#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:34:55 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296381 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572760.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572760 loop_ _publ_author_name 'Anju, Balakrishnan S.' 'Nair, Neeraja R.' 'Rajput, Janavi' 'Bertke, Jeffery A.' 'Mondal, Bhaskar' 'Kundu, Subrata' _publ_section_title ; Role of ancillary ligands in S-nitrosothiol and NO generation from nitrite-thiol interactions at mononuclear zinc(ii) sites. ; _journal_issue 43 _journal_name_full 'Chemical science' _journal_page_first 18000 _journal_page_last 18007 _journal_paper_doi 10.1039/d4sc04853a _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C22 H32 Cl N8 O4 Zn, Cl O4, C2 H3 N' _chemical_formula_sum 'C24 H35 Cl2 N9 O8 Zn' _chemical_formula_weight 713.88 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary intrinsic _audit_creation_method SHELXL-2019/1 _audit_update_record ; 2024-05-16 deposited with the CCDC. 2024-10-03 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 18.1198(16) _cell_length_b 16.7592(14) _cell_length_c 20.9767(19) _cell_measurement_reflns_used 9981 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 23.80 _cell_measurement_theta_min 2.25 _cell_volume 6370.1(10) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELXL-2019/1 (Sheldrick, 2019)' _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device 'Bruker ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0831 _diffrn_reflns_av_unetI/netI 0.0528 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -24 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 90614 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.453 _diffrn_reflns_theta_min 1.919 _exptl_absorpt_coefficient_mu 0.998 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6286 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.489 _exptl_crystal_density_method 'not measured' _exptl_crystal_description needle _exptl_crystal_F_000 2960 _exptl_crystal_size_max 0.095 _exptl_crystal_size_mid 0.075 _exptl_crystal_size_min 0.045 _refine_diff_density_max 0.584 _refine_diff_density_min -0.687 _refine_diff_density_rms 0.093 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.145 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 668 _refine_ls_number_reflns 7981 _refine_ls_number_restraints 1268 _refine_ls_restrained_S_all 1.091 _refine_ls_R_factor_all 0.1002 _refine_ls_R_factor_gt 0.0695 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0290P)^2^+22.9143P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1398 _refine_ls_wR_factor_ref 0.1539 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5786 _reflns_number_total 7981 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc04853a2.cif _cod_data_source_block ABS1357 _cod_depositor_comments 'Adding full bibliography for 1572750--1572760.cif.' _cod_database_code 1572760 _shelx_shelxl_version_number 2019/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.911 _shelx_estimated_absorpt_t_max 0.956 _shelx_res_file ; TITL abs1357_a.res in Pbca ABS1357.res created by SHELXL-2019/1 at 14:41:39 on 15-Aug-2023 REM Old TITL ABS1357 in Pbca REM SHELXT solution in Pbca: R1 0.279, Rweak 0.027, Alpha 0.048 REM 1.130 for 638 systematic absences, Orientation a'=b, b'=a, c'=-c REM Formula found by SHELXT: C29 Cl2 N8 O4 Zn CELL 0.71073 18.1198 16.7592 20.9767 90 90 90 ZERR 8 0.0016 0.0014 0.0019 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Cl N O Zn UNIT 192 280 16 72 64 8 L.S. 20 0 0 PLAN 20 SIZE 0.045 0.075 0.095 SIMU 0.01 0.02 CL2 > O8C SUMP 1.00 0.00001 1 4 1 5 1 6 SIMU 0.01 0.02 N9 > C24B SIMU 0.01 0.02 N1 > C11B RIGU N1 > C11B SADI 0.02 ZN1 N1 ZN1 N1B ZN1 N3 ZN1 N3B TEMP -123.15 BOND $H LIST 4 FMAP 2 53 ACTA WGHT 0.029000 22.914299 FVAR 0.16249 0.54530 0.61990 0.37306 0.34488 0.28206 ZN1 6 0.736072 0.643570 0.518162 11.00000 0.03246 0.01959 = 0.03386 -0.01107 0.02031 -0.00537 CL1 3 0.728040 0.793245 0.433534 11.00000 0.04872 0.01916 = 0.03740 -0.00545 0.01936 -0.00855 O1 5 0.673634 0.765179 0.478688 11.00000 0.05305 0.03135 = 0.03017 -0.00095 0.01724 -0.00718 O2 5 0.701396 0.782795 0.370004 11.00000 0.08583 0.04228 = 0.02860 -0.00827 0.02207 -0.01187 O3 5 0.744542 0.875451 0.444928 11.00000 0.05288 0.01952 = 0.06085 -0.00627 0.01506 -0.00576 O4 5 0.793532 0.745616 0.443002 11.00000 0.04403 0.02316 = 0.08402 -0.01127 0.01757 0.00039 PART 1 21 N1 4 0.769093 0.721328 0.590537 21.00000 0.02423 0.01630 = 0.03497 -0.00705 0.01115 -0.00367 N2 4 0.718022 0.745667 0.634904 21.00000 0.02411 0.01435 = 0.02472 -0.00573 0.00784 -0.00192 N3 4 0.655692 0.594744 0.577528 21.00000 0.02745 0.01653 = 0.02809 -0.01210 0.01504 -0.00293 N4 4 0.632664 0.638768 0.628353 21.00000 0.01857 0.01216 = 0.02330 -0.00747 0.00490 0.00040 C1 1 0.834445 0.747353 0.611275 21.00000 0.02575 0.02000 = 0.04091 -0.00477 0.01163 -0.00525 C2 1 0.824929 0.788802 0.667661 21.00000 0.02987 0.02104 = 0.03964 -0.00714 0.00493 -0.00305 AFIX 43 H2 2 0.862616 0.814155 0.691763 21.00000 -1.20000 AFIX 0 C3 1 0.751909 0.786719 0.682377 21.00000 0.03025 0.01504 = 0.03067 -0.00517 0.00358 -0.00080 C4 1 0.903671 0.733641 0.575130 21.00000 0.03248 0.03673 = 0.07100 -0.01495 0.02219 -0.00746 AFIX 137 H4A 2 0.943153 0.718622 0.604718 21.00000 -1.50000 H4B 2 0.917536 0.782631 0.552609 21.00000 -1.50000 H4C 2 0.896050 0.690611 0.544187 21.00000 -1.50000 AFIX 0 C5 1 0.710118 0.820252 0.737957 21.00000 0.04060 0.03342 = 0.02918 -0.01411 -0.00074 0.00343 AFIX 137 H5A 2 0.676365 0.861930 0.722998 21.00000 -1.50000 H5B 2 0.744915 0.843130 0.768698 21.00000 -1.50000 H5C 2 0.681761 0.777610 0.758498 21.00000 -1.50000 AFIX 0 C6 1 0.641414 0.723732 0.626700 21.00000 0.01837 0.01468 = 0.02018 -0.00584 0.00408 0.00032 AFIX 23 H6A 2 0.611519 0.748197 0.661029 21.00000 -1.20000 H6B 2 0.623289 0.744475 0.585377 21.00000 -1.20000 AFIX 0 C7 1 0.637554 0.519137 0.590557 21.00000 0.02585 0.01710 = 0.03320 -0.00983 0.01450 -0.00372 C8 1 0.603782 0.515497 0.650100 21.00000 0.01959 0.01654 = 0.03088 -0.00679 0.00788 -0.00035 AFIX 43 H8 2 0.585981 0.468891 0.670791 21.00000 -1.20000 AFIX 0 C9 1 0.601146 0.590696 0.672808 21.00000 0.01405 0.01515 = 0.02148 -0.00392 0.00157 0.00183 C10 1 0.653388 0.453306 0.545245 21.00000 0.05812 0.01638 = 0.04946 -0.01795 0.03776 -0.01334 AFIX 137 H10A 2 0.650654 0.473518 0.501470 21.00000 -1.50000 H10B 2 0.616992 0.410654 0.550991 21.00000 -1.50000 H10C 2 0.702974 0.432279 0.553356 21.00000 -1.50000 AFIX 0 C11 1 0.573500 0.624583 0.735177 21.00000 0.03189 0.02286 = 0.02306 -0.00572 0.00062 0.00666 AFIX 137 H11A 2 0.615433 0.643787 0.760380 21.00000 -1.50000 H11B 2 0.547392 0.582930 0.758981 21.00000 -1.50000 H11C 2 0.539751 0.668999 0.726604 21.00000 -1.50000 AFIX 0 PART 2 -21 SAME 0.01 N1 > C11 N1B 4 0.781621 0.726364 0.580074 -21.00000 0.03115 0.01609 = 0.02662 -0.00174 0.01181 -0.00209 N2B 4 0.739810 0.752674 0.630340 -21.00000 0.02900 0.01628 = 0.02539 -0.00212 0.00729 -0.00046 N3B 4 0.654834 0.612128 0.580739 -21.00000 0.02790 0.01565 = 0.02733 -0.00420 0.01207 -0.00016 N4B 4 0.640004 0.660685 0.631042 -21.00000 0.02004 0.01592 = 0.01812 -0.00209 0.00659 0.00388 C1B 1 0.851538 0.742900 0.595290 -21.00000 0.03383 0.01731 = 0.02928 -0.00398 0.01409 -0.00630 C2B 1 0.853360 0.778928 0.654803 -21.00000 0.03237 0.02222 = 0.03017 -0.00401 0.01372 -0.00519 AFIX 43 H2B 2 0.896414 0.796486 0.676508 -21.00000 -1.20000 AFIX 0 C3B 1 0.782977 0.784804 0.676743 -21.00000 0.03157 0.01858 = 0.02590 -0.00259 0.01145 -0.00265 C4B 1 0.913564 0.726033 0.551253 -21.00000 0.03380 0.03603 = 0.02745 -0.01369 0.01357 -0.01024 AFIX 137 H4D 2 0.917084 0.668380 0.544063 -21.00000 -1.50000 H4E 2 0.959721 0.745427 0.570036 -21.00000 -1.50000 H4F 2 0.904902 0.753139 0.510539 -21.00000 -1.50000 AFIX 0 C5B 1 0.749959 0.819852 0.735651 -21.00000 0.04786 0.03346 = 0.02614 -0.00608 0.00721 0.00257 AFIX 137 H5D 2 0.712465 0.859302 0.723808 -21.00000 -1.50000 H5E 2 0.788690 0.845821 0.760807 -21.00000 -1.50000 H5F 2 0.727051 0.777432 0.760999 -21.00000 -1.50000 AFIX 0 C6B 1 0.660431 0.743292 0.627204 -21.00000 0.02779 0.01425 = 0.01978 -0.00033 0.00541 0.00231 AFIX 23 H6C 2 0.637238 0.772966 0.662756 -21.00000 -1.20000 H6D 2 0.641964 0.766064 0.586684 -21.00000 -1.20000 AFIX 0 C7B 1 0.627515 0.540269 0.595150 -21.00000 0.02362 0.01534 = 0.02996 -0.00385 0.00834 0.00271 C8B 1 0.595163 0.543777 0.655381 -21.00000 0.02148 0.01773 = 0.02635 -0.00123 0.00628 0.00091 AFIX 43 H8B 2 0.571719 0.501105 0.677259 -21.00000 -1.20000 AFIX 0 C9B 1 0.603407 0.619130 0.676739 -21.00000 0.01621 0.01995 = 0.02068 0.00040 -0.00058 0.00262 C10B 1 0.636080 0.470706 0.551911 -21.00000 0.03551 0.01981 = 0.04996 -0.00714 0.02382 -0.00260 AFIX 137 H10D 2 0.591796 0.465273 0.525444 -21.00000 -1.50000 H10E 2 0.642877 0.422153 0.577276 -21.00000 -1.50000 H10F 2 0.679219 0.478792 0.524483 -21.00000 -1.50000 AFIX 0 C11B 1 0.578326 0.658411 0.737989 -21.00000 0.02860 0.04097 = 0.01595 -0.00112 0.00590 0.00180 AFIX 137 H11D 2 0.621337 0.669806 0.764810 -21.00000 -1.50000 H11E 2 0.544752 0.622514 0.760770 -21.00000 -1.50000 H11F 2 0.552649 0.708349 0.728045 -21.00000 -1.50000 AFIX 0 PART 0 N5 4 0.705249 0.597301 0.431446 11.00000 0.03707 0.01945 = 0.03657 -0.00740 0.02539 -0.00535 N6 4 0.756181 0.557783 0.395407 11.00000 0.03849 0.01954 = 0.02889 -0.00537 0.01864 -0.00171 N7 4 0.820255 0.559824 0.525318 11.00000 0.03417 0.02110 = 0.04206 -0.01096 0.02237 -0.00441 N8 4 0.851376 0.529438 0.471499 11.00000 0.02804 0.03267 = 0.04246 -0.02222 0.01892 -0.00660 C12 1 0.640386 0.584038 0.403382 11.00000 0.03985 0.02008 = 0.03551 0.00143 0.01270 -0.00527 C13 1 0.650559 0.536144 0.349576 11.00000 0.04822 0.02073 = 0.03017 0.00122 0.00864 0.00074 AFIX 43 H13 2 0.613212 0.518071 0.321259 11.00000 -1.20000 AFIX 0 C14 1 0.723946 0.520288 0.345385 11.00000 0.05824 0.01685 = 0.02298 0.00187 0.01577 0.00281 C15 1 0.570391 0.616734 0.428499 11.00000 0.03554 0.05708 = 0.05013 -0.00879 0.01470 -0.00027 AFIX 137 H15A 2 0.537273 0.572755 0.439884 11.00000 -1.50000 H15B 2 0.546973 0.650023 0.395848 11.00000 -1.50000 H15C 2 0.580537 0.649095 0.466412 11.00000 -1.50000 AFIX 0 C16 1 0.767363 0.472212 0.298810 11.00000 0.07681 0.03991 = 0.02305 -0.00765 0.00556 0.01880 AFIX 137 H16A 2 0.806060 0.505578 0.279978 11.00000 -1.50000 H16B 2 0.734567 0.452700 0.265090 11.00000 -1.50000 H16C 2 0.790003 0.426754 0.320745 11.00000 -1.50000 AFIX 0 C17 1 0.833612 0.565656 0.411038 11.00000 0.04168 0.02674 = 0.04546 -0.01525 0.03067 -0.00905 AFIX 23 H17A 2 0.863498 0.540249 0.377142 11.00000 -1.20000 H17B 2 0.846753 0.622967 0.412442 11.00000 -1.20000 AFIX 0 C18 1 0.846253 0.515148 0.573153 11.00000 0.02586 0.02766 = 0.04995 -0.01366 0.00834 -0.00609 C19 1 0.893953 0.456987 0.550177 11.00000 0.02356 0.04654 = 0.05813 -0.02947 -0.00847 0.00477 AFIX 43 H19 2 0.919912 0.418254 0.574478 11.00000 -1.20000 AFIX 0 C20 1 0.895969 0.466810 0.485371 11.00000 0.01378 0.04475 = 0.06998 -0.03705 0.00252 0.00159 C21 1 0.823907 0.529912 0.640231 11.00000 0.04824 0.04120 = 0.04858 -0.00245 0.01339 0.00606 AFIX 137 H21A 2 0.819783 0.587493 0.647551 11.00000 -1.50000 H21B 2 0.861076 0.507488 0.669055 11.00000 -1.50000 H21C 2 0.776114 0.504498 0.648356 11.00000 -1.50000 AFIX 0 C22 1 0.937854 0.421236 0.435536 11.00000 0.02259 0.07994 = 0.07487 -0.05015 -0.00064 0.01386 AFIX 137 H22A 2 0.902986 0.394217 0.407085 11.00000 -1.50000 H22B 2 0.969522 0.381527 0.456219 11.00000 -1.50000 H22C 2 0.968405 0.458204 0.410760 11.00000 -1.50000 AFIX 0 PART 1 41 CL2 3 0.508011 0.384589 0.801486 41.00000 0.01311 0.02346 = 0.04940 -0.00125 0.00512 -0.00284 O5 5 0.508552 0.356479 0.864711 41.00000 0.02567 0.05351 = 0.04341 0.01277 0.00720 -0.00015 O6 5 0.478632 0.323757 0.760464 41.00000 0.05364 0.05859 = 0.05388 -0.00602 -0.00035 -0.03262 O7 5 0.464309 0.455726 0.794861 41.00000 0.04268 0.04346 = 0.06645 0.00801 0.00784 0.01802 O8 5 0.581783 0.401917 0.780866 41.00000 0.01840 0.05700 = 0.04580 0.00504 -0.00003 -0.00536 PART 2 51 SAME 0.01 CL2 > O8 CL2B 3 0.509272 0.393672 0.778554 51.00000 0.02125 0.02475 = 0.02943 -0.00746 0.01125 -0.00845 O5B 5 0.441559 0.363871 0.801845 51.00000 0.02959 0.04473 = 0.04798 -0.00432 0.01785 -0.01842 O6B 5 0.510005 0.383974 0.711091 51.00000 0.04103 0.04923 = 0.02712 0.00537 0.00151 -0.00307 O7B 5 0.516534 0.475856 0.797384 51.00000 0.04355 0.03242 = 0.05693 -0.01249 0.00329 -0.01059 O8B 5 0.571595 0.352430 0.804495 51.00000 0.03453 0.06614 = 0.04991 0.00146 -0.01066 0.01095 PART 3 61 SAME 0.01 CL2 > O8 CL2C 3 0.508253 0.386036 0.776888 61.00000 0.01869 0.03070 = 0.03548 0.00424 0.00500 -0.00196 O5C 5 0.484836 0.346780 0.833113 61.00000 0.05013 0.04805 = 0.04844 0.00932 0.01433 -0.01641 O6C 5 0.490223 0.336654 0.723452 61.00000 0.03448 0.05836 = 0.04976 -0.01344 0.00064 -0.00915 O7C 5 0.472663 0.462077 0.769018 61.00000 0.03405 0.04839 = 0.04423 0.00431 0.01598 0.01078 O8C 5 0.586615 0.396832 0.777397 61.00000 0.01935 0.04740 = 0.04289 -0.00012 0.00313 -0.00268 PART 0 PART 1 31 N9 4 0.966179 0.852584 0.423528 31.00000 0.05715 0.12136 = 0.06368 0.01728 -0.00123 -0.03842 C23 1 0.933561 0.837288 0.381947 31.00000 0.03021 0.08993 = 0.04599 0.01402 0.00281 -0.00965 C24 1 0.888309 0.821009 0.324612 31.00000 0.03030 0.07490 = 0.04709 0.00577 0.00717 0.01395 AFIX 137 H24A 2 0.907513 0.851829 0.288542 31.00000 -1.50000 H24B 2 0.837024 0.836463 0.332838 31.00000 -1.50000 H24C 2 0.890446 0.763962 0.314517 31.00000 -1.50000 AFIX 0 PART 2 -31 SAME 0.01 N9 > C24 N9B 4 1.001173 0.752365 0.439135 -31.00000 0.04108 0.10852 = 0.05365 -0.00807 0.00701 -0.00812 C23B 1 0.964227 0.785910 0.408333 -31.00000 0.02951 0.08289 = 0.04795 0.00671 0.01747 -0.00012 C24B 1 0.915075 0.828793 0.363575 -31.00000 0.03297 0.07700 = 0.05750 0.02367 0.01755 0.00167 AFIX 137 H24D 2 0.944898 0.856030 0.331242 -31.00000 -1.50000 H24E 2 0.885794 0.868168 0.387096 -31.00000 -1.50000 H24F 2 0.881992 0.790571 0.342755 -31.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM abs1357_a.res in Pbca REM wR2 = 0.1539, GooF = S = 1.145, Restrained GooF = 1.091 for all data REM R1 = 0.0695 for 5786 Fo > 4sig(Fo) and 0.1002 for all 7981 data REM 668 parameters refined using 1268 restraints END WGHT 0.0290 22.9145 REM Highest difference peak 0.584, deepest hole -0.687, 1-sigma level 0.093 Q1 1 0.7458 0.5926 0.5300 11.00000 0.05 0.58 Q2 1 0.7138 0.6391 0.4400 11.00000 0.05 0.50 Q3 1 0.7365 0.6957 0.5216 11.00000 0.05 0.49 Q4 1 0.7019 0.6412 0.5583 11.00000 0.05 0.48 Q5 1 0.7336 0.6158 0.4790 11.00000 0.05 0.46 Q6 1 0.6778 0.7959 0.4414 11.00000 0.05 0.44 Q7 1 0.7769 0.6583 0.4934 11.00000 0.05 0.42 Q8 1 0.6992 0.6368 0.5046 11.00000 0.05 0.41 Q9 1 0.5336 0.6012 0.4017 11.00000 0.05 0.41 Q10 1 0.5592 0.3488 0.7599 11.00000 0.05 0.39 Q11 1 0.8226 0.7632 0.6407 11.00000 0.05 0.39 Q12 1 0.7600 0.7401 0.4410 11.00000 0.05 0.38 Q13 1 0.9416 0.4015 0.4386 11.00000 0.05 0.36 Q14 1 0.9460 0.4604 0.4146 11.00000 0.05 0.36 Q15 1 0.8974 0.5021 0.4636 11.00000 0.05 0.34 Q16 1 0.9046 0.4798 0.5198 11.00000 0.05 0.34 Q17 1 0.7799 0.5601 0.6557 11.00000 0.05 0.33 Q18 1 0.7340 0.5839 0.4158 11.00000 0.05 0.33 Q19 1 0.7554 0.6796 0.5615 11.00000 0.05 0.33 Q20 1 0.4391 0.3837 0.7637 11.00000 0.05 0.32 ; _shelx_res_checksum 45746 _shelx_hkl_file ; 0 1 0 0.10 0.20 0 1 0 -0.10 0.20 0 1 0 -0.20 0.20 0 -1 0 0.30 0.40 0 -1 0 0.90 0.40 0 -1 0 0.40 0.40 0 -2 0 61.79 5.70 0 -2 0 66.19 5.80 0 -3 0 1.60 1.40 0 -3 0 -1.10 1.00 0 3 0 0.50 1.00 0 3 0 0.90 1.10 0 3 0 -0.10 0.80 0 -3 0 0.00 1.10 0 -4 0 33.70 4.00 0 4 0 35.40 4.00 0 -4 0 30.20 4.00 0 4 0 38.00 4.10 0 4 0 32.90 4.20 0 -4 0 41.70 4.60 0 5 0 0.60 1.60 0 -5 0 -0.70 1.70 0 5 0 -0.40 1.60 0 5 0 4.40 2.20 0 -5 0 2.60 1.90 0 -5 0 0.20 2.00 0 6 0 245.08 20.00 0 -6 0 211.58 20.00 0 6 0 227.68 19.40 0 6 0 249.97 20.00 0 6 0 214.48 20.10 0 -6 0 237.08 20.10 0 -6 0 219.98 20.30 0 7 0 7.60 2.00 0 7 0 4.30 2.90 0 7 0 -0.90 2.00 0 -7 0 10.90 3.00 0 7 0 4.70 1.70 0 -7 0 11.90 4.10 0 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338.07 28.00 8 4 0 332.67 27.60 8 4 0 330.47 27.60 -8 5 0 48.00 5.90 -8 -5 0 41.70 5.30 -8 -5 0 51.59 6.30 -8 5 0 40.60 5.40 -8 5 0 46.10 6.10 -8 -5 0 51.09 7.50 8 5 0 51.89 5.70 8 -5 0 55.29 6.60 8 5 0 51.69 5.60 -8 -6 0 422.56 36.70 -8 6 0 454.05 37.20 -8 6 0 420.06 36.80 -8 6 0 437.36 37.00 -8 -6 0 466.15 38.40 8 6 0 450.95 36.90 8 -6 0 413.06 37.10 8 -6 0 430.66 37.40 8 6 0 435.56 36.70 -8 7 0 149.49 14.40 -8 -7 0 162.78 14.00 -8 7 0 161.08 14.10 -8 -7 0 151.38 15.80 -8 7 0 145.99 14.20 8 -7 0 168.58 14.80 8 -7 0 154.88 15.10 8 -7 0 163.48 13.60 8 7 0 150.48 14.20 8 7 0 151.78 13.90 -8 8 0 239.98 21.40 -8 -8 0 243.28 23.10 -8 -8 0 244.78 20.90 -8 8 0 244.88 21.20 -8 8 0 241.88 21.50 8 8 0 240.68 20.30 8 -8 0 224.38 22.00 8 8 0 246.48 20.90 8 -8 0 241.68 20.90 8 8 0 246.98 20.20 8 -8 0 245.08 21.90 -8 9 0 253.67 22.30 -8 -9 0 236.08 23.90 -8 -9 0 247.08 21.30 -8 9 0 245.18 22.10 -8 9 0 244.28 21.60 8 -9 0 250.17 21.70 8 9 0 244.38 21.40 8 9 0 247.28 20.80 8 -9 0 254.17 22.60 8 -9 0 260.57 23.00 -8 10 0 54.69 7.10 -8 10 0 45.80 6.80 -8 10 0 52.99 6.10 -8 -10 0 50.09 5.60 -8 -10 0 66.69 10.50 8 10 0 58.99 5.90 8 10 0 46.20 5.00 8 -10 0 57.59 6.90 8 -10 0 56.99 7.70 8 -10 0 49.80 7.90 -8 -11 0 205.58 21.10 -8 11 0 194.58 18.60 -8 11 0 219.38 18.60 -8 11 0 194.18 17.80 8 -11 0 219.18 19.90 8 -11 0 205.68 19.40 8 11 0 192.48 17.50 8 -11 0 199.38 18.50 8 11 0 196.98 17.10 -8 12 0 244.08 21.10 -8 12 0 201.98 20.80 -8 -12 0 224.68 23.20 -8 12 0 213.28 19.90 8 -12 0 220.28 21.70 8 -12 0 261.27 22.50 8 12 0 242.68 19.80 8 -12 0 226.58 21.00 8 12 0 221.58 19.40 -8 13 0 67.79 7.50 -8 13 0 77.29 9.70 -8 -13 0 63.79 12.30 -8 13 0 69.09 8.80 8 -13 0 61.89 9.90 8 -13 0 64.59 10.20 8 -13 0 81.59 9.50 8 13 0 58.89 6.70 -8 14 0 29.10 4.50 -8 14 0 27.70 6.30 -8 14 0 28.80 6.70 -8 -14 0 26.10 9.80 8 -14 0 25.80 7.10 8 -14 0 45.40 8.80 8 -14 0 26.00 6.80 8 14 0 32.10 4.60 -8 15 0 74.09 7.60 -8 -15 0 55.59 13.20 -8 15 0 60.29 9.20 -8 15 0 61.69 9.10 8 -15 0 62.59 10.10 8 15 0 68.89 8.00 8 -15 0 72.39 10.80 8 -15 0 53.49 10.70 -8 16 0 37.80 7.70 -8 16 0 38.90 7.50 -8 -16 0 25.60 11.10 -8 16 0 33.20 4.90 8 -16 0 31.90 8.70 8 -16 0 39.50 8.90 -8 -17 0 18.00 11.60 -8 17 0 46.10 8.20 -8 17 0 46.40 8.30 8 -17 0 37.50 9.30 8 -17 0 37.30 9.50 -8 18 0 23.70 6.90 -8 -18 0 27.10 12.40 -8 18 0 12.20 6.80 8 -18 0 29.20 8.80 8 -18 0 24.40 9.40 -8 -19 0 52.09 13.70 -8 19 0 34.60 8.30 -8 19 0 29.00 7.80 8 -19 0 23.50 9.80 8 -19 0 42.00 10.30 -8 20 0 6.30 6.40 -8 20 0 9.20 6.50 -8 -20 0 4.00 11.10 8 -20 0 11.80 8.60 8 -20 0 11.40 8.70 -8 21 0 66.49 11.50 -8 21 0 49.99 10.30 8 -21 0 67.59 14.30 8 -21 0 56.39 13.00 -9 3 0 2.10 2.60 -9 -3 0 6.60 2.60 -9 4 0 3.20 2.90 -9 -4 0 5.90 3.40 -9 4 0 5.10 2.20 -9 4 0 5.20 2.40 -9 -4 0 -3.30 2.30 9 4 0 -4.10 2.00 9 4 0 6.30 2.10 -9 -5 0 15.30 4.40 -9 5 0 8.20 3.20 -9 -5 0 4.40 3.00 -9 -6 0 10.40 4.40 -9 6 0 12.20 3.20 -9 6 0 0.70 2.90 -9 6 0 2.70 2.20 -9 -6 0 8.00 2.40 9 -6 0 -2.50 2.70 9 -6 0 4.30 2.90 9 6 0 6.70 2.10 -9 7 0 3.00 2.90 -9 7 0 2.90 2.30 -9 -7 0 2.40 2.40 -9 7 0 11.80 3.70 -9 -7 0 10.50 5.00 9 7 0 2.90 2.20 9 -7 0 -0.10 3.10 9 -7 0 -0.20 3.30 -9 8 0 7.50 3.80 -9 8 0 6.30 2.70 -9 -8 0 2.60 2.40 -9 -8 0 13.10 5.50 -9 8 0 2.60 3.40 9 8 0 5.90 2.30 9 -8 0 2.60 3.40 9 -8 0 0.60 3.80 -9 9 0 14.20 4.40 -9 9 0 9.20 4.10 -9 9 0 6.90 2.70 -9 -9 0 6.80 2.70 -9 -9 0 6.00 5.60 9 -9 0 3.20 4.20 9 9 0 5.60 2.40 9 -9 0 11.60 4.20 -9 10 0 0.90 3.60 -9 -10 0 11.70 6.50 -9 10 0 9.50 4.20 -9 -10 0 6.70 2.60 -9 10 0 10.90 2.80 9 -10 0 13.70 5.00 9 -10 0 5.40 3.20 9 10 0 5.50 1.50 9 10 0 4.10 1.70 9 -10 0 3.30 4.10 9 10 0 3.40 2.10 -9 11 0 13.20 4.50 -9 11 0 1.70 3.90 -9 -11 0 20.20 7.10 -9 -11 0 5.50 2.40 9 11 0 0.80 1.70 9 -11 0 8.70 3.80 9 -11 0 11.20 5.10 9 11 0 5.90 2.20 9 -11 0 4.10 4.70 -9 12 0 4.30 2.60 -9 -12 0 12.70 7.10 -9 12 0 3.80 4.40 -9 12 0 3.50 4.20 9 12 0 1.00 1.90 9 -12 0 -0.10 4.50 9 -12 0 5.90 5.30 -9 -13 0 15.20 7.60 -9 13 0 -1.20 3.90 -9 13 0 1.60 2.60 -9 13 0 2.20 4.00 9 -13 0 0.10 4.80 9 13 0 -0.20 2.10 9 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4.70 -10 2 0 30.70 5.00 -10 -2 0 29.70 3.40 -10 2 0 25.20 4.40 -10 2 0 31.80 4.30 10 -2 0 33.50 3.80 10 2 0 42.20 5.70 -10 3 0 85.09 8.80 -10 3 0 85.09 8.20 -10 3 0 82.29 8.90 -10 -3 0 90.69 8.80 -10 -3 0 91.59 9.50 -10 -3 0 70.49 9.10 -10 -4 0 20.70 4.40 -10 -4 0 25.90 5.70 -10 4 0 28.60 4.40 -10 -4 0 23.60 4.10 -10 4 0 21.50 4.40 -10 4 0 24.60 4.30 10 -4 0 23.80 4.70 -10 -5 0 24.30 5.60 -10 5 0 27.60 4.50 -10 5 0 20.60 3.90 -10 -5 0 27.80 4.70 -10 -5 0 21.20 4.20 -10 5 0 17.30 4.20 10 -5 0 23.70 4.90 10 5 0 25.00 4.10 -10 -6 0 155.78 14.90 -10 6 0 154.98 14.80 -10 -6 0 160.78 14.40 -10 6 0 160.98 14.50 -10 -6 0 159.58 16.10 -10 6 0 155.58 14.50 10 -6 0 145.99 14.80 10 6 0 155.98 14.30 -10 -7 0 393.06 35.60 -10 7 0 384.66 33.90 -10 7 0 396.36 34.10 -10 -7 0 406.36 33.90 -10 7 0 397.06 34.40 10 -7 0 395.86 34.40 10 7 0 393.06 33.80 10 -7 0 403.06 34.70 -10 8 0 0.90 2.70 -10 8 0 -4.10 3.50 -10 8 0 -2.90 3.10 -10 -8 0 0.60 2.80 -10 -8 0 -3.50 4.70 10 8 0 0.50 2.30 10 -8 0 -3.60 3.30 10 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16 0 10.90 6.00 -10 16 0 9.70 3.80 -10 -16 0 6.60 8.70 -10 16 0 12.70 6.00 10 -16 0 5.80 6.70 10 -16 0 -3.60 6.40 -10 -17 0 24.10 11.60 -10 17 0 20.40 4.40 -10 17 0 20.10 6.60 -10 17 0 20.80 6.50 10 -17 0 11.20 7.60 10 -17 0 31.80 9.50 -10 18 0 62.79 10.20 -10 18 0 68.29 11.00 -10 -18 0 37.00 14.00 10 -18 0 54.19 11.40 10 -18 0 66.29 12.50 -10 19 0 107.89 14.30 -10 -19 0 149.88 21.30 -10 19 0 98.59 14.40 10 -19 0 117.19 17.70 10 -19 0 109.39 16.30 -10 20 0 2.50 6.60 -10 20 0 7.10 6.50 10 -20 0 10.70 9.10 10 -20 0 1.80 8.10 -11 2 0 10.30 3.00 -11 -2 0 8.40 3.10 -11 2 0 5.90 3.30 -11 -2 0 13.00 3.20 -11 -3 0 4.20 3.20 -11 -3 0 4.30 1.20 -11 3 0 1.20 3.20 -11 3 0 2.20 2.90 -11 -3 0 4.90 3.00 -11 3 0 10.10 2.90 -11 4 0 14.50 3.80 -11 5 0 0.60 2.90 -11 -5 0 -0.40 2.80 -11 5 0 -4.60 3.20 -11 5 0 1.80 3.00 -11 -5 0 -0.70 3.00 -11 -5 0 -2.60 4.00 11 -5 0 -0.50 3.20 -11 -6 0 6.30 3.60 -11 6 0 11.60 4.20 -11 7 0 1.40 3.00 -11 7 0 -0.50 3.60 -11 -7 0 -0.60 4.40 -11 -7 0 -0.40 3.00 -11 7 0 0.00 3.70 11 -7 0 -1.80 3.10 11 -7 0 -2.70 3.30 11 7 0 -0.80 2.50 -11 -8 0 8.40 3.30 -11 -8 0 9.60 5.70 -11 8 0 12.30 3.50 -11 8 0 13.20 4.30 -11 8 0 4.50 4.10 11 -8 0 -1.10 3.70 11 8 0 6.30 2.80 11 -8 0 5.40 3.90 -11 -9 0 -1.60 4.90 -11 9 0 -4.60 3.90 -11 9 0 -7.00 3.30 -11 -9 0 2.40 3.20 -11 9 0 0.60 2.90 11 -9 0 -7.30 3.90 11 9 0 1.30 2.70 11 -9 0 0.10 3.80 -11 10 0 0.60 3.80 -11 -10 0 0.40 6.50 -11 10 0 2.10 3.20 -11 10 0 5.80 4.60 -11 -10 0 1.00 3.20 11 -10 0 -0.70 4.90 11 -10 0 3.70 4.40 -11 -11 0 31.60 8.50 -11 11 0 14.40 3.70 -11 11 0 9.00 5.00 -11 11 0 10.60 5.20 11 -11 0 11.90 5.00 11 -11 0 20.80 6.20 -11 12 0 -0.80 2.90 -11 12 0 0.10 4.60 -11 12 0 8.30 4.80 -11 -12 0 3.70 7.40 11 -12 0 -0.80 4.60 11 -12 0 0.50 5.30 -11 -13 0 13.90 8.60 -11 13 0 9.40 5.30 -11 13 0 13.50 3.70 -11 13 0 4.80 5.50 11 -13 0 10.80 6.00 11 -13 0 8.80 5.30 -11 -14 0 6.70 7.70 -11 14 0 4.30 5.40 -11 14 0 8.80 3.50 -11 14 0 4.00 5.10 11 -14 0 1.50 5.40 11 -14 0 12.60 6.60 -11 -15 0 -6.10 8.50 -11 15 0 -4.00 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112.89 10.00 -12 3 0 115.99 11.90 -12 3 0 114.99 11.10 -12 -4 0 333.17 29.60 -12 4 0 330.67 29.50 -12 4 0 332.67 29.60 -12 -4 0 343.37 29.40 -12 4 0 357.26 29.10 12 -4 0 319.17 29.60 -12 5 0 423.86 37.80 -12 5 0 444.16 37.50 -12 -5 0 467.65 39.10 -12 -5 0 441.26 38.00 -12 -5 0 450.25 37.70 -12 5 0 405.16 37.80 12 -5 0 448.56 38.20 -12 6 0 4.10 3.10 -12 -6 0 8.30 4.20 -12 6 0 5.00 3.80 -12 6 0 6.70 4.30 -12 -6 0 10.10 3.70 -12 -6 0 6.10 4.90 12 -6 0 6.80 4.20 -12 7 0 127.09 13.10 -12 7 0 113.09 11.80 -12 7 0 109.59 11.60 -12 -7 0 128.29 15.00 -12 -7 0 98.69 11.50 12 -7 0 114.59 12.80 12 -7 0 111.59 12.30 -12 8 0 136.89 13.20 -12 -8 0 160.28 17.30 -12 8 0 122.59 13.30 -12 8 0 125.69 13.70 -12 -8 0 138.59 13.30 12 -8 0 154.18 15.60 12 -8 0 115.79 13.30 -12 9 0 43.40 6.20 -12 -9 0 30.10 5.50 -12 9 0 32.30 6.70 -12 -9 0 42.70 9.30 -12 9 0 29.50 6.10 12 -9 0 40.10 7.10 12 -9 0 38.50 6.50 -12 10 0 28.30 6.60 -12 10 0 25.10 6.10 -12 10 0 28.00 5.30 -12 -10 0 19.40 8.40 -12 -10 0 27.40 5.90 12 -10 0 28.60 6.80 12 -10 0 22.20 5.90 -12 11 0 0.20 4.30 -12 -11 0 5.40 7.70 -12 11 0 0.80 4.50 -12 11 0 0.30 3.10 12 -11 0 -2.80 4.30 12 -11 0 0.20 5.20 -12 -12 0 31.20 10.90 -12 12 0 46.60 8.00 -12 12 0 47.60 6.80 -12 12 0 43.80 8.10 12 -12 0 47.80 8.90 12 -12 0 43.90 8.00 -12 13 0 78.19 11.70 -12 13 0 91.39 12.50 -12 -13 0 107.59 16.40 -12 13 0 104.29 11.00 12 -13 0 102.69 13.90 12 -13 0 119.69 13.20 -12 -14 0 10.80 9.30 -12 14 0 0.50 5.20 -12 14 0 4.60 3.70 -12 14 0 -2.30 5.50 12 -14 0 -1.70 5.30 12 -14 0 2.30 6.60 -12 -15 0 74.39 14.30 -12 15 0 48.60 8.70 -12 15 0 50.99 7.20 -12 15 0 38.40 8.70 12 -15 0 33.30 8.60 12 -15 0 52.09 10.50 -12 16 0 20.90 7.10 -12 16 0 9.50 4.30 -12 16 0 6.70 6.30 -12 -16 0 3.00 9.80 12 -16 0 -2.10 6.30 12 -16 0 12.40 7.80 -12 17 0 27.60 7.90 -12 -17 0 29.50 12.00 -12 17 0 27.70 5.40 -12 17 0 17.20 6.60 12 -17 0 14.40 8.00 12 -17 0 28.40 9.40 -12 18 0 9.00 6.70 -12 18 0 2.20 3.70 -12 18 0 1.50 6.00 12 -18 0 9.50 8.50 12 -18 0 3.90 7.60 -12 19 0 32.50 9.00 -12 19 0 31.10 8.80 12 -19 0 45.50 10.70 12 -19 0 31.50 10.90 -13 1 0 45.30 6.50 -13 1 0 29.10 5.90 -13 -1 0 36.60 5.90 -13 -1 0 53.59 6.30 -13 2 0 0.20 3.40 -13 2 0 4.20 3.10 -13 -2 0 5.30 3.90 -13 -2 0 1.30 3.50 -13 2 0 0.70 4.00 -13 -2 0 0.50 2.00 13 -2 0 3.20 2.30 -13 -3 0 1.00 1.40 -13 3 0 4.60 3.90 -13 -3 0 -4.30 3.60 -13 3 0 5.00 3.40 -13 -3 0 5.70 3.80 -13 3 0 -1.40 3.80 -13 4 0 10.50 4.40 -13 -4 0 4.90 3.50 -13 5 0 -1.70 4.10 -13 5 0 3.50 3.70 -13 -5 0 -3.50 3.70 -13 -5 0 6.40 4.00 -13 5 0 5.80 3.50 13 -5 0 -4.10 3.60 -13 6 0 -0.10 3.90 -13 6 0 26.30 4.70 -13 -6 0 10.50 4.00 -13 6 0 8.30 4.20 -13 -6 0 11.50 5.50 -13 -6 0 14.70 4.70 13 -6 0 19.90 5.00 -13 -7 0 4.90 4.40 -13 7 0 8.50 4.60 -13 -7 0 1.70 3.90 -13 7 0 -1.30 3.70 -13 -7 0 0.60 5.60 -13 7 0 -1.30 4.20 13 -7 0 -4.50 3.90 13 -7 0 2.90 4.00 -13 8 0 -0.80 3.90 -13 8 0 3.60 3.70 -13 -8 0 4.40 3.90 -13 -8 0 4.80 6.30 -13 8 0 6.40 4.80 13 -8 0 -2.80 3.80 13 -8 0 5.90 4.60 -13 9 0 -0.20 4.40 -13 -9 0 5.70 6.60 -13 -9 0 7.30 4.00 -13 9 0 2.50 3.70 -13 9 0 -3.10 4.40 13 -9 0 -0.70 3.80 13 -9 0 -4.00 4.30 -13 10 0 24.70 5.90 -13 10 0 18.40 5.60 -13 10 0 13.70 4.00 13 -10 0 15.60 5.60 13 -10 0 8.60 4.70 -13 11 0 8.30 5.40 -13 11 0 13.00 4.10 -13 -11 0 11.70 7.90 -13 11 0 7.60 5.40 13 -11 0 9.40 5.40 13 -11 0 8.20 4.90 -13 12 0 7.50 5.80 -13 12 0 7.00 3.70 -13 -12 0 9.90 8.10 -13 12 0 5.10 5.60 13 -12 0 3.80 5.00 13 -12 0 1.60 5.30 -13 13 0 2.50 5.70 -13 13 0 -5.10 5.20 -13 -13 0 2.10 7.30 -13 13 0 -1.90 3.40 13 -13 0 4.80 5.70 13 -13 0 9.30 6.30 -13 14 0 1.10 3.60 -13 14 0 5.40 6.10 -13 -14 0 -0.60 7.60 -13 14 0 2.70 5.70 13 -14 0 13.90 6.90 13 -14 0 1.00 5.60 -13 15 0 4.70 3.80 -13 -15 0 5.70 9.10 -13 15 0 7.50 6.30 -13 15 0 0.70 5.90 13 -15 0 6.00 6.40 13 -15 0 2.60 6.80 -13 16 0 -2.70 6.50 -13 16 0 0.50 3.90 -13 16 0 7.30 6.40 13 -16 0 -4.10 6.30 13 -16 0 -3.40 6.40 -13 17 0 -0.50 3.80 -13 17 0 1.10 5.40 -13 17 0 7.30 7.00 13 -17 0 -8.20 6.70 13 -17 0 4.10 7.60 -13 18 0 4.20 6.60 -13 18 0 -2.80 6.80 -13 18 0 0.60 4.00 13 -18 0 -0.20 7.60 13 -18 0 10.90 8.70 -14 0 0 99.49 10.10 -14 0 0 108.49 12.10 -14 0 0 108.09 12.10 14 0 0 115.19 11.10 -14 -1 0 81.29 10.20 -14 1 0 78.79 8.50 -14 1 0 101.39 10.50 -14 -1 0 83.49 10.30 -14 -1 0 82.69 8.10 14 -1 0 82.39 8.90 -14 -2 0 12.30 5.30 -14 -2 0 22.50 3.40 -14 2 0 25.20 4.50 -14 2 0 9.70 4.70 -14 2 0 25.70 5.70 -14 -2 0 20.40 5.20 14 -2 0 22.30 3.80 -14 -3 0 33.80 6.50 -14 3 0 26.00 5.90 -14 3 0 35.10 7.00 -14 3 0 19.90 5.10 -14 -3 0 41.50 6.60 -14 -3 0 36.20 3.70 -14 4 0 16.30 5.40 -14 4 0 19.50 4.90 -14 -4 0 18.40 5.30 -14 4 0 16.50 4.90 -14 -4 0 15.50 4.80 14 -4 0 18.60 5.10 -14 5 0 143.99 13.90 -14 5 0 135.79 13.30 -14 -5 0 142.09 13.90 -14 5 0 127.39 14.00 -14 -5 0 122.89 14.00 14 -5 0 124.89 13.90 -14 -6 0 13.10 5.50 -14 6 0 19.00 5.20 -14 6 0 25.50 6.40 -14 -6 0 17.50 5.10 -14 6 0 22.90 5.50 14 -6 0 17.30 5.60 -14 7 0 48.70 8.00 -14 -7 0 64.89 8.90 -14 7 0 50.19 7.60 -14 -7 0 51.59 7.70 -14 7 0 54.79 7.80 14 -7 0 36.50 7.70 -14 8 0 56.19 7.70 -14 -8 0 55.59 7.60 -14 8 0 49.99 8.30 -14 8 0 58.29 8.20 14 -8 0 41.00 8.30 14 -8 0 40.40 7.20 -14 -9 0 103.99 14.70 -14 -9 0 96.49 10.50 -14 9 0 78.09 11.00 -14 9 0 97.49 11.40 -14 9 0 81.49 10.40 14 -9 0 88.59 12.10 14 -9 0 90.89 11.10 -14 10 0 151.78 15.60 -14 10 0 163.28 15.40 -14 10 0 146.49 16.70 -14 -10 0 169.28 19.80 14 -10 0 132.49 15.90 14 -10 0 153.88 17.50 -14 11 0 28.60 6.70 -14 -11 0 32.10 9.20 -14 11 0 40.50 7.60 -14 11 0 33.30 6.00 14 -11 0 26.50 7.90 14 -11 0 24.30 6.70 -14 12 0 21.70 6.90 -14 12 0 10.10 6.20 -14 -12 0 36.20 10.60 -14 12 0 20.60 5.20 14 -12 0 12.30 5.80 14 -12 0 18.30 7.20 -14 13 0 31.10 6.00 -14 13 0 43.60 8.50 -14 13 0 29.00 7.90 -14 -13 0 38.60 11.40 14 -13 0 38.90 9.00 14 -13 0 28.50 7.20 -14 14 0 26.60 5.90 -14 14 0 31.90 8.10 -14 14 0 29.80 7.50 14 -14 0 33.20 8.50 14 -14 0 23.10 7.60 -14 15 0 94.49 10.40 -14 15 0 67.49 11.10 -14 15 0 68.59 11.60 14 -15 0 58.09 11.00 14 -15 0 92.59 13.80 -14 16 0 14.40 4.80 -14 16 0 19.10 7.60 -14 16 0 16.70 7.70 14 -16 0 19.10 7.70 14 -16 0 3.40 7.30 -14 17 0 20.30 7.70 -14 17 0 13.90 5.40 -14 17 0 10.60 7.80 14 -17 0 10.70 7.90 14 -17 0 13.70 8.40 -14 18 0 -1.80 6.90 -14 18 0 7.10 7.30 -14 18 0 8.90 4.80 14 -18 0 -9.00 6.80 -15 0 0 25.80 5.60 -15 0 0 16.00 5.20 -15 1 0 15.10 4.90 -15 -1 0 18.00 5.20 -15 -1 0 16.50 5.20 -15 1 0 18.60 5.40 -15 -2 0 16.50 5.20 -15 2 0 28.90 5.60 -15 2 0 19.60 5.50 -15 -3 0 6.30 4.40 -15 3 0 -2.10 4.70 -15 -3 0 8.60 2.20 -15 3 0 4.50 3.80 -15 3 0 9.70 4.50 -15 -3 0 3.30 4.30 -15 4 0 4.50 4.00 -15 4 0 11.40 4.70 -15 -4 0 4.60 4.60 -15 4 0 -1.40 4.40 -15 -4 0 14.00 5.10 15 -4 0 12.50 4.70 -15 5 0 2.20 4.70 -15 5 0 10.00 4.60 -15 5 0 12.20 4.60 -15 -5 0 10.00 4.60 -15 -5 0 1.60 4.30 15 -5 0 -0.60 3.70 -15 6 0 16.60 4.90 -15 -6 0 10.60 4.90 -15 -6 0 2.20 4.50 -15 6 0 -1.60 4.30 -15 6 0 6.30 4.60 15 -6 0 16.30 5.30 -15 -7 0 5.90 5.00 -15 7 0 2.20 5.10 -15 -7 0 6.50 4.70 -15 7 0 3.10 4.30 -15 7 0 8.80 5.10 15 -7 0 -0.60 4.40 -15 8 0 6.90 5.20 -15 8 0 12.50 4.80 -15 -8 0 1.40 4.30 -15 8 0 -6.00 4.20 15 -8 0 0.80 3.90 15 -8 0 5.90 4.80 -15 9 0 4.70 5.20 -15 9 0 -7.70 3.80 -15 9 0 2.90 5.40 15 -9 0 -5.40 4.00 15 -9 0 5.80 4.90 -15 10 0 9.60 5.70 -15 10 0 14.50 6.00 -15 10 0 20.50 4.80 15 -10 0 12.50 5.10 15 -10 0 13.80 5.70 -15 11 0 6.60 4.20 -15 11 0 8.00 6.00 -15 11 0 10.90 5.90 15 -11 0 6.30 5.00 15 -11 0 4.40 5.60 -15 12 0 0.40 6.00 -15 12 0 4.00 4.20 -15 12 0 4.20 5.30 15 -12 0 0.20 5.70 15 -12 0 5.00 5.30 -15 13 0 1.00 5.20 -15 13 0 2.00 6.40 -15 13 0 5.20 4.20 15 -13 0 8.50 6.40 15 -13 0 4.70 5.90 -15 14 0 15.10 4.60 -15 14 0 9.90 6.40 -15 14 0 0.40 6.10 15 -14 0 -1.20 6.40 15 -14 0 4.80 6.10 -15 15 0 -1.30 4.30 -15 15 0 5.10 6.60 -15 15 0 -1.40 6.50 15 -15 0 -0.30 6.80 15 -15 0 14.40 6.80 -15 16 0 5.50 4.70 -15 16 0 11.60 7.50 -15 16 0 5.20 6.90 15 -16 0 9.10 7.20 15 -16 0 13.00 7.60 -15 17 0 -10.90 6.70 -15 17 0 0.90 6.80 -15 17 0 -3.70 4.20 15 -17 0 0.40 7.10 -16 0 0 7.30 5.00 -16 0 0 6.50 3.70 -16 0 0 12.10 5.50 -16 1 0 211.08 20.60 -16 1 0 223.18 19.10 -16 -1 0 209.48 20.70 -16 -1 0 212.28 18.70 -16 1 0 210.08 20.70 -16 -1 0 207.58 20.50 -16 -2 0 0.70 3.20 -16 2 0 1.40 3.90 -16 -2 0 7.70 5.20 -16 2 0 3.00 4.50 -16 2 0 -0.70 4.70 -16 -2 0 4.00 5.20 -16 -3 0 38.50 7.50 -16 3 0 32.30 6.90 -16 -3 0 24.90 6.90 -16 3 0 35.90 6.40 -16 3 0 28.50 7.00 -16 -4 0 260.67 24.60 -16 -4 0 261.97 24.60 -16 4 0 284.77 23.70 -16 4 0 252.47 24.60 -16 4 0 254.77 24.70 16 -4 0 255.77 24.50 -16 -5 0 68.99 10.20 -16 -5 0 72.39 9.60 -16 5 0 82.79 9.40 -16 5 0 52.59 9.10 -16 5 0 62.89 10.00 16 -5 0 81.09 10.60 -16 6 0 6.60 5.10 -16 6 0 -3.10 4.20 -16 6 0 1.30 4.50 -16 -6 0 -6.10 4.50 -16 -6 0 -2.30 4.70 16 -6 0 1.30 4.80 -16 7 0 8.20 5.20 -16 -7 0 9.50 5.70 -16 -7 0 12.60 5.50 -16 7 0 16.20 5.80 -16 7 0 11.70 6.30 16 -7 0 18.40 6.00 -16 8 0 14.70 5.80 -16 8 0 9.00 6.00 -16 -8 0 14.60 5.50 -16 8 0 16.60 5.90 16 -8 0 10.20 5.10 16 -8 0 10.80 6.00 -16 9 0 215.48 20.80 -16 9 0 214.48 20.50 -16 9 0 214.08 21.40 16 -9 0 224.58 21.60 16 -9 0 200.68 20.80 -16 10 0 6.10 5.80 -16 10 0 1.60 5.80 -16 10 0 -0.50 4.30 16 -10 0 -2.90 5.30 16 -10 0 3.60 5.00 -16 11 0 30.20 7.80 -16 11 0 12.90 5.40 -16 11 0 33.90 8.00 16 -11 0 20.70 7.50 16 -11 0 22.70 6.40 -16 12 0 3.80 4.40 -16 12 0 9.40 6.50 -16 12 0 12.40 6.90 16 -12 0 7.40 5.90 16 -12 0 3.40 6.30 -16 13 0 16.50 5.50 -16 13 0 10.80 6.90 -16 13 0 20.50 6.90 16 -13 0 17.20 7.40 16 -13 0 18.00 6.90 -16 14 0 7.00 6.60 -16 14 0 6.80 7.20 -16 14 0 9.60 5.10 16 -14 0 8.90 7.20 16 -14 0 -0.90 6.20 -16 15 0 19.10 8.40 -16 15 0 16.30 5.80 -16 15 0 12.20 7.60 16 -15 0 22.00 8.60 16 -15 0 19.10 7.60 -16 16 0 26.20 6.30 -16 16 0 19.20 8.40 -16 16 0 40.80 9.50 16 -16 0 18.40 9.20 -17 1 0 23.90 6.50 -17 1 0 27.20 6.70 -17 -1 0 21.90 6.50 -17 -1 0 19.50 6.00 -17 1 0 29.10 5.00 -17 2 0 39.00 7.50 -17 -2 0 28.70 6.70 -17 -3 0 12.10 5.40 -17 3 0 8.50 5.60 -17 3 0 10.40 4.40 -17 3 0 22.70 6.30 -17 -3 0 10.40 5.70 -17 -4 0 8.90 5.90 -17 -4 0 5.80 5.20 -17 4 0 6.30 4.90 -17 4 0 13.40 5.60 -17 4 0 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20 -11 0 7.90 7.20 20 -11 0 -1.70 6.30 -20 12 0 15.30 8.20 -20 12 0 -5.90 7.40 -20 12 0 -3.60 5.40 20 -12 0 4.10 6.80 -21 0 0 22.40 7.90 -21 0 0 17.70 7.80 -21 1 0 18.70 7.70 -21 -1 0 25.10 8.20 -21 -1 0 12.40 8.00 -21 1 0 2.80 7.60 -21 2 0 5.10 7.10 -21 -2 0 -0.90 7.30 -21 -2 0 -5.90 6.20 -21 2 0 2.60 7.10 -21 3 0 -6.60 6.60 -21 -3 0 9.60 8.20 -21 3 0 0.60 7.30 -21 -3 0 -4.90 6.70 21 -3 0 -3.10 6.00 -21 4 0 10.70 7.40 -21 4 0 15.60 7.30 -21 -4 0 7.50 7.00 -21 -4 0 7.70 7.60 21 -4 0 13.20 7.10 -21 -5 0 8.50 7.70 -21 5 0 -2.90 6.70 -21 5 0 -1.10 6.60 -21 -5 0 12.50 7.30 21 -5 0 8.10 6.80 -21 6 0 -5.50 6.70 -21 -6 0 4.20 7.10 -21 6 0 9.50 7.80 21 -6 0 3.10 6.50 -21 7 0 6.20 7.20 -21 7 0 2.20 7.50 21 -7 0 9.80 6.70 -21 8 0 2.70 7.30 -21 8 0 10.90 7.10 -21 8 0 4.20 7.70 21 -8 0 2.70 6.00 21 -8 0 -1.00 6.00 -21 9 0 1.20 7.60 -21 9 0 -3.20 6.40 -21 9 0 8.90 8.80 21 -9 0 3.30 6.20 21 -9 0 6.50 6.30 -21 10 0 16.20 8.30 -21 10 0 11.20 8.70 -21 10 0 5.10 6.10 21 -10 0 15.30 9.90 21 -10 0 9.40 7.10 -21 11 0 -9.30 8.50 -21 11 0 -12.10 5.20 -21 11 0 -2.80 7.80 21 -11 0 -4.30 7.20 -22 0 0 21.10 8.70 -22 0 0 13.90 8.70 -22 -1 0 29.10 9.30 -22 -1 0 36.00 9.70 -22 1 0 29.20 9.50 -22 1 0 22.30 8.90 -22 2 0 14.20 8.30 -22 -2 0 1.20 7.70 -22 2 0 12.10 8.30 -22 -2 0 6.70 8.00 22 -2 0 11.20 7.20 -22 -3 0 -5.00 7.60 -22 3 0 9.30 7.80 -22 -3 0 3.80 7.80 -22 3 0 -7.30 6.80 22 -3 0 5.50 6.30 -22 4 0 9.30 7.70 -22 4 0 4.40 8.00 -22 -4 0 -4.90 7.70 -22 -4 0 -12.10 6.90 22 -4 0 12.00 7.10 -22 5 0 -1.10 7.10 -22 -5 0 -5.70 6.80 -22 5 0 5.30 8.10 22 -5 0 0.70 6.90 -22 6 0 8.30 7.60 -22 6 0 4.30 7.90 22 -6 0 -12.20 6.10 -22 7 0 15.00 8.30 -22 7 0 9.40 7.90 22 -7 0 16.40 7.40 -22 8 0 -3.30 7.10 -22 8 0 8.60 7.90 22 -8 0 -7.00 5.60 22 -8 0 1.30 6.00 -22 9 0 5.90 7.70 -22 9 0 -7.10 8.10 -22 9 0 8.70 8.90 22 -9 0 11.60 7.50 -23 0 0 8.60 8.50 -23 0 0 5.50 8.10 -23 -1 0 18.30 8.50 -23 1 0 16.60 8.50 -23 1 0 5.60 9.00 -23 -1 0 -2.00 8.50 -23 -2 0 -2.80 7.50 -23 -2 0 3.50 8.90 -23 2 0 5.50 8.70 -23 2 0 5.40 8.00 23 -2 0 6.00 7.00 -23 3 0 -4.20 7.80 -23 -3 0 5.10 8.40 -23 3 0 8.30 9.00 -23 -3 0 -5.20 6.90 23 -3 0 3.90 6.80 -23 -4 0 7.40 8.90 -23 4 0 105.89 13.20 -23 -4 0 17.80 8.70 -23 4 0 15.40 8.70 23 -4 0 22.80 8.10 -23 5 0 11.80 9.20 -23 5 0 5.90 8.40 23 -5 0 -1.40 6.50 -23 6 0 -3.00 7.70 -23 6 0 -9.10 7.90 23 -6 0 8.80 7.40 -24 0 0 42.30 11.60 -24 0 0 27.10 10.90 -24 -1 0 46.20 11.80 -24 1 0 44.80 11.40 -24 1 0 39.80 11.20 -24 -1 0 31.10 10.70 24 -1 0 32.60 9.90 -24 2 0 2.30 9.40 -24 2 0 6.30 9.20 -24 -2 0 7.70 9.90 -24 -2 0 0.20 8.20 24 -2 0 3.10 7.20 0 -22 -1 3.60 10.50 0 -22 -1 42.90 13.20 0 22 1 -2.20 5.60 0 -21 -1 -6.00 10.20 0 -21 -1 -2.40 8.30 0 21 1 -2.50 4.40 0 21 1 11.30 6.10 0 20 1 19.30 6.40 0 20 1 19.50 5.70 0 -20 -1 37.90 11.40 0 -20 -1 26.60 9.80 0 -19 -1 -0.50 7.40 0 -19 -1 8.60 7.80 0 19 1 5.80 4.20 0 -19 -1 1.00 8.70 0 19 1 1.30 4.50 0 -18 -1 0.90 6.80 0 -18 -1 12.20 8.50 0 18 1 -4.20 3.40 0 -18 -1 -0.60 6.60 0 18 1 2.50 4.40 0 -17 -1 9.90 6.80 0 -17 -1 1.60 6.70 0 -17 -1 -3.10 7.30 0 17 1 0.70 4.10 0 17 1 1.90 3.80 0 16 1 90.59 9.90 0 -16 -1 78.49 12.60 0 16 1 80.69 10.30 0 -16 -1 87.39 12.80 0 -16 -1 80.99 13.70 0 -15 -1 8.70 6.90 0 15 1 -0.80 3.10 0 -15 -1 -0.30 5.70 0 15 1 6.40 3.90 0 -15 -1 0.30 5.70 0 -14 -1 24.90 7.40 0 14 1 27.20 4.90 0 -14 -1 29.00 7.50 0 14 1 31.30 5.50 0 -14 -1 21.60 7.80 0 13 1 3.70 2.80 0 -13 -1 7.90 5.10 0 -13 -1 0.70 5.00 0 13 1 4.90 3.30 0 -13 -1 4.80 5.70 0 -12 -1 162.78 15.90 0 12 1 136.49 13.20 0 12 1 132.99 12.90 0 -12 -1 142.79 15.70 0 -12 -1 151.58 15.90 0 11 1 1.00 2.60 0 -11 -1 4.20 4.00 0 11 1 -0.30 2.20 0 -11 -1 -5.40 4.30 0 -11 -1 2.00 4.30 0 -10 -1 16.10 5.10 0 -10 -1 16.70 4.90 0 10 1 22.80 3.90 0 10 1 19.50 3.30 0 -10 -1 23.40 5.30 0 9 1 3.30 2.20 0 -9 -1 2.40 3.40 0 -9 -1 -2.60 2.90 0 -9 -1 6.50 3.80 0 9 1 -1.60 1.90 0 -8 -1 -0.60 3.10 0 -8 -1 0.30 3.40 0 8 1 4.10 1.90 0 8 1 -0.30 2.00 0 -8 -1 2.30 2.80 0 -7 -1 2.30 2.50 0 7 1 0.20 1.50 0 -7 -1 24.80 4.30 0 7 1 1.70 2.40 0 -7 -1 0.40 2.80 0 7 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0.50 0.40 0 -1 -1 -0.10 0.10 0 -1 -1 0.10 0.20 0 1 1 0.20 0.30 0 -1 -1 0.70 0.50 0 0 1 -0.10 0.10 0 0 -1 -0.50 0.20 0 0 1 0.40 0.40 0 0 -1 -0.10 0.20 0 -1 1 0.40 0.20 0 1 -1 0.00 0.10 0 1 -1 0.40 0.20 0 1 -1 0.40 0.30 0 -1 1 0.00 0.20 0 -2 1 408.06 33.40 0 -2 1 409.96 33.70 0 -2 1 392.66 33.80 0 -2 1 411.96 33.60 0 -3 1 -0.10 1.10 0 -3 1 0.10 1.00 0 3 -1 2.10 1.00 0 3 -1 -0.20 1.20 0 3 -1 0.50 0.30 0 3 -1 0.90 0.90 0 -3 1 1.00 1.30 0 -4 1 710.13 58.59 0 4 -1 721.53 58.59 0 4 -1 701.33 58.79 0 -4 1 684.23 58.59 0 -4 1 698.13 58.79 0 4 -1 715.23 58.49 0 -5 1 1.00 1.90 0 -5 1 -1.30 1.70 0 -5 1 2.10 2.00 0 5 -1 -1.20 1.50 0 5 -1 -2.50 1.60 0 5 -1 3.40 2.00 0 6 -1 144.69 12.80 0 -6 1 135.69 12.90 0 -6 1 148.49 13.10 0 6 -1 144.99 12.90 0 6 -1 143.09 13.20 0 -6 1 141.29 13.40 0 -7 1 -1.70 2.30 0 -7 1 -1.20 3.30 0 -7 1 2.10 2.70 0 7 -1 -0.50 1.80 0 7 -1 -0.80 2.00 0 7 -1 0.70 2.40 0 -8 1 2.90 3.70 0 -8 1 -5.10 2.70 0 -8 1 0.30 3.00 0 -9 1 -0.90 3.20 0 -9 1 2.80 3.50 0 9 -1 -4.30 1.90 0 -9 1 1.30 3.30 0 -10 1 20.00 5.60 0 10 -1 23.70 3.70 0 -10 1 20.30 5.10 0 -10 1 23.20 5.30 0 -11 1 -1.00 3.50 0 11 -1 -2.10 2.40 0 -11 1 2.10 3.90 0 -11 1 -5.00 4.30 0 11 -1 1.40 2.50 0 -12 1 134.89 14.10 0 -12 1 119.69 14.80 0 12 -1 134.69 12.40 0 12 -1 122.89 12.20 0 -12 1 140.99 14.90 0 13 -1 0.70 2.80 0 -13 1 7.80 5.90 0 13 -1 9.00 3.40 0 -13 1 4.30 5.00 0 -13 1 17.00 5.80 0 14 -1 36.50 5.70 0 -14 1 16.10 6.60 0 -14 1 36.70 8.60 0 -14 1 29.20 7.20 0 14 -1 25.90 5.00 0 15 -1 -0.90 3.20 0 -15 1 0.70 6.20 0 -15 1 -1.30 5.40 0 15 -1 -0.20 3.40 0 -15 1 9.40 6.00 0 -16 1 89.49 12.70 0 16 -1 92.99 10.10 0 16 -1 88.29 10.50 0 -16 1 72.69 12.10 0 -16 1 78.49 13.30 0 -17 1 5.70 6.50 0 -17 1 7.40 6.50 0 -17 1 -4.20 7.30 0 17 -1 2.90 3.80 0 17 -1 -0.40 3.90 0 -18 1 1.20 7.20 0 -18 1 6.00 7.30 0 18 -1 1.00 4.40 0 18 -1 1.90 3.90 0 -18 1 -1.80 7.60 0 19 -1 5.20 4.60 0 -19 1 -2.20 8.30 0 -19 1 7.30 8.00 0 -19 1 -2.20 7.10 0 19 -1 3.00 4.30 0 20 -1 23.30 6.60 0 -20 1 22.80 9.70 0 -20 1 71.79 12.00 0 20 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30.60 4.10 -11 2 2 186.08 17.80 -11 -2 -2 186.18 17.40 -11 -2 -2 178.78 17.50 -11 -2 -2 201.18 16.40 -11 -2 -2 188.68 17.80 -11 2 2 189.78 17.00 -11 2 2 195.18 17.70 11 -2 -2 206.98 17.20 -11 -1 -2 9.30 3.30 -11 -1 -2 4.60 3.20 -11 -1 -2 19.90 3.60 -11 -1 -2 13.00 2.40 -11 1 2 9.70 3.40 -11 1 2 14.40 3.00 -11 1 2 19.80 3.90 11 1 2 13.20 3.40 11 -1 -2 7.60 3.40 -11 0 -2 90.59 8.50 -11 1 -2 11.10 3.60 -11 -1 2 14.30 3.60 -11 1 -2 8.50 2.70 -11 -1 2 8.00 2.50 -11 1 -2 10.90 3.50 -11 -1 2 6.00 3.70 11 1 -2 11.00 4.00 11 -1 2 6.30 2.40 -11 2 -2 182.18 17.20 -11 -2 2 187.58 16.10 -11 2 -2 201.58 17.20 -11 -2 2 189.68 17.30 -11 2 -2 197.68 16.60 -11 -2 2 163.48 17.30 -11 3 -2 27.50 4.70 -11 -3 2 19.90 5.20 -11 3 -2 22.10 4.70 -11 3 -2 29.70 4.40 -11 -3 2 27.80 4.80 -11 -3 2 28.50 3.40 -11 4 -2 13.70 4.40 -11 -4 2 16.70 3.80 -11 -4 2 12.20 4.50 -11 4 -2 21.40 3.90 -11 4 -2 22.80 4.10 -11 -5 2 16.00 4.80 -11 -5 2 9.10 3.70 -11 5 -2 18.50 3.90 -11 5 -2 15.70 4.00 -11 5 -2 16.10 4.50 11 -5 2 14.80 4.50 -11 -6 2 7.50 3.30 -11 6 -2 -2.10 3.20 -11 6 -2 6.70 3.60 -11 -6 2 0.10 3.80 -11 6 -2 9.40 3.20 11 -6 2 8.50 3.90 -11 7 -2 5.90 3.00 -11 7 -2 0.50 3.70 -11 7 -2 2.20 3.90 -11 -7 2 -2.20 2.90 11 -7 2 2.60 3.20 11 7 -2 3.70 2.80 11 -7 2 -1.60 3.80 -11 8 -2 108.89 10.90 -11 8 -2 89.69 11.30 -11 8 -2 101.49 11.00 -11 -8 2 108.59 10.80 11 -8 2 110.19 11.20 11 8 -2 109.19 10.50 11 -8 2 104.09 12.30 -11 9 -2 91.79 10.60 -11 9 -2 106.79 11.30 -11 -9 2 100.39 10.80 -11 9 -2 117.19 12.30 11 9 -2 112.79 10.50 11 -9 2 113.59 13.10 11 -9 2 97.39 11.30 -11 -10 2 25.10 4.60 -11 10 -2 19.20 5.00 -11 10 -2 17.60 4.10 11 -10 2 23.20 5.40 11 -10 2 12.60 5.70 -11 11 -2 125.69 13.40 -11 11 -2 108.99 12.00 -11 11 -2 101.59 11.50 11 -11 2 116.69 13.90 11 -11 2 115.99 12.80 -11 12 -2 13.00 3.80 -11 12 -2 6.20 5.00 -11 12 -2 -3.20 4.80 11 -12 2 10.50 5.20 11 -12 2 12.90 6.00 -11 13 -2 -0.30 2.90 -11 13 -2 -1.00 4.80 -11 13 -2 -5.40 4.70 11 -13 2 -3.10 4.70 11 -13 2 12.00 6.40 -11 14 -2 16.70 3.70 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157.68 13.80 -12 -1 -3 142.29 14.40 -12 1 3 160.98 14.80 -12 1 3 145.39 14.80 -12 -1 -3 139.19 14.50 12 1 3 149.79 14.10 12 -1 -3 156.88 14.50 -12 0 3 -3.40 3.00 -12 0 -3 -2.90 3.20 -12 0 -3 -3.20 2.40 -12 0 3 -0.90 3.40 -12 0 3 -2.30 2.40 -12 0 -3 -4.60 3.10 12 0 -3 -0.70 3.80 12 0 3 -0.90 2.50 -12 1 -3 150.48 14.00 -12 -1 3 145.99 14.30 -12 -1 3 132.29 14.40 -12 -1 3 147.79 13.10 -12 1 -3 147.99 14.30 12 -1 3 149.69 13.00 -12 2 -3 124.99 12.50 -12 -2 3 132.69 12.90 -12 2 -3 133.39 12.80 -12 -2 3 127.29 12.80 -12 -2 3 122.69 11.40 -12 3 -3 93.89 9.70 -12 -3 3 95.19 10.90 -12 -3 3 84.59 8.20 -12 -3 3 80.29 9.50 -12 3 -3 92.39 10.20 -12 -4 3 -4.60 3.50 -12 -4 3 -0.20 3.70 -12 4 -3 0.20 3.60 -12 4 -3 8.60 3.50 -12 -4 3 5.90 1.80 -12 -5 3 14.60 4.30 -12 5 -3 8.00 4.20 -12 -5 3 9.50 4.80 -12 5 -3 14.30 4.30 12 -5 3 9.70 4.20 -12 -6 3 187.78 19.50 -12 -6 3 226.98 19.00 -12 6 -3 201.88 18.90 -12 6 -3 194.68 19.00 12 -6 3 209.18 19.50 -12 7 -3 3.00 4.50 -12 -7 3 14.30 4.20 -12 7 -3 9.40 3.70 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4.40 5.20 -15 4 3 4.20 4.50 -15 -4 -3 9.10 4.70 -15 -4 -3 -1.90 4.70 -15 -4 -3 6.30 5.10 15 -4 -3 4.90 4.20 -15 3 3 97.49 10.80 -15 -3 -3 89.99 8.80 -15 3 3 87.99 11.50 -15 -3 -3 94.19 12.00 -15 3 3 100.19 11.80 -15 -3 -3 96.59 11.60 -15 -3 -3 103.49 11.60 15 -3 -3 109.29 12.10 -15 2 3 70.99 10.50 -15 -2 -3 60.29 9.90 -15 -2 -3 98.39 8.60 -15 -2 -3 94.89 11.20 -15 2 3 115.69 10.00 -15 2 3 58.09 10.10 -15 -2 -3 119.69 11.10 -15 1 3 17.00 4.80 -15 1 3 -1.70 3.70 -15 -1 -3 5.10 4.50 -15 -1 -3 -3.40 4.30 -15 1 3 5.50 5.10 -15 -1 -3 -0.70 2.80 -15 0 3 -2.90 4.30 -15 0 -3 2.10 3.30 -15 0 3 -0.90 3.70 -15 0 3 1.50 4.80 -15 0 -3 0.30 4.40 -15 0 -3 -5.50 4.00 -15 -1 3 1.40 4.80 -15 1 -3 -4.50 3.80 -15 -1 3 -2.40 4.70 -15 -1 3 0.90 3.40 -15 1 -3 -1.90 4.60 -15 1 -3 -6.70 3.20 -15 2 -3 72.29 9.50 -15 2 -3 84.09 8.50 -15 2 -3 58.79 8.90 -15 -2 3 70.29 9.40 -15 -2 3 73.89 10.20 -15 3 -3 87.99 10.40 -15 -3 3 100.89 11.10 -15 3 -3 95.19 9.90 -15 -3 3 75.19 8.30 -15 -3 3 98.89 11.80 -15 3 -3 76.79 10.60 -15 4 -3 0.90 4.80 -15 -4 3 -0.10 4.50 -15 4 -3 7.70 4.50 -15 -4 3 8.90 5.50 -15 4 -3 -0.80 4.50 -15 5 -3 9.20 4.80 -15 -5 3 6.40 4.70 -15 5 -3 11.00 4.80 -15 -5 3 14.10 5.90 -15 5 -3 13.30 5.30 15 -5 3 3.10 4.30 -15 6 -3 25.00 5.70 -15 -6 3 12.70 5.10 -15 6 -3 11.40 5.30 -15 6 -3 19.60 5.40 -15 -6 3 12.30 6.10 15 -6 3 19.40 6.20 -15 -7 3 168.28 18.10 -15 -7 3 137.49 15.90 -15 7 -3 150.48 16.30 -15 7 -3 158.48 16.10 -15 7 -3 181.28 15.80 15 -7 3 148.89 15.50 15 -7 3 157.78 16.60 -15 8 -3 1.50 4.80 -15 8 -3 1.00 4.00 -15 -8 3 7.30 4.90 15 -8 3 -1.30 4.10 15 -8 3 2.00 3.90 -15 9 -3 90.69 12.20 -15 9 -3 87.39 11.00 -15 9 -3 101.79 11.80 15 -9 3 89.69 10.90 15 -9 3 81.49 12.00 -15 10 -3 5.30 5.80 -15 10 -3 7.70 6.00 -15 10 -3 8.90 4.40 15 -10 3 6.40 4.60 15 -10 3 -1.20 5.10 -15 11 -3 53.49 7.80 -15 11 -3 46.10 8.50 -15 11 -3 48.00 8.60 15 -11 3 44.30 7.80 15 -11 3 51.09 9.50 -15 12 -3 4.80 4.40 -15 12 -3 1.70 5.10 -15 12 -3 -5.90 5.80 15 -12 3 -0.40 5.90 15 -12 3 0.90 5.20 -15 13 -3 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13.20 7.70 -12 -13 -4 121.79 17.50 -12 13 4 112.39 13.60 -12 13 4 100.09 13.50 -12 13 4 102.99 11.90 12 -13 -4 93.09 13.60 12 -13 -4 138.89 15.90 -12 12 4 22.20 5.20 -12 12 4 17.50 5.80 -12 12 4 27.90 7.20 -12 -12 -4 11.10 8.60 12 -12 -4 15.20 6.80 12 -12 -4 20.00 6.90 -12 11 4 19.30 5.00 -12 11 4 24.50 6.70 -12 11 4 19.60 6.20 -12 -11 -4 17.50 8.30 12 -11 -4 25.80 7.20 12 -11 -4 19.00 6.10 -12 10 4 -2.50 5.00 -12 -10 -4 1.10 3.90 -12 10 4 6.40 4.40 -12 10 4 2.10 3.40 -12 -10 -4 -6.80 6.30 12 -10 -4 3.60 4.90 12 -10 -4 9.10 4.90 -12 9 4 23.70 6.30 -12 -9 -4 20.10 5.00 -12 9 4 14.00 5.80 -12 9 4 21.10 4.90 -12 -9 -4 30.70 8.70 12 -9 -4 15.40 6.00 12 -9 -4 28.70 4.60 12 -9 -4 24.90 6.20 -12 8 4 103.09 11.10 -12 8 4 102.69 11.40 -12 8 4 96.39 11.90 -12 -8 -4 94.29 10.80 -12 -8 -4 110.99 14.10 12 -8 -4 99.39 10.10 12 -8 -4 101.89 12.20 12 -8 -4 90.49 11.90 12 8 4 118.79 10.50 -12 7 4 54.19 7.70 -12 -7 -4 49.50 7.10 -12 7 4 49.30 6.80 -12 7 4 58.89 8.60 -12 -7 -4 53.29 9.40 12 -7 -4 53.29 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10 133.99 14.50 -11 -13 -10 105.99 17.60 11 -13 -10 103.89 14.90 11 -13 -10 107.49 15.20 -11 12 10 24.60 6.80 -11 -12 -10 15.30 9.30 -11 12 10 13.50 6.80 11 -12 -10 20.70 7.00 11 -12 -10 12.80 6.60 11 -12 -10 32.90 8.30 -11 11 10 22.70 6.20 -11 -11 -10 25.50 9.80 -11 11 10 12.80 6.60 11 -11 -10 14.40 6.60 11 -11 -10 18.30 6.40 11 -11 -10 18.70 7.10 -11 10 10 103.19 11.90 -11 -10 -10 79.39 13.70 -11 10 10 69.59 11.10 11 -10 -10 82.49 11.20 11 -10 -10 74.19 10.00 11 -10 -10 85.39 12.00 11 -10 -10 93.09 12.20 -11 9 10 88.19 11.20 -11 9 10 92.69 11.30 -11 -9 -10 95.39 14.10 -11 -9 -10 97.29 10.80 11 -9 -10 65.19 9.80 11 -9 -10 75.49 10.40 11 9 10 88.29 9.50 11 -9 -10 83.09 11.50 11 -9 -10 88.49 11.80 -11 8 10 73.99 9.90 -11 8 10 64.49 9.70 -11 -8 -10 62.59 8.80 -11 -8 -10 70.89 12.20 11 -8 -10 58.49 9.30 11 -8 -10 48.70 8.30 11 -8 -10 54.69 9.70 11 8 10 68.09 7.80 11 -8 -10 63.89 8.80 -11 -7 -10 57.59 8.10 -11 7 10 68.19 9.20 -11 -7 -10 66.89 10.70 -11 7 10 42.40 8.00 11 -7 -10 52.39 7.60 11 -7 -10 47.50 8.30 11 -7 -10 56.69 8.60 -11 6 10 2.70 4.70 -11 -6 -10 -8.30 3.90 -11 6 10 0.10 4.30 -11 -6 -10 3.90 5.50 11 -6 -10 -1.30 4.50 11 -6 -10 0.70 4.10 11 -6 -10 -0.60 4.00 -11 -5 -10 -1.70 5.00 -11 -5 -10 -4.00 4.30 -11 5 10 1.40 4.20 -11 5 10 2.60 4.70 -11 -5 -10 -0.80 2.10 11 -5 -10 -6.70 3.10 11 -5 -10 -7.60 3.80 -11 -4 -10 141.79 12.60 -11 4 10 142.09 14.80 -11 -4 -10 149.29 14.80 -11 -4 -10 133.69 15.10 -11 4 10 136.79 14.40 -11 4 10 143.99 14.70 11 -4 -10 140.19 14.10 11 -4 -10 141.09 14.50 -11 3 10 15.70 5.30 -11 3 10 27.70 6.20 -11 -3 -10 13.30 4.80 -11 3 10 9.90 4.90 -11 -3 -10 12.70 3.20 -11 -3 -10 16.20 5.40 11 -3 -10 2.10 4.30 11 -3 -10 9.00 4.00 -11 -2 -10 13.30 5.30 -11 -2 -10 16.70 3.60 -11 2 10 30.90 5.80 -11 2 10 9.30 4.50 -11 2 10 22.60 5.80 -11 -2 -10 12.60 5.10 11 -2 -10 9.70 4.70 11 -2 -10 18.70 4.40 -11 -1 -10 358.86 34.70 -11 -1 -10 378.16 34.70 -11 -1 -10 387.56 33.70 -11 1 10 424.96 35.00 -11 1 10 387.26 35.20 -11 1 10 415.46 34.60 11 -1 -10 403.66 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7.00 3 7 -26 0.00 6.50 -4 -7 -26 -4.10 9.40 -4 7 26 0.90 10.40 4 -7 -26 -6.30 7.40 4 7 26 10.30 9.90 4 -7 -26 5.20 8.10 4 -7 -26 7.50 6.70 -4 -6 -26 -8.00 8.80 -4 -6 -26 10.10 8.40 -4 6 26 16.00 10.00 4 6 26 10.80 10.30 4 -6 -26 10.20 8.90 4 -6 -26 2.20 6.20 -4 -5 -26 7.90 8.00 -4 5 26 -11.30 9.20 -4 -5 -26 -0.60 9.20 4 -5 -26 -3.10 7.40 4 -5 -26 -2.00 5.40 4 5 26 -6.30 8.80 -4 4 26 15.90 10.80 -4 -4 -26 15.50 10.00 -4 -4 -26 11.20 8.60 4 -4 -26 11.00 8.40 4 4 26 14.40 9.30 4 -4 -26 10.70 9.30 -4 -3 -26 0.70 7.90 -4 3 26 6.80 10.80 -4 -3 -26 9.70 9.00 4 -3 -26 -1.50 7.90 4 3 26 4.60 9.30 -4 2 26 4.00 10.60 -4 -2 -26 4.50 8.40 4 2 26 1.90 9.30 4 -2 -26 5.10 7.90 -4 -1 -26 14.00 9.20 -4 1 26 32.00 11.30 4 1 26 21.30 10.30 4 -1 -26 12.50 8.20 -4 0 26 29.90 11.80 -4 0 -26 16.10 9.10 4 0 -26 26.80 9.10 -4 1 -26 4.00 7.50 -4 -1 26 34.40 11.90 4 1 -26 10.10 7.90 -4 2 -26 -7.80 7.10 -4 -2 26 1.80 10.60 4 2 -26 0.70 7.00 -4 3 -26 18.20 8.30 -4 -3 26 -4.90 9.70 4 3 -26 7.90 7.30 -4 4 -26 15.00 8.00 -4 -4 26 19.20 11.70 4 4 -26 12.90 7.80 -4 5 -26 -4.00 7.10 4 5 -26 7.60 7.60 -4 6 -26 1.40 7.50 4 6 -26 20.90 8.40 -4 7 -26 10.10 7.70 4 7 -26 6.40 7.10 -5 6 26 -9.40 9.50 -5 -6 -26 -12.30 8.20 -5 -6 -26 -6.70 9.00 5 -6 -26 2.40 7.80 5 6 26 -5.30 9.00 5 -6 -26 -0.90 6.00 -5 5 26 -2.70 10.00 -5 -5 -26 14.00 9.10 -5 -5 -26 -10.80 7.60 5 -5 -26 -9.90 7.10 5 5 26 21.60 10.10 5 -5 -26 2.70 6.20 -5 4 26 3.80 10.30 -5 -4 -26 0.50 9.00 -5 -4 -26 11.70 9.00 5 4 26 5.40 9.80 5 -4 -26 3.80 7.50 5 -4 -26 1.90 5.60 -5 -3 -26 6.10 9.80 -5 3 26 10.30 11.00 -5 -3 -26 9.10 8.20 5 3 26 -1.50 9.20 5 -3 -26 -8.90 7.30 5 -3 -26 -3.70 6.40 -5 2 26 1.70 9.40 -5 -2 -26 -6.40 7.70 -5 -2 -26 0.00 8.20 5 2 26 -20.50 8.00 5 -2 -26 -5.30 7.40 -5 1 26 17.20 11.50 -5 -1 -26 7.10 8.50 5 -1 -26 -2.80 7.80 -5 0 -26 4.50 7.70 -5 0 26 10.40 9.80 5 0 -26 3.00 7.80 -5 -1 26 8.20 10.40 -5 1 -26 -1.00 8.60 5 1 -26 2.20 7.30 -5 -2 26 5.00 10.40 -5 2 -26 14.40 7.90 5 2 -26 -5.40 7.30 -5 3 -26 -2.30 7.20 -5 -3 26 11.70 11.10 5 3 -26 9.10 8.00 -5 4 -26 -2.80 7.50 -5 -4 26 -0.80 10.40 5 4 -26 7.30 7.40 -5 5 -26 0.20 7.10 5 5 -26 8.00 7.60 -5 6 -26 -3.10 6.90 5 6 -26 -6.40 6.40 -6 6 26 -7.80 15.20 -6 -6 -26 0.60 9.80 -6 -6 -26 8.20 8.60 6 6 26 8.10 10.50 6 -6 -26 2.40 8.20 6 -6 -26 0.20 6.30 -6 5 26 28.40 10.40 -6 -5 -26 20.30 10.50 -6 -5 -26 11.80 9.20 6 5 26 7.10 10.20 6 -5 -26 13.20 7.00 6 -5 -26 1.60 8.60 -6 -4 -26 40.90 12.00 -6 -4 -26 43.40 10.50 -6 4 26 23.20 11.60 6 -4 -26 38.50 9.10 6 -4 -26 41.30 10.80 6 4 26 39.90 12.20 -6 -3 -26 2.70 9.10 -6 -3 -26 6.60 8.80 -6 3 26 19.10 11.20 6 -3 -26 8.10 6.30 6 3 26 10.60 10.00 6 -3 -26 2.60 7.60 -6 2 26 1.00 10.20 -6 -2 -26 -1.60 7.70 -6 -2 -26 2.30 7.80 6 -2 -26 -12.80 7.10 6 -2 -26 7.00 6.80 -6 -1 -26 6.60 8.00 -6 -1 -26 16.90 9.90 -6 1 26 20.80 11.40 6 -1 -26 13.30 8.60 -6 0 -26 37.70 10.40 -6 0 26 15.00 11.70 6 0 -26 21.60 9.30 -6 -1 26 16.50 10.80 -6 1 -26 21.50 8.40 6 1 -26 14.20 8.30 -6 -2 26 -3.80 10.00 -6 2 -26 -4.90 7.40 6 2 -26 5.00 8.00 -6 3 -26 4.80 7.90 -6 -3 26 9.20 11.30 6 3 -26 1.20 7.60 -6 4 -26 17.90 8.40 -6 -4 26 25.70 12.30 6 4 -26 28.30 9.60 -6 5 -26 15.30 8.60 6 5 -26 11.20 8.10 -6 6 -26 6.80 6.20 -6 6 -26 -0.30 7.60 6 6 -26 7.30 8.20 -7 -5 -26 20.40 11.90 -7 5 26 48.20 15.80 -7 -5 -26 16.00 10.00 7 5 26 45.60 14.00 7 -5 -26 53.49 10.10 7 -5 -26 37.80 11.10 -7 4 26 12.10 10.90 -7 -4 -26 8.60 9.00 -7 -4 -26 1.80 8.60 7 4 26 6.60 9.60 7 -4 -26 2.90 6.40 7 -4 -26 8.10 8.80 -7 -3 -26 2.40 7.70 -7 3 26 4.90 10.40 -7 -3 -26 -4.50 9.00 7 -3 -26 -2.10 5.20 7 -3 -26 4.10 7.90 -7 2 26 -7.90 9.90 -7 -2 -26 1.80 8.80 -7 -2 -26 -4.60 8.10 7 -2 -26 -4.20 5.40 7 -2 -26 -1.60 8.00 -7 1 26 19.70 11.20 -7 -1 -26 4.10 8.30 -7 -1 -26 27.00 10.90 7 -1 -26 8.70 8.60 7 -1 -26 9.20 7.80 -7 0 26 7.30 10.30 -7 0 -26 4.20 7.80 -7 0 -26 -4.60 8.10 7 0 -26 7.00 8.10 -7 1 -26 24.20 9.30 -7 -1 26 11.80 11.40 7 1 -26 13.30 8.60 -7 -2 26 -9.60 9.10 -7 2 -26 9.10 8.00 7 2 -26 1.00 7.70 -7 -3 26 7.60 11.20 -7 3 -26 -9.30 7.00 7 3 -26 -6.10 7.00 -7 4 -26 6.00 8.10 -7 -4 26 3.70 11.20 7 4 -26 10.40 8.10 -7 5 -26 33.90 10.10 7 5 -26 43.40 11.30 -8 -4 -26 33.00 10.90 -8 -3 -26 16.00 10.10 -8 -3 -26 -0.70 8.10 -8 3 26 8.90 10.10 8 -3 -26 -7.60 5.40 8 -3 -26 9.60 8.30 -8 -2 -26 5.90 8.90 -8 -2 -26 -2.60 8.00 -8 2 26 7.50 11.40 8 -2 -26 1.10 5.70 8 -2 -26 -3.30 7.50 -8 -1 -26 3.20 8.50 -8 -1 -26 4.40 8.60 -8 1 26 14.90 10.60 8 -1 -26 -2.40 5.10 8 -1 -26 5.10 8.20 -8 0 -26 41.30 11.20 -8 0 26 36.20 13.40 -8 0 -26 27.30 9.80 8 0 -26 47.70 10.90 -8 1 -26 2.40 8.30 -8 1 -26 7.30 8.90 -8 -1 26 14.50 11.00 8 1 -26 7.80 7.70 -8 -2 26 4.80 10.60 -8 2 -26 -7.90 7.50 8 2 -26 11.70 8.20 -8 -3 26 4.50 11.10 -8 3 -26 18.70 8.90 8 3 -26 3.70 7.90 -8 4 -26 49.50 11.60 -9 -2 -26 -2.00 8.50 -9 -1 -26 3.20 8.60 -9 0 -26 3.00 9.20 -9 1 -26 2.10 7.90 -9 2 -26 -4.00 8.70 0 -6 -27 -0.90 9.20 0 5 27 -5.10 10.00 0 -5 -27 -1.90 8.10 0 -5 -27 6.10 8.90 0 -4 -27 -3.30 8.10 0 4 27 11.40 10.30 0 3 27 -0.20 8.90 0 -3 -27 0.40 7.90 0 -2 -27 11.00 8.50 0 2 27 13.10 9.90 0 1 27 17.10 10.70 0 -1 -27 -5.70 7.50 0 0 -27 4.30 7.90 0 0 27 5.80 11.00 0 -1 27 5.50 10.40 0 1 -27 13.40 7.80 0 2 -27 0.80 7.80 0 -2 27 -8.80 10.60 0 3 -27 14.30 8.30 0 4 -27 0.90 7.40 0 5 -27 -5.50 7.40 0 6 -27 10.10 9.00 -1 -5 -27 23.30 10.90 -1 -5 -27 -4.70 8.00 -1 5 27 -4.80 9.80 1 -5 -27 -11.10 7.30 1 -5 -27 9.10 9.20 1 5 27 15.20 11.00 -1 -4 -27 18.20 9.80 -1 4 27 19.40 11.50 -1 -4 -27 20.50 10.30 1 4 27 20.80 11.20 1 -4 -27 32.10 10.00 -1 -3 -27 4.30 8.50 -1 3 27 4.70 10.30 1 3 27 10.30 10.50 1 -3 -27 -3.30 7.40 -1 -2 -27 19.10 9.50 -1 2 27 26.50 11.90 1 -2 -27 27.20 9.70 1 2 27 25.30 11.00 -1 -1 -27 11.20 8.60 -1 1 27 0.10 10.30 1 1 27 -5.50 8.70 1 -1 -27 -5.40 8.00 -1 0 -27 27.00 9.50 -1 0 27 18.80 10.70 1 0 -27 10.30 8.30 1 0 27 -2.40 10.10 -1 -1 27 -4.80 10.40 -1 1 -27 2.40 7.50 1 1 -27 2.20 7.60 1 -1 27 5.70 10.50 -1 -2 27 23.60 12.30 -1 2 -27 17.70 9.00 1 2 -27 22.60 9.20 -1 3 -27 5.30 8.10 1 3 -27 5.10 7.80 -1 4 -27 30.60 9.30 1 4 -27 18.00 8.30 -1 5 -27 9.70 8.10 1 5 -27 7.50 8.00 -2 -5 -27 11.30 10.40 -2 5 27 3.00 10.60 -2 -5 -27 1.70 8.00 2 -5 -27 -2.90 8.00 2 5 27 8.50 10.60 -2 -4 -27 -2.80 8.10 -2 -4 -27 -3.20 8.80 -2 4 27 5.30 9.90 2 4 27 -1.90 9.60 2 -4 -27 12.50 8.60 -2 -3 -27 9.20 8.50 -2 3 27 4.80 10.20 2 3 27 -0.40 8.80 2 -3 -27 1.80 7.80 -2 -2 -27 3.20 8.30 -2 2 27 -6.90 9.60 2 -2 -27 1.70 7.60 2 2 27 0.10 9.60 -2 1 27 14.80 11.20 -2 -1 -27 12.90 9.00 2 1 27 11.30 10.60 2 -1 -27 1.20 7.70 -2 0 -27 -1.90 7.60 -2 0 27 -5.10 10.40 2 0 -27 -2.60 7.10 2 0 27 18.50 11.70 -2 -1 27 -11.90 10.10 -2 1 -27 10.00 7.90 2 1 -27 1.20 7.80 -2 2 -27 -0.20 7.40 -2 -2 27 -3.30 10.10 2 2 -27 4.40 7.50 -2 3 -27 1.80 7.80 -2 -3 27 21.60 12.10 2 3 -27 -6.70 6.90 -2 4 -27 17.80 8.20 2 4 -27 7.80 7.50 -2 5 -27 -3.40 7.40 2 5 -27 -4.40 7.40 -3 5 27 10.50 11.80 -3 -5 -27 22.60 11.80 -3 -5 -27 4.50 8.80 3 -5 -27 10.20 9.20 3 5 27 1.50 10.40 -3 4 27 -4.10 10.40 -3 -4 -27 -10.40 8.60 -3 -4 -27 -5.20 8.20 3 -4 -27 -0.50 8.20 3 4 27 13.10 10.80 -3 -3 -27 -17.20 7.90 -3 -3 -27 -0.50 7.60 -3 3 27 10.50 10.80 3 3 27 16.10 10.90 3 -3 -27 0.80 7.20 -3 -2 -27 24.10 9.70 -3 2 27 19.90 12.20 3 -2 -27 17.40 9.40 3 2 27 21.10 11.20 -3 -1 -27 6.50 8.50 -3 1 27 7.20 10.70 3 1 27 7.80 10.10 3 -1 -27 -10.50 7.70 -3 0 27 4.40 10.80 -3 0 -27 -0.90 8.00 3 0 -27 4.50 8.30 3 0 27 -0.30 10.30 -3 1 -27 -2.80 7.40 -3 -1 27 -3.30 9.80 3 1 -27 1.30 7.20 -3 2 -27 4.30 7.40 -3 -2 27 26.20 11.90 3 2 -27 7.00 8.30 -3 3 -27 -2.40 7.20 -3 -3 27 6.00 10.80 3 3 -27 1.70 7.70 -3 4 -27 -1.10 7.60 3 4 -27 -1.80 7.70 -3 5 -27 13.40 8.40 3 5 -27 9.10 8.00 -4 4 27 3.10 11.60 -4 -4 -27 8.60 9.10 -4 -4 -27 7.50 8.70 4 -4 -27 5.70 8.10 4 4 27 2.00 10.30 -4 3 27 16.00 11.50 -4 -3 -27 8.20 7.90 -4 -3 -27 7.10 9.50 4 3 27 2.40 9.80 4 -3 -27 6.90 8.70 -4 -2 -27 -7.70 8.70 -4 -2 -27 1.40 8.00 -4 2 27 4.20 10.90 4 2 27 5.90 10.00 -4 -1 -27 2.10 8.20 -4 1 27 7.00 10.40 4 -1 -27 8.20 8.10 4 1 27 21.10 11.30 -4 0 -27 0.40 7.50 -4 0 27 0.20 10.90 -4 1 -27 8.60 8.50 -4 -1 27 0.00 9.50 4 1 -27 1.60 8.30 -4 -2 27 -7.90 10.00 -4 2 -27 18.90 8.60 4 2 -27 1.90 7.60 -4 3 -27 3.80 7.80 -4 -3 27 1.80 10.60 4 3 -27 -1.00 7.20 -4 4 -27 -3.40 7.80 4 4 -27 2.70 7.50 -5 3 27 16.20 13.00 -5 -3 -27 10.90 9.20 -5 -3 -27 -7.10 8.80 5 -3 -27 0.00 8.10 5 3 27 -2.10 9.70 -5 2 27 16.30 11.80 -5 -2 -27 13.70 8.80 -5 -2 -27 2.20 9.20 5 -2 -27 18.50 8.70 5 2 27 16.80 10.60 -5 -1 -27 -3.80 8.30 -5 1 27 5.10 9.90 -5 -1 -27 3.00 7.80 5 -1 -27 6.30 8.50 -5 0 27 11.10 11.50 -5 0 -27 -7.90 7.70 5 0 -27 5.20 8.00 -5 1 -27 3.40 8.40 -5 -1 27 5.20 10.90 5 1 -27 -4.20 7.30 -5 -2 27 4.20 11.20 -5 2 -27 8.20 8.60 5 2 -27 5.70 8.10 -5 3 -27 5.20 8.50 -5 -3 27 1.40 11.60 5 3 -27 0.10 8.00 -6 -2 -27 -10.80 8.10 -6 1 27 -10.90 10.10 -6 -1 -27 3.80 8.70 -6 -1 -27 6.60 8.70 6 -1 -27 -3.50 8.20 -6 0 -27 -5.30 8.40 -6 0 27 -0.60 10.40 6 0 -27 -0.10 8.00 -6 1 -27 -7.30 7.50 -6 -1 27 17.10 12.30 6 1 -27 -9.40 7.40 -6 2 -27 -2.40 8.20 0 -1 -28 8.10 9.40 0 0 -28 77.89 14.20 0 1 -28 0.50 7.90 -1 0 -28 -7.60 7.90 1 0 -28 7.10 8.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 48868 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.73607(3) 0.64357(3) 0.51816(2) 0.02864(14) Uani 1 1 d D . . . . Cl1 Cl 0.72804(6) 0.79325(5) 0.43353(5) 0.0351(3) Uani 1 1 d . . . . . O1 O 0.67363(18) 0.76518(17) 0.47869(14) 0.0382(7) Uani 1 1 d . . . . . O2 O 0.7014(2) 0.7828(2) 0.37000(16) 0.0522(10) Uani 1 1 d . . . . . O3 O 0.74454(19) 0.87545(17) 0.44493(17) 0.0444(8) Uani 1 1 d . . . . . O4 O 0.79353(19) 0.74562(18) 0.4430(2) 0.0504(10) Uani 1 1 d . . . . . N1 N 0.7691(5) 0.7213(7) 0.5905(4) 0.0252(16) Uani 0.545(10) 1 d D U P A 1 N2 N 0.7180(4) 0.7457(5) 0.6349(4) 0.0211(14) Uani 0.545(10) 1 d D U P A 1 N3 N 0.6557(6) 0.5947(5) 0.5775(5) 0.0240(16) Uani 0.545(10) 1 d D U P A 1 N4 N 0.6327(5) 0.6388(5) 0.6284(4) 0.0180(13) Uani 0.545(10) 1 d D U P A 1 C1 C 0.8344(5) 0.7474(6) 0.6113(5) 0.0289(16) Uani 0.545(10) 1 d D U P A 1 C2 C 0.8249(6) 0.7888(5) 0.6677(4) 0.0302(17) Uani 0.545(10) 1 d D U P A 1 H2 H 0.862616 0.814155 0.691763 0.036 Uiso 0.545(10) 1 calc R U P A 1 C3 C 0.7519(6) 0.7867(5) 0.6824(4) 0.0253(16) Uani 0.545(10) 1 d D U P A 1 C4 C 0.9037(6) 0.7336(7) 0.5751(7) 0.047(3) Uani 0.545(10) 1 d D U P A 1 H4A H 0.943153 0.718622 0.604718 0.070 Uiso 0.545(10) 1 calc R U P A 1 H4B H 0.917536 0.782631 0.552609 0.070 Uiso 0.545(10) 1 calc R U P A 1 H4C H 0.896050 0.690611 0.544187 0.070 Uiso 0.545(10) 1 calc R U P A 1 C5 C 0.7101(6) 0.8203(6) 0.7380(4) 0.034(2) Uani 0.545(10) 1 d D U P A 1 H5A H 0.676365 0.861930 0.722998 0.052 Uiso 0.545(10) 1 calc R U P A 1 H5B H 0.744915 0.843130 0.768698 0.052 Uiso 0.545(10) 1 calc R U P A 1 H5C H 0.681761 0.777610 0.758498 0.052 Uiso 0.545(10) 1 calc R U P A 1 C6 C 0.6414(4) 0.7237(5) 0.6267(4) 0.0177(15) Uani 0.545(10) 1 d D U P A 1 H6A H 0.611519 0.748197 0.661029 0.021 Uiso 0.545(10) 1 calc R U P A 1 H6B H 0.623289 0.744475 0.585377 0.021 Uiso 0.545(10) 1 calc R U P A 1 C7 C 0.6376(6) 0.5191(5) 0.5906(4) 0.0254(17) Uani 0.545(10) 1 d D U P A 1 C8 C 0.6038(5) 0.5155(5) 0.6501(4) 0.0223(16) Uani 0.545(10) 1 d D U P A 1 H8 H 0.585981 0.468891 0.670791 0.027 Uiso 0.545(10) 1 calc R U P A 1 C9 C 0.6011(5) 0.5907(6) 0.6728(4) 0.0169(15) Uani 0.545(10) 1 d D U P A 1 C10 C 0.6534(8) 0.4533(6) 0.5452(6) 0.041(3) Uani 0.545(10) 1 d D U P A 1 H10A H 0.650654 0.473518 0.501470 0.062 Uiso 0.545(10) 1 calc R U P A 1 H10B H 0.616992 0.410654 0.550991 0.062 Uiso 0.545(10) 1 calc R U P A 1 H10C H 0.702974 0.432279 0.553356 0.062 Uiso 0.545(10) 1 calc R U P A 1 C11 C 0.5735(6) 0.6246(6) 0.7352(4) 0.026(2) Uani 0.545(10) 1 d D U P A 1 H11A H 0.615433 0.643787 0.760380 0.039 Uiso 0.545(10) 1 calc R U P A 1 H11B H 0.547392 0.582930 0.758981 0.039 Uiso 0.545(10) 1 calc R U P A 1 H11C H 0.539751 0.668999 0.726604 0.039 Uiso 0.545(10) 1 calc R U P A 1 N1B N 0.7816(6) 0.7264(8) 0.5801(5) 0.0246(18) Uani 0.455(10) 1 d D U P A 2 N2B N 0.7398(6) 0.7527(7) 0.6303(4) 0.0236(16) Uani 0.455(10) 1 d D U P A 2 N3B N 0.6548(8) 0.6121(6) 0.5807(6) 0.0236(18) Uani 0.455(10) 1 d D U P A 2 N4B N 0.6400(6) 0.6607(6) 0.6310(5) 0.0180(16) Uani 0.455(10) 1 d D U P A 2 C1B C 0.8515(6) 0.7429(7) 0.5953(5) 0.0268(18) Uani 0.455(10) 1 d D U P A 2 C2B C 0.8534(7) 0.7789(6) 0.6548(5) 0.0282(18) Uani 0.455(10) 1 d D U P A 2 H2B H 0.896414 0.796486 0.676508 0.034 Uiso 0.455(10) 1 calc R U P A 2 C3B C 0.7830(7) 0.7848(6) 0.6767(4) 0.0254(17) Uani 0.455(10) 1 d D U P A 2 C4B C 0.9136(6) 0.7260(8) 0.5513(6) 0.032(2) Uani 0.455(10) 1 d D U P A 2 H4D H 0.917084 0.668380 0.544063 0.049 Uiso 0.455(10) 1 calc R U P A 2 H4E H 0.959721 0.745427 0.570036 0.049 Uiso 0.455(10) 1 calc R U P A 2 H4F H 0.904902 0.753139 0.510539 0.049 Uiso 0.455(10) 1 calc R U P A 2 C5B C 0.7500(8) 0.8199(7) 0.7357(4) 0.036(2) Uani 0.455(10) 1 d D U P A 2 H5D H 0.712465 0.859302 0.723808 0.054 Uiso 0.455(10) 1 calc R U P A 2 H5E H 0.788690 0.845821 0.760807 0.054 Uiso 0.455(10) 1 calc R U P A 2 H5F H 0.727051 0.777432 0.760999 0.054 Uiso 0.455(10) 1 calc R U P A 2 C6B C 0.6604(6) 0.7433(6) 0.6272(5) 0.0206(17) Uani 0.455(10) 1 d D U P A 2 H6C H 0.637238 0.772966 0.662756 0.025 Uiso 0.455(10) 1 calc R U P A 2 H6D H 0.641964 0.766064 0.586684 0.025 Uiso 0.455(10) 1 calc R U P A 2 C7B C 0.6275(7) 0.5403(6) 0.5951(5) 0.0230(17) Uani 0.455(10) 1 d D U P A 2 C8B C 0.5952(6) 0.5438(7) 0.6554(5) 0.0219(17) Uani 0.455(10) 1 d D U P A 2 H8B H 0.571719 0.501105 0.677259 0.026 Uiso 0.455(10) 1 calc R U P A 2 C9B C 0.6034(6) 0.6191(7) 0.6767(5) 0.0189(17) Uani 0.455(10) 1 d D U P A 2 C10B C 0.6361(8) 0.4707(8) 0.5519(7) 0.035(3) Uani 0.455(10) 1 d D U P A 2 H10D H 0.591796 0.465273 0.525444 0.053 Uiso 0.455(10) 1 calc R U P A 2 H10E H 0.642877 0.422153 0.577276 0.053 Uiso 0.455(10) 1 calc R U P A 2 H10F H 0.679219 0.478792 0.524483 0.053 Uiso 0.455(10) 1 calc R U P A 2 C11B C 0.5783(7) 0.6584(8) 0.7380(5) 0.029(2) Uani 0.455(10) 1 d D U P A 2 H11D H 0.621337 0.669806 0.764810 0.043 Uiso 0.455(10) 1 calc R U P A 2 H11E H 0.544752 0.622514 0.760770 0.043 Uiso 0.455(10) 1 calc R U P A 2 H11F H 0.552649 0.708349 0.728045 0.043 Uiso 0.455(10) 1 calc R U P A 2 N5 N 0.7052(2) 0.59730(18) 0.43145(17) 0.0310(8) Uani 1 1 d . . . . . N6 N 0.7562(2) 0.55778(18) 0.39541(16) 0.0290(8) Uani 1 1 d . . . . . N7 N 0.8203(2) 0.55982(19) 0.52532(18) 0.0324(8) Uani 1 1 d . . . . . N8 N 0.85138(19) 0.5294(2) 0.47150(18) 0.0344(9) Uani 1 1 d . . . . . C12 C 0.6404(3) 0.5840(2) 0.4034(2) 0.0318(10) Uani 1 1 d . . . . . C13 C 0.6506(3) 0.5361(2) 0.3496(2) 0.0330(10) Uani 1 1 d . . . . . H13 H 0.613212 0.518071 0.321259 0.040 Uiso 1 1 calc R U . . . C14 C 0.7239(3) 0.5203(2) 0.34539(19) 0.0327(10) Uani 1 1 d . . . . . C15 C 0.5704(3) 0.6167(3) 0.4285(3) 0.0476(13) Uani 1 1 d . . . . . H15A H 0.537273 0.572755 0.439884 0.071 Uiso 1 1 calc R U . . . H15B H 0.546973 0.650023 0.395848 0.071 Uiso 1 1 calc R U . . . H15C H 0.580537 0.649095 0.466412 0.071 Uiso 1 1 calc R U . . . C16 C 0.7674(3) 0.4722(3) 0.2988(2) 0.0466(13) Uani 1 1 d . . . . . H16A H 0.806060 0.505578 0.279978 0.070 Uiso 1 1 calc R U . . . H16B H 0.734567 0.452700 0.265090 0.070 Uiso 1 1 calc R U . . . H16C H 0.790003 0.426754 0.320745 0.070 Uiso 1 1 calc R U . . . C17 C 0.8336(3) 0.5657(3) 0.4110(2) 0.0380(11) Uani 1 1 d . . . . . H17A H 0.863498 0.540249 0.377142 0.046 Uiso 1 1 calc R U . . . H17B H 0.846753 0.622967 0.412442 0.046 Uiso 1 1 calc R U . . . C18 C 0.8463(2) 0.5151(3) 0.5732(2) 0.0345(10) Uani 1 1 d . . . . . C19 C 0.8940(2) 0.4570(3) 0.5502(3) 0.0427(12) Uani 1 1 d . . . . . H19 H 0.919912 0.418254 0.574478 0.051 Uiso 1 1 calc R U . . . C20 C 0.8960(2) 0.4668(3) 0.4854(3) 0.0428(13) Uani 1 1 d . . . . . C21 C 0.8239(3) 0.5299(3) 0.6402(2) 0.0460(12) Uani 1 1 d . . . . . H21A H 0.819783 0.587493 0.647551 0.069 Uiso 1 1 calc R U . . . H21B H 0.861076 0.507488 0.669055 0.069 Uiso 1 1 calc R U . . . H21C H 0.776114 0.504498 0.648356 0.069 Uiso 1 1 calc R U . . . C22 C 0.9379(3) 0.4212(4) 0.4355(3) 0.0591(17) Uani 1 1 d . . . . . H22A H 0.902986 0.394217 0.407085 0.089 Uiso 1 1 calc R U . . . H22B H 0.969522 0.381527 0.456219 0.089 Uiso 1 1 calc R U . . . H22C H 0.968405 0.458204 0.410760 0.089 Uiso 1 1 calc R U . . . Cl2 Cl 0.5080(3) 0.3846(4) 0.8015(2) 0.0287(11) Uani 0.373(3) 1 d D U P B 1 O5 O 0.5086(5) 0.3565(6) 0.8647(4) 0.041(2) Uani 0.373(3) 1 d D U P B 1 O6 O 0.4786(6) 0.3238(6) 0.7605(5) 0.055(2) Uani 0.373(3) 1 d D U P B 1 O7 O 0.4643(7) 0.4557(6) 0.7949(6) 0.051(3) Uani 0.373(3) 1 d D U P B 1 O8 O 0.5818(5) 0.4019(11) 0.7809(8) 0.040(3) Uani 0.373(3) 1 d D U P B 1 Cl2B Cl 0.5093(4) 0.3937(4) 0.7786(3) 0.0251(14) Uani 0.345(3) 1 d D U P C 2 O5B O 0.4416(5) 0.3639(6) 0.8018(5) 0.041(2) Uani 0.345(3) 1 d D U P C 2 O6B O 0.5100(5) 0.3840(6) 0.7111(4) 0.039(2) Uani 0.345(3) 1 d D U P C 2 O7B O 0.5165(6) 0.4759(5) 0.7974(5) 0.044(2) Uani 0.345(3) 1 d D U P C 2 O8B O 0.5716(5) 0.3524(7) 0.8045(5) 0.050(2) Uani 0.345(3) 1 d D U P C 2 Cl2C Cl 0.5083(6) 0.3860(6) 0.7769(5) 0.0283(18) Uani 0.282(3) 1 d D U P D 3 O5C O 0.4848(9) 0.3468(8) 0.8331(6) 0.049(3) Uani 0.282(3) 1 d D U P D 3 O6C O 0.4902(7) 0.3367(9) 0.7235(7) 0.048(3) Uani 0.282(3) 1 d D U P D 3 O7C O 0.4727(9) 0.4621(7) 0.7690(7) 0.042(3) Uani 0.282(3) 1 d D U P D 3 O8C O 0.5866(6) 0.3968(13) 0.7774(10) 0.037(3) Uani 0.282(3) 1 d D U P D 3 N9 N 0.9662(5) 0.8526(7) 0.4235(4) 0.081(3) Uani 0.620(8) 1 d D U P E 1 C23 C 0.9336(7) 0.8373(10) 0.3819(6) 0.055(3) Uani 0.620(8) 1 d D U P E 1 C24 C 0.8883(5) 0.8210(6) 0.3246(5) 0.051(2) Uani 0.620(8) 1 d D U P E 1 H24A H 0.907513 0.851829 0.288542 0.076 Uiso 0.620(8) 1 calc R U P E 1 H24B H 0.837024 0.836463 0.332838 0.076 Uiso 0.620(8) 1 calc R U P E 1 H24C H 0.890446 0.763962 0.314517 0.076 Uiso 0.620(8) 1 calc R U P E 1 N9B N 1.0012(7) 0.7524(9) 0.4391(6) 0.068(4) Uani 0.380(8) 1 d D U P E 2 C23B C 0.9642(8) 0.7859(12) 0.4083(7) 0.053(3) Uani 0.380(8) 1 d D U P E 2 C24B C 0.9151(11) 0.8288(16) 0.3636(11) 0.056(4) Uani 0.380(8) 1 d D U P E 2 H24D H 0.944898 0.856030 0.331242 0.084 Uiso 0.380(8) 1 calc R U P E 2 H24E H 0.885794 0.868168 0.387096 0.084 Uiso 0.380(8) 1 calc R U P E 2 H24F H 0.881992 0.790571 0.342755 0.084 Uiso 0.380(8) 1 calc R U P E 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.0325(3) 0.0196(2) 0.0339(3) -0.01107(19) 0.0203(2) -0.00537(19) Cl1 0.0487(6) 0.0192(4) 0.0374(6) -0.0054(4) 0.0194(5) -0.0086(4) O1 0.053(2) 0.0313(16) 0.0302(17) -0.0009(13) 0.0172(15) -0.0072(14) O2 0.086(3) 0.0423(19) 0.0286(18) -0.0083(15) 0.0221(18) -0.0119(18) O3 0.053(2) 0.0195(14) 0.061(2) -0.0063(14) 0.0151(17) -0.0058(13) O4 0.044(2) 0.0232(15) 0.084(3) -0.0113(17) 0.0176(19) 0.0004(14) N1 0.024(3) 0.016(3) 0.035(3) -0.007(3) 0.011(2) -0.004(2) N2 0.024(3) 0.014(2) 0.025(2) -0.006(2) 0.008(2) -0.002(2) N3 0.027(3) 0.017(3) 0.028(3) -0.012(2) 0.015(2) -0.003(3) N4 0.019(2) 0.012(3) 0.023(2) -0.007(2) 0.005(2) 0.000(2) C1 0.026(3) 0.020(3) 0.041(3) -0.005(3) 0.012(3) -0.005(2) C2 0.030(4) 0.021(3) 0.040(3) -0.007(3) 0.005(3) -0.003(3) C3 0.030(4) 0.015(2) 0.031(3) -0.005(2) 0.004(3) -0.001(3) C4 0.032(4) 0.037(5) 0.071(7) -0.015(5) 0.022(5) -0.007(3) C5 0.041(5) 0.033(4) 0.029(4) -0.014(3) -0.001(4) 0.003(4) C6 0.018(3) 0.015(3) 0.020(3) -0.006(2) 0.004(2) 0.000(2) C7 0.026(3) 0.017(3) 0.033(3) -0.010(3) 0.014(2) -0.004(3) C8 0.020(3) 0.017(3) 0.031(3) -0.007(3) 0.008(2) 0.000(3) C9 0.014(2) 0.015(3) 0.021(3) -0.004(3) 0.002(2) 0.002(3) C10 0.058(7) 0.016(4) 0.049(5) -0.018(4) 0.038(5) -0.013(4) C11 0.032(4) 0.023(4) 0.023(3) -0.006(3) 0.001(3) 0.007(4) N1B 0.031(3) 0.016(3) 0.027(3) -0.002(3) 0.012(3) -0.002(3) N2B 0.029(3) 0.016(3) 0.025(3) -0.002(2) 0.007(3) 0.000(3) N3B 0.028(3) 0.016(4) 0.027(3) -0.004(3) 0.012(3) 0.000(3) N4B 0.020(3) 0.016(3) 0.018(3) -0.002(3) 0.007(2) 0.004(3) C1B 0.034(4) 0.017(3) 0.029(4) -0.004(3) 0.014(3) -0.006(3) C2B 0.032(4) 0.022(3) 0.030(3) -0.004(3) 0.014(3) -0.005(3) C3B 0.032(4) 0.019(3) 0.026(3) -0.003(2) 0.011(3) -0.003(3) C4B 0.034(5) 0.036(5) 0.027(5) -0.014(4) 0.014(4) -0.010(4) C5B 0.048(6) 0.033(5) 0.026(4) -0.006(3) 0.007(4) 0.003(5) C6B 0.028(4) 0.014(3) 0.020(3) 0.000(3) 0.005(3) 0.002(3) C7B 0.024(3) 0.015(4) 0.030(3) -0.004(3) 0.008(3) 0.003(3) C8B 0.021(3) 0.018(4) 0.026(3) -0.001(3) 0.006(3) 0.001(3) C9B 0.016(3) 0.020(4) 0.021(3) 0.000(3) -0.001(2) 0.003(3) C10B 0.036(6) 0.020(5) 0.050(6) -0.007(4) 0.024(5) -0.003(4) C11B 0.029(5) 0.041(6) 0.016(4) -0.001(4) 0.006(3) 0.002(5) N5 0.037(2) 0.0195(16) 0.037(2) -0.0074(14) 0.0254(16) -0.0054(14) N6 0.038(2) 0.0195(15) 0.0289(18) -0.0054(13) 0.0186(15) -0.0017(14) N7 0.0342(19) 0.0211(16) 0.042(2) -0.0110(15) 0.0224(17) -0.0044(14) N8 0.0280(18) 0.0327(18) 0.042(2) -0.0222(17) 0.0189(16) -0.0066(15) C12 0.040(2) 0.0201(18) 0.036(2) 0.0014(17) 0.0127(19) -0.0053(17) C13 0.048(3) 0.0207(19) 0.030(2) 0.0012(16) 0.009(2) 0.0007(18) C14 0.058(3) 0.0168(17) 0.023(2) 0.0019(15) 0.016(2) 0.0028(18) C15 0.036(3) 0.057(3) 0.050(3) -0.009(2) 0.015(2) 0.000(2) C16 0.077(4) 0.040(3) 0.023(2) -0.0076(19) 0.006(2) 0.019(3) C17 0.042(3) 0.027(2) 0.045(3) -0.0153(19) 0.031(2) -0.0090(18) C18 0.026(2) 0.028(2) 0.050(3) -0.014(2) 0.008(2) -0.0061(17) C19 0.024(2) 0.047(3) 0.058(3) -0.029(2) -0.008(2) 0.0048(19) C20 0.0138(19) 0.045(3) 0.070(4) -0.037(3) 0.003(2) 0.0016(17) C21 0.048(3) 0.041(3) 0.049(3) -0.002(2) 0.013(2) 0.006(2) C22 0.023(2) 0.080(4) 0.075(4) -0.050(3) -0.001(2) 0.014(2) Cl2 0.0131(14) 0.0235(16) 0.049(3) -0.001(2) 0.005(2) -0.0028(11) O5 0.026(4) 0.054(5) 0.043(5) 0.013(4) 0.007(4) 0.000(4) O6 0.054(5) 0.059(5) 0.054(5) -0.006(5) 0.000(5) -0.033(4) O7 0.043(5) 0.043(5) 0.066(6) 0.008(5) 0.008(5) 0.018(4) O8 0.018(5) 0.057(6) 0.046(5) 0.005(5) 0.000(5) -0.005(5) Cl2B 0.021(2) 0.025(2) 0.029(3) -0.007(2) 0.011(2) -0.0085(18) O5B 0.030(4) 0.045(4) 0.048(5) -0.004(4) 0.018(4) -0.018(4) O6B 0.041(4) 0.049(5) 0.027(4) 0.005(4) 0.002(4) -0.003(4) O7B 0.044(5) 0.032(4) 0.057(5) -0.012(4) 0.003(4) -0.011(4) O8B 0.035(4) 0.066(5) 0.050(5) 0.001(5) -0.011(4) 0.011(4) Cl2C 0.019(3) 0.031(3) 0.035(3) 0.004(3) 0.005(3) -0.002(2) O5C 0.050(6) 0.048(6) 0.048(6) 0.009(6) 0.014(5) -0.016(5) O6C 0.034(5) 0.058(6) 0.050(6) -0.013(6) 0.001(5) -0.009(5) O7C 0.034(6) 0.048(6) 0.044(6) 0.004(5) 0.016(5) 0.011(5) O8C 0.019(6) 0.047(6) 0.043(6) 0.000(6) 0.003(6) -0.003(6) N9 0.057(5) 0.121(7) 0.064(5) 0.017(5) -0.001(4) -0.038(5) C23 0.030(6) 0.090(6) 0.046(6) 0.014(5) 0.003(4) -0.010(5) C24 0.030(4) 0.075(6) 0.047(5) 0.006(5) 0.007(4) 0.014(4) N9B 0.041(7) 0.109(10) 0.054(7) -0.008(7) 0.007(6) -0.008(7) C23B 0.030(6) 0.083(7) 0.048(7) 0.007(6) 0.017(5) 0.000(6) C24B 0.033(9) 0.077(8) 0.057(10) 0.024(8) 0.018(7) 0.002(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3B Zn1 N5 106.0(4) . . ? N3B Zn1 N1B 93.3(4) . . ? N5 Zn1 N1B 156.3(4) . . ? N3B Zn1 N7 108.0(4) . . ? N5 Zn1 N7 90.49(14) . . ? N1B Zn1 N7 96.6(4) . . ? N5 Zn1 N3 101.0(3) . . ? N7 Zn1 N3 101.8(4) . . ? N5 Zn1 N1 163.1(4) . . ? N7 Zn1 N1 99.1(3) . . ? N3 Zn1 N1 90.6(3) . . ? N3B Zn1 O1 95.6(4) . . ? N5 Zn1 O1 83.70(12) . . ? N1B Zn1 O1 80.8(4) . . ? N7 Zn1 O1 156.38(12) . . ? N3 Zn1 O1 101.8(4) . . ? N1 Zn1 O1 82.0(4) . . ? O2 Cl1 O3 110.2(2) . . ? O2 Cl1 O4 109.8(2) . . ? O3 Cl1 O4 109.7(2) . . ? O2 Cl1 O1 109.9(2) . . ? O3 Cl1 O1 110.28(19) . . ? O4 Cl1 O1 106.9(2) . . ? Cl1 O1 Zn1 100.11(17) . . ? C1 N1 N2 106.2(6) . . ? C1 N1 Zn1 134.0(6) . . ? N2 N1 Zn1 119.0(5) . . ? C3 N2 N1 110.0(6) . . ? C3 N2 C6 130.6(6) . . ? N1 N2 C6 119.4(5) . . ? C7 N3 N4 106.1(5) . . ? C7 N3 Zn1 131.8(6) . . ? N4 N3 Zn1 118.0(5) . . ? C9 N4 N3 110.2(6) . . ? C9 N4 C6 130.7(6) . . ? N3 N4 C6 119.0(6) . . ? N1 C1 C2 109.4(7) . . ? N1 C1 C4 122.2(7) . . ? C2 C1 C4 128.4(8) . . ? C3 C2 C1 107.6(6) . . ? C3 C2 H2 126.2 . . ? C1 C2 H2 126.2 . . ? N2 C3 C2 106.7(6) . . ? N2 C3 C5 122.1(8) . . ? C2 C3 C5 131.2(7) . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? N4 C6 N2 110.8(6) . . ? N4 C6 H6A 109.5 . . ? N2 C6 H6A 109.5 . . ? N4 C6 H6B 109.5 . . ? N2 C6 H6B 109.5 . . ? H6A C6 H6B 108.1 . . ? N3 C7 C8 109.4(6) . . ? N3 C7 C10 121.7(6) . . ? C8 C7 C10 128.8(7) . . ? C9 C8 C7 107.0(6) . . ? C9 C8 H8 126.5 . . ? C7 C8 H8 126.5 . . ? C8 C9 N4 107.3(5) . . ? C8 C9 C11 132.0(6) . . ? N4 C9 C11 120.7(7) . . ? C7 C10 H10A 109.5 . . ? C7 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C7 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C9 C11 H11A 109.5 . . ? C9 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C9 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C1B N1B N2B 105.9(6) . . ? C1B N1B Zn1 131.8(7) . . ? N2B N1B Zn1 118.5(6) . . ? C3B N2B N1B 111.1(7) . . ? C3B N2B C6B 130.3(8) . . ? N1B N2B C6B 118.6(7) . . ? C7B N3B N4B 106.9(6) . . ? C7B N3B Zn1 130.2(7) . . ? N4B N3B Zn1 119.2(6) . . ? C9B N4B N3B 109.7(6) . . ? C9B N4B C6B 131.3(7) . . ? N3B N4B C6B 118.9(7) . . ? N1B C1B C2B 109.1(8) . . ? N1B C1B C4B 122.1(8) . . ? C2B C1B C4B 128.8(8) . . ? C3B C2B C1B 108.3(7) . . ? C3B C2B H2B 125.9 . . ? C1B C2B H2B 125.9 . . ? C2B C3B N2B 105.6(7) . . ? C2B C3B C5B 133.2(8) . . ? N2B C3B C5B 121.2(9) . . ? C1B C4B H4D 109.5 . . ? C1B C4B H4E 109.5 . . ? H4D C4B H4E 109.5 . . ? C1B C4B H4F 109.5 . . ? H4D C4B H4F 109.5 . . ? H4E C4B H4F 109.5 . . ? C3B C5B H5D 109.5 . . ? C3B C5B H5E 109.5 . . ? H5D C5B H5E 109.5 . . ? C3B C5B H5F 109.5 . . ? H5D C5B H5F 109.5 . . ? H5E C5B H5F 109.5 . . ? N4B C6B N2B 111.0(7) . . ? N4B C6B H6C 109.4 . . ? N2B C6B H6C 109.4 . . ? N4B C6B H6D 109.4 . . ? N2B C6B H6D 109.4 . . ? H6C C6B H6D 108.0 . . ? N3B C7B C8B 108.8(7) . . ? N3B C7B C10B 122.0(7) . . ? C8B C7B C10B 129.1(8) . . ? C9B C8B C7B 107.1(7) . . ? C9B C8B H8B 126.4 . . ? C7B C8B H8B 126.4 . . ? C8B C9B N4B 107.5(6) . . ? C8B C9B C11B 131.0(8) . . ? N4B C9B C11B 121.5(8) . . ? C7B C10B H10D 109.5 . . ? C7B C10B H10E 109.5 . . ? H10D C10B H10E 109.5 . . ? C7B C10B H10F 109.5 . . ? H10D C10B H10F 109.5 . . ? H10E C10B H10F 109.5 . . ? C9B C11B H11D 109.5 . . ? C9B C11B H11E 109.5 . . ? H11D C11B H11E 109.5 . . ? C9B C11B H11F 109.5 . . ? H11D C11B H11F 109.5 . . ? H11E C11B H11F 109.5 . . ? C12 N5 N6 105.7(3) . . ? C12 N5 Zn1 133.9(3) . . ? N6 N5 Zn1 119.3(3) . . ? C14 N6 N5 111.3(4) . . ? C14 N6 C17 129.5(3) . . ? N5 N6 C17 119.1(3) . . ? C18 N7 N8 105.5(3) . . ? C18 N7 Zn1 133.7(3) . . ? N8 N7 Zn1 119.8(3) . . ? C20 N8 N7 111.0(4) . . ? C20 N8 C17 130.3(4) . . ? N7 N8 C17 118.7(4) . . ? N5 C12 C13 109.6(4) . . ? N5 C12 C15 122.5(4) . . ? C13 C12 C15 127.9(5) . . ? C14 C13 C12 107.1(4) . . ? C14 C13 H13 126.5 . . ? C12 C13 H13 126.5 . . ? N6 C14 C13 106.3(4) . . ? N6 C14 C16 122.0(4) . . ? C13 C14 C16 131.6(4) . . ? C12 C15 H15A 109.5 . . ? C12 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C12 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C14 C16 H16A 109.5 . . ? C14 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C14 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? N8 C17 N6 112.2(3) . . ? N8 C17 H17A 109.2 . . ? N6 C17 H17A 109.2 . . ? N8 C17 H17B 109.2 . . ? N6 C17 H17B 109.2 . . ? H17A C17 H17B 107.9 . . ? N7 C18 C19 110.6(4) . . ? N7 C18 C21 121.4(4) . . ? C19 C18 C21 128.0(5) . . ? C20 C19 C18 106.1(5) . . ? C20 C19 H19 127.0 . . ? C18 C19 H19 127.0 . . ? N8 C20 C19 106.9(4) . . ? N8 C20 C22 123.1(5) . . ? C19 C20 C22 130.1(5) . . ? C18 C21 H21A 109.5 . . ? C18 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C18 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C20 C22 H22A 109.5 . . ? C20 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C20 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? O5 Cl2 O8 110.2(8) . . ? O5 Cl2 O6 109.2(7) . . ? O8 Cl2 O6 108.0(7) . . ? O5 Cl2 O7 111.9(6) . . ? O8 Cl2 O7 108.4(7) . . ? O6 Cl2 O7 109.1(7) . . ? O5B Cl2B O6B 108.2(7) . . ? O5B Cl2B O8B 112.5(8) . . ? O6B Cl2B O8B 108.4(7) . . ? O5B Cl2B O7B 108.8(6) . . ? O6B Cl2B O7B 112.4(7) . . ? O8B Cl2B O7B 106.6(7) . . ? O5C Cl2C O6C 108.4(9) . . ? O5C Cl2C O8C 110.5(9) . . ? O6C Cl2C O8C 107.8(9) . . ? O5C Cl2C O7C 111.9(9) . . ? O6C Cl2C O7C 108.7(8) . . ? O8C Cl2C O7C 109.5(9) . . ? N9 C23 C24 176.9(19) . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? N9B C23B C24B 177(2) . . ? C23B C24B H24D 109.5 . . ? C23B C24B H24E 109.5 . . ? H24D C24B H24E 109.5 . . ? C23B C24B H24F 109.5 . . ? H24D C24B H24F 109.5 . . ? H24E C24B H24F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 N3B 2.041(8) . ? Zn1 N5 2.055(4) . ? Zn1 N1B 2.072(8) . ? Zn1 N7 2.078(4) . ? Zn1 N3 2.084(7) . ? Zn1 N1 2.088(6) . ? Zn1 O1 2.474(3) . ? Cl1 O2 1.428(4) . ? Cl1 O3 1.430(3) . ? Cl1 O4 1.444(4) . ? Cl1 O1 1.446(3) . ? N1 C1 1.335(8) . ? N1 N2 1.374(7) . ? N2 C3 1.357(8) . ? N2 C6 1.446(8) . ? N3 C7 1.337(8) . ? N3 N4 1.362(7) . ? N4 C9 1.358(7) . ? N4 C6 1.433(8) . ? C1 C2 1.382(9) . ? C1 C4 1.484(10) . ? C2 C3 1.359(10) . ? C2 H2 0.9500 . ? C3 C5 1.500(9) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C8 1.392(8) . ? C7 C10 1.484(9) . ? C8 C9 1.348(9) . ? C8 H8 0.9500 . ? C9 C11 1.512(8) . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? N1B C1B 1.336(8) . ? N1B N2B 1.371(8) . ? N2B C3B 1.360(9) . ? N2B C6B 1.448(9) . ? N3B C7B 1.337(8) . ? N3B N4B 1.359(7) . ? N4B C9B 1.358(8) . ? N4B C6B 1.435(9) . ? C1B C2B 1.387(10) . ? C1B C4B 1.482(10) . ? C2B C3B 1.359(11) . ? C2B H2B 0.9500 . ? C3B C5B 1.493(10) . ? C4B H4D 0.9800 . ? C4B H4E 0.9800 . ? C4B H4F 0.9800 . ? C5B H5D 0.9800 . ? C5B H5E 0.9800 . ? C5B H5F 0.9800 . ? C6B H6C 0.9900 . ? C6B H6D 0.9900 . ? C7B C8B 1.394(9) . ? C7B C10B 1.485(10) . ? C8B C9B 1.348(10) . ? C8B H8B 0.9500 . ? C9B C11B 1.513(9) . ? C10B H10D 0.9800 . ? C10B H10E 0.9800 . ? C10B H10F 0.9800 . ? C11B H11D 0.9800 . ? C11B H11E 0.9800 . ? C11B H11F 0.9800 . ? N5 C12 1.333(6) . ? N5 N6 1.364(4) . ? N6 C14 1.355(6) . ? N6 C17 1.447(6) . ? N7 C18 1.338(6) . ? N7 N8 1.361(4) . ? N8 C20 1.356(6) . ? N8 C17 1.442(6) . ? C12 C13 1.397(6) . ? C12 C15 1.479(6) . ? C13 C14 1.359(6) . ? C13 H13 0.9500 . ? C14 C16 1.491(6) . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C18 C19 1.389(6) . ? C18 C21 1.485(6) . ? C19 C20 1.370(7) . ? C19 H19 0.9500 . ? C20 C22 1.501(6) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? Cl2 O5 1.407(8) . ? Cl2 O8 1.435(7) . ? Cl2 O6 1.436(8) . ? Cl2 O7 1.438(7) . ? Cl2B O5B 1.412(8) . ? Cl2B O6B 1.425(8) . ? Cl2B O8B 1.431(8) . ? Cl2B O7B 1.439(7) . ? Cl2C O5C 1.416(9) . ? Cl2C O6C 1.431(9) . ? Cl2C O8C 1.431(8) . ? Cl2C O7C 1.438(8) . ? N9 C23 1.084(12) . ? C23 C24 1.481(13) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? N9B C23B 1.087(13) . ? C23B C24B 1.480(15) . ? C24B H24D 0.9800 . ? C24B H24E 0.9800 . ? C24B H24F 0.9800 . ?