#------------------------------------------------------------------------------ #$Date: 2024-10-04 01:13:05 +0300 (Fri, 04 Oct 2024) $ #$Revision: 295024 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572765.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572765 loop_ _publ_author_name 'Zhang, Chonghe' 'Gilliard, Robert J.' 'Cummins, Christopher' _publ_section_title ; Arene extrusion as an approach to reductive elimination at boron: Implication of carbene-ligated haloborylene as a transient reactive intermediate ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC05524A _journal_year 2024 _chemical_formula_moiety 'C23 H35 B Br N' _chemical_formula_sum 'C23 H35 B Br N' _chemical_formula_weight 416.24 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_date 2023-07-12 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-09-26 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 80.686(3) _cell_angle_beta 87.975(3) _cell_angle_gamma 80.672(3) _cell_formula_units_Z 2 _cell_length_a 8.7428(7) _cell_length_b 9.4037(8) _cell_length_c 13.3258(11) _cell_measurement_reflns_used 9865 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 31.227 _cell_measurement_theta_min 2.500 _cell_volume 1066.79(15) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2018)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2018)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100.00 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0428 _diffrn_reflns_av_unetI/netI 0.0207 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 70071 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.384 _diffrn_reflns_theta_min 1.549 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.933 _exptl_absorpt_correction_T_max 0.7462 _exptl_absorpt_correction_T_min 0.6533 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1042 before and 0.0574 after correction. The Ratio of minimum to maximum transmission is 0.8755. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.296 _exptl_crystal_description plate _exptl_crystal_F_000 440 _exptl_crystal_size_max 0.102 _exptl_crystal_size_mid 0.098 _exptl_crystal_size_min 0.021 _refine_diff_density_max 0.682 _refine_diff_density_min -0.462 _refine_diff_density_rms 0.063 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 241 _refine_ls_number_reflns 6941 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.073 _refine_ls_R_factor_all 0.0283 _refine_ls_R_factor_gt 0.0242 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0387P)^2^+0.2177P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0646 _refine_ls_wR_factor_ref 0.0660 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6289 _reflns_number_total 6941 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05524a3.cif _cod_data_source_block 8 _cod_database_code 1572765 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.961 _shelx_estimated_absorpt_t_min 0.827 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C10(H10), C1(H1) 2.b Secondary CH2 refined with riding coordinates: C21(H21A,H21B), C22(H22A,H22B), C23(H23A,H23B), C20(H20A,H20B), C19(H19A, H19B), C15(H15A,H15B) 2.c Aromatic/amide H refined with riding coordinates: C5(H5), C6(H6), C7(H7) 2.d Idealised Me refined as rotating group: C11(H11A,H11B,H11C), C12(H12A,H12B,H12C), C3(H3A,H3B,H3C), C2(H2A,H2B,H2C), C17(H17A,H17B,H17C), C18(H18A,H18B,H18C) ; _shelx_res_file ; TITL mo_P8_23112_0m_a.res in P-1 mo_p8_23112_0m_a.res created by SHELXL-2016/6 at 22:58:23 on 12-Jul-2023 REM mo_P8_23112_0m_a.res in P-1 REM 241 parameters refined using 0 restraints CELL 0.71073 8.7428 9.4037 13.3258 80.686 87.975 80.672 ZERR 2 0.0007 0.0008 0.0011 0.003 0.003 0.003 LATT 1 SFAC C H B Br N UNIT 46 70 2 2 2 L.S. 20 PLAN 6 0 0 SIZE 0.102 0.021 0.098 TEMP -173.15 CONF HTAB BOND $H MORE -1 fmap 2 acta OMIT 3 4 4 OMIT -3 -3 2 REM REM REM WGHT 0.038700 0.217700 FVAR 0.63362 BR1 4 0.365334 0.713627 0.867565 11.00000 0.01811 0.02431 = 0.01535 -0.00611 0.00303 -0.00414 N1 5 0.736661 0.769761 0.686233 11.00000 0.01380 0.01485 = 0.01220 -0.00223 -0.00049 -0.00215 C21 1 0.807834 0.876789 1.058702 11.00000 0.03140 0.03323 = 0.01663 -0.00908 -0.00194 -0.01230 AFIX 23 H21A 2 0.712946 0.850552 1.094789 11.00000 -1.20000 H21B 2 0.867169 0.918341 1.105605 11.00000 -1.20000 AFIX 0 C22 1 0.906161 0.739509 1.028900 11.00000 0.03314 0.03016 = 0.01916 -0.00396 -0.01102 -0.00529 AFIX 23 H22A 2 0.927770 0.664821 1.090288 11.00000 -1.20000 H22B 2 1.006515 0.763591 1.000188 11.00000 -1.20000 AFIX 0 C23 1 0.823123 0.677395 0.950457 11.00000 0.02816 0.02165 = 0.01570 -0.00260 -0.00726 -0.00331 AFIX 23 H23A 2 0.727232 0.645457 0.981391 11.00000 -1.20000 H23B 2 0.890874 0.590812 0.931208 11.00000 -1.20000 AFIX 0 C14 1 0.781354 0.790584 0.854294 11.00000 0.01680 0.01821 = 0.01313 -0.00402 -0.00155 -0.00376 C13 1 0.690015 0.734026 0.780388 11.00000 0.01499 0.01417 = 0.01215 -0.00211 -0.00084 0.00004 C9 1 0.635107 0.732832 0.610865 11.00000 0.01476 0.01427 = 0.01107 -0.00236 -0.00133 -0.00059 C8 1 0.635083 0.765527 0.504127 11.00000 0.01750 0.01511 = 0.01153 -0.00175 0.00057 -0.00053 C10 1 0.753828 0.830695 0.432126 11.00000 0.02121 0.01827 = 0.01270 -0.00219 0.00224 -0.00321 AFIX 13 H10 2 0.829639 0.863868 0.474149 11.00000 -1.20000 AFIX 0 C11 1 0.680308 0.963444 0.357034 11.00000 0.03248 0.02453 = 0.02119 0.00507 -0.00052 -0.00496 AFIX 137 H11A 2 0.605911 0.933697 0.314415 11.00000 -1.50000 H11B 2 0.761442 1.003131 0.313899 11.00000 -1.50000 H11C 2 0.626611 1.038301 0.394823 11.00000 -1.50000 AFIX 0 C12 1 0.843782 0.713211 0.374873 11.00000 0.02674 0.02838 = 0.02613 -0.01095 0.01031 -0.00623 AFIX 137 H12A 2 0.888423 0.628756 0.423964 11.00000 -1.50000 H12B 2 0.927082 0.753264 0.334247 11.00000 -1.50000 H12C 2 0.773103 0.682822 0.329962 11.00000 -1.50000 AFIX 0 C1 1 0.621772 0.464463 0.832784 11.00000 0.02293 0.01667 = 0.01235 -0.00093 -0.00182 -0.00371 AFIX 13 H1 2 0.648043 0.461016 0.905658 11.00000 -1.20000 AFIX 0 C3 1 0.768389 0.403261 0.778043 11.00000 0.02600 0.01784 = 0.01978 -0.00251 -0.00417 0.00088 AFIX 137 H3A 2 0.803735 0.301989 0.809185 11.00000 -1.50000 H3B 2 0.849691 0.461976 0.783726 11.00000 -1.50000 H3C 2 0.745728 0.406586 0.706125 11.00000 -1.50000 AFIX 0 C2 1 0.499626 0.365697 0.829237 11.00000 0.03136 0.01826 = 0.02112 -0.00138 -0.00210 -0.00796 AFIX 137 H2A 2 0.478041 0.361158 0.758256 11.00000 -1.50000 H2B 2 0.404145 0.405338 0.862631 11.00000 -1.50000 H2C 2 0.538516 0.267381 0.864552 11.00000 -1.50000 AFIX 0 C4 1 0.521439 0.660779 0.666445 11.00000 0.01480 0.01372 = 0.01216 -0.00183 -0.00059 -0.00081 C5 1 0.402782 0.623252 0.615195 11.00000 0.01636 0.01616 = 0.01479 -0.00272 -0.00128 -0.00173 AFIX 43 H5 2 0.326959 0.573266 0.651822 11.00000 -1.20000 AFIX 0 C6 1 0.394864 0.659025 0.509660 11.00000 0.01869 0.02090 = 0.01490 -0.00443 -0.00407 -0.00189 AFIX 43 H6 2 0.311718 0.636645 0.474169 11.00000 -1.20000 AFIX 0 C7 1 0.508835 0.727287 0.457019 11.00000 0.02117 0.02002 = 0.01131 -0.00296 -0.00174 -0.00125 AFIX 43 H7 2 0.501829 0.749752 0.385051 11.00000 -1.20000 AFIX 0 C20 1 0.762748 0.990742 0.965058 11.00000 0.02616 0.02443 = 0.02193 -0.01103 0.00004 -0.00758 AFIX 23 H20A 2 0.857048 1.025335 0.933551 11.00000 -1.20000 H20B 2 0.693649 1.075492 0.985815 11.00000 -1.20000 AFIX 0 C19 1 0.679997 0.927852 0.886960 11.00000 0.01969 0.01963 = 0.01840 -0.00675 -0.00091 -0.00263 AFIX 23 H19A 2 0.655497 1.003255 0.826270 11.00000 -1.20000 H19B 2 0.581083 0.901261 0.916566 11.00000 -1.20000 AFIX 0 C15 1 0.923809 0.827863 0.790129 11.00000 0.01587 0.02956 = 0.01773 -0.00626 -0.00151 -0.00609 AFIX 23 H15A 2 1.013950 0.750033 0.807148 11.00000 -1.20000 H15B 2 0.951016 0.921072 0.803770 11.00000 -1.20000 AFIX 0 C16 1 0.880514 0.840923 0.676760 11.00000 0.01443 0.02018 = 0.01671 -0.00401 0.00104 -0.00521 C17 1 1.011489 0.751363 0.623885 11.00000 0.01650 0.02774 = 0.02112 -0.00565 0.00277 -0.00114 AFIX 137 H17A 2 1.022286 0.648682 0.655509 11.00000 -1.50000 H17B 2 1.108770 0.788006 0.630584 11.00000 -1.50000 H17C 2 0.987329 0.760018 0.551684 11.00000 -1.50000 AFIX 0 C18 1 0.841900 1.001627 0.627266 11.00000 0.02503 0.01859 = 0.02227 -0.00326 0.00315 -0.00767 AFIX 137 H18A 2 0.787870 1.008093 0.563098 11.00000 -1.50000 H18B 2 0.937989 1.042851 0.613896 11.00000 -1.50000 H18C 2 0.775211 1.056444 0.673231 11.00000 -1.50000 AFIX 0 B1 3 0.556668 0.634230 0.785284 11.00000 0.01638 0.01704 = 0.01107 -0.00247 -0.00022 -0.00364 HKLF 4 REM mo_P8_23112_0m_a.res in P-1 REM R1 = 0.0242 for 6289 Fo > 4sig(Fo) and 0.0283 for all 6941 data REM 241 parameters refined using 0 restraints END WGHT 0.0387 0.2177 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 0.682, deepest hole -0.462, 1-sigma level 0.063 Q1 1 0.4240 0.6465 0.8510 11.00000 0.05 0.68 Q2 1 0.3139 0.7829 0.8797 11.00000 0.05 0.67 Q3 1 0.6948 0.4280 0.7986 11.00000 0.05 0.57 Q4 1 0.5689 0.7049 0.6385 11.00000 0.05 0.54 Q5 1 0.3058 0.6676 0.8770 11.00000 0.05 0.52 Q6 1 0.7334 0.8556 0.8681 11.00000 0.05 0.49 ; _shelx_res_checksum 15613 _shelx_hkl_file ; -1 0 0 1934.41 94.19 -1 0 0 2159.98 94.19 -1 0 0 2335.07 94.19 -1 0 0 1993.10 94.29 -1 0 0 1959.70 94.19 -1 0 0 1939.81 94.19 -1 0 0 2150.08 94.19 -1 0 0 1976.10 94.19 -1 0 0 2207.78 94.29 1 0 0 2074.69 94.19 1 0 0 1902.01 94.19 1 0 0 2110.59 94.19 1 0 0 2099.49 94.19 1 0 0 2377.46 94.19 1 0 0 2176.58 94.29 1 0 0 1912.91 94.19 -2 0 0 686.83 27.80 -2 0 0 583.74 27.90 -2 0 0 561.34 27.80 -2 0 0 579.34 27.80 -2 0 0 574.74 27.80 -2 0 0 630.94 27.80 -2 0 0 654.63 27.80 2 0 0 621.64 27.80 2 0 0 625.64 27.80 2 0 0 545.85 27.80 2 0 0 676.73 27.80 2 0 0 606.54 27.80 2 0 0 702.73 27.90 2 0 0 575.04 27.80 2 0 0 592.84 27.90 2 0 0 573.94 27.80 -3 0 0 464.05 21.70 -3 0 0 483.25 21.70 -3 0 0 444.36 21.80 -3 0 0 492.25 21.80 -3 0 0 430.96 21.80 -3 0 0 468.15 21.60 -3 0 0 493.35 21.70 3 0 0 469.65 21.70 3 0 0 464.45 21.70 3 0 0 507.45 21.80 3 0 0 413.56 21.60 3 0 0 483.55 21.70 3 0 0 465.75 21.80 3 0 0 498.45 21.80 3 0 0 462.95 21.70 3 0 0 471.65 21.80 3 0 0 529.05 21.80 3 0 0 523.75 21.80 3 0 0 493.85 21.70 -4 0 0 787.02 36.00 -4 0 0 767.32 35.90 -4 0 0 802.52 35.90 -4 0 0 788.72 36.00 -4 0 0 740.93 36.10 -4 0 0 799.32 36.00 4 0 0 817.52 36.00 4 0 0 777.62 35.90 4 0 0 813.92 36.00 4 0 0 837.92 36.00 4 0 0 772.92 36.10 4 0 0 815.22 36.10 4 0 0 755.32 35.90 4 0 0 856.71 36.10 4 0 0 747.63 35.90 4 0 0 762.42 35.80 4 0 0 788.22 35.90 -5 0 0 171.78 8.40 -5 0 0 183.58 8.30 -5 0 0 173.88 8.60 -5 0 0 170.58 8.50 5 0 0 160.88 8.20 5 0 0 166.48 8.50 5 0 0 186.18 8.70 5 0 0 168.08 8.30 5 0 0 177.78 8.80 5 0 0 163.98 8.20 5 0 0 192.28 8.80 5 0 0 196.18 8.50 5 0 0 177.98 8.40 5 0 0 193.68 8.80 5 0 0 169.78 8.30 -6 0 0 140.09 6.80 -6 0 0 137.99 6.90 6 0 0 126.99 6.80 6 0 0 137.09 6.60 6 0 0 138.09 7.00 6 0 0 124.99 7.00 6 0 0 137.49 7.20 6 0 0 154.38 7.00 6 0 0 142.09 7.00 6 0 0 133.69 6.60 6 0 0 134.99 6.80 6 0 0 157.18 7.80 -7 0 0 597.44 28.30 -7 0 0 605.84 28.20 -7 0 0 584.84 28.40 -7 0 0 646.34 28.70 7 0 0 608.44 28.50 7 0 0 705.53 28.90 7 0 0 640.64 28.30 7 0 0 592.74 28.40 7 0 0 585.24 28.00 7 0 0 579.14 28.00 7 0 0 620.64 28.40 -8 0 0 543.45 24.90 -8 0 0 528.75 24.30 -8 0 0 498.15 24.50 -8 0 0 540.35 24.10 8 0 0 519.15 24.40 8 0 0 508.35 23.90 8 0 0 532.75 24.00 8 0 0 542.65 24.30 8 0 0 492.65 24.50 -9 0 0 24.50 3.60 -9 0 0 28.40 3.30 -9 0 0 27.70 2.80 -9 0 0 25.60 4.00 9 0 0 23.10 3.20 9 0 0 25.30 2.90 9 0 0 25.40 3.40 -10 0 0 19.90 3.20 -10 0 0 24.70 4.80 -10 0 0 27.10 6.70 -10 0 0 19.60 4.10 10 0 0 22.40 3.70 10 0 0 17.00 4.00 -11 0 0 79.49 8.00 -11 0 0 80.59 8.20 -11 0 0 78.29 7.00 -11 0 0 91.39 10.90 11 0 0 67.39 8.70 11 0 0 88.69 8.10 -12 0 0 13.40 5.50 -12 0 0 8.90 4.50 -12 0 0 15.50 10.90 12 0 0 8.50 6.00 12 0 0 20.10 5.40 12 -1 0 9.10 10.00 12 -1 0 -0.40 6.00 12 -1 0 4.60 5.60 -12 1 0 -0.60 7.20 -12 1 0 -1.10 5.60 -12 1 0 4.40 4.40 11 -1 0 31.00 5.50 11 -1 0 39.10 4.80 11 -1 0 20.30 4.70 11 -1 0 33.00 3.30 11 -1 0 34.00 3.70 -11 1 0 29.10 5.00 -11 1 0 37.10 5.40 -11 1 0 40.50 4.30 -11 1 0 41.80 6.20 10 -1 0 25.70 2.70 10 -1 0 16.30 3.60 10 -1 0 25.10 4.00 10 -1 0 16.10 5.00 -10 1 0 24.30 4.90 -10 1 0 23.60 3.20 -10 1 0 21.20 4.10 -10 1 0 27.60 4.40 9 -1 0 49.40 5.30 9 -1 0 43.00 5.50 9 -1 0 44.10 5.10 9 -1 0 38.50 5.10 9 -1 0 39.50 3.70 9 -1 0 45.60 4.30 -9 1 0 42.00 5.60 -9 1 0 43.20 4.40 -9 1 0 43.10 4.00 -9 1 0 47.70 6.60 8 -1 0 49.90 4.50 8 -1 0 71.19 9.60 8 -1 0 48.00 4.80 8 -1 0 40.10 4.60 8 -1 0 45.50 4.40 8 -1 0 48.30 4.90 8 -1 0 48.20 3.40 -8 1 0 52.09 5.50 -8 1 0 40.10 4.50 -8 1 0 53.89 4.80 -8 1 0 46.00 3.80 -8 1 0 50.29 5.30 7 -1 0 205.58 10.60 7 -1 0 208.88 10.00 7 -1 0 218.88 10.60 7 -1 0 216.28 10.50 7 -1 0 212.18 10.60 7 -1 0 221.98 10.60 7 -1 0 225.08 10.30 7 -1 0 233.68 11.40 7 -1 0 207.08 10.10 -7 1 0 217.58 10.50 -7 1 0 211.78 10.20 -7 1 0 195.08 10.60 -7 1 0 215.68 11.00 -7 1 0 206.88 10.30 6 -1 0 731.53 31.80 6 -1 0 709.13 31.80 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115.49 9.20 11 5 0 135.99 8.60 11 5 0 101.09 8.40 11 5 0 119.39 9.10 -12 -5 0 156.08 11.40 12 5 0 154.98 10.50 12 5 0 142.39 9.90 12 5 0 135.29 11.10 10 -6 0 39.30 5.80 10 -6 0 33.50 5.10 10 -6 0 32.10 7.10 10 -6 0 41.00 6.80 10 -6 0 33.40 6.70 -10 6 0 42.20 6.10 -10 6 0 43.80 7.50 9 -6 0 89.79 7.10 9 -6 0 65.59 9.10 9 -6 0 62.79 6.20 9 -6 0 76.59 9.90 9 -6 0 60.99 6.70 9 -6 0 44.60 5.60 -9 6 0 64.79 8.00 -9 6 0 76.29 7.70 8 -6 0 111.59 9.60 8 -6 0 111.09 8.60 8 -6 0 122.89 9.50 8 -6 0 106.09 7.40 8 -6 0 93.29 8.70 8 -6 0 100.39 8.30 -8 6 0 102.89 8.10 -8 6 0 112.19 9.50 -8 6 0 115.39 9.50 7 -6 0 -1.10 4.00 7 -6 0 2.90 3.60 7 -6 0 2.80 3.70 7 -6 0 5.20 4.00 7 -6 0 6.50 3.50 7 -6 0 3.90 3.20 -7 6 0 2.10 4.20 -7 6 0 4.10 2.80 -7 6 0 3.10 3.10 -7 6 0 1.60 3.80 6 -6 0 66.99 5.20 6 -6 0 65.99 6.90 6 -6 0 71.39 5.80 6 -6 0 59.39 5.80 6 -6 0 63.69 6.10 6 -6 0 69.79 5.50 6 -6 0 79.99 6.70 -6 6 0 73.29 6.50 -6 6 0 71.59 4.60 -6 6 0 68.29 5.50 -6 6 0 71.89 5.50 -6 6 0 84.59 5.30 -6 6 0 71.09 5.50 5 -6 0 108.29 7.40 5 -6 0 100.09 6.70 5 -6 0 115.09 6.50 5 -6 0 108.79 6.60 5 -6 0 98.69 7.50 5 -6 0 117.89 7.40 5 -6 0 103.69 6.80 5 -6 0 113.59 7.10 -5 6 0 120.79 6.60 -5 6 0 118.39 6.30 -5 6 0 116.79 6.40 -5 6 0 127.89 7.30 -5 6 0 112.59 5.90 -5 6 0 104.19 6.40 4 -6 0 80.99 5.50 4 -6 0 80.09 5.30 4 -6 0 78.59 5.10 4 -6 0 75.19 6.00 4 -6 0 73.59 5.70 4 -6 0 77.99 5.10 4 -6 0 82.09 5.00 -4 6 0 79.99 5.00 -4 6 0 72.39 7.40 -4 6 0 78.89 4.40 -4 6 0 83.39 4.70 -4 6 0 76.29 4.90 -4 6 0 73.99 4.70 3 -6 0 81.09 4.90 3 -6 0 74.49 5.00 3 -6 0 81.89 5.00 3 -6 0 87.79 4.90 3 -6 0 80.39 5.20 3 -6 0 76.59 5.70 3 -6 0 84.29 5.50 -3 6 0 75.19 4.70 -3 6 0 88.19 4.50 -3 6 0 88.89 4.60 -3 6 0 77.89 4.80 -3 6 0 78.99 5.30 -3 6 0 69.19 4.40 2 -6 0 687.13 28.30 2 -6 0 572.84 28.40 2 -6 0 587.24 28.30 2 -6 0 571.14 28.70 2 -6 0 607.94 28.30 2 -6 0 633.04 28.30 2 -6 0 620.94 28.60 2 -6 0 625.84 28.20 -2 6 0 636.24 28.20 -2 6 0 638.74 28.30 -2 6 0 602.84 28.40 -2 6 0 613.64 28.30 -2 6 0 614.44 28.20 -2 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67.79 6.20 10 6 0 48.50 6.30 -11 -6 0 10.80 6.60 -11 -6 0 15.80 4.70 11 6 0 7.50 4.30 11 6 0 7.80 4.20 11 6 0 12.80 5.20 -12 -6 0 14.40 6.00 -12 -6 0 10.30 8.00 12 6 0 8.30 5.50 12 6 0 12.10 5.40 12 6 0 23.10 5.30 9 -7 0 4.10 4.90 9 -7 0 -0.90 6.90 9 -7 0 7.60 8.90 9 -7 0 8.40 6.20 9 -7 0 3.90 4.40 9 -7 0 8.80 5.90 -9 7 0 10.00 9.90 -9 7 0 4.00 5.50 -9 7 0 3.00 7.80 8 -7 0 77.19 10.00 8 -7 0 77.59 8.20 8 -7 0 82.49 6.60 8 -7 0 76.09 6.90 8 -7 0 64.99 9.00 8 -7 0 77.89 7.30 -8 7 0 75.99 8.00 -8 7 0 74.19 7.20 -8 7 0 78.19 10.10 -8 7 0 67.39 9.70 7 -7 0 64.49 6.20 7 -7 0 64.89 7.90 7 -7 0 72.69 6.50 7 -7 0 64.39 7.70 7 -7 0 73.89 7.20 7 -7 0 75.89 8.30 -7 7 0 81.19 6.70 -7 7 0 81.69 8.60 -7 7 0 95.09 6.80 -7 7 0 75.59 5.50 -7 7 0 72.39 6.80 6 -7 0 31.40 3.80 6 -7 0 26.40 4.40 6 -7 0 32.20 4.70 6 -7 0 25.80 3.50 6 -7 0 28.30 4.90 6 -7 0 22.90 3.90 -6 7 0 24.70 3.40 -6 7 0 21.30 3.20 -6 7 0 28.50 4.50 -6 7 0 23.90 2.80 -6 7 0 34.90 3.80 5 -7 0 101.69 7.50 5 -7 0 89.79 8.00 5 -7 0 120.79 7.10 5 -7 0 98.99 7.10 5 -7 0 111.59 6.80 5 -7 0 124.19 8.10 -5 7 0 118.99 6.90 -5 7 0 112.89 6.70 -5 7 0 105.09 7.70 -5 7 0 90.69 6.50 -5 7 0 123.99 6.50 4 -7 0 373.26 18.60 4 -7 0 376.96 18.90 4 -7 0 402.96 18.80 4 -7 0 362.06 18.60 4 -7 0 400.26 18.60 4 -7 0 420.16 19.90 -4 7 0 378.96 18.50 -4 7 0 389.66 18.90 -4 7 0 409.06 18.40 -4 7 0 408.96 18.50 3 -7 0 31.40 3.80 3 -7 0 30.10 3.40 3 -7 0 38.20 3.80 3 -7 0 33.40 3.80 3 -7 0 26.50 3.20 3 -7 0 29.70 3.00 -3 7 0 27.60 3.20 -3 7 0 35.90 3.80 -3 7 0 33.10 3.40 -3 7 0 29.80 3.40 2 -7 0 0.60 2.40 2 -7 0 1.40 2.30 2 -7 0 -0.40 1.90 2 -7 0 -2.00 2.10 2 -7 0 1.60 1.70 2 -7 0 2.00 2.80 -2 7 0 -0.90 1.70 -2 7 0 0.60 2.30 -2 7 0 1.90 2.70 -2 7 0 1.90 1.70 -2 7 0 -1.20 1.50 1 -7 0 20.60 2.20 1 -7 0 15.50 3.10 1 -7 0 15.40 1.80 1 -7 0 20.20 2.20 1 -7 0 22.00 2.30 1 -7 0 14.80 2.60 -1 7 0 9.20 2.40 -1 7 0 17.00 2.10 -1 7 0 13.20 1.80 -1 7 0 14.30 1.90 -1 7 0 17.90 2.60 -1 7 0 17.60 2.40 -1 7 0 20.40 1.90 0 -7 0 410.86 18.60 0 -7 0 418.76 18.80 0 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233.28 11.70 3 7 0 261.77 12.10 3 7 0 254.17 11.50 3 7 0 227.18 11.30 3 7 0 245.58 11.60 3 7 0 246.38 11.70 -4 -7 0 399.96 20.10 -4 -7 0 460.65 20.10 -4 -7 0 406.36 19.50 -4 -7 0 424.06 19.70 -4 -7 0 420.86 19.70 4 7 0 420.96 19.70 4 7 0 435.36 20.00 4 7 0 423.26 19.60 4 7 0 395.66 19.60 4 7 0 423.26 19.60 4 7 0 416.26 19.70 4 7 0 449.06 19.70 4 7 0 415.16 19.40 -5 -7 0 -0.40 2.80 -5 -7 0 5.30 1.70 -5 -7 0 1.90 2.60 -5 -7 0 2.20 2.60 -5 -7 0 2.80 2.30 -5 -7 0 1.10 2.40 5 7 0 2.80 4.50 5 7 0 1.70 2.40 5 7 0 2.70 2.10 5 7 0 2.60 1.90 5 7 0 2.10 2.00 5 7 0 2.00 1.80 5 7 0 -0.10 1.90 5 7 0 3.00 3.20 5 7 0 -4.30 2.60 -6 -7 0 103.79 6.50 -6 -7 0 100.99 6.40 -6 -7 0 109.89 6.90 -6 -7 0 93.69 7.10 6 7 0 104.39 7.40 6 7 0 106.29 6.20 6 7 0 90.79 6.40 6 7 0 99.59 5.80 -7 -7 0 233.58 11.40 -7 -7 0 190.28 11.60 -7 -7 0 216.58 10.90 -7 -7 0 200.98 10.90 7 7 0 195.28 11.30 7 7 0 223.38 10.60 7 7 0 200.68 11.70 7 7 0 225.08 10.90 -8 -7 0 181.88 10.20 -8 -7 0 167.98 9.30 -8 -7 0 168.48 11.60 -8 -7 0 174.58 12.30 8 7 0 172.58 9.40 8 7 0 179.58 9.20 8 7 0 143.89 10.90 -9 -7 0 4.10 4.40 -9 -7 0 7.20 5.00 -9 -7 0 4.40 3.60 9 7 0 7.80 3.40 9 7 0 8.40 3.20 -10 -7 0 159.58 12.20 -10 -7 0 138.39 11.40 -10 -7 0 147.49 10.90 10 7 0 164.18 9.40 10 7 0 160.58 9.80 -11 -7 0 110.09 13.10 -11 -7 0 133.69 10.20 -11 -7 0 99.69 11.60 11 7 0 122.09 9.30 11 7 0 121.09 9.10 8 -8 0 36.60 7.50 8 -8 0 39.20 6.50 8 -8 0 50.39 6.40 8 -8 0 37.70 6.20 8 -8 0 44.20 5.60 8 -8 0 48.60 5.70 -8 8 0 35.50 5.00 -8 8 0 33.30 7.70 -8 8 0 37.10 6.70 -8 8 0 35.70 5.80 7 -8 0 18.30 5.30 7 -8 0 14.80 6.00 7 -8 0 18.70 4.10 7 -8 0 15.80 4.30 7 -8 0 14.10 5.00 7 -8 0 20.40 5.10 -7 8 0 15.90 5.90 -7 8 0 23.50 4.20 -7 8 0 19.80 4.00 -7 8 0 16.10 3.30 -7 8 0 15.40 4.40 6 -8 0 113.99 9.60 6 -8 0 102.59 8.10 6 -8 0 107.99 8.90 6 -8 0 105.79 9.00 6 -8 0 104.49 7.80 6 -8 0 100.19 8.60 -6 8 0 118.69 6.90 -6 8 0 118.19 9.40 -6 8 0 117.79 7.60 -6 8 0 98.29 7.80 5 -8 0 29.10 3.90 5 -8 0 45.10 4.20 5 -8 0 32.20 3.70 5 -8 0 26.20 5.30 5 -8 0 38.50 5.10 5 -8 0 32.40 4.60 -5 8 0 34.40 4.30 -5 8 0 26.00 4.70 -5 8 0 33.30 3.70 -5 8 0 26.50 3.60 4 -8 0 36.40 4.10 4 -8 0 27.70 3.40 4 -8 0 36.90 4.00 4 -8 0 33.20 4.80 4 -8 0 43.50 4.90 4 -8 0 40.70 3.90 -4 8 0 35.80 4.30 -4 8 0 31.50 4.30 -4 8 0 25.40 3.40 -4 8 0 36.80 3.90 -4 8 0 30.80 3.40 3 -8 0 20.30 3.60 3 -8 0 24.10 2.90 3 -8 0 28.40 3.50 3 -8 0 23.90 3.30 3 -8 0 23.30 3.30 3 -8 0 36.20 4.30 -3 8 0 27.00 3.50 -3 8 0 32.40 3.70 -3 8 0 26.40 3.70 -3 8 0 32.30 3.80 -3 8 0 26.60 2.60 -3 8 0 23.10 3.10 2 -8 0 304.07 14.90 2 -8 0 280.27 15.40 2 -8 0 345.87 15.30 2 -8 0 316.07 15.20 2 -8 0 313.57 15.70 2 -8 0 303.07 15.20 -2 8 0 312.47 14.90 -2 8 0 319.47 15.50 -2 8 0 335.27 14.90 -2 8 0 316.17 15.10 -2 8 0 287.77 15.10 -2 8 0 331.67 14.90 1 -8 0 96.39 5.80 1 -8 0 104.09 6.40 1 -8 0 123.89 6.70 1 -8 0 110.19 6.90 1 -8 0 99.39 6.50 1 -8 0 114.19 7.20 1 -8 0 103.59 6.80 -1 8 0 110.39 6.70 -1 8 0 103.49 6.80 -1 8 0 107.19 6.30 -1 8 0 97.09 5.80 -1 8 0 105.39 5.90 -1 8 0 115.39 6.00 -1 8 0 104.19 6.90 0 -8 0 38.10 4.10 0 -8 0 38.30 3.60 0 -8 0 42.00 5.70 0 -8 0 42.10 4.80 0 -8 0 44.20 4.40 0 -8 0 35.30 4.20 0 8 0 35.70 3.30 0 8 0 34.10 3.40 0 8 0 39.30 4.70 0 8 0 39.90 3.80 0 8 0 40.40 3.40 0 8 0 40.10 3.90 -1 -8 0 97.79 6.10 -1 -8 0 80.69 5.30 -1 -8 0 78.49 5.80 -1 -8 0 84.89 6.10 -1 -8 0 82.99 5.20 -1 -8 0 88.49 5.50 1 8 0 80.19 4.60 1 8 0 68.59 5.10 1 8 0 79.79 4.80 1 8 0 80.09 5.40 1 8 0 78.79 6.20 1 8 0 73.69 5.60 1 8 0 88.59 5.10 1 8 0 74.49 7.30 -2 -8 0 141.49 7.20 -2 -8 0 142.69 8.10 -2 -8 0 146.19 8.10 -2 -8 0 133.19 7.80 -2 -8 0 133.09 7.40 -2 -8 0 136.99 8.10 -2 -8 0 152.38 7.60 2 8 0 131.79 6.90 2 8 0 138.19 8.80 2 8 0 139.59 7.50 2 8 0 139.99 7.70 2 8 0 148.19 7.40 2 8 0 141.69 7.20 2 8 0 123.79 7.50 2 8 0 138.59 7.40 -3 -8 0 1.80 2.50 -3 -8 0 7.70 2.70 -3 -8 0 4.20 2.70 -3 -8 0 7.50 3.00 -3 -8 0 5.20 3.10 3 8 0 3.30 2.40 3 8 0 7.20 2.00 3 8 0 3.00 1.80 3 8 0 3.60 3.40 3 8 0 5.80 2.10 3 8 0 9.00 1.50 -4 -8 0 28.40 3.60 -4 -8 0 24.50 3.90 -4 -8 0 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261.37 15.00 10 5 -3 91.49 7.40 10 5 -3 85.09 7.40 10 5 -3 102.99 7.30 -10 -5 3 82.69 7.40 -10 -5 3 83.29 9.60 9 5 -3 13.50 3.30 9 5 -3 16.70 3.30 9 5 -3 11.80 3.00 -9 -5 3 16.60 4.70 -9 -5 3 13.40 3.20 8 5 -3 184.48 10.10 8 5 -3 201.58 10.20 8 5 -3 189.98 10.30 -8 -5 3 216.08 12.00 -8 -5 3 194.88 11.10 -8 -5 3 206.98 10.60 -8 -5 3 201.38 10.30 7 5 -3 57.19 4.50 7 5 -3 59.69 4.40 -7 -5 3 51.59 4.70 -7 -5 3 55.29 6.80 -7 -5 3 61.79 5.20 -7 -5 3 56.19 5.60 6 5 -3 39.70 3.70 -6 -5 3 52.29 4.60 -6 -5 3 47.40 4.00 -6 -5 3 38.00 4.80 -6 -5 3 45.20 4.10 5 5 -3 -1.20 1.50 5 5 -3 0.80 2.80 5 5 -3 -1.50 1.60 5 5 -3 1.60 2.40 5 5 -3 1.70 1.90 5 5 -3 0.70 2.20 5 5 -3 -0.10 1.70 -5 -5 3 0.00 2.30 -5 -5 3 3.40 2.40 -5 -5 3 -1.70 1.40 -5 -5 3 -1.90 5.60 -5 -5 3 0.30 1.90 -5 -5 3 1.30 1.80 -5 -5 3 -0.50 1.90 4 5 -3 639.64 29.10 4 5 -3 683.13 29.20 4 5 -3 639.34 29.10 4 5 -3 643.34 29.10 4 5 -3 625.64 29.10 -4 -5 3 625.94 29.20 -4 -5 3 599.64 29.40 -4 -5 3 671.53 29.50 -4 -5 3 656.53 29.10 -4 -5 3 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9 4 -4 83.39 6.40 9 4 -4 73.69 6.20 -9 -4 4 81.99 7.90 -9 -4 4 89.29 8.80 -9 -4 4 79.89 6.40 8 4 -4 44.50 4.60 8 4 -4 39.90 4.80 -8 -4 4 57.19 5.30 -8 -4 4 42.60 5.90 -8 -4 4 38.70 4.80 -8 -4 4 44.80 6.90 7 4 -4 205.28 10.00 7 4 -4 196.68 9.40 7 4 -4 193.28 9.90 -7 -4 4 196.18 10.00 -7 -4 4 182.28 10.50 -7 -4 4 202.08 11.00 -7 -4 4 217.08 11.20 6 4 -4 252.77 12.00 6 4 -4 270.37 12.10 6 4 -4 245.18 12.00 6 4 -4 256.57 11.80 6 4 -4 239.68 12.00 6 4 -4 275.87 12.80 -6 -4 4 248.98 12.60 -6 -4 4 222.18 12.60 -6 -4 4 262.57 12.80 -6 -4 4 251.17 12.10 -6 -4 4 247.88 12.10 5 4 -4 7.80 1.50 5 4 -4 5.40 1.60 5 4 -4 8.80 1.80 5 4 -4 8.60 1.60 5 4 -4 6.10 1.20 5 4 -4 9.60 2.00 5 4 -4 7.30 1.90 -5 -4 4 8.80 2.30 -5 -4 4 4.80 1.80 -5 -4 4 7.20 1.80 -5 -4 4 7.80 2.50 -5 -4 4 9.20 1.50 -5 -4 4 11.40 1.90 -5 -4 4 5.10 2.80 -5 -4 4 8.00 1.80 4 4 -4 338.37 15.90 4 4 -4 342.77 15.90 4 4 -4 306.97 15.40 4 4 -4 347.57 15.60 4 4 -4 354.16 15.80 4 4 -4 326.27 15.50 4 4 -4 334.57 15.60 4 4 -4 338.37 15.60 -4 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4 -4 3.20 1.10 -2 4 -4 3.20 1.40 -2 4 -4 4.10 1.80 -2 4 -4 4.40 2.20 -2 4 -4 4.20 2.00 2 -4 4 3.80 2.10 2 -4 4 4.40 1.50 2 -4 4 4.90 1.50 2 -4 4 5.60 2.40 2 -4 4 4.10 1.70 2 -4 4 4.00 1.60 2 -4 4 0.90 1.70 2 -4 4 2.90 1.30 2 -4 4 4.10 1.50 -3 4 -4 118.99 6.50 -3 4 -4 120.29 6.40 -3 4 -4 125.19 6.10 -3 4 -4 117.79 5.90 -3 4 -4 122.09 6.10 -3 4 -4 115.49 5.70 -3 4 -4 118.39 6.10 -3 4 -4 106.09 6.80 3 -4 4 106.09 6.20 3 -4 4 122.39 6.10 3 -4 4 108.39 6.50 3 -4 4 126.39 6.60 3 -4 4 119.29 6.30 3 -4 4 107.79 6.60 3 -4 4 128.39 6.30 -4 4 -4 445.86 19.20 -4 4 -4 424.76 19.40 -4 4 -4 390.16 19.30 -4 4 -4 419.36 19.30 -4 4 -4 421.56 19.50 4 -4 4 435.16 19.40 4 -4 4 385.96 19.30 4 -4 4 409.96 19.40 4 -4 4 414.36 19.30 4 -4 4 424.96 19.30 4 -4 4 411.86 19.50 4 -4 4 408.16 19.60 -5 4 -4 638.24 28.00 -5 4 -4 631.04 28.00 -5 4 -4 605.24 27.90 -5 4 -4 578.64 28.00 -5 4 -4 615.74 28.10 -5 4 -4 642.64 28.20 5 -4 4 619.94 28.30 5 -4 4 575.34 28.00 5 -4 4 597.24 27.90 5 -4 4 621.04 28.10 5 -4 4 563.14 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13.40 6.30 12 3 -4 7.50 5.50 12 3 -4 9.40 5.20 12 3 -4 9.20 5.40 -12 -3 4 7.20 8.30 11 3 -4 5.50 4.50 11 3 -4 8.50 4.10 -11 -3 4 5.90 4.20 -11 -3 4 8.10 6.50 -11 -3 4 9.50 6.20 10 3 -4 33.80 4.10 10 3 -4 30.80 4.20 -10 -3 4 37.70 4.20 -10 -3 4 41.50 6.20 -10 -3 4 38.60 5.30 9 3 -4 289.97 14.90 9 3 -4 310.57 14.80 -9 -3 4 285.97 14.80 -9 -3 4 325.17 20.30 -9 -3 4 299.07 15.60 8 3 -4 185.08 9.60 8 3 -4 185.98 9.50 -8 -3 4 175.38 10.30 -8 -3 4 201.38 10.90 -8 -3 4 188.08 10.90 -8 -3 4 180.48 9.50 7 3 -4 23.60 2.50 7 3 -4 21.90 2.30 -7 -3 4 31.30 4.30 -7 -3 4 19.60 3.60 -7 -3 4 17.40 2.40 6 3 -4 73.69 4.40 6 3 -4 74.09 4.50 6 3 -4 79.69 5.70 6 3 -4 66.49 4.50 6 3 -4 76.49 4.00 -6 -3 4 78.59 4.60 -6 -3 4 79.79 5.60 -6 -3 4 75.79 5.30 -6 -3 4 82.09 5.70 5 3 -4 492.05 22.60 5 3 -4 472.25 22.80 5 3 -4 483.85 22.60 5 3 -4 486.45 22.80 5 3 -4 496.05 22.50 5 3 -4 479.75 22.60 5 3 -4 496.25 22.60 5 3 -4 498.15 22.60 5 3 -4 477.45 22.70 5 3 -4 477.65 22.80 -5 -3 4 515.95 22.90 -5 -3 4 477.15 22.90 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3 -4 3.20 3.50 -9 3 -4 6.40 3.90 9 -3 4 -1.20 3.40 9 -3 4 1.40 3.60 9 -3 4 2.00 4.10 9 -3 4 2.90 2.60 9 -3 4 2.40 3.90 9 -3 4 0.50 3.60 -10 3 -4 207.98 11.80 -10 3 -4 215.88 13.70 -10 3 -4 196.58 11.90 10 -3 4 178.28 12.00 10 -3 4 210.98 12.50 10 -3 4 201.98 11.90 10 -3 4 186.38 10.50 10 -3 4 164.38 11.70 -11 3 -4 88.99 13.50 -11 3 -4 65.89 7.30 -11 3 -4 77.69 7.50 11 -3 4 74.19 9.70 11 -3 4 87.79 9.90 11 -3 4 92.79 10.80 11 -3 4 66.89 7.00 12 2 -4 47.10 5.80 12 2 -4 34.80 6.30 -12 -2 4 59.69 5.90 -12 -2 4 53.49 8.70 11 2 -4 109.89 8.40 11 2 -4 105.29 9.30 -11 -2 4 121.99 11.90 -11 -2 4 103.99 8.40 10 2 -4 59.79 6.80 -10 -2 4 71.79 9.00 -10 -2 4 61.19 6.20 -10 -2 4 73.29 8.20 9 2 -4 2.70 2.80 -9 -2 4 1.10 2.60 -9 -2 4 -1.50 3.90 -9 -2 4 2.10 3.80 8 2 -4 255.57 13.30 8 2 -4 279.27 12.80 -8 -2 4 282.77 14.40 -8 -2 4 262.77 13.20 -8 -2 4 281.07 13.80 7 2 -4 69.99 4.10 7 2 -4 76.59 4.90 7 2 -4 76.29 6.00 -7 -2 4 72.99 6.10 -7 -2 4 80.89 4.70 -7 -2 4 71.89 5.30 -7 -2 4 64.19 5.90 6 2 -4 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109.89 5.10 0 -2 4 100.89 5.10 0 -2 4 111.39 5.20 0 -2 4 103.69 5.30 0 -2 4 109.99 5.40 0 -2 4 107.49 5.30 0 -2 4 111.79 5.00 0 -2 4 101.39 5.20 0 -2 4 107.59 5.10 0 -2 4 106.49 5.40 0 -2 4 107.99 5.10 -1 2 -4 276.57 13.40 -1 2 -4 287.67 13.30 -1 2 -4 285.87 13.30 -1 2 -4 288.17 13.20 -1 2 -4 285.27 13.30 -1 2 -4 292.77 13.20 -1 2 -4 283.17 13.30 -1 2 -4 298.77 13.40 1 -2 4 287.27 13.20 1 -2 4 287.17 13.40 1 -2 4 278.37 13.30 1 -2 4 299.67 13.40 1 -2 4 295.27 13.40 1 -2 4 294.47 13.30 1 -2 4 300.47 13.40 1 -2 4 276.87 13.20 1 -2 4 290.87 13.20 1 -2 4 284.67 13.30 -2 2 -4 13.60 1.30 -2 2 -4 14.50 1.70 -2 2 -4 14.80 1.50 -2 2 -4 14.10 1.50 -2 2 -4 16.60 1.60 -2 2 -4 13.90 1.60 2 -2 4 14.70 1.50 2 -2 4 12.80 1.50 2 -2 4 12.40 1.60 2 -2 4 14.70 1.30 2 -2 4 13.50 1.80 2 -2 4 9.30 1.60 2 -2 4 12.50 1.90 2 -2 4 16.40 1.80 2 -2 4 13.00 1.40 -3 2 -4 278.77 13.30 -3 2 -4 293.37 13.30 -3 2 -4 304.07 13.30 -3 2 -4 290.47 13.20 -3 2 -4 293.17 13.40 -3 2 -4 295.77 13.50 3 -2 4 291.47 13.50 3 -2 4 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11.50 -11 -3 7 136.29 16.90 10 3 -7 2.50 4.10 10 3 -7 2.60 4.40 10 3 -7 -1.10 5.50 -10 -3 7 6.60 7.50 -10 -3 7 1.60 6.40 -10 -3 7 2.10 3.80 -10 -3 7 -1.90 5.80 9 3 -7 41.30 4.40 9 3 -7 36.50 4.40 9 3 -7 47.70 5.10 9 3 -7 47.60 5.90 9 3 -7 46.50 5.80 -9 -3 7 41.90 5.30 -9 -3 7 35.30 6.00 -9 -3 7 31.10 4.00 -9 -3 7 38.80 6.50 8 3 -7 232.28 11.50 8 3 -7 201.58 11.30 8 3 -7 222.78 11.80 8 3 -7 219.98 11.10 8 3 -7 203.38 10.50 8 3 -7 196.78 11.70 -8 -3 7 222.98 12.70 -8 -3 7 220.48 11.80 -8 -3 7 205.48 12.90 -8 -3 7 211.48 11.80 7 3 -7 184.18 9.30 7 3 -7 148.69 10.50 7 3 -7 183.28 9.30 7 3 -7 175.48 9.40 7 3 -7 181.68 10.60 7 3 -7 176.78 8.80 -7 -3 7 181.88 9.80 -7 -3 7 159.68 9.10 -7 -3 7 179.88 10.70 -7 -3 7 179.48 9.50 6 3 -7 0.10 3.00 6 3 -7 -2.00 2.00 6 3 -7 -2.60 2.20 6 3 -7 5.20 2.60 6 3 -7 1.90 2.40 6 3 -7 -2.40 1.70 -6 -3 7 2.40 2.70 -6 -3 7 -0.90 3.60 -6 -3 7 0.10 2.00 5 3 -7 286.67 14.30 5 3 -7 298.57 14.10 5 3 -7 288.87 14.40 5 3 -7 300.67 14.30 5 3 -7 298.47 14.00 5 3 -7 305.17 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445.26 23.30 7 -3 7 508.25 25.10 7 -3 7 479.85 23.80 7 -3 7 573.64 25.80 -8 3 -7 78.99 8.30 -8 3 -7 94.09 11.00 -8 3 -7 68.89 6.60 -8 3 -7 76.89 7.10 8 -3 7 82.09 6.80 8 -3 7 70.39 5.80 8 -3 7 75.39 8.30 8 -3 7 83.89 9.40 8 -3 7 75.09 7.50 8 -3 7 71.69 7.40 -9 3 -7 21.60 4.90 -9 3 -7 25.90 4.40 -9 3 -7 0.80 5.60 9 -3 7 22.70 4.80 9 -3 7 24.90 3.60 9 -3 7 17.70 5.00 9 -3 7 20.70 4.90 -10 3 -7 29.70 5.90 -10 3 -7 19.70 5.30 -10 3 -7 27.40 6.90 10 -3 7 39.30 6.40 10 -3 7 25.80 4.20 10 -3 7 30.80 5.60 10 -3 7 30.90 5.40 10 -3 7 21.00 5.90 11 2 -7 8.20 5.40 11 2 -7 9.80 6.80 11 2 -7 4.00 5.00 -11 -2 7 4.30 4.50 -11 -2 7 1.20 7.40 10 2 -7 162.68 8.90 10 2 -7 169.48 10.20 10 2 -7 158.18 12.00 10 2 -7 162.48 10.80 -10 -2 7 159.68 11.70 -10 -2 7 177.18 13.30 -10 -2 7 163.38 13.10 -10 -2 7 145.59 10.00 9 2 -7 188.38 11.20 9 2 -7 196.98 10.10 9 2 -7 203.68 10.90 9 2 -7 191.08 11.50 9 2 -7 223.18 11.00 9 2 -7 194.18 11.90 -9 -2 7 187.18 11.70 -9 -2 7 199.68 12.90 -9 -2 7 212.78 12.70 -9 -2 7 187.58 10.70 8 2 -7 9.60 3.10 8 2 -7 4.40 2.10 8 2 -7 1.10 3.80 8 2 -7 2.90 2.80 8 2 -7 5.20 3.60 8 2 -7 4.50 3.20 -8 -2 7 4.70 3.30 -8 -2 7 1.20 4.50 -8 -2 7 5.70 2.60 -8 -2 7 3.20 4.30 -8 -2 7 4.70 3.70 7 2 -7 75.59 4.90 7 2 -7 83.39 5.40 7 2 -7 83.09 5.90 7 2 -7 83.79 5.70 7 2 -7 73.19 6.70 -7 -2 7 79.09 5.90 -7 -2 7 77.39 6.10 -7 -2 7 71.59 6.90 -7 -2 7 86.19 7.10 -7 -2 7 67.99 5.20 6 2 -7 116.29 7.50 6 2 -7 124.89 7.00 6 2 -7 122.09 6.70 6 2 -7 126.99 6.90 6 2 -7 119.09 7.20 6 2 -7 121.99 6.40 -6 -2 7 121.39 6.60 -6 -2 7 126.39 7.90 -6 -2 7 129.39 7.00 -6 -2 7 117.29 7.60 -6 -2 7 113.19 7.00 5 2 -7 41.90 4.60 5 2 -7 42.90 3.50 5 2 -7 44.70 4.10 5 2 -7 46.90 4.20 5 2 -7 44.20 3.30 -5 -2 7 46.90 4.10 -5 -2 7 45.60 4.70 -5 -2 7 45.70 3.50 -5 -2 7 43.40 4.10 4 2 -7 29.60 3.80 4 2 -7 32.00 3.30 4 2 -7 29.20 2.80 4 2 -7 35.20 3.90 4 2 -7 31.60 3.50 4 2 -7 34.90 2.80 4 2 -7 32.50 2.80 -4 -2 7 34.70 3.10 -4 -2 7 28.60 2.50 -4 -2 7 28.30 3.20 -4 -2 7 34.20 3.80 -4 -2 7 35.10 2.80 -4 -2 7 34.30 3.60 3 2 -7 72.09 5.30 3 2 -7 69.09 4.10 3 2 -7 71.19 4.50 3 2 -7 70.89 4.80 3 2 -7 72.19 4.60 3 2 -7 74.19 4.10 3 2 -7 71.19 4.30 3 2 -7 69.59 4.90 -3 -2 7 69.69 4.60 -3 -2 7 74.49 4.60 -3 -2 7 78.79 4.70 -3 -2 7 80.49 4.10 -3 -2 7 76.19 4.70 -3 -2 7 76.89 4.00 2 2 -7 685.43 32.40 2 2 -7 713.93 32.30 2 2 -7 726.73 32.30 2 2 -7 680.53 32.40 2 2 -7 678.83 32.30 2 2 -7 685.03 32.30 2 2 -7 705.93 32.40 2 2 -7 656.73 32.40 2 2 -7 722.13 32.60 2 2 -7 717.93 32.30 -2 -2 7 712.73 32.40 -2 -2 7 819.32 32.60 -2 -2 7 685.73 32.30 -2 -2 7 683.53 32.20 -2 -2 7 729.03 32.20 -2 -2 7 714.83 32.40 -2 -2 7 713.13 32.40 -2 -2 7 686.73 32.60 -2 -2 7 708.73 32.20 1 2 -7 93.69 4.50 1 2 -7 72.49 4.20 1 2 -7 74.69 4.50 1 2 -7 80.19 4.60 1 2 -7 83.99 4.30 1 2 -7 77.79 4.80 1 2 -7 79.29 4.70 1 2 -7 79.19 4.90 1 2 -7 77.99 4.30 -1 -2 7 79.59 5.00 -1 -2 7 82.59 4.10 -1 -2 7 82.19 4.70 -1 -2 7 76.69 4.60 -1 -2 7 85.19 4.70 -1 -2 7 79.09 4.30 -1 -2 7 76.89 4.40 -1 -2 7 85.09 5.40 0 2 -7 136.29 7.30 0 2 -7 147.99 7.10 0 2 -7 146.49 7.70 0 2 -7 146.29 7.30 0 2 -7 136.29 7.30 0 2 -7 151.18 7.10 0 2 -7 134.29 7.20 0 2 -7 146.79 6.90 0 2 -7 151.28 7.10 0 -2 7 147.69 7.90 0 -2 7 142.59 7.00 0 -2 7 149.29 7.20 0 -2 7 146.49 7.60 0 -2 7 147.89 7.30 0 -2 7 146.39 6.80 0 -2 7 142.69 7.30 0 -2 7 146.19 7.40 -1 2 -7 482.25 21.30 -1 2 -7 469.35 21.40 -1 2 -7 500.85 21.30 -1 2 -7 477.75 21.60 -1 2 -7 453.65 21.60 -1 2 -7 400.66 21.50 -1 2 -7 462.95 21.50 -1 2 -7 483.45 21.40 1 -2 7 434.86 21.40 1 -2 7 497.15 22.10 1 -2 7 447.36 21.40 1 -2 7 476.75 21.70 1 -2 7 464.95 21.50 1 -2 7 456.85 21.50 1 -2 7 456.15 21.50 1 -2 7 477.25 21.40 1 -2 7 474.55 21.50 -2 2 -7 3.90 1.70 -2 2 -7 1.00 1.40 -2 2 -7 4.40 1.00 -2 2 -7 4.70 1.20 -2 2 -7 4.60 1.30 -2 2 -7 4.60 1.80 -2 2 -7 3.00 1.20 -2 2 -7 2.70 2.10 -2 2 -7 5.60 1.50 2 -2 7 3.10 1.70 2 -2 7 3.20 2.20 2 -2 7 4.30 1.70 2 -2 7 3.00 1.30 2 -2 7 1.70 2.40 2 -2 7 2.40 2.50 2 -2 7 5.10 1.50 2 -2 7 1.20 1.70 2 -2 7 2.00 2.00 2 -2 7 4.20 1.90 2 -2 7 3.50 1.50 -3 2 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5 -8 7.70 3.10 10 5 -8 3.10 5.00 -10 -5 8 6.20 9.30 -10 -5 8 5.70 6.90 9 5 -8 63.59 8.00 9 5 -8 65.59 7.50 9 5 -8 84.49 9.70 9 5 -8 68.39 6.60 9 5 -8 66.59 5.60 9 5 -8 63.69 7.60 -9 -5 8 64.79 8.70 -9 -5 8 61.89 7.60 -9 -5 8 69.19 9.20 8 5 -8 113.89 9.20 8 5 -8 115.19 7.80 8 5 -8 109.89 6.70 8 5 -8 105.19 7.30 8 5 -8 113.89 8.20 -8 -5 8 96.99 7.90 -8 -5 8 82.09 10.60 -8 -5 8 119.39 11.40 7 5 -8 22.60 3.40 7 5 -8 18.90 2.70 7 5 -8 11.00 4.10 7 5 -8 25.20 3.50 7 5 -8 25.50 3.70 7 5 -8 15.60 5.20 -7 -5 8 21.00 5.90 -7 -5 8 16.00 3.70 -7 -5 8 20.10 3.50 -7 -5 8 15.90 4.50 -7 -5 8 18.40 4.90 6 5 -8 31.40 3.20 6 5 -8 33.90 3.90 6 5 -8 31.40 5.10 6 5 -8 27.70 3.30 6 5 -8 23.90 2.80 6 5 -8 34.10 3.50 -6 -5 8 34.00 3.40 -6 -5 8 30.80 4.30 -6 -5 8 44.50 5.70 -6 -5 8 24.80 4.20 5 5 -8 53.29 4.80 5 5 -8 56.39 5.70 5 5 -8 59.19 4.40 5 5 -8 60.29 7.50 5 5 -8 50.89 5.10 5 5 -8 55.79 5.60 -5 -5 8 54.79 4.90 -5 -5 8 57.39 6.10 -5 -5 8 56.99 5.70 -5 -5 8 57.79 6.00 4 5 -8 432.96 21.60 4 5 -8 429.66 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4 -8 417.66 20.70 3 4 -8 429.06 20.00 3 4 -8 431.66 20.00 3 4 -8 408.86 19.80 3 4 -8 434.16 19.80 -3 -4 8 436.36 20.10 -3 -4 8 437.56 20.00 -3 -4 8 410.46 20.20 -3 -4 8 420.86 19.70 -3 -4 8 426.36 20.40 -3 -4 8 422.96 19.70 2 4 -8 284.67 13.40 2 4 -8 288.87 13.40 2 4 -8 282.47 13.60 2 4 -8 275.77 13.30 2 4 -8 281.77 14.10 2 4 -8 287.47 13.60 -2 -4 8 287.87 13.30 -2 -4 8 295.17 13.70 -2 -4 8 276.07 13.60 -2 -4 8 271.17 14.00 -2 -4 8 285.77 13.30 -2 -4 8 268.47 13.40 1 4 -8 17.10 2.10 1 4 -8 20.10 2.20 1 4 -8 13.90 3.40 1 4 -8 21.50 2.60 1 4 -8 13.70 2.30 1 4 -8 21.50 2.00 1 4 -8 17.30 2.00 -1 -4 8 15.70 2.60 -1 -4 8 21.00 2.20 -1 -4 8 29.00 2.90 -1 -4 8 16.70 2.70 -1 -4 8 18.90 3.40 -1 -4 8 20.50 1.90 0 4 -8 678.43 31.90 0 4 -8 716.23 31.80 0 4 -8 707.63 32.00 0 4 -8 695.63 31.70 0 4 -8 691.13 31.70 0 -4 8 701.33 31.70 0 -4 8 665.33 31.60 0 -4 8 708.13 32.20 0 -4 8 669.13 32.10 -1 4 -8 178.68 8.50 -1 4 -8 165.18 8.10 -1 4 -8 169.78 8.30 -1 4 -8 162.58 8.40 -1 4 -8 156.28 8.80 1 -4 8 153.98 8.30 1 -4 8 163.68 9.10 1 -4 8 151.28 9.10 1 -4 8 169.58 8.20 1 -4 8 164.78 8.70 -2 4 -8 219.08 10.90 -2 4 -8 216.58 10.60 -2 4 -8 222.38 11.30 2 -4 8 219.98 11.20 2 -4 8 218.78 11.60 2 -4 8 217.28 11.40 2 -4 8 222.68 11.10 2 -4 8 225.48 10.80 -3 4 -8 5.90 1.60 -3 4 -8 6.50 2.00 -3 4 -8 2.10 2.20 -3 4 -8 5.50 3.10 -3 4 -8 3.80 2.00 -3 4 -8 5.60 2.20 3 -4 8 4.00 3.00 3 -4 8 4.70 2.40 3 -4 8 1.90 3.50 3 -4 8 9.20 2.80 3 -4 8 8.40 2.40 3 -4 8 4.60 3.30 -4 4 -8 128.09 7.50 -4 4 -8 130.99 7.10 -4 4 -8 126.59 7.40 -4 4 -8 135.39 6.80 -4 4 -8 126.39 8.00 4 -4 8 138.59 7.60 4 -4 8 130.89 7.40 4 -4 8 125.99 8.60 4 -4 8 129.39 7.20 4 -4 8 117.19 7.80 -5 4 -8 85.59 7.20 -5 4 -8 94.49 5.30 -5 4 -8 89.99 6.40 -5 4 -8 87.09 6.00 -5 4 -8 84.49 5.70 5 -4 8 83.79 5.90 5 -4 8 85.59 6.10 5 -4 8 84.99 7.80 5 -4 8 86.89 6.70 5 -4 8 84.69 6.60 -6 4 -8 0.40 3.30 -6 4 -8 -0.90 2.40 -6 4 -8 -1.50 4.20 -6 4 -8 0.80 2.70 -6 4 -8 3.90 3.40 6 -4 8 0.30 2.50 6 -4 8 1.60 3.50 6 -4 8 -1.30 3.30 6 -4 8 2.70 4.30 -7 4 -8 79.09 6.30 -7 4 -8 88.99 6.20 -7 4 -8 65.89 7.60 -7 4 -8 81.19 8.50 -7 4 -8 89.99 6.70 7 -4 8 77.89 6.20 7 -4 8 84.79 7.70 7 -4 8 80.99 9.80 7 -4 8 67.29 7.00 7 -4 8 84.49 7.70 -8 4 -8 168.88 12.30 -8 4 -8 179.58 12.20 -8 4 -8 147.79 10.70 -8 4 -8 163.58 10.20 8 -4 8 162.08 10.50 8 -4 8 168.28 10.70 8 -4 8 167.88 9.60 8 -4 8 158.68 11.30 -9 4 -8 77.89 12.70 -9 4 -8 76.49 9.10 -9 4 -8 64.49 6.20 9 -4 8 75.09 7.20 9 -4 8 69.69 6.50 9 -4 8 60.19 6.70 9 -4 8 55.89 7.10 11 3 -8 1.90 7.60 11 3 -8 3.80 5.80 11 3 -8 -0.60 6.00 -11 -3 8 3.70 5.10 -11 -3 8 0.30 7.50 10 3 -8 23.70 5.10 10 3 -8 21.00 4.80 10 3 -8 20.10 3.30 10 3 -8 20.40 6.20 -10 -3 8 22.60 4.40 -10 -3 8 36.30 8.40 -10 -3 8 17.20 6.50 9 3 -8 176.28 10.20 9 3 -8 171.88 11.80 9 3 -8 159.28 9.20 9 3 -8 156.18 10.60 9 3 -8 179.88 10.20 -9 -3 8 190.58 13.20 -9 -3 8 170.58 11.30 -9 -3 8 175.48 10.10 8 3 -8 83.09 8.10 8 3 -8 83.39 5.50 8 3 -8 76.39 6.70 8 3 -8 90.69 6.50 8 3 -8 73.59 6.90 -8 -3 8 70.69 7.20 -8 -3 8 84.69 9.60 -8 -3 8 76.79 6.20 -8 -3 8 66.69 7.60 7 3 -8 3.10 2.70 7 3 -8 5.80 4.30 7 3 -8 5.40 3.50 7 3 -8 8.70 3.00 7 3 -8 9.30 2.20 7 3 -8 6.50 3.20 -7 -3 8 3.10 4.50 -7 -3 8 9.50 2.70 -7 -3 8 9.70 3.50 6 3 -8 189.68 9.50 6 3 -8 184.58 9.60 6 3 -8 186.68 10.40 6 3 -8 187.48 9.80 6 3 -8 194.58 10.10 6 3 -8 184.28 9.20 -6 -3 8 177.78 10.70 -6 -3 8 185.28 9.90 -6 -3 8 169.88 9.90 -6 -3 8 177.28 9.30 5 3 -8 176.88 9.10 5 3 -8 191.28 9.50 5 3 -8 194.68 9.30 5 3 -8 178.68 10.00 5 3 -8 177.38 9.00 5 3 -8 178.98 9.50 -5 -3 8 174.98 9.60 -5 -3 8 169.08 9.90 -5 -3 8 181.58 9.60 -5 -3 8 182.98 9.10 4 3 -8 394.16 19.00 4 3 -8 396.46 19.20 4 3 -8 416.36 19.00 4 3 -8 389.96 18.80 4 3 -8 418.16 18.80 4 3 -8 395.16 18.70 -4 -3 8 403.06 18.60 -4 -3 8 412.16 19.20 -4 -3 8 392.06 18.70 -4 -3 8 422.76 19.00 -4 -3 8 386.16 18.90 -4 -3 8 402.76 18.80 3 3 -8 11.30 2.00 3 3 -8 11.60 1.80 3 3 -8 15.70 3.00 3 3 -8 9.60 2.30 3 3 -8 11.10 1.70 3 3 -8 11.00 2.20 -3 -3 8 10.50 2.40 -3 -3 8 12.20 1.80 -3 -3 8 11.00 1.80 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10 263.77 13.90 2 -6 10 296.47 14.80 -3 6 -10 385.46 18.40 -3 6 -10 394.16 18.20 -3 6 -10 392.76 18.80 -3 6 -10 400.26 18.20 -3 6 -10 376.46 18.60 -3 6 -10 370.26 19.50 3 -6 10 374.26 19.40 3 -6 10 376.06 18.70 3 -6 10 399.56 18.70 3 -6 10 346.87 18.50 -4 6 -10 72.19 7.10 -4 6 -10 66.39 6.20 -4 6 -10 71.49 5.80 -4 6 -10 82.49 8.90 -4 6 -10 65.19 7.40 -4 6 -10 65.89 5.80 4 -6 10 90.99 11.80 4 -6 10 49.60 6.80 4 -6 10 68.89 8.30 4 -6 10 59.19 7.50 -5 6 -10 1.80 3.80 -5 6 -10 1.20 4.00 -5 6 -10 -1.40 4.50 -5 6 -10 5.60 5.90 -5 6 -10 -2.80 3.20 5 -6 10 2.60 4.20 5 -6 10 1.10 4.30 5 -6 10 1.50 5.30 5 -6 10 0.30 4.60 -6 6 -10 113.39 10.80 -6 6 -10 114.79 8.80 -6 6 -10 117.59 9.30 -6 6 -10 136.19 8.30 -6 6 -10 110.59 10.10 6 -6 10 102.09 9.10 6 -6 10 130.29 10.30 6 -6 10 95.19 9.50 6 -6 10 120.89 10.90 -7 6 -10 105.89 13.60 -7 6 -10 94.09 9.70 -7 6 -10 97.49 10.60 -7 6 -10 113.09 9.40 -7 6 -10 91.79 10.70 7 -6 10 100.69 11.40 7 -6 10 99.69 10.70 7 -6 10 87.09 9.00 7 -6 10 88.79 9.30 9 5 -10 20.80 5.80 9 5 -10 16.80 6.80 9 5 -10 8.70 5.10 9 5 -10 6.20 6.20 9 5 -10 14.10 3.70 -9 -5 10 14.70 5.50 -9 -5 10 4.60 6.90 -9 -5 10 14.50 9.30 8 5 -10 1.70 4.40 8 5 -10 4.60 4.60 8 5 -10 -1.50 4.30 8 5 -10 -0.20 3.20 8 5 -10 4.60 6.30 -8 -5 10 0.80 5.60 -8 -5 10 5.30 8.10 -8 -5 10 3.20 4.20 7 5 -10 158.28 8.90 7 5 -10 148.09 9.80 7 5 -10 157.08 9.50 7 5 -10 144.09 9.80 7 5 -10 168.38 10.80 -7 -5 10 141.79 9.50 -7 -5 10 146.59 10.80 -7 -5 10 170.98 13.10 6 5 -10 65.89 6.80 6 5 -10 70.79 6.90 6 5 -10 55.19 5.70 6 5 -10 59.49 7.60 6 5 -10 67.09 6.20 6 5 -10 57.99 7.90 -6 -5 10 70.69 8.40 -6 -5 10 78.59 7.40 -6 -5 10 65.99 6.30 -6 -5 10 61.59 7.50 5 5 -10 39.40 4.60 5 5 -10 48.90 5.80 5 5 -10 45.20 5.10 5 5 -10 45.60 7.00 5 5 -10 47.70 5.10 -5 -5 10 45.70 5.40 -5 -5 10 46.20 5.30 -5 -5 10 52.59 11.20 -5 -5 10 41.90 6.90 4 5 -10 62.39 5.20 4 5 -10 52.69 5.90 4 5 -10 49.99 6.20 4 5 -10 65.79 5.20 4 5 -10 60.89 5.80 -4 -5 10 48.70 6.00 -4 -5 10 57.59 7.10 -4 -5 10 55.79 5.30 -4 -5 10 54.09 5.00 3 5 -10 328.27 15.80 3 5 -10 305.47 15.30 3 5 -10 321.27 15.30 3 5 -10 318.77 15.40 3 5 -10 309.77 15.70 -3 -5 10 317.97 15.20 -3 -5 10 324.87 16.60 -3 -5 10 333.77 16.10 -3 -5 10 302.37 15.20 2 5 -10 196.88 10.00 2 5 -10 202.18 10.10 2 5 -10 208.28 10.50 2 5 -10 207.88 10.70 2 5 -10 204.58 10.10 -2 -5 10 199.08 10.10 -2 -5 10 176.68 11.60 -2 -5 10 190.58 10.00 -2 -5 10 165.28 10.80 -2 -5 10 216.78 11.00 1 5 -10 63.39 6.50 1 5 -10 73.29 5.20 1 5 -10 78.89 6.00 1 5 -10 81.29 6.00 1 5 -10 70.19 5.30 1 5 -10 78.39 5.40 -1 -5 10 72.59 5.00 -1 -5 10 79.89 5.50 -1 -5 10 56.19 6.00 -1 -5 10 70.09 6.60 0 5 -10 148.39 7.90 0 5 -10 141.29 9.20 0 5 -10 154.48 8.60 0 5 -10 153.18 8.30 0 5 -10 148.49 7.90 0 5 -10 156.48 8.50 0 -5 10 138.59 8.30 0 -5 10 145.49 9.10 0 -5 10 148.99 10.00 -1 5 -10 200.88 10.40 -1 5 -10 207.48 11.60 -1 5 -10 217.88 11.10 -1 5 -10 225.78 10.90 -1 5 -10 221.48 10.60 1 -5 10 213.68 12.40 1 -5 10 204.88 10.80 1 -5 10 201.18 11.60 1 -5 10 206.48 10.70 -2 5 -10 2.90 2.90 -2 5 -10 0.80 2.40 -2 5 -10 4.00 2.20 -2 5 -10 0.80 2.40 -2 5 -10 -0.70 3.90 2 -5 10 3.00 3.70 2 -5 10 2.90 3.10 2 -5 10 -3.40 5.00 2 -5 10 -3.70 2.80 -3 5 -10 38.80 5.40 -3 5 -10 28.30 5.10 -3 5 -10 28.90 3.40 -3 5 -10 27.30 3.60 -3 5 -10 25.50 3.00 -3 5 -10 36.70 4.20 3 -5 10 31.30 4.80 3 -5 10 39.00 3.90 3 -5 10 40.60 5.40 3 -5 10 36.60 4.50 -4 5 -10 184.98 10.30 -4 5 -10 162.38 9.60 -4 5 -10 194.08 11.30 -4 5 -10 165.88 9.10 -4 5 -10 193.08 9.40 -4 5 -10 193.48 10.30 4 -5 10 173.48 10.00 4 -5 10 168.58 10.00 4 -5 10 173.48 10.90 4 -5 10 190.48 10.40 -5 5 -10 23.20 3.30 -5 5 -10 24.10 3.60 -5 5 -10 29.90 5.80 -5 5 -10 27.30 4.50 -5 5 -10 35.40 4.20 5 -5 10 23.50 3.80 5 -5 10 33.40 4.40 5 -5 10 22.50 4.50 5 -5 10 25.70 5.30 -6 5 -10 15.50 4.80 -6 5 -10 10.60 4.00 -6 5 -10 10.40 3.40 -6 5 -10 7.90 5.70 6 -5 10 10.60 5.20 6 -5 10 10.90 4.40 6 -5 10 6.00 4.80 6 -5 10 6.60 4.20 -7 5 -10 3.40 6.20 -7 5 -10 -3.30 6.70 -7 5 -10 -0.80 3.90 -7 5 -10 6.00 4.40 -7 5 -10 0.50 5.30 7 -5 10 -0.40 4.20 7 -5 10 4.60 5.10 7 -5 10 -3.60 5.30 7 -5 10 -1.30 5.70 -8 5 -10 77.99 10.20 -8 5 -10 87.89 12.90 -8 5 -10 67.59 6.70 -8 5 -10 79.19 9.50 8 -5 10 78.59 7.40 8 -5 10 68.19 8.20 8 -5 10 75.69 8.20 8 -5 10 86.79 8.60 10 4 -10 -1.10 6.10 10 4 -10 -2.10 5.30 10 4 -10 -0.70 7.40 10 4 -10 1.40 3.70 10 4 -10 0.20 5.60 -10 -4 10 9.70 10.20 -10 -4 10 5.40 7.70 -10 -4 10 -1.20 5.30 9 4 -10 110.79 7.60 9 4 -10 106.19 9.00 9 4 -10 103.79 9.20 9 4 -10 108.39 10.20 -9 -4 10 109.69 8.90 -9 -4 10 127.29 14.60 -9 -4 10 99.29 11.20 8 4 -10 142.29 9.60 8 4 -10 133.69 11.10 8 4 -10 160.18 9.40 8 4 -10 137.19 10.00 8 4 -10 140.39 8.40 -8 -4 10 156.48 13.20 -8 -4 10 125.19 9.20 -8 -4 10 115.19 10.50 7 4 -10 1.90 2.80 7 4 -10 0.40 3.70 7 4 -10 3.60 4.50 7 4 -10 4.80 3.60 7 4 -10 -1.40 4.00 -7 -4 10 -3.50 5.90 -7 -4 10 0.80 4.50 -7 -4 10 -0.20 3.40 -7 -4 10 1.70 5.20 6 4 -10 25.30 3.10 6 4 -10 21.80 4.10 6 4 -10 34.50 4.90 6 4 -10 27.00 3.60 6 4 -10 23.20 3.50 -6 -4 10 24.20 4.50 -6 -4 10 23.10 4.70 -6 -4 10 15.50 4.30 5 4 -10 250.17 12.60 5 4 -10 254.07 12.30 5 4 -10 252.77 12.90 5 4 -10 247.88 12.40 5 4 -10 250.57 12.80 5 4 -10 230.08 14.40 -5 -4 10 224.68 13.10 -5 -4 10 264.07 13.20 -5 -4 10 242.48 12.30 -5 -4 10 247.98 13.80 4 4 -10 2.80 2.50 4 4 -10 3.50 2.70 4 4 -10 2.80 5.30 4 4 -10 3.10 2.50 4 4 -10 7.70 3.20 4 4 -10 0.40 3.00 -4 -4 10 0.20 2.40 -4 -4 10 0.20 2.40 -4 -4 10 11.50 3.80 -4 -4 10 2.50 4.20 3 4 -10 72.19 5.90 3 4 -10 78.99 5.50 3 4 -10 72.39 5.00 3 4 -10 76.89 5.20 3 4 -10 72.29 5.80 -3 -4 10 52.59 5.60 -3 -4 10 70.59 5.10 -3 -4 10 75.29 5.00 -3 -4 10 65.79 6.30 2 4 -10 109.29 6.90 2 4 -10 102.39 6.40 2 4 -10 112.29 6.10 2 4 -10 120.39 6.60 2 4 -10 105.39 6.90 -2 -4 10 103.99 6.10 -2 -4 10 105.19 6.30 -2 -4 10 102.89 7.30 -2 -4 10 105.29 7.10 -2 -4 10 104.29 7.80 1 4 -10 389.56 17.30 1 4 -10 363.46 17.30 1 4 -10 379.76 17.60 1 4 -10 364.06 17.20 1 4 -10 340.67 17.40 1 4 -10 363.36 17.60 -1 -4 10 372.76 17.70 -1 -4 10 361.86 17.20 -1 -4 10 348.67 18.00 -1 -4 10 376.56 17.10 0 4 -10 82.79 5.10 0 4 -10 78.49 5.60 0 4 -10 87.69 5.90 0 4 -10 84.79 5.40 0 4 -10 78.99 5.00 0 -4 10 73.69 5.40 0 -4 10 83.19 4.80 0 -4 10 75.79 5.00 0 -4 10 66.49 6.90 0 -4 10 84.29 6.20 -1 4 -10 36.10 4.60 -1 4 -10 39.40 3.50 -1 4 -10 35.80 3.90 -1 4 -10 45.10 5.00 -1 4 -10 36.40 4.10 -1 4 -10 48.50 4.20 1 -4 10 43.80 5.20 1 -4 10 39.00 4.70 1 -4 10 35.90 4.80 1 -4 10 35.50 4.30 -2 4 -10 372.26 17.40 -2 4 -10 359.56 17.40 -2 4 -10 364.16 17.60 -2 4 -10 337.07 17.90 -2 4 -10 373.56 17.00 -2 4 -10 364.16 17.20 2 -4 10 368.36 17.20 2 -4 10 377.66 17.20 2 -4 10 371.66 17.80 2 -4 10 338.97 18.10 -3 4 -10 305.37 14.50 -3 4 -10 286.97 13.90 -3 4 -10 301.87 14.20 -3 4 -10 274.37 14.10 -3 4 -10 299.37 15.10 3 -4 10 325.67 14.90 3 -4 10 272.57 15.00 3 -4 10 298.27 14.40 3 -4 10 286.97 15.40 3 -4 10 287.37 14.30 -4 4 -10 -2.60 3.10 -4 4 -10 5.50 4.10 -4 4 -10 5.30 3.00 -4 4 -10 4.60 2.20 -4 4 -10 3.10 2.50 4 -4 10 6.20 3.80 4 -4 10 2.50 5.40 4 -4 10 11.30 3.30 4 -4 10 4.40 3.20 -5 4 -10 90.39 7.50 -5 4 -10 107.99 6.20 -5 4 -10 101.49 7.20 -5 4 -10 96.49 6.70 -5 4 -10 98.29 8.80 5 -4 10 99.19 7.90 5 -4 10 88.09 10.00 5 -4 10 107.09 7.00 5 -4 10 103.59 7.70 5 -4 10 88.89 11.00 -6 4 -10 301.87 16.20 -6 4 -10 361.86 15.80 -6 4 -10 317.97 17.50 -6 4 -10 333.37 16.20 -6 4 -10 347.97 18.20 6 -4 10 336.67 16.80 6 -4 10 313.37 17.00 6 -4 10 320.57 16.20 6 -4 10 314.17 16.40 -7 4 -10 90.69 8.90 -7 4 -10 106.79 10.60 -7 4 -10 106.49 7.80 -7 4 -10 114.09 7.30 -7 4 -10 99.79 8.10 7 -4 10 101.89 9.20 7 -4 10 101.79 8.50 7 -4 10 95.29 9.30 7 -4 10 90.59 7.70 -8 4 -10 21.30 4.60 -8 4 -10 5.70 7.30 -8 4 -10 10.10 6.50 -8 4 -10 5.10 5.50 8 -4 10 16.80 5.70 8 -4 10 9.80 4.00 8 -4 10 5.70 5.20 8 -4 10 14.20 5.90 -9 4 -10 22.00 5.80 -9 4 -10 35.90 6.90 9 -4 10 19.50 6.30 9 -4 10 34.20 6.70 9 -4 10 22.50 4.60 9 -4 10 31.70 7.40 10 3 -10 37.40 6.20 10 3 -10 34.80 5.60 10 3 -10 40.30 6.20 10 3 -10 32.20 6.10 10 3 -10 39.60 7.90 -10 -3 10 44.60 16.80 -10 -3 10 48.80 5.90 -10 -3 10 27.80 9.80 9 3 -10 42.50 5.30 9 3 -10 46.40 5.50 9 3 -10 52.59 6.20 9 3 -10 37.40 6.50 9 3 -10 37.60 5.60 -9 -3 10 33.40 6.50 -9 -3 10 48.10 8.30 -9 -3 10 39.20 4.90 8 3 -10 51.59 5.20 8 3 -10 54.19 6.70 8 3 -10 59.99 7.50 8 3 -10 53.49 5.70 8 3 -10 51.79 5.90 -8 -3 10 47.50 4.70 -8 -3 10 52.49 8.00 -8 -3 10 60.59 7.50 7 3 -10 111.39 8.20 7 3 -10 106.99 7.00 7 3 -10 114.89 9.00 7 3 -10 107.49 7.60 7 3 -10 100.29 11.30 7 3 -10 126.99 9.20 -7 -3 10 105.89 8.30 -7 -3 10 117.99 9.10 -7 -3 10 112.49 7.40 6 3 -10 28.90 6.90 6 3 -10 23.40 3.70 6 3 -10 26.10 4.10 6 3 -10 33.50 4.40 6 3 -10 35.20 4.20 6 3 -10 30.80 3.50 -6 -3 10 31.80 4.40 -6 -3 10 31.90 5.10 -6 -3 10 27.50 3.30 -6 -3 10 30.90 4.20 5 3 -10 11.00 3.00 5 3 -10 6.20 2.40 5 3 -10 6.10 3.30 5 3 -10 12.40 5.00 5 3 -10 12.30 2.80 5 3 -10 14.50 3.40 -5 -3 10 8.60 2.60 -5 -3 10 9.90 4.20 -5 -3 10 10.60 3.70 -5 -3 10 12.60 2.60 4 3 -10 107.29 6.90 4 3 -10 101.09 8.70 4 3 -10 111.79 6.70 4 3 -10 106.99 6.20 4 3 -10 103.19 6.30 4 3 -10 101.69 7.10 -4 -3 10 98.99 7.20 -4 -3 10 97.59 6.00 -4 -3 10 104.29 7.60 -4 -3 10 108.99 6.20 3 3 -10 160.58 8.80 3 3 -10 162.58 8.80 3 3 -10 186.78 9.20 3 3 -10 186.28 9.30 3 3 -10 171.48 9.40 -3 -3 10 172.98 8.70 -3 -3 10 163.18 8.70 -3 -3 10 173.28 9.50 -3 -3 10 193.48 9.80 2 3 -10 5.40 2.00 2 3 -10 1.60 2.40 2 3 -10 4.00 2.20 2 3 -10 6.90 2.00 2 3 -10 7.40 2.80 -2 -3 10 -4.20 3.30 -2 -3 10 6.40 1.90 -2 -3 10 4.10 2.10 -2 -3 10 6.80 2.80 1 3 -10 222.48 11.20 1 3 -10 223.48 10.90 1 3 -10 230.38 10.80 1 3 -10 207.18 10.90 1 3 -10 231.48 10.60 -1 -3 10 214.48 10.50 -1 -3 10 195.88 10.60 -1 -3 10 214.48 11.50 -1 -3 10 221.88 11.20 -1 -3 10 230.28 11.40 0 3 -10 333.37 15.50 0 3 -10 347.07 15.80 0 3 -10 341.47 15.70 0 3 -10 327.47 15.50 0 3 -10 331.77 16.00 0 -3 10 323.57 15.50 0 -3 10 310.97 16.10 0 -3 10 329.67 15.30 0 -3 10 318.27 15.50 0 -3 10 333.97 16.00 -1 3 -10 54.59 4.30 -1 3 -10 50.59 3.90 -1 3 -10 50.39 4.50 -1 3 -10 52.09 5.00 1 -3 10 53.49 4.20 1 -3 10 43.90 5.50 1 -3 10 52.79 4.30 1 -3 10 55.69 5.10 -2 3 -10 227.28 11.10 -2 3 -10 235.28 10.80 -2 3 -10 223.08 11.00 -2 3 -10 218.28 11.00 -2 3 -10 228.08 11.50 -2 3 -10 228.08 11.20 2 -3 10 227.78 11.90 2 -3 10 226.68 12.20 2 -3 10 222.38 11.20 2 -3 10 224.98 11.10 2 -3 10 230.58 11.60 2 -3 10 208.88 11.80 -3 3 -10 28.70 3.10 -3 3 -10 32.50 3.20 -3 3 -10 30.20 3.10 -3 3 -10 25.90 3.30 -3 3 -10 32.60 3.90 -3 3 -10 29.30 3.40 3 -3 10 30.00 4.30 3 -3 10 30.30 3.30 3 -3 10 33.00 3.50 3 -3 10 33.70 4.40 3 -3 10 33.30 4.40 3 -3 10 32.50 3.20 -4 3 -10 129.09 6.90 -4 3 -10 117.49 7.50 -4 3 -10 125.29 7.30 -4 3 -10 122.19 8.30 -4 3 -10 130.39 6.50 4 -3 10 119.09 7.50 4 -3 10 119.09 7.80 4 -3 10 110.79 7.40 4 -3 10 116.59 7.20 -5 3 -10 18.60 3.00 -5 3 -10 16.10 3.60 -5 3 -10 16.70 2.40 -5 3 -10 23.00 3.10 -5 3 -10 10.30 4.40 5 -3 10 18.10 3.50 5 -3 10 16.90 3.80 5 -3 10 20.00 3.60 5 -3 10 21.00 3.50 5 -3 10 21.80 5.20 -6 3 -10 41.50 5.30 -6 3 -10 32.20 3.50 -6 3 -10 38.00 4.20 -6 3 -10 29.50 3.60 -6 3 -10 30.60 4.30 6 -3 10 31.30 4.30 6 -3 10 29.30 4.30 6 -3 10 32.90 6.00 6 -3 10 27.20 3.40 6 -3 10 28.00 4.50 6 -3 10 40.40 4.30 -7 3 -10 96.29 9.90 -7 3 -10 108.19 7.70 -7 3 -10 124.79 9.70 -7 3 -10 101.89 8.50 7 -3 10 91.89 8.70 7 -3 10 109.29 7.30 7 -3 10 89.79 8.70 7 -3 10 102.99 8.10 -8 3 -10 67.29 7.60 -8 3 -10 59.49 6.50 -8 3 -10 75.99 10.80 -8 3 -10 74.69 7.50 8 -3 10 71.99 8.90 8 -3 10 72.39 6.10 8 -3 10 59.19 6.70 8 -3 10 77.29 8.60 -9 3 -10 6.90 5.80 -9 3 -10 7.30 5.20 9 -3 10 14.90 5.60 9 -3 10 15.00 6.20 10 2 -10 6.30 7.00 10 2 -10 7.40 5.80 10 2 -10 4.50 5.80 -10 -2 10 4.70 8.60 -10 -2 10 -0.10 8.90 9 2 -10 180.58 9.80 9 2 -10 175.78 12.80 9 2 -10 172.38 10.70 9 2 -10 182.98 11.40 9 2 -10 172.28 11.40 -9 -2 10 160.18 10.40 -9 -2 10 160.68 12.00 -9 -2 10 180.78 13.80 8 2 -10 242.98 13.40 8 2 -10 220.88 12.50 8 2 -10 220.68 11.90 8 2 -10 222.78 11.30 -8 -2 10 203.48 11.50 -8 -2 10 220.48 13.80 -8 -2 10 192.98 12.50 7 2 -10 53.09 5.10 7 2 -10 49.60 5.10 7 2 -10 49.99 5.40 7 2 -10 55.29 6.80 7 2 -10 42.30 4.40 7 2 -10 41.40 6.70 -7 -2 10 45.50 5.00 -7 -2 10 38.60 6.30 -7 -2 10 40.80 5.20 -7 -2 10 53.69 5.80 6 2 -10 227.98 12.90 6 2 -10 225.88 15.40 6 2 -10 278.37 13.20 6 2 -10 257.77 12.50 6 2 -10 260.37 12.40 6 2 -10 273.17 13.30 -6 -2 10 245.28 13.10 -6 -2 10 249.28 12.40 -6 -2 10 230.78 12.80 -6 -2 10 252.17 13.50 5 2 -10 139.79 7.70 5 2 -10 150.78 8.50 5 2 -10 138.49 8.30 5 2 -10 136.79 7.60 5 2 -10 120.59 9.60 5 2 -10 137.09 8.10 -5 -2 10 122.79 8.20 -5 -2 10 138.29 8.70 -5 -2 10 130.79 7.50 -5 -2 10 136.29 7.40 -5 -2 10 145.79 8.30 4 2 -10 22.00 2.60 4 2 -10 22.30 2.90 4 2 -10 19.40 3.30 4 2 -10 21.60 2.60 4 2 -10 29.10 3.30 4 2 -10 20.30 4.50 -4 -2 10 27.70 3.40 -4 -2 10 30.40 3.50 -4 -2 10 20.90 2.50 -4 -2 10 30.00 3.70 3 2 -10 2.40 2.30 3 2 -10 3.20 2.00 3 2 -10 2.00 3.80 3 2 -10 0.50 1.90 3 2 -10 2.70 2.70 3 2 -10 -0.80 2.50 -3 -2 10 0.80 2.70 -3 -2 10 3.60 2.00 -3 -2 10 0.80 1.90 -3 -2 10 -1.10 2.90 2 2 -10 515.45 25.10 2 2 -10 530.85 24.80 2 2 -10 522.65 24.70 2 2 -10 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23.10 6.70 0 0 -19 10.10 6.10 0 0 -19 23.10 9.00 0 0 19 26.90 5.80 0 0 19 33.30 14.70 -1 0 -19 52.39 7.60 -1 0 -19 58.79 6.30 -1 0 -19 52.89 9.10 -1 0 -19 61.09 8.10 1 0 19 66.49 8.90 1 0 19 59.69 9.80 1 0 19 67.29 6.60 2 -1 -19 132.69 15.20 -2 1 19 124.19 14.50 1 -1 -19 117.89 10.10 1 -1 -19 124.29 12.00 1 -1 -19 133.69 12.10 1 -1 -19 124.19 10.40 1 -1 -19 120.89 12.60 -1 1 19 137.99 16.10 -1 1 19 120.79 14.00 -1 1 19 127.09 10.60 0 -1 -19 6.10 8.80 0 -1 -19 2.60 6.60 0 -1 -19 1.80 6.00 0 -1 -19 -1.40 6.70 0 -1 -19 -2.20 5.10 0 -1 -19 3.10 5.10 0 1 19 2.20 7.70 0 1 19 -4.00 5.50 -1 -1 -19 48.60 5.70 -1 -1 -19 39.10 7.80 -1 -1 -19 45.80 8.90 1 1 19 33.80 8.10 1 1 19 22.50 7.90 1 1 19 37.80 6.00 -2 -1 -19 7.20 5.20 -2 -1 -19 9.10 8.50 -2 -1 -19 3.90 8.00 -2 -1 -19 2.40 6.40 2 1 19 11.20 8.40 2 1 19 6.80 5.70 2 1 19 -3.60 7.50 2 -2 -19 64.49 6.90 2 -2 -19 70.09 9.90 2 -2 -19 58.29 7.70 -2 2 19 62.59 9.40 -2 2 19 76.39 8.90 1 -2 -19 118.49 12.10 1 -2 -19 120.89 15.40 1 -2 -19 124.59 10.40 1 -2 -19 123.29 12.00 1 -2 -19 118.59 12.60 1 -2 -19 130.59 10.50 -1 2 19 153.18 15.60 -1 2 19 115.59 15.00 -1 2 19 139.99 10.50 0 -2 -19 110.09 9.30 0 -2 -19 107.09 9.30 0 -2 -19 112.49 11.50 0 -2 -19 85.29 10.30 0 -2 -19 108.99 11.40 0 -2 -19 76.19 9.10 0 2 19 104.59 12.20 0 2 19 134.19 9.70 -1 -2 -19 85.59 8.80 -1 -2 -19 88.99 10.20 -1 -2 -19 64.69 9.10 -1 -2 -19 75.49 10.00 -1 -2 -19 68.29 7.70 1 2 19 92.29 9.00 1 2 19 65.49 8.50 1 2 19 73.79 9.10 -2 -2 -19 25.70 9.40 -2 -2 -19 26.20 6.60 -2 -2 -19 25.90 5.40 -2 -2 -19 1.90 7.20 2 2 19 33.20 7.90 2 2 19 34.00 5.80 2 2 19 24.30 7.90 1 -3 -19 -2.50 7.20 1 -3 -19 4.80 9.10 1 -3 -19 -1.70 5.40 1 -3 -19 -3.70 6.10 1 -3 -19 -7.20 7.00 -1 3 19 -5.80 7.50 -1 3 19 5.50 5.40 0 -3 -19 38.70 8.90 0 -3 -19 50.29 6.90 0 -3 -19 16.70 8.00 0 -3 -19 34.80 8.90 0 -3 -19 20.70 5.50 0 -3 -19 36.40 5.40 0 3 19 35.30 7.80 0 3 19 43.10 10.20 0 3 19 30.70 5.60 -1 -3 -19 45.50 5.80 -1 -3 -19 62.09 9.90 -1 -3 -19 52.59 8.00 -1 -3 -19 36.80 7.40 -1 -3 -19 37.50 6.50 1 3 19 46.30 7.70 1 3 19 50.69 8.10 1 3 19 45.40 5.90 -2 -3 -19 26.50 9.70 -2 -3 -19 13.80 6.90 -2 -3 -19 20.40 5.30 2 3 19 18.80 5.60 2 3 19 22.70 7.60 2 3 19 18.30 7.80 -3 -3 -19 14.90 9.50 -3 -3 -19 0.00 5.50 1 -4 -19 223.38 16.40 1 -4 -19 215.68 13.90 1 -4 -19 230.78 16.00 1 -4 -19 226.08 22.60 -1 4 19 238.48 15.90 -1 4 19 214.08 16.60 0 -4 -19 129.89 14.00 0 -4 -19 123.89 15.60 0 -4 -19 146.09 13.50 0 -4 -19 161.28 16.40 0 -4 -19 147.09 12.70 0 -4 -19 134.09 10.30 0 4 19 139.39 13.90 0 4 19 145.09 10.90 -1 -4 -19 1.00 7.10 -1 -4 -19 -0.80 5.30 -1 -4 -19 0.70 6.90 -1 -4 -19 6.00 6.20 -1 -4 -19 8.90 9.30 -1 -4 -19 -3.50 7.40 1 4 19 8.80 7.30 1 4 19 0.40 5.50 1 4 19 7.30 7.60 -2 -4 -19 201.48 12.20 -2 -4 -19 203.98 18.10 -2 -4 -19 163.28 15.10 -2 -4 -19 194.28 14.40 -2 -4 -19 208.88 14.00 2 4 19 197.58 14.00 2 4 19 202.48 12.80 2 4 19 180.28 15.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 28447 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.36533(2) 0.71363(2) 0.86756(2) 0.01891(4) Uani 1 1 d . . . . . N1 N 0.73666(10) 0.76976(9) 0.68623(6) 0.01361(15) Uani 1 1 d . . . . . C21 C 0.80783(16) 0.87679(14) 1.05870(9) 0.0257(2) Uani 1 1 d . . . . . H21A H 0.712946 0.850552 1.094789 0.031 Uiso 1 1 calc R U . . . H21B H 0.867169 0.918341 1.105605 0.031 Uiso 1 1 calc R U . . . C22 C 0.90616(16) 0.73951(14) 1.02890(9) 0.0272(2) Uani 1 1 d . . . . . H22A H 0.927770 0.664821 1.090288 0.033 Uiso 1 1 calc R U . . . H22B H 1.006515 0.763591 1.000188 0.033 Uiso 1 1 calc R U . . . C23 C 0.82312(15) 0.67740(13) 0.95046(9) 0.0218(2) Uani 1 1 d . . . . . H23A H 0.727232 0.645457 0.981391 0.026 Uiso 1 1 calc R U . . . H23B H 0.890874 0.590812 0.931208 0.026 Uiso 1 1 calc R U . . . C14 C 0.78135(12) 0.79058(11) 0.85429(8) 0.01573(18) Uani 1 1 d . . . . . C13 C 0.69002(12) 0.73403(11) 0.78039(8) 0.01401(17) Uani 1 1 d . . . . . C9 C 0.63511(12) 0.73283(11) 0.61086(7) 0.01349(17) Uani 1 1 d . . . . . C8 C 0.63508(12) 0.76553(11) 0.50413(8) 0.01500(18) Uani 1 1 d . . . . . C10 C 0.75383(13) 0.83069(12) 0.43213(8) 0.01747(19) Uani 1 1 d . . . . . H10 H 0.829639 0.863868 0.474149 0.021 Uiso 1 1 calc R U . . . C11 C 0.68031(16) 0.96344(14) 0.35703(10) 0.0270(2) Uani 1 1 d . . . . . H11A H 0.605911 0.933697 0.314415 0.040 Uiso 1 1 calc R U . . . H11B H 0.761442 1.003131 0.313899 0.040 Uiso 1 1 calc R U . . . H11C H 0.626611 1.038301 0.394823 0.040 Uiso 1 1 calc R U . . . C12 C 0.84378(15) 0.71321(14) 0.37487(10) 0.0264(2) Uani 1 1 d . . . . . H12A H 0.888423 0.628756 0.423964 0.040 Uiso 1 1 calc R U . . . H12B H 0.927082 0.753264 0.334247 0.040 Uiso 1 1 calc R U . . . H12C H 0.773103 0.682822 0.329962 0.040 Uiso 1 1 calc R U . . . C1 C 0.62177(13) 0.46446(11) 0.83278(8) 0.01737(19) Uani 1 1 d . . . . . H1 H 0.648043 0.461016 0.905658 0.021 Uiso 1 1 calc R U . . . C3 C 0.76839(14) 0.40326(12) 0.77804(9) 0.0217(2) Uani 1 1 d . . . . . H3A H 0.803735 0.301989 0.809185 0.032 Uiso 1 1 calc R U . . . H3B H 0.849691 0.461976 0.783726 0.032 Uiso 1 1 calc R U . . . H3C H 0.745728 0.406586 0.706125 0.032 Uiso 1 1 calc R U . . . C2 C 0.49963(15) 0.36570(13) 0.82924(9) 0.0233(2) Uani 1 1 d . . . . . H2A H 0.478041 0.361158 0.758256 0.035 Uiso 1 1 calc R U . . . H2B H 0.404145 0.405338 0.862631 0.035 Uiso 1 1 calc R U . . . H2C H 0.538516 0.267381 0.864552 0.035 Uiso 1 1 calc R U . . . C4 C 0.52144(12) 0.66078(11) 0.66645(7) 0.01374(17) Uani 1 1 d . . . . . C5 C 0.40278(12) 0.62325(11) 0.61520(8) 0.01581(18) Uani 1 1 d . . . . . H5 H 0.326959 0.573266 0.651822 0.019 Uiso 1 1 calc R U . . . C6 C 0.39486(13) 0.65903(12) 0.50966(8) 0.01803(19) Uani 1 1 d . . . . . H6 H 0.311718 0.636645 0.474169 0.022 Uiso 1 1 calc R U . . . C7 C 0.50884(13) 0.72729(12) 0.45702(8) 0.01763(19) Uani 1 1 d . . . . . H7 H 0.501829 0.749752 0.385051 0.021 Uiso 1 1 calc R U . . . C20 C 0.76275(15) 0.99074(13) 0.96506(9) 0.0229(2) Uani 1 1 d . . . . . H20A H 0.857048 1.025335 0.933551 0.028 Uiso 1 1 calc R U . . . H20B H 0.693649 1.075492 0.985815 0.028 Uiso 1 1 calc R U . . . C19 C 0.68000(13) 0.92785(12) 0.88696(8) 0.0189(2) Uani 1 1 d . . . . . H19A H 0.655497 1.003255 0.826270 0.023 Uiso 1 1 calc R U . . . H19B H 0.581083 0.901261 0.916566 0.023 Uiso 1 1 calc R U . . . C15 C 0.92381(13) 0.82786(13) 0.79013(9) 0.0205(2) Uani 1 1 d . . . . . H15A H 1.013950 0.750033 0.807148 0.025 Uiso 1 1 calc R U . . . H15B H 0.951016 0.921072 0.803770 0.025 Uiso 1 1 calc R U . . . C16 C 0.88051(12) 0.84092(12) 0.67676(8) 0.01673(18) Uani 1 1 d . . . . . C17 C 1.01149(13) 0.75136(13) 0.62389(9) 0.0219(2) Uani 1 1 d . . . . . H17A H 1.022286 0.648682 0.655509 0.033 Uiso 1 1 calc R U . . . H17B H 1.108770 0.788006 0.630584 0.033 Uiso 1 1 calc R U . . . H17C H 0.987329 0.760018 0.551684 0.033 Uiso 1 1 calc R U . . . C18 C 0.84190(14) 1.00163(12) 0.62727(9) 0.0216(2) Uani 1 1 d . . . . . H18A H 0.787870 1.008093 0.563098 0.032 Uiso 1 1 calc R U . . . H18B H 0.937989 1.042851 0.613896 0.032 Uiso 1 1 calc R U . . . H18C H 0.775211 1.056444 0.673231 0.032 Uiso 1 1 calc R U . . . B1 B 0.55667(13) 0.63423(12) 0.78528(8) 0.01469(19) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.01811(6) 0.02431(6) 0.01535(5) -0.00611(4) 0.00303(4) -0.00414(4) N1 0.0138(4) 0.0149(4) 0.0122(4) -0.0022(3) -0.0005(3) -0.0022(3) C21 0.0314(6) 0.0332(6) 0.0166(5) -0.0091(4) -0.0019(4) -0.0123(5) C22 0.0331(6) 0.0302(6) 0.0192(5) -0.0040(4) -0.0110(5) -0.0053(5) C23 0.0282(6) 0.0216(5) 0.0157(5) -0.0026(4) -0.0073(4) -0.0033(4) C14 0.0168(4) 0.0182(4) 0.0131(4) -0.0040(3) -0.0015(3) -0.0038(4) C13 0.0150(4) 0.0142(4) 0.0121(4) -0.0021(3) -0.0008(3) 0.0000(3) C9 0.0148(4) 0.0143(4) 0.0111(4) -0.0024(3) -0.0013(3) -0.0006(3) C8 0.0175(4) 0.0151(4) 0.0115(4) -0.0017(3) 0.0006(3) -0.0005(3) C10 0.0212(5) 0.0183(4) 0.0127(4) -0.0022(3) 0.0022(4) -0.0032(4) C11 0.0325(6) 0.0245(5) 0.0212(5) 0.0051(4) -0.0005(5) -0.0050(5) C12 0.0267(6) 0.0284(6) 0.0261(6) -0.0109(5) 0.0103(5) -0.0062(5) C1 0.0229(5) 0.0167(4) 0.0123(4) -0.0009(3) -0.0018(4) -0.0037(4) C3 0.0260(5) 0.0178(5) 0.0198(5) -0.0025(4) -0.0042(4) 0.0009(4) C2 0.0314(6) 0.0183(5) 0.0211(5) -0.0014(4) -0.0021(4) -0.0080(4) C4 0.0148(4) 0.0137(4) 0.0122(4) -0.0018(3) -0.0006(3) -0.0008(3) C5 0.0164(4) 0.0162(4) 0.0148(4) -0.0027(3) -0.0013(3) -0.0017(3) C6 0.0187(5) 0.0209(5) 0.0149(4) -0.0044(4) -0.0041(4) -0.0019(4) C7 0.0212(5) 0.0200(5) 0.0113(4) -0.0030(3) -0.0017(4) -0.0012(4) C20 0.0262(6) 0.0244(5) 0.0219(5) -0.0110(4) 0.0000(4) -0.0076(4) C19 0.0197(5) 0.0196(5) 0.0184(5) -0.0068(4) -0.0009(4) -0.0026(4) C15 0.0159(5) 0.0296(5) 0.0177(5) -0.0063(4) -0.0015(4) -0.0061(4) C16 0.0144(4) 0.0202(5) 0.0167(4) -0.0040(4) 0.0010(4) -0.0052(4) C17 0.0165(5) 0.0277(5) 0.0211(5) -0.0057(4) 0.0028(4) -0.0011(4) C18 0.0250(5) 0.0186(5) 0.0223(5) -0.0033(4) 0.0031(4) -0.0077(4) B1 0.0164(5) 0.0170(5) 0.0111(4) -0.0025(4) -0.0002(4) -0.0036(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C13 N1 C9 112.70(9) . . ? C13 N1 C16 114.06(9) . . ? C9 N1 C16 133.23(8) . . ? H21A C21 H21B 108.0 . . ? C22 C21 H21A 109.4 . . ? C22 C21 H21B 109.4 . . ? C20 C21 H21A 109.4 . . ? C20 C21 H21B 109.4 . . ? C20 C21 C22 110.96(10) . . ? C21 C22 H22A 109.4 . . ? C21 C22 H22B 109.4 . . ? C21 C22 C23 111.23(10) . . ? H22A C22 H22B 108.0 . . ? C23 C22 H22A 109.4 . . ? C23 C22 H22B 109.4 . . ? C22 C23 H23A 109.2 . . ? C22 C23 H23B 109.2 . . ? C22 C23 C14 111.87(10) . . ? H23A C23 H23B 107.9 . . ? C14 C23 H23A 109.2 . . ? C14 C23 H23B 109.2 . . ? C23 C14 C19 108.27(9) . . ? C23 C14 C15 113.40(9) . . ? C13 C14 C23 112.12(9) . . ? C13 C14 C19 108.02(8) . . ? C13 C14 C15 102.31(8) . . ? C15 C14 C19 112.57(9) . . ? N1 C13 C14 111.68(9) . . ? N1 C13 B1 110.89(9) . . ? C14 C13 B1 137.33(9) . . ? C8 C9 N1 130.51(9) . . ? C8 C9 C4 122.51(9) . . ? C4 C9 N1 106.87(8) . . ? C9 C8 C10 129.56(10) . . ? C9 C8 C7 114.87(9) . . ? C7 C8 C10 115.52(9) . . ? C8 C10 H10 107.8 . . ? C8 C10 C11 112.55(9) . . ? C8 C10 C12 110.08(9) . . ? C11 C10 H10 107.8 . . ? C11 C10 C12 110.64(10) . . ? C12 C10 H10 107.8 . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C10 C12 H12A 109.5 . . ? C10 C12 H12B 109.5 . . ? C10 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C3 C1 H1 108.0 . . ? C3 C1 C2 108.78(9) . . ? C3 C1 B1 112.21(9) . . ? C2 C1 H1 108.0 . . ? C2 C1 B1 111.74(9) . . ? B1 C1 H1 108.0 . . ? C1 C3 H3A 109.5 . . ? C1 C3 H3B 109.5 . . ? C1 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? C1 C2 H2A 109.5 . . ? C1 C2 H2B 109.5 . . ? C1 C2 H2C 109.5 . . ? H2A C2 H2B 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? C9 C4 B1 110.53(9) . . ? C5 C4 C9 119.54(9) . . ? C5 C4 B1 129.93(9) . . ? C4 C5 H5 120.1 . . ? C4 C5 C6 119.77(10) . . ? C6 C5 H5 120.1 . . ? C5 C6 H6 120.2 . . ? C7 C6 C5 119.51(10) . . ? C7 C6 H6 120.2 . . ? C8 C7 H7 118.1 . . ? C6 C7 C8 123.71(10) . . ? C6 C7 H7 118.1 . . ? C21 C20 H20A 109.4 . . ? C21 C20 H20B 109.4 . . ? C21 C20 C19 111.27(10) . . ? H20A C20 H20B 108.0 . . ? C19 C20 H20A 109.4 . . ? C19 C20 H20B 109.4 . . ? C14 C19 H19A 109.3 . . ? C14 C19 H19B 109.3 . . ? C20 C19 C14 111.63(9) . . ? C20 C19 H19A 109.3 . . ? C20 C19 H19B 109.3 . . ? H19A C19 H19B 108.0 . . ? C14 C15 H15A 110.3 . . ? C14 C15 H15B 110.3 . . ? C14 C15 C16 107.25(9) . . ? H15A C15 H15B 108.5 . . ? C16 C15 H15A 110.3 . . ? C16 C15 H15B 110.3 . . ? N1 C16 C15 101.10(8) . . ? N1 C16 C17 110.86(9) . . ? N1 C16 C18 110.47(9) . . ? C17 C16 C15 108.23(9) . . ? C17 C16 C18 114.35(9) . . ? C18 C16 C15 111.01(9) . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C13 B1 Br1 111.67(7) . . ? C13 B1 C1 111.29(9) . . ? C1 B1 Br1 110.21(7) . . ? C4 B1 Br1 111.39(7) . . ? C4 B1 C13 97.38(8) . . ? C4 B1 C1 114.37(8) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 B1 2.0708(12) . ? N1 C13 1.3135(13) . ? N1 C9 1.4810(13) . ? N1 C16 1.5099(14) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 C22 1.5314(19) . ? C21 C20 1.5251(18) . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C22 C23 1.5329(16) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C23 C14 1.5408(15) . ? C14 C13 1.5011(14) . ? C14 C19 1.5572(15) . ? C14 C15 1.5409(15) . ? C13 B1 1.6042(16) . ? C9 C8 1.4057(13) . ? C9 C4 1.4139(14) . ? C8 C10 1.5230(15) . ? C8 C7 1.4115(15) . ? C10 H10 1.0000 . ? C10 C11 1.5342(16) . ? C10 C12 1.5394(15) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C1 H1 1.0000 . ? C1 C3 1.5288(16) . ? C1 C2 1.5312(16) . ? C1 B1 1.6362(16) . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 H3C 0.9800 . ? C2 H2A 0.9800 . ? C2 H2B 0.9800 . ? C2 H2C 0.9800 . ? C4 C5 1.3834(14) . ? C4 B1 1.5958(15) . ? C5 H5 0.9500 . ? C5 C6 1.3935(14) . ? C6 H6 0.9500 . ? C6 C7 1.3817(16) . ? C7 H7 0.9500 . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C20 C19 1.5321(15) . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C15 C16 1.5511(15) . ? C16 C17 1.5295(15) . ? C16 C18 1.5364(15) . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C13 B1 Br1 -129.20(8) . . . . ? N1 C13 B1 C1 107.17(10) . . . . ? N1 C13 B1 C4 -12.64(10) . . . . ? N1 C9 C8 C10 9.70(17) . . . . ? N1 C9 C8 C7 -172.81(10) . . . . ? N1 C9 C4 C5 175.06(9) . . . . ? N1 C9 C4 B1 -5.52(11) . . . . ? C21 C22 C23 C14 57.16(14) . . . . ? C21 C20 C19 C14 -57.07(13) . . . . ? C22 C21 C20 C19 55.31(14) . . . . ? C22 C23 C14 C13 -175.91(10) . . . . ? C22 C23 C14 C19 -56.85(13) . . . . ? C22 C23 C14 C15 68.84(13) . . . . ? C23 C14 C13 N1 -138.13(10) . . . . ? C23 C14 C13 B1 37.66(16) . . . . ? C23 C14 C19 C20 56.80(12) . . . . ? C23 C14 C15 C16 139.88(9) . . . . ? C14 C13 B1 Br1 54.98(14) . . . . ? C14 C13 B1 C1 -68.65(15) . . . . ? C14 C13 B1 C4 171.54(11) . . . . ? C14 C15 C16 N1 -15.11(11) . . . . ? C14 C15 C16 C17 -131.65(10) . . . . ? C14 C15 C16 C18 102.09(10) . . . . ? C13 N1 C9 C8 172.84(10) . . . . ? C13 N1 C9 C4 -3.40(11) . . . . ? C13 N1 C16 C15 5.33(11) . . . . ? C13 N1 C16 C17 119.91(10) . . . . ? C13 N1 C16 C18 -112.27(10) . . . . ? C13 C14 C19 C20 178.43(9) . . . . ? C13 C14 C15 C16 18.93(11) . . . . ? C9 N1 C13 C14 -172.24(8) . . . . ? C9 N1 C13 B1 10.81(11) . . . . ? C9 N1 C16 C15 -175.45(10) . . . . ? C9 N1 C16 C17 -60.87(14) . . . . ? C9 N1 C16 C18 66.95(13) . . . . ? C9 C8 C10 C11 -127.91(12) . . . . ? C9 C8 C10 C12 108.15(12) . . . . ? C9 C8 C7 C6 -1.82(15) . . . . ? C9 C4 C5 C6 -1.13(15) . . . . ? C9 C4 B1 Br1 127.23(8) . . . . ? C9 C4 B1 C13 10.44(10) . . . . ? C9 C4 B1 C1 -106.99(10) . . . . ? C8 C9 C4 C5 -1.55(15) . . . . ? C8 C9 C4 B1 177.87(9) . . . . ? C10 C8 C7 C6 176.03(10) . . . . ? C3 C1 B1 Br1 -176.99(7) . . . . ? C3 C1 B1 C13 -52.53(12) . . . . ? C3 C1 B1 C4 56.61(12) . . . . ? C2 C1 B1 Br1 60.52(10) . . . . ? C2 C1 B1 C13 -175.02(9) . . . . ? C2 C1 B1 C4 -65.88(12) . . . . ? C4 C9 C8 C10 -174.57(10) . . . . ? C4 C9 C8 C7 2.92(14) . . . . ? C4 C5 C6 C7 2.20(16) . . . . ? C5 C4 B1 Br1 -53.43(13) . . . . ? C5 C4 B1 C13 -170.22(10) . . . . ? C5 C4 B1 C1 72.35(14) . . . . ? C5 C6 C7 C8 -0.67(17) . . . . ? C7 C8 C10 C11 54.61(13) . . . . ? C7 C8 C10 C12 -69.32(12) . . . . ? C20 C21 C22 C23 -55.18(14) . . . . ? C19 C14 C13 N1 102.65(10) . . . . ? C19 C14 C13 B1 -81.55(14) . . . . ? C19 C14 C15 C16 -96.77(10) . . . . ? C15 C14 C13 N1 -16.30(11) . . . . ? C15 C14 C13 B1 159.49(11) . . . . ? C15 C14 C19 C20 -69.36(12) . . . . ? C16 N1 C13 C14 7.15(12) . . . . ? C16 N1 C13 B1 -169.80(8) . . . . ? C16 N1 C9 C8 -6.39(17) . . . . ? C16 N1 C9 C4 177.37(10) . . . . ? B1 C4 C5 C6 179.58(10) . . . . ?