#------------------------------------------------------------------------------ #$Date: 2024-12-06 18:30:06 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296370 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572763.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572763 loop_ _publ_author_name 'Zhang, Chonghe' 'Gilliard, Jr, Robert J' 'Cummins, Christopher C.' _publ_section_title ; Arene extrusion as an approach to reductive elimination at boron: implication of carbene-ligated haloborylene as a transient reactive intermediate. ; _journal_issue 43 _journal_name_full 'Chemical science' _journal_page_first 17873 _journal_page_last 17880 _journal_paper_doi 10.1039/d4sc05524a _journal_volume 15 _journal_year 2024 _chemical_absolute_configuration unk _chemical_formula_moiety 'C16 H24 B2 Cl2' _chemical_formula_sum 'C16 H24 B2 Cl2' _chemical_formula_weight 308.87 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2023-07-12 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-09-26 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 94.308(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.5963(5) _cell_length_b 14.7551(8) _cell_length_c 13.3230(7) _cell_measurement_reflns_used 5577 _cell_measurement_temperature 100.00 _cell_measurement_theta_max 27.408 _cell_measurement_theta_min 2.376 _cell_volume 1685.11(16) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2018)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2018)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'olex2.solve 1.5 (Bourhis et al., 2015)' _diffrn_ambient_temperature 100.00 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0408 _diffrn_reflns_av_unetI/netI 0.0304 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_number 4036 _diffrn_reflns_point_group_measured_fraction_full 0.521 _diffrn_reflns_point_group_measured_fraction_max 0.517 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.568 _diffrn_reflns_theta_min 1.533 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.372 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; TWINABS-2012/1 (Bruker,2012) was used for absorption correction. For component 1: wR2(int) was 0.1148 before and 0.0457 after correction. For component 2: wR2(int) was 0.1124 before and 0.0541 after correction. The Ratio of minimum to maximum transmission is 0.93. Final HKLF 4 output contains 83802 reflections, Rint = 0.1194 (41511 with I > 3sig(I), Rint = 0.0408) ; _exptl_crystal_colour 'dull colourless' _exptl_crystal_colour_lustre dull _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.217 _exptl_crystal_description plate _exptl_crystal_F_000 656 _exptl_crystal_size_max 0.087 _exptl_crystal_size_mid 0.067 _exptl_crystal_size_min 0.012 _refine_diff_density_max 0.830 _refine_diff_density_min -0.591 _refine_diff_density_rms 0.106 _refine_ls_abs_structure_details ; No quotients, so Flack parameter determined by classical intensity fit ; _refine_ls_abs_structure_Flack 0.06(10) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.082 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 377 _refine_ls_number_reflns 4036 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.082 _refine_ls_R_factor_all 0.0675 _refine_ls_R_factor_gt 0.0545 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0622P)^2^+4.6360P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1415 _refine_ls_wR_factor_ref 0.1558 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full 0.000 _reflns_Friedel_fraction_max 0.000 _reflns_number_gt 3766 _reflns_number_total 4036 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05524a3.cif _cod_data_source_block 1Cl _cod_depositor_comments 'Adding full bibliography for 1572763--1572772.cif.' _cod_database_code 1572763 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.996 _shelx_estimated_absorpt_t_min 0.968 _olex2_refinement_description ; 1. Fixed Uiso At 1.5 times of: All C(H,H,H) groups 2.a Idealised Me refined as rotating group: C6(H6A,H6B,H6C), C11(H11A,H11B,H11C), C12(H12A,H12B,H12C), C13(H13A,H13B, H13C), C14(H14A,H14B,H14C), C16(H16A,H16B,H16C), C17(H17A,H17B,H17C), C18(H18A, H18B,H18C), C24(H24A,H24B,H24C), C29(H29A,H29B,H29C), C30(H30A,H30B,H30C), C31(H31A,H31B,H31C), C32(H32A,H32B,H32C), C34(H34A,H34B,H34C), C35(H35A,H35B, H35C), C36(H36A,H36B,H36C) ; _shelx_res_file ; TITL mo_P8_23066_0m_4_a.res in P2(1) mo_p8_23066_0m_4_a.res created by SHELXL-2016/6 at 18:36:05 on 12-Jul-2023 CELL 0.71073 8.5963 14.7551 13.323 90 94.308 90 ZERR 4 0.0005 0.0008 0.0007 0 0.002 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H B Cl UNIT 64 96 8 8 L.S. 10 PLAN 14 0 0 SIZE 0.087 0.067 0.012 TEMP -173.15 CONF HTAB MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.062200 4.636000 FVAR 0.65697 CL1 4 0.512465 0.952437 0.601418 11.00000 0.02432 0.01562 = 0.02257 0.00802 0.00161 -0.00274 CL2 4 0.135310 0.646931 0.857976 11.00000 0.03209 0.03636 = 0.04463 0.00984 0.01422 -0.00006 CL3 4 1.082818 0.047062 0.923008 11.00000 0.03217 0.02111 = 0.02541 0.00990 0.00480 0.00725 CL4 4 0.608119 0.317114 0.648971 11.00000 0.02822 0.05491 = 0.04407 0.01283 -0.00263 -0.00341 B1 3 0.488496 0.843933 0.657296 11.00000 0.01237 0.01617 = 0.01344 -0.00117 -0.00104 0.00115 C2 1 0.354010 0.808406 0.721905 11.00000 0.01302 0.01313 = 0.01574 0.00231 0.00040 0.00101 C3 1 0.334744 0.704327 0.697174 11.00000 0.01560 0.01380 = 0.01124 -0.00205 -0.00114 0.00010 B4 3 0.312382 0.649498 0.795585 11.00000 0.01442 0.01207 = 0.01556 -0.00077 0.00423 -0.00888 C5 1 0.455550 0.598521 0.829205 11.00000 0.01832 0.01150 = 0.01888 0.00007 -0.00109 -0.00246 C6 1 0.485158 0.541794 0.922749 11.00000 0.03204 0.02507 = 0.02317 0.00966 -0.00010 0.00025 AFIX 137 H6A 2 0.391281 0.540961 0.960171 11.00000 -1.50000 H6B 2 0.572090 0.567754 0.965115 11.00000 -1.50000 H6C 2 0.511355 0.479776 0.903795 11.00000 -1.50000 AFIX 0 C7 1 0.499382 0.671983 0.668488 11.00000 0.01783 0.01280 = 0.01522 -0.00434 0.00041 -0.00363 C8 1 0.600813 0.759214 0.659050 11.00000 0.01284 0.01232 = 0.01734 0.00004 0.00219 -0.00357 C9 1 0.630839 0.804708 0.759955 11.00000 0.01712 0.00995 = 0.01575 0.00382 -0.00115 0.00174 C10 1 0.489802 0.829569 0.796473 11.00000 0.01594 0.01049 = 0.01152 -0.00013 0.00337 -0.00123 C11 1 0.475045 0.890547 0.885436 11.00000 0.02939 0.02527 = 0.01774 -0.00812 0.00278 -0.00565 AFIX 137 H11A 2 0.570012 0.886437 0.930739 11.00000 -1.50000 H11B 2 0.385029 0.871794 0.921384 11.00000 -1.50000 H11C 2 0.460460 0.953222 0.862267 11.00000 -1.50000 AFIX 0 C12 1 0.207051 0.862372 0.735685 11.00000 0.01744 0.01670 = 0.03438 0.00294 0.00739 0.00663 AFIX 137 H12A 2 0.233107 0.926881 0.741988 11.00000 -1.50000 H12B 2 0.160627 0.841876 0.796706 11.00000 -1.50000 H12C 2 0.132425 0.853242 0.677269 11.00000 -1.50000 AFIX 0 C13 1 0.787648 0.833302 0.802491 11.00000 0.01941 0.02450 = 0.03362 -0.00118 -0.00579 -0.00147 AFIX 137 H13A 2 0.827069 0.881636 0.760791 11.00000 -1.50000 H13B 2 0.859018 0.781461 0.803541 11.00000 -1.50000 H13C 2 0.780429 0.855694 0.871236 11.00000 -1.50000 AFIX 0 C14 1 0.737395 0.756170 0.593285 11.00000 0.02171 0.02634 = 0.03001 -0.00055 0.01318 -0.00338 AFIX 137 H14A 2 0.700057 0.738951 0.524618 11.00000 -1.50000 H14B 2 0.813814 0.711523 0.620402 11.00000 -1.50000 H14C 2 0.786517 0.816070 0.592364 11.00000 -1.50000 AFIX 0 C15 1 0.560772 0.612589 0.758360 11.00000 0.01828 0.01581 = 0.02442 -0.00046 0.00136 0.00060 C16 1 0.737052 0.570752 0.764070 11.00000 0.02967 0.01053 = 0.02544 0.00793 0.00781 -0.00182 AFIX 137 H16A 2 0.759067 0.539988 0.828770 11.00000 -1.50000 H16B 2 0.812392 0.619886 0.757724 11.00000 -1.50000 H16C 2 0.745504 0.527270 0.709143 11.00000 -1.50000 AFIX 0 C17 1 0.496598 0.615394 0.572183 11.00000 0.02989 0.02346 = 0.02331 -0.00984 0.00534 -0.00358 AFIX 137 H17A 2 0.432628 0.561188 0.579702 11.00000 -1.50000 H17B 2 0.603183 0.597278 0.559878 11.00000 -1.50000 H17C 2 0.452198 0.651458 0.515265 11.00000 -1.50000 AFIX 0 C18 1 0.202078 0.691657 0.614645 11.00000 0.01542 0.02409 = 0.03071 -0.00218 -0.00415 -0.00229 AFIX 137 H18A 2 0.103230 0.710742 0.640171 11.00000 -1.50000 H18B 2 0.195330 0.627657 0.595136 11.00000 -1.50000 H18C 2 0.222973 0.728482 0.555937 11.00000 -1.50000 AFIX 0 B19 3 1.033546 0.149146 0.855203 11.00000 0.01728 0.01941 = 0.01256 0.00043 0.00055 0.00345 C20 1 0.872804 0.178638 0.798442 11.00000 0.01330 0.01182 = 0.01752 0.00194 0.00146 0.00093 C21 1 0.862243 0.284380 0.806076 11.00000 0.01382 0.01378 = 0.01528 -0.00086 0.00200 0.00199 B22 3 0.804454 0.326826 0.702865 11.00000 0.01360 0.01714 = 0.01651 0.00074 -0.00149 -0.00103 C23 1 0.928188 0.375000 0.654125 11.00000 0.02156 0.01609 = 0.01613 0.00211 0.00165 -0.00057 C24 1 0.917500 0.424165 0.554662 11.00000 0.03228 0.02860 = 0.02361 0.00906 0.00375 0.00316 AFIX 137 H24A 2 0.814099 0.414311 0.520230 11.00000 -1.50000 H24B 2 0.997629 0.400978 0.512793 11.00000 -1.50000 H24C 2 0.933824 0.489168 0.566302 11.00000 -1.50000 AFIX 0 C25 1 1.038834 0.318499 0.818491 11.00000 0.01296 0.01300 = 0.01840 -0.00137 -0.00143 0.00349 C26 1 1.142289 0.230907 0.829381 11.00000 0.01474 0.01423 = 0.01888 -0.00088 0.00237 0.00334 C27 1 1.125448 0.174779 0.734516 11.00000 0.01640 0.01210 = 0.01503 0.00167 0.00575 0.00335 C28 1 0.973038 0.146164 0.716112 11.00000 0.01812 0.01305 = 0.01298 0.00259 0.00156 0.00317 C29 1 0.724005 0.124757 0.807802 11.00000 0.01523 0.02676 = 0.04346 0.00505 0.00667 -0.00193 AFIX 137 H29A 2 0.745087 0.060171 0.798320 11.00000 -1.50000 H29B 2 0.644076 0.145025 0.756366 11.00000 -1.50000 H29C 2 0.686861 0.134315 0.874758 11.00000 -1.50000 AFIX 0 C30 1 0.919150 0.075902 0.640271 11.00000 0.03528 0.02442 = 0.02415 -0.00944 -0.00393 -0.00176 AFIX 137 H30A 2 0.979342 0.081260 0.580934 11.00000 -1.50000 H30B 2 0.808161 0.084987 0.620398 11.00000 -1.50000 H30C 2 0.934660 0.015454 0.669821 11.00000 -1.50000 AFIX 0 C31 1 1.261214 0.138881 0.682715 11.00000 0.02260 0.02037 = 0.03159 0.00307 0.01342 0.00806 AFIX 137 H31A 2 1.333443 0.188528 0.671126 11.00000 -1.50000 H31B 2 1.223897 0.112014 0.618066 11.00000 -1.50000 H31C 2 1.315200 0.092593 0.725033 11.00000 -1.50000 AFIX 0 C32 1 1.306916 0.239418 0.878098 11.00000 0.01696 0.02799 = 0.03682 -0.00105 -0.00662 -0.00065 AFIX 137 H32A 2 1.356901 0.179685 0.880746 11.00000 -1.50000 H32B 2 1.303214 0.263200 0.946557 11.00000 -1.50000 H32C 2 1.366974 0.280865 0.838459 11.00000 -1.50000 AFIX 0 C33 1 1.061885 0.369770 0.719431 11.00000 0.01641 0.01175 = 0.02288 0.00146 0.00556 -0.00043 C34 1 1.233378 0.412399 0.695712 11.00000 0.01646 0.01082 = 0.01269 0.00441 -0.00326 0.00704 AFIX 137 H34A 2 1.245365 0.409601 0.623207 11.00000 -1.50000 H34B 2 1.316627 0.377208 0.731728 11.00000 -1.50000 H34C 2 1.239697 0.475631 0.718156 11.00000 -1.50000 AFIX 0 C35 1 1.073386 0.382222 0.908564 11.00000 0.02662 0.02947 = 0.02526 -0.01046 -0.00023 -0.00070 AFIX 137 H35A 2 1.008402 0.436631 0.899798 11.00000 -1.50000 H35B 2 1.183726 0.399573 0.912692 11.00000 -1.50000 H35C 2 1.050079 0.351124 0.970676 11.00000 -1.50000 AFIX 0 C36 1 0.765967 0.310638 0.893080 11.00000 0.02040 0.02894 = 0.02269 -0.00332 0.00782 0.00578 AFIX 137 H36A 2 0.659615 0.287204 0.880519 11.00000 -1.50000 H36B 2 0.762730 0.376812 0.898865 11.00000 -1.50000 H36C 2 0.813649 0.284783 0.955803 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_P8_23066_0m_4_a.res in P2(1) REM R1 = 0.0545 for 3766 Fo > 4sig(Fo) and 0.0675 for all 4036 data REM 377 parameters refined using 1 restraints END WGHT 0.0622 4.6360 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 0.830, deepest hole -0.591, 1-sigma level 0.106 Q1 1 1.2621 0.4146 0.7131 11.00000 0.05 0.83 Q2 1 1.2364 0.4373 0.6961 11.00000 0.05 0.81 Q3 1 1.1878 0.3987 0.6989 11.00000 0.05 0.73 Q4 1 0.7872 0.5725 0.7737 11.00000 0.05 0.60 Q5 1 0.7386 0.5358 0.7623 11.00000 0.05 0.57 Q6 1 0.7175 0.5717 0.7928 11.00000 0.05 0.56 Q7 1 0.7309 0.5802 0.7405 11.00000 0.05 0.55 Q8 1 0.6148 0.5398 0.9354 11.00000 0.05 0.40 Q9 1 0.2540 0.6525 0.8373 11.00000 0.05 0.40 Q10 1 1.1850 0.1048 0.9634 11.00000 0.05 0.40 Q11 1 0.5860 0.8814 1.0595 11.00000 0.05 0.39 Q12 1 0.7072 0.0980 0.6902 11.00000 0.05 0.39 Q13 1 0.7222 0.0733 0.9564 11.00000 0.05 0.38 Q14 1 1.0535 0.2573 0.6037 11.00000 0.05 0.38 ; _shelx_res_checksum 57258 _shelx_hkl_file ; 1 0 0 35.90 0.40 2 0 0 575.14 4.70 3 0 0 2017.90 15.60 4 0 0 152.88 5.20 5 0 0 819.22 8.30 6 0 0 3.80 0.80 7 0 0 495.45 7.30 8 0 0 274.37 5.50 9 0 0 152.68 3.90 10 0 0 56.29 6.80 11 0 0 71.19 7.80 0 1 0 0.10 0.10 1 1 0 320.67 1.90 2 1 0 13.70 0.20 3 1 0 223.78 1.50 4 1 0 341.17 2.70 5 1 0 401.86 3.20 6 1 0 60.79 1.00 7 1 0 144.29 2.30 8 1 0 18.70 2.00 9 1 0 119.79 2.70 10 1 0 14.40 4.00 11 1 0 40.90 10.00 0 2 0 2795.02 42.20 1 2 0 266.37 1.70 2 2 0 2065.39 12.00 3 2 0 263.67 1.80 4 2 0 1062.29 7.20 5 2 0 1095.89 8.20 6 2 0 97.59 1.20 7 2 0 928.51 9.70 8 2 0 70.09 3.30 9 2 0 95.89 2.70 10 2 0 58.19 4.70 11 2 0 107.99 9.90 0 3 0 0.50 0.10 1 3 0 109.49 0.90 2 3 0 1211.78 7.20 3 3 0 60.99 0.60 4 3 0 682.63 5.60 5 3 0 79.99 1.40 6 3 0 76.19 1.10 7 3 0 20.70 1.40 8 3 0 83.79 2.60 9 3 0 17.40 2.70 10 3 0 50.79 5.70 11 3 0 33.40 16.30 0 4 0 5950.21 83.49 1 4 0 388.76 2.80 2 4 0 163.78 1.20 3 4 0 680.43 4.30 4 4 0 375.86 3.30 5 4 0 349.67 4.70 6 4 0 529.45 4.10 7 4 0 129.79 2.60 8 4 0 27.30 1.80 9 4 0 42.90 3.50 10 4 0 10.30 4.80 0 5 0 2.10 0.20 1 5 0 2614.64 17.70 2 5 0 11.20 0.30 3 5 0 116.39 1.00 4 5 0 16.30 0.60 5 5 0 30.60 1.60 6 5 0 152.48 1.80 7 5 0 70.29 2.30 8 5 0 16.20 2.30 9 5 0 9.40 2.70 10 5 0 26.60 5.50 0 6 0 644.64 9.30 1 6 0 1712.63 12.20 2 6 0 54.29 0.60 3 6 0 36.80 0.60 4 6 0 169.48 2.00 5 6 0 177.28 3.20 6 6 0 401.96 3.50 7 6 0 158.48 2.80 8 6 0 431.06 6.50 9 6 0 42.10 2.90 10 6 0 30.60 6.10 0 7 0 4.80 0.40 1 7 0 673.23 5.10 2 7 0 770.62 5.20 3 7 0 162.38 1.60 4 7 0 330.57 4.60 5 7 0 271.87 4.10 6 7 0 116.49 1.60 7 7 0 110.49 2.70 8 7 0 153.88 3.30 9 7 0 4.00 2.60 10 7 0 28.70 7.30 0 8 0 817.92 11.70 1 8 0 1008.60 10.10 2 8 0 86.99 0.90 3 8 0 134.39 1.40 4 8 0 296.87 3.00 5 8 0 27.60 1.60 6 8 0 85.79 1.50 7 8 0 400.66 4.90 8 8 0 143.09 3.60 9 8 0 3.30 2.60 10 8 0 96.79 6.40 0 9 0 1.10 0.40 1 9 0 104.59 1.30 2 9 0 58.09 0.70 3 9 0 162.48 2.20 4 9 0 135.99 2.10 5 9 0 67.49 1.40 6 9 0 129.09 2.10 7 9 0 124.39 2.80 8 9 0 25.40 2.60 9 9 0 109.49 3.50 0 10 0 752.02 11.70 1 10 0 226.08 3.10 2 10 0 183.48 1.60 3 10 0 180.98 2.20 4 10 0 129.39 2.50 5 10 0 515.15 5.10 6 10 0 15.40 1.30 7 10 0 3.70 1.90 8 10 0 18.50 2.70 9 10 0 70.69 3.70 0 11 0 6.10 0.70 1 11 0 78.79 1.40 2 11 0 356.76 2.80 3 11 0 128.49 2.30 4 11 0 47.70 2.40 5 11 0 50.39 1.90 6 11 0 12.20 1.50 7 11 0 5.70 2.40 8 11 0 14.80 3.40 9 11 0 36.10 3.20 0 12 0 418.06 6.90 1 12 0 163.48 2.40 2 12 0 214.58 2.10 3 12 0 178.68 3.00 4 12 0 87.89 1.80 5 12 0 143.69 2.40 6 12 0 16.00 1.70 7 12 0 110.09 4.90 8 12 0 23.00 3.10 0 13 0 6.70 0.90 1 13 0 53.49 1.60 2 13 0 14.10 0.70 3 13 0 141.59 2.10 4 13 0 8.50 1.50 5 13 0 63.19 2.10 6 13 0 12.80 2.40 7 13 0 76.69 3.50 8 13 0 37.40 3.20 0 14 0 195.68 3.80 1 14 0 363.26 5.40 2 14 0 289.47 2.80 3 14 0 79.59 1.90 4 14 0 36.00 1.50 5 14 0 8.30 2.50 6 14 0 59.39 2.70 7 14 0 90.59 3.60 0 15 0 47.20 33.90 1 15 0 37.20 1.80 2 15 0 132.09 1.80 3 15 0 293.07 4.30 4 15 0 24.20 1.10 5 15 0 31.70 2.50 6 15 0 42.20 3.80 0 16 0 87.19 2.50 1 16 0 64.29 2.20 2 16 0 9.20 0.90 3 16 0 65.29 2.90 4 16 0 102.69 2.80 5 16 0 10.20 2.90 6 16 0 74.79 5.60 0 17 0 1.80 1.50 1 17 0 91.59 2.90 2 17 0 44.80 1.30 3 17 0 51.89 2.60 4 17 0 0.00 6.90 5 17 0 38.70 3.20 0 18 0 63.89 2.90 1 18 0 125.59 3.10 2 18 0 166.58 2.90 3 18 0 335.57 7.40 0 19 0 1.80 2.00 1 19 0 7.80 2.30 -11 0 1 37.80 10.20 -10 0 1 238.98 7.30 -9 0 1 32.20 3.40 -8 0 1 13.60 2.70 -7 0 1 15.50 1.90 -6 0 1 44.20 1.30 -5 0 1 25.70 3.50 -4 0 1 1071.49 10.30 -3 0 1 2.70 0.30 -2 0 1 1133.79 9.00 -1 0 1 928.21 7.20 0 0 1 0.30 0.10 1 0 1 2246.68 17.20 2 0 1 475.45 4.10 3 0 1 22.80 0.50 4 0 1 0.10 0.70 5 0 1 275.77 4.80 6 0 1 211.58 2.80 7 0 1 672.23 10.40 8 0 1 255.17 4.70 9 0 1 181.18 4.30 10 0 1 2.80 6.40 11 0 1 9.60 4.90 -11 1 1 13.40 7.50 -10 1 1 26.90 4.30 -9 1 1 232.18 4.00 -8 1 1 30.50 2.00 -7 1 1 171.58 2.60 -6 1 1 60.99 1.00 -5 1 1 25.00 1.60 -4 1 1 65.49 1.50 -3 1 1 2129.89 12.20 -2 1 1 292.77 2.00 -1 1 1 5569.44 31.60 0 1 1 34.40 0.40 1 1 1 4727.73 26.60 2 1 1 85.49 0.70 3 1 1 70.49 0.60 4 1 1 599.14 6.00 5 1 1 402.96 4.90 6 1 1 1044.70 8.00 7 1 1 149.79 2.90 8 1 1 170.88 3.00 9 1 1 23.60 2.50 10 1 1 62.39 4.50 11 1 1 14.30 3.50 -11 2 1 35.00 8.20 -10 2 1 31.40 4.40 -9 2 1 15.90 2.50 -8 2 1 10.40 63.69 -7 2 1 183.78 2.40 -6 2 1 568.44 4.20 -5 2 1 168.18 4.00 -4 2 1 99.89 3.40 -3 2 1 257.97 1.70 -2 2 1 41.40 0.40 -1 2 1 163.18 1.40 0 2 1 608.74 6.10 1 2 1 630.44 4.30 2 2 1 145.79 1.00 3 2 1 418.96 2.60 4 2 1 987.40 9.10 5 2 1 901.21 9.00 6 2 1 59.19 1.10 7 2 1 292.37 3.70 8 2 1 15.00 2.00 9 2 1 45.30 2.50 10 2 1 16.20 4.70 11 2 1 92.69 27.70 -11 3 1 17.70 8.50 -10 3 1 18.90 4.30 -9 3 1 143.59 3.60 -8 3 1 88.19 2.20 -7 3 1 490.35 5.40 -6 3 1 132.09 1.40 -5 3 1 180.28 1.90 -4 3 1 221.08 3.60 -3 3 1 2770.22 15.50 -2 3 1 1025.90 6.30 -1 3 1 2148.49 16.60 0 3 1 238.28 2.50 1 3 1 1316.37 10.40 2 3 1 1566.74 9.20 3 3 1 1097.59 6.30 4 3 1 770.62 7.60 5 3 1 8.00 0.90 6 3 1 552.64 4.10 7 3 1 26.10 1.60 8 3 1 73.69 2.60 9 3 1 51.39 3.10 10 3 1 52.49 5.00 -10 4 1 60.79 5.80 -9 4 1 55.29 3.10 -8 4 1 52.09 2.10 -7 4 1 925.01 10.00 -6 4 1 69.89 1.10 -5 4 1 663.73 6.40 -4 4 1 140.39 2.30 -3 4 1 1142.09 7.00 -2 4 1 241.28 1.70 -1 4 1 3285.97 24.30 0 4 1 1139.49 10.80 1 4 1 2767.12 19.10 2 4 1 304.37 2.10 3 4 1 13.10 0.30 4 4 1 1049.09 8.60 5 4 1 49.90 1.80 6 4 1 49.00 1.00 7 4 1 22.90 1.40 8 4 1 83.09 2.80 9 4 1 87.19 3.00 10 4 1 19.00 4.70 -10 5 1 56.89 5.60 -9 5 1 14.40 2.70 -8 5 1 26.60 2.30 -7 5 1 53.39 2.30 -6 5 1 30.30 0.90 -5 5 1 300.17 2.90 -4 5 1 6.80 0.50 -3 5 1 399.26 2.80 -2 5 1 633.94 4.10 -1 5 1 396.86 3.20 0 5 1 167.58 1.70 1 5 1 129.79 1.30 2 5 1 1188.98 7.50 3 5 1 845.02 5.30 4 5 1 850.71 7.00 5 5 1 121.79 1.90 6 5 1 272.07 2.50 7 5 1 39.40 1.60 8 5 1 18.80 2.20 9 5 1 247.38 4.10 10 5 1 50.39 5.50 -10 6 1 161.48 6.80 -9 6 1 37.60 2.80 -8 6 1 69.69 2.60 -7 6 1 215.08 3.40 -6 6 1 95.49 1.60 -5 6 1 363.16 4.30 -4 6 1 167.08 2.10 -3 6 1 614.94 4.30 -2 6 1 1028.00 6.70 -1 6 1 1534.45 10.60 0 6 1 715.93 6.90 1 6 1 273.47 2.70 2 6 1 517.85 3.60 3 6 1 24.70 0.50 4 6 1 180.48 3.50 5 6 1 103.39 2.20 6 6 1 123.79 1.60 7 6 1 121.19 2.40 8 6 1 24.50 2.40 9 6 1 127.39 3.80 10 6 1 29.30 5.40 -10 7 1 7.50 5.00 -9 7 1 6.40 2.70 -8 7 1 25.70 2.40 -7 7 1 29.80 2.50 -6 7 1 67.59 1.30 -5 7 1 488.25 5.10 -4 7 1 567.14 5.80 -3 7 1 127.99 1.50 -2 7 1 876.41 5.90 -1 7 1 957.90 7.30 0 7 1 36.70 0.50 1 7 1 392.76 3.60 2 7 1 133.89 1.20 3 7 1 48.20 0.80 4 7 1 789.62 8.90 5 7 1 239.08 3.60 6 7 1 677.73 5.40 7 7 1 321.07 3.90 8 7 1 30.10 3.10 9 7 1 76.29 2.90 10 7 1 3.20 5.00 -10 8 1 24.20 5.10 -9 8 1 14.10 2.70 -8 8 1 33.90 3.00 -7 8 1 20.30 2.10 -6 8 1 112.89 1.60 -5 8 1 246.48 2.60 -4 8 1 48.40 1.80 -3 8 1 92.29 1.30 -2 8 1 49.70 0.70 -1 8 1 683.03 5.20 0 8 1 677.73 6.90 1 8 1 116.59 1.80 2 8 1 399.26 2.90 3 8 1 205.88 2.40 4 8 1 110.89 1.70 5 8 1 46.70 1.60 6 8 1 96.89 1.70 7 8 1 130.29 2.90 8 8 1 5.60 2.80 9 8 1 42.30 2.80 10 8 1 0.00 6.10 -9 9 1 10.10 2.80 -8 9 1 205.58 4.20 -7 9 1 62.79 2.40 -6 9 1 9.80 0.90 -5 9 1 9.60 1.20 -4 9 1 187.08 2.60 -3 9 1 297.97 3.50 -2 9 1 627.14 4.60 -1 9 1 43.70 1.00 0 9 1 252.87 2.70 1 9 1 129.39 1.40 2 9 1 147.59 1.40 3 9 1 768.52 7.50 4 9 1 36.00 1.30 5 9 1 518.65 5.80 6 9 1 2.70 1.20 7 9 1 137.19 2.80 8 9 1 69.79 2.90 9 9 1 57.89 3.00 -9 10 1 90.59 3.50 -8 10 1 100.69 3.60 -7 10 1 55.09 2.70 -6 10 1 89.69 1.80 -5 10 1 50.69 2.50 -4 10 1 372.56 4.90 -3 10 1 10.90 1.50 -2 10 1 305.67 2.60 -1 10 1 123.49 3.70 0 10 1 55.09 0.90 1 10 1 741.63 7.20 2 10 1 96.39 1.10 3 10 1 206.78 2.90 4 10 1 295.77 3.80 5 10 1 66.29 1.70 6 10 1 138.89 2.40 7 10 1 32.20 2.30 8 10 1 3.30 2.90 9 10 1 51.89 3.50 -9 11 1 76.39 3.20 -8 11 1 41.50 2.70 -7 11 1 32.90 2.50 -6 11 1 14.70 1.40 -5 11 1 203.68 2.90 -4 11 1 483.85 5.10 -3 11 1 247.08 3.50 -2 11 1 36.50 0.80 -1 11 1 30.90 1.20 0 11 1 296.07 3.60 1 11 1 157.88 2.10 2 11 1 25.50 0.60 3 11 1 286.67 3.90 4 11 1 202.48 2.40 5 11 1 20.10 1.50 6 11 1 34.60 1.60 7 11 1 31.50 2.50 8 11 1 6.40 3.00 9 11 1 37.90 44.70 -8 12 1 5.40 3.00 -7 12 1 27.50 2.70 -6 12 1 696.63 7.50 -5 12 1 27.70 2.10 -4 12 1 116.89 2.40 -3 12 1 206.18 4.10 -2 12 1 34.00 0.80 -1 12 1 37.10 1.70 0 12 1 323.17 3.80 1 12 1 236.68 2.60 2 12 1 135.29 1.70 3 12 1 60.59 3.30 4 12 1 60.09 1.40 5 12 1 181.78 3.10 6 12 1 73.09 3.00 7 12 1 19.40 3.30 8 12 1 45.40 3.40 -8 13 1 733.23 441.26 -7 13 1 17.90 5.30 -6 13 1 15.60 2.90 -5 13 1 66.79 2.30 -4 13 1 162.98 2.70 -3 13 1 31.60 2.20 -2 13 1 151.88 1.90 -1 13 1 0.50 1.10 0 13 1 7.50 0.70 1 13 1 18.30 1.20 2 13 1 177.38 1.90 3 13 1 20.80 1.40 4 13 1 14.60 1.50 5 13 1 156.18 2.90 6 13 1 78.89 3.70 7 13 1 3.80 2.50 8 13 1 166.98 4.00 -7 14 1 56.69 13.90 -6 14 1 33.50 2.90 -5 14 1 134.59 4.20 -4 14 1 32.40 1.70 -3 14 1 18.60 1.80 -2 14 1 131.99 1.90 -1 14 1 190.38 2.50 0 14 1 15.30 0.70 1 14 1 12.20 1.50 2 14 1 111.89 1.60 3 14 1 37.60 2.10 4 14 1 75.39 2.10 5 14 1 18.90 2.40 6 14 1 35.70 2.30 7 14 1 53.59 3.10 -6 15 1 19.20 5.10 -5 15 1 73.19 3.30 -4 15 1 63.39 2.20 -3 15 1 79.79 3.30 -2 15 1 4.40 0.90 -1 15 1 312.97 3.70 0 15 1 43.20 1.10 1 15 1 44.60 2.10 2 15 1 178.28 2.20 3 15 1 29.70 2.50 4 15 1 256.97 3.90 5 15 1 49.70 2.40 6 15 1 46.60 3.20 -6 16 1 42.30 5.60 -5 16 1 82.79 3.80 -4 16 1 2.10 2.30 -3 16 1 13.00 2.80 -2 16 1 36.70 1.20 -1 16 1 94.39 2.40 0 16 1 127.59 2.10 1 16 1 29.40 2.10 2 16 1 54.69 1.30 3 16 1 9.60 2.70 4 16 1 26.50 1.80 5 16 1 13.70 2.30 6 16 1 16.80 4.60 -5 17 1 162.58 5.20 -4 17 1 138.19 4.60 -3 17 1 16.80 2.90 -2 17 1 77.59 1.90 -1 17 1 69.29 2.30 0 17 1 64.49 1.90 1 17 1 43.30 2.10 2 17 1 235.28 3.10 3 17 1 127.39 3.10 4 17 1 247.38 4.40 5 17 1 91.39 4.20 -3 18 1 117.69 7.60 -2 18 1 15.40 3.50 -1 18 1 148.29 3.30 0 18 1 75.39 2.10 1 18 1 6.10 2.30 2 18 1 136.59 2.60 3 18 1 61.99 3.80 -1 19 1 10.90 2.50 0 19 1 56.09 1.90 1 19 1 3.20 2.70 -11 0 2 0.20 8.80 -10 0 2 201.98 6.70 -9 0 2 0.00 3.20 -8 0 2 130.69 4.30 -7 0 2 71.59 3.10 -6 0 2 4.30 0.80 -5 0 2 294.57 4.70 -4 0 2 64.79 1.10 -3 0 2 6603.14 50.59 -2 0 2 391.96 3.30 -1 0 2 593.14 4.90 0 0 2 9999.00 149.59 1 0 2 556.14 4.70 2 0 2 1848.12 15.10 3 0 2 5070.49 40.20 4 0 2 418.26 4.20 5 0 2 10.00 1.70 6 0 2 122.19 1.90 7 0 2 24.20 2.50 8 0 2 0.00 2.90 9 0 2 13.30 3.80 10 0 2 0.00 8.00 -11 1 2 11.10 7.30 -10 1 2 25.60 4.30 -9 1 2 18.60 2.50 -8 1 2 100.89 2.30 -7 1 2 67.49 1.60 -6 1 2 164.78 1.80 -5 1 2 524.45 5.70 -4 1 2 569.34 5.70 -3 1 2 865.21 5.00 -2 1 2 129.39 0.90 -1 1 2 534.45 3.30 0 1 2 580.04 5.30 1 1 2 209.98 1.40 2 1 2 726.13 4.20 3 1 2 46.60 0.50 4 1 2 870.51 7.40 5 1 2 60.79 2.40 6 1 2 531.15 4.30 7 1 2 93.49 2.60 8 1 2 59.29 2.30 9 1 2 8.30 2.60 10 1 2 14.40 4.60 -11 2 2 26.20 10.10 -10 2 2 87.59 4.40 -9 2 2 66.99 2.40 -8 2 2 595.04 5.90 -7 2 2 594.74 6.50 -6 2 2 199.88 1.90 -5 2 2 763.52 8.50 -4 2 2 674.33 7.90 -3 2 2 363.76 2.30 -2 2 2 780.72 4.60 -1 2 2 60.99 0.60 0 2 2 3648.83 33.80 1 2 2 4.60 0.20 2 2 2 3465.95 19.10 3 2 2 92.79 0.80 4 2 2 263.47 3.10 5 2 2 59.69 2.60 6 2 2 53.09 1.10 7 2 2 269.47 3.60 8 2 2 216.68 3.00 9 2 2 4.90 2.70 10 2 2 188.98 6.00 -11 3 2 60.39 11.80 -10 3 2 252.97 6.70 -9 3 2 101.39 3.00 -8 3 2 40.20 2.10 -7 3 2 143.29 2.30 -6 3 2 109.09 1.30 -5 3 2 105.99 1.30 -4 3 2 605.64 7.10 -3 3 2 440.56 2.80 -2 3 2 1293.17 8.40 -1 3 2 2843.02 21.20 0 3 2 2277.87 21.50 1 3 2 1972.00 13.80 2 3 2 1009.40 6.30 3 3 2 251.87 1.80 4 3 2 34.20 1.10 5 3 2 30.40 1.00 6 3 2 84.39 1.40 7 3 2 379.16 4.20 8 3 2 9.60 2.10 9 3 2 182.18 3.70 10 3 2 22.80 14.40 -10 4 2 48.70 4.80 -9 4 2 323.17 4.80 -8 4 2 5.50 2.00 -7 4 2 261.97 3.40 -6 4 2 299.37 2.70 -5 4 2 388.66 3.40 -4 4 2 445.56 6.30 -3 4 2 724.93 4.40 -2 4 2 159.38 1.20 -1 4 2 142.29 1.40 0 4 2 2379.86 23.90 1 4 2 1176.18 8.00 2 4 2 556.54 3.70 3 4 2 891.01 5.40 4 4 2 248.78 5.90 5 4 2 75.79 1.30 6 4 2 131.89 1.60 7 4 2 55.29 2.00 8 4 2 14.30 2.30 9 4 2 33.30 3.70 10 4 2 42.50 5.00 -10 5 2 35.80 5.00 -9 5 2 38.60 2.70 -8 5 2 16.80 2.20 -7 5 2 15.10 1.40 -6 5 2 17.10 0.70 -5 5 2 121.19 2.00 -4 5 2 220.68 4.40 -3 5 2 17.40 0.50 -2 5 2 133.89 1.10 -1 5 2 185.38 1.70 0 5 2 2774.52 27.70 1 5 2 88.59 0.90 2 5 2 48.00 0.50 3 5 2 320.07 2.70 4 5 2 653.23 6.70 5 5 2 271.77 2.80 6 5 2 13.50 0.80 7 5 2 16.90 1.40 8 5 2 106.89 2.80 9 5 2 11.30 2.40 10 5 2 44.50 5.00 -10 6 2 116.59 5.90 -9 6 2 53.79 2.90 -8 6 2 231.88 4.60 -7 6 2 148.79 3.10 -6 6 2 220.28 2.30 -5 6 2 203.38 2.70 -4 6 2 682.53 6.10 -3 6 2 119.99 1.30 -2 6 2 188.18 1.60 -1 6 2 11.00 0.50 0 6 2 1617.74 16.20 1 6 2 221.68 1.70 2 6 2 562.54 3.80 3 6 2 139.59 1.40 4 6 2 50.19 1.10 5 6 2 97.89 2.40 6 6 2 58.59 1.20 7 6 2 28.40 1.60 8 6 2 74.79 2.90 9 6 2 82.99 3.20 10 6 2 43.40 5.70 -10 7 2 34.90 5.10 -9 7 2 2.80 2.60 -8 7 2 76.09 2.80 -7 7 2 249.97 3.70 -6 7 2 24.10 0.90 -5 7 2 266.67 3.50 -4 7 2 593.74 8.90 -3 7 2 16.10 0.70 -2 7 2 633.94 4.40 -1 7 2 430.86 4.20 0 7 2 211.88 2.40 1 7 2 178.68 2.20 2 7 2 646.14 4.50 3 7 2 619.14 4.90 4 7 2 489.55 4.70 5 7 2 215.58 2.40 6 7 2 49.40 1.30 7 7 2 304.87 4.40 8 7 2 78.19 3.50 9 7 2 123.39 3.40 10 7 2 7.40 5.70 -10 8 2 100.79 5.70 -9 8 2 11.70 2.80 -8 8 2 110.99 3.80 -7 8 2 54.09 2.90 -6 8 2 131.79 1.90 -5 8 2 105.49 1.90 -4 8 2 60.99 1.70 -3 8 2 331.77 3.70 -2 8 2 217.48 1.90 -1 8 2 340.17 2.90 0 8 2 29.40 0.50 1 8 2 6.40 0.70 2 8 2 207.18 1.70 3 8 2 69.99 1.20 4 8 2 133.69 2.20 5 8 2 16.80 1.30 6 8 2 22.20 1.40 7 8 2 48.10 1.90 8 8 2 151.78 3.80 9 8 2 14.50 3.00 -9 9 2 89.29 3.40 -8 9 2 21.60 2.60 -7 9 2 52.39 2.30 -6 9 2 283.67 3.10 -5 9 2 172.08 4.10 -4 9 2 152.98 2.50 -3 9 2 284.77 4.70 -2 9 2 350.46 2.90 -1 9 2 158.38 3.20 0 9 2 117.29 1.40 1 9 2 562.04 5.20 2 9 2 304.27 2.50 3 9 2 82.39 1.50 4 9 2 340.77 3.50 5 9 2 184.68 3.60 6 9 2 310.97 3.70 7 9 2 24.90 3.40 8 9 2 28.50 2.90 9 9 2 72.19 4.20 -9 10 2 2.50 2.80 -8 10 2 44.40 2.60 -7 10 2 26.70 1.80 -6 10 2 31.30 1.90 -5 10 2 7.70 1.80 -4 10 2 155.68 4.10 -3 10 2 164.28 3.40 -2 10 2 45.20 1.20 -1 10 2 786.32 8.00 0 10 2 60.29 0.90 1 10 2 285.67 5.00 2 10 2 360.96 3.10 3 10 2 70.19 1.50 4 10 2 58.89 1.30 5 10 2 295.67 3.80 6 10 2 58.59 1.70 7 10 2 17.90 2.30 8 10 2 51.39 2.80 9 10 2 15.40 3.50 -9 11 2 17.70 3.50 -8 11 2 179.38 4.00 -7 11 2 12.60 1.80 -6 11 2 80.79 3.00 -5 11 2 17.40 1.90 -4 11 2 22.90 2.20 -3 11 2 582.14 7.40 -2 11 2 86.79 1.40 -1 11 2 721.13 8.80 0 11 2 242.38 2.90 1 11 2 605.64 8.10 2 11 2 125.09 1.60 3 11 2 92.99 2.00 4 11 2 245.08 3.10 5 11 2 5.40 1.90 6 11 2 141.09 2.50 7 11 2 20.30 2.90 8 11 2 246.98 4.60 -8 12 2 237.68 5.30 -7 12 2 51.29 4.80 -6 12 2 25.20 3.30 -5 12 2 153.28 4.00 -4 12 2 68.79 2.20 -3 12 2 758.22 8.30 -2 12 2 96.79 1.50 -1 12 2 104.29 2.40 0 12 2 162.08 2.10 1 12 2 216.08 2.70 2 12 2 422.46 3.80 3 12 2 55.99 1.70 4 12 2 53.89 1.60 5 12 2 87.19 2.20 6 12 2 25.20 1.90 7 12 2 16.90 3.10 8 12 2 48.70 24.30 -8 13 2 12.80 4.30 -7 13 2 24.90 4.50 -6 13 2 45.40 3.00 -5 13 2 7.30 2.90 -4 13 2 101.89 2.20 -3 13 2 9.80 1.70 -2 13 2 144.99 2.00 -1 13 2 53.99 1.80 0 13 2 145.19 2.10 1 13 2 176.48 2.50 2 13 2 33.40 0.90 3 13 2 80.99 2.00 4 13 2 216.18 3.10 5 13 2 3.80 1.90 6 13 2 38.40 2.10 7 13 2 47.50 4.10 8 13 2 58.79 22.20 -7 14 2 23.70 5.00 -6 14 2 29.70 5.40 -5 14 2 153.18 4.40 -4 14 2 180.48 3.20 -3 14 2 13.20 1.80 -2 14 2 55.59 1.40 -1 14 2 199.08 3.00 0 14 2 42.40 1.10 1 14 2 59.79 1.90 2 14 2 228.48 2.50 3 14 2 62.39 2.20 4 14 2 45.40 1.80 5 14 2 26.60 2.30 6 14 2 9.80 2.20 7 14 2 78.49 3.60 -6 15 2 7.70 6.30 -5 15 2 89.49 3.60 -4 15 2 66.89 3.30 -3 15 2 115.99 3.00 -2 15 2 38.60 1.50 -1 15 2 79.79 2.00 0 15 2 371.86 5.10 1 15 2 25.30 1.50 2 15 2 13.20 1.00 3 15 2 37.70 2.20 4 15 2 8.30 2.00 5 15 2 224.78 4.20 6 15 2 7.50 2.00 -6 16 2 8.90 3.30 -5 16 2 11.50 2.80 -4 16 2 10.80 2.30 -3 16 2 147.99 4.10 -2 16 2 15.10 1.50 -1 16 2 42.20 1.80 0 16 2 13.10 1.10 1 16 2 2.90 1.90 2 16 2 7.50 1.10 3 16 2 4.40 2.60 4 16 2 74.99 2.60 5 16 2 8.20 2.60 -5 17 2 62.49 4.20 -4 17 2 13.50 3.50 -3 17 2 37.80 3.80 -2 17 2 172.28 3.20 -1 17 2 36.50 2.30 0 17 2 160.78 2.90 1 17 2 13.70 2.20 2 17 2 73.09 1.70 3 17 2 117.99 3.40 4 17 2 89.19 11.60 -3 18 2 223.98 7.40 -2 18 2 68.69 2.70 -1 18 2 0.00 9.30 0 18 2 25.40 1.60 1 18 2 145.79 3.40 2 18 2 3.90 1.40 3 18 2 29.50 5.70 0 19 2 23.70 1.90 -11 0 3 53.39 10.40 -10 0 3 143.09 6.80 -9 0 3 31.80 3.60 -8 0 3 7.10 2.90 -7 0 3 529.75 10.00 -6 0 3 37.20 1.30 -5 0 3 223.98 2.80 -4 0 3 12.30 1.80 -3 0 3 7.40 0.40 -2 0 3 143.19 1.40 -1 0 3 1240.78 12.10 0 0 3 21.90 0.40 1 0 3 490.55 5.50 2 0 3 767.12 6.70 3 0 3 998.10 8.50 4 0 3 29.40 2.40 5 0 3 195.78 2.80 6 0 3 232.58 3.20 7 0 3 457.05 8.40 8 0 3 10.80 3.40 9 0 3 190.48 5.20 10 0 3 152.18 8.10 -11 1 3 18.90 8.50 -10 1 3 25.50 4.40 -9 1 3 110.39 2.60 -8 1 3 79.29 2.70 -7 1 3 432.86 4.40 -6 1 3 1022.80 7.60 -5 1 3 584.24 4.40 -4 1 3 351.36 4.80 -3 1 3 449.66 2.70 -2 1 3 168.48 1.10 -1 1 3 140.99 1.10 0 1 3 109.59 1.00 1 1 3 516.85 3.50 2 1 3 798.92 4.40 3 1 3 1322.97 7.60 4 1 3 198.68 3.60 5 1 3 77.49 1.40 6 1 3 266.17 2.70 7 1 3 22.00 1.80 8 1 3 111.89 2.70 9 1 3 14.80 3.00 10 1 3 7.80 5.30 -11 2 3 13.40 9.90 -10 2 3 18.10 3.80 -9 2 3 40.30 2.60 -8 2 3 14.40 1.80 -7 2 3 207.88 3.00 -6 2 3 19.60 0.70 -5 2 3 737.03 5.60 -4 2 3 384.96 3.90 -3 2 3 319.97 2.00 -2 2 3 75.59 0.60 -1 2 3 938.61 7.60 0 2 3 1040.30 9.50 1 2 3 3009.90 20.10 2 2 3 254.87 1.60 3 2 3 217.78 1.50 4 2 3 333.57 2.50 5 2 3 270.57 2.30 6 2 3 68.49 1.40 7 2 3 93.59 2.30 8 2 3 35.40 2.30 9 2 3 36.80 3.00 10 2 3 50.69 5.00 -10 3 3 46.20 5.10 -9 3 3 104.79 3.30 -8 3 3 253.77 3.70 -7 3 3 53.19 1.50 -6 3 3 887.31 6.90 -5 3 3 12.00 1.00 -4 3 3 242.38 2.00 -3 3 3 816.62 5.00 -2 3 3 440.46 2.80 -1 3 3 6662.63 46.90 0 3 3 3221.38 29.70 1 3 3 2830.32 21.30 2 3 3 61.69 0.60 3 3 3 111.89 1.00 4 3 3 244.78 2.00 5 3 3 96.59 2.00 6 3 3 240.58 2.70 7 3 3 335.27 4.00 8 3 3 272.27 4.00 9 3 3 0.00 3.00 10 3 3 5.40 4.80 -10 4 3 123.99 5.10 -9 4 3 120.39 3.30 -8 4 3 144.29 2.70 -7 4 3 108.09 2.20 -6 4 3 13.10 0.70 -5 4 3 24.60 1.20 -4 4 3 1618.74 11.80 -3 4 3 8.60 0.30 -2 4 3 10.20 0.30 -1 4 3 215.28 2.20 0 4 3 93.69 1.00 1 4 3 570.94 4.50 2 4 3 208.88 1.50 3 4 3 293.37 2.30 4 4 3 537.85 4.90 5 4 3 174.68 2.00 6 4 3 342.07 3.40 7 4 3 43.50 2.20 8 4 3 86.29 2.70 9 4 3 66.59 3.10 10 4 3 7.50 5.30 -10 5 3 34.50 4.50 -9 5 3 25.70 3.20 -8 5 3 93.89 2.40 -7 5 3 79.69 2.00 -6 5 3 316.57 2.90 -5 5 3 89.49 2.00 -4 5 3 747.43 7.60 -3 5 3 603.04 4.80 -2 5 3 233.98 1.80 -1 5 3 1737.33 15.50 0 5 3 476.85 4.50 1 5 3 2804.72 20.90 2 5 3 120.99 1.00 3 5 3 45.90 0.80 4 5 3 171.78 2.50 5 5 3 398.96 3.60 6 5 3 1107.69 8.40 7 5 3 56.79 2.50 8 5 3 81.59 2.90 9 5 3 52.59 3.10 10 5 3 12.20 5.30 -10 6 3 38.00 4.70 -9 6 3 86.29 3.40 -8 6 3 30.40 2.20 -7 6 3 15.90 1.60 -6 6 3 20.00 0.80 -5 6 3 400.56 4.30 -4 6 3 151.08 1.70 -3 6 3 80.59 1.20 -2 6 3 18.00 0.50 -1 6 3 431.76 5.30 0 6 3 429.96 4.30 1 6 3 1013.20 8.20 2 6 3 243.38 1.70 3 6 3 32.90 0.90 4 6 3 34.10 0.90 5 6 3 15.60 1.20 6 6 3 51.99 1.20 7 6 3 4.50 2.40 8 6 3 237.58 3.70 9 6 3 0.00 3.10 10 6 3 165.18 5.90 -10 7 3 6.00 4.80 -9 7 3 6.90 2.70 -8 7 3 36.90 2.50 -7 7 3 42.40 2.20 -6 7 3 817.52 7.00 -5 7 3 42.30 1.60 -4 7 3 101.39 3.20 -3 7 3 328.67 3.60 -2 7 3 285.47 2.30 -1 7 3 597.24 7.50 0 7 3 524.55 5.70 1 7 3 1585.44 13.20 2 7 3 863.21 5.80 3 7 3 585.84 4.50 4 7 3 189.68 2.60 5 7 3 325.47 3.90 6 7 3 146.39 1.90 7 7 3 76.09 2.20 8 7 3 23.30 3.00 9 7 3 1.60 3.50 10 7 3 41.50 6.60 -10 8 3 57.59 5.70 -9 8 3 53.49 2.80 -8 8 3 12.10 2.70 -7 8 3 86.49 2.40 -6 8 3 29.80 1.20 -5 8 3 37.70 1.40 -4 8 3 199.08 3.20 -3 8 3 266.57 2.80 -2 8 3 318.17 2.50 -1 8 3 416.66 4.40 0 8 3 292.77 3.30 1 8 3 183.98 2.30 2 8 3 134.19 1.20 3 8 3 570.14 5.10 4 8 3 270.17 3.10 5 8 3 53.69 1.60 6 8 3 183.98 2.70 7 8 3 28.90 2.30 8 8 3 30.60 9.50 9 8 3 84.39 4.00 -9 9 3 69.19 2.90 -8 9 3 56.79 3.00 -7 9 3 283.17 4.70 -6 9 3 9.00 1.30 -5 9 3 488.65 7.30 -4 9 3 24.30 2.50 -3 9 3 41.50 1.60 -2 9 3 314.87 2.60 -1 9 3 966.00 8.70 0 9 3 273.17 3.10 1 9 3 158.58 3.60 2 9 3 24.10 0.60 3 9 3 106.39 1.80 4 9 3 139.09 2.20 5 9 3 101.69 3.60 6 9 3 38.70 1.50 7 9 3 122.19 3.50 8 9 3 265.57 4.90 9 9 3 89.59 4.10 -9 10 3 36.20 6.40 -8 10 3 10.60 2.40 -7 10 3 1.80 1.80 -6 10 3 50.69 2.40 -5 10 3 61.49 3.40 -4 10 3 26.20 1.80 -3 10 3 172.08 3.00 -2 10 3 138.09 1.70 -1 10 3 218.98 3.00 0 10 3 83.19 1.20 1 10 3 58.09 1.60 2 10 3 618.64 5.00 3 10 3 30.10 1.10 4 10 3 514.85 5.70 5 10 3 152.78 2.60 6 10 3 4.50 1.30 7 10 3 128.79 3.40 8 10 3 17.40 9.50 9 10 3 61.59 4.20 -9 11 3 45.30 12.70 -8 11 3 14.00 3.40 -7 11 3 209.38 5.50 -6 11 3 55.99 2.70 -5 11 3 276.07 4.10 -4 11 3 104.69 3.20 -3 11 3 237.38 3.70 -2 11 3 363.36 3.40 -1 11 3 21.90 1.30 0 11 3 403.96 4.50 1 11 3 21.50 1.10 2 11 3 16.70 0.60 3 11 3 154.28 2.20 4 11 3 85.49 3.20 5 11 3 221.78 3.10 6 11 3 20.00 1.80 7 11 3 36.40 2.60 8 11 3 79.29 3.70 -8 12 3 21.60 4.20 -7 12 3 12.80 11.00 -6 12 3 54.49 3.40 -5 12 3 93.79 3.10 -4 12 3 54.89 2.20 -3 12 3 90.79 2.60 -2 12 3 81.79 1.50 -1 12 3 93.09 1.80 0 12 3 70.69 1.20 1 12 3 70.49 1.50 2 12 3 152.28 1.80 3 12 3 250.37 3.70 4 12 3 65.29 2.00 5 12 3 72.69 2.00 6 12 3 112.99 3.00 7 12 3 105.19 3.40 8 12 3 17.10 4.20 -8 13 3 12.90 5.40 -7 13 3 27.30 8.50 -6 13 3 107.49 4.30 -5 13 3 0.10 6.20 -4 13 3 92.99 2.90 -3 13 3 14.30 2.10 -2 13 3 204.88 2.80 -1 13 3 326.37 3.50 0 13 3 6.80 0.70 1 13 3 36.10 1.90 2 13 3 328.97 3.30 3 13 3 240.48 3.20 4 13 3 85.39 1.70 5 13 3 73.59 2.90 6 13 3 89.69 2.80 7 13 3 11.30 3.20 -7 14 3 13.90 5.00 -6 14 3 4.30 4.10 -5 14 3 12.90 3.30 -4 14 3 136.49 2.90 -3 14 3 80.19 2.60 -2 14 3 112.99 1.90 -1 14 3 32.00 1.70 0 14 3 42.50 1.20 1 14 3 47.30 1.50 2 14 3 2.20 0.80 3 14 3 25.60 2.00 4 14 3 40.40 2.30 5 14 3 102.49 3.20 6 14 3 13.20 2.20 7 14 3 59.79 4.10 -6 15 3 105.09 4.20 -5 15 3 126.99 4.90 -4 15 3 125.29 2.80 -3 15 3 63.39 3.10 -2 15 3 21.10 1.30 -1 15 3 34.10 2.40 0 15 3 40.50 1.20 1 15 3 308.87 3.80 2 15 3 11.20 1.00 3 15 3 88.59 2.90 4 15 3 169.58 2.80 5 15 3 2.00 2.20 6 15 3 81.79 3.80 -5 16 3 34.50 3.10 -4 16 3 69.99 3.00 -3 16 3 90.19 3.30 -2 16 3 54.89 1.80 -1 16 3 18.70 2.30 0 16 3 65.89 1.70 1 16 3 10.90 2.20 2 16 3 11.00 1.20 3 16 3 49.99 3.40 4 16 3 119.49 3.00 5 16 3 1.30 2.80 -4 17 3 44.20 3.20 -3 17 3 0.00 8.00 -2 17 3 27.10 2.20 -1 17 3 174.78 5.20 0 17 3 53.69 1.80 1 17 3 122.59 3.30 2 17 3 1.00 1.30 3 17 3 4.60 3.00 4 17 3 12.50 2.10 -3 18 3 20.20 6.10 -2 18 3 149.09 3.90 -1 18 3 0.00 13.50 0 18 3 11.00 1.50 1 18 3 46.60 7.70 2 18 3 29.00 1.70 3 18 3 124.19 3.40 -11 0 4 217.08 11.20 -10 0 4 108.09 29.00 -9 0 4 137.69 4.60 -8 0 4 36.10 2.60 -7 0 4 194.68 3.80 -6 0 4 64.99 1.50 -5 0 4 17.80 1.60 -4 0 4 528.35 5.40 -3 0 4 1202.48 9.90 -2 0 4 2142.79 17.10 -1 0 4 520.35 14.70 0 0 4 3076.59 40.00 1 0 4 1978.20 22.40 2 0 4 152.18 1.50 3 0 4 237.88 2.60 4 0 4 178.98 2.30 5 0 4 555.54 7.40 6 0 4 92.09 1.90 7 0 4 2.20 8.50 8 0 4 560.04 8.60 9 0 4 129.19 4.40 10 0 4 206.48 8.00 -11 1 4 70.19 10.00 -10 1 4 16.80 3.90 -9 1 4 90.39 2.50 -8 1 4 90.39 2.40 -7 1 4 358.36 3.70 -6 1 4 602.44 4.90 -5 1 4 84.99 1.30 -4 1 4 828.42 6.40 -3 1 4 111.39 0.90 -2 1 4 300.07 1.90 -1 1 4 1404.46 9.50 0 1 4 885.11 8.40 1 1 4 265.67 2.90 2 1 4 184.88 1.20 3 1 4 554.74 3.60 4 1 4 623.94 6.20 5 1 4 71.69 1.70 6 1 4 107.39 1.50 7 1 4 11.70 1.80 8 1 4 21.60 2.40 9 1 4 17.20 2.80 10 1 4 65.59 5.30 -10 2 4 104.09 5.80 -9 2 4 9.60 2.50 -8 2 4 13.40 2.10 -7 2 4 278.77 3.70 -6 2 4 269.97 2.70 -5 2 4 12.00 1.30 -4 2 4 18.20 1.20 -3 2 4 125.09 1.00 -2 2 4 2084.99 11.30 -1 2 4 963.70 8.30 0 2 4 8.30 0.20 1 2 4 1113.59 9.50 2 2 4 321.87 2.00 3 2 4 699.33 4.20 4 2 4 284.77 2.70 5 2 4 660.23 5.50 6 2 4 26.60 1.10 7 2 4 125.19 2.70 8 2 4 71.59 2.80 9 2 4 82.49 3.60 10 2 4 18.30 5.50 -10 3 4 44.30 5.30 -9 3 4 12.90 3.10 -8 3 4 41.50 2.10 -7 3 4 106.39 2.50 -6 3 4 143.19 1.80 -5 3 4 323.67 3.30 -4 3 4 28.30 1.10 -3 3 4 133.89 1.10 -2 3 4 1401.96 8.10 -1 3 4 711.23 5.40 0 3 4 2404.46 23.50 1 3 4 289.37 3.10 2 3 4 747.63 4.40 3 3 4 111.49 1.20 4 3 4 298.57 5.20 5 3 4 189.58 3.00 6 3 4 511.85 4.50 7 3 4 116.39 2.50 8 3 4 57.69 2.40 9 3 4 19.20 3.10 10 3 4 140.39 6.70 -10 4 4 34.90 4.40 -9 4 4 9.40 2.50 -8 4 4 71.39 2.30 -7 4 4 35.20 1.50 -6 4 4 427.46 4.20 -5 4 4 9.70 1.40 -4 4 4 239.88 3.80 -3 4 4 543.05 4.10 -2 4 4 180.18 1.40 -1 4 4 326.57 3.10 0 4 4 241.58 2.40 1 4 4 345.17 3.10 2 4 4 212.18 1.50 3 4 4 254.57 2.20 4 4 4 418.26 4.00 5 4 4 117.49 2.00 6 4 4 186.38 2.30 7 4 4 54.89 9.00 8 4 4 6.50 2.40 9 4 4 21.10 3.10 10 4 4 10.50 5.20 -10 5 4 29.70 4.80 -9 5 4 25.40 2.60 -8 5 4 46.30 2.30 -7 5 4 76.89 1.90 -6 5 4 125.29 1.70 -5 5 4 59.79 2.00 -4 5 4 313.37 3.30 -3 5 4 385.76 3.10 -2 5 4 30.00 0.50 -1 5 4 491.35 7.20 0 5 4 368.66 3.60 1 5 4 1546.65 11.90 2 5 4 492.85 3.30 3 5 4 651.13 5.10 4 5 4 34.30 0.90 5 5 4 308.27 4.40 6 5 4 195.68 2.70 7 5 4 167.88 3.00 8 5 4 2.50 2.70 9 5 4 3.80 3.00 10 5 4 24.80 5.50 -10 6 4 3.50 4.60 -9 6 4 7.40 3.20 -8 6 4 248.98 4.00 -7 6 4 19.50 1.40 -6 6 4 46.30 1.10 -5 6 4 19.70 1.10 -4 6 4 57.09 1.30 -3 6 4 826.72 6.10 -2 6 4 158.28 1.40 -1 6 4 380.56 3.80 0 6 4 45.10 0.60 1 6 4 104.79 1.70 2 6 4 40.80 0.50 3 6 4 55.49 0.90 4 6 4 252.57 3.00 5 6 4 245.38 3.50 6 6 4 107.39 1.90 7 6 4 28.80 2.40 8 6 4 65.89 3.40 9 6 4 87.89 3.40 10 6 4 21.20 6.00 -10 7 4 181.38 6.10 -9 7 4 18.70 2.90 -8 7 4 141.89 3.10 -7 7 4 254.87 3.90 -6 7 4 54.59 1.30 -5 7 4 213.28 3.40 -4 7 4 158.18 3.00 -3 7 4 140.89 2.00 -2 7 4 52.19 0.70 -1 7 4 284.77 4.10 0 7 4 54.69 0.80 1 7 4 377.86 4.10 2 7 4 106.39 1.00 3 7 4 17.30 0.80 4 7 4 228.18 2.40 5 7 4 381.96 4.30 6 7 4 337.67 3.70 7 7 4 211.18 3.90 8 7 4 89.19 2.70 9 7 4 0.20 3.00 -10 8 4 140.39 32.50 -9 8 4 5.60 3.00 -8 8 4 174.18 4.40 -7 8 4 67.69 2.10 -6 8 4 127.99 2.60 -5 8 4 49.90 1.90 -4 8 4 155.48 3.20 -3 8 4 123.09 2.70 -2 8 4 473.45 3.60 -1 8 4 324.97 3.70 0 8 4 6.20 0.40 1 8 4 144.69 2.10 2 8 4 273.77 2.30 3 8 4 424.46 4.90 4 8 4 29.70 1.60 5 8 4 157.98 2.20 6 8 4 32.20 1.30 7 8 4 126.49 2.70 8 8 4 34.30 3.10 9 8 4 13.30 3.30 -9 9 4 69.39 2.90 -8 9 4 151.68 3.60 -7 9 4 42.20 2.30 -6 9 4 469.45 6.60 -5 9 4 627.44 7.90 -4 9 4 152.08 2.80 -3 9 4 279.57 4.10 -2 9 4 273.77 2.60 -1 9 4 1057.09 16.80 0 9 4 127.99 1.70 1 9 4 1467.85 16.10 2 9 4 225.68 2.20 3 9 4 486.55 5.40 4 9 4 128.49 4.20 5 9 4 27.70 1.60 6 9 4 122.99 2.60 7 9 4 29.60 2.60 8 9 4 35.20 3.40 9 9 4 15.00 3.80 -9 10 4 64.89 3.70 -8 10 4 5.80 3.10 -7 10 4 23.50 4.20 -6 10 4 34.10 2.70 -5 10 4 99.69 3.00 -4 10 4 38.40 3.60 -3 10 4 52.59 1.90 -2 10 4 367.16 3.60 -1 10 4 45.30 1.80 0 10 4 236.78 3.20 1 10 4 70.29 1.40 2 10 4 25.50 0.70 3 10 4 176.98 2.50 4 10 4 93.59 2.30 5 10 4 686.73 7.90 6 10 4 74.29 2.30 7 10 4 53.19 2.60 8 10 4 261.17 5.80 -8 11 4 17.50 4.20 -7 11 4 45.20 4.80 -6 11 4 74.99 3.10 -5 11 4 74.99 3.20 -4 11 4 440.56 6.10 -3 11 4 14.30 1.90 -2 11 4 280.87 3.10 -1 11 4 84.39 2.00 0 11 4 136.19 1.80 1 11 4 28.30 1.30 2 11 4 402.56 3.70 3 11 4 26.40 1.70 4 11 4 29.90 1.90 5 11 4 74.49 2.40 6 11 4 70.19 2.30 7 11 4 96.79 30.50 8 11 4 10.50 4.20 -8 12 4 25.40 6.70 -7 12 4 18.20 4.60 -6 12 4 14.30 4.10 -5 12 4 48.80 2.70 -4 12 4 227.28 3.40 -3 12 4 87.09 3.40 -2 12 4 66.79 1.40 -1 12 4 56.89 2.70 0 12 4 94.59 1.40 1 12 4 280.77 3.10 2 12 4 67.29 1.30 3 12 4 473.05 5.30 4 12 4 100.29 1.80 5 12 4 123.79 2.60 6 12 4 47.80 2.40 7 12 4 162.68 5.40 8 12 4 33.10 3.90 -7 13 4 126.89 6.10 -6 13 4 21.70 3.40 -5 13 4 189.78 4.40 -4 13 4 16.10 1.90 -3 13 4 22.90 2.80 -2 13 4 218.18 2.70 -1 13 4 63.29 2.50 0 13 4 54.59 1.20 1 13 4 192.68 2.80 2 13 4 94.99 1.50 3 13 4 22.90 2.00 4 13 4 48.50 1.80 5 13 4 39.10 2.30 6 13 4 7.40 4.90 7 13 4 128.09 5.40 -7 14 4 80.29 6.40 -6 14 4 55.09 3.80 -5 14 4 89.79 4.40 -4 14 4 222.48 3.60 -3 14 4 74.99 2.80 -2 14 4 78.59 1.90 -1 14 4 261.57 3.90 0 14 4 134.99 2.30 1 14 4 100.39 2.90 2 14 4 147.69 2.00 3 14 4 45.90 2.50 4 14 4 127.79 2.50 5 14 4 5.20 2.30 6 14 4 7.40 2.40 -6 15 4 39.80 3.80 -5 15 4 23.90 3.60 -4 15 4 21.40 2.60 -3 15 4 210.28 4.50 -2 15 4 13.60 1.30 -1 15 4 2.30 2.10 0 15 4 94.99 2.00 1 15 4 6.30 1.90 2 15 4 229.48 2.80 3 15 4 53.29 2.90 4 15 4 5.40 1.80 5 15 4 0.00 7.90 6 15 4 94.59 3.60 -5 16 4 11.40 3.60 -4 16 4 66.69 3.70 -3 16 4 348.27 7.20 -2 16 4 19.30 1.50 -1 16 4 80.79 3.20 0 16 4 156.98 3.50 1 16 4 9.50 2.50 2 16 4 198.58 2.70 3 16 4 20.60 2.50 4 16 4 12.90 2.50 5 16 4 12.10 3.40 -4 17 4 11.50 2.80 -3 17 4 61.39 3.90 -2 17 4 21.10 2.10 -1 17 4 22.30 2.90 0 17 4 101.39 2.50 1 17 4 10.60 2.20 2 17 4 72.49 2.10 3 17 4 50.49 3.20 4 17 4 16.40 2.50 -3 18 4 46.10 10.10 -2 18 4 83.09 4.30 -1 18 4 30.10 3.50 0 18 4 11.40 1.70 1 18 4 119.99 3.20 2 18 4 24.00 1.70 -10 0 5 137.09 7.20 -9 0 5 91.59 4.90 -8 0 5 217.38 4.50 -7 0 5 375.96 7.30 -6 0 5 20.60 1.00 -5 0 5 51.59 3.60 -4 0 5 18.40 1.20 -3 0 5 1476.95 12.50 -2 0 5 132.89 1.40 -1 0 5 359.06 5.90 0 0 5 47.60 0.80 1 0 5 601.84 8.00 2 0 5 3.60 0.30 3 0 5 98.79 1.60 4 0 5 326.67 4.80 5 0 5 11.80 1.50 6 0 5 678.23 7.30 7 0 5 33.80 3.30 8 0 5 5.00 3.90 9 0 5 320.17 7.60 10 0 5 0.00 8.10 -10 1 5 48.00 4.40 -9 1 5 131.59 3.30 -8 1 5 117.39 2.40 -7 1 5 93.19 1.70 -6 1 5 239.48 2.30 -5 1 5 180.98 2.20 -4 1 5 464.65 5.60 -3 1 5 972.60 6.20 -2 1 5 31.20 0.40 -1 1 5 294.67 4.80 0 1 5 200.68 2.10 1 1 5 1010.40 7.90 2 1 5 372.76 2.20 3 1 5 295.47 2.60 4 1 5 389.66 5.20 5 1 5 242.18 3.10 6 1 5 55.89 1.40 7 1 5 17.00 2.60 8 1 5 41.80 2.70 9 1 5 5.80 3.20 10 1 5 21.30 4.80 -10 2 5 32.50 5.00 -9 2 5 76.39 3.10 -8 2 5 33.70 2.20 -7 2 5 104.99 2.20 -6 2 5 287.37 2.80 -5 2 5 72.69 3.00 -4 2 5 82.89 1.80 -3 2 5 61.89 0.70 -2 2 5 901.81 5.10 -1 2 5 1572.54 13.90 0 2 5 123.49 1.20 1 2 5 1184.68 12.40 2 2 5 804.92 4.60 3 2 5 65.59 0.80 4 2 5 419.96 3.40 5 2 5 67.39 3.00 6 2 5 181.58 2.20 7 2 5 22.70 2.60 8 2 5 236.38 4.00 9 2 5 2.70 3.00 10 2 5 46.70 5.50 -10 3 5 23.30 5.40 -9 3 5 23.30 2.80 -8 3 5 155.58 3.40 -7 3 5 80.09 2.50 -6 3 5 26.50 0.90 -5 3 5 274.47 3.50 -4 3 5 991.40 8.80 -3 3 5 283.97 2.20 -2 3 5 22.30 0.40 -1 3 5 635.04 7.10 0 3 5 1058.09 9.60 1 3 5 1047.90 8.70 2 3 5 216.58 1.40 3 3 5 539.55 4.30 4 3 5 604.94 5.10 5 3 5 66.09 1.50 6 3 5 123.39 1.90 7 3 5 57.09 2.40 8 3 5 110.39 3.10 9 3 5 24.50 3.00 10 3 5 46.60 5.60 -10 4 5 84.29 5.30 -9 4 5 159.68 3.70 -8 4 5 17.00 2.20 -7 4 5 322.47 4.20 -6 4 5 82.59 1.50 -5 4 5 136.89 2.10 -4 4 5 182.98 2.90 -3 4 5 581.74 4.30 -2 4 5 272.17 1.80 -1 4 5 338.77 3.90 0 4 5 187.08 1.90 1 4 5 692.53 5.90 2 4 5 19.70 0.40 3 4 5 1018.70 7.30 4 4 5 56.19 1.10 5 4 5 70.09 1.60 6 4 5 63.39 1.60 7 4 5 13.90 2.70 8 4 5 72.09 3.40 9 4 5 19.40 2.90 10 4 5 68.69 6.20 -10 5 5 1.80 4.90 -9 5 5 35.40 3.10 -8 5 5 131.59 2.70 -7 5 5 56.09 2.00 -6 5 5 992.10 8.30 -5 5 5 198.18 3.00 -4 5 5 68.69 1.20 -3 5 5 156.98 2.10 -2 5 5 56.69 0.80 -1 5 5 494.75 3.90 0 5 5 721.63 6.90 1 5 5 30.50 1.30 2 5 5 477.75 3.10 3 5 5 503.95 4.50 4 5 5 26.20 1.20 5 5 5 154.08 2.50 6 5 5 56.59 1.50 7 5 5 162.98 3.20 8 5 5 69.49 3.40 9 5 5 144.89 4.00 10 5 5 84.79 9.60 -10 6 5 91.89 5.80 -9 6 5 91.89 3.20 -8 6 5 45.10 2.90 -7 6 5 115.79 2.10 -6 6 5 13.30 0.80 -5 6 5 234.98 3.40 -4 6 5 229.28 3.40 -3 6 5 103.59 1.40 -2 6 5 2252.67 14.10 -1 6 5 13.00 1.60 0 6 5 1465.95 14.20 1 6 5 444.76 3.30 2 6 5 254.77 1.80 3 6 5 608.64 5.10 4 6 5 40.10 2.10 5 6 5 916.61 10.00 6 6 5 23.40 1.80 7 6 5 211.28 3.60 8 6 5 33.10 3.20 9 6 5 29.20 3.30 -10 7 5 14.40 4.30 -9 7 5 72.49 3.30 -8 7 5 24.20 3.10 -7 7 5 157.28 2.80 -6 7 5 65.69 2.00 -5 7 5 133.09 3.30 -4 7 5 27.10 1.80 -3 7 5 499.05 4.30 -2 7 5 120.19 1.20 -1 7 5 507.85 6.20 0 7 5 59.79 0.90 1 7 5 403.86 5.10 2 7 5 175.98 1.50 3 7 5 548.85 5.20 4 7 5 167.48 3.20 5 7 5 472.55 6.60 6 7 5 16.60 1.50 7 7 5 71.89 2.60 8 7 5 20.10 3.10 9 7 5 8.80 3.60 -9 8 5 154.88 3.80 -8 8 5 11.70 2.60 -7 8 5 58.19 2.50 -6 8 5 167.88 3.20 -5 8 5 34.00 2.50 -4 8 5 320.87 3.70 -3 8 5 586.94 7.10 -2 8 5 333.07 3.00 -1 8 5 102.89 1.70 0 8 5 821.42 8.80 1 8 5 28.60 1.10 2 8 5 710.03 5.50 3 8 5 266.87 3.30 4 8 5 232.28 2.50 5 8 5 136.39 2.40 6 8 5 28.10 1.40 7 8 5 203.98 3.80 8 8 5 88.59 3.60 9 8 5 0.00 3.60 -9 9 5 0.00 3.80 -8 9 5 168.98 4.80 -7 9 5 8.40 5.30 -6 9 5 76.69 3.30 -5 9 5 2.90 2.60 -4 9 5 903.41 9.80 -3 9 5 275.07 5.30 -2 9 5 185.78 2.20 -1 9 5 162.28 3.60 0 9 5 432.76 5.10 1 9 5 226.38 3.10 2 9 5 310.47 3.10 3 9 5 64.59 2.60 4 9 5 64.59 1.90 5 9 5 17.30 1.60 6 9 5 1.60 1.30 7 9 5 11.10 2.30 8 9 5 32.40 5.00 9 9 5 100.29 4.40 -9 10 5 0.00 15.10 -8 10 5 170.98 5.00 -7 10 5 39.30 3.80 -6 10 5 29.80 3.10 -5 10 5 168.58 6.30 -4 10 5 176.78 3.60 -3 10 5 119.99 3.20 -2 10 5 593.14 5.10 -1 10 5 286.47 5.60 0 10 5 3.20 0.60 1 10 5 390.76 4.80 2 10 5 61.69 1.10 3 10 5 77.79 1.70 4 10 5 103.49 2.10 5 10 5 25.80 1.90 6 10 5 124.09 2.80 7 10 5 32.70 3.90 8 10 5 18.00 3.80 -8 11 5 115.69 5.30 -7 11 5 14.70 3.90 -6 11 5 16.30 2.50 -5 11 5 216.98 4.10 -4 11 5 224.78 3.50 -3 11 5 4.20 6.10 -2 11 5 240.58 2.90 -1 11 5 301.17 5.20 0 11 5 167.68 2.50 1 11 5 319.57 4.30 2 11 5 68.29 1.20 3 11 5 65.39 1.70 4 11 5 13.90 1.40 5 11 5 31.20 2.00 6 11 5 83.19 2.70 7 11 5 6.20 3.50 8 11 5 122.89 4.80 -8 12 5 150.98 6.30 -7 12 5 11.70 4.40 -6 12 5 99.59 4.60 -5 12 5 34.00 3.10 -4 12 5 21.60 1.90 -3 12 5 160.58 4.40 -2 12 5 144.79 2.20 -1 12 5 270.27 3.90 0 12 5 193.28 2.80 1 12 5 82.09 2.10 2 12 5 217.28 2.60 3 12 5 209.28 3.50 4 12 5 173.28 2.40 5 12 5 126.19 3.10 6 12 5 55.89 2.60 7 12 5 68.39 6.40 -7 13 5 68.19 7.70 -6 13 5 82.89 4.20 -5 13 5 15.00 2.90 -4 13 5 132.99 2.90 -3 13 5 64.69 2.70 -2 13 5 69.69 1.70 -1 13 5 18.50 2.40 0 13 5 131.49 2.50 1 13 5 188.48 2.80 2 13 5 83.29 1.60 3 13 5 208.38 3.60 4 13 5 62.49 2.30 5 13 5 27.30 2.30 6 13 5 18.70 4.00 7 13 5 55.99 5.70 -7 14 5 61.09 6.90 -6 14 5 27.50 6.90 -5 14 5 69.69 3.90 -4 14 5 35.70 2.80 -3 14 5 66.89 3.10 -2 14 5 73.69 1.90 -1 14 5 128.39 2.60 0 14 5 34.30 1.20 1 14 5 48.20 2.20 2 14 5 61.19 1.40 3 14 5 62.29 2.70 4 14 5 80.19 2.20 5 14 5 15.50 2.70 6 14 5 34.70 4.40 -6 15 5 40.60 3.70 -5 15 5 47.60 4.00 -4 15 5 19.30 2.30 -3 15 5 37.20 6.00 -2 15 5 90.29 2.20 -1 15 5 56.39 2.80 0 15 5 35.70 1.40 1 15 5 67.29 2.60 2 15 5 36.70 1.20 3 15 5 53.79 3.10 4 15 5 100.99 2.50 5 15 5 24.10 3.40 -5 16 5 60.49 4.10 -4 16 5 147.69 3.70 -3 16 5 111.49 4.00 -2 16 5 252.97 4.20 -1 16 5 15.20 3.10 0 16 5 96.19 2.70 1 16 5 78.99 2.90 2 16 5 22.60 2.20 3 16 5 108.89 3.40 4 16 5 33.60 2.80 -4 17 5 21.50 3.40 -3 17 5 3.10 3.80 -2 17 5 3.90 2.00 -1 17 5 32.70 3.70 0 17 5 98.69 3.20 1 17 5 24.40 7.30 2 17 5 62.09 2.30 3 17 5 16.00 3.60 -2 18 5 15.60 2.70 -1 18 5 72.59 4.50 0 18 5 173.88 4.40 1 18 5 0.50 2.70 -10 0 6 2.30 5.60 -9 0 6 72.39 3.70 -8 0 6 67.29 5.00 -7 0 6 111.89 3.30 -6 0 6 40.70 1.40 -5 0 6 53.59 1.60 -4 0 6 341.97 5.10 -3 0 6 329.57 3.50 -2 0 6 67.29 0.80 -1 0 6 1595.64 19.70 0 0 6 117.49 1.70 1 0 6 1030.60 16.40 2 0 6 11.40 0.40 3 0 6 31.10 1.40 4 0 6 158.28 2.70 5 0 6 365.86 5.20 6 0 6 89.99 2.60 7 0 6 535.05 11.90 8 0 6 9.60 5.00 9 0 6 145.79 5.20 10 0 6 45.50 53.19 -10 1 6 6.80 4.60 -9 1 6 11.20 2.70 -8 1 6 135.29 2.50 -7 1 6 237.78 3.10 -6 1 6 173.78 2.10 -5 1 6 245.68 3.20 -4 1 6 927.61 8.10 -3 1 6 909.31 6.30 -2 1 6 143.99 1.00 -1 1 6 203.28 3.10 0 1 6 444.66 4.20 1 1 6 600.04 4.80 2 1 6 366.16 2.20 3 1 6 550.54 3.60 4 1 6 492.25 4.00 5 1 6 90.69 1.80 6 1 6 96.09 1.90 7 1 6 172.28 3.40 8 1 6 42.70 3.10 9 1 6 83.09 14.50 10 1 6 158.28 6.20 -10 2 6 92.89 5.10 -9 2 6 120.49 3.50 -8 2 6 147.69 2.90 -7 2 6 159.18 2.80 -6 2 6 35.80 0.90 -5 2 6 853.31 7.50 -4 2 6 66.79 1.90 -3 2 6 78.19 0.90 -2 2 6 664.83 3.90 -1 2 6 44.80 1.40 0 2 6 1553.04 13.60 1 2 6 348.47 2.70 2 2 6 1102.29 6.30 3 2 6 550.94 4.00 4 2 6 69.59 1.60 5 2 6 10.60 1.40 6 2 6 373.26 3.90 7 2 6 9.80 2.20 8 2 6 33.10 10.50 9 2 6 62.19 3.70 10 2 6 90.29 5.70 -10 3 6 193.98 6.60 -9 3 6 37.00 3.10 -8 3 6 41.00 2.30 -7 3 6 18.50 1.70 -6 3 6 175.48 2.10 -5 3 6 68.79 1.60 -4 3 6 144.79 3.00 -3 3 6 615.24 5.10 -2 3 6 414.46 2.50 -1 3 6 83.19 1.40 0 3 6 118.09 1.20 1 3 6 198.48 1.80 2 3 6 133.89 1.00 3 3 6 1054.49 8.80 4 3 6 163.38 3.00 5 3 6 103.19 1.80 6 3 6 167.88 2.40 7 3 6 94.09 2.90 8 3 6 59.99 3.60 9 3 6 99.79 3.60 10 3 6 143.09 25.60 -10 4 6 13.60 4.80 -9 4 6 150.88 3.40 -8 4 6 82.89 2.40 -7 4 6 71.49 2.60 -6 4 6 293.77 3.10 -5 4 6 74.29 1.60 -4 4 6 75.49 1.20 -3 4 6 27.00 1.30 -2 4 6 243.88 1.70 -1 4 6 273.47 2.70 0 4 6 148.99 1.50 1 4 6 162.38 2.00 2 4 6 608.04 3.70 3 4 6 71.59 1.20 4 4 6 124.09 1.60 5 4 6 299.37 3.20 6 4 6 38.40 1.50 7 4 6 51.99 2.60 8 4 6 16.40 3.40 9 4 6 21.00 3.50 -10 5 6 33.20 5.10 -9 5 6 46.90 4.80 -8 5 6 9.60 2.40 -7 5 6 92.29 2.60 -6 5 6 53.09 1.30 -5 5 6 116.59 2.10 -4 5 6 66.19 1.30 -3 5 6 442.16 4.70 -2 5 6 161.68 1.30 -1 5 6 116.09 2.90 0 5 6 73.59 0.90 1 5 6 567.24 4.70 2 5 6 177.78 1.30 3 5 6 48.70 2.10 4 5 6 565.54 5.00 5 5 6 391.26 6.00 6 5 6 84.19 1.80 7 5 6 11.00 2.50 8 5 6 253.87 4.70 9 5 6 43.80 4.00 -10 6 6 52.19 5.80 -9 6 6 56.39 3.10 -8 6 6 67.49 2.90 -7 6 6 107.99 2.40 -6 6 6 398.76 4.20 -5 6 6 457.25 7.40 -4 6 6 408.96 4.50 -3 6 6 210.28 3.10 -2 6 6 226.78 1.90 -1 6 6 651.13 6.40 0 6 6 452.35 4.70 1 6 6 289.67 4.30 2 6 6 19.50 0.40 3 6 6 234.08 3.60 4 6 6 68.79 2.10 5 6 6 67.89 3.40 6 6 6 89.89 1.80 7 6 6 101.59 3.10 8 6 6 53.69 3.40 9 6 6 107.99 4.00 -9 7 6 64.49 3.00 -8 7 6 6.30 2.90 -7 7 6 313.27 5.40 -6 7 6 183.38 3.00 -5 7 6 345.57 6.30 -4 7 6 300.67 4.30 -3 7 6 74.79 2.30 -2 7 6 44.80 0.90 -1 7 6 7.60 1.30 0 7 6 29.80 0.60 1 7 6 269.27 2.40 2 7 6 41.70 0.70 3 7 6 1056.49 10.30 4 7 6 747.33 8.00 5 7 6 123.19 2.00 6 7 6 75.29 2.90 7 7 6 41.00 2.30 8 7 6 46.40 3.60 9 7 6 1.70 3.70 -9 8 6 73.49 3.10 -8 8 6 103.09 4.00 -7 8 6 1.60 2.30 -6 8 6 3.80 2.00 -5 8 6 27.30 3.10 -4 8 6 6.90 2.00 -3 8 6 93.59 2.60 -2 8 6 162.38 2.00 -1 8 6 66.49 1.70 0 8 6 143.69 1.70 1 8 6 94.89 1.70 2 8 6 354.36 3.00 3 8 6 51.39 1.60 4 8 6 227.38 2.60 5 8 6 416.26 5.00 6 8 6 71.69 2.10 7 8 6 92.19 3.50 8 8 6 22.20 3.50 9 8 6 89.89 4.30 -9 9 6 34.10 4.10 -8 9 6 39.20 3.60 -7 9 6 7.50 4.30 -6 9 6 23.00 3.30 -5 9 6 27.10 3.40 -4 9 6 232.98 3.50 -3 9 6 742.73 7.50 -2 9 6 945.01 8.00 -1 9 6 139.79 2.30 0 9 6 182.38 2.40 1 9 6 64.99 1.70 2 9 6 892.41 7.10 3 9 6 387.56 4.90 4 9 6 354.36 5.30 5 9 6 198.28 3.20 6 9 6 90.19 2.30 7 9 6 118.69 5.00 8 9 6 20.10 3.70 -8 10 6 84.19 5.50 -7 10 6 66.09 4.50 -6 10 6 6.80 5.50 -5 10 6 130.09 3.50 -4 10 6 187.68 3.70 -3 10 6 64.29 2.60 -2 10 6 516.65 4.70 -1 10 6 4.40 1.20 0 10 6 108.19 1.70 1 10 6 19.30 1.30 2 10 6 296.47 2.90 3 10 6 139.79 2.70 4 10 6 2.80 1.60 5 10 6 83.09 2.40 6 10 6 48.40 1.90 7 10 6 75.89 4.70 8 10 6 4.20 4.20 -8 11 6 9.70 5.50 -7 11 6 52.39 102.29 -6 11 6 27.40 4.00 -5 11 6 32.10 2.90 -4 11 6 75.79 2.10 -3 11 6 55.79 2.80 -2 11 6 111.39 1.90 -1 11 6 115.39 2.70 0 11 6 117.79 1.80 1 11 6 89.79 2.00 2 11 6 78.79 1.40 3 11 6 121.49 2.50 4 11 6 76.59 2.00 5 11 6 74.79 2.70 6 11 6 157.78 4.00 7 11 6 65.59 5.00 8 11 6 4.00 561.44 -8 12 6 34.40 5.70 -7 12 6 440.26 10.90 -6 12 6 13.40 6.00 -5 12 6 54.99 3.90 -4 12 6 26.80 2.30 -3 12 6 210.88 4.70 -2 12 6 460.65 4.60 -1 12 6 111.09 2.80 0 12 6 509.55 7.30 1 12 6 99.49 2.20 2 12 6 217.48 2.50 3 12 6 75.29 2.20 4 12 6 44.30 1.80 5 12 6 34.10 2.40 6 12 6 1.60 2.00 7 12 6 27.90 4.00 -7 13 6 19.90 6.60 -6 13 6 41.40 5.00 -5 13 6 69.19 4.00 -4 13 6 108.49 2.90 -3 13 6 135.09 4.00 -2 13 6 223.98 3.00 -1 13 6 0.00 1.60 0 13 6 32.40 1.10 1 13 6 38.50 1.90 2 13 6 23.40 1.00 3 13 6 34.50 2.60 4 13 6 136.39 2.50 5 13 6 5.30 2.30 6 13 6 2.30 2.50 -6 14 6 509.75 242.38 -5 14 6 148.79 4.30 -4 14 6 20.80 2.40 -3 14 6 211.88 4.70 -2 14 6 148.29 2.80 -1 14 6 206.48 3.70 0 14 6 74.29 1.70 1 14 6 57.19 2.60 2 14 6 17.10 1.20 3 14 6 115.69 3.30 4 14 6 41.00 2.10 5 14 6 107.99 4.00 6 14 6 19.70 2.70 -6 15 6 27.90 2.80 -5 15 6 25.50 12.30 -4 15 6 17.80 2.60 -3 15 6 155.58 4.30 -2 15 6 3.60 1.60 -1 15 6 7.40 2.80 0 15 6 14.00 1.20 1 15 6 67.09 2.60 2 15 6 13.80 1.40 3 15 6 315.97 5.00 4 15 6 38.20 2.90 5 15 6 147.29 5.00 -5 16 6 44.90 2.60 -4 16 6 89.19 3.80 -3 16 6 0.30 12.30 -2 16 6 40.90 2.00 -1 16 6 85.89 3.80 0 16 6 141.39 3.90 1 16 6 54.39 2.60 2 16 6 74.99 2.40 3 16 6 15.40 3.50 4 16 6 119.89 3.40 -3 17 6 8.10 4.10 -2 17 6 36.40 4.80 -1 17 6 29.00 4.00 0 17 6 15.90 1.90 1 17 6 71.99 2.80 2 17 6 5.40 1.60 3 17 6 27.30 5.50 -10 0 7 246.18 29.20 -9 0 7 37.30 4.20 -8 0 7 94.59 14.00 -7 0 7 17.60 2.90 -6 0 7 551.64 6.40 -5 0 7 61.09 3.10 -4 0 7 126.19 2.70 -3 0 7 66.79 1.30 -2 0 7 39.60 0.70 -1 0 7 93.79 1.70 0 0 7 100.19 1.50 1 0 7 66.49 1.50 2 0 7 701.63 5.60 3 0 7 93.19 2.40 4 0 7 27.40 1.20 5 0 7 138.79 4.90 6 0 7 101.59 4.80 7 0 7 150.68 4.80 8 0 7 0.00 5.30 9 0 7 519.95 12.50 -10 1 7 79.89 5.10 -9 1 7 24.60 3.30 -8 1 7 97.69 2.80 -7 1 7 237.88 3.30 -6 1 7 47.60 1.40 -5 1 7 139.19 2.10 -4 1 7 45.00 2.00 -3 1 7 31.70 0.90 -2 1 7 822.62 4.60 -1 1 7 70.39 1.50 0 1 7 655.23 6.20 1 1 7 307.47 2.50 2 1 7 124.79 1.00 3 1 7 445.26 4.10 4 1 7 8.50 1.30 5 1 7 118.79 1.90 6 1 7 63.19 1.70 7 1 7 61.19 2.80 8 1 7 17.40 3.10 9 1 7 15.70 3.80 -10 2 7 21.90 5.00 -9 2 7 22.70 2.90 -8 2 7 206.18 3.80 -7 2 7 64.79 2.20 -6 2 7 108.99 2.00 -5 2 7 159.18 2.10 -4 2 7 189.98 2.20 -3 2 7 97.99 1.70 -2 2 7 303.17 2.00 -1 2 7 496.05 4.90 0 2 7 107.39 1.10 1 2 7 299.87 3.80 2 2 7 51.59 0.60 3 2 7 51.09 1.30 4 2 7 143.59 1.60 5 2 7 180.38 2.90 6 2 7 58.39 1.90 7 2 7 79.99 2.90 8 2 7 92.69 4.10 9 2 7 126.69 4.00 -10 3 7 17.30 4.90 -9 3 7 76.69 2.80 -8 3 7 39.90 2.50 -7 3 7 3.30 2.30 -6 3 7 61.19 1.60 -5 3 7 34.90 1.50 -4 3 7 573.14 5.50 -3 3 7 685.43 7.10 -2 3 7 148.69 1.20 -1 3 7 592.74 4.90 0 3 7 161.68 1.60 1 3 7 145.39 2.70 2 3 7 215.68 1.50 3 3 7 19.60 2.80 4 3 7 267.77 2.50 5 3 7 107.89 3.20 6 3 7 34.50 1.60 7 3 7 95.99 3.40 8 3 7 84.09 3.30 9 3 7 29.60 3.50 -10 4 7 15.90 8.10 -9 4 7 18.90 2.80 -8 4 7 96.69 3.10 -7 4 7 44.00 2.30 -6 4 7 69.59 1.70 -5 4 7 41.10 1.90 -4 4 7 31.70 1.20 -3 4 7 115.89 1.50 -2 4 7 618.24 3.70 -1 4 7 255.57 2.50 0 4 7 1741.13 16.00 1 4 7 102.29 1.60 2 4 7 101.39 0.90 3 4 7 54.99 1.90 4 4 7 99.69 2.10 5 4 7 108.19 1.90 6 4 7 91.99 2.40 7 4 7 18.00 2.60 8 4 7 51.39 3.50 9 4 7 46.10 3.80 -10 5 7 80.09 3.90 -9 5 7 104.19 3.70 -8 5 7 172.48 3.50 -7 5 7 0.00 2.40 -6 5 7 27.70 1.20 -5 5 7 580.14 6.60 -4 5 7 33.30 2.20 -3 5 7 1275.57 10.40 -2 5 7 235.98 1.80 -1 5 7 158.78 1.80 0 5 7 111.79 1.20 1 5 7 105.99 1.50 2 5 7 105.99 1.00 3 5 7 64.89 1.60 4 5 7 637.64 8.70 5 5 7 38.00 2.00 6 5 7 179.08 2.90 7 5 7 169.38 3.70 8 5 7 86.29 3.40 9 5 7 96.29 4.10 -9 6 7 49.60 3.20 -8 6 7 135.49 3.40 -7 6 7 136.59 2.90 -6 6 7 21.10 1.00 -5 6 7 792.72 7.10 -4 6 7 362.16 4.00 -3 6 7 335.17 4.50 -2 6 7 223.08 2.00 -1 6 7 966.20 10.10 0 6 7 354.96 3.70 1 6 7 611.04 8.80 2 6 7 269.97 2.00 3 6 7 46.00 1.90 4 6 7 8.70 1.50 5 6 7 7.40 1.60 6 6 7 1.20 1.70 7 6 7 56.19 4.30 8 6 7 38.40 3.40 9 6 7 15.80 3.90 -9 7 7 51.79 3.00 -8 7 7 23.70 2.80 -7 7 7 35.00 3.80 -6 7 7 25.10 2.30 -5 7 7 5.50 1.70 -4 7 7 285.17 6.20 -3 7 7 192.98 4.70 -2 7 7 21.10 0.80 -1 7 7 158.38 2.20 0 7 7 136.09 1.60 1 7 7 73.79 1.70 2 7 7 604.04 4.70 3 7 7 82.29 2.70 4 7 7 124.39 1.90 5 7 7 134.59 2.70 6 7 7 87.99 2.50 7 7 7 4.30 3.10 8 7 7 51.29 3.60 9 7 7 0.00 26.00 -9 8 7 40.60 3.20 -8 8 7 34.20 3.30 -7 8 7 143.39 5.20 -6 8 7 89.99 4.60 -5 8 7 66.69 4.30 -4 8 7 11.10 2.20 -3 8 7 197.08 3.20 -2 8 7 19.20 0.90 -1 8 7 73.29 1.50 0 8 7 331.37 3.60 1 8 7 35.20 1.20 2 8 7 174.48 1.80 3 8 7 287.97 3.20 4 8 7 75.19 1.50 5 8 7 81.79 2.40 6 8 7 137.09 2.80 7 8 7 24.90 2.70 8 8 7 143.29 4.60 -9 9 7 45.20 4.70 -8 9 7 15.20 4.00 -7 9 7 187.48 6.30 -6 9 7 10.50 3.60 -5 9 7 4.30 11.80 -4 9 7 313.67 6.10 -3 9 7 335.57 5.80 -2 9 7 232.78 2.70 -1 9 7 107.59 1.70 0 9 7 65.79 1.10 1 9 7 26.20 1.40 2 9 7 253.27 2.40 3 9 7 128.89 2.20 4 9 7 7.80 1.40 5 9 7 79.39 2.60 6 9 7 22.00 2.10 7 9 7 64.49 3.60 8 9 7 33.80 4.20 -8 10 7 36.00 4.80 -7 10 7 103.09 5.10 -6 10 7 99.19 5.00 -5 10 7 60.29 3.30 -4 10 7 10.50 2.30 -3 10 7 74.59 3.10 -2 10 7 125.19 1.90 -1 10 7 90.69 2.40 0 10 7 24.00 0.70 1 10 7 152.18 2.30 2 10 7 13.30 0.80 3 10 7 14.70 1.80 4 10 7 24.60 1.50 5 10 7 107.69 2.80 6 10 7 9.30 2.30 7 10 7 130.79 4.80 8 10 7 25.70 2.90 -8 11 7 2.80 1.90 -7 11 7 91.59 4.90 -6 11 7 37.00 6.70 -5 11 7 67.29 3.90 -4 11 7 203.28 3.80 -3 11 7 25.90 2.70 -2 11 7 715.13 6.40 -1 11 7 25.30 1.70 0 11 7 13.80 0.70 1 11 7 151.48 2.10 2 11 7 304.07 3.30 3 11 7 354.56 5.50 4 11 7 23.70 2.10 5 11 7 24.60 2.70 6 11 7 47.20 2.40 7 11 7 29.00 4.80 -7 12 7 150.08 6.90 -6 12 7 75.89 5.00 -5 12 7 97.89 3.70 -4 12 7 90.09 2.60 -3 12 7 17.70 2.60 -2 12 7 160.48 2.50 -1 12 7 174.88 4.40 0 12 7 9.60 0.90 1 12 7 350.26 4.60 2 12 7 50.49 1.20 3 12 7 60.89 2.40 4 12 7 1.20 1.80 5 12 7 32.10 2.80 6 12 7 61.59 5.00 7 12 7 5.30 2.50 -7 13 7 25.70 20.70 -6 13 7 142.89 6.10 -5 13 7 1.20 3.20 -4 13 7 63.59 2.70 -3 13 7 187.28 4.10 -2 13 7 75.19 1.90 -1 13 7 181.08 3.40 0 13 7 124.79 2.10 1 13 7 48.00 2.40 2 13 7 144.39 2.10 3 13 7 135.09 3.00 4 13 7 92.39 2.60 5 13 7 171.78 6.00 6 13 7 2.60 5.90 -6 14 7 8.40 4.90 -5 14 7 64.69 4.10 -4 14 7 85.89 3.20 -3 14 7 58.09 4.00 -2 14 7 98.19 2.40 -1 14 7 0.00 2.80 0 14 7 245.28 4.30 1 14 7 100.29 2.80 2 14 7 81.09 1.60 3 14 7 6.00 3.00 4 14 7 15.50 2.30 5 14 7 14.50 3.20 -5 15 7 0.00 18.00 -4 15 7 84.59 3.10 -3 15 7 27.40 4.10 -2 15 7 61.59 2.10 -1 15 7 108.39 3.50 0 15 7 55.39 2.10 1 15 7 106.49 3.10 2 15 7 83.09 2.20 3 15 7 47.60 18.80 4 15 7 166.98 4.60 -4 16 7 82.39 4.00 -3 16 7 5.90 4.40 -2 16 7 3.40 2.00 -1 16 7 21.10 3.50 0 16 7 32.40 1.90 1 16 7 84.89 2.90 2 16 7 58.49 1.90 3 16 7 5.80 3.50 -2 17 7 2.00 2.30 -1 17 7 90.89 4.20 0 17 7 5.40 2.70 1 17 7 10.10 2.90 2 17 7 174.28 3.40 -10 0 8 122.19 14.70 -9 0 8 0.00 5.30 -8 0 8 38.00 4.70 -7 0 8 289.57 6.80 -6 0 8 17.70 1.60 -5 0 8 593.94 8.20 -4 0 8 0.10 1.10 -3 0 8 132.39 2.50 -2 0 8 18.60 0.60 -1 0 8 1204.78 13.70 0 0 8 104.99 1.70 1 0 8 204.58 8.10 2 0 8 24.70 0.70 3 0 8 155.38 4.20 4 0 8 109.49 2.40 5 0 8 4.60 2.40 6 0 8 123.89 3.20 7 0 8 73.19 7.70 8 0 8 82.09 5.00 9 0 8 0.00 6.00 -10 1 8 79.09 5.50 -9 1 8 7.10 4.00 -8 1 8 76.69 3.20 -7 1 8 44.00 2.50 -6 1 8 65.39 1.90 -5 1 8 46.30 1.60 -4 1 8 293.57 2.70 -3 1 8 135.39 2.30 -2 1 8 63.19 0.70 -1 1 8 139.79 2.10 0 1 8 124.99 1.30 1 1 8 258.97 2.80 2 1 8 668.63 4.10 3 1 8 156.48 2.00 4 1 8 309.57 2.70 5 1 8 47.30 2.30 6 1 8 279.47 3.90 7 1 8 42.40 3.40 8 1 8 8.60 3.20 9 1 8 65.59 4.20 -10 2 8 36.30 5.20 -9 2 8 22.70 3.10 -8 2 8 0.00 2.90 -7 2 8 5.70 2.40 -6 2 8 478.95 5.20 -5 2 8 197.68 2.90 -4 2 8 41.60 1.30 -3 2 8 200.18 2.10 -2 2 8 200.98 1.50 -1 2 8 462.95 5.30 0 2 8 23.70 0.50 1 2 8 512.35 5.30 2 2 8 21.90 0.50 3 2 8 574.34 5.80 4 2 8 231.78 2.40 5 2 8 41.10 1.80 6 2 8 339.07 4.10 7 2 8 157.68 4.60 8 2 8 48.70 3.30 9 2 8 174.28 4.60 -10 3 8 26.70 3.10 -9 3 8 36.40 3.20 -8 3 8 97.79 3.30 -7 3 8 84.29 2.80 -6 3 8 88.99 2.30 -5 3 8 600.54 5.90 -4 3 8 2.40 1.30 -3 3 8 923.21 7.40 -2 3 8 650.33 4.10 -1 3 8 356.66 3.00 0 3 8 218.18 2.30 1 3 8 33.10 1.40 2 3 8 70.69 0.80 3 3 8 377.76 4.70 4 3 8 394.56 4.10 5 3 8 30.90 1.80 6 3 8 229.98 3.20 7 3 8 5.90 3.40 8 3 8 33.40 3.90 9 3 8 13.50 4.10 -10 4 8 67.79 125.79 -9 4 8 15.50 3.20 -8 4 8 16.90 3.10 -7 4 8 44.80 2.50 -6 4 8 157.18 2.50 -5 4 8 22.00 1.60 -4 4 8 233.38 2.70 -3 4 8 293.87 3.20 -2 4 8 145.89 1.40 -1 4 8 111.19 2.20 0 4 8 99.59 1.20 1 4 8 371.06 3.40 2 4 8 1456.15 9.30 3 4 8 270.97 4.30 4 4 8 167.58 2.60 5 4 8 161.68 2.50 6 4 8 15.10 1.50 7 4 8 0.00 3.10 8 4 8 25.80 3.70 9 4 8 13.30 4.10 -9 5 8 1.30 14.50 -8 5 8 110.79 4.00 -7 5 8 221.38 3.60 -6 5 8 86.39 2.40 -5 5 8 205.28 2.80 -4 5 8 756.32 8.70 -3 5 8 28.80 1.20 -2 5 8 574.94 4.00 -1 5 8 239.78 2.50 0 5 8 232.28 2.40 1 5 8 58.59 1.50 2 5 8 249.48 2.10 3 5 8 189.48 2.70 4 5 8 282.77 3.10 5 5 8 263.77 3.10 6 5 8 51.49 1.90 7 5 8 90.99 3.90 8 5 8 22.50 3.90 9 5 8 3.10 4.00 -9 6 8 3.90 3.10 -8 6 8 18.10 3.50 -7 6 8 93.59 3.00 -6 6 8 26.60 1.80 -5 6 8 76.19 1.70 -4 6 8 257.17 3.20 -3 6 8 201.88 2.60 -2 6 8 138.39 1.40 -1 6 8 58.59 1.60 0 6 8 74.09 1.10 1 6 8 152.78 1.90 2 6 8 55.69 0.80 3 6 8 110.19 2.30 4 6 8 176.18 3.20 5 6 8 30.50 1.90 6 6 8 3.00 1.80 7 6 8 153.68 4.20 8 6 8 48.90 4.30 -9 7 8 56.09 3.10 -8 7 8 209.58 4.20 -7 7 8 12.40 2.70 -6 7 8 9.00 3.20 -5 7 8 170.28 3.50 -4 7 8 42.70 1.90 -3 7 8 499.45 5.80 -2 7 8 94.39 1.30 -1 7 8 41.30 1.40 0 7 8 149.79 1.80 1 7 8 153.38 2.10 2 7 8 56.49 1.00 3 7 8 17.40 1.90 4 7 8 216.78 3.10 5 7 8 15.30 1.90 6 7 8 102.69 4.20 7 7 8 4.20 3.00 8 7 8 35.00 4.70 -9 8 8 90.89 5.10 -8 8 8 25.80 3.70 -7 8 8 123.89 4.60 -6 8 8 155.88 4.10 -5 8 8 230.58 4.80 -4 8 8 4.20 1.80 -3 8 8 75.49 3.10 -2 8 8 12.30 0.90 -1 8 8 218.98 2.50 0 8 8 31.60 0.80 1 8 8 14.10 1.50 2 8 8 251.67 2.60 3 8 8 12.50 1.70 4 8 8 104.69 2.00 5 8 8 2.60 2.00 6 8 8 26.00 3.00 7 8 8 17.80 3.00 8 8 8 11.90 10.20 -8 9 8 139.09 4.90 -7 9 8 33.90 5.20 -6 9 8 156.58 4.50 -5 9 8 270.27 5.10 -4 9 8 83.69 2.30 -3 9 8 73.19 2.80 -2 9 8 76.69 1.50 -1 9 8 573.34 6.50 0 9 8 20.20 0.70 1 9 8 241.98 4.40 2 9 8 130.59 1.60 3 9 8 240.58 3.20 4 9 8 98.99 2.10 5 9 8 49.99 2.30 6 9 8 21.50 2.50 7 9 8 10.00 3.10 8 9 8 135.19 190.68 -8 10 8 35.90 5.40 -7 10 8 163.48 6.10 -6 10 8 61.79 4.30 -5 10 8 107.09 4.80 -4 10 8 56.29 2.80 -3 10 8 33.10 2.50 -2 10 8 172.58 2.40 -1 10 8 61.49 1.70 0 10 8 159.68 2.10 1 10 8 48.10 1.60 2 10 8 95.39 1.40 3 10 8 51.49 2.10 4 10 8 158.68 2.30 5 10 8 57.49 2.70 6 10 8 74.09 2.80 7 10 8 10.70 3.60 -7 11 8 35.70 5.00 -6 11 8 285.27 5.40 -5 11 8 32.00 4.20 -4 11 8 285.17 4.40 -3 11 8 288.07 5.80 -2 11 8 11.70 1.10 -1 11 8 198.18 2.80 0 11 8 88.99 1.50 1 11 8 2.70 1.70 2 11 8 177.08 2.20 3 11 8 41.80 2.30 4 11 8 211.08 3.30 5 11 8 10.80 2.90 6 11 8 19.00 3.70 7 11 8 72.99 2.90 -7 12 8 118.19 6.60 -6 12 8 34.50 5.50 -5 12 8 0.00 10.20 -4 12 8 43.80 2.70 -3 12 8 19.70 2.70 -2 12 8 43.10 1.60 -1 12 8 93.19 3.00 0 12 8 12.20 1.00 1 12 8 104.69 2.40 2 12 8 2.60 0.90 3 12 8 185.28 3.80 4 12 8 72.89 2.60 5 12 8 32.90 2.80 6 12 8 20.20 3.20 -6 13 8 18.80 8.30 -5 13 8 16.20 21.70 -4 13 8 12.90 5.10 -3 13 8 65.79 3.60 -2 13 8 136.19 2.50 -1 13 8 88.79 3.40 0 13 8 107.59 2.10 1 13 8 156.58 3.10 2 13 8 9.80 1.10 3 13 8 374.36 5.20 4 13 8 11.40 2.40 5 13 8 32.90 3.60 6 13 8 0.00 975.00 -6 14 8 24.30 20.60 -5 14 8 25.80 3.50 -4 14 8 29.40 2.80 -3 14 8 42.00 4.00 -2 14 8 86.69 2.40 -1 14 8 23.60 3.60 0 14 8 228.98 3.90 1 14 8 86.89 2.80 2 14 8 166.48 2.40 3 14 8 17.50 2.80 4 14 8 6.00 4.20 5 14 8 45.50 4.00 -5 15 8 14.00 2.30 -4 15 8 203.28 5.50 -3 15 8 20.60 5.30 -2 15 8 38.10 2.00 -1 15 8 13.50 3.50 0 15 8 159.18 4.00 1 15 8 2.70 2.40 2 15 8 16.90 1.50 3 15 8 12.80 3.60 4 15 8 0.50 2.70 -3 16 8 109.89 5.10 -2 16 8 57.19 2.60 -1 16 8 78.09 4.00 0 16 8 29.90 2.00 1 16 8 6.60 2.60 2 16 8 140.69 3.00 -9 0 9 0.00 44.90 -8 0 9 18.60 19.10 -7 0 9 16.70 3.30 -6 0 9 18.10 1.60 -5 0 9 134.19 2.60 -4 0 9 151.68 2.90 -3 0 9 519.75 7.00 -2 0 9 384.36 4.10 -1 0 9 101.89 3.20 0 0 9 14.70 0.60 1 0 9 296.67 4.60 2 0 9 129.79 1.80 3 0 9 81.89 2.50 4 0 9 247.18 7.20 5 0 9 83.89 3.10 6 0 9 329.77 6.10 7 0 9 57.39 5.80 8 0 9 77.89 5.30 9 0 9 22.90 5.90 -9 1 9 117.39 4.10 -8 1 9 43.70 2.70 -7 1 9 23.20 3.10 -6 1 9 73.79 2.40 -5 1 9 370.66 4.40 -4 1 9 19.10 1.50 -3 1 9 77.29 1.70 -2 1 9 70.29 0.90 -1 1 9 313.67 4.30 0 1 9 157.88 1.80 1 1 9 326.57 4.40 2 1 9 167.98 1.50 3 1 9 256.47 3.20 4 1 9 146.49 2.00 5 1 9 30.40 2.00 6 1 9 71.49 2.40 7 1 9 112.59 4.20 8 1 9 66.09 13.00 9 1 9 2.90 4.30 -9 2 9 145.19 4.50 -8 2 9 230.18 4.60 -7 2 9 26.20 2.60 -6 2 9 86.39 2.30 -5 2 9 149.19 2.30 -4 2 9 48.60 1.70 -3 2 9 112.09 3.70 -2 2 9 273.07 2.30 -1 2 9 904.91 7.80 0 2 9 143.89 1.80 1 2 9 86.69 3.60 2 2 9 998.10 6.80 3 2 9 86.59 2.60 4 2 9 151.98 2.70 5 2 9 73.69 2.30 6 2 9 97.69 2.20 7 2 9 92.89 4.10 8 2 9 91.69 4.10 9 2 9 0.00 21.20 -9 3 9 3.80 3.10 -8 3 9 93.99 3.50 -7 3 9 234.68 4.00 -6 3 9 142.59 2.60 -5 3 9 29.50 1.60 -4 3 9 117.19 2.80 -3 3 9 371.86 5.10 -2 3 9 229.48 2.00 -1 3 9 110.29 1.70 0 3 9 96.99 1.30 1 3 9 55.89 1.30 2 3 9 111.79 1.20 3 3 9 10.00 1.40 4 3 9 61.59 1.40 5 3 9 189.38 3.00 6 3 9 136.39 2.90 7 3 9 54.49 3.50 8 3 9 89.09 3.90 -9 4 9 29.80 4.60 -8 4 9 118.19 4.30 -7 4 9 59.39 2.80 -6 4 9 8.70 1.90 -5 4 9 51.19 1.90 -4 4 9 163.68 2.60 -3 4 9 516.85 5.80 -2 4 9 43.90 0.80 -1 4 9 119.49 2.40 0 4 9 115.69 1.60 1 4 9 359.06 3.60 2 4 9 130.69 1.40 3 4 9 1034.50 9.00 4 4 9 11.10 1.30 5 4 9 203.98 3.10 6 4 9 47.50 2.00 7 4 9 44.10 4.70 8 4 9 59.29 3.90 -9 5 9 12.00 3.50 -8 5 9 114.89 3.30 -7 5 9 43.60 2.90 -6 5 9 202.28 3.00 -5 5 9 30.10 1.90 -4 5 9 62.69 1.90 -3 5 9 99.19 2.20 -2 5 9 136.59 1.50 -1 5 9 63.69 1.30 0 5 9 16.80 0.60 1 5 9 30.80 1.00 2 5 9 40.60 0.80 3 5 9 239.88 2.90 4 5 9 21.10 1.50 5 5 9 14.10 2.00 6 5 9 59.49 2.10 7 5 9 55.49 4.00 8 5 9 20.40 4.20 -9 6 9 11.60 3.20 -8 6 9 73.59 3.20 -7 6 9 5.00 3.30 -6 6 9 31.30 1.70 -5 6 9 37.30 1.70 -4 6 9 387.26 4.50 -3 6 9 117.89 2.20 -2 6 9 1014.60 7.50 -1 6 9 390.46 4.40 0 6 9 16.30 0.60 1 6 9 209.18 3.30 2 6 9 443.96 3.50 3 6 9 184.68 3.40 4 6 9 7.90 1.50 5 6 9 145.69 2.90 6 6 9 175.38 3.10 7 6 9 22.30 4.90 8 6 9 66.39 3.80 -9 7 9 38.10 2.90 -8 7 9 16.80 2.70 -7 7 9 118.89 3.50 -6 7 9 70.49 2.90 -5 7 9 8.90 2.00 -4 7 9 187.78 4.10 -3 7 9 242.38 3.20 -2 7 9 106.49 1.30 -1 7 9 469.15 5.20 0 7 9 29.20 0.80 1 7 9 198.08 3.60 2 7 9 10.40 0.70 3 7 9 61.99 1.90 4 7 9 12.40 1.70 5 7 9 95.69 2.60 6 7 9 6.30 1.90 7 7 9 7.80 3.70 8 7 9 56.39 4.30 -8 8 9 11.40 16.60 -7 8 9 9.90 4.00 -6 8 9 127.29 4.80 -5 8 9 57.69 3.00 -4 8 9 55.79 2.40 -3 8 9 243.68 3.40 -2 8 9 83.49 1.50 -1 8 9 168.58 2.20 0 8 9 41.20 0.90 1 8 9 56.39 1.90 2 8 9 40.90 0.90 3 8 9 1.20 1.90 4 8 9 93.89 2.30 5 8 9 155.08 2.90 6 8 9 68.89 2.40 7 8 9 21.60 7.20 -8 9 9 46.40 5.30 -7 9 9 85.49 12.20 -6 9 9 36.40 4.10 -5 9 9 65.49 3.60 -4 9 9 110.99 3.20 -3 9 9 56.59 3.70 -2 9 9 79.99 1.60 -1 9 9 11.10 1.30 0 9 9 285.37 3.50 1 9 9 13.20 1.40 2 9 9 19.10 0.80 3 9 9 68.49 2.10 4 9 9 166.08 2.50 5 9 9 37.70 3.00 6 9 9 16.20 2.30 7 9 9 32.40 3.70 -7 10 9 46.30 5.50 -6 10 9 20.90 3.10 -5 10 9 82.59 5.10 -4 10 9 10.30 2.30 -3 10 9 45.90 2.70 -2 10 9 22.70 2.00 -1 10 9 58.89 1.80 0 10 9 95.99 1.60 1 10 9 46.00 1.80 2 10 9 187.08 2.20 3 10 9 72.29 2.50 4 10 9 106.19 2.70 5 10 9 15.40 2.70 6 10 9 7.90 2.50 7 10 9 30.50 2.40 -7 11 9 47.60 6.50 -6 11 9 12.10 4.00 -5 11 9 51.89 3.90 -4 11 9 20.00 3.30 -3 11 9 23.30 2.80 -2 11 9 5.30 1.20 -1 11 9 121.09 2.60 0 11 9 106.69 1.80 1 11 9 54.19 2.20 2 11 9 11.20 1.00 3 11 9 45.80 2.90 4 11 9 41.90 2.40 5 11 9 102.39 3.70 6 11 9 26.50 4.10 -6 12 9 16.60 5.50 -5 12 9 43.00 4.50 -4 12 9 74.49 3.00 -3 12 9 137.59 4.70 -2 12 9 62.79 2.10 -1 12 9 161.28 3.80 0 12 9 139.59 2.50 1 12 9 165.88 3.20 2 12 9 147.99 2.20 3 12 9 15.30 2.90 4 12 9 71.09 2.80 5 12 9 20.70 3.60 6 12 9 44.60 3.30 -6 13 9 53.59 3.20 -5 13 9 29.20 4.90 -4 13 9 45.30 2.90 -3 13 9 15.80 4.40 -2 13 9 25.90 2.40 -1 13 9 9.70 2.80 0 13 9 56.89 1.90 1 13 9 25.10 3.10 2 13 9 24.50 1.20 3 13 9 50.79 3.20 4 13 9 45.30 12.30 5 13 9 25.70 3.90 -5 14 9 28.90 4.50 -4 14 9 36.90 3.00 -3 14 9 154.68 4.80 -2 14 9 152.38 3.20 -1 14 9 20.10 3.00 0 14 9 22.70 1.80 1 14 9 56.39 2.40 2 14 9 18.50 1.30 3 14 9 126.79 3.90 4 14 9 0.00 2.90 -4 15 9 8.70 3.30 -3 15 9 154.08 5.20 -2 15 9 86.89 3.10 -1 15 9 137.19 4.90 0 15 9 3.40 1.90 1 15 9 47.90 2.70 2 15 9 58.39 1.80 3 15 9 37.60 3.30 -2 16 9 88.49 3.30 -1 16 9 12.50 4.20 0 16 9 1.30 2.10 1 16 9 26.50 3.00 -9 0 10 14.90 5.60 -8 0 10 54.69 12.70 -7 0 10 146.29 5.30 -6 0 10 294.17 5.20 -5 0 10 20.20 2.10 -4 0 10 903.91 11.50 -3 0 10 39.80 2.10 -2 0 10 1.10 0.80 -1 0 10 32.10 2.70 0 0 10 52.79 1.40 1 0 10 179.18 3.30 2 0 10 172.28 2.50 3 0 10 436.16 6.30 4 0 10 372.76 6.20 5 0 10 214.88 4.90 6 0 10 40.50 3.00 7 0 10 19.20 3.50 8 0 10 18.40 5.20 -9 1 10 26.80 4.20 -8 1 10 27.50 3.00 -7 1 10 84.79 3.50 -6 1 10 6.20 1.80 -5 1 10 154.78 2.80 -4 1 10 35.40 1.60 -3 1 10 111.89 2.50 -2 1 10 85.99 1.10 -1 1 10 354.46 3.80 0 1 10 350.26 4.10 1 1 10 25.50 1.90 2 1 10 208.58 2.00 3 1 10 14.80 1.70 4 1 10 47.20 1.70 5 1 10 176.88 3.60 6 1 10 50.99 2.40 7 1 10 34.40 2.80 8 1 10 37.50 4.50 -9 2 10 0.00 16.80 -8 2 10 138.99 3.80 -7 2 10 12.70 3.30 -6 2 10 175.08 2.90 -5 2 10 88.09 2.10 -4 2 10 266.27 3.50 -3 2 10 426.06 4.80 -2 2 10 399.46 3.20 -1 2 10 195.98 2.60 0 2 10 153.58 2.00 1 2 10 195.08 3.00 2 2 10 116.59 1.40 3 2 10 282.77 4.50 4 2 10 48.70 1.70 5 2 10 33.50 2.00 6 2 10 35.60 2.00 7 2 10 23.20 5.10 8 2 10 95.29 4.50 -9 3 10 15.80 3.70 -8 3 10 57.29 10.30 -7 3 10 62.29 3.20 -6 3 10 338.97 4.40 -5 3 10 68.69 2.30 -4 3 10 46.00 1.40 -3 3 10 53.79 1.50 -2 3 10 119.29 1.40 -1 3 10 4.40 1.50 0 3 10 68.69 1.10 1 3 10 312.37 3.10 2 3 10 120.69 1.40 3 3 10 232.48 2.90 4 3 10 50.79 2.10 5 3 10 66.79 3.10 6 3 10 12.40 1.90 7 3 10 48.40 3.10 8 3 10 136.49 16.80 -9 4 10 79.29 4.20 -8 4 10 86.89 3.40 -7 4 10 30.80 3.40 -6 4 10 1.30 1.70 -5 4 10 112.69 2.80 -4 4 10 48.90 1.30 -3 4 10 79.19 4.80 -2 4 10 175.58 1.90 -1 4 10 864.11 7.40 0 4 10 207.98 2.70 1 4 10 96.89 3.50 2 4 10 31.10 0.70 3 4 10 165.98 2.80 4 4 10 74.59 1.80 5 4 10 56.39 2.20 6 4 10 14.00 2.10 7 4 10 9.20 3.40 8 4 10 35.40 17.20 -9 5 10 18.50 3.50 -8 5 10 22.40 3.40 -7 5 10 116.19 4.70 -6 5 10 98.19 3.20 -5 5 10 156.78 2.80 -4 5 10 105.39 1.70 -3 5 10 66.09 2.10 -2 5 10 38.30 0.90 -1 5 10 82.29 1.50 0 5 10 2.70 0.60 1 5 10 38.40 1.40 2 5 10 112.29 1.40 3 5 10 30.80 2.20 4 5 10 12.20 1.50 5 5 10 119.09 3.20 6 5 10 191.98 3.80 7 5 10 24.10 3.60 8 5 10 34.70 4.40 -8 6 10 147.29 3.60 -7 6 10 18.40 3.90 -6 6 10 40.20 3.20 -5 6 10 175.58 3.30 -4 6 10 139.39 2.00 -3 6 10 193.78 3.20 -2 6 10 256.67 2.30 -1 6 10 134.09 1.90 0 6 10 3.60 0.60 1 6 10 46.60 1.60 2 6 10 275.97 2.40 3 6 10 13.60 1.90 4 6 10 368.36 4.00 5 6 10 24.00 2.70 6 6 10 41.60 2.30 7 6 10 34.90 3.70 -8 7 10 52.69 3.10 -7 7 10 59.69 8.50 -6 7 10 189.08 4.30 -5 7 10 118.59 3.00 -4 7 10 26.90 1.70 -3 7 10 39.20 1.70 -2 7 10 178.68 1.80 -1 7 10 214.08 2.70 0 7 10 15.00 0.70 1 7 10 30.80 1.80 2 7 10 56.69 1.20 3 7 10 130.29 2.50 4 7 10 102.69 2.30 5 7 10 10.30 2.60 6 7 10 13.10 2.00 7 7 10 11.30 5.30 -8 8 10 123.79 4.60 -7 8 10 20.70 4.10 -6 8 10 87.49 4.10 -5 8 10 9.20 3.20 -4 8 10 162.18 3.90 -3 8 10 235.98 3.60 -2 8 10 58.29 1.20 -1 8 10 31.50 1.60 0 8 10 50.99 1.20 1 8 10 95.09 1.90 2 8 10 21.80 0.90 3 8 10 180.78 3.20 4 8 10 50.79 2.00 5 8 10 5.50 2.80 6 8 10 122.49 3.80 7 8 10 50.69 3.90 -7 9 10 6.60 6.90 -6 9 10 67.49 7.50 -5 9 10 50.99 3.70 -4 9 10 102.39 3.60 -3 9 10 12.60 2.50 -2 9 10 53.99 1.50 -1 9 10 64.19 2.10 0 9 10 121.69 2.00 1 9 10 153.78 2.40 2 9 10 110.49 1.60 3 9 10 10.60 2.60 4 9 10 0.00 1.90 5 9 10 32.80 3.00 6 9 10 38.10 4.10 -7 10 10 58.49 12.70 -6 10 10 6.20 4.50 -5 10 10 10.50 3.60 -4 10 10 162.18 4.80 -3 10 10 72.29 3.30 -2 10 10 179.88 2.60 -1 10 10 164.98 3.00 0 10 10 6.10 0.90 1 10 10 144.39 2.60 2 10 10 27.70 1.00 3 10 10 41.50 2.90 4 10 10 90.79 2.80 5 10 10 34.50 3.10 6 10 10 2.80 3.10 -6 11 10 49.80 6.30 -5 11 10 0.00 13.30 -4 11 10 9.50 2.50 -3 11 10 49.90 3.70 -2 11 10 3.50 1.40 -1 11 10 19.30 2.30 0 11 10 57.69 1.50 1 11 10 162.58 2.80 2 11 10 55.09 1.50 3 11 10 28.80 2.80 4 11 10 31.10 2.50 5 11 10 40.30 3.50 6 11 10 1030.10 862.11 -6 12 10 31.90 4.20 -5 12 10 38.40 4.60 -4 12 10 178.18 4.10 -3 12 10 28.70 3.50 -2 12 10 224.48 3.60 -1 12 10 24.20 2.60 0 12 10 87.09 2.00 1 12 10 53.99 2.70 2 12 10 10.40 1.30 3 12 10 57.39 3.20 4 12 10 47.00 3.00 5 12 10 123.19 4.80 -5 13 10 52.79 4.40 -4 13 10 15.00 3.40 -3 13 10 16.70 11.40 -2 13 10 25.00 3.00 -1 13 10 18.10 5.10 0 13 10 8.30 1.30 1 13 10 30.30 2.70 2 13 10 31.80 1.50 3 13 10 27.00 8.40 4 13 10 74.49 3.30 -4 14 10 89.49 3.50 -3 14 10 51.49 5.40 -2 14 10 72.69 2.90 -1 14 10 148.49 4.40 0 14 10 68.69 2.50 1 14 10 42.20 2.80 2 14 10 122.29 2.70 3 14 10 223.18 5.60 -3 15 10 24.40 5.10 -2 15 10 87.49 3.30 -1 15 10 30.60 4.00 0 15 10 13.60 2.10 1 15 10 5.10 2.70 2 15 10 1.90 1.70 -9 0 11 73.09 7.50 -8 0 11 0.00 13.50 -7 0 11 44.90 6.40 -6 0 11 399.36 8.70 -5 0 11 38.30 2.70 -4 0 11 227.28 4.70 -3 0 11 77.49 3.80 -2 0 11 817.92 9.20 -1 0 11 278.27 5.30 0 0 11 50.59 1.50 1 0 11 261.77 5.50 2 0 11 260.87 3.80 3 0 11 42.50 3.10 4 0 11 59.99 2.50 5 0 11 0.00 3.20 6 0 11 17.10 8.80 7 0 11 39.80 4.70 8 0 11 16.40 3.50 -9 1 11 16.40 5.00 -8 1 11 17.20 3.60 -7 1 11 71.09 4.20 -6 1 11 48.40 3.20 -5 1 11 190.18 3.70 -4 1 11 48.10 1.70 -3 1 11 11.70 1.50 -2 1 11 370.66 3.10 -1 1 11 203.78 3.70 0 1 11 46.10 1.10 1 1 11 461.75 5.20 2 1 11 282.17 2.70 3 1 11 228.58 3.00 4 1 11 90.89 2.20 5 1 11 22.20 5.80 6 1 11 77.69 2.70 7 1 11 23.90 2.80 8 1 11 92.19 2.90 -9 2 11 96.69 4.60 -8 2 11 84.89 3.50 -7 2 11 49.70 8.00 -6 2 11 7.30 2.70 -5 2 11 10.60 1.90 -4 2 11 130.09 2.00 -3 2 11 438.56 5.70 -2 2 11 265.97 2.60 -1 2 11 78.79 1.70 0 2 11 108.69 1.60 1 2 11 85.79 1.80 2 2 11 83.39 1.30 3 2 11 368.06 4.50 4 2 11 27.10 1.90 5 2 11 45.20 7.40 6 2 11 57.39 6.60 7 2 11 41.30 3.10 8 2 11 128.49 79.19 -8 3 11 15.60 3.30 -7 3 11 29.00 3.60 -6 3 11 135.99 3.10 -5 3 11 366.36 4.50 -4 3 11 279.07 3.30 -3 3 11 12.90 1.90 -2 3 11 69.89 1.20 -1 3 11 86.09 2.00 0 3 11 19.20 0.70 1 3 11 27.90 1.70 2 3 11 185.78 2.10 3 3 11 14.60 2.60 4 3 11 7.10 1.70 5 3 11 331.97 5.40 6 3 11 18.50 2.30 7 3 11 153.18 4.80 -8 4 11 31.60 3.50 -7 4 11 79.39 4.20 -6 4 11 26.40 3.10 -5 4 11 17.70 1.90 -4 4 11 42.70 1.50 -3 4 11 134.19 2.80 -2 4 11 334.47 3.00 -1 4 11 3.60 1.50 0 4 11 402.66 5.40 1 4 11 119.49 1.80 2 4 11 20.90 0.80 3 4 11 75.39 2.20 4 4 11 51.69 2.10 5 4 11 90.39 3.00 6 4 11 19.50 2.30 7 4 11 154.78 6.20 -8 5 11 8.20 3.50 -7 5 11 61.49 4.50 -6 5 11 61.99 3.80 -5 5 11 171.38 3.00 -4 5 11 3.70 1.40 -3 5 11 178.98 2.70 -2 5 11 201.58 2.00 -1 5 11 166.58 2.50 0 5 11 129.29 2.00 1 5 11 95.69 2.10 2 5 11 50.29 1.10 3 5 11 124.49 2.80 4 5 11 21.50 2.30 5 5 11 74.19 3.30 6 5 11 66.89 2.50 7 5 11 33.20 3.60 -8 6 11 6.30 2.90 -7 6 11 139.49 4.20 -6 6 11 6.50 2.10 -5 6 11 236.88 3.70 -4 6 11 48.50 2.40 -3 6 11 34.10 2.40 -2 6 11 58.09 1.10 -1 6 11 13.10 1.70 0 6 11 158.68 2.40 1 6 11 114.29 2.20 2 6 11 174.08 1.90 3 6 11 330.27 4.10 4 6 11 56.49 1.90 5 6 11 45.40 3.10 6 6 11 6.00 2.40 7 6 11 8.80 4.00 -8 7 11 26.90 4.50 -7 7 11 4.00 3.10 -6 7 11 64.69 5.10 -5 7 11 71.39 2.90 -4 7 11 164.48 2.90 -3 7 11 21.60 1.90 -2 7 11 15.50 0.80 -1 7 11 123.49 2.50 0 7 11 279.67 3.90 1 7 11 101.79 2.30 2 7 11 196.18 2.40 3 7 11 4.10 2.40 4 7 11 8.10 2.20 5 7 11 26.60 2.90 6 7 11 39.20 2.40 7 7 11 6.30 2.40 -7 8 11 295.37 26.00 -6 8 11 91.39 5.40 -5 8 11 117.89 3.60 -4 8 11 103.89 2.90 -3 8 11 169.78 3.90 -2 8 11 137.69 1.80 -1 8 11 44.10 1.70 0 8 11 14.90 0.90 1 8 11 37.10 2.00 2 8 11 80.89 1.60 3 8 11 25.70 2.80 4 8 11 117.29 2.70 5 8 11 15.30 3.20 6 8 11 1.80 2.30 -7 9 11 19.10 5.70 -6 9 11 15.30 5.80 -5 9 11 28.00 4.00 -4 9 11 108.69 6.90 -3 9 11 185.98 5.00 -2 9 11 21.80 1.00 -1 9 11 33.10 2.00 0 9 11 2.60 0.90 1 9 11 138.39 2.50 2 9 11 8.10 1.10 3 9 11 153.78 4.10 4 9 11 16.50 2.30 5 9 11 71.59 3.60 6 9 11 93.39 3.40 -6 10 11 25.20 4.50 -5 10 11 53.39 4.10 -4 10 11 17.40 2.80 -3 10 11 152.38 5.30 -2 10 11 38.20 1.50 -1 10 11 129.79 2.80 0 10 11 73.09 1.70 1 10 11 12.10 2.30 2 10 11 49.70 1.30 3 10 11 47.60 3.70 4 10 11 0.10 2.80 5 10 11 3.90 3.40 -6 11 11 4.90 2.40 -5 11 11 37.90 5.70 -4 11 11 60.79 2.90 -3 11 11 12.90 3.30 -2 11 11 28.20 1.70 -1 11 11 3.40 2.60 0 11 11 12.80 1.20 1 11 11 14.90 2.40 2 11 11 131.79 2.30 3 11 11 31.30 3.60 4 11 11 150.68 4.00 5 11 11 46.00 4.50 -5 12 11 9.80 17.50 -4 12 11 16.00 2.90 -3 12 11 50.49 3.90 -2 12 11 183.38 3.30 -1 12 11 101.89 3.80 0 12 11 7.40 1.20 1 12 11 34.30 2.90 2 12 11 15.30 1.60 3 12 11 0.00 4.10 4 12 11 0.00 3.10 -4 13 11 2.80 12.10 -3 13 11 36.00 4.40 -2 13 11 17.80 2.10 -1 13 11 86.09 4.00 0 13 11 64.49 2.10 1 13 11 165.78 3.90 2 13 11 162.08 3.10 3 13 11 78.79 4.70 -3 14 11 10.10 5.20 -2 14 11 42.10 4.80 -1 14 11 39.20 4.00 0 14 11 20.00 3.10 1 14 11 11.30 3.00 2 14 11 12.70 1.70 -8 0 12 96.59 6.40 -7 0 12 267.77 10.80 -6 0 12 19.50 11.10 -5 0 12 66.49 3.40 -4 0 12 21.30 2.40 -3 0 12 16.00 10.90 -2 0 12 512.55 6.00 -1 0 12 34.50 2.80 0 0 12 51.49 1.60 1 0 12 244.28 4.30 2 0 12 30.30 1.40 3 0 12 94.29 12.20 4 0 12 0.00 3.30 5 0 12 3.70 4.30 6 0 12 122.09 9.70 7 0 12 62.69 5.30 -8 1 12 37.40 9.50 -7 1 12 30.80 3.80 -6 1 12 48.90 3.70 -5 1 12 93.59 2.60 -4 1 12 86.09 2.10 -3 1 12 18.50 1.80 -2 1 12 57.29 1.10 -1 1 12 415.56 4.60 0 1 12 308.97 3.70 1 1 12 47.40 2.40 2 1 12 382.86 3.40 3 1 12 47.00 2.20 4 1 12 172.28 2.80 5 1 12 13.60 3.00 6 1 12 5.80 2.60 7 1 12 94.59 3.90 -8 2 12 14.00 9.20 -7 2 12 24.00 11.50 -6 2 12 38.30 2.80 -5 2 12 43.70 2.50 -4 2 12 161.48 2.40 -3 2 12 21.30 2.50 -2 2 12 207.58 2.20 -1 2 12 3.80 1.50 0 2 12 91.89 1.70 1 2 12 117.39 2.10 2 2 12 30.50 1.00 3 2 12 172.18 3.10 4 2 12 34.80 1.90 5 2 12 69.99 3.30 6 2 12 4.80 2.60 7 2 12 128.99 4.10 -8 3 12 70.89 4.70 -7 3 12 9.90 3.70 -6 3 12 47.80 3.70 -5 3 12 169.28 3.90 -4 3 12 79.79 1.70 -3 3 12 284.37 3.50 -2 3 12 129.29 1.70 -1 3 12 20.70 1.80 0 3 12 63.99 1.30 1 3 12 20.90 1.90 2 3 12 21.70 1.00 3 3 12 185.18 3.50 4 3 12 42.20 2.40 5 3 12 131.19 3.60 6 3 12 141.39 3.80 7 3 12 17.90 2.40 -8 4 12 23.80 4.80 -7 4 12 48.20 4.20 -6 4 12 66.09 7.20 -5 4 12 0.70 2.30 -4 4 12 87.09 1.90 -3 4 12 149.19 2.90 -2 4 12 29.70 1.00 -1 4 12 16.70 1.80 0 4 12 144.19 2.30 1 4 12 115.99 2.30 2 4 12 16.30 0.90 3 4 12 4.10 2.20 4 4 12 0.00 2.20 5 4 12 13.70 2.90 6 4 12 5.50 2.60 7 4 12 30.20 2.40 -8 5 12 32.20 3.60 -7 5 12 199.88 5.60 -6 5 12 152.78 3.90 -5 5 12 57.09 2.60 -4 5 12 435.76 4.50 -3 5 12 15.20 2.10 -2 5 12 64.29 1.40 -1 5 12 144.59 2.90 0 5 12 19.60 1.00 1 5 12 241.98 3.60 2 5 12 3.30 0.90 3 5 12 201.08 4.20 4 5 12 192.38 3.40 5 5 12 90.19 3.40 6 5 12 99.39 3.30 -7 6 12 44.80 3.80 -6 6 12 20.30 2.30 -5 6 12 7.60 3.30 -4 6 12 16.70 2.00 -3 6 12 8.00 2.50 -2 6 12 15.40 1.00 -1 6 12 56.09 2.40 0 6 12 87.19 2.00 1 6 12 214.18 3.20 2 6 12 42.40 1.20 3 6 12 33.10 3.20 4 6 12 44.40 2.10 5 6 12 39.60 3.00 6 6 12 10.00 2.90 -7 7 12 18.90 3.80 -6 7 12 46.50 7.60 -5 7 12 4.10 3.00 -4 7 12 87.19 2.60 -3 7 12 89.59 2.70 -2 7 12 179.78 2.30 -1 7 12 35.50 2.50 0 7 12 174.88 2.90 1 7 12 290.27 4.10 2 7 12 58.59 1.40 3 7 12 206.98 4.20 4 7 12 15.50 2.10 5 7 12 20.00 3.20 6 7 12 14.00 3.00 -7 8 12 70.59 5.30 -6 8 12 76.29 4.40 -5 8 12 12.90 3.10 -4 8 12 4.40 2.60 -3 8 12 71.29 2.90 -2 8 12 87.59 1.70 -1 8 12 70.59 2.60 0 8 12 3.10 1.00 1 8 12 19.10 2.30 2 8 12 56.39 1.40 3 8 12 8.50 3.10 4 8 12 10.80 2.40 5 8 12 74.89 3.70 -6 9 12 9.60 8.60 -5 9 12 12.30 4.80 -4 9 12 2.60 2.60 -3 9 12 35.30 3.30 -2 9 12 12.30 1.20 -1 9 12 157.18 3.20 0 9 12 23.50 1.20 1 9 12 0.00 2.30 2 9 12 67.99 1.70 3 9 12 85.69 3.50 4 9 12 43.80 2.80 5 9 12 71.09 4.00 -6 10 12 11.80 2.50 -5 10 12 32.90 5.00 -4 10 12 56.19 3.40 -3 10 12 3.90 13.30 -2 10 12 44.30 1.50 -1 10 12 43.00 2.40 0 10 12 38.80 1.40 1 10 12 4.80 2.60 2 10 12 49.30 1.50 3 10 12 123.29 4.20 4 10 12 56.59 3.80 5 10 12 0.00 1103.69 -5 11 12 216.58 7.30 -4 11 12 13.00 3.40 -3 11 12 121.99 4.50 -2 11 12 21.00 4.60 -1 11 12 10.50 2.60 0 11 12 41.50 1.60 1 11 12 8.30 2.70 2 11 12 67.39 1.80 3 11 12 9.30 4.60 4 11 12 130.59 4.20 -4 12 12 87.39 3.70 -3 12 12 85.09 4.50 -2 12 12 26.00 2.40 -1 12 12 221.88 4.80 0 12 12 91.49 2.40 1 12 12 56.49 3.20 2 12 12 56.49 1.90 3 12 12 2.20 1.80 -3 13 12 16.20 17.20 -2 13 12 11.80 2.10 -1 13 12 6.60 3.50 0 13 12 124.59 3.30 1 13 12 37.30 3.30 2 13 12 68.79 2.30 -7 0 13 5.40 7.30 -6 0 13 78.89 12.50 -5 0 13 26.10 4.10 -4 0 13 37.40 12.00 -3 0 13 29.40 3.40 -2 0 13 81.99 2.10 -1 0 13 105.49 3.00 0 0 13 19.40 1.30 1 0 13 20.50 2.80 2 0 13 35.10 4.40 3 0 13 0.00 4.00 4 0 13 223.58 14.90 5 0 13 0.00 4.60 6 0 13 13.60 4.70 -7 1 13 26.20 10.80 -6 1 13 47.40 2.90 -5 1 13 3.40 2.70 -4 1 13 104.19 2.50 -3 1 13 26.70 1.90 -2 1 13 110.69 1.60 -1 1 13 122.89 2.20 0 1 13 42.40 1.20 1 1 13 22.60 2.10 2 1 13 41.60 1.20 3 1 13 83.79 3.80 4 1 13 83.69 2.50 5 1 13 84.39 3.60 6 1 13 9.40 3.20 -7 2 13 21.40 5.10 -6 2 13 45.60 4.40 -5 2 13 38.70 3.00 -4 2 13 33.10 1.80 -3 2 13 4.10 2.30 -2 2 13 134.49 1.80 -1 2 13 31.90 2.00 0 2 13 527.85 6.40 1 2 13 6.30 1.90 2 2 13 17.70 1.20 3 2 13 16.60 3.30 4 2 13 26.40 2.10 5 2 13 68.39 3.60 6 2 13 22.40 3.40 -7 3 13 203.08 5.70 -6 3 13 24.40 10.20 -5 3 13 255.67 4.60 -4 3 13 126.09 2.50 -3 3 13 108.59 2.70 -2 3 13 213.78 2.50 -1 3 13 117.29 2.80 0 3 13 71.99 1.70 1 3 13 169.08 3.00 2 3 13 199.38 2.50 3 3 13 125.79 3.90 4 3 13 165.88 3.00 5 3 13 47.50 11.50 6 3 13 6.80 3.30 -7 4 13 135.29 6.10 -6 4 13 39.70 7.10 -5 4 13 66.99 3.30 -4 4 13 47.50 2.00 -3 4 13 39.80 2.30 -2 4 13 17.20 1.10 -1 4 13 50.59 2.20 0 4 13 83.99 1.80 1 4 13 88.59 2.50 2 4 13 105.79 1.90 3 4 13 0.00 3.50 4 4 13 47.70 2.40 5 4 13 118.69 3.80 6 4 13 8.60 3.50 -7 5 13 37.90 5.40 -6 5 13 17.50 3.00 -5 5 13 109.09 3.30 -4 5 13 40.50 2.40 -3 5 13 102.69 3.50 -2 5 13 257.47 2.90 -1 5 13 100.19 2.50 0 5 13 109.89 2.10 1 5 13 45.30 2.40 2 5 13 221.38 2.80 3 5 13 12.80 3.10 4 5 13 41.30 2.40 5 5 13 82.09 3.60 6 5 13 7.10 3.50 -7 6 13 24.20 4.00 -6 6 13 7.40 9.60 -5 6 13 16.80 2.80 -4 6 13 0.00 2.10 -3 6 13 41.00 2.90 -2 6 13 26.90 1.30 -1 6 13 0.80 2.30 0 6 13 88.39 2.00 1 6 13 46.70 2.80 2 6 13 14.30 1.30 3 6 13 35.50 3.50 4 6 13 51.89 2.80 5 6 13 13.30 3.70 -6 7 13 15.70 9.80 -5 7 13 14.30 2.50 -4 7 13 19.50 2.00 -3 7 13 252.87 6.00 -2 7 13 263.57 3.10 -1 7 13 76.99 3.20 0 7 13 3.50 1.30 1 7 13 0.00 3.00 2 7 13 6.80 4.20 3 7 13 31.80 3.30 4 7 13 33.90 2.70 5 7 13 14.70 3.50 -6 8 13 37.40 2.60 -5 8 13 0.00 13.40 -4 8 13 16.50 2.30 -3 8 13 13.90 3.00 -2 8 13 28.10 1.30 -1 8 13 43.70 7.70 0 8 13 35.20 9.30 1 8 13 6.90 2.60 2 8 13 5.70 1.30 3 8 13 6.80 3.50 4 8 13 52.39 2.80 5 8 13 24.60 4.00 -5 9 13 21.90 4.10 -4 9 13 65.29 3.40 -3 9 13 27.10 3.10 -2 9 13 110.19 2.00 -1 9 13 0.00 2.50 0 9 13 11.10 1.40 1 9 13 88.49 2.90 2 9 13 102.09 2.20 3 9 13 28.60 4.40 4 9 13 145.59 3.70 -5 10 13 49.99 2.60 -4 10 13 0.00 13.90 -3 10 13 9.70 4.80 -2 10 13 79.19 2.00 -1 10 13 98.39 2.80 0 10 13 43.30 1.80 1 10 13 75.29 3.00 2 10 13 40.50 1.60 3 10 13 66.99 4.10 -4 11 13 1.90 15.10 -3 11 13 54.79 8.70 -2 11 13 7.80 1.80 -1 11 13 33.20 2.90 0 11 13 157.08 3.10 1 11 13 83.69 3.20 2 11 13 87.59 2.40 3 11 13 141.09 16.90 -3 12 13 18.00 43.10 -2 12 13 53.69 2.00 -1 12 13 76.89 3.60 0 12 13 108.89 2.60 1 12 13 26.10 3.10 -7 0 14 16.10 8.00 -6 0 14 4.10 6.60 -5 0 14 22.60 5.10 -4 0 14 147.99 4.20 -3 0 14 8.40 3.40 -2 0 14 4.50 1.50 -1 0 14 55.49 3.40 0 0 14 59.19 2.40 1 0 14 266.47 5.20 2 0 14 44.90 2.20 3 0 14 109.89 6.60 4 0 14 151.78 4.80 5 0 14 0.00 5.50 -7 1 14 38.90 4.60 -6 1 14 12.80 3.10 -5 1 14 55.79 3.30 -4 1 14 102.59 2.60 -3 1 14 310.27 4.80 -2 1 14 11.30 1.10 -1 1 14 151.18 2.80 0 1 14 77.39 1.80 1 1 14 50.79 2.60 2 1 14 2.50 1.30 3 1 14 7.20 3.60 4 1 14 138.99 3.70 5 1 14 25.90 3.90 -7 2 14 37.80 4.70 -6 2 14 51.09 4.50 -5 2 14 0.00 6.40 -4 2 14 15.30 2.00 -3 2 14 17.70 2.70 -2 2 14 47.50 1.40 -1 2 14 236.08 3.70 0 2 14 68.49 1.70 1 2 14 124.29 3.10 2 2 14 42.30 1.50 3 2 14 4.80 3.30 4 2 14 7.10 2.60 5 2 14 46.60 4.20 -7 3 14 67.99 8.20 -6 3 14 142.39 5.00 -5 3 14 31.80 3.20 -4 3 14 10.00 2.40 -3 3 14 8.80 3.00 -2 3 14 57.99 1.60 -1 3 14 56.29 2.70 0 3 14 59.19 1.60 1 3 14 0.00 2.60 2 3 14 136.39 2.40 3 3 14 39.80 3.50 4 3 14 0.10 2.80 5 3 14 11.00 4.30 -6 4 14 23.30 4.70 -5 4 14 62.09 3.10 -4 4 14 13.30 2.20 -3 4 14 155.58 3.80 -2 4 14 40.30 1.40 -1 4 14 119.29 3.30 0 4 14 180.48 3.10 1 4 14 108.19 3.10 2 4 14 123.59 2.30 3 4 14 20.00 3.30 4 4 14 8.70 2.80 5 4 14 27.10 4.20 -6 5 14 64.49 10.40 -5 5 14 25.50 3.20 -4 5 14 6.00 2.40 -3 5 14 76.39 3.40 -2 5 14 107.59 2.20 -1 5 14 82.59 3.20 0 5 14 30.80 1.40 1 5 14 26.80 2.80 2 5 14 48.80 1.70 3 5 14 40.40 3.30 4 5 14 76.49 3.10 5 5 14 3.10 4.10 -6 6 14 80.09 2.70 -5 6 14 33.40 3.10 -4 6 14 40.90 2.50 -3 6 14 58.79 4.10 -2 6 14 30.30 1.50 -1 6 14 140.09 88.59 0 6 14 81.29 2.20 1 6 14 140.19 112.29 2 6 14 58.99 1.90 3 6 14 18.20 13.10 4 6 14 98.79 3.40 -5 7 14 12.80 3.00 -4 7 14 120.39 2.70 -3 7 14 56.39 3.20 -2 7 14 137.19 2.50 -1 7 14 79.99 3.30 0 7 14 14.60 1.40 1 7 14 2.30 2.40 2 7 14 12.60 1.60 3 7 14 70.69 4.20 4 7 14 12.80 3.00 -5 8 14 46.00 4.10 -4 8 14 22.80 2.50 -3 8 14 13.20 2.80 -2 8 14 3.30 1.50 -1 8 14 8.70 3.10 0 8 14 85.59 2.40 1 8 14 16.50 3.00 2 8 14 96.29 2.80 3 8 14 2.70 4.40 4 8 14 217.68 167.48 -4 9 14 4.10 2.90 -3 9 14 238.68 5.00 -2 9 14 23.00 1.50 -1 9 14 3.10 3.10 0 9 14 41.20 1.70 1 9 14 16.10 2.90 2 9 14 3.20 1.80 3 9 14 24.80 1.90 -3 10 14 11.50 4.40 -2 10 14 20.90 1.70 -1 10 14 250.57 4.60 0 10 14 75.79 2.40 1 10 14 147.49 4.40 2 10 14 12.80 4.90 -2 11 14 6.40 1.80 -1 11 14 72.39 2.20 0 11 14 102.19 2.70 -6 0 15 99.89 5.90 -5 0 15 98.49 5.60 -4 0 15 16.20 3.50 -3 0 15 231.48 7.60 -2 0 15 4.40 2.00 -1 0 15 4.70 3.90 0 0 15 145.29 3.80 1 0 15 0.00 4.80 2 0 15 185.88 4.20 3 0 15 50.79 20.40 4 0 15 46.40 4.20 -6 1 15 2.40 2.50 -5 1 15 131.39 4.30 -4 1 15 14.20 3.10 -3 1 15 36.60 3.60 -2 1 15 26.30 1.40 -1 1 15 40.70 3.20 0 1 15 3.50 1.40 1 1 15 40.40 4.20 2 1 15 53.99 1.80 3 1 15 17.40 4.10 4 1 15 20.80 2.90 -6 2 15 3.30 2.20 -5 2 15 19.20 15.40 -4 2 15 27.10 2.40 -3 2 15 35.80 3.30 -2 2 15 47.30 1.80 -1 2 15 121.59 3.70 0 2 15 2.30 1.30 1 2 15 141.09 3.80 2 2 15 43.20 2.70 3 2 15 63.19 4.40 4 2 15 52.59 3.10 -6 3 15 115.19 5.80 -5 3 15 17.30 3.50 -4 3 15 105.19 3.00 -3 3 15 93.29 3.50 -2 3 15 94.39 2.30 -1 3 15 38.80 3.20 0 3 15 63.19 1.90 1 3 15 42.30 3.70 2 3 15 53.59 2.20 3 3 15 43.80 17.20 4 3 15 38.00 3.10 -5 4 15 5.30 3.80 -4 4 15 34.50 2.80 -3 4 15 41.20 5.70 -2 4 15 34.30 1.70 -1 4 15 1.20 3.60 0 4 15 38.60 1.60 1 4 15 91.99 3.50 2 4 15 16.90 1.90 3 4 15 8.50 4.00 4 4 15 10.40 3.50 -5 5 15 101.19 4.00 -4 5 15 49.60 2.60 -3 5 15 10.60 3.30 -2 5 15 29.30 2.00 -1 5 15 43.50 3.20 0 5 15 12.40 1.50 1 5 15 33.90 3.40 2 5 15 16.70 1.80 3 5 15 91.19 4.50 4 5 15 51.09 8.40 -5 6 15 35.80 1.90 -4 6 15 34.40 2.80 -3 6 15 27.10 3.60 -2 6 15 9.10 1.80 -1 6 15 30.60 3.40 0 6 15 83.09 2.50 1 6 15 2.40 3.60 2 6 15 3.80 2.00 3 6 15 81.39 5.00 -4 7 15 18.30 2.50 -3 7 15 3.80 3.50 -2 7 15 9.90 2.00 -1 7 15 91.99 3.70 0 7 15 77.29 2.40 1 7 15 4.30 3.80 2 7 15 79.59 2.60 3 7 15 27.00 6.50 -3 8 15 93.59 3.80 -2 8 15 167.98 3.30 -1 8 15 25.50 4.00 0 8 15 38.10 1.90 1 8 15 104.09 5.20 2 8 15 111.39 3.40 -2 9 15 29.70 3.10 -1 9 15 22.30 21.40 0 9 15 34.30 2.10 1 9 15 167.08 5.90 -5 0 16 8.30 3.30 -4 0 16 31.40 4.80 -3 0 16 6.10 5.70 -2 0 16 175.68 5.10 -1 0 16 45.10 5.70 0 0 16 31.10 2.60 1 0 16 14.00 20.60 2 0 16 17.20 3.80 3 0 16 14.60 2.80 -5 1 16 308.77 493.05 -4 1 16 20.50 2.90 -3 1 16 29.90 3.90 -2 1 16 20.40 2.00 -1 1 16 8.50 3.60 0 1 16 117.89 3.00 1 1 16 0.00 7.80 2 1 16 26.00 2.60 3 1 16 30.50 2.20 -4 2 16 69.49 3.30 -3 2 16 36.70 4.10 -2 2 16 43.30 3.80 -1 2 16 83.89 3.90 0 2 16 41.00 2.00 1 2 16 1.30 3.40 2 2 16 110.49 3.40 3 2 16 27.10 2.10 -4 3 16 13.60 3.20 -3 3 16 0.00 4.80 -2 3 16 6.00 2.40 -1 3 16 31.80 4.00 0 3 16 13.40 1.70 1 3 16 3.20 3.50 2 3 16 29.40 2.70 3 3 16 11.20 2.20 -4 4 16 14.80 3.00 -3 4 16 73.29 4.60 -2 4 16 72.49 2.80 -1 4 16 137.69 4.70 0 4 16 162.28 76.99 1 4 16 66.89 4.10 2 4 16 14.10 5.40 -3 5 16 3.30 4.30 -2 5 16 10.60 2.20 -1 5 16 6.10 3.70 0 5 16 33.10 2.00 1 5 16 114.89 4.40 2 5 16 32.20 3.60 -3 6 16 14.50 4.40 -2 6 16 37.80 2.00 -1 6 16 54.79 4.00 0 6 16 12.90 1.90 1 6 16 108.49 4.60 -2 7 16 68.39 16.00 -1 7 16 283.07 4.70 0 7 16 56.29 2.40 -2 0 17 0.40 2.60 -1 0 17 121.29 6.30 0 0 17 0.00 3.20 1 0 17 22.20 5.80 -2 1 17 29.90 1.90 -1 1 17 115.79 4.90 0 1 17 5.00 2.00 1 1 17 82.19 4.90 -2 2 17 20.60 2.10 -1 2 17 6.30 1.90 0 2 17 70.69 2.80 -2 3 17 7.10 5.60 -1 3 17 7.20 2.00 0 3 17 3.00 2.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 13187 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.51247(15) 0.95244(8) 0.60142(9) 0.0208(3) Uani 1 1 d . . . . . Cl2 Cl 0.13531(19) 0.64693(12) 0.85798(13) 0.0371(4) Uani 1 1 d . . . . . Cl3 Cl 1.08282(16) 0.04706(9) 0.92301(10) 0.0261(3) Uani 1 1 d . . . . . Cl4 Cl 0.60812(19) 0.31711(14) 0.64897(14) 0.0427(4) Uani 1 1 d . . . . . B1 B 0.4885(6) 0.8439(4) 0.6573(4) 0.0141(10) Uani 1 1 d . . . . . C2 C 0.3540(5) 0.8084(3) 0.7219(4) 0.0140(9) Uani 1 1 d . . . . . C3 C 0.3347(6) 0.7043(3) 0.6972(3) 0.0137(9) Uani 1 1 d . . . . . B4 B 0.3124(6) 0.6495(4) 0.7956(4) 0.0139(10) Uani 1 1 d . . . . . C5 C 0.4556(6) 0.5985(3) 0.8292(4) 0.0164(10) Uani 1 1 d . . . . . C6 C 0.4852(7) 0.5418(4) 0.9227(4) 0.0269(12) Uani 1 1 d . . . . . H6A H 0.391281 0.540961 0.960171 0.040 Uiso 1 1 calc R U . . . H6B H 0.572090 0.567754 0.965115 0.040 Uiso 1 1 calc R U . . . H6C H 0.511355 0.479776 0.903795 0.040 Uiso 1 1 calc R U . . . C7 C 0.4994(6) 0.6720(3) 0.6685(4) 0.0153(9) Uani 1 1 d . . . . . C8 C 0.6008(6) 0.7592(3) 0.6591(4) 0.0141(9) Uani 1 1 d . . . . . C9 C 0.6308(6) 0.8047(3) 0.7600(4) 0.0144(9) Uani 1 1 d . . . . . C10 C 0.4898(5) 0.8296(3) 0.7965(3) 0.0125(9) Uani 1 1 d . . . . . C11 C 0.4750(7) 0.8905(4) 0.8854(4) 0.0241(11) Uani 1 1 d . . . . . H11A H 0.570012 0.886437 0.930739 0.036 Uiso 1 1 calc R U . . . H11B H 0.385029 0.871794 0.921384 0.036 Uiso 1 1 calc R U . . . H11C H 0.460460 0.953222 0.862267 0.036 Uiso 1 1 calc R U . . . C12 C 0.2071(6) 0.8624(4) 0.7357(4) 0.0226(11) Uani 1 1 d . . . . . H12A H 0.233107 0.926881 0.741988 0.034 Uiso 1 1 calc R U . . . H12B H 0.160627 0.841876 0.796706 0.034 Uiso 1 1 calc R U . . . H12C H 0.132425 0.853242 0.677269 0.034 Uiso 1 1 calc R U . . . C13 C 0.7876(6) 0.8333(4) 0.8025(5) 0.0262(12) Uani 1 1 d . . . . . H13A H 0.827069 0.881636 0.760791 0.039 Uiso 1 1 calc R U . . . H13B H 0.859018 0.781461 0.803541 0.039 Uiso 1 1 calc R U . . . H13C H 0.780429 0.855694 0.871236 0.039 Uiso 1 1 calc R U . . . C14 C 0.7374(6) 0.7562(4) 0.5933(4) 0.0255(12) Uani 1 1 d . . . . . H14A H 0.700057 0.738951 0.524618 0.038 Uiso 1 1 calc R U . . . H14B H 0.813814 0.711523 0.620402 0.038 Uiso 1 1 calc R U . . . H14C H 0.786517 0.816070 0.592364 0.038 Uiso 1 1 calc R U . . . C15 C 0.5608(6) 0.6126(4) 0.7584(4) 0.0195(10) Uani 1 1 d . . . . . C16 C 0.7371(7) 0.5708(3) 0.7641(4) 0.0216(11) Uani 1 1 d . . . . . H16A H 0.759067 0.539988 0.828770 0.032 Uiso 1 1 calc R U . . . H16B H 0.812392 0.619886 0.757724 0.032 Uiso 1 1 calc R U . . . H16C H 0.745504 0.527270 0.709143 0.032 Uiso 1 1 calc R U . . . C17 C 0.4966(7) 0.6154(4) 0.5722(4) 0.0254(12) Uani 1 1 d . . . . . H17A H 0.432628 0.561188 0.579702 0.038 Uiso 1 1 calc R U . . . H17B H 0.603183 0.597278 0.559878 0.038 Uiso 1 1 calc R U . . . H17C H 0.452198 0.651458 0.515265 0.038 Uiso 1 1 calc R U . . . C18 C 0.2021(6) 0.6917(4) 0.6146(4) 0.0237(11) Uani 1 1 d . . . . . H18A H 0.103230 0.710742 0.640171 0.036 Uiso 1 1 calc R U . . . H18B H 0.195330 0.627657 0.595136 0.036 Uiso 1 1 calc R U . . . H18C H 0.222973 0.728482 0.555937 0.036 Uiso 1 1 calc R U . . . B19 B 1.0335(6) 0.1491(4) 0.8552(4) 0.0164(10) Uani 1 1 d . . . . . C20 C 0.8728(5) 0.1786(3) 0.7984(4) 0.0142(9) Uani 1 1 d . . . . . C21 C 0.8622(6) 0.2844(3) 0.8061(4) 0.0142(9) Uani 1 1 d . . . . . B22 B 0.8045(6) 0.3268(4) 0.7029(4) 0.0159(10) Uani 1 1 d . . . . . C23 C 0.9282(6) 0.3750(4) 0.6541(4) 0.0179(10) Uani 1 1 d . . . . . C24 C 0.9175(7) 0.4242(4) 0.5547(4) 0.0281(12) Uani 1 1 d . . . . . H24A H 0.814099 0.414311 0.520230 0.042 Uiso 1 1 calc R U . . . H24B H 0.997629 0.400978 0.512793 0.042 Uiso 1 1 calc R U . . . H24C H 0.933824 0.489168 0.566302 0.042 Uiso 1 1 calc R U . . . C25 C 1.0388(5) 0.3185(3) 0.8185(4) 0.0149(9) Uani 1 1 d . . . . . C26 C 1.1423(6) 0.2309(3) 0.8294(4) 0.0159(9) Uani 1 1 d . . . . . C27 C 1.1254(6) 0.1748(3) 0.7345(4) 0.0143(9) Uani 1 1 d . . . . . C28 C 0.9730(6) 0.1462(3) 0.7161(3) 0.0147(9) Uani 1 1 d . . . . . C29 C 0.7240(6) 0.1248(4) 0.8078(5) 0.0283(13) Uani 1 1 d . . . . . H29A H 0.745087 0.060171 0.798320 0.042 Uiso 1 1 calc R U . . . H29B H 0.644076 0.145025 0.756366 0.042 Uiso 1 1 calc R U . . . H29C H 0.686861 0.134315 0.874758 0.042 Uiso 1 1 calc R U . . . C30 C 0.9191(7) 0.0759(4) 0.6403(4) 0.0283(12) Uani 1 1 d . . . . . H30A H 0.979342 0.081260 0.580934 0.042 Uiso 1 1 calc R U . . . H30B H 0.808161 0.084987 0.620398 0.042 Uiso 1 1 calc R U . . . H30C H 0.934660 0.015454 0.669821 0.042 Uiso 1 1 calc R U . . . C31 C 1.2612(6) 0.1389(4) 0.6827(4) 0.0243(11) Uani 1 1 d . . . . . H31A H 1.333443 0.188528 0.671126 0.036 Uiso 1 1 calc R U . . . H31B H 1.223897 0.112014 0.618066 0.036 Uiso 1 1 calc R U . . . H31C H 1.315200 0.092593 0.725033 0.036 Uiso 1 1 calc R U . . . C32 C 1.3069(6) 0.2394(4) 0.8781(5) 0.0277(12) Uani 1 1 d . . . . . H32A H 1.356901 0.179685 0.880746 0.042 Uiso 1 1 calc R U . . . H32B H 1.303214 0.263200 0.946557 0.042 Uiso 1 1 calc R U . . . H32C H 1.366974 0.280865 0.838459 0.042 Uiso 1 1 calc R U . . . C33 C 1.0619(6) 0.3698(3) 0.7194(4) 0.0168(9) Uani 1 1 d . . . . . C34 C 1.2334(6) 0.4124(3) 0.6957(3) 0.0135(9) Uani 1 1 d . . . . . H34A H 1.245365 0.409601 0.623207 0.020 Uiso 1 1 calc R U . . . H34B H 1.316627 0.377208 0.731728 0.020 Uiso 1 1 calc R U . . . H34C H 1.239697 0.475631 0.718156 0.020 Uiso 1 1 calc R U . . . C35 C 1.0734(7) 0.3822(4) 0.9086(4) 0.0272(12) Uani 1 1 d . . . . . H35A H 1.008402 0.436631 0.899798 0.041 Uiso 1 1 calc R U . . . H35B H 1.183726 0.399573 0.912692 0.041 Uiso 1 1 calc R U . . . H35C H 1.050079 0.351124 0.970676 0.041 Uiso 1 1 calc R U . . . C36 C 0.7660(6) 0.3106(4) 0.8931(4) 0.0237(11) Uani 1 1 d . . . . . H36A H 0.659615 0.287204 0.880519 0.036 Uiso 1 1 calc R U . . . H36B H 0.762730 0.376812 0.898865 0.036 Uiso 1 1 calc R U . . . H36C H 0.813649 0.284783 0.955803 0.036 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0243(6) 0.0156(5) 0.0226(6) 0.0080(5) 0.0016(4) -0.0027(5) Cl2 0.0321(8) 0.0364(8) 0.0446(9) 0.0098(7) 0.0142(6) -0.0001(7) Cl3 0.0322(7) 0.0211(6) 0.0254(6) 0.0099(5) 0.0048(5) 0.0072(6) Cl4 0.0282(8) 0.0549(11) 0.0441(9) 0.0128(8) -0.0026(7) -0.0034(8) B1 0.012(2) 0.016(3) 0.013(2) -0.0012(19) -0.0010(18) 0.001(2) C2 0.013(2) 0.013(2) 0.016(2) 0.0023(18) 0.0004(17) 0.0010(18) C3 0.016(2) 0.014(2) 0.011(2) -0.0020(17) -0.0011(17) 0.0001(18) B4 0.014(2) 0.012(2) 0.016(2) -0.001(2) 0.0042(19) -0.009(2) C5 0.018(2) 0.012(2) 0.019(2) 0.0001(18) -0.0011(18) -0.0025(19) C6 0.032(3) 0.025(3) 0.023(3) 0.010(2) 0.000(2) 0.000(3) C7 0.018(2) 0.013(2) 0.015(2) -0.0043(18) 0.0004(17) -0.0036(18) C8 0.013(2) 0.012(2) 0.017(2) 0.0000(18) 0.0022(17) -0.0036(17) C9 0.017(2) 0.010(2) 0.016(2) 0.0038(17) -0.0011(18) 0.0017(18) C10 0.016(2) 0.010(2) 0.012(2) -0.0001(17) 0.0034(16) -0.0012(18) C11 0.029(3) 0.025(3) 0.018(2) -0.008(2) 0.003(2) -0.006(2) C12 0.017(2) 0.017(2) 0.034(3) 0.003(2) 0.007(2) 0.007(2) C13 0.019(3) 0.025(3) 0.034(3) -0.001(2) -0.006(2) -0.001(2) C14 0.022(3) 0.026(3) 0.030(3) -0.001(2) 0.013(2) -0.003(2) C15 0.018(2) 0.016(2) 0.024(2) 0.000(2) 0.0014(19) 0.0006(19) C16 0.030(3) 0.011(2) 0.025(3) 0.0079(19) 0.008(2) -0.002(2) C17 0.030(3) 0.023(3) 0.023(3) -0.010(2) 0.005(2) -0.004(2) C18 0.015(2) 0.024(3) 0.031(3) -0.002(2) -0.004(2) -0.002(2) B19 0.017(2) 0.019(3) 0.013(2) 0.000(2) 0.0005(19) 0.003(2) C20 0.013(2) 0.012(2) 0.018(2) 0.0019(18) 0.0015(17) 0.0009(17) C21 0.014(2) 0.014(2) 0.015(2) -0.0009(17) 0.0020(17) 0.0020(18) B22 0.014(2) 0.017(3) 0.017(2) 0.001(2) -0.0015(19) -0.001(2) C23 0.022(2) 0.016(2) 0.016(2) 0.0021(19) 0.0017(19) -0.001(2) C24 0.032(3) 0.029(3) 0.024(3) 0.009(2) 0.004(2) 0.003(2) C25 0.013(2) 0.013(2) 0.018(2) -0.0014(18) -0.0014(17) 0.0035(18) C26 0.015(2) 0.014(2) 0.019(2) -0.0009(19) 0.0024(18) 0.0033(18) C27 0.016(2) 0.012(2) 0.015(2) 0.0017(17) 0.0057(17) 0.0033(18) C28 0.018(2) 0.013(2) 0.013(2) 0.0026(18) 0.0016(17) 0.0032(19) C29 0.015(2) 0.027(3) 0.043(3) 0.005(3) 0.007(2) -0.002(2) C30 0.035(3) 0.024(3) 0.024(3) -0.009(2) -0.004(2) -0.002(2) C31 0.023(3) 0.020(3) 0.032(3) 0.003(2) 0.013(2) 0.008(2) C32 0.017(3) 0.028(3) 0.037(3) -0.001(2) -0.007(2) -0.001(2) C33 0.016(2) 0.012(2) 0.023(2) 0.0015(19) 0.0056(19) -0.0004(18) C34 0.016(2) 0.011(2) 0.013(2) 0.0044(17) -0.0033(17) 0.0070(18) C35 0.027(3) 0.029(3) 0.025(3) -0.010(2) 0.000(2) -0.001(2) C36 0.020(2) 0.029(3) 0.023(3) -0.003(2) 0.008(2) 0.006(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 B1 C9 119.8(3) . . ? Cl1 B1 C10 121.6(3) . . ? C2 B1 Cl1 129.5(4) . . ? C2 B1 C9 87.9(3) . . ? C2 B1 C10 51.1(3) . . ? C8 B1 Cl1 128.8(4) . . ? C8 B1 C2 101.6(4) . . ? C8 B1 C9 51.3(3) . . ? C8 B1 C10 86.4(3) . . ? C9 B1 C10 43.8(2) . . ? C3 C2 B1 106.2(4) . . ? C10 C2 B1 74.3(3) . . ? C10 C2 C3 113.8(4) . . ? C10 C2 C12 115.0(4) . . ? C12 C2 B1 122.8(4) . . ? C12 C2 C3 117.5(4) . . ? B4 C3 C2 110.2(4) . . ? B4 C3 C7 102.5(4) . . ? C7 C3 C2 105.4(4) . . ? C18 C3 C2 109.2(4) . . ? C18 C3 B4 113.9(4) . . ? C18 C3 C7 115.1(4) . . ? C3 B4 Cl2 124.2(4) . . ? C5 B4 Cl2 124.4(4) . . ? C5 B4 C3 111.3(4) . . ? B4 C5 C6 128.1(5) . . ? C15 C5 B4 106.9(4) . . ? C15 C5 C6 125.0(5) . . ? C5 C6 H6A 109.5 . . ? C5 C6 H6B 109.5 . . ? C5 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C8 C7 C3 106.7(4) . . ? C15 C7 C3 104.2(4) . . ? C15 C7 C8 111.7(4) . . ? C17 C7 C3 114.4(4) . . ? C17 C7 C8 110.8(4) . . ? C17 C7 C15 108.9(4) . . ? C7 C8 B1 108.0(4) . . ? C9 C8 B1 74.0(3) . . ? C9 C8 C7 110.7(4) . . ? C9 C8 C14 116.1(4) . . ? C14 C8 B1 120.9(4) . . ? C14 C8 C7 118.8(4) . . ? C8 C9 B1 54.8(3) . . ? C10 C9 B1 68.4(3) . . ? C10 C9 C8 109.5(4) . . ? C10 C9 C13 125.7(5) . . ? C13 C9 B1 136.2(4) . . ? C13 C9 C8 123.9(4) . . ? C2 C10 B1 54.7(3) . . ? C9 C10 B1 67.8(3) . . ? C9 C10 C2 111.6(4) . . ? C9 C10 C11 124.2(4) . . ? C11 C10 B1 136.2(4) . . ? C11 C10 C2 122.5(4) . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C2 C12 H12A 109.5 . . ? C2 C12 H12B 109.5 . . ? C2 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C9 C13 H13A 109.5 . . ? C9 C13 H13B 109.5 . . ? C9 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C8 C14 H14A 109.5 . . ? C8 C14 H14B 109.5 . . ? C8 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C5 C15 C7 114.5(4) . . ? C5 C15 C16 124.7(5) . . ? C7 C15 C16 120.8(4) . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C7 C17 H17A 109.5 . . ? C7 C17 H17B 109.5 . . ? C7 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C3 C18 H18A 109.5 . . ? C3 C18 H18B 109.5 . . ? C3 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? Cl3 B19 C27 120.1(3) . . ? Cl3 B19 C28 120.9(4) . . ? C20 B19 Cl3 129.5(4) . . ? C20 B19 C27 86.8(3) . . ? C20 B19 C28 51.1(3) . . ? C26 B19 Cl3 129.1(4) . . ? C26 B19 C20 101.3(4) . . ? C26 B19 C27 50.8(3) . . ? C26 B19 C28 85.9(3) . . ? C27 B19 C28 43.0(2) . . ? C21 C20 B19 107.2(4) . . ? C28 C20 B19 74.8(3) . . ? C28 C20 C21 113.5(4) . . ? C29 C20 B19 121.8(4) . . ? C29 C20 C21 117.6(4) . . ? C29 C20 C28 114.8(4) . . ? C20 C21 C25 105.2(4) . . ? B22 C21 C20 111.1(4) . . ? B22 C21 C25 101.7(4) . . ? C36 C21 C20 109.9(4) . . ? C36 C21 B22 114.4(4) . . ? C36 C21 C25 114.1(4) . . ? C21 B22 Cl4 123.4(4) . . ? C23 B22 Cl4 123.6(4) . . ? C23 B22 C21 113.0(4) . . ? B22 C23 C24 128.5(5) . . ? C33 C23 B22 106.7(4) . . ? C33 C23 C24 124.7(5) . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C26 C25 C21 106.1(4) . . ? C33 C25 C21 104.3(4) . . ? C33 C25 C26 111.9(4) . . ? C35 C25 C21 113.6(4) . . ? C35 C25 C26 110.9(4) . . ? C35 C25 C33 109.7(4) . . ? C25 C26 B19 108.0(4) . . ? C27 C26 B19 75.1(4) . . ? C27 C26 C25 110.9(4) . . ? C27 C26 C32 115.6(4) . . ? C32 C26 B19 121.2(5) . . ? C32 C26 C25 118.4(4) . . ? C26 C27 B19 54.2(3) . . ? C28 C27 B19 68.7(3) . . ? C28 C27 C26 110.3(4) . . ? C28 C27 C31 124.9(5) . . ? C31 C27 B19 135.6(4) . . ? C31 C27 C26 123.5(4) . . ? C20 C28 B19 54.1(3) . . ? C27 C28 B19 68.3(3) . . ? C27 C28 C20 110.9(4) . . ? C27 C28 C30 125.0(5) . . ? C30 C28 B19 136.7(4) . . ? C30 C28 C20 122.8(4) . . ? C20 C29 H29A 109.5 . . ? C20 C29 H29B 109.5 . . ? C20 C29 H29C 109.5 . . ? H29A C29 H29B 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C28 C30 H30A 109.5 . . ? C28 C30 H30B 109.5 . . ? C28 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C27 C31 H31A 109.5 . . ? C27 C31 H31B 109.5 . . ? C27 C31 H31C 109.5 . . ? H31A C31 H31B 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C26 C32 H32A 109.5 . . ? C26 C32 H32B 109.5 . . ? C26 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C23 C33 C25 114.1(4) . . ? C23 C33 C34 124.4(4) . . ? C25 C33 C34 121.5(4) . . ? C33 C34 H34A 109.5 . . ? C33 C34 H34B 109.5 . . ? C33 C34 H34C 109.5 . . ? H34A C34 H34B 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C25 C35 H35A 109.5 . . ? C25 C35 H35B 109.5 . . ? C25 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C21 C36 H36A 109.5 . . ? C21 C36 H36B 109.5 . . ? C21 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 B1 1.784(6) . ? Cl2 B4 1.789(5) . ? Cl3 B19 1.791(6) . ? Cl4 B22 1.790(6) . ? B1 C2 1.582(7) . ? B1 C8 1.579(7) . ? B1 C9 1.858(7) . ? B1 C10 1.866(7) . ? C2 C3 1.577(7) . ? C2 C10 1.508(6) . ? C2 C12 1.516(7) . ? C3 B4 1.565(7) . ? C3 C7 1.568(7) . ? C3 C18 1.535(7) . ? B4 C5 1.483(7) . ? C5 C6 1.507(7) . ? C5 C15 1.371(7) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 C8 1.565(7) . ? C7 C15 1.544(7) . ? C7 C17 1.530(7) . ? C8 C9 1.507(7) . ? C8 C14 1.517(7) . ? C9 C10 1.389(7) . ? C9 C13 1.484(7) . ? C10 C11 1.501(7) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C16 1.633(7) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? B19 C20 1.585(7) . ? B19 C26 1.580(8) . ? B19 C27 1.882(7) . ? B19 C28 1.887(7) . ? C20 C21 1.567(7) . ? C20 C28 1.522(7) . ? C20 C29 1.519(7) . ? C21 B22 1.558(7) . ? C21 C25 1.596(7) . ? C21 C36 1.524(7) . ? B22 C23 1.470(7) . ? C23 C24 1.507(7) . ? C23 C33 1.391(7) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 C26 1.569(7) . ? C25 C33 1.547(7) . ? C25 C35 1.536(7) . ? C26 C27 1.509(7) . ? C26 C32 1.517(7) . ? C27 C28 1.381(7) . ? C27 C31 1.497(7) . ? C28 C30 1.497(7) . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C33 C34 1.655(7) . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl1 B1 C2 C3 147.3(4) . . . . ? Cl1 B1 C2 C10 -102.0(5) . . . . ? Cl1 B1 C2 C12 7.9(7) . . . . ? Cl1 B1 C8 C7 -153.1(4) . . . . ? Cl1 B1 C8 C9 99.9(5) . . . . ? Cl1 B1 C8 C14 -11.4(7) . . . . ? Cl1 B1 C9 C8 -117.9(4) . . . . ? Cl1 B1 C9 C10 106.1(4) . . . . ? Cl1 B1 C9 C13 -13.5(8) . . . . ? Cl1 B1 C10 C2 117.6(4) . . . . ? Cl1 B1 C10 C9 -101.5(4) . . . . ? Cl1 B1 C10 C11 15.3(8) . . . . ? Cl2 B4 C5 C6 -4.7(8) . . . . ? Cl2 B4 C5 C15 175.6(4) . . . . ? Cl3 B19 C20 C21 148.7(4) . . . . ? Cl3 B19 C20 C28 -100.9(5) . . . . ? Cl3 B19 C20 C29 9.2(7) . . . . ? Cl3 B19 C26 C25 -152.7(4) . . . . ? Cl3 B19 C26 C27 99.8(5) . . . . ? Cl3 B19 C26 C32 -11.3(7) . . . . ? Cl3 B19 C27 C26 -117.9(5) . . . . ? Cl3 B19 C27 C28 104.4(4) . . . . ? Cl3 B19 C27 C31 -14.3(8) . . . . ? Cl3 B19 C28 C20 118.0(5) . . . . ? Cl3 B19 C28 C27 -102.4(4) . . . . ? Cl3 B19 C28 C30 16.1(8) . . . . ? Cl4 B22 C23 C24 0.4(9) . . . . ? Cl4 B22 C23 C33 178.5(4) . . . . ? B1 C2 C3 B4 138.2(4) . . . . ? B1 C2 C3 C7 28.3(5) . . . . ? B1 C2 C3 C18 -95.9(5) . . . . ? B1 C2 C10 C9 -38.9(4) . . . . ? B1 C2 C10 C11 126.7(5) . . . . ? B1 C8 C9 C10 43.2(4) . . . . ? B1 C8 C9 C13 -126.2(5) . . . . ? B1 C9 C10 C2 33.6(4) . . . . ? B1 C9 C10 C11 -131.7(5) . . . . ? C2 B1 C8 C7 29.3(5) . . . . ? C2 B1 C8 C9 -77.8(4) . . . . ? C2 B1 C8 C14 171.0(4) . . . . ? C2 B1 C9 C8 106.6(4) . . . . ? C2 B1 C9 C10 -29.4(3) . . . . ? C2 B1 C9 C13 -149.0(6) . . . . ? C2 B1 C10 C9 140.8(4) . . . . ? C2 B1 C10 C11 -102.3(6) . . . . ? C2 C3 B4 Cl2 75.7(5) . . . . ? C2 C3 B4 C5 -105.5(5) . . . . ? C2 C3 C7 C8 -9.5(5) . . . . ? C2 C3 C7 C15 108.8(4) . . . . ? C2 C3 C7 C17 -132.4(4) . . . . ? C3 C2 C10 B1 101.1(4) . . . . ? C3 C2 C10 C9 62.1(5) . . . . ? C3 C2 C10 C11 -132.2(5) . . . . ? C3 B4 C5 C6 176.5(5) . . . . ? C3 B4 C5 C15 -3.2(6) . . . . ? C3 C7 C8 B1 -12.7(5) . . . . ? C3 C7 C8 C9 66.5(5) . . . . ? C3 C7 C8 C14 -155.4(4) . . . . ? C3 C7 C15 C5 5.5(6) . . . . ? C3 C7 C15 C16 -175.2(4) . . . . ? B4 C3 C7 C8 -124.9(4) . . . . ? B4 C3 C7 C15 -6.6(5) . . . . ? B4 C3 C7 C17 112.2(5) . . . . ? B4 C5 C15 C7 -1.5(6) . . . . ? B4 C5 C15 C16 179.1(5) . . . . ? C6 C5 C15 C7 178.8(5) . . . . ? C6 C5 C15 C16 -0.6(8) . . . . ? C7 C3 B4 Cl2 -172.5(4) . . . . ? C7 C3 B4 C5 6.3(5) . . . . ? C7 C8 C9 B1 -103.6(4) . . . . ? C7 C8 C9 C10 -60.4(5) . . . . ? C7 C8 C9 C13 130.2(5) . . . . ? C8 B1 C2 C3 -35.1(4) . . . . ? C8 B1 C2 C10 75.7(4) . . . . ? C8 B1 C2 C12 -174.5(5) . . . . ? C8 B1 C9 C10 -136.1(4) . . . . ? C8 B1 C9 C13 104.4(7) . . . . ? C8 B1 C10 C2 -108.0(4) . . . . ? C8 B1 C10 C9 32.8(3) . . . . ? C8 B1 C10 C11 149.7(6) . . . . ? C8 C7 C15 C5 120.3(5) . . . . ? C8 C7 C15 C16 -60.3(6) . . . . ? C8 C9 C10 B1 -37.0(4) . . . . ? C8 C9 C10 C2 -3.3(5) . . . . ? C8 C9 C10 C11 -168.7(5) . . . . ? C9 B1 C2 C3 -84.8(4) . . . . ? C9 B1 C2 C10 25.9(3) . . . . ? C9 B1 C2 C12 135.8(5) . . . . ? C9 B1 C8 C7 107.1(4) . . . . ? C9 B1 C8 C14 -111.2(5) . . . . ? C9 B1 C10 C2 -140.8(4) . . . . ? C9 B1 C10 C11 116.9(6) . . . . ? C10 B1 C2 C3 -110.8(4) . . . . ? C10 B1 C2 C12 109.9(5) . . . . ? C10 B1 C8 C7 78.3(4) . . . . ? C10 B1 C8 C9 -28.8(3) . . . . ? C10 B1 C8 C14 -140.0(5) . . . . ? C10 B1 C9 C8 136.1(4) . . . . ? C10 B1 C9 C13 -119.5(7) . . . . ? C10 C2 C3 B4 58.6(5) . . . . ? C10 C2 C3 C7 -51.3(5) . . . . ? C10 C2 C3 C18 -175.5(4) . . . . ? C12 C2 C3 B4 -79.9(5) . . . . ? C12 C2 C3 C7 170.1(4) . . . . ? C12 C2 C3 C18 46.0(6) . . . . ? C12 C2 C10 B1 -119.3(5) . . . . ? C12 C2 C10 C9 -158.2(4) . . . . ? C12 C2 C10 C11 7.4(7) . . . . ? C13 C9 C10 B1 132.2(5) . . . . ? C13 C9 C10 C2 165.8(5) . . . . ? C13 C9 C10 C11 0.4(8) . . . . ? C14 C8 C9 B1 117.0(5) . . . . ? C14 C8 C9 C10 160.2(4) . . . . ? C14 C8 C9 C13 -9.1(7) . . . . ? C15 C7 C8 B1 -126.0(4) . . . . ? C15 C7 C8 C9 -46.8(5) . . . . ? C15 C7 C8 C14 91.3(5) . . . . ? C17 C7 C8 B1 112.4(5) . . . . ? C17 C7 C8 C9 -168.4(4) . . . . ? C17 C7 C8 C14 -30.2(6) . . . . ? C17 C7 C15 C5 -117.0(5) . . . . ? C17 C7 C15 C16 62.3(6) . . . . ? C18 C3 B4 Cl2 -47.5(6) . . . . ? C18 C3 B4 C5 131.3(5) . . . . ? C18 C3 C7 C8 110.9(5) . . . . ? C18 C3 C7 C15 -130.9(4) . . . . ? C18 C3 C7 C17 -12.1(6) . . . . ? B19 C20 C21 B22 135.3(4) . . . . ? B19 C20 C21 C25 26.1(5) . . . . ? B19 C20 C21 C36 -97.1(5) . . . . ? B19 C20 C28 C27 -40.2(4) . . . . ? B19 C20 C28 C30 127.0(5) . . . . ? B19 C26 C27 C28 41.9(4) . . . . ? B19 C26 C27 C31 -125.4(5) . . . . ? B19 C27 C28 C20 34.3(4) . . . . ? B19 C27 C28 C30 -132.6(6) . . . . ? C20 B19 C26 C25 31.2(5) . . . . ? C20 B19 C26 C27 -76.3(4) . . . . ? C20 B19 C26 C32 172.5(5) . . . . ? C20 B19 C27 C26 107.4(4) . . . . ? C20 B19 C27 C28 -30.4(4) . . . . ? C20 B19 C27 C31 -149.1(6) . . . . ? C20 B19 C28 C27 139.5(5) . . . . ? C20 B19 C28 C30 -101.9(7) . . . . ? C20 C21 B22 Cl4 71.6(5) . . . . ? C20 C21 B22 C23 -108.0(5) . . . . ? C20 C21 C25 C26 -6.1(5) . . . . ? C20 C21 C25 C33 112.3(4) . . . . ? C20 C21 C25 C35 -128.2(5) . . . . ? C21 C20 C28 B19 102.4(5) . . . . ? C21 C20 C28 C27 62.2(5) . . . . ? C21 C20 C28 C30 -130.5(5) . . . . ? C21 B22 C23 C24 179.9(5) . . . . ? C21 B22 C23 C33 -1.9(6) . . . . ? C21 C25 C26 B19 -16.2(5) . . . . ? C21 C25 C26 C27 64.3(5) . . . . ? C21 C25 C26 C32 -158.8(4) . . . . ? C21 C25 C33 C23 2.9(6) . . . . ? C21 C25 C33 C34 -176.4(4) . . . . ? B22 C21 C25 C26 -121.9(4) . . . . ? B22 C21 C25 C33 -3.5(5) . . . . ? B22 C21 C25 C35 115.9(5) . . . . ? B22 C23 C33 C25 -0.7(6) . . . . ? B22 C23 C33 C34 178.5(4) . . . . ? C24 C23 C33 C25 177.6(5) . . . . ? C24 C23 C33 C34 -3.2(8) . . . . ? C25 C21 B22 Cl4 -177.0(4) . . . . ? C25 C21 B22 C23 3.5(6) . . . . ? C25 C26 C27 B19 -103.9(4) . . . . ? C25 C26 C27 C28 -62.0(5) . . . . ? C25 C26 C27 C31 130.7(5) . . . . ? C26 B19 C20 C21 -35.2(5) . . . . ? C26 B19 C20 C28 75.2(4) . . . . ? C26 B19 C20 C29 -174.7(5) . . . . ? C26 B19 C27 C28 -137.7(4) . . . . ? C26 B19 C27 C31 103.6(7) . . . . ? C26 B19 C28 C20 -108.1(4) . . . . ? C26 B19 C28 C27 31.5(3) . . . . ? C26 B19 C28 C30 150.0(6) . . . . ? C26 C25 C33 C23 117.2(5) . . . . ? C26 C25 C33 C34 -62.0(6) . . . . ? C26 C27 C28 B19 -35.5(4) . . . . ? C26 C27 C28 C20 -1.3(6) . . . . ? C26 C27 C28 C30 -168.2(5) . . . . ? C27 B19 C20 C21 -84.1(4) . . . . ? C27 B19 C20 C28 26.3(3) . . . . ? C27 B19 C20 C29 136.4(5) . . . . ? C27 B19 C26 C25 107.5(4) . . . . ? C27 B19 C26 C32 -111.1(5) . . . . ? C27 B19 C28 C20 -139.5(5) . . . . ? C27 B19 C28 C30 118.5(7) . . . . ? C28 B19 C20 C21 -110.4(4) . . . . ? C28 B19 C20 C29 110.1(5) . . . . ? C28 B19 C26 C25 80.2(4) . . . . ? C28 B19 C26 C27 -27.4(3) . . . . ? C28 B19 C26 C32 -138.5(5) . . . . ? C28 B19 C27 C26 137.7(4) . . . . ? C28 B19 C27 C31 -118.7(7) . . . . ? C28 C20 C21 B22 54.9(5) . . . . ? C28 C20 C21 C25 -54.4(5) . . . . ? C28 C20 C21 C36 -177.5(4) . . . . ? C29 C20 C21 B22 -83.2(5) . . . . ? C29 C20 C21 C25 167.6(4) . . . . ? C29 C20 C21 C36 44.4(6) . . . . ? C29 C20 C28 B19 -118.4(5) . . . . ? C29 C20 C28 C27 -158.6(5) . . . . ? C29 C20 C28 C30 8.7(7) . . . . ? C31 C27 C28 B19 131.5(5) . . . . ? C31 C27 C28 C20 165.8(5) . . . . ? C31 C27 C28 C30 -1.1(8) . . . . ? C32 C26 C27 B19 117.8(5) . . . . ? C32 C26 C27 C28 159.7(5) . . . . ? C32 C26 C27 C31 -7.6(7) . . . . ? C33 C25 C26 B19 -129.4(4) . . . . ? C33 C25 C26 C27 -49.0(5) . . . . ? C33 C25 C26 C32 88.0(5) . . . . ? C35 C25 C26 B19 107.7(5) . . . . ? C35 C25 C26 C27 -171.9(4) . . . . ? C35 C25 C26 C32 -34.9(6) . . . . ? C35 C25 C33 C23 -119.2(5) . . . . ? C35 C25 C33 C34 61.6(6) . . . . ? C36 C21 B22 Cl4 -53.5(6) . . . . ? C36 C21 B22 C23 126.9(5) . . . . ? C36 C21 C25 C26 114.4(5) . . . . ? C36 C21 C25 C33 -127.2(4) . . . . ? C36 C21 C25 C35 -7.8(6) . . . . ?