#------------------------------------------------------------------------------ #$Date: 2024-10-10 01:20:23 +0300 (Thu, 10 Oct 2024) $ #$Revision: 295411 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/28/1572853.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572853 loop_ _publ_author_name 'Balayan, Kajal' 'Sharma, Himanshu' 'Vanka, Kumar' 'Gonnade, Rajesh G.' 'Sen, Sakya Singha' _publ_section_title ; Uncovering diverse reactivity of NHCs with diazoalkane: C-H activation, C=C bond formation, and access to N-heterocyclic methylenehydrazine ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC05740F _journal_year 2024 _chemical_formula_moiety 'C15 H30 N4 Si' _chemical_formula_sum 'C15 H30 N4 Si' _chemical_formula_weight 294.52 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-04-10 deposited with the CCDC. 2024-10-07 downloaded from the CCDC. ; _cell_angle_alpha 105.886(4) _cell_angle_beta 94.060(5) _cell_angle_gamma 91.388(4) _cell_formula_units_Z 8 _cell_length_a 10.1752(12) _cell_length_b 18.596(3) _cell_length_c 19.949(3) _cell_measurement_reflns_used 9665 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.11 _cell_measurement_theta_min 2.35 _cell_volume 3617.7(9) _computing_cell_refinement 'SAINT (Bruker, 2016)' _computing_data_collection 'APEX3 (Bruker, 2016)' _computing_data_reduction 'SAINT (Bruker, 2016)' _computing_molecular_graphics 'Bruker SHELXTL, Mercury 2020.20' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_detector 'Photon II CPAD Area Detector' _diffrn_detector_area_resol_mean 7.39 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE Kappa Duo PHOTON II CPAD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0725 _diffrn_reflns_av_unetI/netI 0.0417 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 106350 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.499 _diffrn_reflns_theta_min 2.234 _diffrn_source 'micro-focus sealed tube' _diffrn_source_type 'Incoatech I\mS HB' _exptl_absorpt_coefficient_mu 0.128 _exptl_absorpt_correction_T_max 0.1553 _exptl_absorpt_correction_T_min 0.1167 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.081 _exptl_crystal_description block _exptl_crystal_F_000 1296 _exptl_crystal_size_max 0.320 _exptl_crystal_size_mid 0.240 _exptl_crystal_size_min 0.190 _refine_diff_density_max 0.743 _refine_diff_density_min -0.501 _refine_diff_density_rms 0.098 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.223 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 757 _refine_ls_number_reflns 13424 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.223 _refine_ls_R_factor_all 0.1098 _refine_ls_R_factor_gt 0.1004 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+25.4928P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2341 _refine_ls_wR_factor_ref 0.2381 _reflns_Friedel_coverage 0.000 _reflns_number_gt 11761 _reflns_number_total 13424 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05740f2.cif _cod_data_source_block mo_KB_ItBuTMSCHN2_0m_a _cod_original_cell_volume 3617.7(8) _cod_database_code 1572853 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.960 _shelx_estimated_absorpt_t_max 0.976 _shelx_res_file ; TITL mo_KB_ItBuTMSCHN2_0m_a.res in P-1 mo_KB_ItBuTMSCHN2_0m_a.res created by SHELXL-2018/3 at 23:09:12 on 31-Mar-2024 REM Old TITL mo_KB_ItBuTMSCHN2_0m in P-1 REM SHELXT solution in P-1: R1 0.184, Rweak 0.038, Alpha 0.093 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C66 N10 Si4 CELL 0.71073 10.1752 18.5957 19.9493 105.886 94.060 91.388 ZERR 8 0.0012 0.0025 0.0026 0.004 0.005 0.004 LATT 1 SFAC C H N SI UNIT 120 240 32 8 SIZE 0.32 0.24 0.19 ACTA TEMP -173.150 SIZE 0.19 0.24 0.32 L.S. 10 BOND $H HTAB CONF OMIT -3 51 OMIT -4 2 4 OMIT -1 4 1 OMIT -6 3 1 OMIT -1 4 1 OMIT 3 -10 9 OMIT 3 2 2 OMIT 0 5 3 OMIT 1 3 8 OMIT 0 -5 2 OMIT -2 11 0 OMIT 0 -5 5 OMIT 0 -5 3 OMIT 4 2 4 OMIT 1 -9 6 OMIT -2 8 1 OMIT -5 -6 8 OMIT 3 2 1 OMIT 4 -9 5 OMIT 0 -5 9 OMIT 1 3 2 OMIT 0 -5 8 OMIT 0 -1 2 OMIT 1 3 0 LIST 4 FMAP 2 PLAN 20 WGHT 0.000000 25.492800 FVAR 0.40617 SI1 4 -0.013992 0.803449 0.144238 11.00000 0.01815 0.02117 = 0.02567 0.00704 -0.00229 0.00113 SI2 4 0.874068 0.450101 0.108447 11.00000 0.01488 0.01824 = 0.01523 0.00433 0.00334 0.00041 SI3 4 0.973962 0.306761 0.611977 11.00000 0.01581 0.02166 = 0.01454 0.00385 0.00019 0.00225 SI4 4 1.392369 0.005074 0.139066 11.00000 0.01599 0.02537 = 0.02612 0.00586 0.00644 0.00255 N1 3 0.489610 0.726878 0.227424 11.00000 0.01662 0.01769 = 0.01931 0.00380 -0.00272 0.00019 N2 3 0.524405 0.816944 0.327172 11.00000 0.01997 0.01985 = 0.01830 0.00364 -0.00266 -0.00085 N3 3 0.328755 0.827662 0.263407 11.00000 0.01723 0.02280 = 0.02225 -0.00039 -0.00552 0.00641 N4 3 0.229948 0.794576 0.212658 11.00000 0.01848 0.02167 = 0.01895 0.00266 -0.00036 0.00091 N5 3 0.398580 0.464064 0.296368 11.00000 0.01375 0.02262 = 0.01663 0.00501 0.00541 0.00656 N6 3 0.388127 0.387266 0.188981 11.00000 0.01514 0.01979 = 0.01717 0.00662 0.00209 0.00021 N7 3 0.577701 0.480446 0.234879 11.00000 0.01486 0.02028 = 0.01433 0.00343 0.00414 0.00137 N8 3 0.656908 0.447126 0.182541 11.00000 0.01613 0.01673 = 0.01194 0.00411 0.00400 0.00386 N9 3 0.554908 0.271812 0.353841 11.00000 0.00943 0.01375 = 0.01595 0.00456 -0.00236 -0.00201 N10 3 0.748602 0.327786 0.351724 11.00000 0.01122 0.01609 = 0.01708 0.00662 0.00002 -0.00008 N11 3 0.691429 0.282521 0.454773 11.00000 0.01592 0.02033 = 0.01494 0.00412 -0.00198 -0.00159 N12 3 0.815492 0.297559 0.490198 11.00000 0.01565 0.01540 = 0.01796 0.00317 0.00002 0.00074 N13 3 0.907385 0.115972 0.226367 11.00000 0.01596 0.01616 = 0.01355 0.00544 0.00305 0.00543 N14 3 0.920200 0.091438 0.329280 11.00000 0.01453 0.01537 = 0.01589 0.00461 0.00332 0.00070 N15 3 1.100793 0.052316 0.267427 11.00000 0.01842 0.02535 = 0.01724 0.00873 0.00498 0.00445 N16 3 1.172510 0.049581 0.210807 11.00000 0.01521 0.01692 = 0.01793 0.00263 0.00538 0.00162 C1 1 0.435464 0.789940 0.268964 11.00000 0.01603 0.02010 = 0.01742 0.00464 -0.00142 -0.00294 C2 1 0.610646 0.717080 0.261417 11.00000 0.02038 0.02261 = 0.03279 0.00537 -0.00136 0.00395 AFIX 43 H2 2 0.668810 0.678092 0.244840 11.00000 -1.20000 AFIX 0 C3 1 0.630145 0.771645 0.320799 11.00000 0.02017 0.03042 = 0.02705 0.00866 -0.00812 -0.00192 AFIX 43 H3 2 0.705044 0.778213 0.353488 11.00000 -1.20000 AFIX 0 C4 1 0.511153 0.885742 0.385334 11.00000 0.02659 0.02256 = 0.01775 0.00120 -0.00285 -0.00433 C5 1 0.383967 0.879855 0.420678 11.00000 0.03718 0.04238 = 0.02823 -0.00504 0.00614 -0.00814 AFIX 137 H5A 2 0.377785 0.924784 0.459653 11.00000 -1.50000 H5B 2 0.384987 0.835597 0.438346 11.00000 -1.50000 H5C 2 0.307797 0.875418 0.386636 11.00000 -1.50000 AFIX 0 C6 1 0.628735 0.892026 0.439671 11.00000 0.03427 0.03066 = 0.02104 0.00739 -0.00714 -0.00590 AFIX 137 H6A 2 0.622205 0.936983 0.478573 11.00000 -1.50000 H6B 2 0.711121 0.895381 0.417837 11.00000 -1.50000 H6C 2 0.627882 0.847721 0.457265 11.00000 -1.50000 AFIX 0 C7 1 0.515022 0.954042 0.357578 11.00000 0.03806 0.02179 = 0.03085 0.00352 -0.01256 -0.00085 AFIX 137 H7A 2 0.505463 0.999147 0.395877 11.00000 -1.50000 H7B 2 0.442673 0.949385 0.321299 11.00000 -1.50000 H7C 2 0.599427 0.957662 0.337648 11.00000 -1.50000 AFIX 0 C8 1 0.439573 0.676361 0.157009 11.00000 0.02532 0.01680 = 0.01321 0.00589 0.00010 0.00001 C9 1 0.544327 0.620117 0.130370 11.00000 0.03032 0.02801 = 0.01841 0.00451 0.00558 0.00469 AFIX 137 H9A 2 0.510710 0.585247 0.085735 11.00000 -1.50000 H9B 2 0.565032 0.592181 0.164622 11.00000 -1.50000 H9C 2 0.624316 0.646911 0.123698 11.00000 -1.50000 AFIX 0 C10 1 0.315418 0.632704 0.164360 11.00000 0.02437 0.02328 = 0.01839 0.00269 -0.00243 -0.00345 AFIX 137 H10A 2 0.283229 0.599621 0.118571 11.00000 -1.50000 H10B 2 0.247424 0.667714 0.182353 11.00000 -1.50000 H10C 2 0.335690 0.602678 0.196889 11.00000 -1.50000 AFIX 0 C11 1 0.417191 0.723749 0.105177 11.00000 0.03065 0.02534 = 0.02251 0.01141 0.00350 0.00281 AFIX 137 H11A 2 0.384650 0.691149 0.059231 11.00000 -1.50000 H11B 2 0.500596 0.749167 0.101214 11.00000 -1.50000 H11C 2 0.352090 0.761080 0.122111 11.00000 -1.50000 AFIX 0 C12 1 0.133663 0.837486 0.207905 11.00000 0.02240 0.02508 = 0.02246 0.00285 -0.00013 0.00822 AFIX 43 H12 2 0.137828 0.887347 0.237316 11.00000 -1.20000 AFIX 0 C13 1 -0.037909 0.699705 0.123759 11.00000 0.03169 0.02601 = 0.04952 0.01327 -0.00880 -0.00675 AFIX 137 H13A 2 -0.113340 0.682631 0.089121 11.00000 -1.50000 H13B 2 -0.054603 0.685925 0.166523 11.00000 -1.50000 H13C 2 0.041651 0.676056 0.104876 11.00000 -1.50000 AFIX 0 C14 1 0.005721 0.828752 0.061081 11.00000 0.04570 0.03012 = 0.02417 0.00667 0.00095 -0.00370 AFIX 137 H14A 2 -0.073287 0.811470 0.029040 11.00000 -1.50000 H14B 2 0.082915 0.804863 0.039454 11.00000 -1.50000 H14C 2 0.017886 0.883208 0.071086 11.00000 -1.50000 AFIX 0 C15 1 -0.161033 0.851083 0.184332 11.00000 0.02106 0.04216 = 0.03920 0.00841 -0.00076 0.00819 AFIX 137 H15A 2 -0.239523 0.834755 0.151693 11.00000 -1.50000 H15B 2 -0.146538 0.905419 0.194433 11.00000 -1.50000 H15C 2 -0.173965 0.837997 0.227847 11.00000 -1.50000 AFIX 0 C16 1 0.465798 0.444204 0.236074 11.00000 0.01837 0.01746 = 0.01598 0.00749 0.00671 0.00712 C17 1 0.277944 0.372091 0.222552 11.00000 0.01417 0.02844 = 0.02856 0.01567 0.00138 -0.00216 AFIX 43 H17 2 0.209819 0.334911 0.202839 11.00000 -1.20000 AFIX 0 C18 1 0.285645 0.419121 0.287131 11.00000 0.01228 0.02734 = 0.02783 0.01333 0.00843 0.00716 AFIX 43 H18 2 0.223499 0.421088 0.320882 11.00000 -1.20000 AFIX 0 C19 1 0.444014 0.523459 0.362744 11.00000 0.02326 0.02696 = 0.01715 0.00581 0.00313 0.00782 C20 1 0.340907 0.527372 0.416045 11.00000 0.03369 0.03488 = 0.02260 0.01209 0.01385 0.01496 AFIX 137 H20A 2 0.366906 0.567817 0.458400 11.00000 -1.50000 H20B 2 0.335178 0.479682 0.427917 11.00000 -1.50000 H20C 2 0.254805 0.537116 0.395848 11.00000 -1.50000 AFIX 0 C21 1 0.454785 0.599677 0.347827 11.00000 0.02827 0.02042 = 0.02331 0.00590 0.00634 0.00708 AFIX 137 H21A 2 0.485554 0.637972 0.390931 11.00000 -1.50000 H21B 2 0.368097 0.612103 0.330570 11.00000 -1.50000 H21C 2 0.517610 0.597812 0.312419 11.00000 -1.50000 AFIX 0 C22 1 0.575937 0.503239 0.392504 11.00000 0.02916 0.03074 = 0.02033 0.00433 0.00285 0.00857 AFIX 137 H22A 2 0.602763 0.540293 0.437053 11.00000 -1.50000 H22B 2 0.642867 0.502899 0.359442 11.00000 -1.50000 H22C 2 0.566886 0.453544 0.400127 11.00000 -1.50000 AFIX 0 C23 1 0.401999 0.351333 0.112439 11.00000 0.01921 0.01872 = 0.01637 0.00417 0.00015 -0.00288 C24 1 0.272952 0.306985 0.079541 11.00000 0.02304 0.03303 = 0.02744 0.00363 -0.00382 -0.00610 AFIX 137 H24A 2 0.277496 0.287796 0.028893 11.00000 -1.50000 H24B 2 0.198700 0.339883 0.089109 11.00000 -1.50000 H24C 2 0.260410 0.265010 0.099654 11.00000 -1.50000 AFIX 0 C25 1 0.512744 0.297214 0.103721 11.00000 0.02035 0.01963 = 0.01524 0.00227 0.00109 -0.00274 AFIX 137 H25A 2 0.516884 0.271694 0.053989 11.00000 -1.50000 H25B 2 0.496238 0.260144 0.129212 11.00000 -1.50000 H25C 2 0.596677 0.324831 0.122327 11.00000 -1.50000 AFIX 0 C26 1 0.421087 0.412791 0.075826 11.00000 0.02679 0.02213 = 0.01583 0.00777 -0.00113 -0.00089 AFIX 137 H26A 2 0.417805 0.390261 0.025177 11.00000 -1.50000 H26B 2 0.506863 0.439159 0.092259 11.00000 -1.50000 H26C 2 0.350811 0.448296 0.086606 11.00000 -1.50000 AFIX 0 C27 1 0.761782 0.485291 0.179000 11.00000 0.01658 0.01609 = 0.01968 0.00350 0.00126 0.00342 AFIX 43 H27 2 0.782382 0.532004 0.212730 11.00000 -1.20000 AFIX 0 C28 1 0.872960 0.345829 0.081459 11.00000 0.03208 0.02015 = 0.03154 0.00174 0.01178 0.00269 AFIX 137 H28A 2 0.932386 0.329037 0.044233 11.00000 -1.50000 H28B 2 0.783273 0.325593 0.064268 11.00000 -1.50000 H28C 2 0.902637 0.328049 0.121689 11.00000 -1.50000 AFIX 0 C29 1 0.815372 0.483615 0.031791 11.00000 0.02749 0.03099 = 0.02434 0.00683 0.00186 0.00083 AFIX 137 H29A 2 0.867298 0.461719 -0.007736 11.00000 -1.50000 H29B 2 0.825951 0.538308 0.044172 11.00000 -1.50000 H29C 2 0.722093 0.468388 0.018749 11.00000 -1.50000 AFIX 0 C30 1 1.045723 0.488761 0.139156 11.00000 0.01705 0.02610 = 0.01987 0.00434 0.00348 -0.00032 AFIX 137 H30A 2 1.103155 0.472712 0.100884 11.00000 -1.50000 H30B 2 1.078092 0.470304 0.178551 11.00000 -1.50000 H30C 2 1.045978 0.543549 0.154145 11.00000 -1.50000 AFIX 0 C31 1 0.675252 0.294581 0.392454 11.00000 0.01150 0.01342 = 0.01496 0.00137 0.00336 0.00215 C32 1 0.671709 0.323443 0.289491 11.00000 0.02122 0.01763 = 0.01251 0.00383 -0.00165 0.00392 AFIX 43 H32 2 0.698406 0.341171 0.251964 11.00000 -1.20000 AFIX 0 C33 1 0.555374 0.290471 0.291589 11.00000 0.01708 0.01449 = 0.01322 0.00321 -0.00216 0.00367 AFIX 43 H33 2 0.484570 0.281314 0.256207 11.00000 -1.20000 AFIX 0 C34 1 0.440397 0.235735 0.378315 11.00000 0.00964 0.01297 = 0.01763 0.00576 0.00316 0.00088 C35 1 0.478790 0.159998 0.388791 11.00000 0.01815 0.01909 = 0.02815 0.01144 0.00194 -0.00074 AFIX 137 H35A 2 0.401889 0.135164 0.401263 11.00000 -1.50000 H35B 2 0.549488 0.167983 0.426420 11.00000 -1.50000 H35C 2 0.509504 0.128492 0.345378 11.00000 -1.50000 AFIX 0 C36 1 0.392808 0.288319 0.443932 11.00000 0.02013 0.03223 = 0.02418 0.00402 0.00684 0.00119 AFIX 137 H36A 2 0.314527 0.265526 0.457276 11.00000 -1.50000 H36B 2 0.370503 0.335886 0.434727 11.00000 -1.50000 H36C 2 0.462749 0.297407 0.482048 11.00000 -1.50000 AFIX 0 C37 1 0.326575 0.219956 0.319963 11.00000 0.01591 0.02316 = 0.02143 0.00818 -0.00456 -0.00326 AFIX 137 H37A 2 0.251824 0.194927 0.334134 11.00000 -1.50000 H37B 2 0.356627 0.187643 0.276749 11.00000 -1.50000 H37C 2 0.299093 0.267291 0.312001 11.00000 -1.50000 AFIX 0 C38 1 0.885687 0.363393 0.366991 11.00000 0.01131 0.01655 = 0.02199 0.00542 0.00164 0.00025 C39 1 0.986476 0.303873 0.368824 11.00000 0.01530 0.03103 = 0.02404 0.00663 0.00297 0.00659 AFIX 137 H39A 2 1.075765 0.327066 0.376225 11.00000 -1.50000 H39B 2 0.977455 0.264585 0.324325 11.00000 -1.50000 H39C 2 0.970642 0.281917 0.407094 11.00000 -1.50000 AFIX 0 C40 1 0.915392 0.397461 0.308168 11.00000 0.01507 0.04153 = 0.03186 0.01983 -0.00061 -0.00605 AFIX 137 H40A 2 1.000861 0.425211 0.319647 11.00000 -1.50000 H40B 2 0.846270 0.431589 0.302442 11.00000 -1.50000 H40C 2 0.918167 0.357515 0.264549 11.00000 -1.50000 AFIX 0 C41 1 0.893723 0.426928 0.434948 11.00000 0.01488 0.02311 = 0.02930 0.00372 -0.00322 0.00193 AFIX 137 H41A 2 0.983440 0.449615 0.444622 11.00000 -1.50000 H41B 2 0.871494 0.406936 0.473570 11.00000 -1.50000 H41C 2 0.831381 0.464908 0.430159 11.00000 -1.50000 AFIX 0 C42 1 0.820180 0.291122 0.552594 11.00000 0.01623 0.01752 = 0.01610 0.00531 0.00109 0.00198 AFIX 43 H42 2 0.740879 0.277636 0.569486 11.00000 -1.20000 AFIX 0 C43 1 1.116035 0.331506 0.567812 11.00000 0.02253 0.05668 = 0.03298 0.01834 -0.00058 -0.00608 AFIX 137 H43A 2 1.195109 0.341747 0.600557 11.00000 -1.50000 H43B 2 1.097067 0.376113 0.552324 11.00000 -1.50000 H43C 2 1.130912 0.289720 0.527247 11.00000 -1.50000 AFIX 0 C44 1 1.002308 0.219106 0.637802 11.00000 0.03164 0.04921 = 0.05229 0.03075 -0.01100 -0.00039 AFIX 137 H44A 2 1.071869 0.228718 0.676145 11.00000 -1.50000 H44B 2 1.029310 0.180353 0.597681 11.00000 -1.50000 H44C 2 0.920663 0.202114 0.653172 11.00000 -1.50000 AFIX 0 C45 1 0.950823 0.382627 0.691892 11.00000 0.03355 0.05256 = 0.02808 -0.01218 -0.01064 0.00391 AFIX 137 H45A 2 1.029122 0.388406 0.724798 11.00000 -1.50000 H45B 2 0.873332 0.370053 0.713673 11.00000 -1.50000 H45C 2 0.937763 0.429596 0.679521 11.00000 -1.50000 AFIX 0 C46 1 0.986704 0.084469 0.270056 11.00000 0.02140 0.01209 = 0.01456 0.00361 0.00040 -0.00289 C47 1 0.802604 0.125534 0.322022 11.00000 0.01469 0.01761 = 0.02160 0.00462 0.00349 0.00299 AFIX 43 H47 2 0.738706 0.136478 0.355455 11.00000 -1.20000 AFIX 0 C48 1 0.794161 0.140401 0.260283 11.00000 0.01575 0.02730 = 0.02467 0.01071 0.00563 0.00808 AFIX 43 H48 2 0.723151 0.163697 0.242270 11.00000 -1.20000 AFIX 0 C49 1 0.930565 0.123305 0.154928 11.00000 0.02054 0.01965 = 0.01345 0.00695 0.00153 0.00213 C50 1 1.049211 0.176589 0.159805 11.00000 0.02726 0.02155 = 0.02491 0.01276 0.00563 -0.00019 AFIX 137 H50A 2 1.064400 0.180841 0.113048 11.00000 -1.50000 H50B 2 1.127383 0.157190 0.179267 11.00000 -1.50000 H50C 2 1.032164 0.226008 0.190237 11.00000 -1.50000 AFIX 0 C51 1 0.943240 0.046806 0.104253 11.00000 0.02822 0.02398 = 0.01745 0.00311 0.00422 0.00159 AFIX 137 H51A 2 0.960922 0.052633 0.058323 11.00000 -1.50000 H51B 2 0.860932 0.016865 0.100058 11.00000 -1.50000 H51C 2 1.016054 0.021513 0.121648 11.00000 -1.50000 AFIX 0 C52 1 0.810023 0.159500 0.128155 11.00000 0.02836 0.02818 = 0.01892 0.01104 0.00230 0.00581 AFIX 137 H52A 2 0.821668 0.162618 0.080669 11.00000 -1.50000 H52B 2 0.801969 0.209903 0.159097 11.00000 -1.50000 H52C 2 0.729968 0.128940 0.127713 11.00000 -1.50000 AFIX 0 C53 1 0.963103 0.065040 0.391439 11.00000 0.02209 0.01906 = 0.01416 0.00923 -0.00085 0.00103 C54 1 0.973703 -0.019989 0.368418 11.00000 0.04205 0.02362 = 0.02345 0.01081 0.01205 0.01056 AFIX 137 H54A 2 1.001060 -0.037605 0.409071 11.00000 -1.50000 H54B 2 1.039083 -0.033168 0.333780 11.00000 -1.50000 H54C 2 0.887754 -0.043662 0.347657 11.00000 -1.50000 AFIX 0 C55 1 1.094653 0.104421 0.424774 11.00000 0.02466 0.04403 = 0.02155 0.01395 -0.00628 -0.01078 AFIX 137 H55A 2 1.120901 0.088771 0.466683 11.00000 -1.50000 H55B 2 1.085413 0.158721 0.437717 11.00000 -1.50000 H55C 2 1.162099 0.091055 0.391323 11.00000 -1.50000 AFIX 0 C56 1 0.859176 0.084358 0.444481 11.00000 0.02753 0.03362 = 0.01474 0.00914 0.00151 0.00126 AFIX 137 H56A 2 0.884884 0.065710 0.484728 11.00000 -1.50000 H56B 2 0.773694 0.060963 0.422591 11.00000 -1.50000 H56C 2 0.852310 0.138790 0.460137 11.00000 -1.50000 AFIX 0 C57 1 1.281167 0.015736 0.210889 11.00000 0.02061 0.02572 = 0.02512 0.01094 0.00207 0.00499 AFIX 43 H57 2 1.305330 -0.004394 0.248705 11.00000 -1.20000 AFIX 0 C58 1 1.553117 -0.027231 0.167354 11.00000 0.02225 0.05959 = 0.04610 0.01332 0.00817 0.01397 AFIX 137 H58A 2 1.613062 -0.032690 0.130106 11.00000 -1.50000 H58B 2 1.539264 -0.075586 0.177140 11.00000 -1.50000 H58C 2 1.591751 0.009557 0.209727 11.00000 -1.50000 AFIX 0 C59 1 1.321736 -0.066066 0.059292 11.00000 0.04766 0.08550 = 0.02868 -0.00428 -0.00150 -0.02141 AFIX 137 H59A 2 1.379013 -0.068913 0.021255 11.00000 -1.50000 H59B 2 1.233770 -0.051930 0.045652 11.00000 -1.50000 H59C 2 1.315099 -0.114953 0.068812 11.00000 -1.50000 AFIX 0 C60 1 1.416703 0.096818 0.120397 11.00000 0.05086 0.05237 = 0.07661 0.03690 0.03689 0.02016 AFIX 137 H60A 2 1.461199 0.089756 0.077218 11.00000 -1.50000 H60B 2 1.470910 0.130918 0.159244 11.00000 -1.50000 H60C 2 1.330836 0.118179 0.114880 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_KB_ItBuTMSCHN2_0m_a.res in P-1 REM wR2 = 0.238118, GooF = S = 1.22297, Restrained GooF = 1.22297 for all data REM R1 = 0.100368 for 11761 Fo > 4sig(Fo) and 0.109773 for all 13424 data REM 757 parameters refined using 0 restraints END WGHT 0.0000 25.4807 REM Instructions for potential hydrogen bonds HTAB C5 N3 HTAB C7 N3 HTAB C10 N4 HTAB C11 N4 HTAB C21 N7 HTAB C22 N7 HTAB C25 N8 HTAB C26 N8 HTAB C35 N11 HTAB C36 N11 HTAB C39 N12 HTAB C41 N12 HTAB C50 N16 HTAB C51 N16 HTAB C54 N15 HTAB C55 N15 REM Highest difference peak 0.743, deepest hole -0.501, 1-sigma level 0.098 Q1 1 0.7025 0.5837 0.1417 11.00000 0.05 0.74 Q2 1 0.7542 0.8271 0.3909 11.00000 0.05 0.73 Q3 1 1.5742 -0.1411 0.1039 11.00000 0.05 0.73 Q4 1 0.6921 0.2101 0.1439 11.00000 0.05 0.70 Q5 1 0.2876 0.3863 0.1435 11.00000 0.05 0.63 Q6 1 1.0973 0.4109 0.1433 11.00000 0.05 0.61 Q7 1 0.7403 0.1038 0.3895 11.00000 0.05 0.61 Q8 1 1.1733 0.0428 0.1075 11.00000 0.05 0.56 Q9 1 0.3339 0.2808 0.3888 11.00000 0.05 0.56 Q10 1 1.1535 0.0235 0.3722 11.00000 0.05 0.54 Q11 1 0.1393 0.7512 0.1281 11.00000 0.05 0.49 Q12 1 -0.1890 0.8950 0.1075 11.00000 0.05 0.49 Q13 1 0.7508 0.3166 0.6600 11.00000 0.05 0.45 Q14 1 0.5524 0.3654 0.2094 11.00000 0.05 0.44 Q15 1 0.8864 0.2889 0.6820 11.00000 0.05 0.44 Q16 1 1.0000 0.4164 0.6669 11.00000 0.05 0.43 Q17 1 0.5253 0.2553 0.1919 11.00000 0.05 0.41 Q18 1 1.1966 0.1317 0.2221 11.00000 0.05 0.41 Q19 1 0.6858 0.0042 0.0564 11.00000 0.05 0.40 Q20 1 0.4828 0.3373 0.1109 11.00000 0.05 0.39 ; _shelx_res_checksum 22114 _shelx_hkl_file ; -2 0 0 5778.02 291.37 -2 0 0 5948.00 292.17 -2 0 0 5783.22 291.67 -2 0 0 5649.23 291.37 2 0 0 6091.09 291.27 2 0 0 5645.74 291.37 2 0 0 5735.93 291.37 2 0 0 5816.52 292.37 2 0 0 5649.63 292.27 2 0 0 6024.40 292.37 -3 0 0 229.68 15.10 -3 0 0 194.58 13.00 -3 0 0 191.28 12.30 -3 0 0 204.48 13.30 -3 0 0 208.18 12.00 3 0 0 188.18 11.80 3 0 0 214.98 12.10 3 0 0 177.78 11.80 3 0 0 181.88 13.00 3 0 0 210.38 13.50 3 0 0 195.18 13.40 3 0 0 194.18 13.70 -4 0 0 58.39 5.60 -4 0 0 67.39 8.90 -4 0 0 80.89 10.30 -4 0 0 56.89 6.60 -4 0 0 59.29 6.60 -4 0 0 66.49 6.10 -4 0 0 79.39 9.30 4 0 0 63.69 5.40 4 0 0 57.59 5.50 4 0 0 70.19 8.60 4 0 0 63.09 8.10 4 0 0 69.49 7.40 4 0 0 70.29 9.30 4 0 0 47.00 5.70 -5 0 0 102.99 10.10 -5 0 0 87.19 8.60 -5 0 0 90.19 7.90 -5 0 0 130.09 14.50 -5 0 0 91.99 9.00 -5 0 0 77.49 6.70 -5 0 0 95.69 9.90 -5 0 0 85.09 7.40 5 0 0 103.39 12.30 5 0 0 99.99 7.20 5 0 0 88.29 6.70 5 0 0 72.59 7.40 5 0 0 77.89 9.10 5 0 0 97.59 9.50 5 0 0 102.09 11.60 -6 0 0 33.20 6.80 -6 0 0 14.40 4.80 -6 0 0 25.70 5.90 -6 0 0 34.30 5.00 -6 0 0 29.50 6.20 -6 0 0 28.10 5.10 -6 0 0 20.00 6.10 -6 0 0 25.00 4.00 -6 0 0 27.10 7.00 6 0 0 23.40 3.70 6 0 0 23.20 3.60 6 0 0 22.70 6.90 6 0 0 11.80 4.60 6 0 0 19.40 4.40 6 0 0 33.70 7.60 6 0 0 33.30 6.70 -7 0 0 224.68 16.00 -7 0 0 226.08 19.10 -7 0 0 260.67 19.20 -7 0 0 219.58 16.90 -7 0 0 234.38 16.90 -7 0 0 247.78 15.40 -7 0 0 228.28 18.40 -7 0 0 238.38 17.30 -7 0 0 226.28 17.20 7 0 0 242.28 18.20 7 0 0 234.08 15.40 7 0 0 208.58 12.80 7 0 0 224.18 18.30 7 0 0 245.58 18.40 -8 0 0 15.80 6.70 -8 0 0 23.10 6.40 -8 0 0 17.20 6.90 -8 0 0 20.30 4.30 -8 0 0 13.80 5.80 -8 0 0 21.90 5.30 8 0 0 10.00 5.60 8 0 0 12.70 6.80 8 0 0 25.80 8.40 8 0 0 9.80 4.70 -9 0 0 63.39 9.50 -9 0 0 56.39 8.30 -9 0 0 72.59 12.90 -9 0 0 62.89 7.10 -9 0 0 61.59 12.00 -9 0 0 58.59 9.80 9 0 0 51.79 11.30 9 0 0 57.59 8.50 9 0 0 65.29 11.70 -10 0 0 158.58 18.10 -10 0 0 111.29 16.10 -10 0 0 112.99 8.30 -10 0 0 97.59 9.20 -10 0 0 89.89 10.70 10 0 0 104.09 10.30 10 0 0 106.79 15.90 10 0 0 104.89 16.00 -11 0 0 -0.70 3.40 -11 0 0 -0.60 2.70 -11 0 0 -3.70 4.60 -11 0 0 -5.00 6.10 -11 0 0 7.00 6.90 11 0 0 1.00 6.50 11 0 0 12.30 6.40 11 0 0 -2.50 4.90 -12 0 0 -7.70 5.70 -12 0 0 7.10 4.20 -12 0 0 5.10 5.50 -12 0 0 -0.20 7.60 12 0 0 10.00 8.00 12 0 0 23.90 9.20 -13 0 0 4.10 8.50 -13 0 0 5.40 4.30 -13 0 0 11.00 6.30 -13 0 0 16.50 8.80 13 0 0 29.40 10.90 13 0 0 9.80 8.70 -14 0 0 43.20 12.90 -14 0 0 49.60 12.70 14 0 0 74.09 14.80 14 0 0 38.00 11.40 14 -1 0 10.60 9.50 14 -1 0 1.00 8.00 -14 1 0 1.40 8.90 -14 1 0 6.60 7.90 13 -1 0 45.20 11.20 13 -1 0 80.59 14.30 -13 1 0 35.30 11.40 -13 1 0 34.20 8.90 -13 1 0 57.99 13.60 12 -1 0 18.20 9.50 12 -1 0 12.20 7.80 12 -1 0 10.30 6.60 -12 1 0 15.10 8.00 -12 1 0 15.00 9.60 -12 1 0 21.10 7.30 -12 1 0 22.70 4.30 11 -1 0 64.39 11.90 11 -1 0 97.49 15.30 -11 1 0 87.69 12.30 -11 1 0 66.39 12.30 -11 1 0 77.09 10.10 -11 1 0 74.59 7.60 -11 1 0 94.19 15.80 10 -1 0 38.90 10.70 10 -1 0 28.00 8.70 10 -1 0 37.50 7.70 -10 1 0 50.79 12.50 -10 1 0 41.10 9.90 -10 1 0 46.60 6.40 -10 1 0 36.50 9.30 -10 1 0 41.40 7.40 9 -1 0 97.39 9.80 9 -1 0 82.99 15.60 9 -1 0 109.19 12.50 -9 1 0 77.19 12.10 -9 1 0 76.49 11.60 -9 1 0 118.39 15.90 -9 1 0 104.29 8.60 -9 1 0 92.99 9.40 -9 1 0 113.49 10.70 8 -1 0 107.19 10.30 8 -1 0 114.49 14.50 8 -1 0 122.59 12.50 8 -1 0 123.59 14.00 -8 1 0 125.19 11.10 -8 1 0 138.49 9.90 -8 1 0 104.69 14.90 -8 1 0 128.59 10.60 -8 1 0 95.89 11.30 -8 1 0 108.89 12.10 7 -1 0 554.64 35.80 7 -1 0 561.94 34.00 7 -1 0 623.94 37.80 7 -1 0 623.14 36.00 7 -1 0 614.54 37.20 -7 1 0 603.04 35.40 -7 1 0 540.85 32.70 -7 1 0 571.34 37.10 -7 1 0 597.24 34.30 -7 1 0 585.94 35.10 -7 1 0 640.24 34.50 -7 1 0 630.84 37.40 6 -1 0 156.88 10.10 6 -1 0 209.18 15.70 6 -1 0 191.08 13.90 6 -1 0 157.38 13.80 6 -1 0 171.18 13.60 6 -1 0 174.98 12.40 -6 1 0 178.88 13.00 -6 1 0 152.98 11.80 -6 1 0 174.08 14.50 -6 1 0 160.58 12.90 -6 1 0 152.08 14.30 -6 1 0 176.68 12.40 -6 1 0 157.18 11.30 -6 1 0 145.39 13.70 5 -1 0 30.60 3.90 5 -1 0 24.10 7.00 5 -1 0 28.60 5.40 5 -1 0 23.10 3.60 5 -1 0 28.40 6.40 5 -1 0 34.50 6.50 5 -1 0 26.00 6.50 -5 1 0 23.90 5.40 -5 1 0 29.70 5.50 -5 1 0 38.10 7.60 -5 1 0 19.00 6.00 -5 1 0 32.50 5.80 -5 1 0 27.90 6.60 -5 1 0 34.20 5.30 4 -1 0 23.10 5.30 4 -1 0 22.30 5.40 4 -1 0 46.00 8.30 4 -1 0 33.70 4.60 4 -1 0 20.10 4.30 4 -1 0 32.80 6.40 -4 1 0 31.20 6.80 -4 1 0 27.20 5.30 -4 1 0 32.10 5.50 -4 1 0 23.50 4.80 -4 1 0 29.80 4.80 -4 1 0 31.60 6.30 -4 1 0 20.00 5.40 3 -1 0 47.90 5.70 3 -1 0 54.99 6.40 3 -1 0 44.80 4.90 3 -1 0 41.30 5.60 3 -1 0 35.90 3.90 3 -1 0 42.30 6.80 -3 1 0 38.90 5.30 -3 1 0 37.90 5.30 -3 1 0 47.40 7.10 -3 1 0 47.30 6.80 -3 1 0 38.20 6.20 -3 1 0 34.60 5.70 -3 1 0 37.70 4.40 2 -1 0 360.76 20.40 2 -1 0 420.16 21.00 2 -1 0 382.66 21.80 2 -1 0 414.86 20.30 2 -1 0 401.66 21.70 2 -1 0 348.27 20.80 2 -1 0 407.26 20.90 -2 1 0 356.26 20.80 -2 1 0 351.66 21.30 -2 1 0 387.16 20.70 -2 1 0 370.66 20.40 -2 1 0 405.06 21.90 -2 1 0 378.86 21.70 -2 1 0 360.56 20.90 -2 1 0 404.26 21.70 1 -1 0 21.40 3.00 -1 1 0 14.20 2.50 -2 -1 0 1724.33 86.99 -2 -1 0 1739.93 89.09 -2 -1 0 1806.12 88.69 -2 -1 0 1593.24 88.09 -2 -1 0 1774.22 89.19 -2 -1 0 1820.12 87.89 -2 -1 0 1690.83 87.29 -2 -1 0 1790.92 88.29 2 1 0 1792.52 88.19 2 1 0 1690.73 88.49 2 1 0 1708.03 87.39 2 1 0 1714.83 88.09 2 1 0 1703.83 89.09 -3 -1 0 4.90 2.90 -3 -1 0 7.70 1.80 -3 -1 0 2.90 3.70 -3 -1 0 5.80 3.50 -3 -1 0 7.10 3.90 -3 -1 0 6.60 3.50 -3 -1 0 5.80 3.20 -3 -1 0 8.60 2.10 3 1 0 8.30 3.30 3 1 0 12.10 4.70 3 1 0 10.50 3.90 3 1 0 6.40 2.30 3 1 0 12.00 3.40 -4 -1 0 91.19 6.00 -4 -1 0 91.99 9.30 -4 -1 0 89.99 8.10 -4 -1 0 95.89 7.70 -4 -1 0 102.39 7.30 -4 -1 0 96.99 9.00 -4 -1 0 113.09 9.70 4 1 0 84.89 7.20 4 1 0 103.09 9.00 4 1 0 93.99 9.30 4 1 0 88.69 6.80 4 1 0 93.59 7.30 -5 -1 0 82.89 7.60 -5 -1 0 77.29 5.80 -5 -1 0 75.49 7.60 -5 -1 0 70.29 8.00 -5 -1 0 80.99 8.80 -5 -1 0 84.09 9.50 -5 -1 0 84.99 10.40 -5 -1 0 88.99 6.60 5 1 0 87.89 10.10 5 1 0 81.09 8.40 5 1 0 81.39 6.70 5 1 0 82.89 6.70 5 1 0 77.59 7.00 5 1 0 106.69 12.30 -6 -1 0 27.50 7.00 -6 -1 0 37.50 5.10 -6 -1 0 31.60 6.20 -6 -1 0 27.50 7.10 -6 -1 0 41.00 7.50 -6 -1 0 51.79 7.50 -6 -1 0 32.80 7.50 -6 -1 0 28.30 3.90 -6 -1 0 38.00 8.80 6 1 0 29.10 7.80 6 1 0 43.20 7.90 6 1 0 36.30 5.40 6 1 0 33.60 4.80 6 1 0 38.60 5.10 6 1 0 31.10 8.00 -7 -1 0 6.80 3.70 -7 -1 0 6.90 5.50 -7 -1 0 2.00 4.20 -7 -1 0 9.20 4.10 -7 -1 0 3.70 2.20 -7 -1 0 7.80 5.10 -7 -1 0 0.40 4.20 -7 -1 0 0.50 3.20 7 1 0 18.20 6.50 7 1 0 10.60 3.40 7 1 0 5.40 2.20 7 1 0 5.20 2.60 -8 -1 0 59.19 6.50 -8 -1 0 80.29 11.50 -8 -1 0 57.39 5.30 -8 -1 0 76.99 12.30 -8 -1 0 75.89 11.30 -8 -1 0 64.39 9.20 8 1 0 50.79 7.30 8 1 0 82.99 12.80 8 1 0 51.99 11.50 -9 -1 0 224.78 19.20 -9 -1 0 195.88 15.70 -9 -1 0 208.98 12.60 -9 -1 0 215.68 14.20 -9 -1 0 229.58 16.80 9 1 0 194.58 19.10 9 1 0 229.98 19.30 9 1 0 203.58 14.40 -10 -1 0 362.86 25.70 -10 -1 0 323.27 26.50 -10 -1 0 323.47 19.20 -10 -1 0 357.96 23.10 -10 -1 0 342.47 21.20 10 1 0 378.16 22.10 10 1 0 363.26 26.90 10 1 0 395.96 28.40 -11 -1 0 0.00 5.00 -11 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21.20 8.50 9 -2 0 15.80 8.20 9 -2 0 16.50 5.90 -9 2 0 19.50 8.50 -9 2 0 26.20 5.50 -9 2 0 15.00 6.90 -9 2 0 26.80 8.20 -9 2 0 25.50 6.40 -9 2 0 22.50 6.00 8 -2 0 44.60 7.50 -8 2 0 20.70 6.80 7 -2 0 103.39 10.90 7 -2 0 128.09 16.10 7 -2 0 104.39 11.30 7 -2 0 109.49 10.60 7 -2 0 120.99 12.40 -7 2 0 110.59 10.50 -7 2 0 135.09 11.40 -7 2 0 122.79 12.80 -7 2 0 115.69 12.00 -7 2 0 105.59 9.30 -7 2 0 123.49 10.40 6 -2 0 1134.99 58.69 6 -2 0 1077.09 61.89 6 -2 0 1094.09 61.89 6 -2 0 1176.08 61.99 6 -2 0 1234.68 64.49 6 -2 0 1201.68 64.49 -6 2 0 1143.09 62.09 -6 2 0 1119.89 60.99 -6 2 0 1105.39 63.49 -6 2 0 1186.68 61.99 -6 2 0 1126.29 63.99 -6 2 0 1157.98 63.89 5 -2 0 63.49 9.80 5 -2 0 58.99 7.90 5 -2 0 60.49 9.60 5 -2 0 42.80 4.90 5 -2 0 57.39 7.80 5 -2 0 55.29 7.50 5 -2 0 49.80 4.90 -5 2 0 61.89 9.80 -5 2 0 78.99 9.40 -5 2 0 73.69 10.20 -5 2 0 65.19 9.70 -5 2 0 51.79 7.70 -5 2 0 65.19 7.50 4 -2 0 1234.58 62.19 4 -2 0 1061.89 64.39 4 -2 0 1285.17 65.19 4 -2 0 1251.67 63.39 4 -2 0 1178.78 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348.67 20.50 3 5 0 343.37 19.40 3 5 0 341.57 18.60 3 5 0 370.36 23.70 -4 -5 0 48.60 5.20 -4 -5 0 33.10 6.90 -4 -5 0 33.30 8.00 -4 -5 0 44.10 6.60 4 5 0 49.10 7.00 4 5 0 49.10 5.10 4 5 0 35.90 6.90 4 5 0 38.70 8.80 4 5 0 45.60 6.70 4 5 0 37.60 3.00 -5 -5 0 11.00 4.90 -5 -5 0 3.10 5.30 -5 -5 0 0.20 3.80 -5 -5 0 7.50 4.20 -5 -5 0 0.80 2.60 5 5 0 0.50 6.20 5 5 0 2.50 2.90 5 5 0 0.50 3.40 5 5 0 -2.10 3.30 5 5 0 1.60 3.10 -6 -5 0 52.29 9.80 -6 -5 0 61.39 9.30 -6 -5 0 55.69 9.40 -6 -5 0 58.29 6.80 -6 -5 0 52.99 8.60 -6 -5 0 66.69 10.90 6 5 0 55.69 7.90 6 5 0 49.60 8.20 6 5 0 57.19 8.20 6 5 0 51.79 12.80 -7 -5 0 97.09 10.90 -7 -5 0 91.49 9.90 -7 -5 0 68.59 7.30 -7 -5 0 116.79 17.00 -7 -5 0 119.29 13.90 7 5 0 92.49 15.30 7 5 0 90.99 8.70 7 5 0 81.79 8.30 7 5 0 83.49 11.20 -8 -5 0 59.49 6.50 -8 -5 0 58.39 10.60 -8 -5 0 60.49 11.20 8 5 0 59.69 6.90 8 5 0 63.49 10.70 8 5 0 65.29 8.30 8 5 0 43.10 11.50 8 5 0 86.29 14.50 -9 -5 0 56.29 6.60 -9 -5 0 79.89 12.40 -9 -5 0 80.79 12.80 9 5 0 65.99 7.20 9 5 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829.82 43.00 1 6 0 707.63 41.90 1 6 0 825.52 43.30 1 6 0 826.12 41.60 1 6 0 756.72 42.90 -2 -6 0 216.88 14.80 2 6 0 264.07 17.10 -3 -6 0 56.69 6.30 -3 -6 0 57.69 6.60 -3 -6 0 79.79 10.30 -3 -6 0 65.69 9.50 -3 -6 0 76.49 11.10 3 6 0 56.49 8.00 3 6 0 72.69 11.70 3 6 0 57.99 6.60 3 6 0 53.19 5.80 3 6 0 80.49 10.00 -4 -6 0 363.06 20.60 -4 -6 0 365.96 21.80 -4 -6 0 370.86 23.10 -4 -6 0 354.46 24.50 -4 -6 0 374.86 23.30 4 6 0 352.06 22.00 4 6 0 340.87 24.90 4 6 0 321.97 18.80 4 6 0 369.06 22.90 4 6 0 346.87 20.20 4 6 0 342.47 21.60 -5 -6 0 326.87 19.40 -5 -6 0 354.06 21.40 -5 -6 0 312.97 21.90 5 6 0 328.87 21.20 5 6 0 316.57 21.40 5 6 0 333.47 21.10 5 6 0 317.07 19.40 5 6 0 362.96 25.00 -6 -6 0 41.50 8.50 -6 -6 0 43.30 9.30 -6 -6 0 36.60 5.60 -6 -6 0 39.30 7.70 6 6 0 51.59 8.20 6 6 0 39.90 7.20 6 6 0 27.60 6.60 6 6 0 41.00 10.40 -7 -6 0 91.89 8.10 -7 -6 0 111.59 11.20 -7 -6 0 97.19 12.90 7 6 0 93.49 9.90 7 6 0 126.69 17.90 7 6 0 94.59 9.40 7 6 0 109.59 12.20 -8 -6 0 2.60 6.50 -8 -6 0 11.10 5.70 -8 -6 0 12.40 3.80 8 6 0 10.80 5.10 8 6 0 -1.70 4.20 8 6 0 12.90 4.10 8 6 0 16.90 8.70 -9 -6 0 33.70 10.00 -9 -6 0 27.00 4.80 -9 -6 0 29.40 8.40 9 6 0 43.40 11.40 9 6 0 25.20 9.80 9 6 0 33.10 5.80 9 6 0 47.00 9.30 -10 -6 0 28.00 8.70 -10 -6 0 22.10 9.30 -10 -6 0 26.40 4.90 10 6 0 35.20 10.90 10 6 0 38.40 12.20 -11 -6 0 140.49 18.70 -11 -6 0 115.09 8.80 -11 -6 0 127.19 17.20 11 6 0 115.89 21.70 12 6 0 99.29 19.10 12 6 0 106.19 19.70 -13 -6 0 53.29 12.80 13 6 0 55.39 14.60 13 6 0 47.10 13.90 13 -7 0 0.60 7.80 13 -7 0 15.90 8.10 -13 7 0 11.50 8.10 -13 7 0 4.50 8.00 -13 7 0 0.10 8.50 12 -7 0 95.39 18.40 -12 7 0 102.29 16.50 -12 7 0 91.89 18.20 -12 7 0 73.99 12.50 11 -7 0 52.29 13.80 11 -7 0 68.09 9.90 -11 7 0 53.19 11.40 -11 7 0 64.59 14.50 -11 7 0 59.59 11.60 10 -7 0 28.40 7.70 10 -7 0 26.80 10.50 -10 7 0 8.10 7.00 -10 7 0 27.70 9.20 -10 7 0 31.30 8.80 9 -7 0 201.38 15.10 9 -7 0 177.28 18.60 -9 7 0 203.48 18.10 -9 7 0 179.18 19.90 -9 7 0 190.08 17.70 -9 7 0 181.18 18.40 8 -7 0 1.80 5.70 8 -7 0 -2.00 3.60 -8 7 0 -1.90 3.60 -8 7 0 6.50 5.40 -8 7 0 -1.20 6.20 -8 7 0 3.50 5.20 -8 7 0 -4.20 5.50 7 -7 0 5.30 4.10 7 -7 0 5.80 2.60 7 -7 0 14.80 7.20 7 -7 0 6.80 2.70 7 -7 0 2.30 5.00 -7 7 0 0.80 6.50 -7 7 0 11.20 6.50 -7 7 0 6.10 6.30 -7 7 0 9.30 4.50 -7 7 0 4.80 4.00 6 -7 0 59.89 6.70 6 -7 0 66.49 6.30 6 -7 0 66.79 6.60 6 -7 0 79.79 11.60 6 -7 0 104.29 14.00 -6 7 0 62.29 7.50 -6 7 0 88.89 12.40 -6 7 0 100.99 13.00 -6 7 0 79.69 8.50 -6 7 0 84.29 13.10 -6 7 0 74.99 7.90 5 -7 0 90.59 8.00 5 -7 0 83.69 7.50 5 -7 0 93.59 10.20 5 -7 0 85.69 8.90 5 -7 0 110.59 13.80 -5 7 0 67.99 11.00 -5 7 0 90.69 11.80 -5 7 0 80.09 8.70 -5 7 0 78.59 13.40 -5 7 0 81.19 12.40 -5 7 0 78.99 8.00 -5 7 0 83.99 7.90 4 -7 0 96.99 8.70 4 -7 0 95.09 10.40 4 -7 0 88.79 8.30 4 -7 0 79.89 7.80 4 -7 0 99.59 7.60 4 -7 0 92.69 9.90 -4 7 0 87.29 11.90 -4 7 0 83.39 11.20 -4 7 0 85.09 8.90 -4 7 0 96.09 12.60 -4 7 0 94.79 7.90 -4 7 0 86.59 9.80 3 -7 0 0.10 5.00 3 -7 0 7.00 4.50 3 -7 0 5.80 4.00 3 -7 0 12.60 3.70 3 -7 0 2.80 4.10 3 -7 0 4.90 3.20 -3 7 0 6.00 4.90 -3 7 0 0.20 4.00 -3 7 0 3.50 3.60 -3 7 0 4.40 2.90 -3 7 0 1.60 4.40 -3 7 0 6.90 5.00 2 -7 0 346.87 19.70 2 -7 0 325.67 22.30 2 -7 0 362.26 20.90 2 -7 0 369.86 22.10 2 -7 0 344.97 22.70 2 -7 0 358.66 21.60 -2 7 0 369.06 19.90 -2 7 0 376.86 23.20 -2 7 0 346.97 22.80 -2 7 0 333.37 21.70 -2 7 0 322.47 22.10 1 -7 0 1167.08 64.69 1 -7 0 1180.68 62.39 1 -7 0 1205.58 64.39 1 -7 0 1241.88 64.99 1 -7 0 1206.78 64.79 -1 7 0 1241.78 64.59 -1 7 0 1259.77 65.09 -1 7 0 1112.09 64.69 -1 7 0 1188.58 63.79 -1 7 0 1309.77 65.29 -1 7 0 1103.39 62.49 -1 7 0 1258.47 65.69 0 -7 0 483.25 27.00 0 -7 0 501.65 29.00 0 -7 0 431.66 28.20 0 -7 0 501.85 28.50 0 -7 0 459.55 28.20 0 -7 0 482.15 28.10 0 7 0 472.95 29.00 0 7 0 509.25 28.40 0 7 0 476.45 28.20 0 7 0 466.95 28.00 0 7 0 468.15 28.30 -1 -7 0 24.90 6.30 -1 -7 0 28.40 6.60 -1 -7 0 18.30 5.00 -1 -7 0 24.60 6.70 1 7 0 41.20 6.30 1 7 0 15.20 5.20 1 7 0 25.70 5.40 1 7 0 34.20 5.50 1 7 0 27.90 7.10 1 7 0 17.00 6.20 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16.10 -4 13 -9 6.30 4.90 -4 13 -9 2.50 7.80 -4 13 -9 -0.70 5.90 4 -13 9 15.00 8.10 4 -13 9 5.20 6.30 4 -13 9 12.90 7.30 -5 13 -9 82.99 15.60 -5 13 -9 74.49 13.30 -5 13 -9 86.59 14.50 5 -13 9 49.99 10.70 5 -13 9 57.19 12.40 5 -13 9 74.39 13.30 -6 13 -9 -6.00 5.50 -6 13 -9 1.50 8.50 -6 13 -9 2.90 6.40 6 -13 9 11.30 7.80 6 -13 9 -5.20 6.40 6 -13 9 0.10 5.00 -7 13 -9 19.50 9.90 -7 13 -9 4.80 8.60 -7 13 -9 4.40 6.00 7 -13 9 14.50 8.90 7 -13 9 16.30 7.90 7 -13 9 11.30 8.50 -8 13 -9 1.80 7.60 -8 13 -9 6.50 6.30 -8 13 -9 -11.70 6.20 8 -13 9 1.90 8.20 8 -13 9 1.60 8.10 8 -13 9 9.60 6.60 -9 13 -9 3.70 6.30 -9 13 -9 3.40 7.80 -9 13 -9 12.30 8.90 9 -13 9 -0.60 7.30 9 -13 9 2.10 9.20 9 -13 9 4.10 8.60 9 -13 9 9.00 7.20 -10 13 -9 24.30 12.50 -10 13 -9 -11.60 5.60 -10 13 -9 6.00 6.30 -10 13 -9 8.40 10.00 10 -13 9 -3.10 7.60 10 -13 9 6.30 9.50 10 -13 9 1.80 6.70 10 -13 9 14.80 8.60 -11 13 -9 21.10 10.40 -11 13 -9 11.90 9.70 -11 13 -9 18.30 8.90 -11 13 -9 23.20 11.40 11 -13 9 32.90 11.20 11 -13 9 22.50 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9.30 4 12 -9 32.90 7.50 4 12 -9 36.60 6.00 -4 -12 9 25.10 5.60 -4 -12 9 22.90 8.40 -4 -12 9 45.00 10.80 -4 -12 9 16.50 7.10 3 12 -9 173.78 13.20 3 12 -9 169.58 14.50 3 12 -9 138.09 15.70 3 12 -9 178.68 14.10 3 12 -9 176.08 15.10 3 12 -9 175.38 17.10 -3 -12 9 173.58 15.50 -3 -12 9 172.28 16.20 -3 -12 9 168.08 16.40 -3 -12 9 176.28 13.60 2 12 -9 85.29 6.90 2 12 -9 125.09 15.30 2 12 -9 91.49 9.80 2 12 -9 107.49 10.60 2 12 -9 90.29 13.60 -2 -12 9 106.39 11.60 -2 -12 9 114.89 14.10 -2 -12 9 118.39 15.40 -2 -12 9 87.79 13.50 -2 -12 9 96.89 9.80 1 12 -9 -5.40 3.90 1 12 -9 2.50 3.90 1 12 -9 -1.80 2.10 1 12 -9 7.50 5.80 -1 -12 9 1.50 5.60 -1 -12 9 10.30 4.90 -1 -12 9 8.50 6.10 -1 -12 9 1.10 4.40 -1 -12 9 -3.40 4.90 0 12 -9 88.09 10.40 0 12 -9 97.99 14.30 0 12 -9 115.19 15.20 0 12 -9 118.79 16.10 0 12 -9 132.09 12.00 0 12 -9 80.09 8.50 0 -12 9 112.59 13.90 0 -12 9 94.09 10.60 0 -12 9 119.69 15.40 0 -12 9 132.59 17.10 0 -12 9 150.38 20.10 0 -12 9 92.29 13.40 -1 12 -9 550.34 36.80 -1 12 -9 587.74 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134.89 12.40 3 14 -10 137.19 16.30 3 14 -10 140.69 13.90 3 14 -10 135.99 14.30 -3 -14 10 137.29 15.50 -3 -14 10 180.58 13.70 -3 -14 10 144.39 16.00 -3 -14 10 169.78 15.50 2 14 -10 3.40 3.70 2 14 -10 -5.60 3.80 2 14 -10 16.30 7.60 2 14 -10 5.40 2.20 2 14 -10 6.20 5.50 2 14 -10 1.40 5.10 2 14 -10 10.50 7.00 -2 -14 10 7.60 6.20 -2 -14 10 12.60 7.00 -2 -14 10 -0.40 6.30 -2 -14 10 14.40 5.10 1 14 -10 247.68 26.80 1 14 -10 229.28 18.80 1 14 -10 237.98 20.60 1 14 -10 313.57 22.90 1 14 -10 262.37 16.00 -1 -14 10 223.38 19.90 -1 -14 10 236.08 20.80 -1 -14 10 233.08 20.00 -1 -14 10 254.67 19.40 0 14 -10 5.50 7.40 0 14 -10 7.00 5.60 0 14 -10 6.60 4.00 0 14 -10 6.70 4.80 0 -14 10 1.70 6.00 0 -14 10 13.30 7.30 0 -14 10 10.20 6.60 -1 14 -10 114.99 11.70 -1 14 -10 120.49 13.10 -1 14 -10 157.78 20.20 -1 14 -10 106.39 11.50 1 -14 10 135.89 16.80 1 -14 10 124.29 16.80 1 -14 10 134.89 17.40 -2 14 -10 16.70 4.90 -2 14 -10 19.90 8.20 -2 14 -10 19.00 6.50 -2 14 -10 6.80 7.30 2 -14 10 17.10 7.70 2 -14 10 13.40 7.70 2 -14 10 17.30 8.00 -3 14 -10 163.28 17.90 -3 14 -10 152.98 10.70 -3 14 -10 167.68 16.30 -3 14 -10 171.78 15.90 3 -14 10 153.28 15.90 3 -14 10 157.28 16.50 3 -14 10 157.18 15.70 -4 14 -10 326.27 24.90 -4 14 -10 295.07 24.70 -4 14 -10 374.16 28.50 4 -14 10 307.67 24.60 4 -14 10 304.17 25.40 4 -14 10 314.47 24.50 -5 14 -10 106.59 15.70 -5 14 -10 70.09 13.20 -5 14 -10 90.39 16.80 5 -14 10 111.39 15.90 5 -14 10 84.99 14.50 5 -14 10 75.89 14.10 -6 14 -10 2.60 8.00 -6 14 -10 7.70 7.50 -6 14 -10 -3.80 6.40 6 -14 10 -1.20 5.80 6 -14 10 0.30 7.20 6 -14 10 1.40 8.20 -7 14 -10 16.00 10.00 -7 14 -10 22.60 9.60 -7 14 -10 11.40 9.80 7 -14 10 30.00 9.10 7 -14 10 22.90 10.80 7 -14 10 21.70 11.20 -8 14 -10 2.70 8.50 -8 14 -10 0.20 6.30 -8 14 -10 9.90 7.50 8 -14 10 -1.30 7.60 8 -14 10 5.90 6.70 8 -14 10 -4.10 8.10 -9 14 -10 1.20 8.30 -9 14 -10 26.20 10.60 -9 14 -10 5.80 7.30 9 -14 10 -4.70 6.20 9 -14 10 26.40 10.90 9 -14 10 7.00 9.50 9 -14 10 -5.60 7.50 -10 14 -10 40.70 12.90 -10 14 -10 60.19 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2.70 -9 -3 10 -1.60 5.10 -9 -3 10 2.30 4.40 -9 -3 10 12.90 6.70 -9 -3 10 3.90 1.90 8 3 -10 197.38 16.20 8 3 -10 188.38 19.30 8 3 -10 205.78 16.00 -8 -3 10 205.18 18.10 -8 -3 10 172.18 14.70 -8 -3 10 188.78 16.30 -8 -3 10 191.28 11.90 -8 -3 10 175.38 16.00 -8 -3 10 207.68 15.00 -8 -3 10 192.48 15.30 -8 -3 10 201.48 12.00 7 3 -10 11.90 6.10 7 3 -10 20.40 8.70 -7 -3 10 14.50 2.60 -7 -3 10 9.10 4.20 -7 -3 10 32.00 7.10 -7 -3 10 16.90 5.10 -7 -3 10 13.60 4.30 -7 -3 10 16.00 5.20 -7 -3 10 20.10 7.70 -7 -3 10 11.20 5.40 6 3 -10 0.60 4.70 6 3 -10 6.20 5.50 -6 -3 10 6.00 3.10 -6 -3 10 5.20 3.90 -6 -3 10 -0.90 4.20 -6 -3 10 -0.20 3.70 -6 -3 10 1.80 3.00 -6 -3 10 2.90 1.60 -6 -3 10 2.10 1.60 5 3 -10 22.30 6.00 5 3 -10 28.10 8.00 5 3 -10 13.30 4.30 -5 -3 10 20.40 5.00 -5 -3 10 30.30 7.70 -5 -3 10 13.70 5.30 -5 -3 10 11.00 5.70 -5 -3 10 14.00 2.40 -5 -3 10 11.10 4.60 -5 -3 10 18.30 3.00 -5 -3 10 17.20 4.10 4 3 -10 229.08 15.70 4 3 -10 190.48 13.80 4 3 -10 239.88 18.50 -4 -3 10 206.58 12.40 -4 -3 10 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51.09 14.90 -8 6 -14 55.09 12.90 -8 6 -14 22.40 11.90 8 -6 14 24.10 12.60 8 -6 14 41.30 15.50 8 -6 14 45.90 14.40 -9 6 -14 15.70 8.30 -9 6 -14 3.00 7.10 -9 6 -14 11.20 6.20 -9 6 -14 -3.10 9.90 -9 6 -14 -5.80 6.10 9 -6 14 15.70 10.60 9 -6 14 0.40 8.10 9 -6 14 -1.10 7.80 -10 6 -14 45.40 11.20 -10 6 -14 56.79 14.10 -10 6 -14 41.70 8.40 -10 6 -14 34.60 13.20 -10 6 -14 47.60 13.50 10 -6 14 37.80 12.10 10 -6 14 70.59 17.20 -11 6 -14 41.40 14.80 -11 6 -14 5.90 6.00 -11 6 -14 12.00 11.00 -11 6 -14 36.10 12.40 11 -6 14 13.00 9.90 11 -6 14 15.60 10.30 12 5 -14 4.80 7.50 -12 -5 14 8.60 8.00 -12 -5 14 13.50 6.30 11 5 -14 83.69 16.30 -11 -5 14 111.79 18.00 -11 -5 14 69.19 8.00 -11 -5 14 101.09 10.90 -11 -5 14 113.69 10.00 10 5 -14 66.99 12.20 10 5 -14 62.39 14.80 -10 -5 14 74.89 8.40 -10 -5 14 66.19 7.00 -10 -5 14 71.39 21.50 -10 -5 14 60.59 10.30 -10 -5 14 57.19 9.10 9 5 -14 43.30 10.00 9 5 -14 34.50 11.00 -9 -5 14 34.00 6.40 -9 -5 14 50.29 11.60 -9 -5 14 39.40 5.90 -9 -5 14 30.50 5.30 -9 -5 14 35.40 7.30 8 5 -14 100.89 13.20 8 5 -14 91.39 17.00 -8 -5 14 68.69 6.80 -8 -5 14 70.49 9.20 -8 -5 14 72.19 9.50 -8 -5 14 67.39 7.30 -8 -5 14 96.59 8.60 -8 -5 14 109.89 16.30 7 5 -14 198.18 19.40 7 5 -14 163.88 16.30 -7 -5 14 197.88 18.20 -7 -5 14 179.68 14.30 -7 -5 14 173.78 12.80 -7 -5 14 192.68 13.10 -7 -5 14 192.48 17.00 -7 -5 14 188.18 12.60 -7 -5 14 178.58 13.60 -7 -5 14 188.58 12.90 -7 -5 14 179.88 13.40 6 5 -14 23.10 7.60 6 5 -14 12.90 7.90 6 5 -14 11.00 4.80 -6 -5 14 30.40 8.80 -6 -5 14 26.40 5.00 -6 -5 14 15.30 4.50 -6 -5 14 21.20 6.20 -6 -5 14 38.60 9.00 -6 -5 14 21.30 4.50 -6 -5 14 38.70 7.60 -6 -5 14 28.40 6.00 -6 -5 14 41.30 6.10 5 5 -14 383.66 26.90 5 5 -14 412.06 29.70 5 5 -14 442.16 25.40 -5 -5 14 413.76 27.90 -5 -5 14 396.66 23.40 -5 -5 14 410.96 25.80 -5 -5 14 389.56 23.90 -5 -5 14 419.96 28.50 -5 -5 14 368.96 21.40 -5 -5 14 411.66 24.60 -5 -5 14 399.36 25.60 4 5 -14 136.29 15.30 4 5 -14 158.58 13.40 4 5 -14 156.18 14.40 4 5 -14 139.49 14.50 -4 -5 14 153.48 11.50 -4 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35.60 8.10 -8 -3 14 54.69 10.00 -8 -3 14 55.79 8.00 -8 -3 14 50.39 9.10 -8 -3 14 71.49 7.30 -8 -3 14 57.59 11.60 -8 -3 14 49.10 5.00 7 3 -14 10.30 6.90 7 3 -14 5.10 6.40 7 3 -14 8.00 4.90 -7 -3 14 7.90 4.50 -7 -3 14 13.50 3.50 -7 -3 14 9.60 6.60 -7 -3 14 8.90 6.20 -7 -3 14 10.50 2.90 -7 -3 14 15.80 5.70 -7 -3 14 15.20 6.80 6 3 -14 6.10 6.00 6 3 -14 1.70 6.50 6 3 -14 -1.20 4.20 -6 -3 14 5.80 4.80 -6 -3 14 0.30 2.10 -6 -3 14 2.50 4.60 -6 -3 14 7.40 4.50 -6 -3 14 4.80 2.90 -6 -3 14 8.40 3.10 -6 -3 14 -0.50 5.10 -6 -3 14 0.20 4.00 5 3 -14 60.49 11.00 5 3 -14 61.29 9.90 5 3 -14 50.99 11.20 -5 -3 14 66.29 9.30 -5 -3 14 57.39 6.40 -5 -3 14 69.19 7.30 -5 -3 14 60.59 10.00 -5 -3 14 56.89 10.30 -5 -3 14 54.59 6.10 4 3 -14 7.60 5.60 4 3 -14 5.40 6.20 4 3 -14 18.40 6.20 4 3 -14 20.70 7.20 -4 -3 14 8.50 5.10 -4 -3 14 12.60 4.80 -4 -3 14 21.90 6.40 -4 -3 14 10.30 4.10 -4 -3 14 14.40 4.70 3 3 -14 675.23 43.40 3 3 -14 736.83 42.70 3 3 -14 682.73 41.60 3 3 -14 676.33 42.20 -3 -3 14 692.23 42.00 -3 -3 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8.30 -7 9 -21 22.30 9.50 -7 9 -21 5.20 11.10 7 -9 21 -0.20 9.40 7 -9 21 3.80 9.50 7 -9 21 2.50 11.70 -8 9 -21 1.60 6.50 -8 9 -21 11.80 12.20 -8 9 -21 6.90 11.00 -8 9 -21 -9.80 7.30 8 -9 21 -12.10 9.40 10 8 -21 24.00 11.50 10 8 -21 21.20 9.70 -10 -8 21 15.80 8.40 -10 -8 21 32.80 11.30 9 8 -21 4.20 14.10 9 8 -21 6.00 8.10 -9 -8 21 -5.40 7.00 -9 -8 21 0.40 5.30 -9 -8 21 -11.30 7.20 8 8 -21 5.80 9.00 8 8 -21 30.80 7.20 8 8 -21 6.20 7.70 -8 -8 21 14.30 6.30 -8 -8 21 21.50 10.70 7 8 -21 97.89 10.90 7 8 -21 85.89 16.10 7 8 -21 68.79 14.40 -7 -8 21 93.29 16.40 -7 -8 21 86.89 11.80 6 8 -21 119.69 14.40 6 8 -21 120.79 17.90 6 8 -21 89.79 16.60 -6 -8 21 122.59 12.30 -6 -8 21 101.19 8.80 -6 -8 21 122.29 18.50 5 8 -21 18.70 9.10 5 8 -21 2.80 5.90 5 8 -21 2.40 7.30 -5 -8 21 20.50 7.00 -5 -8 21 21.70 12.20 4 8 -21 17.90 8.50 4 8 -21 14.30 8.40 4 8 -21 35.30 10.80 -4 -8 21 43.80 12.50 -4 -8 21 32.70 8.40 -4 -8 21 30.60 6.10 3 8 -21 21.50 8.60 3 8 -21 23.40 8.70 -3 -8 21 15.90 5.50 -3 -8 21 29.50 10.90 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11.10 -5 8 -21 8.80 8.00 5 -8 21 9.50 9.50 5 -8 21 12.10 10.60 -6 8 -21 1.40 7.40 -6 8 -21 2.70 7.90 -6 8 -21 9.20 8.20 -6 8 -21 18.40 9.60 6 -8 21 9.00 10.60 6 -8 21 14.70 9.60 6 -8 21 -5.10 8.80 -7 8 -21 3.70 9.40 -7 8 -21 9.00 9.10 -7 8 -21 -3.30 9.10 -7 8 -21 4.30 8.30 7 -8 21 29.00 12.60 7 -8 21 19.60 12.50 7 -8 21 6.70 10.10 -8 8 -21 0.10 10.90 -8 8 -21 1.00 8.60 -8 8 -21 11.00 8.80 -8 8 -21 13.90 12.20 8 -8 21 -6.10 9.50 10 7 -21 3.30 8.00 10 7 -21 -8.70 8.20 -10 -7 21 1.50 8.10 -10 -7 21 33.50 10.70 9 7 -21 4.30 10.60 9 7 -21 19.20 8.60 -9 -7 21 17.80 9.50 -9 -7 21 9.40 8.60 -9 -7 21 39.20 11.60 8 7 -21 77.79 14.40 8 7 -21 76.99 17.10 8 7 -21 34.00 10.30 -8 -7 21 50.59 9.00 -8 -7 21 51.09 12.60 7 7 -21 46.70 11.30 7 7 -21 22.50 10.70 7 7 -21 36.60 8.30 -7 -7 21 31.90 10.80 -7 -7 21 48.10 8.80 -7 -7 21 33.00 6.40 6 7 -21 4.50 6.40 6 7 -21 7.10 8.20 6 7 -21 3.00 9.20 -6 -7 21 5.40 4.70 -6 -7 21 7.30 6.20 -6 -7 21 4.60 4.30 -6 -7 21 19.40 11.60 5 7 -21 -7.00 6.70 5 7 -21 3.10 6.30 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16.90 -4 7 -21 96.69 17.30 -4 7 -21 122.19 28.00 -4 7 -21 93.89 14.80 4 -7 21 134.29 20.40 4 -7 21 70.99 16.70 -5 7 -21 93.39 17.20 -5 7 -21 66.09 15.20 -5 7 -21 88.19 14.60 -5 7 -21 104.29 17.60 5 -7 21 67.29 16.60 5 -7 21 98.39 18.70 5 -7 21 64.29 13.40 5 -7 21 99.59 17.90 -6 7 -21 27.20 9.20 -6 7 -21 7.20 9.80 -6 7 -21 18.20 11.30 -6 7 -21 26.20 11.40 6 -7 21 22.60 12.10 6 -7 21 16.90 9.60 6 -7 21 3.80 8.80 -7 7 -21 102.89 18.40 -7 7 -21 69.99 13.30 -7 7 -21 89.79 18.80 7 -7 21 92.79 17.80 7 -7 21 76.89 17.40 7 -7 21 78.99 19.70 -8 7 -21 10.40 12.50 -8 7 -21 16.20 8.30 8 -7 21 13.00 12.70 10 6 -21 15.80 10.50 10 6 -21 13.00 8.40 -10 -6 21 -0.90 7.90 -10 -6 21 22.60 10.00 9 6 -21 -3.20 7.40 9 6 -21 5.10 7.90 -9 -6 21 2.90 8.30 -9 -6 21 -1.50 7.80 8 6 -21 -2.10 8.60 8 6 -21 28.70 8.00 8 6 -21 -8.10 6.00 -8 -6 21 0.80 7.90 -8 -6 21 8.90 5.00 -8 -6 21 11.50 5.40 7 6 -21 26.60 8.10 7 6 -21 12.30 9.30 7 6 -21 30.70 11.70 -7 -6 21 23.70 6.90 -7 -6 21 28.70 6.70 -7 -6 21 39.40 10.60 6 6 -21 31.20 10.70 6 6 -21 13.10 8.60 6 6 -21 20.10 8.30 -6 -6 21 11.80 5.90 -6 -6 21 33.50 11.40 -6 -6 21 16.90 5.90 5 6 -21 129.09 18.50 5 6 -21 129.19 14.60 -5 -6 21 126.69 13.20 -5 -6 21 148.89 16.40 4 6 -21 32.50 9.90 4 6 -21 1.00 7.10 -4 -6 21 10.50 6.00 -4 -6 21 -5.20 4.20 -4 -6 21 8.30 8.00 3 6 -21 25.60 10.00 3 6 -21 42.00 10.60 -3 -6 21 52.09 12.60 -3 -6 21 70.99 9.80 -3 -6 21 50.59 10.40 2 6 -21 385.16 28.80 2 6 -21 380.26 29.40 -2 -6 21 409.16 30.50 -2 -6 21 399.06 28.50 1 6 -21 82.19 9.20 1 6 -21 89.99 23.80 1 6 -21 69.49 9.00 1 6 -21 49.70 11.90 -1 -6 21 75.79 13.40 -1 -6 21 74.99 14.80 0 6 -21 5.50 6.20 0 6 -21 7.80 6.50 0 6 -21 -2.00 5.90 0 6 -21 0.30 5.80 0 -6 21 5.10 7.00 0 -6 21 2.50 7.60 -1 6 -21 9.40 7.70 -1 6 -21 7.80 7.50 -1 6 -21 6.10 7.10 1 -6 21 19.70 8.40 1 -6 21 25.00 10.60 -2 6 -21 40.80 11.60 -2 6 -21 29.10 11.10 -2 6 -21 24.90 10.30 -2 6 -21 62.39 9.00 -2 6 -21 68.19 12.10 2 -6 21 40.00 15.20 -3 6 -21 37.20 9.60 -3 6 -21 24.10 10.60 -3 6 -21 48.70 11.30 -3 6 -21 27.90 11.10 -3 6 -21 29.00 9.80 3 -6 21 30.20 10.50 3 -6 21 27.10 12.40 -4 6 -21 142.99 17.90 -4 6 -21 111.29 18.20 -4 6 -21 112.49 18.80 -4 6 -21 84.29 15.30 4 -6 21 91.89 18.60 4 -6 21 122.49 18.60 -5 6 -21 136.39 19.90 -5 6 -21 157.48 22.60 -5 6 -21 144.19 16.00 -5 6 -21 139.09 21.20 5 -6 21 137.39 20.90 5 -6 21 128.09 22.40 5 -6 21 98.49 19.20 -6 6 -21 69.39 14.50 -6 6 -21 93.59 18.50 -6 6 -21 74.79 12.90 -6 6 -21 77.49 16.50 6 -6 21 67.39 15.60 6 -6 21 56.59 15.00 6 -6 21 71.39 19.00 -7 6 -21 3.90 7.60 -7 6 -21 15.20 10.80 -7 6 -21 22.80 11.40 -7 6 -21 12.20 10.30 7 -6 21 -5.20 8.40 7 -6 21 -2.80 7.80 7 -6 21 -16.60 8.20 -8 6 -21 -0.80 7.30 -8 6 -21 20.40 14.80 8 -6 21 17.00 19.20 8 -6 21 16.40 14.30 10 5 -21 9.80 10.30 10 5 -21 12.70 8.80 -10 -5 21 6.30 7.70 -10 -5 21 7.50 8.70 9 5 -21 2.80 8.80 9 5 -21 0.90 9.80 -9 -5 21 0.30 6.60 -9 -5 21 4.60 8.20 -9 -5 21 9.50 7.00 8 5 -21 -1.00 7.60 8 5 -21 6.00 6.80 8 5 -21 18.80 10.30 -8 -5 21 5.80 8.30 -8 -5 21 22.70 9.10 -8 -5 21 0.80 4.60 7 5 -21 78.79 14.40 7 5 -21 114.49 12.70 7 5 -21 96.29 16.80 -7 -5 21 88.69 15.10 -7 -5 21 77.49 12.40 6 5 -21 -0.90 6.30 6 5 -21 -5.40 6.70 -6 -5 21 12.00 7.80 -6 -5 21 6.20 5.40 -6 -5 21 0.90 4.30 5 5 -21 -9.30 7.70 5 5 -21 9.70 7.50 -5 -5 21 7.50 7.20 -5 -5 21 15.90 6.70 -5 -5 21 12.80 6.00 4 5 -21 21.30 9.60 4 5 -21 22.60 8.60 -4 -5 21 19.30 9.00 -4 -5 21 36.20 8.80 -4 -5 21 28.20 7.50 3 5 -21 -0.80 6.80 3 5 -21 8.10 7.30 -3 -5 21 27.70 8.30 -3 -5 21 6.10 8.40 2 5 -21 19.90 8.80 2 5 -21 -2.80 6.60 -2 -5 21 2.20 6.70 -2 -5 21 -2.30 6.80 1 5 -21 53.79 12.70 1 5 -21 82.59 8.40 1 5 -21 78.99 8.70 -1 -5 21 51.59 12.60 -1 -5 21 67.59 14.30 0 5 -21 69.69 14.50 0 5 -21 65.29 9.90 0 -5 21 94.19 15.30 0 -5 21 58.89 13.70 -1 5 -21 8.70 8.70 -1 5 -21 1.60 7.00 -1 5 -21 -1.60 6.10 -1 5 -21 -6.30 3.70 1 -5 21 20.70 8.80 1 -5 21 7.80 9.30 -2 5 -21 -1.70 5.50 -2 5 -21 1.70 7.80 -2 5 -21 -0.50 6.90 -2 5 -21 16.70 7.40 -3 5 -21 11.10 7.90 -3 5 -21 -0.30 7.30 -3 5 -21 5.70 8.00 -3 5 -21 15.40 9.30 -3 5 -21 -0.40 8.40 3 -5 21 12.10 8.40 3 -5 21 14.20 11.50 -4 5 -21 26.30 11.20 -4 5 -21 15.40 8.70 -4 5 -21 22.80 9.60 -4 5 -21 17.10 9.70 4 -5 21 15.20 9.60 4 -5 21 31.50 10.30 4 -5 21 28.30 11.30 -5 5 -21 32.50 11.20 -5 5 -21 48.20 13.50 -5 5 -21 43.10 11.30 -5 5 -21 45.30 12.90 5 -5 21 62.49 14.60 5 -5 21 53.29 14.70 5 -5 21 45.50 13.90 -6 5 -21 43.00 11.90 -6 5 -21 51.99 11.60 -6 5 -21 37.00 12.60 -6 5 -21 50.19 13.40 6 -5 21 38.70 14.70 6 -5 21 37.00 12.50 6 -5 21 40.80 13.50 -7 5 -21 16.70 9.80 -7 5 -21 30.40 11.90 -7 5 -21 23.40 11.10 -7 5 -21 28.00 9.40 7 -5 21 35.70 14.10 7 -5 21 35.50 16.80 7 -5 21 40.70 13.30 -8 5 -21 150.08 16.30 8 -5 21 162.58 29.00 8 -5 21 136.69 27.10 10 4 -21 34.60 10.50 -10 -4 21 13.20 8.50 -10 -4 21 34.50 9.50 9 4 -21 -4.90 9.00 -9 -4 21 10.20 6.30 -9 -4 21 0.80 7.60 -9 -4 21 -3.40 8.00 8 4 -21 19.00 8.90 8 4 -21 10.60 6.70 -8 -4 21 -3.50 7.60 -8 -4 21 19.40 5.20 -8 -4 21 11.00 6.70 7 4 -21 13.30 8.30 7 4 -21 25.20 8.60 -7 -4 21 -5.60 5.10 -7 -4 21 24.30 9.00 -7 -4 21 9.60 4.80 6 4 -21 37.60 12.50 6 4 -21 46.70 10.50 -6 -4 21 40.60 11.30 -6 -4 21 43.20 8.40 5 4 -21 153.28 17.10 5 4 -21 157.08 17.10 -5 -4 21 164.68 17.40 -5 -4 21 147.79 14.50 4 4 -21 50.79 11.70 4 4 -21 49.50 12.40 -4 -4 21 58.59 10.10 -4 -4 21 61.49 13.30 3 4 -21 -3.40 7.40 3 4 -21 -5.00 6.20 -3 -4 21 11.00 8.10 -3 -4 21 13.80 7.20 2 4 -21 25.00 10.20 2 4 -21 12.60 7.90 -2 -4 21 11.90 7.80 -2 -4 21 24.20 9.50 1 4 -21 4.70 9.30 1 4 -21 11.20 4.90 1 4 -21 1.30 4.40 1 4 -21 12.50 8.70 -1 -4 21 14.20 9.00 -1 -4 21 5.30 7.50 0 4 -21 0.90 6.40 0 4 -21 8.70 5.80 0 4 -21 14.70 8.20 0 -4 21 3.90 8.10 0 -4 21 -2.80 5.70 -1 4 -21 58.79 11.80 -1 4 -21 62.99 7.60 -1 4 -21 54.29 10.90 1 -4 21 61.29 15.00 1 -4 21 61.39 13.80 -2 4 -21 13.80 8.10 -2 4 -21 16.10 8.40 -2 4 -21 5.70 5.80 -2 4 -21 19.90 9.40 2 -4 21 19.60 10.30 2 -4 21 3.20 9.20 -3 4 -21 19.00 8.50 -3 4 -21 12.50 8.70 -3 4 -21 27.80 9.40 -3 4 -21 23.80 10.20 3 -4 21 0.80 7.60 3 -4 21 -2.00 7.90 3 -4 21 15.10 9.20 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57.19 13.50 -3 -16 22 29.00 9.80 2 16 -22 91.09 14.60 2 16 -22 75.39 10.60 2 16 -22 62.19 14.00 -2 -16 22 80.89 16.00 -2 -16 22 58.39 15.90 -2 -16 22 67.69 10.60 1 16 -22 102.79 15.50 1 16 -22 152.88 20.60 1 16 -22 159.58 15.50 1 16 -22 122.79 17.90 -1 -16 22 112.19 12.80 -1 -16 22 157.88 20.80 -1 -16 22 135.09 21.40 0 16 -22 19.70 7.80 0 16 -22 7.60 9.30 0 16 -22 34.00 10.60 0 16 -22 19.90 9.50 0 -16 22 9.20 8.90 0 -16 22 35.80 13.80 0 -16 22 30.30 8.30 -1 16 -22 1.90 7.20 -1 16 -22 8.50 8.90 -1 16 -22 11.60 6.90 -1 16 -22 8.20 7.50 1 -16 22 7.30 5.90 1 -16 22 0.80 9.30 1 -16 22 23.50 11.30 -2 16 -22 31.90 11.10 -2 16 -22 10.70 6.50 -2 16 -22 10.00 9.80 -2 16 -22 8.70 7.90 -2 16 -22 16.00 9.30 2 -16 22 17.70 8.70 2 -16 22 17.50 10.70 2 -16 22 6.90 6.60 -3 16 -22 20.90 9.50 -3 16 -22 37.50 11.20 -3 16 -22 43.90 13.90 -3 16 -22 29.30 12.00 -3 16 -22 56.89 12.90 3 -16 22 51.39 11.20 3 -16 22 19.40 13.10 3 -16 22 33.80 11.80 -4 16 -22 54.79 12.50 -4 16 -22 58.29 14.50 -4 16 -22 74.69 16.60 -4 16 -22 90.39 15.40 -4 16 -22 54.09 14.60 4 -16 22 51.09 12.10 4 -16 22 87.19 17.10 4 -16 22 66.79 17.00 -5 16 -22 -3.80 9.20 -5 16 -22 19.90 11.50 -5 16 -22 -5.80 7.60 -5 16 -22 -1.60 7.50 5 -16 22 3.70 9.30 5 -16 22 -10.50 8.10 -6 16 -22 28.30 12.70 -6 16 -22 11.10 10.80 -6 16 -22 14.70 8.40 -6 16 -22 18.80 10.90 -6 16 -22 43.80 13.90 6 -16 22 15.50 9.90 6 -16 22 18.10 11.90 6 -16 22 13.80 9.40 7 15 -22 17.10 8.00 -7 -15 22 -13.60 13.60 -7 -15 22 -3.50 7.60 6 15 -22 44.00 10.00 6 15 -22 15.70 10.90 -6 -15 22 32.90 9.00 -6 -15 22 33.80 12.30 5 15 -22 28.20 9.00 5 15 -22 27.90 10.40 5 15 -22 17.60 7.90 -5 -15 22 33.30 12.60 -5 -15 22 23.50 9.00 -5 -15 22 27.90 7.60 4 15 -22 8.60 8.50 4 15 -22 27.80 8.10 4 15 -22 40.20 11.40 -4 -15 22 14.60 11.00 -4 -15 22 12.30 8.30 -4 -15 22 26.80 6.20 3 15 -22 25.70 9.20 3 15 -22 22.40 4.20 3 15 -22 11.80 8.00 3 15 -22 0.20 6.90 -3 -15 22 20.30 12.20 -3 -15 22 24.20 6.10 -3 -15 22 23.40 10.00 2 15 -22 19.50 8.70 2 15 -22 18.90 9.00 2 15 -22 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15 -22 0.90 9.30 -5 15 -22 9.60 8.20 5 -15 22 6.50 9.20 5 -15 22 4.10 10.80 5 -15 22 7.90 11.70 -6 15 -22 2.80 9.60 -6 15 -22 12.30 9.00 -6 15 -22 0.40 8.40 6 -15 22 26.20 13.70 6 -15 22 9.40 9.80 6 -15 22 32.60 11.00 8 14 -22 19.30 10.20 8 14 -22 7.00 8.30 -8 -14 22 18.50 10.50 -8 -14 22 8.50 11.20 7 14 -22 41.80 12.20 7 14 -22 60.79 12.90 -7 -14 22 70.79 16.50 6 14 -22 3.00 8.30 6 14 -22 17.70 8.50 6 14 -22 24.30 7.90 -6 -14 22 16.50 11.10 5 14 -22 5.50 8.00 5 14 -22 20.40 9.60 5 14 -22 16.90 7.20 -5 -14 22 5.80 9.40 4 14 -22 1.70 6.90 4 14 -22 -2.00 6.50 4 14 -22 -8.20 7.30 -4 -14 22 9.50 8.40 -4 -14 22 -0.40 9.20 -4 -14 22 3.10 3.50 3 14 -22 -1.40 6.80 3 14 -22 18.30 9.70 3 14 -22 -6.00 6.60 -3 -14 22 17.50 10.80 -3 -14 22 10.00 8.00 -3 -14 22 6.50 4.20 2 14 -22 104.49 15.30 2 14 -22 94.19 15.20 2 14 -22 85.49 16.00 -2 -14 22 111.79 17.40 -2 -14 22 138.59 22.50 -2 -14 22 125.49 10.90 1 14 -22 12.80 8.70 1 14 -22 -2.30 6.50 1 14 -22 5.70 7.20 -1 -14 22 12.10 9.60 -1 -14 22 26.30 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6.20 -6 14 -22 -10.90 9.10 -6 14 -22 12.30 8.60 -6 14 -22 4.20 8.50 6 -14 22 11.10 10.90 6 -14 22 -1.50 11.70 6 -14 22 1.00 9.00 8 13 -22 50.79 12.60 8 13 -22 23.80 10.40 -8 -13 22 31.90 9.60 7 13 -22 6.10 9.30 7 13 -22 1.70 7.60 -7 -13 22 10.60 6.50 -7 -13 22 1.90 8.60 6 13 -22 -6.60 6.40 6 13 -22 6.30 6.60 6 13 -22 6.90 8.00 -6 -13 22 6.80 9.30 -6 -13 22 6.70 6.90 5 13 -22 41.60 9.20 5 13 -22 39.70 11.60 5 13 -22 53.89 11.40 -5 -13 22 25.80 12.70 -5 -13 22 62.89 12.60 4 13 -22 45.10 10.20 4 13 -22 25.30 10.90 4 13 -22 42.30 11.90 -4 -13 22 31.20 13.00 -4 -13 22 45.90 11.20 3 13 -22 42.30 10.10 3 13 -22 50.09 12.70 3 13 -22 30.60 8.10 -3 -13 22 40.90 5.30 -3 -13 22 33.20 12.00 2 13 -22 5.40 4.90 2 13 -22 0.40 6.90 2 13 -22 -9.20 6.30 2 13 -22 16.20 8.50 2 13 -22 -0.80 7.30 -2 -13 22 -10.50 6.60 -2 -13 22 18.20 9.70 -2 -13 22 -3.10 3.70 -2 -13 22 -2.80 3.90 1 13 -22 61.09 12.90 1 13 -22 54.19 12.60 1 13 -22 50.19 9.70 -1 -13 22 54.09 8.30 -1 -13 22 60.09 16.70 -1 -13 22 50.29 12.90 -1 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10.70 -7 13 -22 20.40 10.10 -7 13 -22 1.90 8.80 7 -13 22 29.30 11.80 7 -13 22 13.70 9.60 7 -13 22 15.80 13.50 8 12 -22 33.10 10.70 8 12 -22 39.10 19.60 -8 -12 22 18.70 12.40 -8 -12 22 57.19 10.20 7 12 -22 18.90 10.40 7 12 -22 15.60 9.40 -7 -12 22 31.20 8.40 -7 -12 22 30.00 11.80 6 12 -22 8.00 7.00 6 12 -22 21.40 7.40 6 12 -22 30.90 10.30 -6 -12 22 29.70 8.50 -6 -12 22 9.10 9.50 5 12 -22 6.50 8.40 5 12 -22 3.60 6.70 5 12 -22 -1.20 6.90 -5 -12 22 0.70 6.50 -5 -12 22 -3.50 7.30 4 12 -22 9.50 8.00 4 12 -22 10.60 8.00 4 12 -22 -0.40 7.30 -4 -12 22 13.00 7.40 -4 -12 22 7.70 10.00 3 12 -22 0.00 6.70 3 12 -22 1.30 7.60 3 12 -22 -3.50 6.60 -3 -12 22 25.30 11.20 -3 -12 22 -0.30 6.20 2 12 -22 18.40 8.80 2 12 -22 1.80 5.40 2 12 -22 4.90 7.80 2 12 -22 6.20 4.40 2 12 -22 1.00 7.00 -2 -12 22 7.70 3.30 -2 -12 22 1.30 8.20 -2 -12 22 11.40 4.80 -2 -12 22 7.50 8.90 1 12 -22 134.79 18.50 1 12 -22 111.89 13.10 1 12 -22 154.88 13.90 1 12 -22 155.78 20.00 -1 -12 22 109.29 10.10 -1 -12 22 104.19 18.70 -1 -12 22 131.89 19.30 0 12 -22 12.80 6.90 0 12 -22 7.80 8.50 0 12 -22 25.70 10.20 0 12 -22 19.60 8.10 0 -12 22 27.60 12.50 0 -12 22 17.30 6.20 0 -12 22 26.60 9.60 -1 12 -22 24.10 10.50 -1 12 -22 17.30 7.60 -1 12 -22 29.50 10.90 -1 12 -22 28.40 9.50 1 -12 22 18.90 9.90 1 -12 22 22.90 6.70 1 -12 22 20.80 11.60 -2 12 -22 165.18 21.10 -2 12 -22 188.18 20.80 -2 12 -22 217.38 18.00 2 -12 22 150.78 21.50 2 -12 22 187.28 21.20 2 -12 22 177.28 16.50 -3 12 -22 16.90 9.00 -3 12 -22 37.10 12.30 -3 12 -22 24.20 9.10 -3 12 -22 36.60 11.30 3 -12 22 28.80 11.60 3 -12 22 23.90 8.90 3 -12 22 30.80 11.60 -4 12 -22 110.89 19.10 -4 12 -22 118.69 18.50 -4 12 -22 112.49 16.80 -4 12 -22 96.59 15.30 4 -12 22 70.29 15.60 4 -12 22 104.59 14.70 4 -12 22 79.49 16.90 -5 12 -22 -3.00 7.70 -5 12 -22 -2.30 6.70 -5 12 -22 6.40 8.90 -5 12 -22 3.20 9.30 5 -12 22 8.60 10.70 5 -12 22 10.70 8.30 -6 12 -22 1.30 9.20 -6 12 -22 8.30 8.50 -6 12 -22 3.90 8.50 -6 12 -22 16.40 8.80 6 -12 22 5.90 10.90 6 -12 22 19.70 9.90 6 -12 22 27.00 10.90 -7 12 -22 67.79 13.70 -7 12 -22 82.09 18.00 -7 12 -22 52.79 13.20 -7 12 -22 70.49 17.80 7 -12 22 45.30 12.90 7 -12 22 67.09 18.80 7 -12 22 64.29 16.60 7 -12 22 73.39 15.50 9 11 -22 8.50 8.60 -9 -11 22 2.90 8.00 8 11 -22 -0.80 8.50 8 11 -22 -1.70 14.30 -8 -11 22 0.90 6.60 -8 -11 22 4.30 8.30 7 11 -22 1.40 8.30 7 11 -22 4.20 7.90 7 11 -22 4.20 6.70 -7 -11 22 0.70 5.90 -7 -11 22 8.40 10.00 6 11 -22 3.50 6.60 6 11 -22 11.20 8.00 6 11 -22 13.10 8.50 -6 -11 22 6.10 6.00 -6 -11 22 1.40 7.70 5 11 -22 5.00 6.90 5 11 -22 -4.80 7.30 5 11 -22 7.20 8.10 -5 -11 22 -5.90 8.60 -5 -11 22 13.00 7.60 4 11 -22 2.60 7.20 4 11 -22 13.80 6.90 4 11 -22 -6.90 7.20 -4 -11 22 12.00 7.10 -4 -11 22 -1.40 7.80 3 11 -22 7.20 7.90 3 11 -22 -2.80 8.30 3 11 -22 -13.90 5.60 -3 -11 22 1.40 9.30 -3 -11 22 4.00 6.90 -3 -11 22 9.70 3.80 2 11 -22 30.50 5.80 2 11 -22 39.60 10.70 2 11 -22 46.30 7.30 2 11 -22 40.90 11.30 -2 -11 22 48.70 11.90 -2 -11 22 24.30 5.90 -2 -11 22 31.10 11.80 1 11 -22 26.70 9.20 1 11 -22 43.80 12.10 1 11 -22 34.30 7.70 1 11 -22 36.00 10.90 -1 -11 22 4.20 10.10 -1 -11 22 26.40 4.90 -1 -11 22 19.80 6.40 0 11 -22 95.29 12.20 0 11 -22 109.39 14.50 0 11 -22 68.19 14.60 0 -11 22 75.99 16.60 0 -11 22 56.39 8.40 0 -11 22 76.59 14.00 -1 11 -22 2.80 8.40 -1 11 -22 5.10 7.20 -1 11 -22 13.10 6.80 -1 11 -22 2.60 10.60 -1 11 -22 -1.00 7.00 1 -11 22 6.50 7.30 1 -11 22 8.80 11.90 1 -11 22 6.80 5.00 -2 11 -22 49.90 10.60 -2 11 -22 71.29 14.90 -2 11 -22 49.90 12.20 -2 11 -22 70.49 13.80 2 -11 22 68.69 16.90 2 -11 22 57.39 14.10 2 -11 22 62.49 10.50 -3 11 -22 20.20 9.50 -3 11 -22 11.50 7.80 -3 11 -22 22.30 9.10 -3 11 -22 9.90 8.90 3 -11 22 -2.00 10.80 3 -11 22 24.40 7.60 3 -11 22 20.00 10.00 3 -11 22 26.00 12.50 -4 11 -22 74.99 15.00 -4 11 -22 52.49 11.80 -4 11 -22 78.19 15.70 -4 11 -22 52.89 13.30 4 -11 22 71.79 12.10 4 -11 22 42.60 11.90 4 -11 22 64.39 15.20 -5 11 -22 53.09 12.80 -5 11 -22 42.40 10.80 -5 11 -22 41.70 12.70 -5 11 -22 73.29 14.10 5 -11 22 53.09 15.30 5 -11 22 30.60 11.20 5 -11 22 29.50 11.30 -6 11 -22 6.20 10.00 -6 11 -22 4.90 7.40 -6 11 -22 -3.10 7.00 -6 11 -22 7.10 9.40 6 -11 22 -0.70 9.90 6 -11 22 0.40 8.60 6 -11 22 -8.90 6.90 -7 11 -22 4.70 10.00 -7 11 -22 9.10 10.50 -7 11 -22 13.40 8.40 7 -11 22 12.60 12.00 7 -11 22 20.40 12.60 7 -11 22 14.70 11.50 9 10 -22 -3.00 9.10 9 10 -22 30.90 9.80 -9 -10 22 -3.50 9.20 -9 -10 22 -5.50 7.80 8 10 -22 -6.00 7.90 8 10 -22 -1.40 7.60 -8 -10 22 -14.10 7.10 -8 -10 22 6.30 6.30 7 10 -22 5.10 9.50 7 10 -22 17.70 9.40 -7 -10 22 0.40 7.90 -7 -10 22 15.90 6.40 6 10 -22 2.60 6.10 6 10 -22 6.60 9.10 6 10 -22 7.60 8.00 -6 -10 22 14.60 5.90 -6 -10 22 4.60 8.40 5 10 -22 27.50 9.10 5 10 -22 14.70 7.70 5 10 -22 18.30 10.80 -5 -10 22 27.90 8.70 -5 -10 22 25.60 10.70 4 10 -22 10.10 8.40 4 10 -22 2.70 6.90 4 10 -22 12.20 7.60 -4 -10 22 1.30 3.70 -4 -10 22 16.70 11.00 -4 -10 22 1.10 6.30 3 10 -22 10.20 7.90 3 10 -22 2.70 8.30 -3 -10 22 17.60 9.20 -3 -10 22 -0.40 6.80 -3 -10 22 -3.30 3.60 2 10 -22 58.39 12.40 2 10 -22 65.29 12.30 -2 -10 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16.90 8.40 -9 -8 22 30.50 10.80 8 8 -22 29.30 10.20 8 8 -22 10.20 10.10 -8 -8 22 38.40 7.90 -8 -8 22 28.80 12.40 7 8 -22 34.70 11.80 7 8 -22 49.30 11.90 7 8 -22 29.00 8.50 -7 -8 22 45.90 9.10 -7 -8 22 48.70 12.70 6 8 -22 1.00 6.40 6 8 -22 7.50 9.70 6 8 -22 9.20 9.20 -6 -8 22 15.90 6.20 -6 -8 22 23.10 10.10 -6 -8 22 1.10 3.90 5 8 -22 -0.90 8.60 5 8 -22 1.90 7.40 5 8 -22 5.10 6.80 -5 -8 22 -6.90 4.90 -5 -8 22 4.70 9.10 -5 -8 22 2.60 6.30 4 8 -22 9.80 7.00 4 8 -22 10.10 9.30 -4 -8 22 -2.10 4.40 -4 -8 22 5.70 8.40 -4 -8 22 10.60 5.90 3 8 -22 10.70 8.30 3 8 -22 2.20 7.00 -3 -8 22 -1.00 6.10 -3 -8 22 -1.90 7.30 -3 -8 22 1.40 4.40 2 8 -22 6.20 6.80 2 8 -22 4.10 7.60 -2 -8 22 8.00 12.30 -2 -8 22 1.00 6.70 -2 -8 22 2.30 5.20 1 8 -22 39.30 10.10 1 8 -22 40.20 10.90 1 8 -22 39.80 7.70 -1 -8 22 41.00 11.00 -1 -8 22 49.50 13.10 0 8 -22 65.39 15.80 0 8 -22 72.09 22.80 0 8 -22 64.89 11.10 0 8 -22 53.59 12.70 0 8 -22 49.60 9.70 0 -8 22 56.59 12.50 0 -8 22 59.99 14.80 -1 8 -22 -8.00 6.60 -1 8 -22 10.50 8.10 -1 8 -22 9.90 7.60 -1 8 -22 11.70 9.40 -1 8 -22 7.10 5.70 1 -8 22 -9.60 8.00 1 -8 22 10.90 9.30 -2 8 -22 -1.70 6.00 -2 8 -22 -5.20 6.50 -2 8 -22 10.10 7.80 -2 8 -22 2.70 7.00 -2 8 -22 5.40 8.10 2 -8 22 8.00 10.50 2 -8 22 0.20 8.00 -3 8 -22 9.70 8.80 -3 8 -22 10.20 10.30 -3 8 -22 25.90 9.10 -3 8 -22 19.40 9.30 3 -8 22 22.70 10.80 3 -8 22 7.20 10.40 -4 8 -22 -2.80 6.10 -4 8 -22 0.40 8.50 -4 8 -22 11.30 8.40 -4 8 -22 11.60 7.90 4 -8 22 3.00 9.40 4 -8 22 -2.30 9.40 -5 8 -22 19.70 8.90 -5 8 -22 10.90 9.40 -5 8 -22 -0.70 7.70 -5 8 -22 11.10 11.10 5 -8 22 21.10 8.90 5 -8 22 17.40 9.50 5 -8 22 28.90 12.00 -6 8 -22 15.70 9.00 -6 8 -22 -0.60 8.80 -6 8 -22 11.70 9.80 -6 8 -22 16.50 10.60 6 -8 22 4.20 9.30 6 -8 22 6.50 10.50 6 -8 22 12.00 8.50 -7 8 -22 5.80 11.00 -7 8 -22 17.10 10.10 -7 8 -22 12.00 7.30 -8 8 -22 38.10 9.10 -8 8 -22 52.89 14.40 -8 8 -22 20.80 11.60 -8 8 -22 40.60 12.40 8 -8 22 11.60 13.70 8 -8 22 53.99 15.80 8 -8 22 35.00 12.30 9 7 -22 90.89 15.00 9 7 -22 70.79 16.00 -9 -7 22 68.39 14.00 -9 -7 22 108.89 18.10 8 7 -22 19.90 11.00 8 7 -22 30.30 11.40 8 7 -22 23.70 8.20 -8 -7 22 6.20 7.40 -8 -7 22 18.50 6.90 7 7 -22 10.00 6.10 7 7 -22 30.90 11.50 7 7 -22 3.30 7.30 -7 -7 22 19.50 7.30 -7 -7 22 12.60 5.20 -7 -7 22 10.00 8.60 6 7 -22 5.20 9.30 6 7 -22 23.70 9.10 6 7 -22 17.60 11.30 -6 -7 22 22.40 10.50 -6 -7 22 18.50 5.70 -6 -7 22 31.90 8.00 5 7 -22 23.70 9.90 5 7 -22 19.00 7.90 -5 -7 22 9.10 6.00 -5 -7 22 5.30 8.40 -5 -7 22 41.60 7.80 4 7 -22 81.29 14.10 4 7 -22 71.09 14.60 -4 -7 22 81.99 9.30 -4 -7 22 86.69 13.40 3 7 -22 39.10 11.30 3 7 -22 38.30 10.80 -3 -7 22 49.30 8.50 -3 -7 22 30.50 13.00 -3 -7 22 36.30 10.00 2 7 -22 99.29 15.60 2 7 -22 137.59 18.30 -2 -7 22 149.59 15.50 -2 -7 22 154.18 22.90 1 7 -22 34.40 10.30 1 7 -22 47.30 13.20 1 7 -22 61.89 8.30 -1 -7 22 54.59 12.20 0 7 -22 85.39 12.10 0 7 -22 62.39 10.50 0 7 -22 70.69 20.60 0 7 -22 62.69 13.00 0 7 -22 61.39 11.70 0 -7 22 54.19 16.50 0 -7 22 77.69 14.60 -1 7 -22 84.29 13.80 -1 7 -22 89.39 13.80 -1 7 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7.80 8 6 -22 5.80 9.50 8 6 -22 3.40 9.10 8 6 -22 -3.10 6.60 -8 -6 22 -2.10 8.00 -8 -6 22 3.30 5.30 -8 -6 22 9.70 5.70 7 6 -22 23.00 11.10 7 6 -22 29.30 12.10 7 6 -22 32.10 8.50 -7 -6 22 30.20 7.00 -7 -6 22 50.69 12.10 -7 -6 22 48.20 8.90 6 6 -22 40.40 11.50 6 6 -22 27.90 9.70 -6 -6 22 44.00 9.00 -6 -6 22 49.90 12.70 5 6 -22 35.70 10.60 5 6 -22 45.80 11.90 -5 -6 22 39.10 9.60 -5 -6 22 28.30 12.90 -5 -6 22 30.50 7.50 4 6 -22 88.49 13.70 4 6 -22 60.99 13.10 -4 -6 22 51.19 9.30 -4 -6 22 86.09 12.70 -4 -6 22 81.49 14.70 3 6 -22 7.00 8.40 3 6 -22 -7.60 5.50 -3 -6 22 14.20 8.90 -3 -6 22 -1.80 5.20 2 6 -22 21.10 8.30 2 6 -22 10.00 7.90 -2 -6 22 26.70 9.80 -2 -6 22 25.60 8.50 1 6 -22 184.68 13.90 1 6 -22 175.88 18.80 1 6 -22 182.78 13.90 1 6 -22 155.78 18.10 -1 -6 22 160.28 18.10 -1 -6 22 180.18 20.30 0 6 -22 11.80 8.50 0 6 -22 17.10 7.30 0 -6 22 21.40 10.10 0 -6 22 33.60 18.50 -1 6 -22 33.90 10.20 -1 6 -22 15.80 9.20 -1 6 -22 37.30 10.30 -1 6 -22 36.60 6.80 -1 6 -22 58.89 12.10 1 -6 22 19.20 10.80 1 -6 22 32.50 13.10 -2 6 -22 246.48 21.10 -2 6 -22 221.88 21.00 -2 6 -22 246.98 17.60 -2 6 -22 215.78 22.50 -2 6 -22 259.37 21.60 2 -6 22 221.68 22.60 2 -6 22 189.98 22.20 -3 6 -22 13.10 9.50 -3 6 -22 16.40 10.70 -3 6 -22 21.80 9.80 3 -6 22 18.60 9.90 3 -6 22 11.10 11.50 -4 6 -22 -2.30 7.10 -4 6 -22 8.10 8.50 -4 6 -22 26.50 10.30 -4 6 -22 17.40 8.60 4 -6 22 5.30 9.90 4 -6 22 5.70 9.80 4 -6 22 -1.50 5.90 -5 6 -22 -1.80 7.30 -5 6 -22 -0.40 8.20 -5 6 -22 0.90 8.70 -5 6 -22 9.00 8.80 5 -6 22 18.40 11.50 5 -6 22 15.20 9.40 5 -6 22 17.00 10.90 -6 6 -22 42.20 12.90 -6 6 -22 58.69 14.20 -6 6 -22 58.59 14.80 -6 6 -22 52.49 11.70 6 -6 22 88.79 19.00 6 -6 22 100.99 18.40 6 -6 22 55.39 15.40 -7 6 -22 3.90 7.90 -7 6 -22 3.80 10.80 -7 6 -22 3.80 10.70 -7 6 -22 5.40 9.40 7 -6 22 -12.10 17.50 7 -6 22 7.30 10.70 -8 6 -22 54.19 11.40 -8 6 -22 54.49 15.70 -8 6 -22 50.69 14.00 -8 6 -22 24.00 13.00 8 -6 22 49.40 19.10 8 -6 22 54.39 13.50 8 -6 22 71.69 17.20 9 5 -22 20.40 9.40 -9 -5 22 47.70 11.90 -9 -5 22 20.60 10.20 8 5 -22 19.90 9.70 8 5 -22 38.20 9.80 -8 -5 22 42.30 11.70 -8 -5 22 27.20 10.90 -8 -5 22 38.10 8.40 7 5 -22 19.30 8.40 7 5 -22 10.90 8.80 -7 -5 22 22.10 6.90 -7 -5 22 21.50 8.80 -7 -5 22 18.60 6.50 6 5 -22 13.80 8.20 6 5 -22 -5.40 7.20 -6 -5 22 9.00 8.50 -6 -5 22 -0.50 5.20 5 5 -22 39.90 10.40 5 5 -22 34.20 11.10 -5 -5 22 35.10 11.20 -5 -5 22 39.80 8.90 4 5 -22 -0.80 8.70 4 5 -22 -2.70 7.70 -4 -5 22 -2.70 6.80 -4 -5 22 11.80 5.50 3 5 -22 12.50 10.10 3 5 -22 16.60 8.00 -3 -5 22 22.50 7.70 -3 -5 22 11.80 8.60 2 5 -22 2.70 7.30 2 5 -22 13.30 9.60 -2 -5 22 26.80 10.60 -2 -5 22 -4.70 5.90 1 5 -22 39.00 7.50 1 5 -22 44.20 6.90 1 5 -22 26.00 11.20 -1 -5 22 44.90 11.50 -1 -5 22 17.10 9.60 0 5 -22 72.09 10.80 0 5 -22 67.69 13.50 0 5 -22 70.39 16.80 0 -5 22 77.99 16.10 0 -5 22 100.89 15.90 -1 5 -22 2.70 4.90 -1 5 -22 4.20 7.00 -1 5 -22 20.40 8.00 -1 5 -22 -5.80 4.90 -1 5 -22 21.50 10.20 1 -5 22 11.00 10.60 -2 5 -22 209.08 19.50 -2 5 -22 199.68 14.80 -2 5 -22 172.58 23.50 -2 5 -22 181.88 18.90 -2 5 -22 151.48 17.50 2 -5 22 189.68 20.10 2 -5 22 173.78 24.00 -3 5 -22 21.40 9.90 -3 5 -22 25.00 8.80 -3 5 -22 19.40 14.20 -3 5 -22 29.60 11.20 -3 5 -22 12.20 10.10 3 -5 22 10.90 11.60 3 -5 22 18.30 8.60 -4 5 -22 40.50 10.20 -4 5 -22 12.40 9.30 -4 5 -22 21.00 9.40 -4 5 -22 19.80 9.70 4 -5 22 12.40 11.60 4 -5 22 18.70 9.90 4 -5 22 10.20 9.30 -5 5 -22 9.50 9.10 -5 5 -22 11.20 10.10 -5 5 -22 19.30 9.50 5 -5 22 16.40 11.50 5 -5 22 13.20 9.10 5 -5 22 10.30 9.40 -6 5 -22 11.70 8.80 -6 5 -22 20.60 10.50 -6 5 -22 -0.60 6.30 -6 5 -22 11.10 10.30 6 -5 22 21.40 9.60 6 -5 22 10.00 10.60 6 -5 22 -0.30 10.20 -7 5 -22 -1.90 16.10 -7 5 -22 -0.10 7.70 -7 5 -22 14.00 10.90 -7 5 -22 21.30 10.00 7 -5 22 -3.50 11.60 7 -5 22 1.50 9.70 -8 5 -22 19.40 12.80 -8 5 -22 2.50 8.80 -8 5 -22 -0.30 9.00 -8 5 -22 -4.70 7.80 8 -5 22 -6.60 9.90 8 -5 22 13.20 11.90 8 -5 22 9.40 9.90 9 4 -22 3.40 9.30 -9 -4 22 5.00 6.10 -9 -4 22 10.90 9.50 -9 -4 22 2.60 8.20 8 4 -22 11.80 8.90 8 4 -22 15.20 8.50 -8 -4 22 -0.20 8.60 -8 -4 22 14.60 8.20 -8 -4 22 5.90 5.90 -8 -4 22 28.40 9.40 7 4 -22 50.19 10.10 7 4 -22 51.39 13.10 -7 -4 22 66.49 10.40 -7 -4 22 82.69 17.10 -7 -4 22 83.09 10.70 6 4 -22 5.70 7.40 6 4 -22 -7.10 7.00 -6 -4 22 4.30 5.20 -6 -4 22 18.30 8.80 5 4 -22 21.90 8.90 -5 -4 22 31.00 10.00 -5 -4 22 34.80 8.20 4 4 -22 4.30 7.70 4 4 -22 -5.20 6.60 -4 -4 22 7.70 8.30 -4 -4 22 8.20 5.50 3 4 -22 22.90 9.00 3 4 -22 54.99 12.30 -3 -4 22 61.29 13.50 -3 -4 22 47.90 9.80 2 4 -22 205.08 20.90 2 4 -22 204.68 20.90 -2 -4 22 239.68 20.60 -2 -4 22 252.17 22.70 1 4 -22 2.80 4.70 1 4 -22 8.50 4.90 1 4 -22 16.20 9.10 1 4 -22 30.70 10.80 -1 -4 22 5.20 7.40 -1 -4 22 15.20 9.10 0 4 -22 30.70 7.60 0 4 -22 25.60 8.00 0 4 -22 9.70 8.10 0 4 -22 32.60 11.20 0 -4 22 38.70 12.50 0 -4 22 32.20 10.60 -1 4 -22 -1.40 6.50 -1 4 -22 6.30 8.00 -1 4 -22 33.80 11.70 -1 4 -22 9.40 5.10 1 -4 22 10.40 10.20 -2 4 -22 50.69 12.80 -2 4 -22 42.80 11.60 -2 4 -22 35.60 10.20 -2 4 -22 52.99 12.00 -2 4 -22 45.60 8.60 2 -4 22 26.80 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17.70 9.40 -7 -3 22 17.80 6.90 -7 -3 22 21.10 9.50 6 3 -22 17.60 10.70 6 3 -22 7.70 7.40 -6 -3 22 3.20 5.30 -6 -3 22 16.10 8.40 5 3 -22 8.50 9.00 5 3 -22 28.20 10.10 -5 -3 22 16.00 7.60 -5 -3 22 23.60 9.30 4 3 -22 45.10 12.00 4 3 -22 47.40 11.60 -4 -3 22 53.19 10.30 -4 -3 22 80.89 13.60 3 3 -22 6.90 9.00 3 3 -22 4.20 8.00 -3 -3 22 5.10 8.20 -3 -3 22 5.30 5.80 2 3 -22 3.30 7.40 2 3 -22 2.40 9.10 -2 -3 22 6.80 8.60 -2 -3 22 19.00 8.30 1 3 -22 13.90 5.10 1 3 -22 14.70 9.50 1 3 -22 12.60 15.10 1 3 -22 24.30 5.60 -1 -3 22 17.40 8.80 -1 -3 22 8.80 7.80 0 3 -22 11.70 8.90 0 3 -22 -10.40 6.80 0 3 -22 12.90 6.40 0 3 -22 13.90 6.60 0 -3 22 -10.40 7.30 0 -3 22 8.30 8.80 -1 3 -22 5.90 8.10 -1 3 -22 8.40 4.80 -1 3 -22 2.40 8.00 -1 3 -22 2.90 7.70 -1 3 -22 22.10 9.50 1 -3 22 27.60 11.30 1 -3 22 6.40 7.80 -2 3 -22 36.20 13.20 -2 3 -22 56.99 12.60 -2 3 -22 55.79 9.00 2 -3 22 67.09 15.40 2 -3 22 80.49 15.80 2 -3 22 43.20 13.10 -3 3 -22 57.39 13.60 -3 3 -22 68.59 12.80 -3 3 -22 50.59 12.80 -3 3 -22 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6.80 8.10 3 -7 23 28.50 12.80 3 -7 23 24.10 12.00 -4 7 -23 17.90 10.80 -4 7 -23 2.30 9.30 -4 7 -23 9.00 7.50 -4 7 -23 9.40 8.20 4 -7 23 2.80 9.50 4 -7 23 16.70 10.50 -5 7 -23 10.80 9.20 -5 7 -23 5.50 8.10 -5 7 -23 8.50 7.60 -5 7 -23 5.90 8.70 5 -7 23 2.30 8.90 5 -7 23 -5.20 9.90 5 -7 23 -1.30 8.80 -6 7 -23 102.29 18.90 -6 7 -23 87.19 14.90 -6 7 -23 62.19 16.90 -6 7 -23 118.49 19.60 6 -7 23 95.09 20.80 6 -7 23 108.49 19.30 6 -7 23 77.19 18.40 -7 7 -23 6.90 10.80 -7 7 -23 29.10 13.10 -7 7 -23 26.10 9.60 7 -7 23 48.40 17.50 7 -7 23 23.80 13.00 7 -7 23 18.80 10.30 9 6 -23 13.20 10.40 -9 -6 23 12.10 8.80 -9 -6 23 6.00 9.50 8 6 -23 5.40 8.30 8 6 -23 7.10 8.90 -8 -6 23 24.00 7.00 -8 -6 23 5.20 9.50 7 6 -23 14.90 9.90 7 6 -23 5.90 7.10 -7 -6 23 -1.00 8.00 -7 -6 23 16.80 6.80 6 6 -23 32.30 10.30 6 6 -23 22.30 8.70 -6 -6 23 31.00 8.20 -6 -6 23 35.00 11.70 5 6 -23 59.69 14.00 5 6 -23 58.59 11.90 -5 -6 23 66.09 10.90 -5 -6 23 74.69 14.90 4 6 -23 60.79 12.50 4 6 -23 54.99 13.40 -4 -6 23 49.99 10.60 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-11 27 55.19 12.20 1 11 -27 -2.90 10.20 1 11 -27 9.60 9.40 -1 -11 27 0.80 12.10 -1 -11 27 24.00 9.40 0 11 -27 27.90 12.20 0 11 -27 32.50 11.60 0 -11 27 10.00 9.70 -1 11 -27 22.90 11.00 -1 11 -27 14.20 8.50 1 -11 27 -0.20 10.90 -2 11 -27 10.80 11.10 -2 11 -27 30.30 10.90 -2 11 -27 12.90 10.70 -2 11 -27 27.50 10.80 2 -11 27 46.10 13.20 2 -11 27 27.80 12.10 4 10 -27 29.00 12.60 4 10 -27 2.50 8.80 -4 -10 27 8.90 11.50 -4 -10 27 4.80 7.50 3 10 -27 13.80 11.80 3 10 -27 8.40 9.50 -3 -10 27 3.60 11.10 -3 -10 27 14.10 9.60 2 10 -27 6.50 9.70 2 10 -27 9.60 8.70 -2 -10 27 23.30 9.90 -2 -10 27 3.80 11.50 1 10 -27 -1.70 8.20 1 10 -27 -17.80 8.60 -1 -10 27 4.10 10.80 -1 -10 27 5.30 8.50 0 10 -27 4.80 10.20 0 10 -27 16.70 9.70 0 -10 27 25.10 12.60 0 -10 27 5.40 9.10 -1 10 -27 9.00 8.80 -1 10 -27 7.20 9.10 -1 10 -27 3.30 10.70 1 -10 27 15.80 9.80 -2 10 -27 -2.60 9.90 -2 10 -27 14.60 9.90 -2 10 -27 30.80 9.70 -2 10 -27 17.80 10.90 2 -10 27 32.00 11.60 2 -10 27 2.20 11.80 4 9 -27 18.40 11.30 4 9 -27 -7.80 8.30 -4 -9 27 27.70 9.60 -4 -9 27 21.00 10.30 3 9 -27 -11.20 8.90 3 9 -27 5.90 9.90 -3 -9 27 4.90 10.00 -3 -9 27 5.80 10.70 2 9 -27 32.60 11.50 2 9 -27 13.50 10.10 -2 -9 27 38.40 14.00 -2 -9 27 29.50 10.40 1 9 -27 3.30 8.90 1 9 -27 13.30 10.80 -1 -9 27 10.20 11.40 -1 -9 27 18.50 9.30 0 9 -27 2.50 9.90 0 9 -27 -1.60 7.50 0 9 -27 20.30 10.80 0 -9 27 -2.30 10.10 0 -9 27 34.70 11.20 -1 9 -27 6.10 8.30 -1 9 -27 3.80 11.10 1 -9 27 22.40 10.90 1 -9 27 30.70 14.70 -2 9 -27 8.10 10.00 -2 9 -27 22.00 10.70 -2 9 -27 15.60 8.80 -2 9 -27 11.00 12.70 2 -9 27 -7.80 11.00 2 -9 27 11.40 10.10 4 8 -27 12.50 10.90 4 8 -27 29.70 11.40 -4 -8 27 21.80 9.00 -4 -8 27 50.59 13.90 3 8 -27 26.70 11.70 3 8 -27 31.90 12.00 -3 -8 27 44.50 13.00 -3 -8 27 46.60 12.60 2 8 -27 6.00 10.30 2 8 -27 31.10 12.30 -2 -8 27 14.20 8.80 -2 -8 27 39.50 12.90 1 8 -27 24.80 19.10 1 8 -27 2.70 9.40 -1 -8 27 13.80 8.70 -1 -8 27 -15.50 9.60 0 8 -27 15.20 15.10 0 8 -27 7.80 10.30 0 8 -27 3.30 6.20 0 -8 27 10.70 11.60 0 -8 27 7.10 8.80 -1 8 -27 74.29 18.20 -1 8 -27 71.79 16.50 1 -8 27 64.29 15.20 1 -8 27 85.39 18.30 -2 8 -27 10.70 10.20 -2 8 -27 9.00 10.60 -2 8 -27 7.40 12.70 3 -8 27 101.09 19.60 4 7 -27 23.00 12.60 4 7 -27 4.70 10.00 -4 -7 27 26.50 9.60 -4 -7 27 -4.10 9.80 3 7 -27 38.90 13.00 3 7 -27 29.00 10.70 -3 -7 27 44.50 13.50 -3 -7 27 21.50 10.50 2 7 -27 24.00 12.60 2 7 -27 -2.80 9.30 -2 -7 27 28.90 12.50 -2 -7 27 5.00 8.80 1 7 -27 26.60 14.00 -1 -7 27 18.50 11.30 -1 -7 27 6.30 8.50 0 7 -27 3.20 10.20 0 7 -27 -9.60 6.60 0 -7 27 -1.30 9.00 0 -7 27 2.30 8.20 -1 7 -27 5.10 10.40 -1 7 -27 14.70 9.40 1 -7 27 17.70 10.60 1 -7 27 -11.30 11.20 -2 7 -27 11.40 10.90 -2 7 -27 7.40 12.50 -2 7 -27 -0.80 9.60 2 -7 27 38.90 22.00 3 -7 27 23.10 10.90 4 6 -27 30.60 11.00 4 6 -27 24.10 11.70 -4 -6 27 42.70 13.50 -4 -6 27 15.00 8.90 3 6 -27 27.30 12.00 3 6 -27 20.40 10.80 -3 -6 27 31.30 11.40 -3 -6 27 33.30 11.90 2 6 -27 0.80 9.60 2 6 -27 -6.90 9.80 -2 -6 27 -13.80 8.00 -2 -6 27 6.10 9.10 1 6 -27 22.80 12.30 -1 -6 27 22.50 9.60 -1 -6 27 20.50 11.60 0 6 -27 -10.80 6.50 0 6 -27 -8.80 9.50 0 -6 27 3.90 10.10 0 -6 27 23.10 9.00 -1 6 -27 11.00 9.20 -1 6 -27 -5.10 10.50 1 -6 27 -13.20 7.30 1 -6 27 -3.50 10.90 -2 6 -27 20.80 11.70 -2 6 -27 43.90 11.50 -2 6 -27 15.30 11.80 2 -6 27 11.70 17.80 2 -6 27 30.40 15.20 4 5 -27 22.30 10.00 4 5 -27 -9.10 10.30 -4 -5 27 27.90 11.10 -4 -5 27 18.80 8.60 3 5 -27 51.69 14.90 3 5 -27 52.39 14.20 -3 -5 27 70.09 14.30 -3 -5 27 64.99 14.70 2 5 -27 22.50 14.90 2 5 -27 50.69 15.50 -2 -5 27 40.00 12.60 -2 -5 27 69.69 13.20 1 5 -27 28.40 12.00 -1 -5 27 35.40 11.20 0 5 -27 -3.30 8.70 0 -5 27 -13.20 8.60 0 -5 27 0.40 7.30 -1 5 -27 5.70 9.00 1 -5 27 41.50 13.10 1 -5 27 9.40 11.10 1 -5 27 8.40 9.80 -2 5 -27 -3.10 13.40 -2 5 -27 15.40 9.20 -2 5 -27 -6.30 9.50 2 -5 27 5.50 8.40 2 -5 27 15.20 12.40 4 4 -27 21.60 10.90 4 4 -27 36.50 12.90 -4 -4 27 24.10 9.90 -4 -4 27 12.30 10.40 3 4 -27 -18.40 9.30 3 4 -27 7.00 11.20 -3 -4 27 7.30 10.90 -3 -4 27 19.40 9.80 2 4 -27 1.60 10.30 2 4 -27 9.50 10.60 -2 -4 27 19.90 11.10 -2 -4 27 16.20 9.20 1 4 -27 3.60 10.90 1 4 -27 1.90 12.80 -1 -4 27 6.50 8.30 -1 -4 27 10.30 8.30 -1 -4 27 -12.60 8.50 0 4 -27 10.10 15.90 0 4 -27 6.40 10.00 0 -4 27 0.50 9.60 0 -4 27 3.20 8.20 0 -4 27 12.10 9.40 -1 4 -27 15.40 17.40 -1 4 -27 33.20 10.30 -1 4 -27 30.70 20.80 1 -4 27 45.00 13.60 1 -4 27 28.50 13.70 1 -4 27 43.70 13.60 -2 4 -27 76.59 13.40 -2 4 -27 60.79 17.10 -2 4 -27 45.60 16.10 2 -4 27 73.89 18.60 2 -4 27 76.19 18.50 4 3 -27 16.90 10.20 4 3 -27 15.30 9.70 -4 -3 27 13.40 9.80 -4 -3 27 15.90 9.30 3 3 -27 12.60 10.80 3 3 -27 -6.10 7.40 -3 -3 27 -1.40 9.20 -3 -3 27 -3.80 7.90 -3 -3 27 13.30 7.80 2 3 -27 62.69 15.10 -2 -3 27 93.09 16.00 -2 -3 27 104.19 19.40 -2 -3 27 68.79 14.40 1 3 -27 62.09 16.40 1 3 -27 73.09 15.50 -1 -3 27 21.80 11.60 -1 -3 27 59.09 13.50 -1 -3 27 46.10 14.00 0 3 -27 24.50 13.30 0 3 -27 5.40 18.60 0 -3 27 71.09 15.30 0 -3 27 36.40 12.50 0 -3 27 40.90 13.00 -1 3 -27 22.00 10.20 -1 3 -27 31.00 13.20 -1 3 -27 36.30 13.20 1 -3 27 44.10 13.50 1 -3 27 62.79 18.40 1 -3 27 37.00 13.40 -2 3 -27 12.90 10.60 -2 3 -27 9.40 12.60 -2 3 -27 -10.70 9.50 2 -3 27 23.20 11.10 2 -3 27 -4.10 13.30 2 -3 27 20.80 10.80 3 2 -27 8.40 10.80 3 2 -27 1.10 7.80 -3 -2 27 -0.60 8.10 -3 -2 27 0.00 7.50 -3 -2 27 1.30 8.70 2 2 -27 25.80 11.50 2 2 -27 35.00 12.50 -2 -2 27 23.00 9.80 -2 -2 27 50.69 12.40 -2 -2 27 5.70 10.00 1 2 -27 44.90 18.70 1 2 -27 68.49 15.90 -1 -2 27 58.29 13.50 -1 -2 27 54.39 12.60 -1 -2 27 65.69 15.20 0 2 -27 39.30 17.70 0 2 -27 35.80 12.40 0 -2 27 36.30 11.90 0 -2 27 50.19 12.80 0 -2 27 67.69 15.60 -1 2 -27 -11.70 8.40 -1 2 -27 -0.40 8.80 -1 2 -27 -17.50 8.30 1 -2 27 19.10 13.00 1 -2 27 25.90 11.60 3 1 -27 8.00 9.30 3 1 -27 2.20 10.00 -3 -1 27 7.70 11.20 -3 -1 27 4.60 8.30 -3 -1 27 0.10 8.00 2 1 -27 45.70 22.20 2 1 -27 58.49 15.70 -2 -1 27 41.90 13.20 -2 -1 27 55.09 13.30 -2 -1 27 65.59 15.00 1 1 -27 10.60 9.20 -1 -1 27 8.30 8.70 -1 -1 27 -6.60 8.90 -1 -1 27 -1.80 9.40 0 1 -27 7.20 9.20 0 1 -27 6.40 9.90 0 -1 27 5.00 9.80 0 -1 27 -2.30 8.50 0 -1 27 -4.40 7.50 1 -1 27 84.49 18.10 1 0 -27 25.30 11.50 -1 0 27 2.00 11.20 -1 0 27 37.40 11.30 1 9 -28 -5.10 10.50 -1 -9 28 11.70 9.10 2 8 -28 27.20 12.40 -2 -8 28 3.40 7.90 1 8 -28 39.00 14.00 1 8 -28 5.10 10.10 -1 -8 28 36.40 15.90 -1 -8 28 35.80 10.30 2 7 -28 31.90 13.20 -2 -7 28 35.70 11.50 1 7 -28 1.20 10.00 1 7 -28 16.70 12.50 -1 -7 28 13.00 11.50 -1 -7 28 -5.30 6.80 0 7 -28 0.70 17.70 2 6 -28 3.00 11.90 -2 -6 28 4.50 9.30 1 6 -28 70.39 17.30 1 6 -28 37.70 12.20 -1 -6 28 76.99 15.70 -1 -6 28 54.39 12.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 26496 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si -0.01399(14) 0.80345(8) 0.14424(8) 0.0217(3) Uani 1 1 d . . . . . Si2 Si 0.87407(13) 0.45010(8) 0.10845(7) 0.0161(3) Uani 1 1 d . . . . . Si3 Si 0.97396(13) 0.30676(8) 0.61198(7) 0.0176(3) Uani 1 1 d . . . . . Si4 Si 1.39237(14) 0.00507(9) 0.13907(8) 0.0225(3) Uani 1 1 d . . . . . N1 N 0.4896(4) 0.7269(2) 0.2274(2) 0.0184(9) Uani 1 1 d . . . . . N2 N 0.5244(4) 0.8169(2) 0.3272(2) 0.0199(9) Uani 1 1 d . . . . . N3 N 0.3288(4) 0.8277(2) 0.2634(2) 0.0223(10) Uani 1 1 d . . . . . N4 N 0.2299(4) 0.7946(2) 0.2127(2) 0.0204(9) Uani 1 1 d . . . . . N5 N 0.3986(4) 0.4641(2) 0.2964(2) 0.0174(9) Uani 1 1 d . . . . . N6 N 0.3881(4) 0.3873(2) 0.1890(2) 0.0170(9) Uani 1 1 d . . . . . N7 N 0.5777(4) 0.4804(2) 0.2349(2) 0.0166(9) Uani 1 1 d . . . . . N8 N 0.6569(4) 0.4471(2) 0.1825(2) 0.0147(8) Uani 1 1 d . . . . . N9 N 0.5549(4) 0.2718(2) 0.3538(2) 0.0132(8) Uani 1 1 d . . . . . N10 N 0.7486(4) 0.3278(2) 0.3517(2) 0.0145(8) Uani 1 1 d . . . . . N11 N 0.6914(4) 0.2825(2) 0.4548(2) 0.0174(9) Uani 1 1 d . . . . . N12 N 0.8155(4) 0.2976(2) 0.4902(2) 0.0167(9) Uani 1 1 d . . . . . N13 N 0.9074(4) 0.1160(2) 0.2264(2) 0.0148(8) Uani 1 1 d . . . . . N14 N 0.9202(4) 0.0914(2) 0.3293(2) 0.0151(8) Uani 1 1 d . . . . . N15 N 1.1008(4) 0.0523(2) 0.2674(2) 0.0195(9) Uani 1 1 d . . . . . N16 N 1.1725(4) 0.0496(2) 0.2108(2) 0.0169(9) Uani 1 1 d . . . . . C1 C 0.4355(5) 0.7899(3) 0.2690(3) 0.0182(10) Uani 1 1 d . . . . . C2 C 0.6106(5) 0.7171(3) 0.2614(3) 0.0258(12) Uani 1 1 d . . . . . H2 H 0.668810 0.678092 0.244840 0.031 Uiso 1 1 calc R U . . . C3 C 0.6301(5) 0.7716(3) 0.3208(3) 0.0263(12) Uani 1 1 d . . . . . H3 H 0.705044 0.778213 0.353488 0.032 Uiso 1 1 calc R U . . . C4 C 0.5112(5) 0.8857(3) 0.3853(3) 0.0235(11) Uani 1 1 d . . . . . C5 C 0.3840(6) 0.8799(4) 0.4207(3) 0.0389(15) Uani 1 1 d . . . . . H5A H 0.377785 0.924784 0.459653 0.058 Uiso 1 1 calc R U . . . H5B H 0.384987 0.835597 0.438346 0.058 Uiso 1 1 calc R U . . . H5C H 0.307797 0.875418 0.386636 0.058 Uiso 1 1 calc R U . . . C6 C 0.6287(6) 0.8920(3) 0.4397(3) 0.0292(13) Uani 1 1 d . . . . . H6A H 0.622205 0.936983 0.478573 0.044 Uiso 1 1 calc R U . . . H6B H 0.711121 0.895381 0.417837 0.044 Uiso 1 1 calc R U . . . H6C H 0.627882 0.847721 0.457265 0.044 Uiso 1 1 calc R U . . . C7 C 0.5150(6) 0.9540(3) 0.3576(3) 0.0318(14) Uani 1 1 d . . . . . H7A H 0.505463 0.999147 0.395877 0.048 Uiso 1 1 calc R U . . . H7B H 0.442673 0.949385 0.321299 0.048 Uiso 1 1 calc R U . . . H7C H 0.599427 0.957662 0.337648 0.048 Uiso 1 1 calc R U . . . C8 C 0.4396(5) 0.6764(3) 0.1570(3) 0.0182(10) Uani 1 1 d . . . . . C9 C 0.5443(6) 0.6201(3) 0.1304(3) 0.0257(12) Uani 1 1 d . . . . . H9A H 0.510710 0.585247 0.085735 0.039 Uiso 1 1 calc R U . . . H9B H 0.565032 0.592181 0.164622 0.039 Uiso 1 1 calc R U . . . H9C H 0.624316 0.646911 0.123698 0.039 Uiso 1 1 calc R U . . . C10 C 0.3154(5) 0.6327(3) 0.1644(3) 0.0229(11) Uani 1 1 d . . . . . H10A H 0.283229 0.599621 0.118571 0.034 Uiso 1 1 calc R U . . . H10B H 0.247424 0.667714 0.182353 0.034 Uiso 1 1 calc R U . . . H10C H 0.335690 0.602678 0.196889 0.034 Uiso 1 1 calc R U . . . C11 C 0.4172(6) 0.7237(3) 0.1052(3) 0.0251(12) Uani 1 1 d . . . . . H11A H 0.384650 0.691149 0.059231 0.038 Uiso 1 1 calc R U . . . H11B H 0.500596 0.749167 0.101214 0.038 Uiso 1 1 calc R U . . . H11C H 0.352090 0.761080 0.122111 0.038 Uiso 1 1 calc R U . . . C12 C 0.1337(5) 0.8375(3) 0.2079(3) 0.0240(12) Uani 1 1 d . . . . . H12 H 0.137828 0.887347 0.237316 0.029 Uiso 1 1 calc R U . . . C13 C -0.0379(6) 0.6997(3) 0.1238(4) 0.0359(15) Uani 1 1 d . . . . . H13A H -0.113340 0.682631 0.089121 0.054 Uiso 1 1 calc R U . . . H13B H -0.054603 0.685925 0.166523 0.054 Uiso 1 1 calc R U . . . H13C H 0.041651 0.676056 0.104876 0.054 Uiso 1 1 calc R U . . . C14 C 0.0057(7) 0.8288(3) 0.0611(3) 0.0337(14) Uani 1 1 d . . . . . H14A H -0.073287 0.811470 0.029040 0.051 Uiso 1 1 calc R U . . . H14B H 0.082915 0.804863 0.039454 0.051 Uiso 1 1 calc R U . . . H14C H 0.017886 0.883208 0.071086 0.051 Uiso 1 1 calc R U . . . C15 C -0.1610(6) 0.8511(4) 0.1843(3) 0.0347(14) Uani 1 1 d . . . . . H15A H -0.239523 0.834755 0.151693 0.052 Uiso 1 1 calc R U . . . H15B H -0.146538 0.905419 0.194433 0.052 Uiso 1 1 calc R U . . . H15C H -0.173965 0.837997 0.227847 0.052 Uiso 1 1 calc R U . . . C16 C 0.4658(5) 0.4442(3) 0.2361(3) 0.0163(10) Uani 1 1 d . . . . . C17 C 0.2779(5) 0.3721(3) 0.2226(3) 0.0222(11) Uani 1 1 d . . . . . H17 H 0.209819 0.334911 0.202839 0.027 Uiso 1 1 calc R U . . . C18 C 0.2856(5) 0.4191(3) 0.2871(3) 0.0209(11) Uani 1 1 d . . . . . H18 H 0.223499 0.421088 0.320882 0.025 Uiso 1 1 calc R U . . . C19 C 0.4440(5) 0.5235(3) 0.3627(3) 0.0223(11) Uani 1 1 d . . . . . C20 C 0.3409(6) 0.5274(3) 0.4160(3) 0.0288(13) Uani 1 1 d . . . . . H20A H 0.366906 0.567817 0.458400 0.043 Uiso 1 1 calc R U . . . H20B H 0.335178 0.479682 0.427917 0.043 Uiso 1 1 calc R U . . . H20C H 0.254805 0.537116 0.395848 0.043 Uiso 1 1 calc R U . . . C21 C 0.4548(5) 0.5997(3) 0.3478(3) 0.0237(11) Uani 1 1 d . . . . . H21A H 0.485554 0.637972 0.390931 0.036 Uiso 1 1 calc R U . . . H21B H 0.368097 0.612103 0.330570 0.036 Uiso 1 1 calc R U . . . H21C H 0.517610 0.597812 0.312419 0.036 Uiso 1 1 calc R U . . . C22 C 0.5759(6) 0.5032(3) 0.3925(3) 0.0271(12) Uani 1 1 d . . . . . H22A H 0.602763 0.540293 0.437053 0.041 Uiso 1 1 calc R U . . . H22B H 0.642867 0.502899 0.359442 0.041 Uiso 1 1 calc R U . . . H22C H 0.566886 0.453544 0.400127 0.041 Uiso 1 1 calc R U . . . C23 C 0.4020(5) 0.3513(3) 0.1124(3) 0.0184(10) Uani 1 1 d . . . . . C24 C 0.2730(5) 0.3070(3) 0.0795(3) 0.0292(13) Uani 1 1 d . . . . . H24A H 0.277496 0.287796 0.028893 0.044 Uiso 1 1 calc R U . . . H24B H 0.198700 0.339883 0.089109 0.044 Uiso 1 1 calc R U . . . H24C H 0.260410 0.265010 0.099654 0.044 Uiso 1 1 calc R U . . . C25 C 0.5127(5) 0.2972(3) 0.1037(3) 0.0190(10) Uani 1 1 d . . . . . H25A H 0.516884 0.271694 0.053989 0.028 Uiso 1 1 calc R U . . . H25B H 0.496238 0.260144 0.129212 0.028 Uiso 1 1 calc R U . . . H25C H 0.596677 0.324831 0.122327 0.028 Uiso 1 1 calc R U . . . C26 C 0.4211(5) 0.4128(3) 0.0758(3) 0.0213(11) Uani 1 1 d . . . . . H26A H 0.417805 0.390261 0.025177 0.032 Uiso 1 1 calc R U . . . H26B H 0.506863 0.439159 0.092259 0.032 Uiso 1 1 calc R U . . . H26C H 0.350811 0.448296 0.086606 0.032 Uiso 1 1 calc R U . . . C27 C 0.7618(5) 0.4853(3) 0.1790(3) 0.0177(10) Uani 1 1 d . . . . . H27 H 0.782382 0.532004 0.212730 0.021 Uiso 1 1 calc R U . . . C28 C 0.8730(6) 0.3458(3) 0.0815(3) 0.0285(13) Uani 1 1 d . . . . . H28A H 0.932386 0.329037 0.044233 0.043 Uiso 1 1 calc R U . . . H28B H 0.783273 0.325593 0.064268 0.043 Uiso 1 1 calc R U . . . H28C H 0.902637 0.328049 0.121689 0.043 Uiso 1 1 calc R U . . . C29 C 0.8154(6) 0.4836(3) 0.0318(3) 0.0278(12) Uani 1 1 d . . . . . H29A H 0.867298 0.461719 -0.007736 0.042 Uiso 1 1 calc R U . . . H29B H 0.825951 0.538308 0.044172 0.042 Uiso 1 1 calc R U . . . H29C H 0.722093 0.468388 0.018749 0.042 Uiso 1 1 calc R U . . . C30 C 1.0457(5) 0.4888(3) 0.1392(3) 0.0213(11) Uani 1 1 d . . . . . H30A H 1.103155 0.472712 0.100884 0.032 Uiso 1 1 calc R U . . . H30B H 1.078092 0.470304 0.178551 0.032 Uiso 1 1 calc R U . . . H30C H 1.045978 0.543549 0.154145 0.032 Uiso 1 1 calc R U . . . C31 C 0.6753(4) 0.2946(3) 0.3925(2) 0.0137(9) Uani 1 1 d . . . . . C32 C 0.6717(5) 0.3234(3) 0.2895(3) 0.0173(10) Uani 1 1 d . . . . . H32 H 0.698406 0.341171 0.251964 0.021 Uiso 1 1 calc R U . . . C33 C 0.5554(5) 0.2905(3) 0.2916(2) 0.0152(10) Uani 1 1 d . . . . . H33 H 0.484570 0.281314 0.256207 0.018 Uiso 1 1 calc R U . . . C34 C 0.4404(4) 0.2357(3) 0.3783(2) 0.0130(9) Uani 1 1 d . . . . . C35 C 0.4788(5) 0.1600(3) 0.3888(3) 0.0208(11) Uani 1 1 d . . . . . H35A H 0.401889 0.135164 0.401263 0.031 Uiso 1 1 calc R U . . . H35B H 0.549488 0.167983 0.426420 0.031 Uiso 1 1 calc R U . . . H35C H 0.509504 0.128492 0.345378 0.031 Uiso 1 1 calc R U . . . C36 C 0.3928(5) 0.2883(3) 0.4439(3) 0.0260(12) Uani 1 1 d . . . . . H36A H 0.314527 0.265526 0.457276 0.039 Uiso 1 1 calc R U . . . H36B H 0.370503 0.335886 0.434727 0.039 Uiso 1 1 calc R U . . . H36C H 0.462749 0.297407 0.482048 0.039 Uiso 1 1 calc R U . . . C37 C 0.3266(5) 0.2200(3) 0.3200(3) 0.0201(11) Uani 1 1 d . . . . . H37A H 0.251824 0.194927 0.334134 0.030 Uiso 1 1 calc R U . . . H37B H 0.356627 0.187643 0.276749 0.030 Uiso 1 1 calc R U . . . H37C H 0.299093 0.267291 0.312001 0.030 Uiso 1 1 calc R U . . . C38 C 0.8857(5) 0.3634(3) 0.3670(3) 0.0166(10) Uani 1 1 d . . . . . C39 C 0.9865(5) 0.3039(3) 0.3688(3) 0.0235(11) Uani 1 1 d . . . . . H39A H 1.075765 0.327066 0.376225 0.035 Uiso 1 1 calc R U . . . H39B H 0.977455 0.264585 0.324325 0.035 Uiso 1 1 calc R U . . . H39C H 0.970642 0.281917 0.407094 0.035 Uiso 1 1 calc R U . . . C40 C 0.9154(5) 0.3975(3) 0.3082(3) 0.0278(13) Uani 1 1 d . . . . . H40A H 1.000861 0.425211 0.319647 0.042 Uiso 1 1 calc R U . . . H40B H 0.846270 0.431589 0.302442 0.042 Uiso 1 1 calc R U . . . H40C H 0.918167 0.357515 0.264549 0.042 Uiso 1 1 calc R U . . . C41 C 0.8937(5) 0.4269(3) 0.4349(3) 0.0234(11) Uani 1 1 d . . . . . H41A H 0.983440 0.449615 0.444622 0.035 Uiso 1 1 calc R U . . . H41B H 0.871494 0.406936 0.473570 0.035 Uiso 1 1 calc R U . . . H41C H 0.831381 0.464908 0.430159 0.035 Uiso 1 1 calc R U . . . C42 C 0.8202(5) 0.2911(3) 0.5526(3) 0.0165(10) Uani 1 1 d . . . . . H42 H 0.740879 0.277636 0.569486 0.020 Uiso 1 1 calc R U . . . C43 C 1.1160(6) 0.3315(4) 0.5678(3) 0.0365(15) Uani 1 1 d . . . . . H43A H 1.195109 0.341747 0.600557 0.055 Uiso 1 1 calc R U . . . H43B H 1.097067 0.376113 0.552324 0.055 Uiso 1 1 calc R U . . . H43C H 1.130912 0.289720 0.527247 0.055 Uiso 1 1 calc R U . . . C44 C 1.0023(6) 0.2191(4) 0.6378(4) 0.0418(16) Uani 1 1 d . . . . . H44A H 1.071869 0.228718 0.676145 0.063 Uiso 1 1 calc R U . . . H44B H 1.029310 0.180353 0.597681 0.063 Uiso 1 1 calc R U . . . H44C H 0.920663 0.202114 0.653172 0.063 Uiso 1 1 calc R U . . . C45 C 0.9508(6) 0.3826(4) 0.6919(3) 0.0433(17) Uani 1 1 d . . . . . H45A H 1.029122 0.388406 0.724798 0.065 Uiso 1 1 calc R U . . . H45B H 0.873332 0.370053 0.713673 0.065 Uiso 1 1 calc R U . . . H45C H 0.937763 0.429596 0.679521 0.065 Uiso 1 1 calc R U . . . C46 C 0.9867(5) 0.0845(3) 0.2701(3) 0.0161(10) Uani 1 1 d . . . . . C47 C 0.8026(5) 0.1255(3) 0.3220(3) 0.0180(10) Uani 1 1 d . . . . . H47 H 0.738706 0.136478 0.355455 0.022 Uiso 1 1 calc R U . . . C48 C 0.7942(5) 0.1404(3) 0.2603(3) 0.0216(11) Uani 1 1 d . . . . . H48 H 0.723151 0.163697 0.242270 0.026 Uiso 1 1 calc R U . . . C49 C 0.9306(5) 0.1233(3) 0.1549(3) 0.0174(10) Uani 1 1 d . . . . . C50 C 1.0492(5) 0.1766(3) 0.1598(3) 0.0232(11) Uani 1 1 d . . . . . H50A H 1.064400 0.180841 0.113048 0.035 Uiso 1 1 calc R U . . . H50B H 1.127383 0.157190 0.179267 0.035 Uiso 1 1 calc R U . . . H50C H 1.032164 0.226008 0.190237 0.035 Uiso 1 1 calc R U . . . C51 C 0.9432(5) 0.0468(3) 0.1043(3) 0.0236(11) Uani 1 1 d . . . . . H51A H 0.960922 0.052633 0.058323 0.035 Uiso 1 1 calc R U . . . H51B H 0.860932 0.016865 0.100058 0.035 Uiso 1 1 calc R U . . . H51C H 1.016054 0.021513 0.121648 0.035 Uiso 1 1 calc R U . . . C52 C 0.8100(5) 0.1595(3) 0.1282(3) 0.0242(12) Uani 1 1 d . . . . . H52A H 0.821668 0.162618 0.080669 0.036 Uiso 1 1 calc R U . . . H52B H 0.801969 0.209903 0.159097 0.036 Uiso 1 1 calc R U . . . H52C H 0.729968 0.128940 0.127713 0.036 Uiso 1 1 calc R U . . . C53 C 0.9631(5) 0.0650(3) 0.3914(3) 0.0176(10) Uani 1 1 d . . . . . C54 C 0.9737(6) -0.0200(3) 0.3684(3) 0.0282(13) Uani 1 1 d . . . . . H54A H 1.001060 -0.037605 0.409071 0.042 Uiso 1 1 calc R U . . . H54B H 1.039083 -0.033168 0.333780 0.042 Uiso 1 1 calc R U . . . H54C H 0.887754 -0.043662 0.347657 0.042 Uiso 1 1 calc R U . . . C55 C 1.0947(5) 0.1044(4) 0.4248(3) 0.0297(13) Uani 1 1 d . . . . . H55A H 1.120901 0.088771 0.466683 0.045 Uiso 1 1 calc R U . . . H55B H 1.085413 0.158721 0.437717 0.045 Uiso 1 1 calc R U . . . H55C H 1.162099 0.091055 0.391323 0.045 Uiso 1 1 calc R U . . . C56 C 0.8592(5) 0.0844(3) 0.4445(3) 0.0248(12) Uani 1 1 d . . . . . H56A H 0.884884 0.065710 0.484728 0.037 Uiso 1 1 calc R U . . . H56B H 0.773694 0.060963 0.422591 0.037 Uiso 1 1 calc R U . . . H56C H 0.852310 0.138790 0.460137 0.037 Uiso 1 1 calc R U . . . C57 C 1.2812(5) 0.0157(3) 0.2109(3) 0.0230(11) Uani 1 1 d . . . . . H57 H 1.305330 -0.004394 0.248705 0.028 Uiso 1 1 calc R U . . . C58 C 1.5531(6) -0.0272(4) 0.1674(4) 0.0424(17) Uani 1 1 d . . . . . H58A H 1.613062 -0.032690 0.130106 0.064 Uiso 1 1 calc R U . . . H58B H 1.539264 -0.075586 0.177140 0.064 Uiso 1 1 calc R U . . . H58C H 1.591751 0.009557 0.209727 0.064 Uiso 1 1 calc R U . . . C59 C 1.3217(8) -0.0661(5) 0.0593(4) 0.059(2) Uani 1 1 d . . . . . H59A H 1.379013 -0.068913 0.021255 0.088 Uiso 1 1 calc R U . . . H59B H 1.233770 -0.051930 0.045652 0.088 Uiso 1 1 calc R U . . . H59C H 1.315099 -0.114953 0.068812 0.088 Uiso 1 1 calc R U . . . C60 C 1.4167(8) 0.0968(4) 0.1204(5) 0.054(2) Uani 1 1 d . . . . . H60A H 1.461199 0.089756 0.077218 0.081 Uiso 1 1 calc R U . . . H60B H 1.470910 0.130918 0.159244 0.081 Uiso 1 1 calc R U . . . H60C H 1.330836 0.118179 0.114880 0.081 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0182(7) 0.0212(7) 0.0257(8) 0.0070(6) -0.0023(6) 0.0011(6) Si2 0.0149(7) 0.0182(7) 0.0152(7) 0.0043(5) 0.0033(5) 0.0004(5) Si3 0.0158(7) 0.0217(7) 0.0145(7) 0.0038(6) 0.0002(5) 0.0023(5) Si4 0.0160(7) 0.0254(8) 0.0261(8) 0.0059(6) 0.0064(6) 0.0026(6) N1 0.017(2) 0.018(2) 0.019(2) 0.0038(18) -0.0027(17) 0.0002(17) N2 0.020(2) 0.020(2) 0.018(2) 0.0036(18) -0.0027(17) -0.0008(18) N3 0.017(2) 0.023(2) 0.022(2) -0.0004(19) -0.0055(18) 0.0064(18) N4 0.018(2) 0.022(2) 0.019(2) 0.0027(18) -0.0004(17) 0.0009(18) N5 0.014(2) 0.023(2) 0.017(2) 0.0050(18) 0.0054(16) 0.0066(17) N6 0.015(2) 0.020(2) 0.017(2) 0.0066(17) 0.0021(16) 0.0002(17) N7 0.015(2) 0.020(2) 0.014(2) 0.0034(17) 0.0041(16) 0.0014(17) N8 0.016(2) 0.017(2) 0.0119(19) 0.0041(16) 0.0040(16) 0.0039(16) N9 0.0094(19) 0.014(2) 0.016(2) 0.0046(16) -0.0024(15) -0.0020(15) N10 0.0112(19) 0.016(2) 0.017(2) 0.0066(17) 0.0000(16) -0.0001(16) N11 0.016(2) 0.020(2) 0.015(2) 0.0041(17) -0.0020(16) -0.0016(17) N12 0.016(2) 0.015(2) 0.018(2) 0.0032(17) 0.0000(16) 0.0007(16) N13 0.016(2) 0.016(2) 0.014(2) 0.0054(16) 0.0031(16) 0.0054(16) N14 0.015(2) 0.015(2) 0.016(2) 0.0046(17) 0.0033(16) 0.0007(16) N15 0.018(2) 0.025(2) 0.017(2) 0.0087(18) 0.0050(17) 0.0044(18) N16 0.015(2) 0.017(2) 0.018(2) 0.0026(17) 0.0054(16) 0.0016(17) C1 0.016(2) 0.020(3) 0.017(2) 0.005(2) -0.0014(19) -0.003(2) C2 0.020(3) 0.023(3) 0.033(3) 0.005(2) -0.001(2) 0.004(2) C3 0.020(3) 0.030(3) 0.027(3) 0.009(2) -0.008(2) -0.002(2) C4 0.027(3) 0.023(3) 0.018(3) 0.001(2) -0.003(2) -0.004(2) C5 0.037(4) 0.042(4) 0.028(3) -0.005(3) 0.006(3) -0.008(3) C6 0.034(3) 0.031(3) 0.021(3) 0.007(2) -0.007(2) -0.006(3) C7 0.038(3) 0.022(3) 0.031(3) 0.004(2) -0.013(3) -0.001(2) C8 0.025(3) 0.017(2) 0.013(2) 0.006(2) 0.000(2) 0.000(2) C9 0.030(3) 0.028(3) 0.018(3) 0.005(2) 0.006(2) 0.005(2) C10 0.024(3) 0.023(3) 0.018(3) 0.003(2) -0.002(2) -0.003(2) C11 0.031(3) 0.025(3) 0.023(3) 0.011(2) 0.003(2) 0.003(2) C12 0.022(3) 0.025(3) 0.022(3) 0.003(2) 0.000(2) 0.008(2) C13 0.032(3) 0.026(3) 0.050(4) 0.013(3) -0.009(3) -0.007(3) C14 0.046(4) 0.030(3) 0.024(3) 0.007(3) 0.001(3) -0.004(3) C15 0.021(3) 0.042(4) 0.039(4) 0.008(3) -0.001(3) 0.008(3) C16 0.018(2) 0.017(2) 0.016(2) 0.007(2) 0.0067(19) 0.007(2) C17 0.014(2) 0.028(3) 0.029(3) 0.016(2) 0.001(2) -0.002(2) C18 0.012(2) 0.027(3) 0.028(3) 0.013(2) 0.008(2) 0.007(2) C19 0.023(3) 0.027(3) 0.017(3) 0.006(2) 0.003(2) 0.008(2) C20 0.034(3) 0.035(3) 0.023(3) 0.012(2) 0.014(2) 0.015(3) C21 0.028(3) 0.020(3) 0.023(3) 0.006(2) 0.006(2) 0.007(2) C22 0.029(3) 0.031(3) 0.020(3) 0.004(2) 0.003(2) 0.009(2) C23 0.019(3) 0.019(3) 0.016(2) 0.004(2) 0.000(2) -0.003(2) C24 0.023(3) 0.033(3) 0.027(3) 0.004(3) -0.004(2) -0.006(2) C25 0.020(3) 0.020(3) 0.015(2) 0.002(2) 0.001(2) -0.003(2) C26 0.027(3) 0.022(3) 0.016(2) 0.008(2) -0.001(2) -0.001(2) C27 0.017(2) 0.016(2) 0.020(3) 0.004(2) 0.001(2) 0.0034(19) C28 0.032(3) 0.020(3) 0.032(3) 0.002(2) 0.012(2) 0.003(2) C29 0.027(3) 0.031(3) 0.024(3) 0.007(2) 0.002(2) 0.001(2) C30 0.017(3) 0.026(3) 0.020(3) 0.004(2) 0.003(2) 0.000(2) C31 0.011(2) 0.013(2) 0.015(2) 0.0014(19) 0.0034(18) 0.0022(18) C32 0.021(3) 0.018(2) 0.013(2) 0.0038(19) -0.0016(19) 0.004(2) C33 0.017(2) 0.014(2) 0.013(2) 0.0032(19) -0.0022(19) 0.0037(19) C34 0.010(2) 0.013(2) 0.018(2) 0.0058(19) 0.0032(18) 0.0009(18) C35 0.018(3) 0.019(3) 0.028(3) 0.011(2) 0.002(2) -0.001(2) C36 0.020(3) 0.032(3) 0.024(3) 0.004(2) 0.007(2) 0.001(2) C37 0.016(2) 0.023(3) 0.021(3) 0.008(2) -0.005(2) -0.003(2) C38 0.011(2) 0.017(2) 0.022(3) 0.005(2) 0.0016(19) 0.0002(19) C39 0.015(2) 0.031(3) 0.024(3) 0.007(2) 0.003(2) 0.007(2) C40 0.015(3) 0.042(3) 0.032(3) 0.020(3) -0.001(2) -0.006(2) C41 0.015(2) 0.023(3) 0.029(3) 0.004(2) -0.003(2) 0.002(2) C42 0.016(2) 0.018(2) 0.016(2) 0.005(2) 0.0011(19) 0.0020(19) C43 0.023(3) 0.057(4) 0.033(3) 0.018(3) -0.001(2) -0.006(3) C44 0.032(3) 0.049(4) 0.052(4) 0.031(3) -0.011(3) 0.000(3) C45 0.034(3) 0.053(4) 0.028(3) -0.012(3) -0.011(3) 0.004(3) C46 0.021(3) 0.012(2) 0.015(2) 0.0036(19) 0.0004(19) -0.0029(19) C47 0.015(2) 0.018(2) 0.022(3) 0.005(2) 0.003(2) 0.0030(19) C48 0.016(2) 0.027(3) 0.025(3) 0.011(2) 0.006(2) 0.008(2) C49 0.021(3) 0.020(3) 0.013(2) 0.007(2) 0.0015(19) 0.002(2) C50 0.027(3) 0.022(3) 0.025(3) 0.013(2) 0.006(2) 0.000(2) C51 0.028(3) 0.024(3) 0.017(3) 0.003(2) 0.004(2) 0.002(2) C52 0.028(3) 0.028(3) 0.019(3) 0.011(2) 0.002(2) 0.006(2) C53 0.022(3) 0.019(3) 0.014(2) 0.009(2) -0.001(2) 0.001(2) C54 0.042(3) 0.024(3) 0.023(3) 0.011(2) 0.012(3) 0.011(3) C55 0.025(3) 0.044(4) 0.022(3) 0.014(3) -0.006(2) -0.011(3) C56 0.028(3) 0.034(3) 0.015(3) 0.009(2) 0.002(2) 0.001(2) C57 0.021(3) 0.026(3) 0.025(3) 0.011(2) 0.002(2) 0.005(2) C58 0.022(3) 0.060(5) 0.046(4) 0.013(3) 0.008(3) 0.014(3) C59 0.048(4) 0.085(6) 0.029(4) -0.004(4) -0.001(3) -0.021(4) C60 0.051(4) 0.052(5) 0.077(6) 0.037(4) 0.037(4) 0.020(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C13 Si1 C14 108.6(3) . . ? C13 Si1 C15 110.9(3) . . ? C14 Si1 C15 108.1(3) . . ? C13 Si1 C12 110.5(3) . . ? C14 Si1 C12 110.9(3) . . ? C15 Si1 C12 107.9(3) . . ? C27 Si2 C28 111.4(2) . . ? C27 Si2 C30 109.8(2) . . ? C28 Si2 C30 109.5(3) . . ? C27 Si2 C29 107.8(2) . . ? C28 Si2 C29 109.3(3) . . ? C30 Si2 C29 109.0(2) . . ? C45 Si3 C43 110.1(3) . . ? C45 Si3 C42 109.3(3) . . ? C43 Si3 C42 110.7(3) . . ? C45 Si3 C44 108.2(3) . . ? C43 Si3 C44 110.8(3) . . ? C42 Si3 C44 107.7(3) . . ? C59 Si4 C60 110.2(4) . . ? C59 Si4 C58 108.3(4) . . ? C60 Si4 C58 110.1(3) . . ? C59 Si4 C57 110.6(3) . . ? C60 Si4 C57 109.2(3) . . ? C58 Si4 C57 108.6(3) . . ? C1 N1 C2 107.6(4) . . ? C1 N1 C8 130.0(4) . . ? C2 N1 C8 122.4(4) . . ? C3 N2 C1 108.7(4) . . ? C3 N2 C4 125.3(4) . . ? C1 N2 C4 125.9(4) . . ? C1 N3 N4 118.3(4) . . ? C12 N4 N3 113.9(4) . . ? C18 N5 C16 109.4(4) . . ? C18 N5 C19 124.9(4) . . ? C16 N5 C19 125.7(4) . . ? C16 N6 C17 108.0(4) . . ? C16 N6 C23 129.3(4) . . ? C17 N6 C23 122.3(4) . . ? C16 N7 N8 116.2(4) . . ? C27 N8 N7 115.7(4) . . ? C33 N9 C31 109.4(4) . . ? C33 N9 C34 125.7(4) . . ? C31 N9 C34 124.8(4) . . ? C31 N10 C32 107.9(4) . . ? C31 N10 C38 129.4(4) . . ? C32 N10 C38 122.6(4) . . ? C31 N11 N12 117.9(4) . . ? C42 N12 N11 114.1(4) . . ? C46 N13 C48 107.8(4) . . ? C46 N13 C49 129.1(4) . . ? C48 N13 C49 123.1(4) . . ? C46 N14 C47 109.2(4) . . ? C46 N14 C53 126.7(4) . . ? C47 N14 C53 124.0(4) . . ? C46 N15 N16 118.3(4) . . ? C57 N16 N15 114.8(4) . . ? N3 C1 N1 135.3(5) . . ? N3 C1 N2 118.4(5) . . ? N1 C1 N2 106.2(4) . . ? C3 C2 N1 108.5(5) . . ? C3 C2 H2 125.8 . . ? N1 C2 H2 125.8 . . ? C2 C3 N2 109.0(5) . . ? C2 C3 H3 125.5 . . ? N2 C3 H3 125.5 . . ? N2 C4 C7 109.7(4) . . ? N2 C4 C5 110.3(4) . . ? C7 C4 C5 111.5(5) . . ? N2 C4 C6 107.9(4) . . ? C7 C4 C6 108.9(4) . . ? C5 C4 C6 108.3(5) . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C4 C6 H6A 109.5 . . ? C4 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C4 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C4 C7 H7A 109.5 . . ? C4 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C4 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? N1 C8 C10 109.5(4) . . ? N1 C8 C9 108.9(4) . . ? C10 C8 C9 108.0(4) . . ? N1 C8 C11 109.1(4) . . ? C10 C8 C11 112.9(4) . . ? C9 C8 C11 108.3(4) . . ? C8 C9 H9A 109.5 . . ? C8 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C8 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C8 C10 H10A 109.5 . . ? C8 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C8 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C8 C11 H11A 109.5 . . ? C8 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C8 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N4 C12 Si1 121.4(4) . . ? N4 C12 H12 119.3 . . ? Si1 C12 H12 119.3 . . ? Si1 C13 H13A 109.5 . . ? Si1 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? Si1 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? Si1 C14 H14A 109.5 . . ? Si1 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? Si1 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? Si1 C15 H15A 109.5 . . ? Si1 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? Si1 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? N7 C16 N5 118.6(4) . . ? N7 C16 N6 135.7(4) . . ? N5 C16 N6 105.7(4) . . ? C18 C17 N6 108.2(5) . . ? C18 C17 H17 125.9 . . ? N6 C17 H17 125.9 . . ? C17 C18 N5 108.6(4) . . ? C17 C18 H18 125.7 . . ? N5 C18 H18 125.7 . . ? N5 C19 C22 109.6(4) . . ? N5 C19 C21 109.7(4) . . ? C22 C19 C21 111.2(5) . . ? N5 C19 C20 108.8(4) . . ? C22 C19 C20 109.3(4) . . ? C21 C19 C20 108.1(4) . . ? C19 C20 H20A 109.5 . . ? C19 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C19 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C19 C21 H21A 109.5 . . ? C19 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C19 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C19 C22 H22A 109.5 . . ? C19 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C19 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? N6 C23 C25 110.2(4) . . ? N6 C23 C26 109.0(4) . . ? C25 C23 C26 113.3(4) . . ? N6 C23 C24 108.9(4) . . ? C25 C23 C24 108.2(4) . . ? C26 C23 C24 107.2(4) . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C23 C25 H25A 109.5 . . ? C23 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? C23 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C23 C26 H26A 109.5 . . ? C23 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C23 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? N8 C27 Si2 120.8(4) . . ? N8 C27 H27 119.6 . . ? Si2 C27 H27 119.6 . . ? Si2 C28 H28A 109.5 . . ? Si2 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? Si2 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? Si2 C29 H29A 109.5 . . ? Si2 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? Si2 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? Si2 C30 H30A 109.5 . . ? Si2 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? Si2 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? N11 C31 N9 117.7(4) . . ? N11 C31 N10 136.8(4) . . ? N9 C31 N10 105.5(4) . . ? C33 C32 N10 108.8(4) . . ? C33 C32 H32 125.6 . . ? N10 C32 H32 125.6 . . ? C32 C33 N9 108.4(4) . . ? C32 C33 H33 125.8 . . ? N9 C33 H33 125.8 . . ? N9 C34 C36 110.5(4) . . ? N9 C34 C35 109.9(4) . . ? C36 C34 C35 112.6(4) . . ? N9 C34 C37 108.0(4) . . ? C36 C34 C37 108.4(4) . . ? C35 C34 C37 107.2(4) . . ? C34 C35 H35A 109.5 . . ? C34 C35 H35B 109.5 . . ? H35A C35 H35B 109.5 . . ? C34 C35 H35C 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C34 C36 H36A 109.5 . . ? C34 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C34 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C34 C37 H37A 109.5 . . ? C34 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C34 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? N10 C38 C40 108.5(4) . . ? N10 C38 C41 110.0(4) . . ? C40 C38 C41 107.6(4) . . ? N10 C38 C39 110.0(4) . . ? C40 C38 C39 107.9(4) . . ? C41 C38 C39 112.6(4) . . ? C38 C39 H39A 109.5 . . ? C38 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C38 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C38 C40 H40A 109.5 . . ? C38 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C38 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? C38 C41 H41A 109.5 . . ? C38 C41 H41B 109.5 . . ? H41A C41 H41B 109.5 . . ? C38 C41 H41C 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? N12 C42 Si3 123.5(4) . . ? N12 C42 H42 118.2 . . ? Si3 C42 H42 118.2 . . ? Si3 C43 H43A 109.5 . . ? Si3 C43 H43B 109.5 . . ? H43A C43 H43B 109.5 . . ? Si3 C43 H43C 109.5 . . ? H43A C43 H43C 109.5 . . ? H43B C43 H43C 109.5 . . ? Si3 C44 H44A 109.5 . . ? Si3 C44 H44B 109.5 . . ? H44A C44 H44B 109.5 . . ? Si3 C44 H44C 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? Si3 C45 H45A 109.5 . . ? Si3 C45 H45B 109.5 . . ? H45A C45 H45B 109.5 . . ? Si3 C45 H45C 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? N15 C46 N14 117.6(4) . . ? N15 C46 N13 136.5(5) . . ? N14 C46 N13 105.9(4) . . ? C48 C47 N14 108.5(4) . . ? C48 C47 H47 125.7 . . ? N14 C47 H47 125.7 . . ? C47 C48 N13 108.6(4) . . ? C47 C48 H48 125.7 . . ? N13 C48 H48 125.7 . . ? N13 C49 C51 110.5(4) . . ? N13 C49 C50 109.8(4) . . ? C51 C49 C50 113.3(4) . . ? N13 C49 C52 108.4(4) . . ? C51 C49 C52 108.0(4) . . ? C50 C49 C52 106.7(4) . . ? C49 C50 H50A 109.5 . . ? C49 C50 H50B 109.5 . . ? H50A C50 H50B 109.5 . . ? C49 C50 H50C 109.5 . . ? H50A C50 H50C 109.5 . . ? H50B C50 H50C 109.5 . . ? C49 C51 H51A 109.5 . . ? C49 C51 H51B 109.5 . . ? H51A C51 H51B 109.5 . . ? C49 C51 H51C 109.5 . . ? H51A C51 H51C 109.5 . . ? H51B C51 H51C 109.5 . . ? C49 C52 H52A 109.5 . . ? C49 C52 H52B 109.5 . . ? H52A C52 H52B 109.5 . . ? C49 C52 H52C 109.5 . . ? H52A C52 H52C 109.5 . . ? H52B C52 H52C 109.5 . . ? N14 C53 C55 109.5(4) . . ? N14 C53 C56 108.8(4) . . ? C55 C53 C56 109.3(4) . . ? N14 C53 C54 109.2(4) . . ? C55 C53 C54 111.4(5) . . ? C56 C53 C54 108.7(4) . . ? C53 C54 H54A 109.5 . . ? C53 C54 H54B 109.5 . . ? H54A C54 H54B 109.5 . . ? C53 C54 H54C 109.5 . . ? H54A C54 H54C 109.5 . . ? H54B C54 H54C 109.5 . . ? C53 C55 H55A 109.5 . . ? C53 C55 H55B 109.5 . . ? H55A C55 H55B 109.5 . . ? C53 C55 H55C 109.5 . . ? H55A C55 H55C 109.5 . . ? H55B C55 H55C 109.5 . . ? C53 C56 H56A 109.5 . . ? C53 C56 H56B 109.5 . . ? H56A C56 H56B 109.5 . . ? C53 C56 H56C 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? N16 C57 Si4 121.8(4) . . ? N16 C57 H57 119.1 . . ? Si4 C57 H57 119.1 . . ? Si4 C58 H58A 109.5 . . ? Si4 C58 H58B 109.5 . . ? H58A C58 H58B 109.5 . . ? Si4 C58 H58C 109.5 . . ? H58A C58 H58C 109.5 . . ? H58B C58 H58C 109.5 . . ? Si4 C59 H59A 109.5 . . ? Si4 C59 H59B 109.5 . . ? H59A C59 H59B 109.5 . . ? Si4 C59 H59C 109.5 . . ? H59A C59 H59C 109.5 . . ? H59B C59 H59C 109.5 . . ? Si4 C60 H60A 109.5 . . ? Si4 C60 H60B 109.5 . . ? H60A C60 H60B 109.5 . . ? Si4 C60 H60C 109.5 . . ? H60A C60 H60C 109.5 . . ? H60B C60 H60C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 C13 1.865(6) . ? Si1 C14 1.866(6) . ? Si1 C15 1.873(6) . ? Si1 C12 1.875(6) . ? Si2 C27 1.864(5) . ? Si2 C28 1.864(6) . ? Si2 C30 1.868(5) . ? Si2 C29 1.869(6) . ? Si3 C45 1.851(6) . ? Si3 C43 1.857(6) . ? Si3 C42 1.861(5) . ? Si3 C44 1.862(6) . ? Si4 C59 1.854(7) . ? Si4 C60 1.858(7) . ? Si4 C58 1.859(6) . ? Si4 C57 1.859(5) . ? N1 C1 1.389(7) . ? N1 C2 1.404(7) . ? N1 C8 1.506(6) . ? N2 C3 1.374(7) . ? N2 C1 1.389(6) . ? N2 C4 1.490(7) . ? N3 C1 1.321(7) . ? N3 N4 1.378(6) . ? N4 C12 1.293(7) . ? N5 C18 1.376(7) . ? N5 C16 1.392(6) . ? N5 C19 1.508(7) . ? N6 C16 1.392(7) . ? N6 C17 1.407(6) . ? N6 C23 1.508(6) . ? N7 C16 1.314(6) . ? N7 N8 1.383(5) . ? N8 C27 1.284(6) . ? N9 C33 1.378(6) . ? N9 C31 1.391(6) . ? N9 C34 1.506(6) . ? N10 C31 1.392(6) . ? N10 C32 1.402(6) . ? N10 C38 1.504(6) . ? N11 C31 1.322(6) . ? N11 N12 1.385(6) . ? N12 C42 1.280(6) . ? N13 C46 1.399(6) . ? N13 C48 1.400(6) . ? N13 C49 1.503(6) . ? N14 C46 1.380(6) . ? N14 C47 1.385(6) . ? N14 C53 1.495(6) . ? N15 C46 1.316(7) . ? N15 N16 1.378(6) . ? N16 C57 1.286(7) . ? C2 C3 1.331(8) . ? C2 H2 0.9500 . ? C3 H3 0.9500 . ? C4 C7 1.519(8) . ? C4 C5 1.532(8) . ? C4 C6 1.536(7) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 C10 1.523(7) . ? C8 C9 1.530(7) . ? C8 C11 1.540(7) . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12 0.9500 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C17 C18 1.340(8) . ? C17 H17 0.9500 . ? C18 H18 0.9500 . ? C19 C22 1.526(7) . ? C19 C21 1.529(7) . ? C19 C20 1.535(7) . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C23 C25 1.516(7) . ? C23 C26 1.531(7) . ? C23 C24 1.538(7) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27 0.9500 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C32 C33 1.328(7) . ? C32 H32 0.9500 . ? C33 H33 0.9500 . ? C34 C36 1.522(7) . ? C34 C35 1.535(7) . ? C34 C37 1.545(6) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 C40 1.522(7) . ? C38 C41 1.531(7) . ? C38 C39 1.533(7) . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? C41 H41A 0.9800 . ? C41 H41B 0.9800 . ? C41 H41C 0.9800 . ? C42 H42 0.9500 . ? C43 H43A 0.9800 . ? C43 H43B 0.9800 . ? C43 H43C 0.9800 . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C47 C48 1.332(7) . ? C47 H47 0.9500 . ? C48 H48 0.9500 . ? C49 C51 1.517(7) . ? C49 C50 1.524(7) . ? C49 C52 1.545(7) . ? C50 H50A 0.9800 . ? C50 H50B 0.9800 . ? C50 H50C 0.9800 . ? C51 H51A 0.9800 . ? C51 H51B 0.9800 . ? C51 H51C 0.9800 . ? C52 H52A 0.9800 . ? C52 H52B 0.9800 . ? C52 H52C 0.9800 . ? C53 C55 1.526(7) . ? C53 C56 1.528(7) . ? C53 C54 1.530(7) . ? C54 H54A 0.9800 . ? C54 H54B 0.9800 . ? C54 H54C 0.9800 . ? C55 H55A 0.9800 . ? C55 H55B 0.9800 . ? C55 H55C 0.9800 . ? C56 H56A 0.9800 . ? C56 H56B 0.9800 . ? C56 H56C 0.9800 . ? C57 H57 0.9500 . ? C58 H58A 0.9800 . ? C58 H58B 0.9800 . ? C58 H58C 0.9800 . ? C59 H59A 0.9800 . ? C59 H59B 0.9800 . ? C59 H59C 0.9800 . ? C60 H60A 0.9800 . ? C60 H60B 0.9800 . ? C60 H60C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 N3 N4 C12 -175.5(5) . . . . ? C16 N7 N8 C27 175.6(4) . . . . ? C31 N11 N12 C42 173.8(4) . . . . ? C46 N15 N16 C57 -178.3(5) . . . . ? N4 N3 C1 N1 14.5(9) . . . . ? N4 N3 C1 N2 -168.9(4) . . . . ? C2 N1 C1 N3 176.8(6) . . . . ? C8 N1 C1 N3 -0.7(10) . . . . ? C2 N1 C1 N2 -0.1(5) . . . . ? C8 N1 C1 N2 -177.6(4) . . . . ? C3 N2 C1 N3 -177.2(5) . . . . ? C4 N2 C1 N3 0.1(8) . . . . ? C3 N2 C1 N1 0.4(6) . . . . ? C4 N2 C1 N1 177.6(4) . . . . ? C1 N1 C2 C3 -0.2(6) . . . . ? C8 N1 C2 C3 177.5(5) . . . . ? N1 C2 C3 N2 0.5(7) . . . . ? C1 N2 C3 C2 -0.5(6) . . . . ? C4 N2 C3 C2 -177.8(5) . . . . ? C3 N2 C4 C7 112.9(6) . . . . ? C1 N2 C4 C7 -63.9(6) . . . . ? C3 N2 C4 C5 -123.8(6) . . . . ? C1 N2 C4 C5 59.4(7) . . . . ? C3 N2 C4 C6 -5.6(7) . . . . ? C1 N2 C4 C6 177.6(5) . . . . ? C1 N1 C8 C10 -68.4(6) . . . . ? C2 N1 C8 C10 114.4(5) . . . . ? C1 N1 C8 C9 173.7(5) . . . . ? C2 N1 C8 C9 -3.6(6) . . . . ? C1 N1 C8 C11 55.6(7) . . . . ? C2 N1 C8 C11 -121.6(5) . . . . ? N3 N4 C12 Si1 -178.2(4) . . . . ? C13 Si1 C12 N4 25.8(6) . . . . ? C14 Si1 C12 N4 -94.7(5) . . . . ? C15 Si1 C12 N4 147.2(5) . . . . ? N8 N7 C16 N5 163.8(4) . . . . ? N8 N7 C16 N6 -17.7(8) . . . . ? C18 N5 C16 N7 -179.3(4) . . . . ? C19 N5 C16 N7 -1.4(7) . . . . ? C18 N5 C16 N6 1.8(5) . . . . ? C19 N5 C16 N6 179.7(4) . . . . ? C17 N6 C16 N7 179.4(6) . . . . ? C23 N6 C16 N7 -7.7(9) . . . . ? C17 N6 C16 N5 -2.0(5) . . . . ? C23 N6 C16 N5 171.0(4) . . . . ? C16 N6 C17 C18 1.5(6) . . . . ? C23 N6 C17 C18 -172.1(4) . . . . ? N6 C17 C18 N5 -0.4(6) . . . . ? C16 N5 C18 C17 -0.9(6) . . . . ? C19 N5 C18 C17 -178.8(4) . . . . ? C18 N5 C19 C22 117.0(5) . . . . ? C16 N5 C19 C22 -60.6(6) . . . . ? C18 N5 C19 C21 -120.6(5) . . . . ? C16 N5 C19 C21 61.8(6) . . . . ? C18 N5 C19 C20 -2.5(7) . . . . ? C16 N5 C19 C20 179.9(4) . . . . ? C16 N6 C23 C25 76.5(6) . . . . ? C17 N6 C23 C25 -111.4(5) . . . . ? C16 N6 C23 C26 -48.4(6) . . . . ? C17 N6 C23 C26 123.7(5) . . . . ? C16 N6 C23 C24 -165.0(5) . . . . ? C17 N6 C23 C24 7.1(6) . . . . ? N7 N8 C27 Si2 -176.8(3) . . . . ? C28 Si2 C27 N8 -31.2(5) . . . . ? C30 Si2 C27 N8 -152.7(4) . . . . ? C29 Si2 C27 N8 88.6(5) . . . . ? N12 N11 C31 N9 173.1(4) . . . . ? N12 N11 C31 N10 -9.0(8) . . . . ? C33 N9 C31 N11 178.6(4) . . . . ? C34 N9 C31 N11 1.3(7) . . . . ? C33 N9 C31 N10 0.1(5) . . . . ? C34 N9 C31 N10 -177.2(4) . . . . ? C32 N10 C31 N11 -178.7(5) . . . . ? C38 N10 C31 N11 1.2(9) . . . . ? C32 N10 C31 N9 -0.7(5) . . . . ? C38 N10 C31 N9 179.2(4) . . . . ? C31 N10 C32 C33 1.1(5) . . . . ? C38 N10 C32 C33 -178.9(4) . . . . ? N10 C32 C33 N9 -1.0(5) . . . . ? C31 N9 C33 C32 0.5(5) . . . . ? C34 N9 C33 C32 177.8(4) . . . . ? C33 N9 C34 C36 -115.7(5) . . . . ? C31 N9 C34 C36 61.2(6) . . . . ? C33 N9 C34 C35 119.4(5) . . . . ? C31 N9 C34 C35 -63.7(6) . . . . ? C33 N9 C34 C37 2.7(6) . . . . ? C31 N9 C34 C37 179.6(4) . . . . ? C31 N10 C38 C40 -175.0(5) . . . . ? C32 N10 C38 C40 4.9(6) . . . . ? C31 N10 C38 C41 -57.5(6) . . . . ? C32 N10 C38 C41 122.4(5) . . . . ? C31 N10 C38 C39 67.1(6) . . . . ? C32 N10 C38 C39 -113.0(5) . . . . ? N11 N12 C42 Si3 179.2(3) . . . . ? C45 Si3 C42 N12 120.9(5) . . . . ? C43 Si3 C42 N12 -0.6(5) . . . . ? C44 Si3 C42 N12 -121.8(5) . . . . ? N16 N15 C46 N14 -175.6(4) . . . . ? N16 N15 C46 N13 4.5(9) . . . . ? C47 N14 C46 N15 -179.3(4) . . . . ? C53 N14 C46 N15 -1.0(7) . . . . ? C47 N14 C46 N13 0.6(5) . . . . ? C53 N14 C46 N13 178.9(4) . . . . ? C48 N13 C46 N15 179.2(6) . . . . ? C49 N13 C46 N15 0.3(9) . . . . ? C48 N13 C46 N14 -0.6(5) . . . . ? C49 N13 C46 N14 -179.6(4) . . . . ? C46 N14 C47 C48 -0.3(6) . . . . ? C53 N14 C47 C48 -178.7(4) . . . . ? N14 C47 C48 N13 -0.1(6) . . . . ? C46 N13 C48 C47 0.4(6) . . . . ? C49 N13 C48 C47 179.5(4) . . . . ? C46 N13 C49 C51 59.6(6) . . . . ? C48 N13 C49 C51 -119.2(5) . . . . ? C46 N13 C49 C50 -66.1(6) . . . . ? C48 N13 C49 C50 115.1(5) . . . . ? C46 N13 C49 C52 177.7(5) . . . . ? C48 N13 C49 C52 -1.1(6) . . . . ? C46 N14 C53 C55 60.8(6) . . . . ? C47 N14 C53 C55 -121.2(5) . . . . ? C46 N14 C53 C56 -179.9(4) . . . . ? C47 N14 C53 C56 -1.8(6) . . . . ? C46 N14 C53 C54 -61.4(6) . . . . ? C47 N14 C53 C54 116.7(5) . . . . ? N15 N16 C57 Si4 179.5(4) . . . . ? C59 Si4 C57 N16 -73.7(6) . . . . ? C60 Si4 C57 N16 47.6(6) . . . . ? C58 Si4 C57 N16 167.6(5) . . . . ?