#------------------------------------------------------------------------------ #$Date: 2024-10-04 01:13:05 +0300 (Fri, 04 Oct 2024) $ #$Revision: 295024 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/27/1572769.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572769 loop_ _publ_author_name 'Zhang, Chonghe' 'Gilliard, Robert J.' 'Cummins, Christopher' _publ_section_title ; Arene extrusion as an approach to reductive elimination at boron: Implication of carbene-ligated haloborylene as a transient reactive intermediate ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC05524A _journal_year 2024 _chemical_formula_moiety 'Br, C35 H53 B N' _chemical_formula_sum 'C35 H53 B Br N' _chemical_formula_weight 578.50 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2023-07-12 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-09-26 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 93.75(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.810(11) _cell_length_b 12.282(8) _cell_length_c 23.47(3) _cell_measurement_reflns_used 9764 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 31.058 _cell_measurement_theta_min 2.406 _cell_volume 3109(5) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2018)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2018)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100.00 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0401 _diffrn_reflns_av_unetI/netI 0.0154 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -34 _diffrn_reflns_number 207305 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.069 _diffrn_reflns_theta_min 1.739 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.346 _exptl_absorpt_correction_T_max 0.7462 _exptl_absorpt_correction_T_min 0.6659 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0948 before and 0.0545 after correction. The Ratio of minimum to maximum transmission is 0.8924. The \l/2 correction factor is Not present. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.236 _exptl_crystal_description block _exptl_crystal_F_000 1240 _exptl_crystal_size_max 0.091 _exptl_crystal_size_mid 0.054 _exptl_crystal_size_min 0.023 _refine_diff_density_max 0.955 _refine_diff_density_min -0.288 _refine_diff_density_rms 0.098 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.100 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 355 _refine_ls_number_reflns 9960 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.100 _refine_ls_R_factor_all 0.0345 _refine_ls_R_factor_gt 0.0289 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0472P)^2^+0.8465P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0800 _refine_ls_wR_factor_ref 0.0822 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8747 _reflns_number_total 9960 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05524a3.cif _cod_data_source_block 7 _cod_original_cell_volume 3110(5) _cod_database_code 1572769 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.970 _shelx_estimated_absorpt_t_min 0.887 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C33(H33), C30(H30) 2.b Secondary CH2 refined with riding coordinates: C21(H21A,H21B), C20(H20A,H20B), C19(H19A,H19B), C15(H15A,H15B), C18(H18A, H18B), C17(H17A,H17B) 2.c Aromatic/amide H refined with riding coordinates: C27(H27), C26(H26), C28(H28) 2.d Idealised Me refined as rotating group: C35(H35A,H35B,H35C), C23(H23A,H23B,H23C), C22(H22A,H22B,H22C), C12(H12A,H12B, H12C), C11(H11A,H11B,H11C), C8(H8A,H8B,H8C), C7(H7A,H7B,H7C), C5(H5A,H5B,H5C), C6(H6A,H6B,H6C), C32(H32A,H32B,H32C), C31(H31A,H31B,H31C), C34(H34A,H34B,H34C) ; _shelx_res_file ; TITL mo_P8_23089_0m_a.res in P2(1)/c mo_p8_23089_0m_a.res created by SHELXL-2016/6 at 22:50:47 on 12-Jul-2023 CELL 0.71073 10.8102 12.282 23.4727 90 93.752 90 ZERR 4 0.0106 0.008 0.0266 0 0.046 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H B Br N UNIT 140 212 4 4 4 L.S. 10 PLAN 5 0 0 SIZE 0.054 0.023 0.091 TEMP -173.15 CONF HTAB BOND $H fmap 2 acta MORE -1 REM REM REM WGHT 0.047200 0.846500 FVAR 0.31094 BR01 4 0.194811 0.733781 0.304966 11.00000 0.02003 0.01855 = 0.02183 0.00337 -0.00165 0.00046 N1 5 0.156445 0.355612 0.366448 11.00000 0.01031 0.01593 = 0.01001 -0.00092 0.00036 -0.00056 C27 1 0.275319 0.342269 0.542147 11.00000 0.03225 0.02963 = 0.01050 0.00104 -0.00174 -0.00467 AFIX 43 H27 2 0.306216 0.339106 0.580943 11.00000 -1.20000 AFIX 0 C26 1 0.223088 0.250870 0.515792 11.00000 0.03192 0.02495 = 0.01342 0.00485 0.00197 -0.00541 AFIX 43 H26 2 0.217200 0.185614 0.537175 11.00000 -1.20000 AFIX 0 C25 1 0.178743 0.252198 0.458435 11.00000 0.01807 0.01996 = 0.01271 -0.00004 0.00349 -0.00364 C24 1 0.192205 0.349576 0.427768 11.00000 0.01243 0.01896 = 0.00869 -0.00159 0.00165 -0.00096 C13 1 0.227619 0.324959 0.326214 11.00000 0.01061 0.01308 = 0.01043 -0.00134 0.00076 -0.00236 C14 1 0.179356 0.373732 0.268634 11.00000 0.01160 0.01599 = 0.00918 -0.00046 0.00072 0.00130 C21 1 0.146159 0.290754 0.220465 11.00000 0.01457 0.01748 = 0.01104 -0.00208 -0.00007 -0.00014 AFIX 23 H21A 2 0.217552 0.241595 0.216229 11.00000 -1.20000 H21B 2 0.075135 0.245867 0.231048 11.00000 -1.20000 AFIX 0 C20 1 0.112622 0.347637 0.163192 11.00000 0.01851 0.02545 = 0.01101 -0.00163 -0.00115 0.00087 AFIX 23 H20A 2 0.097067 0.291955 0.133077 11.00000 -1.20000 H20B 2 0.035374 0.389986 0.166120 11.00000 -1.20000 AFIX 0 C19 1 0.215665 0.423700 0.146272 11.00000 0.02350 0.02439 = 0.01106 0.00296 0.00204 0.00190 AFIX 23 H19A 2 0.188627 0.462285 0.110574 11.00000 -1.20000 H19B 2 0.290289 0.380444 0.139007 11.00000 -1.20000 AFIX 0 C35 1 0.179272 0.045527 0.447726 11.00000 0.02924 0.02111 = 0.02632 0.00289 0.01013 -0.00302 AFIX 137 H35A 2 0.263544 0.051099 0.434943 11.00000 -1.50000 H35B 2 0.135500 -0.014358 0.427523 11.00000 -1.50000 H35C 2 0.183177 0.031474 0.488902 11.00000 -1.50000 AFIX 0 C33 1 0.109798 0.152489 0.434910 11.00000 0.02020 0.01965 = 0.01705 -0.00056 0.00517 -0.00588 AFIX 13 H33 2 0.096091 0.160557 0.392575 11.00000 -1.20000 AFIX 0 C28 1 0.282280 0.438293 0.511664 11.00000 0.02387 0.02285 = 0.01252 -0.00321 -0.00064 -0.00350 AFIX 43 H28 2 0.315871 0.501263 0.530400 11.00000 -1.20000 AFIX 0 C29 1 0.241162 0.445140 0.453972 11.00000 0.01533 0.01736 = 0.01156 -0.00223 0.00118 -0.00096 C16 1 0.029193 0.397274 0.341973 11.00000 0.00993 0.02539 = 0.01301 -0.00276 0.00005 0.00290 C23 1 -0.029734 0.482506 0.378859 11.00000 0.01604 0.03863 = 0.01870 -0.00814 0.00139 0.00975 AFIX 137 H23A 2 0.016787 0.550821 0.377379 11.00000 -1.50000 H23B 2 -0.028103 0.456670 0.418403 11.00000 -1.50000 H23C 2 -0.115773 0.494825 0.364511 11.00000 -1.50000 AFIX 0 C22 1 -0.056801 0.298487 0.334675 11.00000 0.01245 0.03516 = 0.01834 -0.00087 0.00095 -0.00493 AFIX 137 H22A 2 -0.131322 0.318685 0.311014 11.00000 -1.50000 H22B 2 -0.080472 0.274160 0.372208 11.00000 -1.50000 H22C 2 -0.013645 0.239394 0.316134 11.00000 -1.50000 AFIX 0 C15 1 0.065385 0.440889 0.284339 11.00000 0.01328 0.02038 = 0.01284 -0.00040 -0.00012 0.00503 AFIX 23 H15A 2 0.086561 0.519198 0.287262 11.00000 -1.20000 H15B 2 -0.003818 0.431658 0.254974 11.00000 -1.20000 AFIX 0 B1 3 0.342593 0.244006 0.338935 11.00000 0.01169 0.01395 = 0.01128 -0.00087 0.00133 -0.00008 C1 1 0.501514 0.255821 0.319532 11.00000 0.01033 0.01540 = 0.01610 0.00036 0.00165 0.00167 C4 1 0.467717 0.243457 0.380832 11.00000 0.01177 0.01645 = 0.01284 -0.00164 -0.00056 0.00039 C10 1 0.489371 0.127907 0.401745 11.00000 0.01413 0.01768 = 0.01387 0.00084 0.00072 0.00238 C12 1 0.583816 0.103998 0.449949 11.00000 0.02253 0.02489 = 0.01916 0.00243 -0.00533 0.00388 AFIX 137 H12A 2 0.587268 0.025320 0.456821 11.00000 -1.50000 H12B 2 0.560410 0.141273 0.484556 11.00000 -1.50000 H12C 2 0.665368 0.129805 0.439910 11.00000 -1.50000 AFIX 0 C9 1 0.425438 0.057095 0.368203 11.00000 0.01558 0.01571 = 0.01411 0.00152 0.00191 0.00181 C11 1 0.431695 -0.064892 0.369714 11.00000 0.02473 0.01522 = 0.02180 0.00156 0.00050 0.00248 AFIX 137 H11A 2 0.470686 -0.091368 0.335817 11.00000 -1.50000 H11B 2 0.347689 -0.094726 0.370192 11.00000 -1.50000 H11C 2 0.480796 -0.088275 0.404122 11.00000 -1.50000 AFIX 0 C3 1 0.350640 0.115174 0.320225 11.00000 0.01362 0.01300 = 0.01327 -0.00091 0.00109 -0.00038 C8 1 0.246516 0.050283 0.289812 11.00000 0.01790 0.01484 = 0.01837 -0.00230 -0.00123 -0.00201 AFIX 137 H8A 2 0.204291 0.095481 0.260127 11.00000 -1.50000 H8B 2 0.187150 0.027986 0.317394 11.00000 -1.50000 H8C 2 0.280919 -0.014491 0.272289 11.00000 -1.50000 AFIX 0 C2 1 0.435565 0.181529 0.284712 11.00000 0.01236 0.01463 = 0.01346 -0.00081 0.00237 0.00247 C7 1 0.445096 0.173544 0.221103 11.00000 0.01906 0.02175 = 0.01298 -0.00136 0.00449 0.00323 AFIX 137 H7A 2 0.427306 0.244748 0.203591 11.00000 -1.50000 H7B 2 0.385111 0.119957 0.205260 11.00000 -1.50000 H7C 2 0.529071 0.150733 0.213081 11.00000 -1.50000 AFIX 0 C5 1 0.512874 0.332844 0.421339 11.00000 0.01797 0.02075 = 0.02037 -0.00665 -0.00435 0.00016 AFIX 137 H5A 2 0.470840 0.326868 0.456953 11.00000 -1.50000 H5B 2 0.494487 0.403884 0.403756 11.00000 -1.50000 H5C 2 0.602560 0.325706 0.429558 11.00000 -1.50000 AFIX 0 C6 1 0.585055 0.343185 0.299765 11.00000 0.01345 0.02074 = 0.02532 0.00293 0.00178 -0.00275 AFIX 137 H6A 2 0.612043 0.324361 0.261949 11.00000 -1.50000 H6B 2 0.657646 0.349875 0.326812 11.00000 -1.50000 H6C 2 0.540213 0.412561 0.297583 11.00000 -1.50000 AFIX 0 C18 1 0.247982 0.506986 0.193458 11.00000 0.02267 0.01946 = 0.01479 0.00390 0.00192 0.00013 AFIX 23 H18A 2 0.175677 0.554825 0.198218 11.00000 -1.20000 H18B 2 0.317645 0.553051 0.182405 11.00000 -1.20000 AFIX 0 C17 1 0.284357 0.449605 0.250222 11.00000 0.01453 0.01630 = 0.01371 0.00072 0.00145 -0.00145 AFIX 23 H17A 2 0.302792 0.504945 0.280250 11.00000 -1.20000 H17B 2 0.360442 0.406193 0.246163 11.00000 -1.20000 AFIX 0 C30 1 0.247924 0.555786 0.424720 11.00000 0.01842 0.01543 = 0.01496 -0.00151 0.00004 0.00042 AFIX 13 H30 2 0.206120 0.549178 0.385592 11.00000 -1.20000 AFIX 0 C32 1 0.380525 0.596471 0.418560 11.00000 0.02003 0.01850 = 0.02556 0.00096 0.00011 -0.00245 AFIX 137 H32A 2 0.429140 0.587779 0.455000 11.00000 -1.50000 H32B 2 0.378438 0.673548 0.407741 11.00000 -1.50000 H32C 2 0.418720 0.554083 0.389001 11.00000 -1.50000 AFIX 0 C31 1 0.177454 0.641716 0.457713 11.00000 0.02775 0.02204 = 0.02110 -0.00645 0.00060 0.00456 AFIX 137 H31A 2 0.096011 0.612948 0.466014 11.00000 -1.50000 H31B 2 0.166676 0.707816 0.434533 11.00000 -1.50000 H31C 2 0.224828 0.659072 0.493588 11.00000 -1.50000 AFIX 0 C34 1 -0.017092 0.147271 0.460786 11.00000 0.02331 0.02870 = 0.02555 -0.00104 0.00963 -0.00823 AFIX 137 H34A 2 -0.005328 0.131162 0.501673 11.00000 -1.50000 H34B 2 -0.067436 0.089879 0.441775 11.00000 -1.50000 H34C 2 -0.059398 0.217446 0.455405 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_P8_23089_0m_a.res in P2(1)/c REM R1 = 0.0289 for 8747 Fo > 4sig(Fo) and 0.0345 for all 9960 data REM 355 parameters refined using 0 restraints END WGHT 0.0472 0.8465 REM Instructions for potential hydrogen bonds EQIV $1 -x, y-1/2, -z+1/2 HTAB C22 Br01_$1 HTAB C15 Br01 REM Highest difference peak 0.955, deepest hole -0.288, 1-sigma level 0.098 Q1 1 0.1319 0.7470 0.2844 11.00000 0.05 0.96 Q2 1 0.2208 0.7910 0.3123 11.00000 0.05 0.86 Q3 1 0.1733 0.3029 0.4439 11.00000 0.05 0.60 Q4 1 0.4818 0.1845 0.3929 11.00000 0.05 0.58 Q5 1 0.4959 0.2832 0.4008 11.00000 0.05 0.58 ; _shelx_res_checksum 61302 _shelx_hkl_file ; 1 0 0 32.27 1.15 1 0 0 32.91 1.17 1 0 0 29.62 1.13 1 0 0 32.06 1.10 1 0 0 35.63 1.15 1 0 0 32.27 1.07 1 0 0 33.85 1.10 1 0 0 32.34 1.11 -1 0 0 32.69 1.12 -1 0 0 34.35 1.16 -1 0 0 30.01 1.15 -1 0 0 32.27 1.14 -1 0 0 34.68 1.11 -1 0 0 32.44 1.14 -1 0 0 33.67 1.07 -1 0 0 36.07 1.11 -1 0 0 33.20 1.14 2 0 0 1968.28 52.91 2 0 0 1568.49 52.85 2 0 0 1859.47 52.85 2 0 0 1554.23 52.89 2 0 0 1541.78 52.86 2 0 0 1813.39 52.77 2 0 0 1919.95 52.92 -2 0 0 1951.88 52.90 -2 0 0 1576.02 52.83 -2 0 0 1629.64 52.76 -2 0 0 1482.12 52.85 -2 0 0 1593.77 52.88 -2 0 0 1987.19 52.93 -2 0 0 1481.95 52.88 -2 0 0 1505.14 52.86 3 0 0 8215.98 224.31 3 0 0 7605.20 224.24 -3 0 0 6408.75 224.07 -3 0 0 6460.91 224.15 3 0 0 7510.47 224.30 -3 0 0 7608.42 224.20 -3 0 0 7505.90 224.29 3 0 0 7365.01 224.29 3 0 0 6647.63 224.33 3 0 0 6738.95 224.23 4 0 0 1221.12 37.88 4 0 0 1209.67 37.84 4 0 0 1223.59 37.78 -4 0 0 1226.74 37.89 -4 0 0 1181.09 37.75 4 0 0 1193.06 37.76 -4 0 0 1255.45 37.94 -4 0 0 1196.28 37.80 4 0 0 1200.70 37.74 4 0 0 1184.24 37.90 4 0 0 1273.11 37.95 4 0 0 1218.61 37.93 4 0 0 1218.35 37.88 -4 0 0 1199.28 37.86 -4 0 0 1167.85 37.84 -4 0 0 1196.30 37.76 -4 0 0 1184.82 37.91 -4 0 0 1231.22 37.65 -4 0 0 1138.57 37.91 -5 0 0 2315.18 73.22 -5 0 0 2332.25 73.25 5 0 0 2325.90 73.06 5 0 0 2381.43 73.19 -5 0 0 2300.48 73.29 5 0 0 2276.99 73.08 5 0 0 2354.53 73.24 -5 0 0 2351.77 72.94 5 0 0 2423.76 73.31 5 0 0 2362.66 73.31 5 0 0 2356.44 73.23 -5 0 0 2345.50 73.15 5 0 0 2311.17 73.10 5 0 0 2330.60 73.27 -5 0 0 2315.02 73.34 -5 0 0 2330.81 73.09 -5 0 0 2306.88 73.21 -5 0 0 2396.36 73.30 -5 0 0 2321.41 73.29 -5 0 0 2378.06 73.11 6 0 0 79.64 3.24 6 0 0 92.05 3.81 6 0 0 83.48 3.63 6 0 0 90.60 3.71 6 0 0 86.20 3.34 6 0 0 83.07 3.61 -6 0 0 85.12 3.73 6 0 0 89.62 3.61 6 0 0 94.07 3.26 6 0 0 88.95 3.25 -6 0 0 90.62 3.83 -6 0 0 91.50 3.85 -6 0 0 89.21 3.27 -6 0 0 81.62 3.61 -6 0 0 83.42 3.53 -6 0 0 84.82 3.06 -6 0 0 81.98 3.40 -6 0 0 84.73 3.57 -6 0 0 84.61 3.83 -6 0 0 85.89 3.67 -7 0 0 190.44 6.94 7 0 0 204.98 6.79 -7 0 0 201.40 6.84 7 0 0 196.29 7.21 -7 0 0 205.48 7.30 -7 0 0 202.10 7.11 7 0 0 195.75 7.12 7 0 0 205.56 6.91 -7 0 0 206.55 7.40 -7 0 0 196.80 7.35 7 0 0 185.51 6.78 7 0 0 202.77 7.30 7 0 0 203.25 6.77 -7 0 0 207.95 7.11 -7 0 0 199.96 6.56 -7 0 0 200.44 7.21 -7 0 0 193.76 7.11 -7 0 0 203.62 7.80 7 0 0 196.69 7.45 7 0 0 194.64 7.11 7 0 0 205.78 7.38 8 0 0 449.21 14.08 8 0 0 441.24 14.07 8 0 0 402.13 14.10 -8 0 0 445.48 14.68 -8 0 0 456.11 14.76 8 0 0 430.12 14.64 8 0 0 445.68 14.47 -8 0 0 416.57 14.55 -8 0 0 436.40 14.71 -8 0 0 439.64 14.13 -8 0 0 421.25 14.28 -8 0 0 439.20 14.47 8 0 0 423.73 14.14 8 0 0 428.73 14.54 9 0 0 19.93 2.50 9 0 0 19.39 2.23 9 0 0 22.46 2.23 9 0 0 15.91 1.89 9 0 0 12.01 2.22 9 0 0 20.24 3.02 9 0 0 26.53 3.22 -9 0 0 17.41 2.23 -9 0 0 22.44 1.76 -9 0 0 16.03 2.55 -9 0 0 19.48 2.77 -9 0 0 14.76 2.30 10 0 0 147.16 5.68 -10 0 0 149.56 7.00 -10 0 0 135.41 6.31 10 0 0 148.61 6.65 10 0 0 161.70 6.59 -10 0 0 145.69 5.15 10 0 0 144.00 7.36 10 0 0 145.49 5.96 -10 0 0 156.77 7.06 10 0 0 143.01 5.79 -10 0 0 153.42 6.57 10 0 0 143.31 5.94 -11 0 0 62.81 5.83 -11 0 0 59.16 3.27 -11 0 0 60.79 4.65 11 0 0 59.00 4.57 11 0 0 55.04 3.69 -11 0 0 67.55 5.21 -11 0 0 75.04 5.06 11 0 0 66.02 5.12 11 0 0 54.88 3.98 11 0 0 65.23 4.24 11 0 0 55.74 6.50 12 0 0 4.37 2.61 -12 0 0 4.54 6.18 12 0 0 5.34 3.35 12 0 0 4.10 4.71 12 0 0 0.70 2.60 12 0 0 2.42 2.32 12 0 0 5.04 3.61 -12 0 0 2.70 3.99 -12 0 0 6.42 6.71 -12 0 0 6.20 3.19 13 0 0 392.69 14.77 -13 0 0 373.81 15.47 -13 0 0 373.67 14.59 -13 0 0 378.79 14.26 13 0 0 386.82 13.66 13 0 0 402.00 14.69 -13 0 0 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63.99 3.90 10 -3 0 69.49 4.47 10 -3 0 77.09 3.59 10 -3 0 72.75 4.13 10 -3 0 67.27 3.70 -10 -3 0 77.92 5.37 -10 -3 0 65.42 4.81 -10 -3 0 71.52 5.09 -10 3 0 70.06 3.80 10 3 0 70.64 3.86 10 3 0 68.62 5.22 -10 3 0 74.18 4.32 10 3 0 81.30 4.56 -10 3 0 76.53 5.73 -10 3 0 68.36 5.36 -10 3 0 68.98 4.94 10 3 0 83.03 4.26 -10 3 0 71.75 6.59 10 3 0 67.66 3.79 10 3 0 76.05 4.87 11 -3 0 143.75 6.14 -11 -3 0 132.88 7.08 11 -3 0 146.78 6.29 11 -3 0 144.34 5.68 11 -3 0 139.35 7.04 -11 -3 0 125.80 7.27 -11 -3 0 141.35 6.89 -11 -3 0 145.05 7.59 11 -3 0 142.84 6.06 11 -3 0 125.34 8.10 11 3 0 136.46 5.81 11 3 0 142.11 7.52 -11 3 0 156.10 6.74 -11 3 0 143.17 5.88 -11 3 0 156.11 7.84 11 3 0 154.98 6.63 11 3 0 146.20 6.02 11 3 0 139.78 6.67 11 3 0 153.56 7.98 -11 3 0 145.92 7.13 -11 3 0 133.96 7.42 12 -3 0 119.86 5.76 -12 -3 0 115.91 7.37 -12 -3 0 139.76 7.06 12 -3 0 117.48 6.31 -12 -3 0 119.89 7.75 12 -3 0 131.12 6.07 12 -3 0 137.06 5.89 12 -3 0 128.71 7.75 -12 -3 0 129.30 8.18 12 -3 0 127.46 7.42 -12 3 0 135.30 8.39 12 3 0 128.26 6.87 -12 3 0 129.29 5.72 12 3 0 135.61 5.97 12 3 0 131.59 6.07 -12 3 0 135.68 7.28 12 3 0 121.84 8.49 12 3 0 120.47 6.42 12 3 0 131.36 7.49 -12 3 0 131.80 6.91 -12 3 0 126.53 8.59 13 -3 0 18.91 4.68 13 -3 0 23.60 3.32 -13 -3 0 22.19 4.28 13 -3 0 17.26 5.05 13 -3 0 16.05 3.47 -13 -3 0 17.20 5.06 13 -3 0 21.90 3.18 -13 -3 0 29.68 4.80 -13 -3 0 14.77 5.68 13 -3 0 20.72 3.61 13 3 0 16.97 3.25 -13 3 0 26.36 5.74 -13 3 0 19.80 5.67 -13 3 0 16.66 4.51 13 3 0 18.29 3.34 13 3 0 17.38 4.12 -13 3 0 14.06 4.55 13 3 0 15.40 4.58 -13 3 0 21.54 3.34 13 3 0 13.07 5.63 -14 -3 0 118.38 9.69 14 -3 0 119.54 9.82 -14 -3 0 99.19 9.03 14 -3 0 115.01 9.17 14 -3 0 106.82 7.30 14 -3 0 117.19 6.65 14 -3 0 114.03 6.97 -14 -3 0 117.51 9.20 -14 -3 0 115.28 8.47 14 3 0 128.52 8.98 -14 3 0 126.42 10.96 -14 3 0 122.11 9.37 14 3 0 135.07 8.15 -14 3 0 106.07 8.43 -14 3 0 118.42 8.18 -14 3 0 117.13 8.60 -14 3 0 124.35 10.95 14 3 0 105.81 8.57 15 -3 0 3.32 4.65 15 -3 0 2.57 6.66 -15 -3 0 10.71 7.55 15 -3 0 4.88 4.02 -15 -3 0 8.85 6.78 15 -3 0 5.46 6.21 -15 -3 0 9.65 6.92 -15 3 0 8.55 6.41 -15 3 0 13.90 7.49 15 3 0 5.08 5.18 15 3 0 9.04 4.20 15 3 0 9.84 4.49 15 3 0 8.17 10.79 -15 3 0 4.63 6.10 15 3 0 13.15 5.58 -15 3 0 6.49 7.70 -15 3 0 11.85 5.69 0 -4 0 67.09 2.15 0 -4 0 60.64 2.41 0 -4 0 69.14 2.43 0 -4 0 68.91 2.52 0 -4 0 65.09 2.15 0 -4 0 62.48 2.29 0 -4 0 61.92 2.41 0 -4 0 67.05 2.52 0 -4 0 63.69 2.17 0 -4 0 64.65 2.42 0 -4 0 66.05 2.16 0 4 0 65.19 2.45 0 4 0 65.39 2.18 0 4 0 64.61 2.47 0 4 0 65.54 2.14 0 4 0 68.70 2.15 0 4 0 66.84 2.16 1 -4 0 283.56 8.91 1 -4 0 282.13 8.83 -1 -4 0 277.50 9.01 1 -4 0 274.74 9.02 1 -4 0 280.80 8.80 1 -4 0 278.57 8.86 1 -4 0 287.20 8.90 1 -4 0 282.64 8.91 1 -4 0 276.06 8.91 1 -4 0 283.42 8.96 -1 -4 0 283.47 9.01 1 -4 0 275.06 8.86 1 -4 0 285.43 9.08 -1 -4 0 292.46 9.01 1 -4 0 280.26 9.04 1 -4 0 275.70 8.91 -1 -4 0 272.25 8.99 -1 4 0 287.32 9.03 -1 4 0 273.01 8.92 -1 4 0 280.62 8.93 1 4 0 281.66 8.99 -1 4 0 282.52 8.90 -1 4 0 274.26 8.89 -1 4 0 273.51 9.05 -1 4 0 274.18 8.88 1 4 0 259.42 8.99 1 4 0 290.27 9.04 2 -4 0 1286.71 39.33 -2 -4 0 1328.03 39.17 2 -4 0 1264.97 39.11 2 -4 0 1239.67 39.33 2 -4 0 1262.93 39.37 -2 -4 0 1221.60 39.41 2 -4 0 1183.22 39.39 -2 -4 0 1272.73 39.39 2 -4 0 1263.82 39.28 2 -4 0 1294.27 39.29 -2 -4 0 1258.21 39.37 -2 -4 0 1277.78 39.16 -2 -4 0 1292.63 39.31 -2 -4 0 1252.13 39.18 -2 -4 0 1259.71 39.16 2 -4 0 1252.71 39.37 2 -4 0 1270.29 39.36 -2 -4 0 1253.20 39.33 2 -4 0 1306.58 39.45 2 -4 0 1292.76 39.22 2 -4 0 1257.94 39.37 2 4 0 1239.13 39.36 -2 4 0 1263.77 39.34 2 4 0 1219.54 39.40 2 4 0 1237.87 39.20 2 4 0 1244.58 39.15 -2 4 0 1254.24 39.26 -2 4 0 1187.53 39.34 -2 4 0 1248.64 39.45 -2 4 0 1242.09 39.39 2 4 0 1243.58 39.13 2 4 0 1181.69 39.35 -2 4 0 1294.43 39.25 -2 4 0 1212.64 39.35 -2 4 0 1268.87 39.23 -2 4 0 1264.57 39.31 2 4 0 1283.79 39.28 -2 4 0 1263.61 39.43 -2 4 0 1267.37 39.12 3 -4 0 493.49 16.65 3 -4 0 527.34 16.88 3 -4 0 518.77 16.52 -3 -4 0 515.18 16.72 -3 -4 0 518.38 16.67 -3 -4 0 524.29 16.47 -3 -4 0 535.19 16.49 -3 -4 0 523.55 16.49 -3 -4 0 518.51 16.50 3 -4 0 524.43 16.48 3 -4 0 521.45 16.57 3 -4 0 517.57 16.69 -3 -4 0 545.43 16.64 3 -4 0 508.84 16.64 -3 -4 0 540.84 16.42 3 -4 0 532.23 16.66 -3 -4 0 546.61 16.50 -3 -4 0 507.07 16.51 -3 -4 0 530.64 16.40 3 -4 0 552.76 16.73 3 -4 0 518.50 16.69 -3 4 0 524.26 16.60 -3 4 0 528.86 16.57 -3 4 0 509.62 16.67 -3 4 0 524.09 16.77 -3 4 0 531.83 16.68 -3 4 0 541.12 16.90 3 4 0 515.75 16.61 -3 4 0 504.36 16.67 -3 4 0 526.28 16.94 3 4 0 536.63 16.50 3 4 0 508.99 16.62 -3 4 0 522.00 16.37 -3 4 0 519.63 16.56 -3 4 0 516.77 16.49 3 4 0 521.75 16.48 3 4 0 504.61 16.66 3 4 0 523.45 16.48 4 -4 0 441.57 14.83 -4 -4 0 473.54 14.61 -4 -4 0 459.72 14.77 -4 -4 0 461.59 14.73 4 -4 0 459.44 14.69 -4 -4 0 461.84 14.79 -4 -4 0 451.26 14.94 4 -4 0 454.02 14.93 4 -4 0 465.18 14.98 -4 -4 0 461.02 14.61 4 -4 0 480.57 15.00 4 -4 0 480.48 14.91 -4 -4 0 471.90 14.59 -4 -4 0 472.41 14.72 4 -4 0 472.51 14.70 -4 -4 0 460.69 14.74 4 -4 0 458.44 14.87 -4 -4 0 467.12 14.74 -4 -4 0 468.46 14.67 -4 -4 0 455.76 14.85 4 -4 0 444.96 14.86 4 -4 0 459.99 14.79 4 4 0 456.16 14.71 4 4 0 466.64 14.87 -4 4 0 485.41 14.82 -4 4 0 458.04 14.94 -4 4 0 472.08 14.57 4 4 0 469.46 14.74 4 4 0 471.86 14.74 -4 4 0 463.92 14.76 -4 4 0 460.97 14.96 -4 4 0 471.37 14.87 -4 4 0 465.59 14.92 4 4 0 446.91 14.67 -4 4 0 443.14 14.91 4 4 0 436.24 14.78 -4 4 0 463.08 15.02 -4 4 0 457.03 14.83 -4 4 0 455.48 14.95 4 4 0 471.88 14.78 -5 -4 0 236.69 7.80 -5 -4 0 234.04 7.66 -5 -4 0 229.82 7.84 5 -4 0 231.38 7.93 5 -4 0 244.07 7.98 5 -4 0 242.75 8.26 -5 -4 0 238.24 7.92 -5 -4 0 242.54 7.55 -5 -4 0 237.71 7.90 -5 -4 0 240.13 7.75 -5 -4 0 225.15 7.85 5 -4 0 235.52 7.89 5 -4 0 219.06 7.99 -5 -4 0 237.05 7.96 -5 -4 0 236.61 7.88 -5 -4 0 233.19 8.09 5 -4 0 247.13 8.26 5 -4 0 230.86 8.12 5 -4 0 244.58 7.83 5 -4 0 228.98 7.75 -5 4 0 233.38 7.99 -5 4 0 238.27 7.66 5 4 0 236.98 7.84 5 4 0 239.14 7.81 -5 4 0 231.59 8.13 5 4 0 234.79 7.84 -5 4 0 238.39 8.13 5 4 0 237.91 7.54 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328.60 11.85 7 -4 0 340.28 11.29 -7 -4 0 339.99 11.49 7 -4 0 350.28 11.14 -7 -4 0 327.86 11.01 7 -4 0 343.89 11.29 -7 -4 0 335.92 11.40 7 -4 0 346.31 11.30 7 -4 0 351.99 11.55 -7 -4 0 319.20 11.61 7 -4 0 327.40 11.25 7 4 0 339.83 11.38 7 4 0 337.65 11.01 7 4 0 345.15 10.93 -7 4 0 336.56 11.22 -7 4 0 337.42 11.19 7 4 0 328.76 11.27 -7 4 0 322.60 11.71 -7 4 0 357.66 11.68 7 4 0 335.18 11.06 -7 4 0 341.16 11.82 -7 4 0 353.81 11.90 7 4 0 346.52 11.43 -7 4 0 345.43 11.10 -8 -4 0 247.57 9.09 -8 -4 0 261.94 9.20 8 -4 0 249.15 8.85 -8 -4 0 254.40 8.64 -8 -4 0 257.35 9.10 8 -4 0 248.04 8.62 8 -4 0 255.61 8.84 8 -4 0 258.38 9.72 -8 -4 0 250.69 9.21 8 -4 0 246.46 9.34 8 -4 0 263.78 8.88 8 -4 0 251.02 8.98 8 -4 0 267.42 9.21 -8 -4 0 243.55 8.95 8 4 0 251.74 8.96 8 4 0 257.65 8.89 8 4 0 259.11 8.94 -8 4 0 269.36 8.88 8 4 0 252.32 9.06 -8 4 0 245.28 9.62 -8 4 0 262.00 9.39 -8 4 0 258.25 8.79 -8 4 0 260.88 9.15 -8 4 0 247.73 8.71 8 4 0 245.26 8.62 8 4 0 260.00 8.49 8 4 0 250.84 8.62 9 -4 0 4.14 2.14 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725.20 21.87 2 -5 0 675.91 21.93 -2 5 0 689.21 21.77 -2 5 0 698.38 21.68 2 5 0 706.23 21.81 -2 5 0 696.71 21.84 -2 5 0 682.74 21.96 -2 5 0 695.33 21.67 -2 5 0 687.80 21.81 -2 5 0 683.09 21.80 2 5 0 689.81 21.94 -2 5 0 667.64 21.82 -2 5 0 703.39 21.88 -2 5 0 666.95 21.98 2 5 0 700.52 21.91 2 5 0 705.07 21.90 -3 -5 0 5.53 0.87 3 -5 0 6.50 1.06 -3 -5 0 6.77 0.87 3 -5 0 3.63 0.88 -3 -5 0 7.25 0.65 -3 -5 0 6.15 0.89 -3 -5 0 4.64 1.03 3 -5 0 7.25 0.80 -3 -5 0 4.20 1.24 -3 -5 0 5.91 0.72 3 -5 0 5.84 0.90 -3 -5 0 5.87 0.67 3 -5 0 4.99 0.74 3 -5 0 8.00 1.10 3 -5 0 5.58 1.09 -3 -5 0 5.34 0.70 3 -5 0 4.55 1.15 -3 -5 0 6.34 0.94 -3 -5 0 6.07 1.03 3 -5 0 5.29 1.10 3 -5 0 7.53 1.09 3 -5 0 5.03 0.83 -3 5 0 7.87 0.94 3 5 0 4.36 1.11 -3 5 0 6.18 0.60 3 5 0 8.22 0.98 3 5 0 5.91 0.64 3 5 0 5.70 0.77 -3 5 0 6.28 1.10 -3 5 0 6.28 1.15 3 5 0 4.97 0.87 -3 5 0 5.01 0.93 3 5 0 7.51 1.03 -3 5 0 4.91 1.07 3 5 0 5.86 0.74 -3 5 0 5.72 1.28 -3 5 0 7.36 0.98 -3 5 0 6.45 0.84 -3 5 0 7.58 1.04 -3 5 0 5.86 0.74 -4 -5 0 393.05 12.77 -4 -5 0 408.05 12.83 -4 -5 0 409.46 12.82 4 -5 0 394.47 13.04 -4 -5 0 411.83 12.78 -4 -5 0 398.02 12.89 4 -5 0 401.49 13.05 4 -5 0 405.38 12.86 4 -5 0 406.54 13.09 -4 -5 0 400.18 13.15 4 -5 0 389.78 12.81 -4 -5 0 401.54 12.84 4 -5 0 397.90 13.11 -4 -5 0 407.53 12.73 4 -5 0 396.35 12.95 -4 -5 0 402.20 12.85 4 -5 0 423.89 13.16 4 -5 0 392.00 13.16 -4 5 0 418.79 13.12 -4 5 0 397.20 12.96 4 5 0 404.17 12.83 -4 5 0 402.58 13.22 -4 5 0 374.18 13.07 4 5 0 406.77 13.02 4 5 0 402.02 12.81 4 5 0 401.15 12.83 -4 5 0 400.41 12.93 4 5 0 396.37 13.07 -4 5 0 412.07 12.66 -4 5 0 410.00 12.99 -4 5 0 413.24 12.97 -4 5 0 397.82 13.12 4 5 0 396.52 12.99 5 -5 0 122.52 4.26 -5 -5 0 122.52 4.47 5 -5 0 129.82 4.57 -5 -5 0 121.67 4.21 -5 -5 0 114.73 4.34 5 -5 0 114.43 4.56 -5 -5 0 121.71 4.72 -5 -5 0 124.71 4.45 -5 -5 0 116.59 4.27 -5 -5 0 115.01 4.62 -5 -5 0 125.00 4.38 5 -5 0 116.00 4.86 -5 -5 0 118.34 4.12 5 -5 0 121.05 4.43 5 -5 0 123.23 4.96 5 -5 0 125.81 4.79 5 -5 0 119.80 4.73 -5 -5 0 117.52 4.58 5 -5 0 118.98 4.31 -5 -5 0 123.70 4.14 5 -5 0 123.10 5.00 5 5 0 114.37 4.43 5 5 0 122.40 4.48 -5 5 0 125.50 4.29 5 5 0 121.62 4.61 -5 5 0 122.64 5.00 5 5 0 120.48 4.27 -5 5 0 124.26 4.82 5 5 0 115.10 4.40 5 5 0 119.39 4.70 -5 5 0 117.61 4.76 5 5 0 110.41 4.24 -5 5 0 115.04 4.58 -5 5 0 120.50 4.87 -5 5 0 123.08 4.57 -5 5 0 113.35 4.49 -5 5 0 120.20 4.48 -5 5 0 115.61 4.25 -5 5 0 121.24 4.69 6 -5 0 96.90 4.47 -6 -5 0 102.98 4.09 6 -5 0 101.31 4.05 -6 -5 0 96.43 3.97 6 -5 0 91.96 4.70 6 -5 0 99.96 3.84 -6 -5 0 105.28 3.55 -6 -5 0 102.92 3.72 6 -5 0 101.64 4.00 6 -5 0 108.87 4.90 -6 -5 0 105.16 4.09 6 -5 0 94.06 4.32 -6 -5 0 101.29 3.94 -6 -5 0 101.16 4.17 -6 -5 0 102.13 4.10 -6 -5 0 99.04 4.40 -6 5 0 92.31 4.38 6 5 0 106.14 4.05 -6 5 0 103.47 4.60 -6 5 0 104.82 4.23 -6 5 0 108.81 4.24 6 5 0 104.39 3.38 6 5 0 98.36 4.25 6 5 0 103.70 4.26 -6 5 0 101.38 4.33 6 5 0 97.36 3.98 6 5 0 100.66 4.03 6 5 0 104.06 3.39 -6 5 0 104.13 4.15 -6 5 0 111.37 3.90 -6 5 0 99.07 4.69 6 5 0 98.35 3.91 -6 5 0 105.05 3.72 7 -5 0 117.45 4.90 -7 -5 0 109.81 4.81 7 -5 0 116.20 5.69 7 -5 0 118.11 4.66 -7 -5 0 105.25 4.28 7 -5 0 121.88 4.98 -7 -5 0 114.22 4.61 7 -5 0 110.94 4.60 -7 -5 0 109.42 4.83 -7 -5 0 109.77 4.79 -7 -5 0 108.25 4.79 7 -5 0 119.71 4.71 -7 -5 0 112.54 4.59 7 5 0 126.35 4.72 7 5 0 117.46 4.79 7 5 0 114.05 4.51 -7 5 0 115.63 4.47 -7 5 0 112.72 4.30 7 5 0 115.27 4.82 -7 5 0 119.11 4.98 -7 5 0 113.87 5.09 -7 5 0 104.43 4.68 -7 5 0 109.99 5.30 -7 5 0 116.64 5.41 7 5 0 113.05 3.96 7 5 0 121.48 4.58 -8 -5 0 46.24 3.75 8 -5 0 41.73 3.61 -8 -5 0 52.32 3.18 8 -5 0 49.47 4.03 8 -5 0 59.55 3.25 8 -5 0 50.16 2.89 -8 -5 0 54.54 3.95 -8 -5 0 47.29 3.41 -8 -5 0 52.08 3.60 -8 -5 0 46.09 3.69 8 -5 0 49.20 3.66 8 -5 0 50.40 3.21 -8 5 0 48.60 3.27 8 5 0 44.39 3.26 8 5 0 45.44 3.09 -8 5 0 55.36 4.54 8 5 0 44.09 2.62 -8 5 0 47.80 4.01 8 5 0 47.05 3.39 -8 5 0 48.33 3.58 8 5 0 49.36 3.09 -8 5 0 47.44 3.13 8 5 0 49.18 3.45 -8 5 0 46.70 3.21 -8 5 0 55.61 6.81 8 5 0 49.79 2.41 -9 -5 0 153.13 6.82 -9 -5 0 161.27 7.15 9 -5 0 157.84 7.13 9 -5 0 160.23 6.31 9 -5 0 158.63 6.32 -9 -5 0 160.27 6.92 -9 -5 0 144.26 6.20 9 -5 0 164.66 6.11 9 -5 0 160.23 6.57 -9 -5 0 163.34 6.57 -9 -5 0 168.69 6.66 -9 5 0 149.41 6.67 -9 5 0 156.79 7.12 9 5 0 156.39 6.33 -9 5 0 142.58 7.41 -9 5 0 164.92 6.33 9 5 0 159.78 6.26 9 5 0 148.51 5.88 9 5 0 165.30 5.68 9 5 0 174.68 6.60 -9 5 0 152.22 7.64 -9 5 0 168.87 6.34 -9 5 0 159.55 6.29 9 5 0 163.80 6.72 9 5 0 159.09 6.45 10 -5 0 -2.11 2.79 -10 -5 0 -2.01 2.78 10 -5 0 -0.29 2.77 -10 -5 0 0.49 2.82 -10 -5 0 -1.22 3.70 10 -5 0 1.98 2.15 -10 -5 0 1.93 2.61 10 -5 0 2.96 2.08 -10 -5 0 -0.89 2.71 10 -5 0 -3.88 2.13 10 5 0 0.45 2.44 10 5 0 -1.02 2.26 -10 5 0 0.77 2.95 -10 5 0 -1.10 3.62 10 5 0 0.55 2.26 10 5 0 -0.23 1.69 -10 5 0 -2.13 2.16 10 5 0 -1.54 2.54 -10 5 0 1.15 2.32 10 5 0 -0.31 1.98 -10 5 0 1.80 2.71 10 5 0 -0.45 2.71 -11 -5 0 105.00 8.46 11 -5 0 105.49 5.15 -11 -5 0 116.69 6.48 -11 -5 0 116.36 6.67 -11 -5 0 103.30 7.14 11 -5 0 109.86 6.60 11 -5 0 102.76 5.36 11 -5 0 108.99 7.14 -11 5 0 128.26 7.24 -11 5 0 116.28 9.37 11 5 0 107.20 6.65 -11 5 0 99.11 5.77 11 5 0 111.77 6.01 -11 5 0 111.20 5.50 -11 5 0 105.06 7.66 -11 5 0 102.64 6.41 11 5 0 103.37 6.85 11 5 0 110.21 5.58 11 5 0 96.70 6.00 11 5 0 117.81 5.89 12 -5 0 163.51 7.19 12 -5 0 172.52 7.64 -12 -5 0 173.14 8.29 12 -5 0 163.95 8.12 12 -5 0 165.54 7.36 12 -5 0 170.00 6.62 -12 -5 0 159.13 8.35 -12 -5 0 168.69 9.56 -12 -5 0 185.95 8.83 12 5 0 163.86 6.73 12 5 0 155.80 7.79 12 5 0 141.49 8.22 -12 5 0 165.59 9.37 12 5 0 172.83 8.39 -12 5 0 165.10 7.12 12 5 0 160.79 7.91 -12 5 0 177.58 8.80 -12 5 0 160.63 7.81 -12 5 0 165.96 9.94 12 5 0 169.58 7.97 13 -5 0 10.41 3.79 -13 -5 0 17.17 4.70 -13 -5 0 13.61 5.18 -13 -5 0 13.95 4.61 13 -5 0 10.10 4.75 13 -5 0 15.03 4.44 13 -5 0 16.63 3.47 13 -5 0 11.40 2.98 13 -5 0 14.96 3.41 -13 5 0 15.08 4.35 13 5 0 18.16 3.14 -13 5 0 9.10 6.00 13 5 0 13.86 4.14 -13 5 0 9.87 4.95 -13 5 0 17.15 5.05 13 5 0 18.33 4.95 -13 5 0 14.84 3.55 13 5 0 14.25 3.84 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0 6 0 697.62 21.83 0 6 0 698.88 21.50 0 6 0 695.80 21.86 1 -6 0 14.29 1.46 -1 -6 0 14.99 1.64 1 -6 0 15.35 1.37 -1 -6 0 15.20 1.33 1 -6 0 13.97 1.17 -1 -6 0 17.23 1.41 1 -6 0 16.53 1.06 1 -6 0 14.97 1.84 1 -6 0 14.53 1.47 -1 -6 0 17.47 1.79 1 -6 0 15.29 0.99 1 -6 0 15.78 1.22 -1 -6 0 13.82 1.38 1 -6 0 16.84 1.52 -1 -6 0 14.88 1.65 1 -6 0 14.38 1.13 -1 -6 0 13.34 1.60 1 -6 0 13.65 0.95 1 -6 0 15.02 1.16 1 -6 0 14.95 1.14 -1 6 0 14.25 1.06 -1 6 0 14.02 1.00 1 6 0 13.41 1.54 -1 6 0 13.62 1.14 -1 6 0 13.99 1.36 1 6 0 14.05 1.57 1 6 0 16.09 1.47 -1 6 0 14.53 1.59 -1 6 0 15.63 1.43 -1 6 0 14.79 1.59 1 6 0 16.68 1.44 -1 6 0 12.14 1.27 -2 -6 0 356.76 11.16 2 -6 0 338.75 10.89 -2 -6 0 351.20 11.18 -2 -6 0 333.09 11.18 2 -6 0 338.88 10.72 2 -6 0 355.69 11.02 2 -6 0 349.18 11.04 2 -6 0 348.44 11.06 2 -6 0 337.80 10.95 2 -6 0 361.90 11.31 -2 -6 0 348.33 11.13 2 -6 0 344.92 11.19 2 -6 0 331.00 10.97 -2 -6 0 339.97 11.15 2 -6 0 350.26 11.06 2 -6 0 342.06 11.22 2 -6 0 337.70 11.18 2 6 0 336.11 11.16 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0 487.33 15.30 5 -6 0 474.85 15.54 -5 6 0 487.80 15.37 5 6 0 485.32 15.39 -5 6 0 483.12 15.58 5 6 0 504.76 15.62 -5 6 0 458.28 15.71 -5 6 0 491.30 15.88 -5 6 0 488.10 15.71 5 6 0 471.47 15.35 5 6 0 473.54 15.37 -5 6 0 489.12 15.16 5 6 0 470.98 15.60 5 6 0 466.97 15.72 -5 6 0 474.87 15.55 6 -6 0 94.16 4.45 -6 -6 0 98.83 3.82 6 -6 0 87.28 4.77 6 -6 0 97.44 4.01 6 -6 0 95.85 3.91 -6 -6 0 93.17 4.04 6 -6 0 95.02 4.20 6 -6 0 92.47 3.79 -6 -6 0 95.11 3.59 -6 -6 0 108.02 3.91 -6 -6 0 95.52 3.56 -6 -6 0 97.25 3.98 6 -6 0 84.38 4.06 -6 -6 0 103.32 4.01 -6 -6 0 99.54 4.27 6 6 0 96.37 3.73 6 6 0 102.92 4.09 6 6 0 98.63 4.04 6 6 0 97.80 3.83 -6 6 0 97.89 4.40 -6 6 0 97.68 4.21 -6 6 0 94.71 4.17 6 6 0 98.54 3.88 -6 6 0 101.75 4.61 -6 6 0 100.82 4.39 -6 6 0 92.25 3.75 -6 6 0 95.16 4.41 6 6 0 93.98 4.14 -6 6 0 81.30 4.69 -6 6 0 96.65 3.49 -7 -6 0 360.87 12.88 -7 -6 0 365.62 12.40 7 -6 0 365.90 13.19 -7 -6 0 379.41 12.58 7 -6 0 380.55 12.62 -7 -6 0 365.23 12.63 -7 -6 0 379.98 11.99 7 -6 0 377.47 12.35 -7 -6 0 371.64 12.19 7 -6 0 372.55 12.48 -7 -6 0 373.86 12.47 7 -6 0 393.13 13.01 7 -6 0 366.41 12.76 -7 -6 0 373.43 12.54 7 -6 0 381.67 12.60 7 6 0 382.03 12.78 -7 6 0 387.19 12.40 -7 6 0 397.66 12.75 7 6 0 381.76 12.57 7 6 0 384.67 13.54 7 6 0 358.76 12.39 -7 6 0 377.13 13.15 -7 6 0 384.65 12.16 -7 6 0 385.89 12.64 7 6 0 372.98 12.42 -8 -6 0 199.63 7.59 8 -6 0 210.20 7.97 -8 -6 0 216.57 8.10 -8 -6 0 211.91 7.92 -8 -6 0 204.65 7.77 8 -6 0 203.72 8.20 -8 -6 0 205.16 7.84 8 -6 0 205.19 7.32 8 -6 0 208.22 7.63 8 -6 0 203.10 7.60 -8 -6 0 200.65 7.21 8 -6 0 206.33 7.75 8 6 0 203.31 7.45 -8 6 0 202.96 7.63 -8 6 0 218.69 7.51 8 6 0 218.11 7.70 -8 6 0 211.91 7.25 -8 6 0 209.54 7.94 -8 6 0 206.74 8.47 8 6 0 196.72 7.67 8 6 0 199.20 7.49 8 6 0 211.21 7.62 -8 6 0 214.34 8.21 -8 6 0 214.55 8.49 9 -6 0 11.00 2.62 -9 -6 0 9.10 2.76 9 -6 0 4.94 4.79 9 -6 0 14.83 2.36 -9 -6 0 3.18 2.12 -9 -6 0 7.09 2.33 9 -6 0 7.43 2.21 -9 -6 0 8.17 2.64 -9 -6 0 6.87 3.03 9 -6 0 11.97 3.19 -9 -6 0 9.87 2.74 -9 6 0 9.88 3.38 -9 6 0 11.40 2.87 9 6 0 10.60 2.44 9 6 0 9.04 2.39 9 6 0 6.56 1.36 -9 6 0 9.99 2.32 -9 6 0 8.24 2.25 9 6 0 8.44 2.29 -9 6 0 13.18 2.21 9 6 0 13.45 2.06 9 6 0 9.33 1.84 -9 6 0 6.20 3.12 9 6 0 16.49 2.67 -9 6 0 9.61 2.72 10 -6 0 85.21 4.38 10 -6 0 82.64 5.03 -10 -6 0 69.25 5.40 10 -6 0 88.20 6.16 10 -6 0 86.56 5.61 -10 -6 0 83.91 5.60 -10 -6 0 79.57 6.48 -10 -6 0 83.36 5.93 10 -6 0 88.08 4.75 -10 -6 0 70.58 5.21 10 6 0 79.91 3.71 -10 6 0 70.77 4.61 -10 6 0 83.88 4.92 10 6 0 77.16 3.42 -10 6 0 75.16 4.98 -10 6 0 75.70 6.69 -10 6 0 88.54 5.70 10 6 0 81.27 4.79 10 6 0 76.98 5.03 10 6 0 74.83 4.58 10 6 0 87.56 5.26 10 6 0 80.12 5.90 -10 6 0 90.87 5.98 -10 6 0 84.88 7.53 -11 -6 0 26.78 4.02 -11 -6 0 22.15 5.36 11 -6 0 21.87 2.90 -11 -6 0 29.00 4.38 11 -6 0 17.70 4.06 -11 -6 0 23.00 3.77 11 -6 0 18.92 3.62 -11 -6 0 18.95 6.25 11 -6 0 22.62 3.27 11 -6 0 22.55 2.83 -11 6 0 29.47 4.04 11 6 0 23.34 3.53 -11 6 0 26.37 3.21 11 6 0 27.28 3.38 11 6 0 20.75 2.47 11 6 0 21.89 2.76 -11 6 0 19.95 6.00 -11 6 0 23.61 3.31 -11 6 0 23.03 3.93 -11 6 0 31.97 5.22 11 6 0 21.39 3.61 11 6 0 23.57 3.16 12 -6 0 18.03 4.86 12 -6 0 22.23 3.45 -12 -6 0 30.46 4.69 12 -6 0 19.90 4.47 12 -6 0 24.32 2.67 -12 -6 0 27.41 4.59 12 -6 0 24.68 3.68 -12 -6 0 25.44 4.47 12 -6 0 19.89 3.24 -12 6 0 26.69 5.04 12 6 0 27.54 4.37 12 6 0 21.82 3.72 -12 6 0 15.10 5.81 -12 6 0 19.46 3.81 12 6 0 17.99 2.43 12 6 0 20.35 3.33 12 6 0 22.46 4.09 -12 6 0 24.59 3.56 -12 6 0 19.36 3.76 -12 6 0 15.70 4.43 13 -6 0 45.11 5.44 -13 -6 0 46.90 6.27 -13 -6 0 39.15 5.00 13 -6 0 65.74 7.80 -13 -6 0 41.13 5.43 13 -6 0 42.65 6.22 -13 -6 0 48.19 5.78 13 -6 0 39.87 4.65 13 -6 0 50.28 5.61 13 -6 0 41.22 4.67 13 6 0 53.86 5.93 -13 6 0 41.16 5.69 -13 6 0 45.33 6.01 -13 6 0 47.79 6.08 13 6 0 46.00 5.15 -13 6 0 43.95 4.94 13 6 0 48.54 6.08 -13 6 0 44.49 6.99 -13 6 0 52.91 7.01 14 -6 0 1.04 7.41 14 -6 0 0.08 4.13 -14 -6 0 1.08 7.00 14 -6 0 3.41 3.74 14 -6 0 0.36 5.98 14 -6 0 1.72 4.19 -14 -6 0 2.07 5.74 -14 -6 0 2.52 6.06 -14 -6 0 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533.61 17.32 -1 7 0 514.81 16.97 -1 7 0 545.15 16.99 1 7 0 550.50 17.32 -1 7 0 534.33 17.17 -1 7 0 529.40 16.97 -1 7 0 552.70 17.02 2 -7 0 115.21 4.07 2 -7 0 113.05 4.15 -2 -7 0 112.41 4.50 -2 -7 0 112.07 4.27 2 -7 0 114.42 4.18 2 -7 0 108.21 4.49 2 -7 0 123.48 4.40 2 -7 0 110.22 4.18 -2 -7 0 124.36 5.21 2 -7 0 120.29 4.15 2 -7 0 115.11 3.73 2 -7 0 116.48 4.07 -2 -7 0 119.69 4.49 2 -7 0 115.92 4.32 2 -7 0 117.81 3.98 -2 -7 0 116.84 4.36 -2 -7 0 121.65 4.32 -2 -7 0 112.73 4.23 2 -7 0 119.35 4.01 -2 -7 0 112.95 4.39 2 -7 0 121.85 4.59 2 7 0 115.30 4.26 -2 7 0 116.45 4.17 -2 7 0 115.27 4.26 -2 7 0 105.32 4.03 -2 7 0 113.55 4.20 -2 7 0 113.44 4.10 -2 7 0 106.90 4.15 2 7 0 107.46 4.32 2 7 0 115.15 4.40 2 7 0 112.91 4.25 3 -7 0 134.33 5.09 3 -7 0 125.19 4.50 3 -7 0 124.64 4.57 3 -7 0 121.49 4.68 -3 -7 0 128.35 4.68 -3 -7 0 118.76 4.77 -3 -7 0 129.29 4.72 3 -7 0 125.16 4.64 3 -7 0 126.39 4.86 -3 -7 0 118.58 4.68 3 -7 0 132.34 4.38 -3 -7 0 112.57 4.54 3 -7 0 122.34 4.38 3 -7 0 125.71 4.25 3 -7 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5.29 -11 -7 0 15.70 4.58 -11 -7 0 11.46 3.50 -11 -7 0 20.73 4.02 11 -7 0 19.51 2.89 -11 -7 0 17.97 3.83 11 7 0 20.17 3.56 11 7 0 13.66 3.63 -11 7 0 18.67 3.80 -11 7 0 17.07 4.42 -11 7 0 14.57 3.36 -11 7 0 15.48 6.65 11 7 0 19.80 3.91 -11 7 0 22.20 4.49 11 7 0 17.00 3.65 11 7 0 13.43 2.73 -11 7 0 18.91 3.38 -11 7 0 16.04 3.09 -11 7 0 24.92 5.53 12 -7 0 60.68 5.64 -12 -7 0 50.89 5.34 12 -7 0 50.30 5.05 -12 -7 0 48.07 5.56 -12 -7 0 63.45 6.88 12 -7 0 56.28 6.84 12 -7 0 51.97 5.37 -12 -7 0 49.53 6.41 12 -7 0 50.64 6.34 -12 7 0 41.07 5.21 12 7 0 59.41 5.21 12 7 0 56.80 6.59 -12 7 0 62.14 7.26 -12 7 0 42.57 5.52 -12 7 0 53.88 5.66 12 7 0 47.02 5.93 -12 7 0 54.08 6.06 -12 7 0 53.42 5.64 -13 -7 0 63.37 8.39 -13 -7 0 68.47 7.94 13 -7 0 58.04 5.88 13 -7 0 48.55 5.04 -13 -7 0 61.87 7.66 -13 -7 0 54.15 6.45 13 -7 0 59.25 8.02 13 -7 0 55.77 5.95 13 -7 0 42.54 7.49 13 -7 0 54.35 6.88 13 7 0 53.16 5.77 -13 7 0 57.13 6.47 13 7 0 52.18 6.00 -13 7 0 52.29 6.55 -13 7 0 49.24 6.01 -13 7 0 63.26 9.25 -13 7 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52.16 5.22 -8 -10 0 49.34 4.07 -8 -10 0 41.06 4.03 -8 -10 0 49.60 4.03 -8 10 0 63.71 4.89 -8 10 0 45.77 4.86 -8 10 0 56.77 6.33 8 10 0 47.34 3.28 -8 10 0 55.52 6.72 -8 10 0 56.07 3.64 8 10 0 53.44 3.14 -8 10 0 61.97 4.59 -8 10 0 47.26 3.70 8 10 0 52.00 4.90 8 10 0 48.02 2.92 -9 -10 0 2.81 4.09 9 -10 0 0.22 4.37 9 -10 0 2.85 3.06 9 -10 0 0.96 3.34 -9 -10 0 -1.21 3.02 -9 -10 0 3.93 3.59 9 -10 0 1.05 4.57 9 -10 0 -0.81 3.55 9 -10 0 0.36 2.38 -9 -10 0 0.85 1.92 -9 -10 0 -0.24 3.02 -9 -10 0 1.44 2.87 9 10 0 3.56 3.43 -9 10 0 -0.49 3.19 -9 10 0 4.46 4.62 -9 10 0 0.70 4.59 9 10 0 -0.56 2.09 -9 10 0 0.53 2.36 9 10 0 -2.92 3.49 -9 10 0 2.18 3.14 -9 10 0 1.19 2.49 9 10 0 -0.11 1.79 10 -10 0 81.61 5.51 -10 -10 0 95.24 7.85 10 -10 0 83.95 9.10 -10 -10 0 78.97 6.46 10 -10 0 81.13 5.77 10 -10 0 100.50 6.77 10 -10 0 97.57 6.44 -10 -10 0 83.28 7.16 -10 -10 0 76.64 6.19 10 10 0 73.40 7.15 -10 10 0 98.05 9.47 -10 10 0 81.05 5.06 -10 10 0 79.58 6.98 10 10 0 84.55 5.19 -10 10 0 84.90 5.53 10 10 0 88.49 6.54 -10 10 0 93.68 6.44 10 10 0 93.77 4.68 -10 10 0 91.96 6.53 -11 -10 0 38.04 4.71 11 -10 0 39.40 5.26 -11 -10 0 36.65 5.61 11 -10 0 38.95 4.49 11 -10 0 34.48 4.49 -11 -10 0 43.80 6.10 11 -10 0 51.42 5.50 -11 -10 0 37.05 4.92 11 10 0 38.86 4.41 -11 10 0 30.11 5.16 -11 10 0 35.36 4.25 11 10 0 39.74 5.27 -11 10 0 52.22 7.37 11 10 0 40.65 5.08 11 10 0 35.94 3.94 -11 10 0 33.73 4.71 -12 -10 0 7.72 5.69 -12 -10 0 8.28 5.02 -12 -10 0 9.33 5.32 -12 -10 0 14.91 6.44 12 -10 0 14.42 4.02 12 -10 0 11.91 4.34 12 -10 0 0.80 5.20 12 -10 0 3.82 4.60 -12 10 0 12.43 5.05 -12 10 0 1.12 4.57 -12 10 0 10.18 4.83 12 10 0 3.40 5.13 12 10 0 7.86 4.22 12 10 0 12.33 3.28 -12 10 0 9.30 5.32 12 10 0 5.83 5.52 0 -11 0 -0.19 1.58 0 -11 0 2.40 1.70 0 -11 0 1.54 1.89 0 -11 0 0.66 1.29 0 -11 0 1.51 1.95 0 -11 0 -0.44 1.03 0 -11 0 -1.48 1.47 0 11 0 1.54 1.78 0 11 0 -1.21 1.91 0 11 0 2.44 2.00 -1 -11 0 21.91 2.84 1 -11 0 17.37 1.67 1 -11 0 21.45 2.47 -1 -11 0 19.89 2.11 1 -11 0 22.92 2.89 1 -11 0 18.17 1.89 1 -11 0 21.62 1.98 1 -11 0 19.91 2.10 -1 -11 0 21.81 2.11 1 -11 0 21.21 2.60 1 -11 0 24.74 2.35 1 11 0 27.88 3.24 1 11 0 24.48 2.98 1 11 0 19.69 2.53 -1 11 0 14.31 2.22 1 11 0 20.78 2.47 -1 11 0 23.34 2.84 2 -11 0 0.41 1.91 -2 -11 0 -0.34 1.91 2 -11 0 0.30 1.63 2 -11 0 0.72 1.60 2 -11 0 2.27 1.54 -2 -11 0 1.79 1.90 -2 -11 0 0.07 1.87 -2 -11 0 1.27 1.78 2 -11 0 -0.53 2.04 2 -11 0 0.47 1.48 2 -11 0 -0.55 1.33 2 -11 0 -0.19 1.42 -2 11 0 0.12 1.87 -2 11 0 1.50 1.88 -2 11 0 2.06 1.11 2 11 0 1.89 2.18 -2 11 0 0.92 1.58 -2 11 0 0.74 1.59 2 11 0 -2.62 1.81 2 11 0 -3.01 2.09 2 11 0 0.01 1.99 -2 11 0 0.89 1.23 3 -11 0 -0.15 1.56 3 -11 0 1.75 1.98 -3 -11 0 3.14 2.12 3 -11 0 1.14 1.53 3 -11 0 1.26 1.53 3 -11 0 1.53 2.00 -3 -11 0 1.50 2.25 -3 -11 0 4.16 1.94 3 -11 0 2.54 2.43 3 -11 0 1.34 1.48 3 -11 0 1.57 2.38 -3 -11 0 1.39 1.97 -3 11 0 1.74 1.48 -3 11 0 -0.48 2.02 -3 11 0 2.18 1.34 -3 11 0 3.03 1.84 3 11 0 0.25 2.24 -3 11 0 1.87 2.62 3 11 0 2.71 2.06 3 11 0 1.87 1.81 3 11 0 3.72 2.33 4 -11 0 67.04 3.20 4 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2 -28 9.14 4.97 4 2 -28 6.93 4.03 -4 2 28 1.88 4.62 4 2 -28 4.24 4.33 -4 2 28 2.09 3.99 4 2 -28 3.96 2.66 3 -2 -28 19.97 4.81 -3 -2 28 16.37 3.65 -3 -2 28 15.05 4.25 3 -2 -28 7.07 4.80 3 -2 -28 8.02 4.00 -3 -2 28 18.81 5.40 3 -2 -28 17.26 3.97 -3 2 28 12.45 3.55 3 2 -28 13.66 3.81 -3 2 28 11.88 4.37 -3 2 28 7.33 3.97 3 2 -28 10.54 4.93 3 2 -28 12.03 4.02 3 2 -28 13.05 2.82 3 2 -28 8.31 3.46 2 -2 -28 114.31 6.28 2 -2 -28 114.03 7.19 2 -2 -28 114.53 6.95 2 -2 -28 110.32 8.16 -2 -2 28 113.10 7.55 2 -2 -28 109.00 8.55 -2 -2 28 89.60 6.39 -2 -2 28 103.75 9.62 2 2 -28 111.45 8.26 2 2 -28 103.55 7.26 -2 2 28 102.44 7.93 2 2 -28 118.96 5.65 2 2 -28 117.84 6.28 -2 2 28 101.22 6.56 1 -2 -28 32.79 5.75 -1 -2 28 45.10 6.45 1 -2 -28 53.45 6.57 1 -2 -28 51.80 6.83 -1 -2 28 48.96 6.62 -1 -2 28 44.61 5.20 1 -2 -28 51.17 5.10 1 -2 -28 45.43 5.79 1 2 -28 50.07 5.49 1 2 -28 57.31 6.35 -1 2 28 38.28 4.19 1 2 -28 48.21 7.10 -1 2 28 50.78 6.50 -1 2 28 47.93 6.81 -1 2 28 40.87 5.29 1 2 -28 43.42 4.47 0 -2 28 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20.53 5.45 -5 -2 -28 13.46 7.16 -5 2 -28 17.83 6.96 -5 2 -28 22.25 4.50 -5 2 -28 20.10 5.46 5 2 28 18.73 5.78 -5 2 -28 23.41 5.49 5 2 28 14.11 4.19 -5 2 -28 24.96 4.85 5 2 28 15.34 4.30 5 2 28 24.59 5.84 -5 2 -28 19.31 6.66 -6 -2 -28 2.00 5.07 6 -2 28 4.29 4.37 6 -2 28 2.28 5.76 6 -2 28 -2.58 6.63 -6 -2 -28 2.82 6.21 -6 -2 -28 -2.69 5.25 6 -2 28 -1.43 3.85 -6 -2 -28 -2.04 5.31 -6 -2 -28 -3.48 5.61 -6 2 -28 -1.74 4.70 6 2 28 -7.47 4.30 6 2 28 -2.73 6.12 6 2 28 -0.17 5.73 -6 2 -28 -4.12 7.28 -6 2 -28 -2.13 5.47 6 2 28 -1.65 4.30 -6 2 -28 -1.82 5.56 -6 2 -28 6.52 7.14 -6 2 -28 2.58 5.00 -7 -2 -28 158.83 10.29 -7 -2 -28 183.40 13.44 -7 -2 -28 180.02 10.21 -7 -2 -28 149.34 13.43 -7 -2 -28 148.78 12.19 7 -2 28 148.11 13.25 7 -2 28 135.99 8.38 7 -2 28 150.38 11.38 7 2 28 133.79 12.23 -7 2 -28 144.87 10.07 -7 2 -28 154.04 12.80 -7 2 -28 145.02 9.66 7 2 28 152.13 12.00 -7 2 -28 148.65 13.73 -7 2 -28 165.56 12.87 7 2 28 135.24 8.82 -7 2 -28 172.58 10.54 7 2 28 142.30 9.07 9 -3 -28 83.87 8.38 9 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70.46 7.04 -7 3 28 62.23 7.02 6 -3 -28 36.99 4.96 6 -3 -28 38.82 4.64 6 -3 -28 40.25 4.85 6 -3 -28 48.27 5.99 -6 -3 28 44.30 6.62 6 -3 -28 40.61 5.08 -6 -3 28 48.05 4.94 6 -3 -28 35.81 4.35 6 -3 -28 34.48 6.15 -6 -3 28 26.13 5.23 6 3 -28 35.89 5.39 -6 3 28 35.89 5.67 6 3 -28 35.86 6.32 -6 3 28 36.42 5.55 6 3 -28 39.66 5.08 6 3 -28 35.41 4.76 6 3 -28 32.44 4.36 -6 3 28 36.59 4.67 6 3 -28 41.05 4.65 -6 3 28 33.33 6.12 -6 3 28 46.52 5.00 5 -3 -28 26.91 4.95 5 -3 -28 39.02 4.84 -5 -3 28 39.10 5.36 5 -3 -28 36.54 3.47 -5 -3 28 30.88 5.63 5 -3 -28 34.89 4.66 5 -3 -28 34.41 4.02 -5 -3 28 30.18 4.29 5 -3 -28 36.84 6.32 5 3 -28 38.37 5.65 -5 3 28 39.69 5.88 5 3 -28 37.71 4.51 -5 3 28 33.64 4.43 -5 3 28 38.40 4.58 -5 3 28 30.66 5.62 5 3 -28 34.04 4.04 5 3 -28 38.03 7.53 -5 3 28 42.30 5.82 5 3 -28 38.31 4.70 5 3 -28 30.37 4.59 5 3 -28 42.02 4.29 4 -3 -28 75.41 10.11 4 -3 -28 101.65 6.14 -4 -3 28 82.34 9.17 4 -3 -28 100.63 6.78 4 -3 -28 90.64 5.34 4 -3 -28 80.79 7.89 4 -3 -28 78.51 7.06 -4 -3 28 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-3 28 3.94 5.05 1 -3 -28 1.82 3.44 -1 3 28 3.96 4.60 1 3 -28 6.88 4.62 -1 3 28 1.50 3.22 1 3 -28 3.69 3.63 1 3 -28 1.44 5.05 1 3 -28 0.79 3.84 -1 3 28 1.35 2.83 1 3 -28 1.59 2.62 -1 3 28 2.40 4.14 0 -3 -28 2.96 5.19 0 -3 -28 0.76 3.65 0 -3 28 3.37 4.71 0 -3 -28 -2.11 4.69 0 -3 -28 -2.71 3.91 0 -3 28 3.76 4.35 0 -3 28 -2.05 3.36 0 -3 -28 -1.65 3.55 0 3 28 -2.76 4.26 0 3 -28 4.16 3.98 0 3 -28 4.55 3.59 0 3 28 0.42 4.51 0 3 28 5.89 3.30 0 3 28 -0.62 3.06 0 3 -28 -1.16 4.35 0 3 -28 1.83 2.71 -1 -3 -28 116.86 7.92 1 -3 28 117.19 8.15 -1 -3 -28 104.71 7.33 -1 -3 -28 117.16 8.65 1 -3 28 117.27 5.46 -1 -3 -28 115.61 10.76 -1 -3 -28 113.14 9.37 -1 -3 -28 127.72 7.48 1 -3 28 117.50 6.74 -1 3 -28 124.10 7.76 1 3 28 134.64 6.65 1 3 28 130.10 8.20 -1 3 -28 125.33 7.02 -1 3 -28 118.66 8.95 -1 3 -28 120.67 6.05 1 3 28 124.31 8.33 1 3 28 115.57 6.81 -1 3 -28 125.12 9.17 2 -3 28 104.32 6.32 -2 -3 -28 90.44 8.39 -2 -3 -28 89.33 7.81 -2 -3 -28 101.36 7.27 2 -3 28 94.31 6.29 2 -3 28 86.43 7.73 -2 -3 -28 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4 3 28 121.08 9.85 -4 3 -28 116.90 6.89 5 -3 28 3.15 5.53 -5 -3 -28 4.58 5.61 5 -3 28 2.85 4.22 -5 -3 -28 -2.45 4.76 5 -3 28 4.90 3.42 -5 -3 -28 -3.03 5.24 -5 -3 -28 1.66 4.82 -5 -3 -28 3.99 5.14 5 -3 28 -1.88 6.59 -5 3 -28 -0.91 5.23 5 3 28 -3.35 4.08 -5 3 -28 1.24 5.11 5 3 28 -1.61 5.71 -5 3 -28 -2.28 6.53 5 3 28 0.92 5.10 5 3 28 2.20 4.18 -5 3 -28 6.46 4.28 -5 3 -28 0.99 4.61 -5 3 -28 5.71 6.56 6 -3 28 31.06 4.96 6 -3 28 35.07 7.92 -6 -3 -28 32.97 5.88 6 -3 28 27.40 6.46 -6 -3 -28 31.89 6.01 -6 -3 -28 32.07 6.10 -6 -3 -28 26.88 6.30 -6 -3 -28 25.40 6.61 6 3 28 37.37 6.50 -6 3 -28 25.69 7.68 6 3 28 26.46 6.78 6 3 28 30.28 4.88 6 3 28 30.60 5.01 -6 3 -28 35.88 6.28 -6 3 -28 25.78 6.18 -6 3 -28 29.13 5.01 -6 3 -28 37.45 5.61 6 3 28 29.61 4.53 -6 3 -28 32.93 7.61 -7 -3 -28 25.30 6.90 -7 -3 -28 40.86 6.54 7 -3 28 32.51 5.39 -7 -3 -28 20.15 7.21 7 -3 28 41.98 7.39 -7 -3 -28 48.87 10.34 7 -3 28 32.50 8.20 7 3 28 29.35 7.55 -7 3 -28 35.89 7.00 7 3 28 27.71 5.47 7 3 28 27.73 6.93 7 3 28 32.67 4.83 -7 3 -28 39.66 6.65 -7 3 -28 39.64 6.89 -7 3 -28 35.81 5.94 7 3 28 41.69 5.53 -7 3 -28 35.33 8.34 -7 3 -28 27.33 8.23 9 -4 -28 23.31 7.04 9 -4 -28 9.59 8.01 -9 -4 28 11.06 6.67 9 4 -28 17.30 6.42 -9 4 28 14.33 6.71 -9 4 28 20.38 7.58 -9 4 28 18.43 5.92 9 4 -28 24.19 8.02 8 -4 -28 47.72 7.98 -8 -4 28 43.81 6.79 8 -4 -28 50.80 5.85 8 -4 -28 42.98 7.83 8 -4 -28 55.63 6.77 8 -4 -28 52.32 6.60 8 -4 -28 56.24 6.26 -8 4 28 48.74 5.94 8 4 -28 57.12 5.65 -8 4 28 55.28 7.12 8 4 -28 57.61 7.67 -8 4 28 47.97 7.40 8 4 -28 57.92 7.23 -8 4 28 58.95 8.01 8 4 -28 50.41 6.26 8 4 -28 54.41 6.83 7 -4 -28 23.96 5.10 -7 -4 28 17.02 5.69 7 -4 -28 17.56 5.10 7 -4 -28 21.86 7.55 7 -4 -28 13.66 5.69 -7 -4 28 20.00 4.83 7 -4 -28 12.55 5.05 7 -4 -28 17.22 4.34 7 4 -28 13.85 3.43 -7 4 28 15.28 4.97 -7 4 28 26.10 6.55 7 4 -28 19.75 5.10 7 4 -28 20.49 4.59 -7 4 28 18.30 4.93 -7 4 28 22.74 6.20 7 4 -28 18.40 4.67 7 4 -28 11.39 6.53 6 -4 -28 4.32 4.40 6 -4 -28 2.23 4.75 -6 -4 28 5.05 4.20 6 -4 -28 2.61 4.60 6 -4 -28 1.15 3.86 -6 -4 28 2.94 4.88 -6 -4 28 3.43 7.89 6 -4 -28 -0.08 5.90 6 -4 -28 5.55 5.56 6 4 -28 1.45 4.23 6 4 -28 2.48 5.01 -6 4 28 3.10 5.75 6 4 -28 1.98 4.23 -6 4 28 -0.79 4.29 6 4 -28 0.00 4.14 6 4 -28 3.09 2.93 6 4 -28 -3.57 7.33 -6 4 28 -1.24 4.36 5 -4 -28 108.74 5.70 5 -4 -28 99.18 8.07 5 -4 -28 97.78 9.72 5 -4 -28 108.44 8.67 5 -4 -28 106.19 7.43 -5 -4 28 100.80 8.20 5 -4 -28 113.24 7.91 -5 -4 28 112.24 10.04 5 -4 -28 88.39 6.74 -5 -4 28 103.10 7.19 5 4 -28 109.25 7.41 -5 4 28 109.07 8.52 -5 4 28 115.20 7.19 5 4 -28 115.55 5.40 5 4 -28 102.77 9.03 -5 4 28 103.40 7.28 -5 4 28 113.13 8.97 5 4 -28 120.69 7.32 -5 4 28 105.92 8.85 5 4 -28 101.08 8.41 5 4 -28 114.26 7.34 4 -4 -28 2.56 4.71 4 -4 -28 -1.51 4.58 4 -4 -28 1.24 4.00 4 -4 -28 -1.86 4.41 4 -4 -28 1.50 4.17 4 -4 -28 3.76 3.55 -4 -4 28 2.74 5.76 -4 -4 28 1.16 3.80 -4 -4 28 1.90 4.27 4 4 -28 0.47 2.47 -4 4 28 -1.57 3.81 4 4 -28 -2.03 5.27 -4 4 28 -1.23 5.03 4 4 -28 2.76 3.99 4 4 -28 2.24 3.75 -4 4 28 -1.33 3.86 4 4 -28 0.63 3.90 4 4 -28 3.25 5.56 -4 4 28 3.21 3.78 4 4 -28 -0.48 3.27 3 -4 -28 26.43 4.31 -3 -4 28 29.38 4.92 3 -4 -28 15.24 3.85 3 -4 -28 29.16 4.65 3 -4 -28 14.28 4.89 -3 -4 28 25.46 5.69 3 -4 -28 32.75 6.20 -3 -4 28 26.52 4.07 3 4 -28 27.71 2.75 -3 4 28 23.49 4.04 3 4 -28 19.06 3.82 -3 4 28 27.91 5.13 3 4 -28 26.63 5.50 -3 4 28 27.15 5.43 3 4 -28 21.31 4.20 3 4 -28 21.84 4.87 -3 4 28 23.25 4.18 3 4 -28 29.08 4.21 -2 -4 28 58.20 6.83 -2 -4 28 67.72 8.55 2 -4 -28 63.63 7.49 2 -4 -28 56.60 6.25 2 -4 -28 56.54 5.95 2 -4 -28 58.62 6.66 2 -4 -28 60.97 5.72 -2 -4 28 60.47 5.76 -2 4 28 67.29 7.11 2 4 -28 49.13 7.25 -2 4 28 53.31 5.67 2 4 -28 68.28 8.10 -2 4 28 61.51 4.89 2 4 -28 57.23 6.37 -2 4 28 51.72 7.11 2 4 -28 52.16 5.59 -2 4 28 53.24 5.93 2 4 -28 53.39 4.21 2 4 -28 56.07 5.65 -1 -4 28 35.28 4.13 1 -4 -28 43.79 6.22 1 -4 -28 41.56 4.42 1 -4 -28 34.32 5.21 1 -4 -28 47.42 5.93 -1 -4 28 36.19 5.98 1 -4 -28 37.17 4.88 -1 -4 28 42.00 5.18 1 4 -28 44.72 5.23 -1 4 28 38.04 4.48 1 4 -28 42.79 4.63 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145.16 8.72 -2 -4 -28 149.44 9.35 -2 -4 -28 153.33 10.52 -2 4 -28 156.75 8.09 2 4 28 149.64 7.69 -2 4 -28 150.90 8.76 -2 4 -28 142.32 9.97 2 4 28 153.16 9.29 -2 4 -28 159.22 6.74 2 4 28 152.04 7.87 2 4 28 156.85 9.14 -2 4 -28 153.85 10.26 2 4 28 141.89 7.70 -3 -4 -28 17.98 4.72 3 -4 28 12.72 2.96 3 -4 28 17.46 5.16 -3 -4 -28 10.13 4.91 -3 -4 -28 11.49 4.68 -3 -4 -28 12.37 5.20 -3 -4 -28 15.52 6.14 3 -4 28 13.70 5.13 3 -4 28 9.41 3.69 -3 -4 -28 12.44 4.38 3 4 28 10.66 3.91 3 4 28 8.29 4.43 -3 4 -28 4.41 4.90 -3 4 -28 13.05 4.07 3 4 28 10.08 3.83 -3 4 -28 15.84 4.88 -3 4 -28 18.45 6.37 3 4 28 19.00 5.51 -3 4 -28 10.10 3.35 3 4 28 13.07 4.01 -4 -4 -28 69.18 7.98 4 -4 28 61.73 6.40 -4 -4 -28 60.28 7.80 4 -4 28 59.36 6.38 -4 -4 -28 64.99 7.37 4 -4 28 73.41 7.62 4 -4 28 50.56 5.14 -4 -4 -28 64.64 8.45 -4 -4 -28 64.99 7.56 -4 4 -28 62.56 5.89 -4 4 -28 66.55 9.58 4 4 28 59.82 6.32 -4 4 -28 64.96 8.58 4 4 28 65.60 6.60 -4 4 -28 65.65 6.98 4 4 28 63.11 7.81 4 4 28 55.32 6.37 -4 4 -28 79.53 8.02 4 4 28 53.77 6.67 -4 4 -28 67.55 7.99 5 -4 28 71.90 6.81 5 -4 28 78.10 8.67 -5 -4 -28 66.30 8.07 -5 -4 -28 63.85 7.93 -5 -4 -28 75.64 8.15 -5 -4 -28 68.21 8.93 5 -4 28 55.56 7.65 -5 -4 -28 75.10 9.11 5 4 28 52.23 7.99 -5 4 -28 51.33 6.37 -5 4 -28 56.38 7.81 5 4 28 65.66 8.21 -5 4 -28 63.64 7.39 5 4 28 65.44 6.92 -5 4 -28 60.81 8.34 5 4 28 68.25 6.74 -5 4 -28 77.66 10.57 -5 4 -28 68.83 6.51 -6 -4 -28 30.87 6.13 6 -4 28 36.43 7.96 6 -4 28 18.58 6.11 -6 -4 -28 28.55 5.97 -6 -4 -28 29.72 6.65 -6 -4 -28 31.22 6.22 -6 4 -28 38.31 5.12 -6 4 -28 29.62 7.86 6 4 28 28.67 5.88 6 4 28 26.95 5.09 6 4 28 26.27 5.04 6 4 28 26.52 4.62 -6 4 -28 33.61 5.56 -6 4 -28 33.06 6.36 6 4 28 31.89 6.83 -6 4 -28 33.89 7.98 -7 -4 -28 148.52 11.89 7 -4 28 125.94 9.34 -7 -4 -28 130.74 10.67 -7 -4 -28 138.19 11.17 7 -4 28 138.70 11.49 7 -4 28 124.90 14.33 -7 -4 -28 140.35 10.62 -7 4 -28 162.35 13.50 -7 4 -28 142.53 13.55 7 4 28 138.82 11.82 -7 4 -28 139.33 9.72 7 4 28 150.48 11.08 -7 4 -28 137.26 9.33 7 4 28 132.94 9.38 7 4 28 132.78 8.70 -7 4 -28 131.71 10.96 7 4 28 129.96 9.23 -7 4 -28 158.26 11.55 8 -5 -28 6.75 5.50 -8 -5 28 4.29 5.54 -8 -5 28 1.24 5.74 8 -5 -28 2.32 6.15 8 -5 -28 4.95 5.58 8 5 -28 5.80 7.33 8 5 -28 -0.89 3.76 8 5 -28 -1.11 4.78 -8 5 28 0.53 7.27 -8 5 28 -0.99 4.92 8 5 -28 1.23 5.74 -8 5 28 -0.52 5.47 8 5 -28 1.62 4.81 -8 5 28 4.61 5.55 -8 5 28 3.06 6.34 7 -5 -28 37.92 6.93 -7 -5 28 31.56 5.29 7 -5 -28 33.77 6.06 7 -5 -28 49.16 8.33 7 -5 -28 31.92 5.44 7 -5 -28 41.41 4.72 7 -5 -28 36.81 5.74 -7 -5 28 40.69 8.95 -7 5 28 40.68 6.26 -7 5 28 33.13 5.81 7 5 -28 35.21 3.85 -7 5 28 29.72 5.37 7 5 -28 36.79 5.09 7 5 -28 46.98 7.35 7 5 -28 43.48 5.92 -7 5 28 43.68 7.30 7 5 -28 39.52 5.07 6 -5 -28 36.07 5.08 6 -5 -28 43.51 5.35 -6 -5 28 29.32 5.39 6 -5 -28 30.65 4.61 6 -5 -28 40.01 5.65 6 -5 -28 32.51 7.55 6 -5 -28 35.90 6.26 -6 -5 28 43.80 5.18 6 5 -28 36.10 5.00 6 5 -28 33.11 4.75 -6 5 28 41.41 5.48 6 5 -28 35.54 3.47 -6 5 28 44.57 6.81 6 5 -28 34.32 4.85 -6 5 28 30.48 6.21 -6 5 28 34.68 5.02 6 5 -28 31.82 6.88 5 -5 -28 6.33 4.01 5 -5 -28 10.44 5.05 -5 -5 28 13.37 5.09 5 -5 -28 8.82 4.79 5 -5 -28 8.60 5.11 5 -5 -28 11.53 6.34 5 -5 -28 12.00 4.17 5 -5 -28 13.07 2.90 -5 -5 28 12.36 4.33 -5 5 28 18.59 4.89 5 5 -28 12.36 4.97 -5 5 28 7.43 5.14 -5 5 28 18.32 6.11 -5 5 28 9.06 5.18 5 5 -28 12.26 4.49 5 5 -28 19.41 5.99 5 5 -28 14.48 4.28 -5 5 28 14.36 4.37 5 5 -28 9.23 4.20 5 5 -28 10.85 2.78 4 -5 -28 8.87 5.57 4 -5 -28 26.03 4.88 -4 -5 28 20.04 6.49 -4 -5 28 20.19 4.24 4 -5 -28 24.42 5.45 -4 -5 28 22.64 4.88 4 -5 -28 23.25 4.54 4 -5 -28 17.95 4.04 4 -5 -28 13.64 4.88 4 5 -28 22.69 4.36 -4 5 28 11.56 3.93 4 5 -28 23.93 4.37 4 5 -28 16.13 5.76 4 5 -28 23.43 5.03 -4 5 28 29.89 4.87 -4 5 28 15.73 4.23 4 5 -28 18.38 4.24 -3 -5 28 23.74 5.61 3 -5 -28 28.56 5.07 -3 -5 28 36.23 4.46 3 -5 -28 32.95 4.97 3 -5 -28 36.87 4.80 3 -5 -28 33.62 5.20 -3 -5 28 30.42 5.05 3 -5 -28 46.84 6.74 3 -5 -28 37.99 4.57 -3 5 28 28.38 5.65 3 5 -28 36.88 4.58 3 5 -28 27.88 4.63 3 5 -28 41.96 6.18 -3 5 28 32.08 4.71 3 5 -28 38.79 4.42 -3 5 28 34.21 5.24 -3 5 28 31.12 4.31 3 5 -28 37.66 4.42 2 -5 -28 155.15 10.49 -2 -5 28 159.54 8.14 -2 -5 28 155.71 10.63 2 -5 -28 161.80 8.47 2 -5 -28 132.57 8.83 -2 -5 28 170.62 8.82 2 -5 -28 158.83 9.16 2 -5 -28 143.54 7.94 -2 5 28 145.52 8.19 2 5 -28 155.54 7.81 2 5 -28 141.10 8.24 -2 5 28 159.20 9.01 -2 5 28 158.98 7.29 2 5 -28 145.74 8.95 2 5 -28 159.23 9.84 -2 5 28 151.99 9.30 -2 5 28 137.70 7.72 2 5 -28 144.39 8.12 1 -5 -28 27.91 5.81 1 -5 -28 8.04 4.56 -1 -5 28 8.67 3.77 1 -5 -28 15.74 4.39 1 -5 -28 19.94 4.75 -1 -5 28 18.30 5.96 -1 -5 28 18.12 4.61 1 -5 -28 15.94 4.21 -1 5 28 23.39 5.29 1 5 -28 19.49 5.74 -1 5 28 13.60 3.60 1 5 -28 21.61 4.06 -1 5 28 14.09 4.15 1 5 -28 10.35 4.14 1 5 -28 20.57 3.83 -1 5 28 12.29 3.79 -1 5 28 13.49 4.10 0 -5 -28 8.32 4.29 0 -5 -28 3.07 5.90 0 -5 -28 9.24 4.15 0 -5 -28 8.62 4.45 0 -5 28 12.78 3.79 0 -5 28 8.08 5.52 0 -5 -28 5.19 4.80 0 -5 28 6.24 4.52 0 5 -28 6.98 5.57 0 5 28 6.91 3.65 0 5 -28 8.15 3.76 0 5 28 13.61 4.53 0 5 -28 11.84 4.17 0 5 28 9.30 5.05 0 5 28 7.21 3.96 0 5 -28 9.83 5.76 0 5 28 9.49 3.81 -1 -5 -28 38.07 6.33 -1 -5 -28 52.92 6.68 1 -5 28 41.84 6.59 1 -5 28 50.04 5.66 -1 -5 -28 34.28 5.56 -1 -5 -28 42.94 4.77 1 -5 28 33.40 3.73 -1 -5 -28 40.26 4.93 -1 -5 -28 45.68 5.41 1 -5 28 49.64 5.55 -1 5 -28 39.14 4.49 1 5 28 35.23 5.54 1 5 28 36.34 4.25 1 5 28 30.91 4.52 -1 5 -28 46.25 4.99 -1 5 -28 53.02 7.58 -1 5 -28 38.93 7.28 1 5 28 36.05 4.51 1 5 28 40.16 4.39 -2 -5 -28 59.30 7.60 -2 -5 -28 26.56 7.38 -2 -5 -28 44.75 5.26 -2 -5 -28 47.15 5.53 2 -5 28 43.54 5.29 2 -5 28 45.43 5.83 2 -5 28 37.68 5.51 -2 -5 -28 46.71 5.07 -2 -5 -28 47.85 5.25 -2 5 -28 44.68 5.13 2 5 28 43.93 5.88 -2 5 -28 40.68 6.55 -2 5 -28 33.38 8.30 2 5 28 43.70 4.44 2 5 28 50.73 6.17 2 5 28 46.06 5.91 2 5 28 54.15 7.03 -2 5 -28 52.55 6.14 -3 -5 -28 -5.83 4.45 3 -5 28 1.01 5.24 3 -5 28 -1.09 4.88 -3 -5 -28 0.86 5.07 3 -5 28 0.78 3.87 -3 -5 -28 1.93 4.64 -3 -5 -28 5.63 4.63 -3 -5 -28 -3.07 5.13 -3 5 -28 3.48 4.02 -3 5 -28 -0.37 2.77 3 5 28 -1.38 4.07 -3 5 -28 -0.79 4.80 3 5 28 0.70 3.84 -3 5 -28 -1.13 5.40 3 5 28 2.12 5.49 -3 5 -28 -1.03 5.92 3 5 28 2.10 4.73 3 5 28 -0.05 3.99 -4 -5 -28 11.27 5.00 -4 -5 -28 18.86 5.51 -4 -5 -28 9.46 5.60 -4 -5 -28 20.58 5.04 4 -5 28 10.01 6.53 4 -5 28 17.37 4.31 -4 -5 -28 8.39 5.17 4 -5 28 9.53 5.17 -4 5 -28 13.25 4.40 -4 5 -28 17.43 5.29 4 5 28 18.90 4.59 -4 5 -28 9.60 7.03 4 5 28 15.25 4.89 4 5 28 14.46 4.29 4 5 28 12.78 5.84 -4 5 -28 16.00 5.90 4 5 28 18.65 4.42 -5 -5 -28 4.90 5.97 -5 -5 -28 1.20 5.27 -5 -5 -28 1.63 5.84 5 -5 28 0.05 5.74 5 -5 28 1.64 7.24 -5 -5 -28 0.92 5.41 -5 -5 -28 6.50 5.46 5 -5 28 2.83 4.41 -5 5 -28 3.31 5.02 -5 5 -28 -0.28 5.67 -5 5 -28 2.65 6.44 5 5 28 -0.52 4.73 5 5 28 -3.55 6.03 -5 5 -28 -0.43 4.59 -5 5 -28 2.63 7.33 5 5 28 0.75 4.33 5 5 28 -2.79 4.72 5 5 28 -0.38 5.01 -5 5 -28 -1.94 3.78 -6 -5 -28 15.06 6.56 -6 -5 -28 19.24 6.21 -6 -5 -28 20.78 8.03 -6 -5 -28 16.42 5.99 6 -5 28 21.68 4.92 -6 -5 -28 16.47 6.24 6 -5 28 16.92 8.28 6 5 28 24.57 5.95 6 5 28 20.20 4.86 6 5 28 15.75 4.99 -6 5 -28 25.01 8.37 -6 5 -28 12.74 5.15 6 5 28 13.37 5.20 -6 5 -28 31.75 6.63 -6 5 -28 18.28 6.30 -6 5 -28 21.90 7.70 -8 -6 28 89.66 10.21 8 -6 -28 77.71 10.08 8 6 -28 68.18 8.83 -8 6 28 84.56 10.49 -8 6 28 81.33 9.10 8 6 -28 80.70 9.61 -8 6 28 76.57 9.00 7 -6 -28 -0.65 5.15 -7 -6 28 2.45 5.54 7 -6 -28 -3.17 5.45 -7 -6 28 0.04 5.64 7 -6 -28 -1.91 5.88 7 -6 -28 -1.80 7.24 7 -6 -28 2.74 5.35 -7 6 28 -1.62 5.29 7 6 -28 -2.45 4.85 7 6 -28 0.64 5.05 -7 6 28 -1.24 5.36 -7 6 28 -0.45 6.25 7 6 -28 -1.06 8.02 -7 6 28 5.87 7.03 7 6 -28 -0.26 4.52 6 -6 -28 12.27 5.32 6 -6 -28 11.92 4.53 6 -6 -28 22.36 5.15 -6 -6 28 13.13 4.82 6 -6 -28 18.07 5.49 -6 -6 28 19.19 5.45 6 -6 -28 11.14 5.66 6 6 -28 12.65 5.09 6 6 -28 14.22 6.76 -6 6 28 18.05 5.29 6 6 -28 12.26 4.76 -6 6 28 16.09 5.08 6 6 -28 10.95 4.47 -6 6 28 14.29 6.55 -6 6 28 15.46 6.06 -5 -6 28 106.78 8.47 5 -6 -28 107.49 8.10 5 -6 -28 96.15 8.72 5 -6 -28 108.84 7.64 5 -6 -28 107.43 8.32 -5 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4.90 2 -6 -28 8.37 8.61 -2 -6 28 2.81 8.03 2 -6 -28 9.05 4.02 -2 6 28 5.29 4.46 2 6 -28 10.98 6.07 -2 6 28 4.59 3.62 2 6 -28 -6.18 3.81 2 6 -28 7.70 3.98 -2 6 28 3.04 4.13 2 6 -28 5.51 4.13 -2 6 28 3.67 5.36 2 6 -28 4.87 4.75 -2 6 28 1.94 3.84 1 -6 -28 23.62 4.37 -1 -6 28 27.03 5.00 -1 -6 28 26.39 4.21 1 -6 -28 19.94 5.15 1 -6 -28 27.23 5.15 1 -6 -28 18.33 4.53 -1 -6 28 27.26 6.27 1 6 -28 24.92 4.29 -1 6 28 26.10 5.59 -1 6 28 24.38 4.85 1 6 -28 26.15 6.37 -1 6 28 26.69 4.59 1 6 -28 16.24 4.34 -1 6 28 32.71 4.24 1 6 -28 39.69 5.40 -1 6 28 24.06 4.23 1 6 -28 25.71 4.27 0 -6 -28 100.23 7.88 0 -6 28 111.68 7.78 0 -6 -28 107.06 8.23 0 -6 28 89.39 10.04 0 -6 -28 100.00 7.58 0 -6 28 96.28 7.09 0 -6 -28 89.18 7.58 0 6 28 92.10 7.25 0 6 28 99.79 8.44 0 6 -28 108.96 7.48 0 6 -28 94.59 9.60 0 6 28 103.87 7.71 0 6 -28 92.81 6.90 0 6 28 95.50 7.13 0 6 -28 82.48 6.86 0 6 -28 105.72 8.49 1 -6 28 29.06 5.18 -1 -6 -28 25.58 5.02 -1 -6 -28 25.36 4.93 1 -6 28 27.51 2.64 -1 -6 -28 22.76 5.24 1 -6 28 20.11 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-4 4 32 1.75 6.93 4 4 -32 -3.08 7.10 4 4 -32 0.40 6.04 -4 4 32 -1.20 6.36 4 4 -32 2.42 8.49 4 4 -32 1.63 5.19 -3 -4 32 -2.93 5.95 3 -4 -32 1.09 5.24 3 -4 -32 5.92 4.88 3 -4 -32 -2.13 6.31 3 -4 -32 5.22 5.77 -3 -4 32 0.30 4.92 3 -4 -32 -2.86 6.09 3 4 -32 -3.92 4.88 3 4 -32 -5.45 6.35 -3 4 32 9.16 5.03 -3 4 32 -5.51 5.73 3 4 -32 0.60 5.34 3 4 -32 7.19 7.52 -3 4 32 5.38 7.01 -3 4 32 -1.80 5.12 3 4 -32 -3.24 4.94 2 -4 -32 0.67 4.86 2 -4 -32 11.34 6.08 2 -4 -32 -0.52 4.78 2 -4 -32 -0.74 9.93 -2 -4 32 -0.75 4.87 -2 -4 32 12.57 10.25 2 4 -32 4.70 5.07 -2 4 32 13.08 5.76 2 4 -32 4.25 6.65 2 4 -32 1.42 5.44 -2 4 32 3.70 6.30 2 4 -32 -1.45 7.39 -2 4 32 0.57 6.58 2 4 -32 1.12 4.70 -2 4 32 7.21 4.96 1 -4 -32 38.32 5.31 -1 -4 32 37.45 5.70 1 -4 -32 39.77 10.46 1 -4 -32 38.20 5.79 1 -4 -32 33.65 7.07 1 4 -32 40.25 7.23 1 4 -32 39.31 5.42 1 4 -32 35.63 5.47 -1 4 32 35.10 5.67 -1 4 32 29.87 5.89 -1 4 32 32.60 4.89 1 4 -32 34.53 5.90 -1 4 32 29.94 7.08 1 4 -32 42.86 8.09 -1 4 32 35.57 5.32 0 -4 32 9.85 5.00 0 -4 -32 8.52 5.26 0 -4 -32 9.25 5.56 0 -4 -32 13.06 6.75 0 -4 -32 5.06 7.63 0 4 -32 7.76 5.61 0 4 -32 18.07 7.89 0 4 32 12.42 6.61 0 4 -32 6.88 6.19 0 4 32 12.75 5.83 0 4 32 8.82 5.27 0 4 32 14.62 4.84 0 4 -32 6.68 5.04 0 4 32 10.44 4.66 1 -4 32 12.66 4.97 -1 -4 -32 19.90 6.96 1 -4 32 2.57 7.17 -1 -4 -32 7.09 5.54 -1 -4 -32 12.81 5.81 -1 -4 -32 27.09 6.30 1 4 32 12.35 5.51 -1 4 -32 14.24 5.25 1 4 32 12.81 4.92 -1 4 -32 19.33 6.97 1 4 32 13.84 5.04 1 4 32 14.87 5.32 -1 4 -32 8.61 5.79 -1 4 -32 17.81 8.24 1 4 32 12.71 6.88 2 -4 32 0.94 6.12 -2 -4 -32 -2.24 5.61 -2 -4 -32 8.75 6.93 -2 -4 -32 7.20 5.58 -2 -4 -32 1.73 6.24 2 -4 32 3.96 4.87 -2 4 -32 2.55 9.13 2 4 32 5.48 6.37 2 4 32 4.37 7.01 2 4 32 -1.89 5.19 2 4 32 2.53 4.91 -2 4 -32 3.04 7.26 -2 4 -32 -3.24 5.25 2 4 32 3.87 5.21 -2 4 -32 0.50 7.94 -3 -4 -32 4.48 7.20 3 -4 32 20.85 6.81 -3 4 -32 10.94 8.47 3 4 32 5.09 7.45 -3 4 -32 11.15 7.28 4 5 -32 0.47 6.70 -3 -5 32 39.14 5.79 3 -5 -32 31.13 6.60 3 -5 -32 29.29 5.59 -3 -5 32 47.85 6.93 3 -5 -32 28.41 6.10 3 -5 -32 30.47 7.06 3 -5 -32 45.69 7.13 3 5 -32 28.98 6.30 3 5 -32 41.87 8.23 -3 5 32 39.89 7.99 3 5 -32 42.27 5.87 -3 5 32 34.93 5.80 3 5 -32 42.59 6.16 -3 5 32 32.68 6.34 -3 5 32 51.34 7.05 3 5 -32 35.83 6.41 2 -5 -32 2.09 5.41 -2 -5 32 1.76 5.14 -2 -5 32 5.47 6.34 2 -5 -32 2.74 6.53 2 -5 -32 2.05 5.35 2 -5 -32 5.07 5.94 2 5 -32 1.69 5.12 -2 5 32 4.58 5.49 2 5 -32 4.06 5.68 -2 5 32 6.75 5.19 2 5 -32 -3.15 5.00 2 5 -32 6.53 7.83 2 5 -32 1.54 6.28 -2 5 32 4.08 7.05 -2 5 32 8.61 6.50 1 -5 -32 12.31 5.64 -1 -5 32 13.02 5.24 1 -5 -32 17.01 6.24 -1 -5 32 18.83 6.42 1 -5 -32 14.84 5.48 1 -5 -32 6.81 6.56 1 5 -32 19.82 7.96 -1 5 32 18.90 5.23 -1 5 32 14.78 5.72 1 5 -32 13.62 5.31 -1 5 32 10.32 4.80 -1 5 32 11.61 6.86 1 5 -32 16.74 5.73 1 5 -32 14.85 5.32 -1 5 32 6.73 6.18 1 5 -32 8.43 6.04 0 -5 -32 91.35 8.86 0 -5 -32 90.87 9.12 0 -5 -32 79.94 10.20 0 -5 -32 63.47 7.80 0 -5 32 91.03 8.09 0 -5 32 86.37 9.75 0 5 -32 60.90 9.16 0 5 32 91.95 7.99 0 5 32 88.72 10.72 0 5 32 73.03 9.56 0 5 -32 82.54 9.37 0 5 -32 80.37 10.64 0 5 -32 81.25 8.99 0 5 32 65.77 8.44 0 5 -32 74.45 7.86 0 5 32 87.78 8.07 -1 -5 -32 3.44 5.82 -1 -5 -32 3.88 6.71 -1 -5 -32 5.66 5.74 1 -5 32 -0.48 6.17 1 -5 32 -2.16 5.06 -1 -5 -32 5.45 6.24 1 5 32 5.07 5.58 1 5 32 3.29 5.76 -1 5 -32 0.99 6.63 1 5 32 1.28 7.25 -1 5 -32 7.75 8.49 -1 5 -32 2.29 5.87 1 5 32 2.73 5.11 1 5 32 2.28 5.41 -1 5 -32 4.63 5.26 -2 -5 -32 6.42 7.28 -2 5 -32 11.04 7.55 -2 5 -32 4.39 8.62 -1 -6 32 54.45 7.23 1 -6 -32 57.08 7.53 1 -6 -32 48.95 6.41 -1 6 32 55.66 5.83 1 6 -32 49.48 6.16 1 6 -32 57.26 9.13 -1 6 32 59.58 8.44 -1 6 32 50.35 6.38 1 6 -32 62.56 7.72 4 0 -33 3.54 11.30 4 0 -33 -1.28 5.79 4 0 -33 -0.62 5.44 -4 0 33 1.81 5.11 4 0 -33 -0.31 4.42 -4 0 33 0.67 6.02 4 0 -33 0.45 4.77 4 0 -33 -4.67 7.23 4 0 -33 2.90 5.99 3 0 -33 4.42 7.14 3 0 -33 0.41 6.93 -3 0 33 -1.77 6.53 -3 0 33 -1.37 6.95 3 0 -33 2.36 5.88 3 0 -33 0.35 5.39 3 0 -33 -1.27 4.87 3 0 -33 -0.09 4.37 -3 0 33 -2.28 5.00 -2 0 33 4.43 6.15 -2 0 33 0.13 7.33 2 0 -33 -1.50 4.46 2 0 -33 2.06 6.52 2 0 -33 4.18 6.63 -2 0 33 -3.43 6.25 2 0 -33 1.43 6.99 2 0 -33 -1.71 7.53 1 0 -33 -4.94 4.36 1 0 -33 1.89 6.72 1 0 -33 -3.64 7.15 1 0 -33 -4.77 7.01 -1 0 33 0.73 6.59 -1 0 33 -0.03 6.45 0 0 -33 2.45 7.22 0 0 -33 4.46 5.72 0 0 -33 2.74 4.73 0 0 -33 5.86 6.73 0 0 33 2.52 7.83 0 0 33 -0.93 6.53 1 0 33 -1.83 6.36 -1 0 -33 -5.08 4.82 1 0 33 0.19 6.48 -1 0 -33 3.13 7.02 -1 0 -33 2.82 6.09 1 0 33 1.25 5.90 -1 0 -33 0.60 7.54 2 0 33 -2.78 5.05 -2 0 -33 -0.99 8.49 2 0 33 2.57 7.58 -2 0 -33 3.58 5.28 -2 0 -33 5.25 6.36 -2 0 -33 1.20 11.69 2 0 33 9.96 7.05 -2 0 -33 2.65 6.31 -4 -1 33 22.88 8.29 4 -1 -33 25.73 5.61 4 -1 -33 24.37 5.05 4 -1 -33 25.26 8.58 4 -1 -33 23.36 6.31 4 -1 -33 20.73 4.84 4 -1 -33 28.86 6.24 -4 -1 33 25.21 7.29 -4 -1 33 22.83 5.54 -4 1 33 29.24 7.77 4 1 -33 25.93 5.23 4 1 -33 25.75 6.30 -4 1 33 27.21 7.27 4 1 -33 20.09 4.41 4 1 -33 24.70 7.78 4 1 -33 32.50 8.11 4 1 -33 13.67 5.55 -4 1 33 29.14 5.61 -3 -1 33 11.97 5.09 3 -1 -33 16.85 7.27 -3 -1 33 18.58 7.67 3 -1 -33 18.68 5.96 3 -1 -33 19.31 6.93 3 -1 -33 21.00 4.87 3 -1 -33 14.02 4.81 -3 -1 33 15.04 10.36 3 -1 -33 14.38 5.52 3 1 -33 19.22 7.49 3 1 -33 15.41 5.05 -3 1 33 16.04 7.26 3 1 -33 14.41 7.64 -3 1 33 11.71 5.39 3 1 -33 16.69 4.38 -3 1 33 22.57 7.00 3 1 -33 23.40 5.67 3 1 -33 19.79 7.08 2 -1 -33 10.37 7.19 2 -1 -33 5.63 5.87 -2 -1 33 10.41 6.14 2 -1 -33 2.75 7.37 -2 -1 33 4.41 6.65 2 -1 -33 6.64 4.63 2 -1 -33 6.80 5.18 -2 -1 33 7.22 4.96 2 1 -33 4.93 4.41 2 1 -33 6.01 4.77 -2 1 33 7.23 6.39 2 1 -33 4.47 7.27 -2 1 33 7.35 7.00 -1 -1 33 -1.83 6.24 1 -1 -33 1.96 5.72 -1 -1 33 2.88 5.05 1 -1 -33 0.97 7.28 1 -1 -33 -0.06 4.66 1 -1 -33 -7.64 6.08 -1 -1 33 5.98 7.80 1 -1 -33 -1.92 6.87 -1 1 33 1.76 6.34 1 1 -33 -7.04 8.07 1 1 -33 -0.07 4.33 -1 1 33 -1.10 5.94 1 1 -33 3.71 7.66 -1 1 33 0.56 6.24 1 1 -33 -3.27 6.82 0 -1 -33 31.18 6.47 0 -1 33 35.82 7.64 0 -1 -33 24.82 7.67 0 -1 -33 33.11 8.65 0 -1 -33 32.33 5.19 0 -1 -33 22.13 6.54 0 -1 33 33.96 5.46 0 -1 33 34.10 6.98 0 1 -33 18.55 6.32 0 1 33 25.47 6.67 0 1 33 21.43 6.46 0 1 -33 31.39 6.54 0 1 33 29.45 6.85 0 1 -33 33.09 4.82 0 1 -33 41.33 7.86 0 1 -33 29.17 7.39 -1 -1 -33 1.07 7.43 -1 -1 -33 -0.26 5.11 -1 -1 -33 -2.25 5.99 1 -1 33 1.92 5.08 -1 -1 -33 0.40 5.68 1 -1 33 0.98 7.64 1 -1 33 11.40 6.34 -1 1 -33 4.48 4.73 -1 1 -33 -0.08 7.85 -1 1 -33 4.25 8.12 1 1 33 -2.40 6.69 -1 1 -33 0.71 6.04 1 1 33 0.67 6.34 -1 1 -33 0.11 7.22 -2 -1 -33 113.15 9.14 2 -1 33 109.42 11.11 -2 -1 -33 110.30 12.14 2 -1 33 114.88 8.60 -2 -1 -33 108.76 9.26 -2 -1 -33 103.52 12.11 -2 -1 -33 105.25 10.06 -2 1 -33 112.83 9.91 2 1 33 98.42 11.45 -2 1 -33 114.76 8.35 2 1 33 100.13 10.91 2 1 33 97.75 10.58 4 -2 -33 14.10 6.22 -4 -2 33 14.87 5.30 -4 -2 33 11.69 6.86 4 -2 -33 10.04 8.28 4 -2 -33 11.86 5.47 4 -2 -33 12.95 7.48 4 -2 -33 13.59 5.56 4 -2 -33 8.66 4.93 4 -2 -33 9.21 6.30 4 2 -33 7.51 4.09 -4 2 33 7.63 5.34 4 2 -33 4.88 5.18 4 2 -33 12.58 7.58 -4 2 33 16.33 5.51 4 2 -33 7.84 6.02 4 2 -33 6.79 5.71 4 2 -33 11.29 5.70 -4 2 33 14.57 7.41 -4 2 33 10.83 6.39 4 2 -33 1.55 7.31 -3 -2 33 21.26 6.93 3 -2 -33 17.78 8.60 -3 -2 33 23.68 7.88 -3 -2 33 25.09 5.48 3 -2 -33 24.94 4.88 3 -2 -33 26.90 5.11 3 -2 -33 24.16 8.03 3 -2 -33 22.63 6.22 3 -2 -33 23.61 5.76 3 -2 -33 26.10 6.48 -3 2 33 23.48 7.12 -3 2 33 27.57 6.95 3 2 -33 30.58 5.63 -3 2 33 23.00 6.79 3 2 -33 25.19 7.45 3 2 -33 25.84 5.29 3 2 -33 30.76 7.72 3 2 -33 23.12 4.76 -2 -2 33 -1.14 7.06 -2 -2 33 2.79 5.04 2 -2 -33 1.41 5.87 2 -2 -33 4.37 4.85 2 -2 -33 -0.81 8.17 2 -2 -33 0.76 5.24 -2 2 33 -2.35 6.60 2 2 -33 -0.33 6.61 -2 2 33 2.72 6.75 -2 2 33 0.07 7.63 2 2 -33 3.29 7.32 2 2 -33 5.94 4.04 2 2 -33 1.34 4.90 1 -2 -33 -0.59 5.63 -1 -2 33 -4.18 7.80 -1 -2 33 2.69 7.86 1 -2 -33 -2.12 7.78 1 -2 -33 2.60 5.02 1 -2 -33 -0.90 5.51 -1 -2 33 7.06 5.08 1 2 -33 -0.02 5.81 1 2 -33 1.99 7.25 1 2 -33 -4.16 7.43 -1 2 33 1.11 6.76 -1 2 33 2.25 6.73 -1 2 33 4.80 4.81 1 2 -33 -1.70 4.20 0 -2 -33 3.93 5.21 0 -2 -33 6.64 5.07 0 -2 -33 -1.84 5.91 0 -2 33 6.79 6.95 0 -2 -33 4.41 7.41 0 -2 -33 -2.25 8.79 0 -2 33 3.97 7.73 0 -2 33 3.09 4.91 0 2 -33 9.30 6.68 0 2 33 4.03 6.71 0 2 -33 3.39 5.31 0 2 33 4.55 4.88 0 2 -33 2.70 7.14 0 2 -33 2.82 4.28 0 2 33 10.68 6.91 0 2 -33 5.51 9.97 1 -2 33 36.72 8.08 1 -2 33 47.12 5.81 -1 -2 -33 35.75 5.84 -1 -2 -33 42.02 7.82 -1 -2 -33 33.56 6.77 -1 -2 -33 38.49 6.21 -1 2 -33 29.46 6.59 1 2 33 37.75 7.35 -1 2 -33 26.58 4.97 1 2 33 30.49 7.08 -1 2 -33 35.91 6.12 -1 2 -33 29.75 8.04 1 2 33 35.12 5.70 -1 2 -33 43.66 8.08 -2 -2 -33 -3.03 7.47 2 -2 33 -0.22 7.77 2 -2 33 5.90 5.24 -2 -2 -33 0.34 5.62 2 -2 33 0.81 7.51 -2 -2 -33 3.78 6.51 -2 -2 -33 -5.45 5.86 2 2 33 4.75 5.07 -2 2 -33 3.88 8.32 -2 2 -33 1.21 7.69 -2 2 -33 -1.23 6.35 -2 2 -33 -2.32 6.86 -2 2 -33 3.78 4.91 2 2 33 3.22 6.93 2 2 33 -1.48 6.59 3 -3 -33 7.80 5.00 -3 -3 33 5.15 6.62 -3 -3 33 6.49 5.27 3 -3 -33 -0.92 6.70 3 -3 -33 -1.47 5.33 3 -3 -33 -3.05 6.06 3 -3 -33 -3.13 6.41 -3 3 33 8.65 6.01 3 3 -33 4.36 5.31 3 3 -33 -2.91 3.76 -3 3 33 10.91 5.51 3 3 -33 4.88 5.11 3 3 -33 1.49 6.67 3 3 -33 4.57 7.52 -3 3 33 -0.39 7.05 2 -3 -33 0.09 6.02 2 -3 -33 5.85 5.66 2 -3 -33 3.56 7.00 2 -3 -33 6.33 5.12 -2 -3 33 10.65 6.53 -2 -3 33 3.15 5.17 2 3 -33 0.96 4.98 2 3 -33 -1.86 3.65 2 3 -33 5.42 7.04 -2 3 33 4.21 5.15 2 3 -33 0.94 7.06 -2 3 33 10.91 7.07 -2 3 33 6.09 6.62 2 3 -33 6.28 7.56 -2 3 33 8.09 5.33 -1 -3 33 2.16 10.23 -1 -3 33 -3.29 4.89 1 -3 -33 -3.24 5.54 -1 -3 33 -1.04 6.43 1 -3 -33 -1.24 5.80 1 -3 -33 -0.37 6.97 1 -3 -33 0.11 5.06 1 3 -33 -2.34 7.31 -1 3 33 -1.08 8.59 -1 3 33 0.42 6.09 -1 3 33 -7.90 4.91 1 3 -33 2.29 5.84 1 3 -33 -4.35 3.67 1 3 -33 -5.38 7.07 -1 3 33 -3.50 6.90 1 3 -33 0.38 7.03 1 3 -33 1.21 4.90 0 -3 -33 95.50 11.06 0 -3 33 74.47 10.11 0 -3 33 91.99 8.30 0 -3 -33 81.64 8.65 0 -3 -33 91.25 9.03 0 -3 -33 81.51 9.78 0 -3 33 77.28 9.59 0 3 -33 75.03 8.75 0 3 33 61.55 7.21 0 3 -33 82.11 9.31 0 3 -33 80.68 8.35 0 3 33 87.63 10.64 0 3 33 82.76 8.20 0 3 33 77.61 10.45 -1 -3 -33 -2.74 7.19 1 -3 33 8.78 5.23 -1 -3 -33 3.31 5.90 -1 -3 -33 0.47 6.33 1 -3 33 -4.79 6.66 1 -3 33 1.76 8.48 -1 -3 -33 -0.80 5.41 -1 3 -33 -0.35 6.14 -1 3 -33 -2.03 6.20 1 3 33 -1.58 6.78 1 3 33 1.93 7.38 1 3 33 1.27 5.67 1 3 33 -0.97 5.21 1 3 33 4.31 5.20 -1 3 -33 3.29 8.15 -1 3 -33 0.57 5.46 -1 3 -33 0.52 7.82 2 -4 -33 -5.69 6.06 -2 -4 33 1.20 5.40 2 -4 -33 4.31 7.14 2 -4 -33 2.89 5.65 2 -4 -33 -2.22 5.16 -2 -4 33 -5.74 6.23 2 4 -33 0.22 8.02 2 4 -33 6.74 5.23 -2 4 33 -1.48 6.60 2 4 -33 -3.48 6.00 -2 4 33 7.44 7.63 -2 4 33 1.30 5.33 2 4 -33 3.01 6.57 2 4 -33 -2.85 9.12 -2 4 33 -2.75 5.29 1 -4 -33 35.29 6.61 1 -4 -33 32.41 5.75 -1 -4 33 25.20 5.59 1 -4 -33 27.08 7.39 1 -4 -33 21.18 5.94 -1 -4 33 30.50 7.00 -1 4 33 23.29 5.94 1 4 -33 46.20 8.57 1 4 -33 25.03 6.18 -1 4 33 27.96 7.01 1 4 -33 16.74 7.65 1 4 -33 21.83 7.08 -1 4 33 20.31 7.69 1 4 -33 29.04 5.78 -1 4 33 27.21 5.50 0 -4 -33 16.88 5.92 0 -4 -33 19.77 7.26 0 -4 -33 20.77 5.76 0 -4 33 27.78 7.17 0 -4 33 23.46 5.55 0 -4 -33 17.30 6.75 0 4 -33 24.07 8.62 0 4 -33 19.82 5.70 0 4 33 22.86 7.60 0 4 33 25.57 5.55 0 4 -33 14.33 7.06 0 4 33 27.99 7.07 1 0 -34 2.13 7.35 1 0 -34 6.81 8.30 0 0 0 0.00 0.00 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7462 _exptl_absorpt_correction_T_min 0.6659 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71096 10.820 12.289 23.450 89.995 93.774 89.997 ) _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 85147 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br01 Br 0.19481(2) 0.73378(2) 0.30497(2) 0.02027(4) Uani 1 1 d . . . . . N1 N 0.15644(8) 0.35561(7) 0.36645(4) 0.01210(15) Uani 1 1 d . . . . . C27 C 0.27532(12) 0.34227(11) 0.54215(5) 0.0243(2) Uani 1 1 d . . . . . H27 H 0.306216 0.339106 0.580943 0.029 Uiso 1 1 calc R U . . . C26 C 0.22309(13) 0.25087(11) 0.51579(5) 0.0234(2) Uani 1 1 d . . . . . H26 H 0.217200 0.185614 0.537175 0.028 Uiso 1 1 calc R U . . . C25 C 0.17874(11) 0.25220(9) 0.45843(5) 0.0168(2) Uani 1 1 d . . . . . C24 C 0.19221(9) 0.34958(9) 0.42777(4) 0.01332(18) Uani 1 1 d . . . . . C13 C 0.22762(9) 0.32496(8) 0.32621(4) 0.01137(17) Uani 1 1 d . . . . . C14 C 0.17936(9) 0.37373(8) 0.26863(4) 0.01226(17) Uani 1 1 d . . . . . C21 C 0.14616(10) 0.29075(9) 0.22046(4) 0.01440(18) Uani 1 1 d . . . . . H21A H 0.217552 0.241595 0.216229 0.017 Uiso 1 1 calc R U . . . H21B H 0.075135 0.245867 0.231048 0.017 Uiso 1 1 calc R U . . . C20 C 0.11262(10) 0.34764(10) 0.16319(4) 0.0184(2) Uani 1 1 d . . . . . H20A H 0.097067 0.291955 0.133077 0.022 Uiso 1 1 calc R U . . . H20B H 0.035374 0.389986 0.166120 0.022 Uiso 1 1 calc R U . . . C19 C 0.21566(11) 0.42370(10) 0.14627(5) 0.0196(2) Uani 1 1 d . . . . . H19A H 0.188627 0.462285 0.110574 0.024 Uiso 1 1 calc R U . . . H19B H 0.290289 0.380444 0.139007 0.024 Uiso 1 1 calc R U . . . C35 C 0.17927(12) 0.04553(10) 0.44773(6) 0.0252(2) Uani 1 1 d . . . . . H35A H 0.263544 0.051099 0.434943 0.038 Uiso 1 1 calc R U . . . H35B H 0.135500 -0.014358 0.427523 0.038 Uiso 1 1 calc R U . . . H35C H 0.183177 0.031474 0.488902 0.038 Uiso 1 1 calc R U . . . C33 C 0.10980(11) 0.15249(9) 0.43491(5) 0.0188(2) Uani 1 1 d . . . . . H33 H 0.096091 0.160557 0.392575 0.023 Uiso 1 1 calc R U . . . C28 C 0.28228(11) 0.43829(10) 0.51166(5) 0.0198(2) Uani 1 1 d . . . . . H28 H 0.315871 0.501263 0.530400 0.024 Uiso 1 1 calc R U . . . C29 C 0.24116(10) 0.44514(9) 0.45397(4) 0.01474(18) Uani 1 1 d . . . . . C16 C 0.02919(9) 0.39727(10) 0.34197(4) 0.01614(19) Uani 1 1 d . . . . . C23 C -0.02973(11) 0.48251(12) 0.37886(5) 0.0244(2) Uani 1 1 d . . . . . H23A H 0.016787 0.550821 0.377379 0.037 Uiso 1 1 calc R U . . . H23B H -0.028103 0.456670 0.418403 0.037 Uiso 1 1 calc R U . . . H23C H -0.115773 0.494825 0.364511 0.037 Uiso 1 1 calc R U . . . C22 C -0.05680(10) 0.29849(11) 0.33468(5) 0.0220(2) Uani 1 1 d . . . . . H22A H -0.131322 0.318685 0.311014 0.033 Uiso 1 1 calc R U . . . H22B H -0.080472 0.274160 0.372208 0.033 Uiso 1 1 calc R U . . . H22C H -0.013645 0.239394 0.316134 0.033 Uiso 1 1 calc R U . . . C15 C 0.06538(10) 0.44089(9) 0.28434(4) 0.01555(19) Uani 1 1 d . . . . . H15A H 0.086561 0.519198 0.287262 0.019 Uiso 1 1 calc R U . . . H15B H -0.003818 0.431658 0.254974 0.019 Uiso 1 1 calc R U . . . B1 B 0.34259(11) 0.24401(9) 0.33894(5) 0.01228(19) Uani 1 1 d . . . . . C1 C 0.50151(9) 0.25582(9) 0.31953(5) 0.01391(18) Uani 1 1 d . . . . . C4 C 0.46772(10) 0.24346(9) 0.38083(5) 0.01375(18) Uani 1 1 d . . . . . C10 C 0.48937(10) 0.12791(9) 0.40174(4) 0.01524(19) Uani 1 1 d . . . . . C12 C 0.58382(11) 0.10400(10) 0.44995(5) 0.0225(2) Uani 1 1 d . . . . . H12A H 0.587268 0.025320 0.456821 0.034 Uiso 1 1 calc R U . . . H12B H 0.560410 0.141273 0.484556 0.034 Uiso 1 1 calc R U . . . H12C H 0.665368 0.129805 0.439910 0.034 Uiso 1 1 calc R U . . . C9 C 0.42544(10) 0.05709(9) 0.36820(4) 0.01509(18) Uani 1 1 d . . . . . C11 C 0.43169(11) -0.06489(9) 0.36971(5) 0.0206(2) Uani 1 1 d . . . . . H11A H 0.470686 -0.091368 0.335817 0.031 Uiso 1 1 calc R U . . . H11B H 0.347689 -0.094726 0.370192 0.031 Uiso 1 1 calc R U . . . H11C H 0.480796 -0.088275 0.404122 0.031 Uiso 1 1 calc R U . . . C3 C 0.35064(9) 0.11517(8) 0.32022(4) 0.01329(17) Uani 1 1 d . . . . . C8 C 0.24652(10) 0.05028(9) 0.28981(5) 0.01714(19) Uani 1 1 d . . . . . H8A H 0.204291 0.095481 0.260127 0.026 Uiso 1 1 calc R U . . . H8B H 0.187150 0.027986 0.317394 0.026 Uiso 1 1 calc R U . . . H8C H 0.280919 -0.014491 0.272289 0.026 Uiso 1 1 calc R U . . . C2 C 0.43556(9) 0.18153(8) 0.28471(4) 0.01342(18) Uani 1 1 d . . . . . C7 C 0.44510(10) 0.17354(10) 0.22110(5) 0.0178(2) Uani 1 1 d . . . . . H7A H 0.427306 0.244748 0.203591 0.027 Uiso 1 1 calc R U . . . H7B H 0.385111 0.119957 0.205260 0.027 Uiso 1 1 calc R U . . . H7C H 0.529071 0.150733 0.213081 0.027 Uiso 1 1 calc R U . . . C5 C 0.51287(10) 0.33284(10) 0.42134(5) 0.0199(2) Uani 1 1 d . . . . . H5A H 0.470840 0.326868 0.456953 0.030 Uiso 1 1 calc R U . . . H5B H 0.494487 0.403884 0.403756 0.030 Uiso 1 1 calc R U . . . H5C H 0.602560 0.325706 0.429558 0.030 Uiso 1 1 calc R U . . . C6 C 0.58505(10) 0.34318(10) 0.29977(5) 0.0198(2) Uani 1 1 d . . . . . H6A H 0.612043 0.324361 0.261949 0.030 Uiso 1 1 calc R U . . . H6B H 0.657646 0.349875 0.326812 0.030 Uiso 1 1 calc R U . . . H6C H 0.540213 0.412561 0.297583 0.030 Uiso 1 1 calc R U . . . C18 C 0.24798(11) 0.50699(9) 0.19346(5) 0.0189(2) Uani 1 1 d . . . . . H18A H 0.175677 0.554825 0.198218 0.023 Uiso 1 1 calc R U . . . H18B H 0.317645 0.553051 0.182405 0.023 Uiso 1 1 calc R U . . . C17 C 0.28436(10) 0.44960(9) 0.25022(4) 0.01482(18) Uani 1 1 d . . . . . H17A H 0.302792 0.504945 0.280250 0.018 Uiso 1 1 calc R U . . . H17B H 0.360442 0.406193 0.246163 0.018 Uiso 1 1 calc R U . . . C30 C 0.24792(10) 0.55579(9) 0.42472(5) 0.01632(19) Uani 1 1 d . . . . . H30 H 0.206120 0.549178 0.385592 0.020 Uiso 1 1 calc R U . . . C32 C 0.38052(11) 0.59647(10) 0.41856(5) 0.0214(2) Uani 1 1 d . . . . . H32A H 0.429140 0.587779 0.455000 0.032 Uiso 1 1 calc R U . . . H32B H 0.378438 0.673548 0.407741 0.032 Uiso 1 1 calc R U . . . H32C H 0.418720 0.554083 0.389001 0.032 Uiso 1 1 calc R U . . . C31 C 0.17745(12) 0.64172(10) 0.45771(5) 0.0237(2) Uani 1 1 d . . . . . H31A H 0.096011 0.612948 0.466014 0.036 Uiso 1 1 calc R U . . . H31B H 0.166676 0.707816 0.434533 0.036 Uiso 1 1 calc R U . . . H31C H 0.224828 0.659072 0.493588 0.036 Uiso 1 1 calc R U . . . C34 C -0.01709(12) 0.14727(11) 0.46079(6) 0.0255(2) Uani 1 1 d . . . . . H34A H -0.005328 0.131162 0.501673 0.038 Uiso 1 1 calc R U . . . H34B H -0.067436 0.089879 0.441775 0.038 Uiso 1 1 calc R U . . . H34C H -0.059398 0.217446 0.455405 0.038 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br01 0.02003(6) 0.01855(6) 0.02183(6) 0.00337(4) -0.00165(4) 0.00046(4) N1 0.0103(3) 0.0159(4) 0.0100(4) -0.0009(3) 0.0004(3) -0.0006(3) C27 0.0322(6) 0.0296(6) 0.0105(4) 0.0010(4) -0.0017(4) -0.0047(5) C26 0.0319(6) 0.0250(6) 0.0134(5) 0.0048(4) 0.0020(4) -0.0054(5) C25 0.0181(5) 0.0200(5) 0.0127(5) 0.0000(4) 0.0035(4) -0.0036(4) C24 0.0124(4) 0.0190(5) 0.0087(4) -0.0016(3) 0.0016(3) -0.0010(3) C13 0.0106(4) 0.0131(4) 0.0104(4) -0.0013(3) 0.0008(3) -0.0024(3) C14 0.0116(4) 0.0160(4) 0.0092(4) -0.0005(3) 0.0007(3) 0.0013(3) C21 0.0146(4) 0.0175(5) 0.0110(4) -0.0021(3) -0.0001(3) -0.0001(4) C20 0.0185(5) 0.0255(5) 0.0110(4) -0.0016(4) -0.0011(4) 0.0009(4) C19 0.0235(5) 0.0244(5) 0.0111(4) 0.0030(4) 0.0020(4) 0.0019(4) C35 0.0292(6) 0.0211(5) 0.0263(6) 0.0029(4) 0.0101(5) -0.0030(5) C33 0.0202(5) 0.0196(5) 0.0170(5) -0.0006(4) 0.0052(4) -0.0059(4) C28 0.0239(5) 0.0228(5) 0.0125(4) -0.0032(4) -0.0006(4) -0.0035(4) C29 0.0153(4) 0.0174(5) 0.0116(4) -0.0022(3) 0.0012(3) -0.0010(4) C16 0.0099(4) 0.0254(5) 0.0130(4) -0.0028(4) 0.0000(3) 0.0029(4) C23 0.0160(5) 0.0386(7) 0.0187(5) -0.0081(5) 0.0014(4) 0.0097(5) C22 0.0124(5) 0.0352(6) 0.0183(5) -0.0009(5) 0.0009(4) -0.0049(4) C15 0.0133(4) 0.0204(5) 0.0128(4) -0.0004(4) -0.0001(3) 0.0050(4) B1 0.0117(5) 0.0140(5) 0.0113(5) -0.0009(4) 0.0013(4) -0.0001(4) C1 0.0103(4) 0.0154(4) 0.0161(5) 0.0004(3) 0.0016(3) 0.0017(3) C4 0.0118(4) 0.0164(4) 0.0128(4) -0.0016(3) -0.0006(3) 0.0004(3) C10 0.0141(4) 0.0177(5) 0.0139(4) 0.0008(4) 0.0007(3) 0.0024(4) C12 0.0225(5) 0.0249(6) 0.0192(5) 0.0024(4) -0.0053(4) 0.0039(4) C9 0.0156(4) 0.0157(5) 0.0141(4) 0.0015(3) 0.0019(3) 0.0018(4) C11 0.0247(5) 0.0152(5) 0.0218(5) 0.0016(4) 0.0005(4) 0.0025(4) C3 0.0136(4) 0.0130(4) 0.0133(4) -0.0009(3) 0.0011(3) -0.0004(3) C8 0.0179(5) 0.0148(5) 0.0184(5) -0.0023(4) -0.0012(4) -0.0020(4) C2 0.0124(4) 0.0146(4) 0.0135(4) -0.0008(3) 0.0024(3) 0.0025(3) C7 0.0191(5) 0.0218(5) 0.0130(4) -0.0014(4) 0.0045(4) 0.0032(4) C5 0.0180(5) 0.0207(5) 0.0204(5) -0.0066(4) -0.0044(4) 0.0002(4) C6 0.0134(4) 0.0207(5) 0.0253(5) 0.0029(4) 0.0018(4) -0.0027(4) C18 0.0227(5) 0.0195(5) 0.0148(5) 0.0039(4) 0.0019(4) 0.0001(4) C17 0.0145(4) 0.0163(5) 0.0137(4) 0.0007(3) 0.0014(3) -0.0015(4) C30 0.0184(5) 0.0154(5) 0.0150(4) -0.0015(4) 0.0000(4) 0.0004(4) C32 0.0200(5) 0.0185(5) 0.0256(6) 0.0010(4) 0.0001(4) -0.0025(4) C31 0.0278(6) 0.0220(5) 0.0211(5) -0.0065(4) 0.0006(4) 0.0046(5) C34 0.0233(6) 0.0287(6) 0.0255(6) -0.0010(5) 0.0096(5) -0.0082(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C24 N1 C16 123.58(9) . . ? C13 N1 C24 124.22(10) . . ? C13 N1 C16 112.19(11) . . ? C26 C27 H27 120.2 . . ? C28 C27 H27 120.2 . . ? C28 C27 C26 119.63(12) . . ? C27 C26 H26 119.2 . . ? C27 C26 C25 121.64(11) . . ? C25 C26 H26 119.2 . . ? C26 C25 C24 117.47(11) . . ? C26 C25 C33 118.00(11) . . ? C24 C25 C33 124.31(11) . . ? C25 C24 N1 120.98(10) . . ? C25 C24 C29 122.12(11) . . ? C29 C24 N1 116.90(10) . . ? N1 C13 C14 109.86(11) . . ? N1 C13 B1 121.84(10) . . ? C14 C13 B1 128.25(9) . . ? C13 C14 C21 115.78(11) . . ? C13 C14 C15 103.17(9) . . ? C13 C14 C17 105.45(9) . . ? C21 C14 C15 112.03(10) . . ? C21 C14 C17 109.33(10) . . ? C15 C14 C17 110.77(10) . . ? C14 C21 H21A 109.3 . . ? C14 C21 H21B 109.3 . . ? H21A C21 H21B 107.9 . . ? C20 C21 C14 111.71(11) . . ? C20 C21 H21A 109.3 . . ? C20 C21 H21B 109.3 . . ? C21 C20 H20A 109.3 . . ? C21 C20 H20B 109.3 . . ? H20A C20 H20B 107.9 . . ? C19 C20 C21 111.80(10) . . ? C19 C20 H20A 109.3 . . ? C19 C20 H20B 109.3 . . ? C20 C19 H19A 109.5 . . ? C20 C19 H19B 109.5 . . ? C20 C19 C18 110.89(10) . . ? H19A C19 H19B 108.0 . . ? C18 C19 H19A 109.5 . . ? C18 C19 H19B 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C33 C35 H35A 109.5 . . ? C33 C35 H35B 109.5 . . ? C33 C35 H35C 109.5 . . ? C25 C33 C35 113.40(11) . . ? C25 C33 H33 108.6 . . ? C25 C33 C34 108.62(10) . . ? C35 C33 H33 108.6 . . ? C35 C33 C34 108.97(10) . . ? C34 C33 H33 108.6 . . ? C27 C28 H28 119.1 . . ? C27 C28 C29 121.78(11) . . ? C29 C28 H28 119.1 . . ? C24 C29 C30 124.87(11) . . ? C28 C29 C24 117.24(10) . . ? C28 C29 C30 117.85(10) . . ? C23 C16 N1 114.32(10) . . ? C23 C16 C22 109.54(11) . . ? C23 C16 C15 113.73(11) . . ? C22 C16 N1 107.39(10) . . ? C15 C16 N1 99.91(10) . . ? C15 C16 C22 111.54(10) . . ? C16 C23 H23A 109.5 . . ? C16 C23 H23B 109.5 . . ? C16 C23 H23C 109.5 . . ? H23A C23 H23B 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C16 C22 H22A 109.5 . . ? C16 C22 H22B 109.5 . . ? C16 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C14 C15 H15A 110.5 . . ? C14 C15 H15B 110.5 . . ? C16 C15 C14 106.13(9) . . ? C16 C15 H15A 110.5 . . ? C16 C15 H15B 110.5 . . ? H15A C15 H15B 108.7 . . ? C13 B1 C1 129.75(10) . . ? C13 B1 C4 136.19(10) . . ? C13 B1 C3 126.87(9) . . ? C13 B1 C2 125.54(10) . . ? C1 B1 C2 44.74(6) . . ? C4 B1 C1 52.04(9) . . ? C4 B1 C3 95.82(8) . . ? C4 B1 C2 86.90(10) . . ? C3 B1 C1 86.70(7) . . ? C3 B1 C2 51.23(6) . . ? C4 C1 B1 57.43(7) . . ? C2 C1 B1 68.71(9) . . ? C2 C1 C4 110.26(10) . . ? C2 C1 C6 125.83(11) . . ? C6 C1 B1 137.49(9) . . ? C6 C1 C4 123.68(10) . . ? C1 C4 B1 70.53(10) . . ? C10 C4 B1 107.81(9) . . ? C10 C4 C1 111.09(9) . . ? C5 C4 B1 126.96(10) . . ? C5 C4 C1 115.87(10) . . ? C5 C4 C10 116.09(11) . . ? C12 C10 C4 120.67(10) . . ? C9 C10 C4 110.86(11) . . ? C9 C10 C12 128.08(11) . . ? C10 C12 H12A 109.5 . . ? C10 C12 H12B 109.5 . . ? C10 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C10 C9 C11 128.01(11) . . ? C10 C9 C3 111.15(11) . . ? C11 C9 C3 120.47(10) . . ? C9 C11 H11A 109.5 . . ? C9 C11 H11B 109.5 . . ? C9 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C9 C3 B1 106.75(9) . . ? C8 C3 B1 125.41(9) . . ? C8 C3 C9 116.35(10) . . ? C2 C3 B1 71.01(8) . . ? C2 C3 C9 110.33(11) . . ? C2 C3 C8 118.69(11) . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C1 C2 B1 66.54(9) . . ? C1 C2 C3 109.57(11) . . ? C1 C2 C7 124.04(10) . . ? C3 C2 B1 57.76(8) . . ? C7 C2 B1 142.04(9) . . ? C7 C2 C3 126.34(10) . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C19 C18 H18A 109.5 . . ? C19 C18 H18B 109.5 . . ? C19 C18 C17 110.76(11) . . ? H18A C18 H18B 108.1 . . ? C17 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? C14 C17 H17A 109.3 . . ? C14 C17 H17B 109.3 . . ? C18 C17 C14 111.52(10) . . ? C18 C17 H17A 109.3 . . ? C18 C17 H17B 109.3 . . ? H17A C17 H17B 108.0 . . ? C29 C30 H30 108.0 . . ? C29 C30 C32 113.89(9) . . ? C29 C30 C31 110.13(11) . . ? C32 C30 H30 108.0 . . ? C32 C30 C31 108.68(11) . . ? C31 C30 H30 108.0 . . ? C30 C32 H32A 109.5 . . ? C30 C32 H32B 109.5 . . ? C30 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C30 C31 H31A 109.5 . . ? C30 C31 H31B 109.5 . . ? C30 C31 H31C 109.5 . . ? H31A C31 H31B 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C33 C34 H34A 109.5 . . ? C33 C34 H34B 109.5 . . ? C33 C34 H34C 109.5 . . ? H34A C34 H34B 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C24 1.468(2) . ? N1 C13 1.3118(16) . ? N1 C16 1.5430(18) . ? C27 H27 0.9500 . ? C27 C26 1.3842(19) . ? C27 C28 1.3840(19) . ? C26 H26 0.9500 . ? C26 C25 1.399(2) . ? C25 C24 1.4084(17) . ? C25 C33 1.5186(18) . ? C24 C29 1.4119(16) . ? C13 C14 1.538(2) . ? C13 B1 1.6044(18) . ? C14 C21 1.5468(18) . ? C14 C15 1.5471(18) . ? C14 C17 1.5517(17) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 C20 1.537(2) . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C20 C19 1.5262(19) . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C19 C18 1.5312(19) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C35 C33 1.5332(19) . ? C33 H33 1.0000 . ? C33 C34 1.537(2) . ? C28 H28 0.9500 . ? C28 C29 1.400(2) . ? C29 C30 1.5265(17) . ? C16 C23 1.5243(18) . ? C16 C22 1.5313(19) . ? C16 C15 1.530(2) . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? B1 C1 1.812(2) . ? B1 C4 1.619(2) . ? B1 C3 1.6460(18) . ? B1 C2 1.840(2) . ? C1 C4 1.515(2) . ? C1 C2 1.3902(17) . ? C1 C6 1.4957(17) . ? C4 C10 1.5149(17) . ? C4 C5 1.5122(17) . ? C10 C12 1.503(2) . ? C10 C9 1.3352(17) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C9 C11 1.5001(18) . ? C9 C3 1.5204(18) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C3 C8 1.5188(18) . ? C3 C2 1.5172(17) . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C2 C7 1.507(2) . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C18 C17 1.536(2) . ? C17 H17A 0.9900 . ? C17 H17B 0.9900 . ? C30 H30 1.0000 . ? C30 C32 1.534(2) . ? C30 C31 1.5398(18) . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C31 H31A 0.9800 . ? C31 H31B 0.9800 . ? C31 H31C 0.9800 . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C24 C29 C28 -176.33(9) . . . . ? N1 C24 C29 C30 6.11(15) . . . . ? N1 C13 C14 C21 -121.99(10) . . . . ? N1 C13 C14 C15 0.76(11) . . . . ? N1 C13 C14 C17 117.02(11) . . . . ? N1 C13 B1 C1 -131.31(11) . . . . ? N1 C13 B1 C4 -58.09(17) . . . . ? N1 C13 B1 C3 106.69(13) . . . . ? N1 C13 B1 C2 171.46(9) . . . . ? N1 C16 C15 C14 27.37(10) . . . . ? C27 C26 C25 C24 1.69(19) . . . . ? C27 C26 C25 C33 -173.16(12) . . . . ? C27 C28 C29 C24 -0.16(17) . . . . ? C27 C28 C29 C30 177.58(11) . . . . ? C26 C27 C28 C29 -2.0(2) . . . . ? C26 C25 C24 N1 175.56(10) . . . . ? C26 C25 C24 C29 -3.92(16) . . . . ? C26 C25 C33 C35 -50.28(15) . . . . ? C26 C25 C33 C34 71.02(15) . . . . ? C25 C24 C29 C28 3.17(16) . . . . ? C25 C24 C29 C30 -174.39(10) . . . . ? C24 N1 C13 C14 -162.80(9) . . . . ? C24 N1 C13 B1 19.62(15) . . . . ? C24 N1 C16 C23 30.05(15) . . . . ? C24 N1 C16 C22 -91.69(11) . . . . ? C24 N1 C16 C15 151.87(10) . . . . ? C24 C25 C33 C35 135.25(12) . . . . ? C24 C25 C33 C34 -103.45(14) . . . . ? C24 C29 C30 C32 -115.61(12) . . . . ? C24 C29 C30 C31 122.02(13) . . . . ? C13 N1 C24 C25 -83.51(14) . . . . ? C13 N1 C24 C29 95.99(13) . . . . ? C13 N1 C16 C23 -150.88(10) . . . . ? C13 N1 C16 C22 87.38(11) . . . . ? C13 N1 C16 C15 -29.06(11) . . . . ? C13 C14 C21 C20 -173.78(8) . . . . ? C13 C14 C15 C16 -18.83(11) . . . . ? C13 C14 C17 C18 -178.61(8) . . . . ? C13 B1 C1 C4 122.80(12) . . . . ? C13 B1 C1 C2 -103.58(13) . . . . ? C13 B1 C1 C6 16.73(19) . . . . ? C13 B1 C4 C1 -110.99(14) . . . . ? C13 B1 C4 C10 142.31(12) . . . . ? C13 B1 C4 C5 -2.74(19) . . . . ? C13 B1 C3 C9 -144.50(10) . . . . ? C13 B1 C3 C8 -2.99(16) . . . . ? C13 B1 C3 C2 109.24(13) . . . . ? C13 B1 C2 C1 113.30(12) . . . . ? C13 B1 C2 C3 -111.84(12) . . . . ? C13 B1 C2 C7 -2.5(2) . . . . ? C14 C13 B1 C1 51.59(16) . . . . ? C14 C13 B1 C4 124.81(14) . . . . ? C14 C13 B1 C3 -70.41(15) . . . . ? C14 C13 B1 C2 -5.64(16) . . . . ? C14 C21 C20 C19 55.48(12) . . . . ? C21 C14 C15 C16 106.37(12) . . . . ? C21 C14 C17 C18 56.28(12) . . . . ? C21 C20 C19 C18 -55.53(14) . . . . ? C20 C19 C18 C17 56.42(13) . . . . ? C19 C18 C17 C14 -57.60(12) . . . . ? C33 C25 C24 N1 -9.94(16) . . . . ? C33 C25 C24 C29 170.58(10) . . . . ? C28 C27 C26 C25 1.2(2) . . . . ? C28 C29 C30 C32 66.84(14) . . . . ? C28 C29 C30 C31 -55.53(15) . . . . ? C16 N1 C24 C25 95.44(13) . . . . ? C16 N1 C24 C29 -85.05(13) . . . . ? C16 N1 C13 C14 18.14(12) . . . . ? C16 N1 C13 B1 -159.44(9) . . . . ? C23 C16 C15 C14 149.61(9) . . . . ? C22 C16 C15 C14 -85.89(12) . . . . ? C15 C14 C21 C20 68.29(11) . . . . ? C15 C14 C17 C18 -67.65(12) . . . . ? B1 C13 C14 C21 55.40(14) . . . . ? B1 C13 C14 C15 178.14(9) . . . . ? B1 C13 C14 C17 -65.59(14) . . . . ? B1 C1 C4 C10 102.20(9) . . . . ? B1 C1 C4 C5 -122.50(11) . . . . ? B1 C1 C2 C3 -39.51(8) . . . . ? B1 C1 C2 C7 138.08(11) . . . . ? B1 C4 C10 C12 -168.15(10) . . . . ? B1 C4 C10 C9 18.47(12) . . . . ? B1 C3 C2 C1 43.63(9) . . . . ? B1 C3 C2 C7 -133.89(12) . . . . ? C1 B1 C4 C10 -106.70(9) . . . . ? C1 B1 C4 C5 108.25(13) . . . . ? C1 B1 C3 C9 76.28(11) . . . . ? C1 B1 C3 C8 -142.21(11) . . . . ? C1 B1 C3 C2 -29.98(7) . . . . ? C1 B1 C2 C3 134.87(10) . . . . ? C1 B1 C2 C7 -115.83(17) . . . . ? C1 C4 C10 C12 116.41(13) . . . . ? C1 C4 C10 C9 -56.97(13) . . . . ? C4 B1 C1 C2 133.62(10) . . . . ? C4 B1 C1 C6 -106.08(14) . . . . ? C4 B1 C3 C9 24.98(10) . . . . ? C4 B1 C3 C8 166.48(10) . . . . ? C4 B1 C3 C2 -81.29(11) . . . . ? C4 B1 C2 C1 -34.87(8) . . . . ? C4 B1 C2 C3 100.00(9) . . . . ? C4 B1 C2 C7 -150.70(14) . . . . ? C4 C1 C2 B1 40.57(8) . . . . ? C4 C1 C2 C3 1.06(12) . . . . ? C4 C1 C2 C7 178.65(9) . . . . ? C4 C10 C9 C11 172.44(10) . . . . ? C4 C10 C9 C3 -0.54(12) . . . . ? C10 C9 C3 B1 -17.19(12) . . . . ? C10 C9 C3 C8 -162.70(9) . . . . ? C10 C9 C3 C2 58.29(12) . . . . ? C12 C10 C9 C11 -0.33(19) . . . . ? C12 C10 C9 C3 -173.31(10) . . . . ? C9 C3 C2 B1 -101.40(10) . . . . ? C9 C3 C2 C1 -57.76(12) . . . . ? C9 C3 C2 C7 124.71(12) . . . . ? C11 C9 C3 B1 169.23(9) . . . . ? C11 C9 C3 C8 23.71(14) . . . . ? C11 C9 C3 C2 -115.30(11) . . . . ? C3 B1 C1 C4 -100.01(8) . . . . ? C3 B1 C1 C2 33.61(7) . . . . ? C3 B1 C1 C6 153.91(13) . . . . ? C3 B1 C4 C1 81.20(8) . . . . ? C3 B1 C4 C10 -25.50(10) . . . . ? C3 B1 C4 C5 -170.55(10) . . . . ? C3 B1 C2 C1 -134.87(10) . . . . ? C3 B1 C2 C7 109.30(16) . . . . ? C8 C3 C2 B1 120.68(11) . . . . ? C8 C3 C2 C1 164.31(9) . . . . ? C8 C3 C2 C7 -13.21(15) . . . . ? C2 B1 C1 C4 -133.62(10) . . . . ? C2 B1 C1 C6 120.31(16) . . . . ? C2 B1 C4 C1 30.69(7) . . . . ? C2 B1 C4 C10 -76.01(9) . . . . ? C2 B1 C4 C5 138.94(11) . . . . ? C2 B1 C3 C9 106.26(12) . . . . ? C2 B1 C3 C8 -112.23(13) . . . . ? C2 C1 C4 B1 -45.98(9) . . . . ? C2 C1 C4 C10 56.23(12) . . . . ? C2 C1 C4 C5 -168.47(9) . . . . ? C5 C4 C10 C12 -18.79(15) . . . . ? C5 C4 C10 C9 167.83(9) . . . . ? C6 C1 C4 B1 128.72(11) . . . . ? C6 C1 C4 C10 -129.08(12) . . . . ? C6 C1 C4 C5 6.23(15) . . . . ? C6 C1 C2 B1 -133.99(12) . . . . ? C6 C1 C2 C3 -173.50(10) . . . . ? C6 C1 C2 C7 4.09(17) . . . . ? C17 C14 C21 C20 -54.90(12) . . . . ? C17 C14 C15 C16 -131.25(9) . . . . ?