 2.49 eA-3 C105 0.136 0.399 0.282 ! 2.39 eA-3 C106 0.346 0.875 0.316 ! 2.36 eA-3 C107 0.221 0.029 0.309 ! 1.24 eA-3 Q108 0.425 0.500 0.747 ! 0.77 eA-3 Q109 0.414 0.793 0.250 ! 0.73 eA-3 Q110 0.062 0.781 0.297 ! 0.71 eA-3 Q111 0.434 0.503 0.217 ! 0.71 eA-3 C112 0.735 0.406 0.774 ! 0.71 eA-3 C113 0.777 0.282 0.697 ! 0.71 eA-3 C114 0.689 0.160 0.812 ! 0.69 eA-3 Q115 0.289 0.685 0.531 ! 0.67 eA-3 Q116 0.423 0.439 0.178 ! 0.65 eA-3 C117 0.705 0.367 0.789 ! 0.64 eA-3 Q118 0.056 0.872 0.858 ! 0.64 eA-3 C119 0.162 0.249 0.295 ! 0.63 eA-3 Q120 0.689 0.277 0.713 ! 0.61 eA-3 Q121 0.732 0.688 0.875 ! 0.60 eA-3 Q122 0.933 0.663 0.717 ! 0.59 eA-3 C123 0.816 0.372 0.704 ! 0.58 eA-3 Q124 0.204 0.871 0.235 ! 0.58 eA-3 Q125 0.687 0.315 0.687 ! 0.57 eA-3 Q126 0.816 0.255 0.702 ! 0.57 eA-3 Q127 0.783 0.978 0.062 ! 0.57 eA-3 Q128 0.750 0.624 0.506 ! 0.57 eA-3 Q129 0.839 0.586 0.905 ! 0.57 eA-3 C130 0.827 0.379 0.737 ! 0.56 eA-3 Q131 0.488 0.558 0.736 ! 0.56 eA-3 Q132 0.470 0.934 0.022 ! 0.56 eA-3 Q133 0.607 0.382 0.035 ! 0.56 eA-3 Q134 0.232 0.132 0.235 ! 0.55 eA-3 Q135 0.933 0.806 0.266 ! 0.55 eA-3 Q136 0.615 0.929 0.791 ! 0.54 eA-3 C137 0.784 0.344 0.665 ! 0.54 eA-3 Q138 0.063 0.346 0.553 ! 0.54 eA-3 Q139 0.776 0.963 0.992 ! 0.54 eA-3 Q140 0.788 0.156 0.033 ! 0.54 eA-3 Q141 0.998 0.855 0.344 ! 0.54 eA-3 Q142 0.471 0.409 0.135 ! 0.54 eA-3 Q143 0.674 0.597 0.494 ! 0.53 eA-3 Q144 0.431 0.410 0.235 ! 0.53 eA-3 C145 0.780 0.257 0.734 ! 0.53 eA-3 Q146 0.338 0.322 0.187 ! 0.52 eA-3 Q147 0.443 0.521 0.183 ! 0.52 eA-3 Q148 0.986 0.757 0.274 ! 0.52 eA-3 Q149 0.192 0.053 0.352 ! 0.51 eA-3 Q150 0.827 0.371 0.805 ! 0.51 eA-3 Q151 0.028 0.877 0.398 ! 0.51 eA-3 Q152 0.876 0.061 0.936 ! 0.51 eA-3 Q153 0.107 0.952 0.306 ! 0.51 eA-3 Q154 0.521 0.092 0.876 ! 0.51 eA-3 C155 0.670 0.341 0.751 ! 0.51 eA-3 Q156 0.585 0.662 0.001 ! 0.51 eA-3 Q157 0.066 0.935 0.385 ! 0.50 eA-3 Q158 0.604 0.256 0.850 ! 0.50 eA-3 Q159 0.122 0.559 0.132 ! 0.50 eA-3 Q160 0.238 0.685 0.975 ! 0.50 eA-3 Q161 0.145 0.748 0.616 ! 0.50 eA-3 C162 0.268 0.144 0.350 ! 0.50 eA-3 ) ; _shelx_fab_checksum 83684 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.71283(2) 0.46930(5) 0.46793(2) 0.04274(16) Uani 1 1 d . . . . . N1 N 0.79541(17) 0.5830(4) 0.53723(13) 0.0479(8) Uani 1 1 d . . . . . N2 N 0.85819(17) 0.5003(4) 0.56675(14) 0.0459(7) Uani 1 1 d . . . . . N3 N 0.80328(16) 0.3117(3) 0.45323(13) 0.0407(7) Uani 1 1 d . . . . . N4 N 0.70455(16) 0.6368(3) 0.40134(13) 0.0444(7) Uani 1 1 d . . . . . N5 N 0.63862(17) 0.7077(4) 0.37221(13) 0.0448(7) Uani 1 1 d . . . . . N6 N 0.61611(16) 0.5900(4) 0.48150(13) 0.0443(7) Uani 1 1 d . . . . . N7 N 0.64666(19) 0.1869(4) 0.46268(19) 0.0597(9) Uani 1 1 d . . . . . O1 O 0.63732(15) 0.2735(3) 0.41793(13) 0.0606(7) Uani 1 1 d . . . . . O2 O 0.69116(16) 0.2492(3) 0.51020(14) 0.0594(7) Uani 1 1 d . . . . . C1 C 0.8110(3) 0.7405(5) 0.55009(18) 0.0558(10) Uani 1 1 d . . . . . C2 C 0.8830(3) 0.7567(5) 0.58715(19) 0.0659(12) Uani 1 1 d . . . . . H2 H 0.907858 0.855804 0.602837 0.079 Uiso 1 1 calc R U . . . C3 C 0.9123(2) 0.6026(6) 0.59718(18) 0.0589(11) Uani 1 1 d . . . . . C4 C 0.7553(3) 0.8712(5) 0.5261(2) 0.0708(13) Uani 1 1 d . . . . . H4A H 0.754006 0.939033 0.559377 0.106 Uiso 1 1 calc R U . . . H4B H 0.707261 0.821635 0.505358 0.106 Uiso 1 1 calc R U . . . H4C H 0.768043 0.939154 0.497788 0.106 Uiso 1 1 calc R U . . . C5 C 0.9875(3) 0.5449(6) 0.6333(2) 0.0876(16) Uani 1 1 d . . . . . H5A H 1.017687 0.637888 0.653948 0.131 Uiso 1 1 calc R U . . . H5B H 1.008757 0.493578 0.606707 0.131 Uiso 1 1 calc R U . . . H5C H 0.985434 0.465100 0.663150 0.131 Uiso 1 1 calc R U . . . C6 C 0.8592(2) 0.3253(5) 0.56141(16) 0.0480(9) Uani 1 1 d . . . . . H6A H 0.815287 0.278879 0.566122 0.058 Uiso 1 1 calc R U . . . H6B H 0.902718 0.281007 0.594000 0.058 Uiso 1 1 calc R U . . . C7 C 0.8606(2) 0.2746(4) 0.50182(18) 0.0462(9) Uani 1 1 d . . . . . C8 C 0.9207(2) 0.1915(5) 0.4992(2) 0.0651(12) Uani 1 1 d . . . . . H8 H 0.960549 0.165078 0.535113 0.078 Uiso 1 1 calc R U . . . C9 C 0.9223(2) 0.1482(6) 0.4448(2) 0.0706(13) Uani 1 1 d . . . . . H9 H 0.963637 0.093924 0.442384 0.085 Uiso 1 1 calc R U . . . C10 C 0.8603(3) 0.1408(6) 0.3355(2) 0.0745(13) Uani 1 1 d . . . . . H10 H 0.900053 0.082656 0.331734 0.089 Uiso 1 1 calc R U . . . C11 C 0.8035(3) 0.1797(5) 0.2862(2) 0.0733(13) Uani 1 1 d . . . . . H11 H 0.803494 0.152272 0.247738 0.088 Uiso 1 1 calc R U . . . C12 C 0.7433(3) 0.2613(5) 0.29115(19) 0.0651(12) Uani 1 1 d . . . . . H12 H 0.702534 0.287976 0.255869 0.078 Uiso 1 1 calc R U . . . C13 C 0.7430(2) 0.3022(4) 0.34567(17) 0.0506(9) Uani 1 1 d . . . . . H13 H 0.701550 0.355547 0.348318 0.061 Uiso 1 1 calc R U . . . C14 C 0.8027(2) 0.2673(4) 0.39812(17) 0.0438(8) Uani 1 1 d . . . . . C15 C 0.8628(2) 0.1842(5) 0.3931(2) 0.0553(10) Uani 1 1 d . . . . . C16 C 0.7528(2) 0.7322(4) 0.38981(17) 0.0479(9) Uani 1 1 d . . . . . C17 C 0.7172(3) 0.8622(5) 0.35456(17) 0.0564(10) Uani 1 1 d . . . . . H17 H 0.739201 0.947465 0.340368 0.068 Uiso 1 1 calc R U . . . C18 C 0.6443(3) 0.8460(5) 0.34368(17) 0.0564(10) Uani 1 1 d . . . . . C19 C 0.8328(2) 0.6960(5) 0.4134(2) 0.0654(12) Uani 1 1 d . . . . . H19A H 0.859977 0.796746 0.414271 0.098 Uiso 1 1 calc R U . . . H19B H 0.843128 0.616102 0.387129 0.098 Uiso 1 1 calc R U . . . H19C H 0.847751 0.651331 0.454128 0.098 Uiso 1 1 calc R U . . . C20 C 0.5809(3) 0.9477(6) 0.3090(2) 0.0838(16) Uani 1 1 d . . . . . H20A H 0.597419 1.041316 0.291930 0.126 Uiso 1 1 calc R U . . . H20B H 0.556848 0.986814 0.335595 0.126 Uiso 1 1 calc R U . . . H20C H 0.546418 0.882647 0.276467 0.126 Uiso 1 1 calc R U . . . C21 C 0.5736(2) 0.6312(5) 0.37467(16) 0.0471(9) Uani 1 1 d . . . . . H21A H 0.575110 0.512785 0.366882 0.056 Uiso 1 1 calc R U . . . H21B H 0.530132 0.677402 0.342521 0.056 Uiso 1 1 calc R U . . . C22 C 0.56612(19) 0.6548(4) 0.43403(16) 0.0435(8) Uani 1 1 d . . . . . C23 C 0.5063(2) 0.7439(5) 0.4368(2) 0.0573(11) Uani 1 1 d . . . . . H23 H 0.471204 0.789910 0.401452 0.069 Uiso 1 1 calc R U . . . C24 C 0.4997(2) 0.7628(5) 0.4902(2) 0.0606(11) Uani 1 1 d . . . . . H24 H 0.460023 0.824145 0.492654 0.073 Uiso 1 1 calc R U . . . C25 C 0.5504(2) 0.6933(5) 0.54191(19) 0.0518(10) Uani 1 1 d . . . . . C26 C 0.5450(3) 0.7035(6) 0.5993(2) 0.0682(12) Uani 1 1 d . . . . . H26 H 0.506026 0.763175 0.603729 0.082 Uiso 1 1 calc R U . . . C27 C 0.5945(3) 0.6294(7) 0.6473(2) 0.0747(13) Uani 1 1 d . . . . . H27 H 0.589793 0.635495 0.685282 0.090 Uiso 1 1 calc R U . . . C28 C 0.6528(3) 0.5432(6) 0.6416(2) 0.0761(14) Uani 1 1 d . . . . . H28 H 0.687824 0.492835 0.675973 0.091 Uiso 1 1 calc R U . . . C29 C 0.6600(2) 0.5308(6) 0.58787(18) 0.0624(11) Uani 1 1 d . . . . . H29 H 0.699803 0.471097 0.584941 0.075 Uiso 1 1 calc R U . . . C30 C 0.6094(2) 0.6051(5) 0.53618(16) 0.0451(9) Uani 1 1 d . . . . . Cl1 Cl 0.5035(2) 0.4102(5) 0.2164(2) 0.0547(9) Uani 0.631(3) 1 d D U P A 1 O3 O 0.5794(3) 0.3964(10) 0.2546(3) 0.0964(18) Uani 0.631(3) 1 d D U P A 1 O4 O 0.4637(4) 0.2776(8) 0.2276(3) 0.097(2) Uani 0.631(3) 1 d D U P A 1 O5 O 0.4747(4) 0.5604(8) 0.2279(3) 0.105(2) Uani 0.631(3) 1 d D U P A 1 O6 O 0.4955(3) 0.4048(9) 0.1542(2) 0.0644(18) Uani 0.631(3) 1 d D U P A 1 Cl1' Cl 0.4995(8) 0.4065(16) 0.2141(7) 0.075(3) Uani 0.212(3) 1 d D U P B 2 O3' O 0.5216(10) 0.354(2) 0.1659(7) 0.075(4) Uani 0.212(3) 1 d D U P B 2 O4' O 0.5417(11) 0.315(2) 0.2654(7) 0.098(4) Uani 0.212(3) 1 d D U P B 2 O5' O 0.5134(9) 0.5756(16) 0.2258(8) 0.058(3) Uani 0.212(3) 1 d D U P B 2 O6' O 0.4234(7) 0.375(2) 0.1991(8) 0.096(4) Uani 0.212(3) 1 d D U P B 2 Cl1" Cl 0.5173(8) 0.3895(18) 0.2188(7) 0.076(3) Uani 0.157(3) 1 d D U P C 3 O3" O 0.5773(9) 0.290(2) 0.2179(10) 0.084(4) Uani 0.157(3) 1 d D U P C 3 O4" O 0.4866(14) 0.301(3) 0.2547(10) 0.083(4) Uani 0.157(3) 1 d D U P C 3 O5" O 0.5471(13) 0.539(2) 0.2476(9) 0.074(4) Uani 0.157(3) 1 d D U P C 3 O6" O 0.4686(11) 0.415(3) 0.1582(8) 0.074(5) Uani 0.157(3) 1 d D U P C 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.0471(3) 0.0366(3) 0.0414(3) 0.00357(18) 0.0129(2) 0.00480(19) N1 0.058(2) 0.0355(16) 0.0463(19) -0.0015(14) 0.0147(16) 0.0071(14) N2 0.0493(18) 0.0377(17) 0.0400(17) 0.0016(13) 0.0043(14) 0.0009(13) N3 0.0446(17) 0.0315(16) 0.0451(17) 0.0027(13) 0.0156(14) 0.0063(13) N4 0.0495(18) 0.0366(17) 0.0476(18) 0.0039(14) 0.0188(15) 0.0040(14) N5 0.0536(18) 0.0399(18) 0.0367(17) 0.0035(13) 0.0122(15) 0.0090(14) N6 0.0461(18) 0.0442(18) 0.0380(16) -0.0020(13) 0.0104(14) 0.0025(14) N7 0.051(2) 0.048(2) 0.080(3) 0.0063(19) 0.0257(19) 0.0007(17) O1 0.0581(18) 0.0570(18) 0.0633(19) 0.0016(15) 0.0187(15) 0.0065(14) O2 0.0579(18) 0.0587(18) 0.0633(19) 0.0068(15) 0.0244(15) 0.0095(14) C1 0.073(3) 0.041(2) 0.049(2) -0.0121(18) 0.017(2) -0.0018(19) C2 0.083(3) 0.050(2) 0.055(3) -0.013(2) 0.014(2) -0.020(2) C3 0.061(3) 0.061(3) 0.044(2) -0.0014(19) 0.007(2) -0.010(2) C4 0.092(3) 0.037(2) 0.076(3) -0.012(2) 0.022(3) 0.011(2) C5 0.065(3) 0.090(4) 0.079(4) 0.002(3) -0.006(3) -0.016(3) C6 0.041(2) 0.049(2) 0.042(2) 0.0108(17) 0.0019(17) 0.0059(17) C7 0.046(2) 0.033(2) 0.055(2) 0.0058(16) 0.0138(18) 0.0097(16) C8 0.048(2) 0.059(3) 0.077(3) 0.004(2) 0.011(2) 0.018(2) C9 0.059(3) 0.064(3) 0.096(3) 0.002(3) 0.038(3) 0.022(2) C10 0.100(4) 0.063(3) 0.086(3) -0.002(3) 0.064(3) 0.005(3) C11 0.130(4) 0.047(3) 0.070(3) -0.001(2) 0.069(3) -0.003(3) C12 0.109(4) 0.041(2) 0.049(2) 0.0058(18) 0.033(3) 0.003(2) C13 0.070(3) 0.038(2) 0.046(2) 0.0010(17) 0.0236(19) 0.0062(19) C14 0.057(2) 0.0314(19) 0.048(2) 0.0048(16) 0.0249(18) 0.0066(16) C15 0.068(3) 0.041(2) 0.070(3) 0.001(2) 0.041(2) 0.0040(19) C16 0.065(2) 0.036(2) 0.045(2) 0.0001(16) 0.024(2) -0.0032(17) C17 0.085(3) 0.040(2) 0.042(2) 0.0031(17) 0.021(2) -0.005(2) C18 0.085(3) 0.036(2) 0.041(2) 0.0054(17) 0.015(2) 0.007(2) C19 0.064(3) 0.056(3) 0.083(3) 0.007(2) 0.035(3) -0.003(2) C20 0.092(4) 0.071(3) 0.061(3) 0.028(2) -0.002(3) 0.015(3) C21 0.049(2) 0.045(2) 0.037(2) 0.0029(16) 0.0038(17) 0.0107(17) C22 0.043(2) 0.041(2) 0.0397(19) -0.0011(16) 0.0078(16) 0.0042(16) C23 0.049(2) 0.056(3) 0.063(3) 0.008(2) 0.018(2) 0.0152(19) C24 0.046(2) 0.063(3) 0.076(3) -0.002(2) 0.026(2) 0.0105(19) C25 0.041(2) 0.054(2) 0.063(2) -0.0141(19) 0.0225(19) -0.0072(17) C26 0.061(3) 0.083(3) 0.071(3) -0.025(2) 0.036(2) -0.010(2) C27 0.070(3) 0.108(4) 0.052(3) -0.023(3) 0.029(2) -0.022(3) C28 0.064(3) 0.114(4) 0.048(3) -0.002(3) 0.018(2) 0.002(3) C29 0.054(2) 0.091(3) 0.040(2) 0.005(2) 0.0143(19) 0.008(2) C30 0.043(2) 0.050(2) 0.043(2) -0.0064(17) 0.0160(17) -0.0026(16) Cl1 0.0539(16) 0.0591(17) 0.0479(15) 0.0073(13) 0.0151(13) -0.0035(14) O3 0.063(3) 0.143(5) 0.067(3) 0.020(3) 0.006(3) 0.003(3) O4 0.099(5) 0.099(4) 0.103(5) 0.017(4) 0.049(4) -0.032(4) O5 0.127(5) 0.084(4) 0.086(4) -0.009(3) 0.019(4) 0.035(4) O6 0.056(4) 0.076(4) 0.054(3) -0.006(3) 0.013(3) -0.007(3) Cl1' 0.071(4) 0.074(4) 0.065(4) 0.005(4) 0.009(4) -0.008(4) O3' 0.078(7) 0.075(7) 0.060(6) -0.012(6) 0.013(6) -0.009(6) O4' 0.096(7) 0.094(6) 0.076(6) 0.032(6) -0.001(6) 0.007(6) O5' 0.050(7) 0.068(6) 0.061(6) 0.002(5) 0.028(6) 0.009(5) O6' 0.076(6) 0.109(7) 0.090(7) 0.009(6) 0.017(5) -0.015(6) Cl1" 0.070(4) 0.077(4) 0.068(4) 0.015(4) 0.010(4) -0.010(4) O3" 0.072(7) 0.083(7) 0.081(7) 0.013(6) 0.010(6) 0.003(6) O4" 0.074(7) 0.093(7) 0.071(7) 0.024(7) 0.014(6) -0.021(7) O5" 0.082(7) 0.078(7) 0.055(7) 0.002(6) 0.016(6) -0.013(6) O6" 0.068(8) 0.082(8) 0.061(7) 0.014(6) 0.011(6) -0.009(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N4 Zn1 N1 97.66(12) . . ? N4 Zn1 O2 158.94(12) . . ? N1 Zn1 O2 103.37(12) . . ? N4 Zn1 O1 102.69(12) . . ? N1 Zn1 O1 158.86(12) . . ? O2 Zn1 O1 56.29(11) . . ? N4 Zn1 N6 89.61(11) . . ? N1 Zn1 N6 98.14(11) . . ? O2 Zn1 N6 88.41(10) . . ? O1 Zn1 N6 87.75(10) . . ? N4 Zn1 N3 95.45(11) . . ? N1 Zn1 N3 87.25(11) . . ? O2 Zn1 N3 84.67(10) . . ? O1 Zn1 N3 85.19(10) . . ? N6 Zn1 N3 172.07(11) . . ? C1 N1 N2 106.0(3) . . ? C1 N1 Zn1 131.8(3) . . ? N2 N1 Zn1 119.2(2) . . ? C3 N2 N1 111.0(3) . . ? C3 N2 C6 129.6(3) . . ? N1 N2 C6 119.4(3) . . ? C7 N3 C14 119.1(3) . . ? C7 N3 Zn1 116.5(2) . . ? C14 N3 Zn1 124.2(2) . . ? C16 N4 N5 105.3(3) . . ? C16 N4 Zn1 133.7(3) . . ? N5 N4 Zn1 117.8(2) . . ? C18 N5 N4 112.1(3) . . ? C18 N5 C21 128.7(3) . . ? N4 N5 C21 119.2(3) . . ? C22 N6 C30 118.9(3) . . ? C22 N6 Zn1 116.9(2) . . ? C30 N6 Zn1 124.1(2) . . ? O1 N7 O2 112.3(3) . . ? N7 O1 Zn1 95.3(2) . . ? N7 O2 Zn1 96.1(2) . . ? N1 C1 C2 109.7(4) . . ? N1 C1 C4 122.2(4) . . ? C2 C1 C4 128.1(4) . . ? C3 C2 C1 106.9(4) . . ? C3 C2 H2 126.5 . . ? C1 C2 H2 126.5 . . ? N2 C3 C2 106.4(4) . . ? N2 C3 C5 122.5(4) . . ? C2 C3 C5 131.1(4) . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? N2 C6 C7 111.5(3) . . ? N2 C6 H6A 109.3 . . ? C7 C6 H6A 109.3 . . ? N2 C6 H6B 109.3 . . ? C7 C6 H6B 109.3 . . ? H6A C6 H6B 108.0 . . ? N3 C7 C8 122.5(4) . . ? N3 C7 C6 117.5(3) . . ? C8 C7 C6 120.0(4) . . ? C9 C8 C7 119.7(4) . . ? C9 C8 H8 120.1 . . ? C7 C8 H8 120.1 . . ? C8 C9 C15 119.1(4) . . ? C8 C9 H9 120.4 . . ? C15 C9 H9 120.4 . . ? C11 C10 C15 121.3(4) . . ? C11 C10 H10 119.4 . . ? C15 C10 H10 119.4 . . ? C10 C11 C12 120.0(4) . . ? C10 C11 H11 120.0 . . ? C12 C11 H11 120.0 . . ? C13 C12 C11 120.5(4) . . ? C13 C12 H12 119.8 . . ? C11 C12 H12 119.8 . . ? C12 C13 C14 120.9(4) . . ? C12 C13 H13 119.5 . . ? C14 C13 H13 119.5 . . ? N3 C14 C13 121.1(3) . . ? N3 C14 C15 120.4(4) . . ? C13 C14 C15 118.4(4) . . ? C9 C15 C10 122.1(4) . . ? C9 C15 C14 119.0(4) . . ? C10 C15 C14 118.8(4) . . ? N4 C16 C17 109.8(4) . . ? N4 C16 C19 122.6(3) . . ? C17 C16 C19 127.6(4) . . ? C18 C17 C16 107.6(4) . . ? C18 C17 H17 126.2 . . ? C16 C17 H17 126.2 . . ? N5 C18 C17 105.3(3) . . ? N5 C18 C20 123.1(4) . . ? C17 C18 C20 131.5(4) . . ? C16 C19 H19A 109.5 . . ? C16 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C16 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C18 C20 H20A 109.5 . . ? C18 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C18 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N5 C21 C22 112.7(3) . . ? N5 C21 H21A 109.1 . . ? C22 C21 H21A 109.1 . . ? N5 C21 H21B 109.1 . . ? C22 C21 H21B 109.1 . . ? H21A C21 H21B 107.8 . . ? N6 C22 C23 122.8(3) . . ? N6 C22 C21 117.7(3) . . ? C23 C22 C21 119.5(3) . . ? C24 C23 C22 119.1(4) . . ? C24 C23 H23 120.5 . . ? C22 C23 H23 120.5 . . ? C23 C24 C25 120.5(4) . . ? C23 C24 H24 119.7 . . ? C25 C24 H24 119.7 . . ? C24 C25 C30 117.7(4) . . ? C24 C25 C26 123.3(4) . . ? C30 C25 C26 119.0(4) . . ? C27 C26 C25 120.6(4) . . ? C27 C26 H26 119.7 . . ? C25 C26 H26 119.7 . . ? C26 C27 C28 120.3(4) . . ? C26 C27 H27 119.8 . . ? C28 C27 H27 119.8 . . ? C29 C28 C27 120.9(5) . . ? C29 C28 H28 119.5 . . ? C27 C28 H28 119.5 . . ? C28 C29 C30 120.9(4) . . ? C28 C29 H29 119.5 . . ? C30 C29 H29 119.5 . . ? N6 C30 C29 120.8(3) . . ? N6 C30 C25 120.9(3) . . ? C29 C30 C25 118.3(4) . . ? O5 Cl1 O4 109.6(5) . . ? O5 Cl1 O3 109.9(5) . . ? O4 Cl1 O3 109.7(5) . . ? O5 Cl1 O6 109.2(4) . . ? O4 Cl1 O6 108.5(5) . . ? O3 Cl1 O6 110.0(4) . . ? O4' Cl1' O5' 109.7(11) . . ? O4' Cl1' O6' 110.2(12) . . ? O5' Cl1' O6' 109.3(10) . . ? O4' Cl1' O3' 106.4(10) . . ? O5' Cl1' O3' 110.8(11) . . ? O6' Cl1' O3' 110.4(11) . . ? O4" Cl1" O5" 109.8(11) . . ? O4" Cl1" O6" 114.3(12) . . ? O5" Cl1" O6" 111.7(11) . . ? O4" Cl1" O3" 105.0(11) . . ? O5" Cl1" O3" 107.6(11) . . ? O6" Cl1" O3" 108.1(12) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 N4 2.064(3) . ? Zn1 N1 2.065(3) . ? Zn1 O2 2.186(3) . ? Zn1 O1 2.213(3) . ? Zn1 N6 2.278(3) . ? Zn1 N3 2.334(3) . ? N1 C1 1.334(5) . ? N1 N2 1.357(4) . ? N2 C3 1.340(5) . ? N2 C6 1.439(5) . ? N3 C7 1.321(4) . ? N3 C14 1.366(4) . ? N4 C16 1.338(5) . ? N4 N5 1.357(4) . ? N5 C18 1.349(5) . ? N5 C21 1.449(5) . ? N6 C22 1.309(4) . ? N6 C30 1.371(4) . ? N7 O1 1.241(4) . ? N7 O2 1.258(4) . ? C1 C2 1.374(6) . ? C1 C4 1.488(6) . ? C2 C3 1.371(6) . ? C2 H2 0.9500 . ? C3 C5 1.489(6) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.498(5) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C8 1.390(5) . ? C8 C9 1.362(6) . ? C8 H8 0.9500 . ? C9 C15 1.384(6) . ? C9 H9 0.9500 . ? C10 C11 1.328(6) . ? C10 C15 1.409(6) . ? C10 H10 0.9500 . ? C11 C12 1.406(6) . ? C11 H11 0.9500 . ? C12 C13 1.351(5) . ? C12 H12 0.9500 . ? C13 C14 1.395(5) . ? C13 H13 0.9500 . ? C14 C15 1.412(5) . ? C16 C17 1.377(5) . ? C16 C19 1.495(5) . ? C17 C18 1.370(6) . ? C17 H17 0.9500 . ? C18 C20 1.474(6) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C22 1.497(5) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C22 C23 1.411(5) . ? C23 C24 1.342(6) . ? C23 H23 0.9500 . ? C24 C25 1.392(6) . ? C24 H24 0.9500 . ? C25 C30 1.419(5) . ? C25 C26 1.421(6) . ? C26 C27 1.345(6) . ? C26 H26 0.9500 . ? C27 C28 1.400(6) . ? C27 H27 0.9500 . ? C28 C29 1.351(6) . ? C28 H28 0.9500 . ? C29 C30 1.407(5) . ? C29 H29 0.9500 . ? Cl1 O5 1.423(6) . ? Cl1 O4 1.424(6) . ? Cl1 O3 1.440(6) . ? Cl1 O6 1.441(6) . ? Cl1' O4' 1.417(9) . ? Cl1' O5' 1.420(9) . ? Cl1' O6' 1.431(10) . ? Cl1' O3' 1.442(10) . ? Cl1" O4" 1.420(9) . ? Cl1" O5" 1.422(9) . ? Cl1" O6" 1.427(9) . ? Cl1" O3" 1.445(10) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 N1 N2 C3 -0.5(4) . . . . ? Zn1 N1 N2 C3 162.0(3) . . . . ? C1 N1 N2 C6 -179.6(3) . . . . ? Zn1 N1 N2 C6 -17.1(4) . . . . ? C16 N4 N5 C18 -1.1(4) . . . . ? Zn1 N4 N5 C18 161.4(2) . . . . ? C16 N4 N5 C21 178.7(3) . . . . ? Zn1 N4 N5 C21 -18.9(4) . . . . ? O2 N7 O1 Zn1 -0.2(3) . . . . ? O1 N7 O2 Zn1 0.2(3) . . . . ? N2 N1 C1 C2 0.3(4) . . . . ? Zn1 N1 C1 C2 -159.1(3) . . . . ? N2 N1 C1 C4 -179.6(4) . . . . ? Zn1 N1 C1 C4 21.1(6) . . . . ? N1 C1 C2 C3 0.0(5) . . . . ? C4 C1 C2 C3 179.8(4) . . . . ? N1 N2 C3 C2 0.4(5) . . . . ? C6 N2 C3 C2 179.5(4) . . . . ? N1 N2 C3 C5 -179.6(4) . . . . ? C6 N2 C3 C5 -0.6(7) . . . . ? C1 C2 C3 N2 -0.2(5) . . . . ? C1 C2 C3 C5 179.8(5) . . . . ? C3 N2 C6 C7 -103.2(4) . . . . ? N1 N2 C6 C7 75.7(4) . . . . ? C14 N3 C7 C8 -0.1(5) . . . . ? Zn1 N3 C7 C8 -175.4(3) . . . . ? C14 N3 C7 C6 -179.9(3) . . . . ? Zn1 N3 C7 C6 4.8(4) . . . . ? N2 C6 C7 N3 -64.5(4) . . . . ? N2 C6 C7 C8 115.6(4) . . . . ? N3 C7 C8 C9 1.2(6) . . . . ? C6 C7 C8 C9 -178.9(4) . . . . ? C7 C8 C9 C15 -1.7(7) . . . . ? C15 C10 C11 C12 -1.9(7) . . . . ? C10 C11 C12 C13 0.6(7) . . . . ? C11 C12 C13 C14 1.2(6) . . . . ? C7 N3 C14 C13 179.3(3) . . . . ? Zn1 N3 C14 C13 -5.8(5) . . . . ? C7 N3 C14 C15 -0.6(5) . . . . ? Zn1 N3 C14 C15 174.3(3) . . . . ? C12 C13 C14 N3 178.5(3) . . . . ? C12 C13 C14 C15 -1.6(6) . . . . ? C8 C9 C15 C10 -179.1(4) . . . . ? C8 C9 C15 C14 1.0(6) . . . . ? C11 C10 C15 C9 -178.5(4) . . . . ? C11 C10 C15 C14 1.4(7) . . . . ? N3 C14 C15 C9 0.1(6) . . . . ? C13 C14 C15 C9 -179.8(4) . . . . ? N3 C14 C15 C10 -179.8(4) . . . . ? C13 C14 C15 C10 0.3(6) . . . . ? N5 N4 C16 C17 0.8(4) . . . . ? Zn1 N4 C16 C17 -157.6(3) . . . . ? N5 N4 C16 C19 -179.4(3) . . . . ? Zn1 N4 C16 C19 22.3(6) . . . . ? N4 C16 C17 C18 -0.3(5) . . . . ? C19 C16 C17 C18 179.9(4) . . . . ? N4 N5 C18 C17 0.9(4) . . . . ? C21 N5 C18 C17 -178.8(3) . . . . ? N4 N5 C18 C20 -179.5(4) . . . . ? C21 N5 C18 C20 0.8(6) . . . . ? C16 C17 C18 N5 -0.4(4) . . . . ? C16 C17 C18 C20 -179.9(4) . . . . ? C18 N5 C21 C22 -105.2(4) . . . . ? N4 N5 C21 C22 75.2(4) . . . . ? C30 N6 C22 C23 1.8(6) . . . . ? Zn1 N6 C22 C23 -175.1(3) . . . . ? C30 N6 C22 C21 -177.9(3) . . . . ? Zn1 N6 C22 C21 5.2(4) . . . . ? N5 C21 C22 N6 -63.8(4) . . . . ? N5 C21 C22 C23 116.5(4) . . . . ? N6 C22 C23 C24 -0.4(6) . . . . ? C21 C22 C23 C24 179.3(4) . . . . ? C22 C23 C24 C25 -1.0(7) . . . . ? C23 C24 C25 C30 1.0(6) . . . . ? C23 C24 C25 C26 -177.5(4) . . . . ? C24 C25 C26 C27 177.9(4) . . . . ? C30 C25 C26 C27 -0.7(6) . . . . ? C25 C26 C27 C28 1.1(7) . . . . ? C26 C27 C28 C29 -1.0(8) . . . . ? C27 C28 C29 C30 0.5(7) . . . . ? C22 N6 C30 C29 177.0(4) . . . . ? Zn1 N6 C30 C29 -6.3(5) . . . . ? C22 N6 C30 C25 -1.7(5) . . . . ? Zn1 N6 C30 C25 174.9(3) . . . . ? C28 C29 C30 N6 -178.9(4) . . . . ? C28 C29 C30 C25 -0.1(6) . . . . ? C24 C25 C30 N6 0.3(6) . . . . ? C26 C25 C30 N6 179.0(4) . . . . ? C24 C25 C30 C29 -178.4(4) . . . . ? C26 C25 C30 C29 0.2(6) . . . . ?