#------------------------------------------------------------------------------ #$Date: 2024-10-11 04:02:00 +0300 (Fri, 11 Oct 2024) $ #$Revision: 295419 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/28/1572857.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572857 loop_ _publ_author_name 'Zhang, Mengyao' 'Dai, Shengyu' _publ_section_title ; Nickel-Catalyzed Direct Synthesis of Hyperbranched Liquid Oligoethylene ; _journal_name_full 'Polymer Chemistry' _journal_paper_doi 10.1039/D4PY00709C _journal_year 2024 _chemical_formula_moiety 'C31 H41 Br3 N2 Ni, 0.1[H2O]' _chemical_formula_sum 'C31 H41 Br3 N2 Ni O2' _chemical_formula_weight 772.10 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-06-20 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2024-07-19 deposited with the CCDC. 2024-10-07 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 105.8140(10) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 18.9221(2) _cell_length_b 18.1077(2) _cell_length_c 21.0075(3) _cell_measurement_reflns_used 20487 _cell_measurement_temperature 296.93(10) _cell_measurement_theta_max 77.4410 _cell_measurement_theta_min 2.1880 _cell_volume 6925.49(15) _computing_cell_refinement 'CrysAlisPro 1.171.42.93a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.42.93a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.42.93a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment air _diffrn_ambient_temperature 296.93(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.957 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -61.00 -33.00 0.50 0.80 -- -104.50 57.00 60.00 56 2 \w -62.00 -33.00 0.50 0.80 -- -104.50 57.00-120.00 58 3 \w -62.00 -33.00 0.50 0.80 -- -104.50 57.00-150.00 58 4 \w -58.00 -32.00 0.50 0.80 -- -104.50 57.00-180.00 52 5 \w -19.00 24.00 0.50 0.20 -- -49.58 19.00-150.00 86 6 \w -22.00 11.00 0.50 0.20 -- -49.58 19.00-180.00 66 7 \w -22.00 13.00 0.50 0.20 -- -49.58 19.00 -60.00 70 8 \w 26.00 51.00 0.50 0.20 -- 49.58-116.00 -74.00 50 9 \w 58.00 83.00 0.50 0.20 -- 49.58-167.00 139.00 50 10 \w 67.00 92.00 0.50 0.80 -- 106.85-167.00 139.00 50 11 \w 66.00 92.00 0.50 0.80 -- 106.85-116.00 -74.00 52 12 \w 40.00 102.00 0.50 0.80 -- 106.85 -99.00 -90.00 124 13 \w 36.00 108.00 0.50 0.80 -- 106.85 -77.00 -90.00 144 14 \w 39.00 68.00 0.50 0.80 -- 106.85 -57.00 -90.00 58 15 \w 37.00 69.00 0.50 0.80 -- 106.85 -57.00 -60.00 64 16 \w 37.00 66.00 0.50 0.80 -- 106.85 -57.00 -30.00 58 17 \w 35.00 66.00 0.50 0.80 -- 106.85 -57.00 120.00 62 18 \w -20.00 44.00 0.50 0.20 -- 49.58 -38.00 150.00 128 19 \w 102.00 152.00 0.50 0.80 -- 106.85 19.00 120.00 100 20 \w -111.00 -78.00 0.50 0.20 -- -49.58 167.00 159.00 66 21 \w -102.00 -77.00 0.50 0.80 -- -104.50 116.00 13.00 50 22 \w -111.00 -39.00 0.50 0.80 -- -104.50 125.00 -30.00 144 23 \w 60.00 122.00 0.50 0.20 -- 49.58 167.00 159.00 124 24 \w 106.00 131.00 0.50 0.80 -- 106.85 116.00 13.00 50 25 \w -174.00 -98.00 0.50 0.80 -- -104.50 -38.00 120.00 152 26 \w -106.00 -81.00 0.50 0.80 -- -104.50-167.00 139.00 50 27 \w -114.00 -49.00 0.50 0.20 -- -49.58-167.00 139.00 130 28 \w -171.00 -80.00 0.50 0.80 -- -104.50-116.00 -74.00 182 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0163583000 _diffrn_orient_matrix_UB_12 0.0726731000 _diffrn_orient_matrix_UB_13 -0.0393702000 _diffrn_orient_matrix_UB_21 -0.0019330000 _diffrn_orient_matrix_UB_22 -0.0421136000 _diffrn_orient_matrix_UB_23 -0.0641755000 _diffrn_orient_matrix_UB_31 -0.0830150000 _diffrn_orient_matrix_UB_32 -0.0133790000 _diffrn_orient_matrix_UB_33 -0.0119232000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0455 _diffrn_reflns_av_unetI/netI 0.0262 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.957 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 27208 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.957 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 78.102 _diffrn_reflns_theta_min 3.707 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'PhotonJet R (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 5.074 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.64392 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.93a (Rigaku Oxford Diffraction, 2023) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear bluish red' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier bluish _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.481 _exptl_crystal_description block _exptl_crystal_F_000 3120 _exptl_crystal_size_max 0.12 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.1 _refine_diff_density_max 1.446 _refine_diff_density_min -0.620 _refine_diff_density_rms 0.131 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 353 _refine_ls_number_reflns 7105 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.043 _refine_ls_R_factor_all 0.0508 _refine_ls_R_factor_gt 0.0486 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1038P)^2^+11.3704P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1505 _refine_ls_wR_factor_ref 0.1530 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6573 _reflns_number_total 7105 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL zmy_auto_a.res in C2/c zmy_auto.res created by SHELXL-2018/3 at 12:55:46 on 20-Jun-2024 REM Old TITL zmy_auto in C2/c REM SHELXT solution in C2/c: R1 0.149, Rweak 0.009, Alpha 0.035 REM 1.275 for 230 systematic absences, Orientation as input REM Formula found by SHELXT: C30 N5 Ni Br3 CELL 1.54184 18.9221 18.1077 21.0075 90 105.814 90 ZERR 8 0.0002 0.0002 0.0003 0 0.001 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Br N Ni O UNIT 248 328 24 16 8 16 L.S. 4 0 0 PLAN 10 SIZE 0.1 0.11 0.12 TEMP 24 CONF list 4 MORE -1 BOND $H fmap 2 53 acta OMIT 4 0 0 OMIT -2 0 4 OMIT 2 2 0 OMIT 1 1 0 OMIT 3 1 0 OMIT 1 1 2 REM REM REM WGHT 0.103800 11.370399 FVAR 0.14077 BR1 3 0.809897 0.691698 0.477548 11.00000 0.04037 0.05453 = 0.04138 -0.00659 0.00298 0.00272 BR2 3 0.696521 0.716047 0.308671 11.00000 0.05632 0.06190 = 0.03457 0.00460 0.01079 -0.00035 BR3 3 0.643337 0.912224 0.365845 11.00000 0.07729 0.04841 = 0.09328 0.01710 0.01126 -0.01632 NI1 5 0.684055 0.732933 0.421175 11.00000 0.03392 0.03863 = 0.03133 0.00241 0.00365 -0.00342 N1 4 0.619331 0.645875 0.431845 11.00000 0.03722 0.03349 = 0.02671 0.00093 0.00740 0.00072 N2 4 0.582557 0.777433 0.378526 11.00000 0.04022 0.03727 = 0.03164 0.00377 0.00388 -0.00095 C19 1 0.650398 0.512729 0.572183 11.00000 0.04536 0.03794 = 0.03254 0.00352 0.01228 0.00235 AFIX 43 H19 2 0.640226 0.508824 0.612939 11.00000 -1.20000 AFIX 0 C20 1 0.626433 0.575669 0.533781 11.00000 0.03676 0.03542 = 0.03255 0.00095 0.00989 0.00119 C6 1 0.551574 0.653350 0.400020 11.00000 0.03700 0.03791 = 0.03045 -0.00061 0.00443 -0.00193 C8 1 0.642672 0.580726 0.472450 11.00000 0.03715 0.03302 = 0.02966 0.00258 0.00759 -0.00039 C18 1 0.688701 0.455774 0.552239 11.00000 0.04635 0.03732 = 0.03868 0.00505 0.01135 0.00541 C9 1 0.682832 0.524734 0.451143 11.00000 0.04667 0.03736 = 0.03366 0.00198 0.01380 0.00355 C21 1 0.587038 0.635338 0.561326 11.00000 0.04480 0.03624 = 0.03387 0.00078 0.01569 0.00188 AFIX 13 H21 2 0.575702 0.675709 0.529068 11.00000 -1.20000 AFIX 0 C5 1 0.528209 0.726702 0.369659 11.00000 0.03865 0.04021 = 0.03093 0.00017 0.00471 -0.00126 C16 1 0.704447 0.463590 0.491568 11.00000 0.05663 0.03850 = 0.04396 0.00308 0.01992 0.01116 AFIX 43 H16 2 0.730520 0.426291 0.477582 11.00000 -1.20000 AFIX 0 C10 1 0.700178 0.529200 0.384534 11.00000 0.05689 0.03819 = 0.03574 0.00081 0.01900 0.00523 AFIX 13 H10 2 0.697809 0.581394 0.371789 11.00000 -1.20000 AFIX 0 C27 1 0.715417 0.389527 0.596949 11.00000 0.05467 0.03897 = 0.04187 0.00861 0.01862 0.01031 AFIX 13 H27 2 0.691949 0.392593 0.633088 11.00000 -1.20000 AFIX 0 C1 1 0.565495 0.845054 0.356548 11.00000 0.05167 0.04124 = 0.04333 0.00370 0.00884 -0.00137 C4 1 0.456781 0.743892 0.336814 11.00000 0.04103 0.05342 = 0.04852 0.00533 0.00077 0.00272 AFIX 43 H4 2 0.420589 0.707675 0.329152 11.00000 -1.20000 AFIX 0 C26 1 0.513969 0.608402 0.572672 11.00000 0.04729 0.04874 = 0.06602 -0.00494 0.02375 -0.00198 AFIX 23 H26A 2 0.482098 0.590324 0.531287 11.00000 -1.20000 H26B 2 0.523660 0.567842 0.604020 11.00000 -1.20000 AFIX 0 C22 1 0.635927 0.666552 0.626283 11.00000 0.05419 0.05283 = 0.04178 -0.00830 0.01406 -0.00140 AFIX 23 H22A 2 0.648736 0.627263 0.658786 11.00000 -1.20000 H22B 2 0.681032 0.685357 0.618880 11.00000 -1.20000 AFIX 0 C2 1 0.493856 0.867424 0.325626 11.00000 0.06464 0.04579 = 0.05315 0.01002 0.00851 0.01361 AFIX 43 H2 2 0.483480 0.916170 0.312426 11.00000 -1.20000 AFIX 0 C7 1 0.494054 0.595551 0.393381 11.00000 0.04466 0.04563 = 0.06356 0.00797 0.00080 -0.00915 AFIX 137 H7A 2 0.516734 0.549610 0.410517 11.00000 -1.50000 H7B 2 0.468119 0.589628 0.347556 11.00000 -1.50000 H7C 2 0.460220 0.610147 0.417791 11.00000 -1.50000 AFIX 0 C3 1 0.439166 0.815559 0.315236 11.00000 0.04853 0.06141 = 0.05476 0.01212 0.00008 0.01397 AFIX 43 H3 2 0.390884 0.828302 0.293987 11.00000 -1.20000 AFIX 0 C15 1 0.776962 0.501648 0.386891 11.00000 0.05770 0.07618 = 0.04504 -0.00560 0.02165 0.00532 AFIX 23 H15A 2 0.781592 0.450294 0.400538 11.00000 -1.20000 H15B 2 0.813050 0.529957 0.419381 11.00000 -1.20000 AFIX 0 C25 1 0.475397 0.670478 0.599042 11.00000 0.05865 0.06407 = 0.09051 -0.00378 0.03975 0.00789 AFIX 23 H25A 2 0.462031 0.709242 0.566073 11.00000 -1.20000 H25B 2 0.430627 0.651643 0.607106 11.00000 -1.20000 AFIX 0 C11 1 0.642959 0.488527 0.331397 11.00000 0.06476 0.07815 = 0.04195 -0.00933 0.01685 0.00133 AFIX 23 H11A 2 0.594667 0.508286 0.329047 11.00000 -1.20000 H11B 2 0.643163 0.436664 0.343003 11.00000 -1.20000 AFIX 0 C28 1 0.797179 0.392586 0.628161 11.00000 0.05890 0.05737 = 0.07111 0.02313 0.00227 -0.00042 AFIX 23 H28A 2 0.809115 0.438142 0.653069 11.00000 -1.20000 H28B 2 0.822165 0.393182 0.593516 11.00000 -1.20000 AFIX 0 C32 1 0.693402 0.316114 0.563135 11.00000 0.07438 0.04329 = 0.06413 0.00644 0.00774 0.00341 AFIX 23 H32A 2 0.712407 0.312750 0.524761 11.00000 -1.20000 H32B 2 0.640255 0.313375 0.547843 11.00000 -1.20000 AFIX 0 C30 1 0.804055 0.255495 0.639254 11.00000 0.08655 0.06439 = 0.08572 0.02740 0.03546 0.03638 AFIX 23 H30A 2 0.819663 0.215258 0.670401 11.00000 -1.20000 H30B 2 0.828860 0.250182 0.604736 11.00000 -1.20000 AFIX 0 C14 1 0.792329 0.508914 0.319340 11.00000 0.07104 0.08497 = 0.05803 -0.00380 0.03631 0.00246 AFIX 23 H14A 2 0.792053 0.560688 0.307425 11.00000 -1.20000 H14B 2 0.840624 0.489096 0.321788 11.00000 -1.20000 AFIX 0 C31 1 0.722160 0.251080 0.609137 11.00000 0.09067 0.04300 = 0.08545 0.01490 0.02070 0.01056 AFIX 23 H31A 2 0.697764 0.250379 0.644193 11.00000 -1.20000 H31B 2 0.710399 0.205369 0.584439 11.00000 -1.20000 AFIX 0 C23 1 0.597639 0.728199 0.653096 11.00000 0.08416 0.06614 = 0.06061 -0.02472 0.02688 -0.00015 AFIX 23 H23A 2 0.589300 0.769601 0.622655 11.00000 -1.20000 H23B 2 0.629059 0.744928 0.695198 11.00000 -1.20000 AFIX 0 C12 1 0.658138 0.496164 0.263731 11.00000 0.08662 0.09960 = 0.03828 -0.01228 0.01572 0.00125 AFIX 23 H12A 2 0.622047 0.468056 0.231067 11.00000 -1.20000 H12B 2 0.653877 0.547587 0.250285 11.00000 -1.20000 AFIX 0 C24 1 0.524101 0.702226 0.662440 11.00000 0.09687 0.07447 = 0.07336 -0.00766 0.05146 0.01561 AFIX 23 H24A 2 0.532891 0.664965 0.696885 11.00000 -1.20000 H24B 2 0.499374 0.743564 0.676450 11.00000 -1.20000 AFIX 0 C29 1 0.825301 0.327459 0.674122 11.00000 0.06515 0.07164 = 0.08371 0.03329 -0.00050 0.00967 AFIX 23 H29A 2 0.878381 0.330232 0.690356 11.00000 -1.20000 H29B 2 0.805203 0.330169 0.711888 11.00000 -1.20000 AFIX 0 C13 1 0.735250 0.468005 0.266916 11.00000 0.09667 0.08652 = 0.04839 -0.01300 0.03525 0.00390 AFIX 23 H13A 2 0.738237 0.415610 0.276907 11.00000 -1.20000 H13B 2 0.744880 0.474850 0.224251 11.00000 -1.20000 AFIX 0 O1 6 0.501352 0.921652 0.626840 11.00000 0.10448 0.13780 = 0.39762 -0.11752 0.08186 -0.01828 O2 6 0.453040 0.869758 0.493804 11.00000 0.18861 0.18820 = 0.13867 0.04351 0.02318 0.00268 HKLF 4 REM zmy_auto_a.res in C2/c REM wR2 = 0.1530, GooF = S = 1.043, Restrained GooF = 1.043 for all data REM R1 = 0.0486 for 6573 Fo > 4sig(Fo) and 0.0508 for all 7105 data REM 353 parameters refined using 0 restraints END WGHT 0.1038 11.3699 REM Highest difference peak 1.446, deepest hole -0.620, 1-sigma level 0.131 Q1 1 0.5249 0.9088 0.5507 11.00000 0.05 1.45 Q2 1 0.4777 0.9653 0.5806 11.00000 0.05 1.05 Q3 1 0.4628 0.8867 0.5399 11.00000 0.05 0.93 Q4 1 0.4751 0.8410 0.4977 11.00000 0.05 0.80 Q5 1 0.6290 0.9235 0.3964 11.00000 0.05 0.80 Q6 1 0.4971 0.9899 0.4829 11.00000 0.05 0.72 Q7 1 0.5140 0.9203 0.6648 11.00000 0.05 0.67 Q8 1 0.7414 0.7382 0.3370 11.00000 0.05 0.66 Q9 1 0.4388 0.8863 0.4668 11.00000 0.05 0.63 Q10 1 0.7497 0.7013 0.4557 11.00000 0.05 0.54 REM The information below was added by Olex2. REM REM R1 = 0.0486 for 6573 Fo > 4sig(Fo) and 0.0508 for all 27825 data REM 353 parameters refined using n/a restraints REM Highest difference peak 1.45, deepest hole -0.62 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0508 REM R1_gt = 0.0486 REM wR_ref = 0.1530 REM GOOF = 1.043 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 27825 REM Reflections_gt = 6573 REM Parameters = 353 REM Hole = -0.62 REM Peak = 1.45 REM Flack = n/a ; _cod_data_source_file d4py00709c2.cif _cod_data_source_block zmy_auto _cod_database_code 1572857 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C H N Br Ni' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.631 _shelx_estimated_absorpt_t_min 0.581 _olex2_refinement_description ; 1.a Ternary CH refined with riding coordinates: C21(H21), C10(H10), C27(H27) 1.b Secondary CH2 refined with riding coordinates: C26(H26A,H26B), C22(H22A,H22B), C15(H15A,H15B), C25(H25A,H25B), C11(H11A, H11B), C28(H28A,H28B), C32(H32A,H32B), C30(H30A,H30B), C14(H14A,H14B), C31(H31A,H31B), C23(H23A,H23B), C12(H12A,H12B), C24(H24A,H24B), C29(H29A,H29B), C13(H13A,H13B) 1.c Aromatic/amide H refined with riding coordinates: C19(H19), C16(H16), C4(H4), C2(H2), C3(H3) 1.d Idealised Me refined as rotating group: C7(H7A,H7B,H7C) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.498 _oxdiff_exptl_absorpt_empirical_full_min 0.412 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.80990(2) 0.69170(2) 0.47755(2) 0.04703(13) Uani 1 1 d . . . . . Br2 Br 0.69652(2) 0.71605(2) 0.30867(2) 0.05124(13) Uani 1 1 d . . . . . Br3 Br 0.64334(3) 0.91222(3) 0.36585(3) 0.07534(18) Uani 1 1 d . . . . . Ni1 Ni 0.68405(3) 0.73293(3) 0.42117(2) 0.03565(15) Uani 1 1 d . . . . . N1 N 0.61933(13) 0.64588(13) 0.43184(11) 0.0327(5) Uani 1 1 d . . . . . N2 N 0.58256(14) 0.77743(14) 0.37853(12) 0.0375(5) Uani 1 1 d . . . . . C19 C 0.65040(17) 0.51273(17) 0.57218(15) 0.0383(6) Uani 1 1 d . . . . . H19 H 0.640226 0.508824 0.612939 0.046 Uiso 1 1 calc R U . . . C20 C 0.62643(16) 0.57567(17) 0.53378(14) 0.0348(6) Uani 1 1 d . . . . . C6 C 0.55157(16) 0.65335(17) 0.40002(14) 0.0361(6) Uani 1 1 d . . . . . C8 C 0.64267(15) 0.58073(16) 0.47245(14) 0.0336(5) Uani 1 1 d . . . . . C18 C 0.68870(18) 0.45577(18) 0.55224(16) 0.0408(6) Uani 1 1 d . . . . . C9 C 0.68283(17) 0.52473(17) 0.45114(15) 0.0387(6) Uani 1 1 d . . . . . C21 C 0.58704(17) 0.63534(17) 0.56133(15) 0.0373(6) Uani 1 1 d . . . . . H21 H 0.575702 0.675709 0.529068 0.045 Uiso 1 1 calc R U . . . C5 C 0.52821(17) 0.72670(17) 0.36966(15) 0.0375(6) Uani 1 1 d . . . . . C16 C 0.70445(19) 0.46359(19) 0.49157(17) 0.0451(7) Uani 1 1 d . . . . . H16 H 0.730520 0.426291 0.477582 0.054 Uiso 1 1 calc R U . . . C10 C 0.70018(19) 0.52920(18) 0.38453(16) 0.0424(7) Uani 1 1 d . . . . . H10 H 0.697809 0.581394 0.371789 0.051 Uiso 1 1 calc R U . . . C27 C 0.71542(19) 0.38953(18) 0.59695(17) 0.0441(7) Uani 1 1 d . . . . . H27 H 0.691949 0.392593 0.633088 0.053 Uiso 1 1 calc R U . . . C1 C 0.56550(19) 0.84505(19) 0.35655(17) 0.0462(7) Uani 1 1 d . . . . . C4 C 0.45678(19) 0.7439(2) 0.33681(18) 0.0499(8) Uani 1 1 d . . . . . H4 H 0.420589 0.707675 0.329152 0.060 Uiso 1 1 calc R U . . . C26 C 0.5140(2) 0.6084(2) 0.5727(2) 0.0524(8) Uani 1 1 d . . . . . H26A H 0.482098 0.590324 0.531287 0.063 Uiso 1 1 calc R U . . . H26B H 0.523660 0.567842 0.604020 0.063 Uiso 1 1 calc R U . . . C22 C 0.6359(2) 0.6666(2) 0.62628(18) 0.0494(8) Uani 1 1 d . . . . . H22A H 0.648736 0.627263 0.658786 0.059 Uiso 1 1 calc R U . . . H22B H 0.681032 0.685357 0.618880 0.059 Uiso 1 1 calc R U . . . C2 C 0.4939(2) 0.8674(2) 0.3256(2) 0.0560(9) Uani 1 1 d . . . . . H2 H 0.483480 0.916170 0.312426 0.067 Uiso 1 1 calc R U . . . C7 C 0.4941(2) 0.5956(2) 0.3934(2) 0.0540(9) Uani 1 1 d . . . . . H7A H 0.516734 0.549610 0.410517 0.081 Uiso 1 1 calc R U . . . H7B H 0.468119 0.589628 0.347556 0.081 Uiso 1 1 calc R U . . . H7C H 0.460220 0.610147 0.417791 0.081 Uiso 1 1 calc R U . . . C3 C 0.4392(2) 0.8156(2) 0.3152(2) 0.0576(9) Uani 1 1 d . . . . . H3 H 0.390884 0.828302 0.293987 0.069 Uiso 1 1 calc R U . . . C15 C 0.7770(2) 0.5016(3) 0.38689(19) 0.0581(9) Uani 1 1 d . . . . . H15A H 0.781592 0.450294 0.400538 0.070 Uiso 1 1 calc R U . . . H15B H 0.813050 0.529957 0.419381 0.070 Uiso 1 1 calc R U . . . C25 C 0.4754(2) 0.6705(3) 0.5990(3) 0.0673(11) Uani 1 1 d . . . . . H25A H 0.462031 0.709242 0.566073 0.081 Uiso 1 1 calc R U . . . H25B H 0.430627 0.651643 0.607106 0.081 Uiso 1 1 calc R U . . . C11 C 0.6430(2) 0.4885(3) 0.33140(19) 0.0612(10) Uani 1 1 d . . . . . H11A H 0.594667 0.508286 0.329047 0.073 Uiso 1 1 calc R U . . . H11B H 0.643163 0.436664 0.343003 0.073 Uiso 1 1 calc R U . . . C28 C 0.7972(2) 0.3926(3) 0.6282(2) 0.0655(11) Uani 1 1 d . . . . . H28A H 0.809115 0.438142 0.653069 0.079 Uiso 1 1 calc R U . . . H28B H 0.822165 0.393182 0.593516 0.079 Uiso 1 1 calc R U . . . C32 C 0.6934(3) 0.3161(2) 0.5631(2) 0.0628(10) Uani 1 1 d . . . . . H32A H 0.712407 0.312750 0.524761 0.075 Uiso 1 1 calc R U . . . H32B H 0.640255 0.313375 0.547843 0.075 Uiso 1 1 calc R U . . . C30 C 0.8041(3) 0.2555(3) 0.6393(3) 0.0765(14) Uani 1 1 d . . . . . H30A H 0.819663 0.215258 0.670401 0.092 Uiso 1 1 calc R U . . . H30B H 0.828860 0.250182 0.604736 0.092 Uiso 1 1 calc R U . . . C14 C 0.7923(3) 0.5089(3) 0.3193(2) 0.0677(11) Uani 1 1 d . . . . . H14A H 0.792053 0.560688 0.307425 0.081 Uiso 1 1 calc R U . . . H14B H 0.840624 0.489096 0.321788 0.081 Uiso 1 1 calc R U . . . C31 C 0.7222(3) 0.2511(2) 0.6091(3) 0.0737(12) Uani 1 1 d . . . . . H31A H 0.697764 0.250379 0.644193 0.088 Uiso 1 1 calc R U . . . H31B H 0.710399 0.205369 0.584439 0.088 Uiso 1 1 calc R U . . . C23 C 0.5976(3) 0.7282(3) 0.6531(2) 0.0689(12) Uani 1 1 d . . . . . H23A H 0.589300 0.769601 0.622655 0.083 Uiso 1 1 calc R U . . . H23B H 0.629059 0.744928 0.695198 0.083 Uiso 1 1 calc R U . . . C12 C 0.6581(3) 0.4962(3) 0.2637(2) 0.0751(13) Uani 1 1 d . . . . . H12A H 0.622047 0.468056 0.231067 0.090 Uiso 1 1 calc R U . . . H12B H 0.653877 0.547587 0.250285 0.090 Uiso 1 1 calc R U . . . C24 C 0.5241(3) 0.7022(3) 0.6624(3) 0.0760(13) Uani 1 1 d . . . . . H24A H 0.532891 0.664965 0.696885 0.091 Uiso 1 1 calc R U . . . H24B H 0.499374 0.743564 0.676450 0.091 Uiso 1 1 calc R U . . . C29 C 0.8253(3) 0.3275(3) 0.6741(3) 0.0776(14) Uani 1 1 d . . . . . H29A H 0.878381 0.330232 0.690356 0.093 Uiso 1 1 calc R U . . . H29B H 0.805203 0.330169 0.711888 0.093 Uiso 1 1 calc R U . . . C13 C 0.7353(3) 0.4680(3) 0.2669(2) 0.0742(13) Uani 1 1 d . . . . . H13A H 0.738237 0.415610 0.276907 0.089 Uiso 1 1 calc R U . . . H13B H 0.744880 0.474850 0.224251 0.089 Uiso 1 1 calc R U . . . O1 O 0.5014(4) 0.9217(4) 0.6268(6) 0.211(5) Uani 1 1 d . . . . . O2 O 0.4530(5) 0.8698(5) 0.4938(4) 0.176(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.0404(2) 0.0545(2) 0.0414(2) -0.00659(14) 0.00298(14) 0.00272(13) Br2 0.0563(2) 0.0619(3) 0.0346(2) 0.00460(14) 0.01079(15) -0.00035(16) Br3 0.0773(3) 0.0484(3) 0.0933(4) 0.0171(2) 0.0113(3) -0.0163(2) Ni1 0.0339(3) 0.0386(3) 0.0313(3) 0.0024(2) 0.0037(2) -0.00342(19) N1 0.0372(11) 0.0335(12) 0.0267(10) 0.0009(9) 0.0074(9) 0.0007(9) N2 0.0402(12) 0.0373(13) 0.0316(12) 0.0038(10) 0.0039(10) -0.0009(10) C19 0.0454(15) 0.0379(15) 0.0325(14) 0.0035(11) 0.0123(11) 0.0023(12) C20 0.0368(13) 0.0354(14) 0.0325(13) 0.0009(11) 0.0099(11) 0.0012(11) C6 0.0370(14) 0.0379(15) 0.0304(13) -0.0006(11) 0.0044(11) -0.0019(11) C8 0.0372(13) 0.0330(14) 0.0297(13) 0.0026(11) 0.0076(10) -0.0004(10) C18 0.0464(16) 0.0373(15) 0.0387(15) 0.0051(12) 0.0114(12) 0.0054(12) C9 0.0467(15) 0.0374(15) 0.0337(14) 0.0020(12) 0.0138(12) 0.0035(12) C21 0.0448(15) 0.0362(14) 0.0339(14) 0.0008(11) 0.0157(12) 0.0019(12) C5 0.0387(14) 0.0402(16) 0.0309(13) 0.0002(11) 0.0047(11) -0.0013(11) C16 0.0566(18) 0.0385(16) 0.0440(17) 0.0031(13) 0.0199(14) 0.0112(13) C10 0.0569(18) 0.0382(15) 0.0357(15) 0.0008(12) 0.0190(13) 0.0052(13) C27 0.0547(18) 0.0390(16) 0.0419(16) 0.0086(13) 0.0186(14) 0.0103(13) C1 0.0517(17) 0.0412(16) 0.0433(17) 0.0037(13) 0.0088(13) -0.0014(14) C4 0.0410(16) 0.0534(19) 0.0485(18) 0.0053(15) 0.0008(14) 0.0027(14) C26 0.0473(18) 0.0487(19) 0.066(2) -0.0049(17) 0.0238(16) -0.0020(14) C22 0.0542(18) 0.0528(19) 0.0418(17) -0.0083(15) 0.0141(14) -0.0014(15) C2 0.065(2) 0.0458(19) 0.053(2) 0.0100(16) 0.0085(16) 0.0136(16) C7 0.0447(17) 0.0456(19) 0.064(2) 0.0080(16) 0.0008(15) -0.0092(14) C3 0.0485(19) 0.061(2) 0.055(2) 0.0121(18) 0.0001(16) 0.0140(16) C15 0.058(2) 0.076(3) 0.0450(19) -0.0056(18) 0.0217(16) 0.0053(19) C25 0.059(2) 0.064(2) 0.091(3) -0.004(2) 0.040(2) 0.0079(19) C11 0.065(2) 0.078(3) 0.0420(19) -0.0093(18) 0.0168(16) 0.001(2) C28 0.059(2) 0.057(2) 0.071(3) 0.023(2) 0.0023(19) -0.0004(18) C32 0.074(3) 0.043(2) 0.064(2) 0.0064(18) 0.008(2) 0.0034(18) C30 0.087(3) 0.064(3) 0.086(3) 0.027(2) 0.035(3) 0.036(2) C14 0.071(3) 0.085(3) 0.058(2) -0.004(2) 0.036(2) 0.002(2) C31 0.091(3) 0.043(2) 0.085(3) 0.015(2) 0.021(3) 0.011(2) C23 0.084(3) 0.066(3) 0.061(2) -0.025(2) 0.027(2) 0.000(2) C12 0.087(3) 0.100(4) 0.0383(19) -0.012(2) 0.0157(19) 0.001(3) C24 0.097(3) 0.074(3) 0.073(3) -0.008(2) 0.051(3) 0.016(3) C29 0.065(3) 0.072(3) 0.084(3) 0.033(3) -0.001(2) 0.010(2) C13 0.097(3) 0.087(3) 0.048(2) -0.013(2) 0.035(2) 0.004(3) O1 0.104(4) 0.138(5) 0.398(14) -0.118(7) 0.082(6) -0.018(4) O2 0.189(7) 0.188(7) 0.139(6) 0.044(5) 0.023(5) 0.003(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni -3.0029 0.5091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 1 1.88 0.21 0 0 2 3264.47 71.23 0 0 3 0.64 0.69 0 0 3 0.16 0.49 0 0 4 5526.39 126.53 0 0 4 6026 126.43 0 0 5 0.97 0.9 0 0 5 1.1 0.74 0 0 6 1056.26 24.42 0 0 7 0.27 0.99 0 0 8 8.48 1.39 0 0 9 0.45 1.15 0 0 10 151.4 5.56 0 0 11 0.94 1.4 0 0 12 11.41 2.08 0 0 13 -0.12 0.86 0 0 -13 0.56 0.55 0 0 14 23.85 2.84 0 0 14 20.37 1.43 0 0 -14 23.49 1.25 0 0 15 1.65 1.93 0 0 15 0.45 0.91 0 0 -15 -0.08 0.68 0 0 16 227.6 6.49 0 0 -16 262.1 6.53 0 0 17 0.12 0.98 0 0 -17 -0.39 0.76 0 0 18 630.41 15.09 0 0 -18 689.67 15.17 0 0 -19 0.84 0.96 0 0 -19 0.48 1.22 0 0 -20 232.83 6.06 0 0 -20 186.18 7.25 0 0 -21 -0.04 0.85 0 0 -22 27.91 1.54 0 0 -23 0.24 0.7 0 0 -24 90.75 2.73 0 0 -25 0.06 0.43 0 0 -25 0.43 0.32 0 0 25 -0.38 0.37 0 -2 0 3027.28 66.11 0 -2 -1 13.97 0.69 0 -2 2 9.73 0.95 0 -2 -2 7.56 0.56 0 -2 3 218.29 5.68 0 -2 -3 213.08 5.22 0 -2 4 301.94 7.77 0 -2 5 2066.67 44.6 0 -2 5 1921.07 44.38 0 -2 6 703.38 16.96 0 -2 6 719.96 16.96 0 -2 7 370.86 9.61 0 -2 7 359.22 9.61 0 -2 8 1206.71 28.22 0 -2 8 1217.19 28.37 0 -2 9 450.41 11.94 0 2 9 468.5 12.22 0 2 10 769.38 18.89 0 -2 10 750.84 18.55 0 2 11 350.89 10.68 0 -2 -12 94.39 2.75 0 2 -12 98.86 2.83 0 2 12 95.38 4.8 0 2 -13 503.62 11.28 0 -2 -13 485.54 11.19 0 -2 13 445.21 11.31 0 2 13 467.06 11.66 0 2 13 511.36 14.42 0 2 14 2 1.94 0 2 -14 1 0.64 0 -2 -14 2.04 0.62 0 2 14 1.13 1.01 0 -2 14 1.71 0.87 0 2 15 8.63 2.48 0 2 -15 8.89 0.97 0 -2 -15 8.7 0.89 0 2 15 7.2 1.29 0 -2 15 6.53 1.05 0 2 -16 11.59 1.11 0 -2 -16 10.56 1.03 0 -2 16 11.27 1.18 0 2 16 9.23 1.39 0 2 16 9.86 2.47 0 2 17 22.88 1.66 0 -2 -17 18.43 2.05 0 2 17 22.32 3.16 0 -2 -17 30.62 1.53 0 2 -17 26.62 1.57 0 -2 -18 600.56 13.6 0 2 -18 617.7 13.77 0 2 19 1.6 1.02 0 -2 -19 -0.25 1.03 0 -2 -19 0.55 0.82 0 2 -19 0.99 0.95 0 2 -20 46.06 2.08 0 -2 -20 44.34 1.97 0 2 20 40.18 1.95 0 2 -21 19.73 1.36 0 -2 -21 19.64 1.3 0 -2 -22 27.83 1.46 0 2 -22 25.99 1.49 0 2 -23 0.42 0.71 0 -2 -23 0.05 0.66 0 2 -24 37.19 1.49 0 -2 -24 31.39 1.37 0 2 25 19.26 0.73 0 -2 -25 20.53 0.75 0 2 -25 20.77 0.93 0 -2 -25 17.96 0.85 0 -4 0 1648.1 36.61 0 -4 1 918.03 21.07 0 -4 -1 940.47 21.03 0 -4 -2 809.23 18.43 0 -4 -3 21.8 1.24 0 -4 4 27.78 1.96 0 -4 -4 28.93 1.4 0 -4 5 343.71 9.59 0 -4 -5 361.17 8.8 0 -4 6 10.57 1.56 0 -4 7 1035.89 24.82 0 -4 8 831.79 20.54 0 -4 9 54.09 2.99 0 -4 10 150.45 5.63 0 -4 11 345.19 10.64 0 4 11 402.75 11.6 0 -4 12 109.23 4.82 0 4 12 116 3.84 0 4 -12 113.94 3.18 0 -4 -12 109.48 3.09 0 4 13 96.9 3.63 0 4 -13 101.34 3.01 0 -4 -13 98.96 2.89 0 4 13 99.9 5.45 0 4 14 37.77 2.19 0 4 -14 34.48 1.58 0 -4 -14 32.31 1.45 0 4 15 164.33 5.22 0 -4 -15 160.6 4.48 0 4 -15 170.95 4.7 0 4 15 167.08 7.56 0 -4 -16 54.69 2.08 0 4 -16 59.93 2.29 0 4 16 54.8 2.66 0 4 16 53.11 4.27 0 -4 -17 642.52 14.92 0 4 -17 696.36 15.19 0 4 17 638.77 15.51 0 4 17 671.19 19.39 0 4 -17 653.32 17.25 0 4 18 43.53 2.35 0 4 -18 53.32 2.19 0 -4 -18 49.37 2.01 0 4 18 48.13 4.12 0 4 -18 45.4 3.16 0 4 19 1.39 0.98 0 -4 -19 1.8 0.71 0 4 -19 1.27 0.8 0 -4 19 2.45 2.75 0 4 19 4.85 2.58 0 4 -19 1.82 1.11 0 -4 -19 1 0.86 0 4 19 1.07 1.83 0 4 20 11.72 1.24 0 -4 -20 11.65 1.05 0 4 -20 15.2 1.24 0 4 21 4.4 0.87 0 -4 -21 3.5 0.72 0 4 -21 4.5 0.85 0 4 -22 1.53 0.76 0 -4 -22 2.07 0.68 0 -4 -23 2.2 0.62 0 4 -23 1.99 0.7 0 4 24 2 0.39 0 -4 -24 1.71 0.35 0 4 -24 3.05 0.44 0 4 -24 2.62 0.58 0 -4 25 38.23 1.08 0 -6 0 897.16 20.77 0 -6 1 1035.1 23.93 0 -6 -1 1044.95 23.83 0 -6 2 44.01 2.07 0 -6 2 38.54 1.41 0 6 -2 42.09 1.09 0 -6 -3 316.74 8.01 0 -6 -3 309.49 7.03 0 -6 4 2824.23 63.85 0 -6 -4 2809.24 62.47 0 -6 5 259 8.46 0 -6 -5 294.23 7.55 0 -6 6 15.79 2.06 0 -6 -6 19.87 1.45 0 -6 7 1973.88 48.15 0 -6 -7 2127.42 46.75 0 -6 8 127.61 5.39 0 -6 9 64.09 3.73 0 -6 10 23.27 2.36 0 -6 11 153.75 6.38 0 6 11 171.24 5.12 0 -6 12 65.95 3.94 0 -6 -12 69 2.12 0 6 -12 65.92 2.19 0 -6 13 22.04 2.52 0 6 13 31.12 3.34 0 6 13 29.95 2.11 0 6 -13 26.18 1.29 0 -6 -13 26.18 1.2 0 -6 14 111.72 5.56 0 6 14 145.88 4.74 0 6 14 150.23 7.16 0 -6 -14 112.56 4.42 0 6 -14 138.45 3.79 0 -6 -14 128.83 3.6 0 6 15 3.75 2.25 0 -6 -15 0.75 0.6 0 6 -15 2.76 0.75 0 -6 -15 1.83 0.83 0 6 -15 0.66 1.09 0 6 15 1.72 1.56 0 6 16 15.68 1.91 0 6 -16 13.69 1.15 0 -6 -16 12.46 1 0 -6 -16 11.72 1.42 0 6 -16 16.08 1.92 0 6 16 12.98 2.9 0 6 17 578.26 16.2 0 6 17 444.1 11.06 0 6 -17 445.88 10.41 0 -6 -17 399.68 10.09 0 -6 -17 338.2 11.14 0 6 -17 488.8 12.56 0 6 17 437.84 14.37 0 -6 18 152.87 8.3 0 6 18 144.27 7.53 0 6 18 111.63 3.97 0 6 -18 121.63 3.6 0 -6 -18 104.42 3.28 0 -6 -18 86.27 4 0 6 -18 129.2 5.15 0 6 18 114.57 6.36 0 6 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197.99 5.3 0 -8 -13 203.35 5.2 0 8 -14 106.39 3.24 0 -8 -14 105.55 3.11 0 -8 14 97.42 5.44 0 8 14 128.23 6.8 0 8 14 125.3 4.48 0 8 -14 138.63 4.71 0 8 14 155.05 6.73 0 8 -15 7 0.8 0 -8 -15 5.7 0.65 0 -8 15 7.75 1.85 0 8 15 9.61 2.57 0 8 15 8.4 1.8 0 8 -15 8.95 1.38 0 -8 15 12.43 2.9 0 8 15 10.42 2.6 0 -8 16 42.26 4.39 0 -8 -16 36.23 1.5 0 8 -16 37.37 1.64 0 8 16 42.59 2.64 0 8 -16 48.49 2.77 0 8 16 41.3 4.15 0 8 -17 177.18 4.98 0 8 17 193.32 5.91 0 8 17 171.95 8.16 0 8 18 57.12 2.74 0 8 -18 57.34 2.12 0 8 19 23.89 1.75 0 8 -19 28.13 1.39 0 8 -20 6.09 0.71 0 8 -20 7.08 0.82 0 8 20 5.47 1.02 0 8 -21 6.38 0.69 0 8 21 5.31 0.81 0 8 22 14.72 1.11 0 8 23 0.63 0.59 0 8 24 21.03 0.8 0 -10 0 943.19 22.7 0 -10 -1 789.59 18.97 0 -10 1 754.34 18.99 0 -10 2 1.2 1.16 0 -10 -2 0.89 1 0 -10 -3 235.16 7.15 0 -10 3 242.97 7.51 0 -10 4 31.52 3.45 0 -10 -4 27.68 2.01 0 -10 4 24.49 2.18 0 -10 5 215.05 8.84 0 -10 -5 220.64 6.94 0 -10 5 230.96 7.45 0 -10 6 688.68 17.25 0 -10 -6 643.35 16.5 0 10 6 658.94 15.26 0 -10 -7 59.57 1.9 0 -10 7 60.73 4.59 0 -10 -7 67.61 3.31 0 10 7 65.18 2.42 0 -10 -8 64.46 2.02 0 -10 8 66.63 4.87 0 -10 -8 74.14 3.56 0 10 9 366.95 9.74 0 -10 -9 357.42 8.54 0 -10 9 351.46 12.72 0 -10 10 8.19 2.28 0 10 10 10.07 1.77 0 -10 11 8.96 2.36 0 10 11 6.62 1.81 0 -10 12 116.28 6.44 0 10 12 134.77 4.82 0 -10 13 114.44 6.32 0 10 13 129.29 4.74 0 -10 14 61.95 4.51 0 10 14 70.89 3.38 0 10 15 100.07 4.13 0 10 15 97.61 6.1 0 10 16 1.02 2.08 0 10 16 0.54 1.57 0 10 17 104.43 3.99 0 10 18 119.84 4.07 0 10 19 93.12 3.32 0 10 19 109.53 3.45 0 10 20 10.48 1.03 0 10 20 13.16 1.21 0 10 21 45.28 1.78 0 10 22 9.09 0.78 0 10 23 0.44 0.34 0 -12 0 178.04 5.99 0 -12 0 165.18 4.07 0 -12 -1 173.71 5.98 0 -12 1 173.76 6 0 -12 -1 156.84 4.06 0 -12 1 152.88 4.05 0 12 1 176.89 4.67 0 12 -1 172.76 4.67 0 -12 -2 5.6 1.35 0 -12 2 5.14 1.5 0 12 -2 3.89 0.9 0 12 2 3.1 0.85 0 -12 2 4.17 0.57 0 -12 -2 4.63 0.57 0 -12 -3 1.71 1.17 0 -12 3 2.71 1.36 0 12 3 1.36 0.8 0 -12 3 3.72 2.37 0 -12 -3 2.93 0.49 0 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441.74 11.62 -2 8 -11 570.35 12.3 -2 -8 -11 451.92 10.86 2 8 11 523.8 12.18 2 -8 11 413.36 13.67 -2 8 -12 1.49 0.51 -2 8 -12 1.05 0.8 -2 -8 -12 0.06 0.66 2 -8 12 0.32 1.28 2 8 12 0.34 1.37 -2 8 -12 0.56 0.5 -2 -8 -12 0.34 0.46 -2 8 -13 65.3 2.23 -2 -8 -13 68.17 2.18 -2 8 -13 69.92 2.08 2 8 13 71.38 3.18 -2 -8 -13 60.15 2.72 2 8 13 71.89 4.85 -2 8 -14 48.38 1.86 -2 -8 -14 48.38 1.78 2 8 14 50.95 2.76 -2 8 -14 50.5 1.67 2 8 14 46.92 4.12 -2 8 -14 55.03 2.77 -2 8 -15 2.21 1.09 2 8 15 2.95 1.94 -2 -8 -15 1.59 0.57 -2 8 -15 1.61 0.67 -2 8 -15 3.05 1.07 2 8 15 2.06 1.47 -2 -8 -16 8.09 0.79 -2 8 -16 7.53 0.87 -2 8 -16 7.35 1.27 -2 8 -16 10.45 1.39 2 8 16 9.34 1.52 -2 8 -17 31.06 1.52 2 8 17 28.23 1.88 -2 -8 -18 3.9 0.47 -2 8 -18 3.48 0.74 2 8 18 2.42 0.99 -2 8 -19 46.99 1.81 -2 8 -19 48.6 1.73 -2 8 -20 10.48 0.85 -2 8 -20 11.05 0.83 -2 8 -21 10.76 0.74 -2 8 -21 9.92 0.7 2 8 22 35.57 1.41 2 8 23 4.2 0.46 -2 10 22 0.53 0.54 -2 10 21 8.78 1.01 -2 10 21 8.05 0.97 -2 10 20 28.94 1.67 -2 10 20 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22 1 17.31 1.11 -4 -22 -1 14.78 0.69 4 22 2 5.4 0.8 -4 -22 -2 4.79 0.45 4 22 3 2.76 0.71 -4 -22 -3 2.38 0.37 4 22 4 6.22 0.66 -5 -1 26 10.12 1.14 -5 1 26 11.62 1.06 5 1 -26 11.45 0.7 -5 -1 26 14.06 0.62 -5 1 26 15.27 0.6 5 1 -25 26.7 1.2 -5 1 25 28.51 1.07 5 1 -24 -0.18 0.65 -5 1 24 -0.86 0.59 -5 -1 24 -0.87 0.63 5 1 -23 16.86 1.19 -5 1 23 16.05 1.04 -5 -1 23 17.55 1.1 5 1 -22 28.36 1.59 5 1 -21 0.46 0.88 -5 1 21 1.39 1.23 -5 1 20 127.75 8.92 -5 -1 20 122.92 8.79 5 1 -20 119.5 3.85 -5 1 20 114.32 4.1 -5 1 19 10.61 1.51 -5 -1 19 10.7 1.5 5 1 -19 10.55 1.17 -5 -1 19 8.92 4.2 -5 1 19 10.04 4.13 -5 -1 18 0.73 1.2 -5 1 18 0.96 1.32 -5 1 18 -2.27 2.35 -5 -1 18 2.77 3.27 -5 -1 17 215.57 6.17 -5 1 17 236.79 9.5 -5 -1 17 230.86 11.12 -5 -1 16 10.01 1.39 -5 1 16 12.44 1.57 -5 -1 16 11.44 3.43 -5 1 16 10.77 2.63 -5 -1 16 8.98 2.69 -5 -1 15 368.91 9.62 -5 -1 15 425.39 12.99 -5 1 15 417.79 13.17 -5 1 15 371.51 9.77 -5 -1 15 415.67 14.52 -5 -1 14 194.62 5.55 -5 -1 14 225.04 8.36 -5 1 14 217.9 8.31 -5 1 14 193.34 5.7 -5 -1 14 222.96 9.25 -5 -1 13 113.67 3.62 -5 1 13 117.03 3.79 -5 -1 13 124.81 6.5 -5 1 13 136.34 6.06 -5 -1 13 128.59 5.84 -5 -1 12 2.37 2.29 -5 -1 11 376.49 12.13 -5 -1 10 105.92 5.35 -5 -1 9 4120.3 93.42 -5 -1 9 4131.7 92.22 -5 -1 8 15.63 1.71 -5 1 8 13.03 1.77 -5 -1 8 13.3 2.58 -5 -1 7 7.86 2.19 -5 1 7 7.73 1.41 -5 -1 7 9.22 1.39 -5 -1 6 58.35 2.59 -5 -1 6 57.82 3.62 -5 -1 5 37.4 1.9 -5 -1 5 35.91 3.02 -5 -1 4 33.03 1.8 -5 -1 4 29.2 2.73 -5 -1 3 55.12 3.34 -5 -1 3 55.42 2.44 -5 -1 2 1108.76 24.78 -5 1 2 1147.25 25.26 -5 -1 2 1208.19 26.9 -5 -1 2 1160.45 25.6 -5 -1 1 161.42 5.24 -5 -1 1 153.49 5.22 -5 -1 1 170.58 4.43 -5 -1 1 161.56 4.31 -5 -1 0 7.9 1.39 -5 -1 0 8.71 0.65 5 -1 0 4.75 0.27 -5 -1 0 5.65 0.72 -5 -1 -1 4160.28 91.46 -5 -1 -1 4200.08 91.47 -5 -1 -1 4149.41 92.4 -5 -1 -2 486.12 11.5 -5 -1 -2 490.86 11.49 -5 -1 -3 4.09 0.66 -5 -1 -3 1.95 0.55 5 1 4 110.01 3 -5 -1 -4 113.95 3.37 -5 -1 -4 115.78 3.4 5 1 5 3.88 0.62 -5 -1 -5 2.62 0.65 5 1 6 1026.23 24.45 -5 -1 -6 1142.86 24.65 5 1 7 2.1 0.73 -5 -1 -7 1.4 0.65 5 1 8 1.06 0.79 -5 -1 -8 0.65 0.64 5 1 9 2012.7 44.99 -5 -1 -9 1958.57 44.65 -5 1 -10 137.44 3.94 -5 1 -10 144.26 4.88 -5 -1 -10 135.34 4.77 -5 -1 -10 159.75 3.87 -5 1 -10 161.65 3.88 -5 1 -11 97.07 2.9 -5 -1 -11 86.38 3.6 -5 1 -11 91.44 3.69 -5 1 -12 31.07 1.44 -5 -1 -12 33.69 1.26 -5 -1 -12 25.87 1.94 -5 1 -12 27.22 2.02 -5 1 -12 34.27 1.34 -5 -1 -13 47.37 1.6 -5 -1 -13 39.54 2.46 -5 1 -13 40.35 2.5 -5 1 -13 44.85 1.85 -5 -1 -14 15.6 1.66 -5 1 -14 16.01 1.7 -5 -1 -14 18.74 0.95 -5 1 -14 18.39 1.23 -5 -1 -15 90.74 4.19 -5 1 -15 97.21 4.33 -5 -1 -15 92.64 4.24 -5 1 -16 51.9 1.78 -5 -1 -16 35.66 2.6 -5 1 -16 36.87 2.71 -5 1 -16 52.69 2.19 -5 -1 -16 41.34 2.72 -5 -1 -17 1.25 0.99 -5 1 -17 0.59 1.05 -5 -1 -17 1.13 0.93 -5 1 -17 2.35 0.96 -5 1 -18 11.25 1.21 -5 -1 -19 279.71 7.25 -5 1 -19 297.39 7.33 -5 1 -20 16.79 1.03 -5 -1 -20 15.38 0.95 -5 1 -21 33.63 1.4 -5 -1 -21 33.35 1.36 -5 1 -22 8.63 0.88 -5 -1 -22 9.74 0.65 -5 1 -23 0.14 0.44 -5 -1 -23 0.08 0.28 -5 1 -23 -0.16 0.41 5 3 -26 21.78 0.88 -5 3 26 22.22 0.71 -5 -3 26 21.28 1.24 5 3 -25 39.02 1.46 5 -3 -25 35.73 1.37 -5 3 25 41.32 1.27 -5 -3 25 40.9 2.08 -5 -3 24 3.73 0.62 -5 3 24 3 0.53 5 3 -24 3.28 0.68 5 -3 -24 2.61 0.61 -5 3 23 11.49 0.83 5 3 -23 12.61 1.04 5 -3 -23 10.87 0.96 -5 3 22 51.49 2.4 -5 3 22 50.67 1.83 5 3 -22 55.07 2.19 5 -3 -22 51.69 2.04 -5 3 21 6.58 1.47 5 3 -21 7.98 1.11 5 -3 -21 6 0.89 -5 3 20 107.74 4.03 -5 3 20 114.99 8.19 -5 -3 20 128.54 9.05 -5 3 20 114.6 6.62 5 -3 -20 111.98 3.59 5 3 -20 124.62 3.84 -5 3 19 97.99 3.86 5 -3 -19 101.94 3.36 5 3 -19 112.3 3.57 -5 3 19 109.26 8.11 -5 3 19 106.16 6.45 -5 -3 18 1 3.67 -5 3 18 0.54 3.39 -5 3 18 4.83 2.62 -5 3 18 1.27 1.47 -5 3 17 490.94 17.49 -5 -3 17 469.57 17.24 -5 3 17 445.81 14.82 -5 -3 16 376.85 14.45 -5 3 16 395.2 14.66 -5 3 16 347.41 9.5 -5 3 16 377.96 12.86 -5 -3 16 347.2 9.16 -5 -3 15 26.04 4.24 -5 3 15 26.53 4.04 -5 3 15 34.89 3.71 -5 3 15 25.04 2.03 -5 -3 15 22.78 1.65 -5 3 14 5.38 2.87 -5 -3 14 8.07 2.87 -5 3 14 5.48 1.47 -5 -3 14 4.54 1.08 -5 3 14 3.48 2.43 -5 3 13 218.4 9.19 -5 -3 13 216.45 8.95 -5 3 13 195.14 5.8 -5 3 13 220.4 8.3 -5 -3 13 194.2 5.44 -5 3 12 2.72 1.13 -5 -3 12 3.82 0.88 -5 3 12 3.52 2.55 -5 -3 12 4.16 2.32 -5 -3 12 3.97 1.58 -5 -3 11 1296.59 33.45 -5 -3 11 1267.01 32.4 -5 -3 10 311.76 10.84 -5 -3 10 310.84 9.98 -5 -3 9 544.54 16.12 -5 -3 9 552.37 15.12 -5 3 8 702.78 18.23 -5 -3 8 669.49 17.8 -5 -3 7 1180.89 30.67 -5 3 7 1348.36 31.29 -5 3 6 4.02 2.18 -5 -3 6 1.46 1.84 -5 3 5 218.59 7.45 -5 -3 5 190.63 6.97 -5 -3 4 363.28 8.83 5 -3 -4 289.85 7.42 -5 3 4 328.8 9.56 -5 -3 4 291.09 9.17 -5 3 4 315.26 7.8 -5 -3 4 344.38 7.77 -5 -3 3 86.96 3.17 5 -3 -3 83.34 2.18 -5 3 3 59.46 2.23 -5 -3 3 66.22 2.23 -5 -3 3 75.52 2.39 -5 -3 3 82.27 3.65 -5 3 3 84.74 3.7 -5 -3 2 1946.85 41.21 -5 3 2 1871.5 41.23 -5 -3 2 1780.9 42.51 -5 3 2 1920.02 42.71 -5 3 2 1957.17 42.65 -5 -3 2 1801.96 42.5 -5 -3 2 1841.15 41.29 -5 -3 2 1763.5 41.99 -5 3 1 2867.03 62.37 -5 -3 1 2877.51 62.82 -5 -3 1 2906.98 62.04 -5 3 1 3036.31 63.5 -5 -3 1 2784.49 63.2 -5 -3 1 2882.36 62.16 5 -3 -1 2684.56 61.92 -5 -3 1 2794.67 63.2 -5 -3 0 12.85 0.76 5 -3 0 14.42 0.77 -5 -3 0 15.06 1.15 -5 3 0 15.47 0.95 -5 -3 0 12.6 0.94 -5 -3 0 12.16 1.43 -5 3 0 14.01 1.57 -5 -3 -1 179.61 5.46 -5 -3 -1 231.39 5.63 -5 3 -1 239.82 5.62 -5 -3 -1 228.46 5.6 -5 3 -1 245.52 5.62 -5 -3 -1 193.27 5.27 -5 -3 -2 1413.03 32.5 -5 -3 -2 1431.16 32.62 -5 3 -2 1473.85 32.54 -5 -3 -2 1489.86 32.64 -5 3 -2 1491.92 32.55 5 -3 3 229.31 6.21 -5 -3 -3 238.1 6.2 -5 3 -3 250.87 6.18 -5 -3 -3 244.14 6.19 -5 3 -3 243.08 6.18 5 -3 4 1805.8 41.68 -5 -3 -4 1807.03 41.76 -5 3 -4 1900.63 41.77 -5 -3 -4 1944.2 41.81 -5 3 -4 1934.31 41.73 -5 -3 -5 9.66 0.88 -5 3 -5 11.34 0.91 -5 -3 -5 9.46 0.88 -5 3 -5 9.58 0.9 -5 -3 -6 314.93 7.85 5 3 6 313.19 8.07 -5 -3 -6 308.92 7.8 -5 3 -6 329.07 7.84 5 3 7 688.3 16.67 -5 3 -7 710.79 16.28 -5 -3 -7 665.49 16.2 5 3 8 394.55 10.47 -5 -3 -8 383.5 9.95 -5 3 -8 405.71 10.04 5 3 9 1392.98 31.3 -5 -3 -9 1297.55 30.56 -5 3 -9 1442.95 30.79 -5 3 -9 1245.67 29.62 -5 -3 -9 1388.74 29.66 5 3 10 130.18 4.82 -5 3 -10 137.21 3.35 -5 3 -10 112.49 3.4 -5 -3 -10 123.92 3.44 -5 -3 -10 121.32 4.21 -5 3 -10 135.08 4.4 -5 3 -11 100.62 3.05 -5 -3 -11 103.79 3.03 -5 -3 -11 96.1 3.76 -5 3 -11 99.46 3.89 -5 3 -12 9.68 0.79 -5 3 -12 8.35 0.86 -5 -3 -12 7.5 0.82 -5 3 -13 3.04 0.65 -5 -3 -13 1.07 0.82 -5 3 -13 1.93 1.07 -5 3 -13 0.78 0.68 -5 -3 -13 1.51 0.68 -5 -3 -14 0.48 0.91 -5 3 -14 0.69 0.95 -5 3 -14 1.05 0.6 -5 3 -14 1.17 0.75 -5 -3 -14 1.22 0.74 -5 3 -14 0.92 1.03 -5 -3 -14 0.1 0.84 -5 -3 -15 22.16 1.41 -5 3 -15 22.7 1.45 -5 -3 -15 19.56 1.85 -5 3 -15 22.31 2.08 -5 -3 -15 19.68 1.81 -5 3 -15 23.71 2.07 -5 -3 -16 4.48 1.19 -5 3 -16 6.03 1.32 -5 -3 -16 4.53 1.18 -5 3 -16 6.19 1.38 -5 -3 -16 4.91 0.92 -5 3 -16 4.18 0.97 -5 -3 -17 146.03 5.91 -5 3 -17 174.89 6.48 -5 -3 -17 137.59 5.85 -5 3 -17 171.18 6.44 -5 3 -17 216.4 5.45 -5 -3 -17 207.48 5.26 -5 3 -18 32.52 1.74 -5 -3 -18 31.06 1.65 -5 3 -19 18.78 1.06 -5 -3 -19 15.49 0.94 -5 3 -19 19.7 1.44 -5 -3 -19 19.51 1.29 -5 3 -20 26.4 1.22 -5 3 -20 26.46 1.53 -5 -3 -20 23.92 1.4 -5 -3 -21 25.55 1.19 -5 -3 -21 24.93 1.34 -5 3 -21 26.71 1.47 -5 3 -22 40.75 1.57 -5 -3 -22 36.62 1.42 -5 3 -22 42.14 1.34 -5 -3 -22 35.42 1.21 -5 3 -22 41.83 1.45 -5 3 -23 1.8 0.39 -5 -3 -23 1.03 0.24 -5 3 -23 1.46 0.29 -5 3 -23 1.59 0.39 5 5 -25 27.61 1.04 -5 5 25 27.4 0.81 -5 -5 25 26.1 1.5 5 5 -24 6.75 0.69 -5 5 24 6.98 0.52 -5 -5 24 8.75 0.67 5 5 -23 1.75 0.66 -5 5 23 1.07 0.92 -5 5 23 1.84 0.45 -5 -5 23 1.66 0.56 5 5 -22 38.97 1.74 5 -5 -22 35.18 1.55 -5 5 22 35.83 1.39 -5 5 22 38.54 2.07 5 5 -21 5.25 0.92 5 -5 -21 4.73 0.77 -5 5 21 4.81 1.37 -5 5 21 3.81 0.64 5 5 -20 23.33 1.44 5 -5 -20 18.3 1.23 -5 5 20 18.79 1.85 5 5 -19 0.02 0.8 5 -5 -19 0.99 0.71 -5 -5 19 -2.27 3.5 -5 5 19 1.99 3.13 -5 5 19 1.26 2.28 -5 5 19 0.81 1.46 5 5 -18 2.03 0.84 5 -5 -18 1.15 0.7 -5 5 18 1.75 2.35 -5 5 18 1.68 1.59 -5 5 18 -1.48 3.1 -5 -5 18 -0.38 3.3 -5 5 17 192.42 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16.07 -5 -5 3 675 17.56 5 -5 -3 679.6 16.28 -5 5 3 723.77 17.48 -5 -5 3 661.37 17.28 -5 -5 3 707.74 16.61 -5 5 3 726.03 17.48 5 -5 -2 82 2.59 -5 -5 2 86.15 2.87 -5 -5 2 79.63 3.43 -5 -5 2 78.41 3.22 -5 -5 2 72.65 3.15 -5 5 2 87.51 3.39 -5 -5 1 30.08 1.54 5 -5 -1 32.49 1.42 -5 -5 1 27.36 1.93 -5 -5 1 29.62 1.86 -5 5 1 30.71 1.92 -5 5 0 270.02 6.18 -5 -5 0 245.97 6.37 5 -5 0 229.46 6.18 -5 -5 0 248.14 6.29 -5 -5 0 225.59 6.7 -5 -5 0 217.44 6.84 -5 -5 0 240.75 6.21 -5 5 -1 1289.83 27.94 -5 -5 -1 1326.83 28.15 5 -5 1 1250.05 28.12 5 -5 2 2366.45 55.14 -5 -5 -2 2436.79 55.09 -5 -5 -2 2412.81 55 -5 5 -2 2563.29 54.93 -5 5 -2 2624.18 54.96 -5 5 -3 84.79 2.71 -5 -5 -3 81.57 2.79 -5 -5 -3 81.34 2.79 -5 5 -3 84.93 2.75 -5 -5 -4 40.07 1.76 -5 5 -4 44.7 1.77 -5 -5 -4 42.65 1.78 -5 5 -4 43.96 1.78 -5 5 -5 20.26 1.21 -5 -5 -5 20.1 1.22 -5 5 -5 20.29 1.24 -5 -5 -5 20.76 1.24 5 -5 5 18.96 1.61 -5 5 -6 6.14 0.84 -5 -5 -6 7.7 0.85 5 -5 6 5.7 1.13 -5 -5 -6 8.88 0.89 -5 5 -6 7.24 0.85 -5 -5 -7 20.88 1.35 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89.31 3.18 -7 -9 10 108.43 3.8 -7 9 10 125.23 4.33 -7 9 10 115.3 5.55 -7 -9 10 101.99 5.46 -7 -9 10 134.09 5.27 -7 9 10 116.95 3.78 -7 -9 9 448.45 11.37 -7 9 9 470.94 11.72 -7 9 9 438.58 13.2 -7 -9 9 389.13 13.17 -7 -9 9 538.86 11.43 -7 -9 9 465.77 10.95 -7 -9 9 510.56 13.06 -7 9 9 429.25 13.18 -7 9 9 450.05 11.28 -7 9 8 258 7.03 -7 -9 8 292.22 8.57 7 -9 -8 285.54 7.95 -7 -9 8 304.94 7.09 -7 -9 8 235.75 8.62 -7 9 8 261.7 8.54 -7 -9 8 279.04 6.76 -7 9 8 271.31 8.66 -7 -9 8 233.74 8.53 -7 -9 8 283.9 7.25 -7 9 8 265.64 7.39 -7 -9 8 313.24 10.69 -7 -9 7 37.18 3.52 -7 9 7 28.92 2.32 -7 -9 7 26.67 2.35 -7 9 7 30.05 2.34 -7 -9 7 31.16 2.27 7 -9 -7 35.61 2.09 -7 9 7 28.18 1.82 -7 9 7 32.28 1.61 -7 -9 7 35.2 1.74 -7 -9 7 32.31 1.37 -7 -9 6 576.66 13.41 -7 9 6 559.99 13.91 -7 9 6 565.92 14.95 7 -9 -6 606.46 14.64 -7 -9 6 605.58 15.11 -7 -9 6 618.44 17.45 -7 -9 6 604.22 13.95 -7 9 6 585.72 13.76 -7 -9 5 248.56 7.42 7 -9 -5 245.63 7.01 -7 -9 5 238.98 6.01 -7 9 5 236.73 7.22 -7 -9 5 254.06 6.52 -7 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7.38 -7 9 -7 300.41 7.21 -7 9 -7 287.61 7.1 -7 9 -7 283.64 7.31 -7 9 -8 2.07 0.82 -7 9 -8 2.37 0.64 -7 9 -8 2.88 0.85 7 -9 8 2.22 1.2 -7 9 -9 244.21 6.11 -7 9 -9 238.98 6.12 -7 9 -9 244.94 6.31 7 -9 9 230.51 7.92 7 -9 10 216.17 7.74 -7 9 -10 243.13 7.13 -7 9 -10 210.36 5.88 -7 9 -10 216.12 5.82 -7 9 -10 244.39 6.12 -7 9 -10 259.59 5.69 -7 9 -11 57.59 2.9 -7 9 -11 49.6 1.97 -7 9 -11 54.06 2.16 -7 9 -12 0.81 0.44 -7 9 -12 0.35 0.6 -7 9 -12 -0.27 0.89 -7 9 -13 23.47 1.43 -7 9 -13 22.15 1.2 -7 9 -14 32.41 1.62 -7 9 -14 32.88 1.41 -7 9 -15 59.12 1.96 7 9 15 57.11 2.13 7 9 16 4.14 0.74 -7 9 -16 7.24 0.97 -7 9 -16 5.8 0.89 -7 9 -17 30.27 1.4 -7 9 -17 25.89 1.28 -7 9 -18 120.22 2.9 -7 9 -18 103.62 2.73 -7 9 -19 13.39 0.78 -7 11 23 14.85 0.76 -7 11 22 17.47 1.07 -7 -11 21 0.41 0.4 -7 11 21 0.63 0.62 -7 11 21 1.05 0.87 -7 -11 20 38.52 1.4 -7 11 20 38.78 2.01 -7 11 20 37.38 1.6 -7 -11 19 9.85 0.85 -7 11 19 10.62 1.54 -7 11 19 11.16 1.1 -7 11 18 0.95 0.93 -7 -11 18 0.92 0.68 -7 11 17 32.38 1.8 -7 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1.61 -7 -11 7 11.14 2.85 7 -11 -6 6.64 1.24 -7 -11 6 7.49 1.5 -7 -11 6 6.58 1.2 -7 -11 6 6.59 2.42 -7 11 6 8.6 1.2 -7 11 6 8.41 1.44 -7 -11 6 6.17 0.82 -7 -11 5 285.02 6.88 -7 -11 5 274.27 8.43 7 -11 -5 277.79 8.15 -7 -11 5 301.34 7.57 -7 11 5 264.61 7.23 -7 11 5 262.91 7.33 -7 -11 5 296.28 11.04 7 -11 -4 189.43 6.1 -7 -11 4 199.74 4.95 -7 -11 4 184.91 6.29 -7 11 4 188.32 5.37 -7 11 4 178.19 5.32 -7 -11 4 198.01 8.47 -7 -11 3 1.06 0.63 7 -11 -3 1.52 0.99 -7 -11 3 1.38 0.96 -7 11 3 0.57 0.95 -7 -11 3 1.09 1.07 -7 -11 3 2.06 0.72 -7 -11 3 -0.1 1.89 -7 11 3 1.11 0.95 -7 -11 2 345.27 9.52 7 -11 -2 328.56 9.47 -7 11 2 318 8.55 -7 -11 2 352.52 8.18 -7 11 2 337.45 8.17 -7 -11 2 363.25 11.99 -7 -11 1 36.19 2.32 -7 11 1 40.76 2.03 -7 -11 1 35.75 3.41 -7 11 1 45.14 1.67 -7 -11 1 41.62 1.67 -7 -11 0 149.12 6.64 -7 11 0 136.89 3.86 -7 -11 0 148.89 5.16 7 -11 0 138.6 4.91 -7 -11 0 149.22 3.94 -7 -11 -1 316.64 7.57 -7 -11 -1 289.74 10.22 -7 11 -1 310.62 7.52 7 -11 1 284.43 8.61 -7 -11 -1 326.05 9.05 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11 13 93.4 2.94 -7 11 -14 4.1 0.62 -7 11 -14 2.84 0.83 7 11 14 2.61 0.65 7 11 15 22.72 1.1 -7 11 -15 26.47 1.34 -7 11 -15 25.14 1.07 -7 11 -16 2.96 0.7 -7 11 -17 0.41 0.51 -7 11 -18 9.26 0.71 -7 13 21 14.02 0.87 -7 13 20 47.99 1.9 -7 13 20 47.87 1.64 -7 13 19 15.95 1.04 -7 -13 19 13.72 0.73 -7 13 18 28.97 1.46 -7 -13 18 29.29 1.18 -7 13 17 86.81 2.84 -7 -13 17 83.77 2.51 -7 13 16 0.59 0.91 -7 -13 16 0.3 0.61 -7 -13 15 1.13 0.68 -7 13 15 2.73 1.01 -7 13 14 13.01 1.34 -7 13 14 13.75 1.96 -7 -13 14 11.85 1 -7 -13 13 6.74 0.89 -7 13 13 6.92 1.22 -7 -13 13 7.05 1.6 -7 13 13 8.33 1.92 -7 -13 13 10.47 2.69 -7 -13 12 83.65 4.49 -7 13 12 93.18 3.31 -7 -13 12 94.23 2.94 -7 13 12 94.32 3.9 -7 13 11 6.39 1.19 -7 -13 11 3.31 1.37 -7 -13 11 4.27 1.09 -7 -13 11 4.04 0.8 -7 13 11 3.72 1.65 -7 -13 10 121.49 5.31 -7 -13 10 121.01 4.13 -7 13 10 123.73 4.01 -7 -13 10 125.08 3.61 -7 13 10 125.88 4.56 -7 -13 9 28.04 3.81 -7 -13 9 21.19 2.17 -7 -13 9 24.54 1.71 -7 13 9 24.42 1.72 -7 -13 9 22.31 1.31 -7 13 9 21.1 2 -7 -13 8 132.57 7.56 -7 -13 8 125.96 5.35 7 -13 -8 123.08 4.95 -7 -13 8 133.02 4.39 -7 13 8 134.4 4.26 -7 -13 8 130.45 3.76 -7 13 8 136.27 4.61 -7 -13 7 2.87 2.58 7 -13 -7 7.14 1.32 -7 -13 7 4.54 1.43 -7 -13 7 7.22 1.26 -7 13 7 6.08 1.21 -7 13 7 6.39 1.56 -7 -13 7 5.63 0.84 7 -13 -6 0.82 0.97 -7 -13 6 1.4 1.14 -7 -13 6 1.9 1.15 -7 -13 6 1.75 2.24 -7 13 6 2.26 1.15 -7 13 6 3.78 1.41 -7 -13 6 2.1 0.78 -7 -13 5 344.48 8.35 -7 -13 5 348.44 13.13 -7 13 5 346.33 8.88 -7 -13 5 359.71 9.14 -7 13 5 339.38 8.92 -7 -13 5 313.03 10.02 7 -13 -5 325.32 9.8 -7 -13 5 341.75 8.35 7 -13 -4 6.82 1.36 -7 -13 4 7.74 1.41 -7 13 4 9.37 1.42 -7 -13 4 8.99 2.67 -7 -13 4 10.97 1.45 -7 13 4 7.1 1.29 -7 13 4 7.87 0.83 -7 -13 4 8.12 1.53 -7 -13 4 9.47 1.01 -7 -13 3 66.3 2.22 7 -13 -3 54.92 3.08 -7 -13 3 58.21 3.14 -7 13 3 62.59 2.6 -7 13 3 56.94 2.61 -7 -13 3 67.81 5.27 -7 13 3 60.83 2.12 -7 -13 2 131.88 3.66 -7 13 2 129.35 4 7 -13 -2 111.15 4.74 -7 -13 2 122.59 4.84 -7 13 2 123.6 4.17 -7 -13 2 124.31 6.89 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419.83 10.13 -8 -8 16 1.52 0.99 -8 8 16 2.43 2.46 -8 -8 16 5.24 2.66 -8 8 16 2.66 1.01 -8 8 16 2.1 0.5 -8 -8 16 3.31 0.62 -8 -8 16 2.59 1.51 -8 8 16 1.46 1.32 -8 8 15 257.51 7.32 -8 8 15 276.79 10.81 -8 -8 15 283.23 7.42 -8 8 15 228.1 7.13 -8 -8 15 237.66 9.84 -8 8 15 200.33 9.43 -8 -8 15 191.91 9.58 -8 8 15 219.6 6.58 -8 -8 15 202.19 6.58 -8 8 15 215.51 6.3 -8 -8 15 263.77 5.83 -8 8 14 53.35 2.91 -8 8 14 61.57 4.94 -8 -8 14 60.47 2.74 -8 8 14 45.1 2.51 -8 -8 14 43.87 2.43 -8 -8 14 37.11 4.23 -8 8 14 50.03 2.48 -8 8 14 44.86 4.35 -8 -8 14 50.86 4.28 -8 8 14 46.22 2.17 -8 -8 14 53.32 1.68 -8 8 13 15.84 1.34 -8 8 13 20.14 3.2 -8 -8 13 14.52 1.63 -8 -8 13 13.28 3.07 -8 8 13 16.2 1.61 -8 -8 13 15.77 1.45 -8 8 13 12.01 1.35 -8 -8 13 19.11 3.01 -8 8 13 15.14 2.01 -8 -8 13 16.2 0.83 -8 -8 13 13.54 1.95 -8 8 12 0.63 2.19 -8 -8 12 0.54 2.12 -8 -8 12 1.53 1.17 -8 8 12 2.42 1.19 -8 -8 12 1.8 0.8 -8 8 12 0.86 0.8 -8 8 12 1.32 0.92 -8 -8 12 0.97 1.32 -8 -8 12 1.93 0.44 -8 8 12 1.89 1.42 -8 -8 11 3.93 0.98 -8 8 11 3.71 1.53 -8 -8 11 4.42 0.49 -8 -8 11 4.4 0.88 -8 8 11 4.03 0.86 -8 8 11 4.33 0.91 -8 -8 11 4.81 1.4 -8 -8 11 6.33 2.38 -8 8 11 4.42 2.29 -8 8 10 45.9 2 -8 -8 10 53.26 2.22 -8 8 10 43.96 2.22 -8 -8 10 49.14 1.46 -8 8 10 49.41 3.95 -8 -8 10 39.84 3.59 -8 -8 10 42.04 2.06 -8 -8 10 50.01 2.93 -8 -8 10 46.89 3.9 -8 8 10 44.79 2.41 -8 -8 9 186.77 7.67 -8 8 9 174.36 7.21 -8 8 9 163.48 5.08 -8 8 9 176.41 7.2 -8 -8 9 154.57 6.89 -8 8 9 159.83 5.08 -8 -8 9 201.31 5.16 -8 -8 9 174.47 4.94 -8 -8 9 171.36 5.9 -8 8 9 167.61 4.77 -8 -8 8 11.56 2.3 -8 -8 8 8.63 0.89 -8 8 8 10.66 1.03 -8 8 8 8.07 1.29 -8 -8 8 11.06 1.12 -8 8 8 9.57 2.08 -8 -8 8 8.84 1.99 -8 -8 8 9.61 0.84 -8 8 8 8.52 1.02 -8 8 8 7.19 2 -8 -8 8 9.49 1.41 -8 -8 7 485.15 12.39 8 -8 -7 479.1 11.89 -8 8 7 502.42 13.64 -8 -8 7 425.16 13.16 -8 -8 7 498.34 11.47 -8 -8 7 491.89 14.49 -8 8 7 442.8 11.36 -8 -8 7 432.8 13.23 -8 8 7 493.15 13.66 -8 -8 6 286 9.57 -8 8 6 341.97 10.07 -8 -8 6 304.31 9.71 8 -8 -6 327.38 8.54 -8 -8 6 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1.53 -8 -12 10 6.84 2.43 -8 12 9 742.85 17.62 -8 -12 9 768.55 17.25 -8 -12 9 678.54 19.05 -8 -12 9 765.87 17.92 -8 12 9 731.53 16.9 -8 12 9 780.81 18.08 -8 -12 9 817.73 22.97 -8 12 8 9.29 1.31 -8 -12 8 8.98 1.03 -8 -12 8 7.58 1.5 -8 -12 8 6.82 1.34 -8 12 8 8.3 0.71 -8 12 8 10.99 1.66 -8 -12 8 8.03 2.72 -8 12 7 194.72 5.61 -8 -12 7 198.67 5.23 -8 -12 7 182.17 6.62 8 -12 -7 181.26 6.26 -8 -12 7 204.81 5.93 -8 12 7 204.45 4.93 -8 -12 7 199.6 9.1 -8 12 7 195 5.81 -8 -12 6 195.51 5.04 8 -12 -6 178.94 6.11 -8 -12 6 180.28 6.38 -8 -12 6 206.21 5.76 -8 12 6 181.97 5.42 -8 12 6 183.35 5.52 -8 -12 6 194.79 8.85 -8 -12 5 2.92 0.82 8 -12 -5 2.87 1.05 -8 -12 5 3.04 1.03 -8 -12 5 2.46 2.15 -8 -12 5 3.39 1.16 -8 12 5 3.97 1.2 -8 -12 5 3.29 1.21 -8 -12 5 2.86 0.8 -8 12 5 4.48 1.2 -8 -12 4 22.05 1.3 -8 -12 4 19.9 1.76 -8 -12 4 21.18 3.13 8 -12 -4 20.92 1.8 -8 -12 4 20.09 1.98 -8 -12 4 21.41 1.74 -8 12 4 21.9 1.62 -8 12 4 20.53 1.56 -8 -12 4 21.26 1.27 -8 12 3 3.65 1.04 -8 -12 3 3.65 1.09 8 -12 -3 2.29 1 -8 -12 3 4.66 2.15 -8 -12 3 3.65 0.8 -8 12 3 3.16 0.75 -8 12 3 5.07 1.18 8 -12 -2 125.07 4.72 -8 -12 2 126.02 4.69 -8 -12 2 141.37 3.74 -8 -12 2 138.22 6.82 -8 12 2 128.47 3.65 -8 12 2 113.3 4.05 -8 -12 1 19.09 1.75 8 -12 -1 17.03 1.73 -8 -12 1 19.81 2.82 -8 12 1 17.59 1.12 -8 -12 1 21.54 1.24 -8 -12 0 452.6 10.72 -8 12 0 454.18 10.7 -8 -12 0 423.17 13.95 -8 -12 0 414.02 11.92 -8 12 0 462.19 10.41 -8 -12 -1 13.52 2.27 -8 12 -1 18.01 1.14 -8 -12 -1 14.77 1.68 -8 -12 -1 18.24 1.21 -8 12 -1 19.3 0.94 -8 12 -2 191.59 5.11 -8 -12 -2 208.06 5.31 -8 12 -2 213.66 5.32 -8 -12 -2 200.36 7.84 -8 -12 -2 203.79 6.63 -8 12 -2 199.94 4.99 -8 12 -3 77.58 2.5 -8 -12 -3 78.1 2.55 -8 12 -3 76.4 2.21 -8 12 -4 26.37 1.36 -8 12 -4 25.75 1.12 -8 -12 -4 27.14 1.43 -8 12 -5 127.39 3.63 -8 12 -5 121.31 3.37 -8 12 -6 13.9 1.01 -8 12 -6 13.38 0.85 -8 -12 -6 12.47 1.1 -8 12 -6 13.08 1.26 -8 12 -7 1.55 0.67 8 12 7 0.53 1.17 -8 12 -7 0.56 0.95 -8 12 -7 1.84 0.54 -8 12 -8 3.19 0.74 -8 12 -8 3.28 0.98 -8 12 -9 239.41 6.03 -8 12 -9 241.06 6.31 -8 12 -10 56.24 2.06 -8 12 -10 58.32 2.27 -8 12 -11 124.12 3.66 -8 12 -11 121.4 3.44 -8 12 -12 40.89 1.76 -8 12 -12 39 1.72 -8 12 -13 2.27 0.81 -8 12 -13 2.51 0.58 -8 12 -13 2.36 0.81 -8 12 -14 42.45 1.66 -8 12 -14 40.71 1.44 -8 12 -15 10.58 0.86 -8 12 -16 16.45 0.94 -8 -14 20 36.47 1.16 -8 14 18 4.35 0.71 -8 -14 18 2.99 0.48 -8 14 18 4.56 1.01 -8 14 17 0.64 0.71 -8 -14 17 0.84 0.51 -8 14 17 1.23 1.09 -8 14 16 0.62 0.78 -8 -14 16 -0.05 0.56 -8 14 16 1.02 1.23 -8 14 15 5.62 0.96 -8 -14 15 5.17 0.72 -8 14 15 5.76 1.48 -8 14 14 0.79 0.93 -8 -14 14 1.47 0.64 -8 14 14 0.82 1.46 -8 -14 13 34.97 1.57 -8 14 13 40.08 2.43 -8 14 13 37.06 1.89 -8 14 12 9.9 1.68 -8 -14 12 10.6 1 -8 14 12 10.45 1.28 -8 -14 11 174.16 8.67 -8 14 11 172.65 4.97 -8 -14 11 168.43 4.55 -8 14 11 180.49 5.46 -8 -14 10 122.23 7.11 -8 -14 10 121.65 3.99 -8 14 10 112.37 3.79 -8 -14 10 116.93 3.43 -8 14 10 120.05 4.2 -8 -14 9 120.08 7.09 -8 -14 9 121.92 4.06 -8 14 9 119.14 3.88 -8 14 9 116.55 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2 211.17 9.21 -8 -14 1 104.15 3.12 8 -14 -1 86.08 4.02 -8 14 1 108.33 3.08 -8 -14 1 90.21 4.02 -8 -14 1 103.85 5.95 -8 -14 0 36.44 1.61 -8 -14 0 37.93 1.71 8 -14 0 30.48 2.3 -8 14 0 32.93 1.51 -8 -14 0 38.64 3.61 -8 -14 0 32.25 2.3 -8 -14 -1 17.07 1.72 -8 -14 -1 20.82 1.33 -8 -14 -1 20.93 1.26 8 -14 1 12.6 2.78 8 -14 1 15.91 1.74 -8 -14 -1 16.62 2.6 -8 14 -1 20.04 1.16 -8 -14 -2 111.18 3.37 -8 -14 -3 117.14 3.5 -8 14 -3 119.18 3.44 -8 -14 -4 10.67 1.07 -8 14 -4 9.77 0.82 -8 14 -4 11.64 0.94 -8 14 -5 34.05 1.45 -8 -14 -5 33.8 1.55 -8 14 -6 4.17 0.72 8 14 6 3.87 1.4 -8 -14 -6 4.72 0.91 -8 14 -6 3.98 0.72 8 14 7 192.01 5.84 -8 14 -7 177.97 5.12 -8 14 -8 42.48 1.71 -8 14 -8 47.23 1.65 -8 14 -9 93.81 2.87 -8 14 -10 8.71 0.79 -8 14 -10 7.28 0.86 -8 14 -11 37.2 1.4 -8 14 -11 36.85 1.54 -8 14 -12 3.18 0.53 -8 14 -12 4.22 0.71 -8 14 -13 31.56 1.09 -8 14 -13 29.54 1.29 -8 14 -14 4.55 0.62 -8 14 -15 1.06 0.42 -8 16 18 1.42 0.52 -8 -16 18 1.2 0.32 -8 16 17 1.22 0.65 -8 -16 17 1.42 0.42 -8 -16 16 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-5 8 555.88 12.45 -11 -5 7 2.77 1.5 -11 -5 7 4.1 0.85 -11 -5 7 2.61 2.12 -11 5 7 4.72 2.65 -11 -5 7 5.11 0.72 -11 -5 7 1.58 2.01 -11 5 7 3.7 2.47 -11 5 7 3.11 0.58 -11 -5 7 5.03 0.56 -11 -5 6 698.26 17.6 -11 -5 6 673.37 15.51 -11 -5 6 676.31 18.84 -11 5 6 810.86 20.12 -11 -5 6 685.73 15.17 -11 5 6 659.62 15.08 -11 5 6 814.59 20.31 -11 5 6 616.64 15.23 -11 -5 6 652.96 18.69 -11 -5 5 549.82 12.56 -11 5 5 521.1 12.26 -11 -5 5 551.38 12.23 -11 -5 5 541.24 15.77 -11 5 5 456.21 12.29 -11 -5 5 589.06 12.57 -11 5 5 653.64 16.99 -11 -5 5 542.76 14.34 -11 5 5 531.98 12.15 -11 5 4 12.39 0.85 -11 -5 4 12.2 0.83 -11 5 4 14.66 0.91 -11 -5 4 15.32 1.06 -11 5 4 10.92 1.01 -11 -5 4 12.08 1.1 -11 5 4 11.87 0.78 -11 -5 4 13.19 1.54 -11 -5 4 10.11 2.3 -11 5 4 13.38 2.8 -11 5 3 3.52 0.62 -11 -5 3 7.57 0.67 -11 5 3 4.57 0.69 -11 -5 3 2.58 0.72 -11 -5 3 1.81 0.82 -11 5 3 3.43 0.84 -11 5 3 3.64 0.5 -11 -5 3 2.42 1.93 -11 5 3 2.42 2.18 -11 -5 3 6.4 1.14 -11 -5 2 637.17 17.2 -11 -5 2 640.6 15.02 -11 5 2 586.59 13.69 -11 -5 2 655.63 14.07 -11 5 2 524.94 13.8 -11 5 2 553.26 13.74 -11 5 2 586.21 13.59 -11 -5 2 618.6 13.67 -11 5 2 624.05 13.87 -11 -5 2 639.07 13.95 -11 5 2 542.85 13.86 -11 -5 2 647.85 14.12 -11 -5 2 640.5 13.72 -11 5 1 52.63 1.72 -11 5 1 49.38 1.74 -11 5 1 44.33 1.88 -11 -5 1 65.61 2.18 -11 5 1 50.23 1.81 -11 -5 1 55.1 1.79 -11 5 1 48.09 1.85 -11 -5 1 54.32 1.96 -11 5 1 48.76 1.94 -11 -5 1 58.16 1.58 -11 5 1 52.62 1.57 -11 -5 1 64 2.2 -11 5 0 105.53 2.76 -11 -5 0 109.54 2.74 -11 5 0 106.8 3.17 -11 5 0 101.89 3.03 -11 5 0 111.51 2.93 -11 -5 0 113.33 3.19 -11 5 0 111.35 3.15 -11 5 0 106.9 2.98 -11 5 0 100.54 3.16 -11 -5 0 120.09 3.4 -11 -5 0 112.15 2.98 -11 -5 0 101.52 2.91 -11 5 -1 36.08 1.55 -11 -5 -1 35.4 1.53 -11 5 -1 38.8 1.54 -11 5 -1 30.82 1.5 -11 -5 -1 39.55 1.71 -11 5 -1 33.75 1.34 -11 5 -1 31.28 1.38 -11 5 -1 31.64 1.32 -11 -5 -1 36.56 1.37 -11 5 -1 33.9 1.28 -11 5 -2 1.47 0.51 -11 -5 -2 1.85 0.65 -11 5 -2 1.01 0.66 -11 -5 -2 3.82 0.8 -11 5 -2 2.33 0.64 -11 5 -2 2.7 0.65 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63.22 2.29 -11 -5 -7 62.82 2.04 -11 5 -7 67.8 2.09 -11 -5 -7 57.71 3.19 -11 5 -7 68.73 3.42 -11 5 -7 59.89 2.32 -11 -5 -7 62.85 2.39 -11 5 -8 337.06 8.21 -11 -5 -8 321.05 8.07 -11 -5 -8 332.15 8.07 -11 5 -8 370.5 8.14 -11 -5 -8 318.46 9.88 -11 5 -8 373.3 10.24 -11 5 -8 315.21 8.43 -11 -5 -8 353.08 8.56 -11 5 -9 124.8 3.57 -11 5 -9 116.93 3.77 -11 -5 -9 128.85 3.84 -11 -5 -9 118.86 3.39 -11 5 -9 135.02 3.47 -11 -5 -9 114.77 4.85 -11 5 -9 128.17 5.11 -11 -5 -9 122.09 3.37 -11 5 -10 61.69 2.28 -11 5 -10 56.86 2.31 -11 -5 -10 58.86 2.3 -11 -5 -10 54.46 1.89 -11 5 -10 61.88 2.01 -11 5 -10 56.52 2.06 -11 -5 -10 51.85 3.06 -11 5 -10 58.75 3.27 -11 5 -11 21.22 1.3 -11 5 -11 20 1.39 -11 -5 -11 17.91 1.3 -11 -5 -11 16.88 0.99 -11 5 -11 20.73 1.09 -11 5 -11 20.05 1.19 -11 -5 -11 14.35 1.69 -11 5 -11 19.23 1.98 -11 5 -12 309.38 7.97 -11 -5 -12 296.58 7.81 -11 5 -12 375.57 8.03 -11 5 -12 328.52 8.35 -11 -5 -12 334.75 8.29 -11 5 -12 358.6 8.3 -11 5 -13 46.71 1.65 -11 5 -13 49.67 1.91 -11 5 -13 45.04 1.96 -11 -5 -13 45.91 1.87 -11 5 -14 0.72 0.7 -11 5 -14 0.22 0.7 -11 -5 -14 -0.52 0.7 -11 5 -15 3.24 0.72 -11 5 -15 3.13 0.8 -11 -5 -15 2.97 0.72 -11 5 -16 70.38 2.33 -11 5 -17 22.27 1.08 -11 5 -18 9.6 0.6 -11 -7 24 5.79 0.51 -11 -7 23 1.01 0.52 11 7 -23 0.78 0.35 -11 -7 22 0.84 0.9 11 7 -22 0.07 0.45 -11 -7 22 0.51 0.61 -11 7 22 0.49 0.26 -11 -7 21 2.15 1.14 11 7 -21 2.32 0.59 -11 7 21 1.91 0.38 -11 7 21 2.27 1.08 -11 -7 20 85.8 3.22 -11 7 20 85.51 2.33 -11 -7 19 31.05 2.06 -11 7 19 32.7 1.19 -11 7 19 32.75 2 -11 -7 18 75.37 3.29 -11 7 18 84.81 3.32 -11 7 18 77.08 2.38 -11 -7 17 52.15 2.72 -11 7 17 53.41 2.6 -11 -7 17 47.58 4.75 -11 7 17 42.84 4.39 -11 -7 17 66.2 2.97 -11 7 17 66.72 4.83 -11 7 17 59.27 2.8 -11 -7 17 71.87 1.96 -11 7 17 52.96 1.81 -11 7 16 10.9 1.62 -11 -7 16 8.57 1.64 -11 7 16 9.57 1.55 -11 -7 16 9.3 2.94 -11 7 16 9.07 2.86 -11 -7 16 13.51 0.84 -11 -7 16 11.31 1.4 -11 7 16 10.44 1.37 -11 7 16 12.32 2.64 -11 7 15 182.94 8 -11 -7 15 179.11 5.48 -11 7 15 144.99 5.28 -11 7 15 165.72 5.12 -11 7 15 146.79 4.07 -11 -7 15 143.72 4.94 -11 -7 15 130.52 7.61 -11 7 15 163.61 5.02 -11 7 15 151.65 7.95 -11 -7 15 180.61 4.15 -11 7 15 159.82 4.34 -11 7 14 235.4 9.01 -11 -7 14 217.63 6.26 -11 7 14 186.19 6.15 -11 7 14 210.06 5.89 -11 7 14 178.76 8.7 -11 7 14 187.34 4.88 -11 -7 14 180.45 5.73 -11 -7 14 184.33 8.86 -11 7 14 181.54 8.75 -11 7 14 190.68 5.73 -11 7 14 192.06 5.12 -11 -7 14 209.01 4.9 -11 7 13 351.96 8.57 -11 7 13 362.13 13.12 -11 7 13 388.37 9.55 -11 7 13 463.19 13.49 -11 -7 13 444.82 10.15 -11 7 13 355.41 9.94 -11 7 13 373.58 9.48 -11 -7 13 324.64 9.32 -11 -7 13 314 12.61 -11 7 13 351.64 12.97 -11 -7 13 387.28 12.83 -11 -7 12 29.46 3.29 -11 7 12 28.86 1.9 -11 7 12 27.08 1.9 -11 -7 12 35.03 2.02 -11 7 12 27.11 3.56 -11 7 12 35.06 3.44 -11 7 12 31.46 3.77 -11 7 12 30.84 2.02 -11 -7 12 25.72 1.9 -11 -7 12 27.58 3.53 -11 7 12 27.89 1.19 -11 -7 11 133.41 6.36 -11 7 11 119.59 4.33 -11 -7 11 149.41 4.44 -11 7 11 127.96 6.73 -11 7 11 129.93 4.12 -11 -7 11 110.34 3.91 -11 -7 11 106.09 6.25 -11 7 11 154.2 6.59 -11 7 11 121.2 6.7 -11 -7 11 102.81 6.2 -11 7 11 128.63 4.03 -11 7 11 117.1 3.26 -11 -7 10 3.54 0.77 -11 -7 10 4.28 1.18 -11 7 10 3.69 1.11 -11 -7 10 3.68 2.23 -11 7 10 3.52 2.28 -11 7 10 3.82 0.56 -11 -7 10 5.46 2.21 -11 7 10 5.22 2.42 -11 -7 10 4.02 1.72 -11 -7 9 134.21 4.03 -11 7 9 117.96 3.83 -11 -7 9 133.93 6.19 -11 -7 9 106.95 5.93 -11 7 9 131.03 6.57 -11 -7 9 144.03 3.32 -11 7 9 118.21 3.35 -11 7 9 126.74 6.53 -11 -7 9 106.8 5.9 -11 -7 9 128.46 3.6 -11 -7 8 64.28 2.53 -11 -7 8 54.51 4.09 -11 7 8 61.15 4.49 -11 -7 8 62.76 2.15 -11 -7 8 65.06 4.06 -11 7 8 63.41 1.99 -11 7 8 59.41 2.34 -11 7 8 56.45 4.42 -11 -7 8 52.76 4.03 -11 -7 7 21.54 2.69 -11 7 7 18 1.08 -11 -7 7 20.16 1.11 -11 -7 7 20.1 2.66 -11 7 7 19.06 2.99 -11 -7 7 21.57 1.4 -11 -7 7 19.81 2.33 -11 7 7 18.64 0.91 -11 7 6 139.15 3.73 -11 -7 6 140.71 3.73 -11 7 6 145.32 6.69 -11 -7 6 122.18 5.97 -11 -7 6 132.66 4.07 -11 -7 6 125.4 5.59 -11 7 6 135.64 3.52 -11 -7 5 108.35 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141.19 4.01 -11 -7 1 160.08 3.61 -11 7 0 170.82 4.6 -11 -7 0 187.88 4.79 -11 7 0 182.67 4.78 -11 -7 0 175.74 4.89 -11 7 0 152.5 4.66 -11 -7 0 204.64 4.97 -11 -7 0 198.46 4.74 -11 -7 0 190.94 4.67 -11 7 0 155.66 4.71 -11 -7 0 207.95 5.02 -11 7 0 176.09 4.48 -11 7 -1 17.57 0.9 -11 7 -1 16.98 1.13 -11 -7 -1 18.9 1.15 -11 7 -1 20.69 1.18 -11 7 -1 17.28 1.03 -11 -7 -1 22 1.17 -11 7 -2 10.79 0.74 -11 7 -2 8.13 0.89 -11 -7 -2 10.83 1.05 -11 7 -2 8.73 0.87 -11 -7 -2 9.11 0.88 -11 7 -2 10.83 0.84 -11 -7 -2 8.78 0.88 -11 7 -3 0.72 0.67 -11 -7 -3 2.45 0.83 -11 7 -3 3.66 0.78 -11 -7 -3 2.47 0.81 -11 7 -3 1.63 0.65 -11 7 -3 3.03 0.57 -11 -7 -4 630.93 13.78 -11 7 -4 605.14 13.5 -11 -7 -4 580.77 13.46 -11 7 -4 589.52 13.65 -11 7 -4 631.28 15.34 -11 7 -5 215.71 5.6 -11 -7 -5 207.99 5.34 -11 -7 -5 199.61 6.85 -11 7 -5 221.38 5.45 -11 7 -5 206.04 5.45 -11 7 -5 194.25 5.52 -11 -7 -5 228.86 5.72 -11 7 -5 228.93 7.02 -11 -7 -6 1.7 1.01 -11 7 -6 1.76 0.96 -11 7 -6 2.98 0.81 -11 7 -6 2.81 0.84 -11 7 -6 3.11 0.81 -11 -7 -6 3.84 0.85 -11 7 -6 2.19 0.72 -11 -7 -7 191.6 6.79 -11 7 -7 230.11 7.08 -11 7 -7 209.97 5.51 -11 7 -7 212.86 5.65 -11 7 -7 213.86 5.65 -11 7 -7 201.09 5.62 -11 -7 -7 225.29 5.75 -11 7 -7 217.55 5.49 -11 -7 -8 94.05 3.03 -11 7 -8 84.43 2.95 -11 -7 -8 81.25 3.83 -11 7 -8 100.1 4.16 -11 7 -8 89.86 2.84 -11 7 -8 96.6 3.03 -11 7 -8 91.33 3 -11 7 -8 92.83 2.86 -11 7 -8 97.86 2.88 -11 7 -9 -0.48 0.91 -11 -7 -9 0.25 0.77 -11 7 -9 0.23 0.65 -11 7 -9 0.5 0.88 -11 7 -9 0.12 0.72 -11 7 -9 0.29 0.73 -11 -7 -9 0.04 0.71 -11 7 -9 -0.12 0.66 -11 7 -10 56.38 2.13 -11 7 -10 44.43 1.97 -11 7 -10 53.01 2.97 -11 7 -10 46.62 2 -11 -7 -10 49.78 1.99 -11 7 -10 47.23 1.88 -11 7 -11 10.74 1.02 -11 -7 -11 12.59 1.03 -11 7 -11 12.88 1.18 -11 7 -11 11.65 1.02 -11 7 -12 159.33 4.53 -11 7 -12 152.34 4.33 -11 7 -13 51.15 2.01 -11 7 -13 58.26 2.12 -11 7 -13 51.38 1.87 -11 7 -13 59.87 2.15 -11 7 -14 1.92 0.72 -11 7 -14 2 0.83 -11 7 -14 1.37 0.65 -11 7 -15 16.13 1.02 -11 7 -15 16.55 1.1 -11 7 -15 13.5 0.93 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2.38 2.44 -13 5 15 4.04 2.62 -13 5 15 4.06 1.11 -13 5 15 3.02 0.63 -13 5 15 2.02 1.8 -13 -5 15 4.29 1.05 -13 5 15 5.1 1.15 -13 5 15 2.88 2.73 -13 -5 15 3.25 2.55 -13 -5 14 13.61 3.25 -13 5 14 15.7 3.34 -13 -5 14 17.23 1.83 -13 5 14 15.49 1.85 -13 -5 14 21.72 1.74 -13 5 14 16.36 1.61 -13 5 14 16.86 0.94 -13 -5 14 13.46 3.12 -13 5 14 15.36 3.27 -13 5 14 14.94 1.32 -13 5 14 19.69 2.53 -13 -5 13 8.58 2.74 -13 5 13 8.97 2.97 -13 -5 13 10.13 1.62 -13 5 13 12.89 1.72 -13 -5 13 12.32 1.41 -13 5 13 11.18 1.41 -13 5 13 9.77 0.78 -13 -5 13 7.83 2.78 -13 5 13 10.35 3.11 -13 5 13 10.46 1.13 -13 5 13 10.58 2.08 -13 -5 12 10.39 1.67 -13 -5 12 12.12 2.99 -13 5 12 10.15 3 -13 5 12 11.71 1.65 -13 5 12 8.58 1.07 -13 -5 12 12.67 1.39 -13 5 12 7.3 1.2 -13 5 12 7.39 0.72 -13 -5 12 7.86 2.75 -13 5 12 11.91 3.13 -13 5 12 7.72 1.82 -13 5 11 16.45 1.2 -13 -5 11 17.94 3.22 -13 5 11 17.7 1.03 -13 -5 11 23.62 1.04 -13 5 11 21.74 3.64 -13 5 11 19.34 2.21 -13 -5 11 16.95 3.26 -13 5 11 24.44 3.61 -13 -5 11 18.2 1.77 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1.07 -13 5 1 17.63 1.08 -13 -5 1 20.8 0.9 -13 5 1 20.24 0.91 -13 5 1 17.88 1.21 -13 -5 1 21.77 1.3 -13 -5 1 23.5 1.52 -13 5 1 16.03 1.34 -13 5 0 1.72 0.79 -13 -5 0 1.11 0.9 -13 5 0 1.4 0.71 -13 5 0 1.42 0.74 -13 5 0 2.59 0.65 -13 -5 0 0.77 0.73 -13 -5 0 1.06 1.03 -13 5 0 4.16 0.67 -13 5 0 1.62 0.56 -13 -5 0 1.29 0.46 -13 -5 -1 202.29 5.19 -13 5 -1 194.22 5.2 -13 5 -1 184.67 4.92 -13 5 -1 178.88 5 -13 -5 -1 207.44 4.73 -13 5 -1 188.76 4.9 -13 5 -1 188.32 5.17 -13 5 -1 182.62 5.24 -13 -5 -1 212.42 5.49 -13 -5 -2 24.13 1.35 -13 5 -2 25.56 1.44 -13 5 -2 22.21 1.36 -13 5 -2 21.86 1.17 -13 5 -2 20.37 1.22 -13 5 -2 21.37 1.08 -13 -5 -2 21.18 0.94 -13 5 -2 20.58 1.34 -13 -5 -2 25.23 1.56 -13 5 -3 1.74 0.78 -13 5 -3 1.37 0.9 -13 5 -3 1.2 0.61 -13 5 -3 2.69 0.77 -13 5 -3 1.23 0.66 -13 -5 -3 0.98 0.75 -13 5 -3 1.77 0.84 -13 -5 -3 1.39 0.87 -13 -5 -4 573.56 12.85 -13 5 -4 486.3 12.59 -13 5 -4 539.24 12.55 -13 5 -4 534.12 12.28 -13 5 -4 533.99 12.37 -13 5 -4 508 12.26 -13 -5 -4 547.65 12.51 -13 5 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2.32 -13 5 -13 74.43 2.35 -13 5 -13 66.67 2.33 -13 -5 -13 63.33 2.21 -13 5 -14 14.63 0.91 -13 5 -14 15.34 1.01 -13 5 -14 12.87 0.96 -13 5 -15 4.43 0.7 -13 5 -15 3.23 0.61 -13 5 -16 35.71 1.2 -13 5 -16 27.73 1.07 -13 7 23 3.51 0.38 -13 -7 23 3.39 0.47 -13 -7 22 0.56 0.5 13 7 -22 0.47 0.34 -13 7 21 0.77 0.29 -13 7 21 0.6 0.8 13 7 -21 0.51 0.43 -13 7 20 7.37 1.06 -13 7 20 5.98 0.47 -13 7 19 11.9 1.24 -13 -7 19 10.5 1.34 -13 7 19 11.01 0.64 -13 7 18 11.34 1.27 -13 -7 18 9.77 1.39 -13 7 18 12.1 0.71 -13 7 17 44.67 2.07 -13 -7 17 42.02 2.19 -13 7 17 40.38 1.42 -13 7 16 196.33 5.48 -13 -7 16 199.03 5.18 -13 7 16 200.77 4.86 -13 -7 15 71.39 5.21 -13 7 15 70.2 5.13 -13 -7 15 83.73 3.23 -13 7 15 94.56 5.15 -13 -7 15 68.23 5.14 -13 7 15 70.38 5.1 -13 -7 15 89.99 2.79 -13 7 15 86.87 3.03 -13 7 15 86.37 2.46 -13 -7 14 14.17 2.86 -13 7 14 16.99 3.09 -13 -7 14 19.11 1.73 -13 7 14 24.5 2.82 -13 7 14 24.29 1.1 -13 -7 14 25.92 1.06 -13 -7 14 21.6 1.32 -13 -7 14 16.8 3.04 -13 7 14 16.47 2.99 -13 7 14 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12.34 -14 6 -4 1.43 0.71 -14 -6 -4 0.55 0.84 -14 6 -4 1.04 0.75 -14 6 -4 0.61 0.8 -14 -6 -4 0.66 0.65 -14 6 -4 1.17 0.91 -14 6 -4 0.8 0.67 -14 6 -4 0.39 0.62 -14 -6 -5 26.47 1.29 -14 6 -5 26.43 1.49 -14 6 -5 27.93 1.32 -14 6 -5 25.9 1.53 -14 6 -5 27 1.36 -14 6 -5 26.78 1.36 -14 6 -5 24.49 1.47 -14 -6 -5 28.99 1.59 -14 6 -6 0.3 0.7 -14 -6 -6 0.76 0.75 -14 6 -6 -0.1 0.67 -14 6 -6 0.91 0.69 -14 6 -6 0.44 0.88 -14 6 -6 0.7 0.76 -14 6 -6 0.41 0.62 -14 6 -7 141.01 4.02 -14 6 -7 148.46 4.19 -14 6 -7 152.3 3.98 -14 6 -7 147.88 4.21 -14 -6 -7 150.93 4.25 -14 6 -8 49.06 1.87 -14 6 -8 50.95 1.82 -14 -6 -8 50.3 1.99 -14 6 -8 48.62 2.01 -14 6 -8 49.49 2.01 -14 6 -9 14.33 1.2 -14 6 -9 15.4 1.03 -14 6 -9 14.5 1.11 -14 -6 -9 15.35 1.11 -14 6 -10 3.45 0.76 -14 -6 -10 3.58 0.74 -14 6 -10 3.33 0.87 -14 6 -11 5.18 0.78 -14 6 -11 5.97 0.88 -14 6 -12 128.1 3.43 -14 6 -12 127.35 3.44 -14 6 -13 44.02 1.62 -14 6 -13 45.6 1.57 -14 6 -14 25.78 1.01 -14 6 -14 25.27 1.07 -14 8 22 6.86 0.44 -14 8 21 1.58 0.39 14 8 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8 37.89 1.6 -14 8 8 36.78 1.28 -14 -8 8 47.18 1.32 -14 8 8 36.27 1.42 -14 8 8 38.04 1.64 -14 8 7 104.15 3 -14 8 7 102.79 2.82 -14 -8 7 126.03 2.84 -14 -8 7 106.99 3.13 -14 -8 7 109.78 3.59 -14 -8 7 106.78 3.17 -14 -8 7 87.27 5.21 -14 8 7 105.65 3.24 -14 8 6 198.41 5.03 -14 8 6 195.3 5.23 -14 -8 6 210.9 5.23 -14 8 6 189.98 5.36 -14 -8 6 206.31 5.18 -14 -8 6 171.96 4.85 -14 -8 6 205.55 5.62 -14 8 6 195.62 4.83 -14 -8 6 232.35 4.85 -14 8 5 19.02 0.87 -14 -8 5 21.16 0.85 -14 8 5 19.1 1.29 -14 8 5 19.01 1.03 -14 8 5 19.44 1.22 -14 -8 5 22.71 1.44 -14 -8 5 20.3 1.18 -14 -8 5 18.45 0.95 -14 -8 4 430.43 9.7 -14 -8 4 368.24 9.41 -14 8 4 389.11 9.86 -14 8 4 393.56 9.53 -14 8 4 402.76 9.74 -14 8 4 389.71 9.69 -14 -8 4 421.91 10.06 -14 8 4 388.79 9.31 -14 8 3 4.71 0.84 -14 8 3 5.43 0.82 -14 8 3 4.7 0.67 -14 8 3 2.96 0.74 -14 -8 3 3.92 0.87 -14 -8 3 3.94 0.79 -14 -8 3 4.27 0.65 -14 8 2 89.15 3 -14 8 2 99.7 3.02 -14 8 2 97.68 2.85 -14 8 2 97.75 3.16 -14 8 2 100.19 3.07 -14 -8 2 105.26 3.23 -14 -8 2 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57.74 2.22 -14 8 -6 5.22 0.77 -14 8 -6 7.05 0.85 -14 8 -6 4.47 0.86 -14 8 -6 5.14 0.88 -14 8 -6 6.63 0.79 -14 8 -7 0.96 0.62 -14 8 -7 0.97 0.74 -14 8 -7 0.79 0.66 -14 8 -7 1.11 0.64 -14 8 -8 9.32 0.98 -14 8 -8 7.73 0.83 -14 8 -9 10.78 0.97 -14 8 -9 9.04 0.81 -14 8 -10 7.25 0.87 -14 8 -10 5.89 0.76 -14 8 -10 6.29 0.68 -14 8 -11 17.68 0.97 -14 8 -11 18.45 0.9 -14 8 -11 20.15 1.02 -14 8 -14 54.26 1.57 -14 10 21 0.14 0.22 -14 -10 21 -0.13 0.34 -14 10 20 2.51 0.35 -14 -10 20 3.21 0.49 -14 10 19 26.18 0.95 -14 10 18 7.55 0.6 -14 10 17 0.6 0.47 -14 -10 16 0.43 0.51 -14 10 16 0.59 0.5 -14 -10 15 24.77 1.16 -14 10 15 28.47 1.19 -14 10 14 10.22 0.8 -14 -10 14 9.27 0.8 -14 -10 14 10.76 0.94 -14 10 13 11.27 0.85 -14 -10 13 10.4 0.83 -14 -10 13 10.66 0.93 -14 10 12 0.78 0.6 -14 -10 12 0.17 0.67 -14 -10 12 0.44 0.6 -14 10 11 1.8 0.64 -14 10 11 1.22 0.39 -14 -10 11 1.35 0.61 -14 -10 11 0.91 0.67 -14 -10 10 74.35 2.42 -14 -10 10 78.4 2.52 -14 10 10 78.08 2.2 -14 10 10 82.01 2.49 -14 -10 9 33.06 1.47 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81.8 2.58 -15 -7 9 53.79 4.44 -15 -7 9 69.65 2.31 -15 -7 9 79.24 2.05 -15 7 9 66.51 2.18 -15 -7 9 81.61 2.08 -15 7 9 66.71 2.04 -15 7 9 68.64 2.36 -15 7 9 69.31 5.14 -15 -7 9 65.79 2.17 -15 -7 8 169.49 4.6 -15 -7 8 204.37 4.36 -15 7 8 161.34 4.48 -15 -7 8 207.73 4.39 -15 7 8 159.62 4.32 -15 7 8 163.93 4.69 -15 -7 8 148.98 7.39 -15 7 8 173.07 8.09 -15 -7 8 163.03 4.49 -15 -7 7 331.74 8.24 -15 7 7 307.3 8.03 -15 -7 7 390.14 8.07 -15 7 7 326.28 8.25 -15 -7 7 393.75 8.09 -15 7 7 342.48 8.56 -15 7 7 335.76 8.45 -15 -7 7 305.64 11.55 -15 -7 7 348.08 8.36 -15 7 6 0.74 0.59 -15 7 6 0.7 0.76 -15 -7 6 -0.2 0.6 -15 7 6 0.42 0.53 -15 -7 6 0.3 0.41 -15 7 6 0.12 0.44 -15 -7 6 -0.06 0.45 -15 7 5 87.02 2.61 -15 -7 5 106.37 2.63 -15 7 5 93.89 3.07 -15 -7 5 98.56 2.82 -15 7 5 96.58 2.97 -15 -7 5 110.23 2.65 -15 7 5 92.85 2.82 -15 7 5 92.89 2.97 -15 -7 4 3.87 0.8 -15 7 4 4.92 0.89 -15 7 4 3.68 0.81 -15 7 4 5.08 0.77 -15 -7 4 3.57 0.64 -15 7 4 3.59 0.51 -15 7 4 4.15 0.77 -15 7 4 4.54 0.69 -15 -7 4 4.75 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-21 3 12 4.11 0.49 -21 3 12 3.97 0.4 -21 -3 12 3.7 0.4 -21 3 11 20.67 0.85 -21 -3 11 21.66 0.83 -21 3 11 20.34 0.88 -21 3 11 19.44 0.79 -21 -3 11 21.5 0.8 -21 3 10 9.29 0.63 -21 -3 10 10.6 0.6 -21 3 10 9.22 0.67 -21 3 10 8.37 0.56 -21 -3 10 10.71 0.58 -21 3 9 142.22 3.53 -21 -3 9 149.73 3.49 -21 3 8 7.68 0.62 -21 -3 8 7.85 0.56 -21 3 8 7.16 0.63 -21 3 7 0.1 0.47 -21 -3 7 0.43 0.39 -21 3 7 0.25 0.49 -21 -3 6 22.9 0.88 -21 3 6 20.11 0.96 -21 3 6 20.7 1.04 -21 3 6 21.7 0.94 -21 3 5 38.52 1.37 -21 3 5 37.04 1.46 -21 3 5 41.23 1.34 -21 3 4 3.99 0.58 -21 3 4 4.4 0.53 -21 3 4 4.89 0.69 -21 3 3 18.48 0.84 -21 3 3 16.46 0.86 -21 3 3 17.2 1.01 -21 3 2 68.79 1.88 -21 3 2 60.87 2.05 -21 3 1 1.18 0.57 -21 -3 1 0.84 0.51 -21 -3 0 20.07 0.94 -21 3 0 18.42 0.97 -21 -3 -1 3.86 0.5 -21 3 -1 4.43 0.57 -21 3 -2 20.51 0.93 -21 3 -3 0.15 0.39 -21 5 16 26.26 0.8 -21 5 16 26.22 0.78 -21 5 15 1.67 0.31 -21 5 15 1.75 0.3 -21 5 15 1.37 0.23 -21 5 14 33.89 1.02 -21 5 14 32.18 1 -21 5 14 31.35 0.9 -21 5 13 13.62 0.63 -21 5 13 12.28 0.6 -21 5 13 11.88 0.51 -21 5 12 6.22 0.5 -21 5 12 5.79 0.47 -21 5 11 0.39 0.38 -21 5 11 0.04 0.37 -21 5 10 0.26 0.41 -21 5 10 -0.05 0.39 -21 5 9 1.91 0.47 -21 5 9 1.61 0.42 -21 5 8 23.38 0.96 -21 5 8 25.53 1.01 -21 5 7 12.13 0.69 -21 5 7 13.32 0.76 -21 5 6 9.52 0.65 -21 5 6 9.98 0.69 -21 5 5 32.16 1.18 -21 5 5 29.31 1.19 -21 5 4 5.64 0.56 -21 5 4 7.2 0.61 -21 5 4 5.7 0.61 -21 5 3 2.51 0.5 -21 5 3 2.37 0.53 -21 5 2 80.14 2.1 -21 5 2 68.51 2.13 -21 5 1 0.61 0.43 -21 5 1 0.35 0.47 -21 5 0 1.42 0.44 -21 5 0 1.07 0.46 -21 5 -1 26.27 0.95 -21 5 -1 24.61 1.01 -21 5 -2 21.91 0.9 -21 5 -3 20.3 0.81 -21 5 -4 97.68 2.44 -21 7 14 14.09 0.48 -21 7 13 3.2 0.29 -21 7 12 -0.16 0.26 -21 7 11 1.35 0.31 -21 7 10 4.95 0.41 -21 7 9 12.06 0.6 -21 7 8 56.32 1.58 -21 7 7 29.5 1 -21 7 6 15.45 0.7 -21 7 4 10.81 0.55 -21 7 3 5.37 0.44 -21 7 2 12.47 0.61 -21 7 1 0.8 0.33 -21 7 0 0.69 0.38 -21 7 0 0.71 0.33 -21 7 -1 11.75 0.57 -21 7 -1 13.15 0.61 -21 7 -2 2.28 0.32 -21 9 13 11.19 0.45 -21 9 12 -0.02 0.25 -21 9 11 4.05 0.37 -21 9 10 11.34 0.56 -21 9 9 9.59 0.53 -21 9 8 21.83 0.81 -21 9 7 31.59 1.03 -21 9 6 4.18 0.45 -21 9 5 14.62 0.67 -21 9 4 34.19 1.08 -21 9 3 0.63 0.34 -21 9 2 5.06 0.42 -21 9 1 3.47 0.37 -21 11 7 3.51 0.26 -21 11 6 1.97 0.23 -22 0 16 2.24 0.24 -22 0 16 2.64 0.26 -22 0 15 0.19 0.22 -22 0 15 0.29 0.25 -22 0 14 28.27 0.86 -22 0 14 29.07 0.9 -22 0 13 0.24 0.28 -22 0 13 0.39 0.32 -22 0 12 0.43 0.31 -22 0 12 0.45 0.34 -22 0 11 0.16 0.35 -22 0 10 2.04 0.4 -22 0 9 0.23 0.38 -22 0 8 26.59 0.97 -22 0 7 -0.04 0.38 -22 0 6 0.2 0.38 -22 0 5 -0.24 0.38 -22 0 3 -0.4 0.47 -22 0 2 11.75 0.73 -22 0 1 0.2 0.42 -22 0 -2 42.98 1.26 -22 2 16 5.41 0.31 -22 2 15 10.02 0.42 -22 2 15 9.83 0.46 -22 2 14 39.63 1.1 -22 2 14 38.54 1.16 -22 2 13 8.84 0.44 -22 -2 13 10.21 0.46 -22 -2 13 9.2 0.47 -22 2 13 8.39 0.5 -22 -2 12 37.59 1.09 -22 2 12 36.76 1.14 -22 -2 11 31.01 0.95 -22 2 11 28.41 1 -22 -2 10 84.58 2.15 -22 -2 9 0.56 0.34 -22 -2 8 32.35 1.04 -22 -2 7 11.18 0.58 -22 -2 6 12.76 0.61 -22 2 4 13.35 0.78 -22 2 3 7.01 0.62 -22 2 2 15.05 0.79 -22 2 1 15.69 0.79 -22 2 0 6.18 0.53 -22 2 -1 7.67 0.53 -22 2 -2 10.23 0.53 -22 4 15 31.32 0.87 -22 4 14 8.11 0.41 -22 4 13 1.3 0.29 -22 4 12 0.21 0.3 -22 4 11 1.76 0.35 -22 4 10 13.16 0.62 -22 4 9 0.49 0.36 -22 4 8 -0.12 0.36 -22 4 7 13.82 0.69 -22 4 6 38.56 1.22 -22 4 5 1.77 0.41 -22 4 4 1.51 0.4 -22 4 3 24.41 0.93 -22 4 2 3.22 0.44 -22 4 1 2.84 0.42 -22 4 0 3.33 0.41 -22 4 -1 10.47 0.54 -22 4 -2 6.67 0.41 -22 6 13 -0.09 0.18 -22 6 13 0.03 0.22 -22 6 12 0.24 0.21 -22 6 12 0.38 0.27 -22 6 11 -0.06 0.24 -22 6 11 -0.27 0.29 -22 6 10 4.11 0.39 -22 6 10 3.47 0.33 -22 6 9 -0.05 0.29 -22 6 9 0.08 0.32 -22 6 8 21.16 0.77 -22 6 8 18.52 0.71 -22 6 7 2.24 0.38 -22 6 7 2.17 0.34 -22 6 6 35.29 1.1 -22 6 5 11.07 0.57 -22 6 4 17.12 0.69 -22 6 3 6.72 0.47 -22 6 2 6.8 0.45 -22 6 1 2.36 0.34 -23 -1 12 11.51 0.45 -23 -1 11 5.53 0.35 -23 1 10 4.01 0.35 -23 -1 10 4.5 0.33 -23 -1 9 31.05 0.95 -23 1 9 34.78 0.99 -23 -1 8 -0.14 0.27 -23 1 8 0.02 0.29 -23 1 7 2.79 0.35 -23 3 13 4.12 0.26 -23 3 12 11.6 0.46 -23 3 11 4.19 0.33 -23 3 10 12.39 0.52 -23 3 9 16.16 0.61 -23 3 8 2.83 0.34 -23 3 7 13.76 0.57 -23 5 11 3.38 0.24 -23 5 10 8.75 0.37 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Ni1 Br1 Ni1 93.298(19) . 7_666 ? Br1 Ni1 Br1 86.702(19) . 7_666 ? Br2 Ni1 Br1 95.22(2) . . ? Br2 Ni1 Br1 152.99(3) . 7_666 ? N1 Ni1 Br1 104.03(7) . . ? N1 Ni1 Br1 102.53(7) . 7_666 ? N1 Ni1 Br2 103.11(7) . . ? N1 Ni1 N2 80.40(10) . . ? N2 Ni1 Br1 174.22(8) . . ? N2 Ni1 Br1 88.71(8) . 7_666 ? N2 Ni1 Br2 87.28(7) . . ? C6 N1 Ni1 113.9(2) . . ? C6 N1 C8 119.5(2) . . ? C8 N1 Ni1 126.51(18) . . ? C5 N2 Ni1 112.3(2) . . ? C1 N2 Ni1 129.0(2) . . ? C1 N2 C5 118.6(3) . . ? C20 C19 H19 118.5 . . ? C18 C19 H19 118.5 . . ? C18 C19 C20 123.0(3) . . ? C19 C20 C8 117.6(3) . . ? C19 C20 C21 118.5(3) . . ? C8 C20 C21 123.8(3) . . ? N1 C6 C5 117.1(3) . . ? N1 C6 C7 125.2(3) . . ? C5 C6 C7 117.6(3) . . ? C20 C8 N1 118.9(3) . . ? C20 C8 C9 121.0(3) . . ? C9 C8 N1 120.1(2) . . ? C19 C18 C16 117.4(3) . . ? C19 C18 C27 120.8(3) . . ? C16 C18 C27 121.8(3) . . ? C8 C9 C10 121.5(3) . . ? C16 C9 C8 118.3(3) . . ? C16 C9 C10 120.2(3) . . ? C20 C21 H21 107.8 . . ? C20 C21 C26 112.8(3) . . ? C20 C21 C22 111.3(3) . . ? C26 C21 H21 107.8 . . ? C22 C21 H21 107.8 . . ? C22 C21 C26 109.1(3) . . ? N2 C5 C6 114.9(3) . . ? N2 C5 C4 121.4(3) . . ? C4 C5 C6 123.6(3) . . ? C18 C16 H16 118.6 . . ? C9 C16 C18 122.7(3) . . ? C9 C16 H16 118.6 . . ? C9 C10 H10 107.3 . . ? C9 C10 C15 113.2(3) . . ? C15 C10 H10 107.3 . . ? C11 C10 C9 111.1(3) . . ? C11 C10 H10 107.3 . . ? C11 C10 C15 110.4(3) . . ? C18 C27 H27 106.8 . . ? C28 C27 C18 111.6(3) . . ? C28 C27 H27 106.8 . . ? C28 C27 C32 110.8(3) . . ? C32 C27 C18 113.6(3) . . ? C32 C27 H27 106.8 . . ? N2 C1 Br3 117.1(2) . . ? N2 C1 C2 123.2(3) . . ? C2 C1 Br3 119.7(3) . . ? C5 C4 H4 120.3 . . ? C5 C4 C3 119.5(4) . . ? C3 C4 H4 120.3 . . ? C21 C26 H26A 109.4 . . ? C21 C26 H26B 109.4 . . ? H26A C26 H26B 108.0 . . ? C25 C26 C21 111.1(3) . . ? C25 C26 H26A 109.4 . . ? C25 C26 H26B 109.4 . . ? C21 C22 H22A 109.3 . . ? C21 C22 H22B 109.3 . . ? H22A C22 H22B 108.0 . . ? C23 C22 C21 111.6(3) . . ? C23 C22 H22A 109.3 . . ? C23 C22 H22B 109.3 . . ? C1 C2 H2 120.9 . . ? C3 C2 C1 118.1(3) . . ? C3 C2 H2 120.9 . . ? C6 C7 H7A 109.5 . . ? C6 C7 H7B 109.5 . . ? C6 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C4 C3 H3 120.5 . . ? C2 C3 C4 119.1(3) . . ? C2 C3 H3 120.5 . . ? C10 C15 H15A 109.4 . . ? C10 C15 H15B 109.4 . . ? C10 C15 C14 111.2(3) . . ? H15A C15 H15B 108.0 . . ? C14 C15 H15A 109.4 . . ? C14 C15 H15B 109.4 . . ? C26 C25 H25A 109.4 . . ? C26 C25 H25B 109.4 . . ? H25A C25 H25B 108.0 . . ? C24 C25 C26 111.3(4) . . ? C24 C25 H25A 109.4 . . ? C24 C25 H25B 109.4 . . ? C10 C11 H11A 109.4 . . ? C10 C11 H11B 109.4 . . ? C10 C11 C12 111.2(4) . . ? H11A C11 H11B 108.0 . . ? C12 C11 H11A 109.4 . . ? C12 C11 H11B 109.4 . . ? C27 C28 H28A 109.0 . . ? C27 C28 H28B 109.0 . . ? C27 C28 C29 112.7(4) . . ? H28A C28 H28B 107.8 . . ? C29 C28 H28A 109.0 . . ? C29 C28 H28B 109.0 . . ? C27 C32 H32A 109.2 . . ? C27 C32 H32B 109.2 . . ? C27 C32 C31 112.1(4) . . ? H32A C32 H32B 107.9 . . ? C31 C32 H32A 109.2 . . ? C31 C32 H32B 109.2 . . ? H30A C30 H30B 108.0 . . ? C31 C30 H30A 109.4 . . ? C31 C30 H30B 109.4 . . ? C29 C30 H30A 109.4 . . ? C29 C30 H30B 109.4 . . ? C29 C30 C31 111.1(4) . . ? C15 C14 H14A 109.5 . . ? C15 C14 H14B 109.5 . . ? H14A C14 H14B 108.1 . . ? C13 C14 C15 110.8(4) . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C32 C31 H31A 109.2 . . ? C32 C31 H31B 109.2 . . ? C30 C31 C32 111.9(4) . . ? C30 C31 H31A 109.2 . . ? C30 C31 H31B 109.2 . . ? H31A C31 H31B 107.9 . . ? C22 C23 H23A 109.4 . . ? C22 C23 H23B 109.4 . . ? C22 C23 C24 111.3(4) . . ? H23A C23 H23B 108.0 . . ? C24 C23 H23A 109.4 . . ? C24 C23 H23B 109.4 . . ? C11 C12 H12A 109.6 . . ? C11 C12 H12B 109.6 . . ? H12A C12 H12B 108.1 . . ? C13 C12 C11 110.3(4) . . ? C13 C12 H12A 109.6 . . ? C13 C12 H12B 109.6 . . ? C25 C24 C23 111.2(4) . . ? C25 C24 H24A 109.4 . . ? C25 C24 H24B 109.4 . . ? C23 C24 H24A 109.4 . . ? C23 C24 H24B 109.4 . . ? H24A C24 H24B 108.0 . . ? C28 C29 H29A 109.4 . . ? C28 C29 H29B 109.4 . . ? C30 C29 C28 111.3(4) . . ? C30 C29 H29A 109.4 . . ? C30 C29 H29B 109.4 . . ? H29A C29 H29B 108.0 . . ? C14 C13 C12 110.6(4) . . ? C14 C13 H13A 109.5 . . ? C14 C13 H13B 109.5 . . ? C12 C13 H13A 109.5 . . ? C12 C13 H13B 109.5 . . ? H13A C13 H13B 108.1 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 Ni1 2.4684(6) . ? Br1 Ni1 2.5039(6) 7_666 ? Br2 Ni1 2.4574(6) . ? Br3 C1 1.879(4) . ? Ni1 N1 2.046(2) . ? Ni1 N2 2.050(3) . ? N1 C6 1.281(4) . ? N1 C8 1.452(4) . ? N2 C5 1.353(4) . ? N2 C1 1.317(4) . ? C19 H19 0.9300 . ? C19 C20 1.399(4) . ? C19 C18 1.389(4) . ? C20 C8 1.407(4) . ? C20 C21 1.514(4) . ? C6 C5 1.488(4) . ? C6 C7 1.489(4) . ? C8 C9 1.411(4) . ? C18 C16 1.393(5) . ? C18 C27 1.522(4) . ? C9 C16 1.387(4) . ? C9 C10 1.524(4) . ? C21 H21 0.9800 . ? C21 C26 1.545(4) . ? C21 C22 1.533(5) . ? C5 C4 1.375(4) . ? C16 H16 0.9300 . ? C10 H10 0.9800 . ? C10 C15 1.524(5) . ? C10 C11 1.517(5) . ? C27 H27 0.9800 . ? C27 C28 1.508(5) . ? C27 C32 1.511(5) . ? C1 C2 1.394(5) . ? C4 H4 0.9300 . ? C4 C3 1.385(6) . ? C26 H26A 0.9700 . ? C26 H26B 0.9700 . ? C26 C25 1.524(5) . ? C22 H22A 0.9700 . ? C22 H22B 0.9700 . ? C22 C23 1.520(5) . ? C2 H2 0.9300 . ? C2 C3 1.370(6) . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C3 H3 0.9300 . ? C15 H15A 0.9700 . ? C15 H15B 0.9700 . ? C15 C14 1.530(5) . ? C25 H25A 0.9700 . ? C25 H25B 0.9700 . ? C25 C24 1.511(8) . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C11 C12 1.531(6) . ? C28 H28A 0.9700 . ? C28 H28B 0.9700 . ? C28 C29 1.525(6) . ? C32 H32A 0.9700 . ? C32 H32B 0.9700 . ? C32 C31 1.527(6) . ? C30 H30A 0.9700 . ? C30 H30B 0.9700 . ? C30 C31 1.508(7) . ? C30 C29 1.495(8) . ? C14 H14A 0.9700 . ? C14 H14B 0.9700 . ? C14 C13 1.510(7) . ? C31 H31A 0.9700 . ? C31 H31B 0.9700 . ? C23 H23A 0.9700 . ? C23 H23B 0.9700 . ? C23 C24 1.531(7) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C12 C13 1.530(7) . ? C24 H24A 0.9700 . ? C24 H24B 0.9700 . ? C29 H29A 0.9700 . ? C29 H29B 0.9700 . ? C13 H13A 0.9700 . ? C13 H13B 0.9700 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Br3 C1 C2 C3 175.2(3) . . . . ? Ni1 N1 C6 C5 -9.2(3) . . . . ? Ni1 N1 C6 C7 173.4(3) . . . . ? Ni1 N1 C8 C20 102.3(3) . . . . ? Ni1 N1 C8 C9 -75.9(3) . . . . ? Ni1 N2 C5 C6 7.6(3) . . . . ? Ni1 N2 C5 C4 -174.5(3) . . . . ? Ni1 N2 C1 Br3 -1.1(4) . . . . ? Ni1 N2 C1 C2 177.0(3) . . . . ? N1 C6 C5 N2 1.0(4) . . . . ? N1 C6 C5 C4 -176.8(3) . . . . ? N1 C8 C9 C16 179.6(3) . . . . ? N1 C8 C9 C10 -2.4(4) . . . . ? N2 C5 C4 C3 -3.4(6) . . . . ? N2 C1 C2 C3 -2.8(6) . . . . ? C19 C20 C8 N1 -179.2(3) . . . . ? C19 C20 C8 C9 -1.1(4) . . . . ? C19 C20 C21 C26 -62.9(4) . . . . ? C19 C20 C21 C22 60.1(4) . . . . ? C19 C18 C16 C9 -0.7(5) . . . . ? C19 C18 C27 C28 -105.3(4) . . . . ? C19 C18 C27 C32 128.5(4) . . . . ? C20 C19 C18 C16 1.2(5) . . . . ? C20 C19 C18 C27 178.2(3) . . . . ? C20 C8 C9 C16 1.5(5) . . . . ? C20 C8 C9 C10 179.4(3) . . . . ? C20 C21 C26 C25 -178.8(3) . . . . ? C20 C21 C22 C23 178.2(3) . . . . ? C6 N1 C8 C20 -75.5(4) . . . . ? C6 N1 C8 C9 106.4(3) . . . . ? C6 C5 C4 C3 174.3(3) . . . . ? C8 N1 C6 C5 168.8(3) . . . . ? C8 N1 C6 C7 -8.6(5) . . . . ? C8 C20 C21 C26 119.2(3) . . . . ? C8 C20 C21 C22 -117.7(3) . . . . ? C8 C9 C16 C18 -0.6(5) . . . . ? C8 C9 C10 C15 141.1(3) . . . . ? C8 C9 C10 C11 -94.0(4) . . . . ? C18 C19 C20 C8 -0.3(5) . . . . ? C18 C19 C20 C21 -178.3(3) . . . . ? C18 C27 C28 C29 179.1(4) . . . . ? C18 C27 C32 C31 179.1(4) . . . . ? C9 C10 C15 C14 -178.7(3) . . . . ? C9 C10 C11 C12 177.2(4) . . . . ? C21 C20 C8 N1 -1.4(4) . . . . ? C21 C20 C8 C9 176.8(3) . . . . ? C21 C26 C25 C24 -57.1(5) . . . . ? C21 C22 C23 C24 56.2(5) . . . . ? C5 N2 C1 Br3 -176.8(2) . . . . ? C5 N2 C1 C2 1.3(5) . . . . ? C5 C4 C3 C2 1.7(6) . . . . ? C16 C18 C27 C28 71.6(5) . . . . ? C16 C18 C27 C32 -54.6(5) . . . . ? C16 C9 C10 C15 -41.0(5) . . . . ? C16 C9 C10 C11 83.9(4) . . . . ? C10 C9 C16 C18 -178.6(3) . . . . ? C10 C15 C14 C13 -56.7(5) . . . . ? C10 C11 C12 C13 56.9(6) . . . . ? C27 C18 C16 C9 -177.7(3) . . . . ? C27 C28 C29 C30 55.0(6) . . . . ? C27 C32 C31 C30 -54.1(6) . . . . ? C1 N2 C5 C6 -176.0(3) . . . . ? C1 N2 C5 C4 1.9(5) . . . . ? C1 C2 C3 C4 1.2(6) . . . . ? C26 C21 C22 C23 -56.7(4) . . . . ? C26 C25 C24 C23 55.4(6) . . . . ? C22 C21 C26 C25 56.9(4) . . . . ? C22 C23 C24 C25 -54.9(6) . . . . ? C7 C6 C5 N2 178.6(3) . . . . ? C7 C6 C5 C4 0.8(5) . . . . ? C15 C10 C11 C12 -56.3(5) . . . . ? C15 C14 C13 C12 57.0(6) . . . . ? C11 C10 C15 C14 56.0(5) . . . . ? C11 C12 C13 C14 -57.0(6) . . . . ? C28 C27 C32 C31 52.5(5) . . . . ? C32 C27 C28 C29 -53.2(5) . . . . ? C31 C30 C29 C28 -55.2(6) . . . . ? C29 C30 C31 C32 55.1(6) . . . . ?