#------------------------------------------------------------------------------ #$Date: 2024-10-12 01:11:25 +0300 (Sat, 12 Oct 2024) $ #$Revision: 295437 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/28/1572859.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572859 loop_ _publ_author_name 'Zhu, Jiaxuan' 'Wu, Wenbo' 'Qi, Haoqiang' 'Yao, Yutong' 'Yu, Hui' 'Huang, Xin' 'Wang, Na' 'Wang, Ting' 'Hao, Hongxun' _publ_section_title ; Dynamic organic crystal as exceptionally efficient artificial natural light-harvesting actuator ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC05684A _journal_year 2024 _chemical_formula_moiety 'C16 H16 Cl N3 O' _chemical_formula_sum 'C16 H16 Cl N3 O' _chemical_formula_weight 301.77 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-04-11 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-08-24 deposited with the CCDC. 2024-10-07 downloaded from the CCDC. ; _cell_angle_alpha 99.161(3) _cell_angle_beta 96.187(3) _cell_angle_gamma 90.692(3) _cell_formula_units_Z 2 _cell_length_a 5.2898(2) _cell_length_b 7.8669(3) _cell_length_c 17.5590(6) _cell_measurement_reflns_used 4635 _cell_measurement_temperature 99.99(10) _cell_measurement_theta_max 71.7470 _cell_measurement_theta_min 2.5870 _cell_volume 716.87(5) _computing_cell_refinement 'CrysAlisPro 1.171.43.104a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.43.104a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.43.104a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 99.99(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.987 _diffrn_measured_fraction_theta_max 0.934 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 37.00 81.00 0.50 0.05 -- 36.12-143.00 -30.00 88 2 \w 93.00 120.00 0.50 0.05 -- 108.45-143.00 -30.00 54 3 \w 39.00 98.00 0.50 0.05 -- 36.12-127.00 138.00 118 4 \w 83.00 111.00 0.50 0.05 -- 108.45-127.00 138.00 56 5 \w 30.00 74.00 0.50 0.05 -- 108.45-127.00 138.00 88 6 \w 39.00 64.00 0.50 0.05 -- 108.45 -61.00 150.00 50 7 \w 41.00 81.00 0.50 0.05 -- 108.45 -77.00 30.00 80 8 \w 32.00 86.00 0.50 0.05 -- 108.45 -77.00-150.00 108 9 \w 50.00 103.00 0.50 0.05 -- 108.45 -77.00 -90.00 106 10 \w 49.00 75.00 0.50 0.05 -- 108.45 -77.00 -60.00 52 11 \w -2.00 115.00 0.50 0.05 -- 36.12 37.00 150.00 234 12 \w 98.00 123.00 0.50 0.05 -- 108.45 143.00 24.00 50 13 \w 113.00 144.00 0.50 0.05 -- 108.45 179.00 -30.00 62 14 \w 118.00 145.00 0.50 0.05 -- 108.45 179.00-120.00 54 15 \w 77.00 105.00 0.50 0.05 -- 108.45 127.00-145.00 56 16 \w 45.00 77.00 0.50 0.05 -- 108.45 179.00-120.00 64 17 \w 53.00 97.00 0.50 0.05 -- 108.45 179.00 -30.00 88 18 \w 130.00 169.00 0.50 0.05 -- 108.45 111.00 90.00 78 19 \w 88.00 117.00 0.50 0.05 -- 108.45 111.00 90.00 58 20 \w -42.00 22.00 0.50 0.05 -- 36.12 -19.00 -30.00 128 21 \w -43.00 17.00 0.50 0.05 -- 36.12 -19.00-150.00 120 22 \w -50.00 -15.00 0.50 0.05 -- 36.12 -19.00-180.00 70 23 \w -151.00-124.00 0.50 0.05 -- -100.00 -94.00 -90.00 54 24 \w -116.00 -88.00 0.50 0.05 -- -100.00 -94.00 -90.00 56 25 \w -125.00 -74.00 0.50 0.05 -- -36.12-179.00 60.00 102 26 \w -101.00 -70.00 0.50 0.05 -- -100.00-143.00 -30.00 62 27 \w -171.00 -68.00 0.50 0.05 -- -100.00 -61.00 60.00 206 28 \w -163.00 -68.00 0.50 0.05 -- -100.00 -61.00 30.00 190 29 \w -151.00-126.00 0.50 0.05 -- -100.00-127.00 138.00 50 30 \w -54.00 -20.00 0.50 0.05 -- -100.00 45.00 -30.00 68 31 \w -53.00 -20.00 0.50 0.05 -- -100.00 45.00 30.00 66 32 \w -52.00 -21.00 0.50 0.05 -- -100.00 45.00 0.00 62 33 \w -102.00 -55.00 0.50 0.05 -- -100.00 77.00-150.00 94 34 \w -54.00 -19.00 0.50 0.05 -- -100.00 45.00-180.00 70 35 \w -46.00 -21.00 0.50 0.05 -- -100.00 77.00-150.00 50 36 \w -64.00 -31.00 0.50 0.05 -- -100.00 127.00-145.00 66 37 \w -88.00 -54.00 0.50 0.05 -- -100.00 179.00 -90.00 68 38 \w -150.00 -92.00 0.50 0.05 -- -100.00 179.00 -90.00 116 39 \w -120.00 -68.00 0.50 0.05 -- -100.00 143.00 24.00 104 40 \w -108.00 -48.00 0.50 0.05 -- -100.00 179.00 30.00 120 41 \w -95.00 -70.00 0.50 0.05 -- -36.12 143.00 24.00 50 42 \w -77.00 -50.00 0.50 0.05 -- -36.12 127.00-145.00 54 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'ROD, Synergy Custom system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0092387000 _diffrn_orient_matrix_UB_12 0.0268948000 _diffrn_orient_matrix_UB_13 0.0891118000 _diffrn_orient_matrix_UB_21 -0.1452695000 _diffrn_orient_matrix_UB_22 -0.1731899000 _diffrn_orient_matrix_UB_23 -0.0054478000 _diffrn_orient_matrix_UB_31 0.2543651000 _diffrn_orient_matrix_UB_32 -0.0930758000 _diffrn_orient_matrix_UB_33 0.0051009000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0243 _diffrn_reflns_av_unetI/netI 0.0286 _diffrn_reflns_Laue_measured_fraction_full 0.987 _diffrn_reflns_Laue_measured_fraction_max 0.934 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 5886 _diffrn_reflns_point_group_measured_fraction_full 0.987 _diffrn_reflns_point_group_measured_fraction_max 0.934 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.149 _diffrn_reflns_theta_min 2.565 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 2.375 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.74505 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.43.104a (Rigaku Oxford Diffraction, 2023) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.398 _exptl_crystal_description plate _exptl_crystal_F_000 316 _refine_diff_density_max 0.251 _refine_diff_density_min -0.276 _refine_diff_density_rms 0.056 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.079 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 192 _refine_ls_number_reflns 2655 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.079 _refine_ls_R_factor_all 0.0376 _refine_ls_R_factor_gt 0.0359 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0676P)^2^+0.1778P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1041 _refine_ls_wR_factor_ref 0.1059 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2481 _reflns_number_total 2655 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05684a11.cif _cod_data_source_block form_I _cod_database_code 1572859 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: N003(H003), C007(H007), C009(H009), C00B(H00B), C00C(H00C), C00D(H00D), C00E(H00E), C00H(H00H), C00I(H00I), C00J(H00J) 2.b Idealised Me refined as rotating group: C00K(H00A,H00F,H00G), C00L(H00K,H00L,H00M) ; _shelx_res_file ; TITL form_I_a.res in P-1 form_I.res created by SHELXL-2018/3 at 15:14:28 on 11-Apr-2024 REM Old TITL form_I in P-1 REM SHELXT solution in P-1: R1 0.108, Rweak 0.005, Alpha 0.020 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C16 N3 O Cl CELL 1.54184 5.2898 7.8669 17.559 99.161 96.187 90.692 ZERR 2 0.0002 0.0003 0.0006 0.003 0.003 0.003 LATT 1 SFAC C H Cl N O UNIT 32 32 2 6 2 L.S. 4 PLAN 5 TEMP -173 CONF BOND list 4 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.067600 0.177800 FVAR 0.97110 CL01 3 0.044342 0.910693 0.100127 11.00000 0.03826 0.02409 = 0.01600 0.00506 0.00563 0.00554 O002 5 -0.237728 0.780586 0.448820 11.00000 0.02365 0.03347 = 0.02115 0.00800 0.00466 0.00186 N003 4 0.194436 0.765492 0.469380 11.00000 0.02337 0.02300 = 0.01352 0.00342 0.00334 0.00125 AFIX 43 H003 2 0.338775 0.764651 0.448673 11.00000 -1.20000 AFIX 0 N004 4 0.193662 0.743440 0.545955 11.00000 0.02697 0.02029 = 0.01406 0.00230 0.00261 0.00020 N005 4 0.538192 0.626134 0.896864 11.00000 0.02884 0.01805 = 0.01588 0.00259 0.00040 0.00253 C006 1 0.434936 0.673226 0.658638 11.00000 0.02186 0.01380 = 0.01638 0.00084 0.00086 -0.00256 C007 1 0.681545 0.573124 0.766881 11.00000 0.02151 0.01410 = 0.02045 0.00203 -0.00021 0.00126 AFIX 43 H007 2 0.824463 0.513683 0.785630 11.00000 -1.20000 AFIX 0 C008 1 0.509557 0.642750 0.818163 11.00000 0.02333 0.01274 = 0.01701 0.00179 0.00047 -0.00298 C009 1 0.403743 0.692709 0.576828 11.00000 0.02443 0.01586 = 0.01736 0.00082 0.00352 -0.00006 AFIX 43 H009 2 0.540443 0.667529 0.546308 11.00000 -1.20000 AFIX 0 C00A 1 0.003113 0.819666 0.345659 11.00000 0.02174 0.01394 = 0.01772 0.00201 0.00237 0.00384 C00B 1 0.261998 0.741387 0.709667 11.00000 0.02023 0.01607 = 0.01894 0.00190 0.00031 0.00064 AFIX 43 H00B 2 0.116866 0.797984 0.690385 11.00000 -1.20000 AFIX 0 C00C 1 -0.186827 0.752541 0.286896 11.00000 0.02146 0.01851 = 0.02053 0.00245 0.00233 0.00034 AFIX 43 H00C 2 -0.326428 0.688581 0.298994 11.00000 -1.20000 AFIX 0 C00D 1 0.207825 0.914258 0.327893 11.00000 0.02118 0.01710 = 0.02071 0.00124 -0.00057 0.00134 AFIX 43 H00D 2 0.338816 0.959244 0.367582 11.00000 -1.20000 AFIX 0 C00E 1 0.298672 0.727794 0.787276 11.00000 0.02101 0.01720 = 0.01811 0.00102 0.00361 0.00138 AFIX 43 H00E 2 0.179567 0.776668 0.820679 11.00000 -1.20000 AFIX 0 C00F 1 -0.027142 0.788395 0.426242 11.00000 0.02401 0.01579 = 0.01779 0.00096 0.00217 0.00118 C00G 1 0.029724 0.873803 0.195292 11.00000 0.02734 0.01468 = 0.01575 0.00276 0.00423 0.00551 C00H 1 0.644776 0.590301 0.689018 11.00000 0.02178 0.01434 = 0.01849 -0.00034 0.00334 -0.00009 AFIX 43 H00H 2 0.765659 0.544388 0.655607 11.00000 -1.20000 AFIX 0 C00I 1 -0.174601 0.777909 0.211106 11.00000 0.02444 0.01974 = 0.01882 0.00057 -0.00083 0.00218 AFIX 43 H00I 2 -0.302876 0.730845 0.170943 11.00000 -1.20000 AFIX 0 C00J 1 0.220177 0.942652 0.252290 11.00000 0.02339 0.01625 = 0.02278 0.00394 0.00525 0.00142 AFIX 43 H00J 2 0.357515 1.008418 0.239985 11.00000 -1.20000 AFIX 0 C00K 1 0.465487 0.771893 0.951575 11.00000 0.03634 0.02562 = 0.01654 0.00182 0.00353 0.00410 AFIX 137 H00A 2 0.574770 0.872445 0.949954 11.00000 -1.50000 H00F 2 0.485158 0.742924 1.004107 11.00000 -1.50000 H00G 2 0.287658 0.798294 0.937445 11.00000 -1.50000 AFIX 0 C00L 1 0.767720 0.547262 0.925988 11.00000 0.04098 0.03405 = 0.02082 0.00944 -0.00008 0.01268 AFIX 137 H00K 2 0.781194 0.432556 0.895609 11.00000 -1.50000 H00L 2 0.760630 0.536961 0.980613 11.00000 -1.50000 H00M 2 0.916333 0.619009 0.921409 11.00000 -1.50000 AFIX 0 HKLF 4 REM form_I_a.res in P-1 REM wR2 = 0.1059, GooF = S = 1.079, Restrained GooF = 1.079 for all data REM R1 = 0.0359 for 2481 Fo > 4sig(Fo) and 0.0376 for all 2655 data REM 192 parameters refined using 0 restraints END WGHT 0.0676 0.1778 REM Highest difference peak 0.251, deepest hole -0.276, 1-sigma level 0.056 Q1 1 -0.1407 0.9353 0.1166 11.00000 0.05 0.25 Q2 1 0.2214 0.8749 0.0822 11.00000 0.05 0.25 Q3 1 0.1504 0.9205 0.1441 11.00000 0.05 0.24 Q4 1 0.4063 0.6688 0.6153 11.00000 0.05 0.24 Q5 1 -0.0019 0.8110 0.3876 11.00000 0.05 0.24 ; _shelx_res_checksum 55373 _shelx_hkl_file ; 0 0 1 112.36 3.22 0 0 2 406.20 11.43 0 0 3 202.83 5.98 0 0 4 13.10 0.98 0 0 4 12.29 1.19 0 0 5 1088.50 30.54 0 0 5 1073.55 30.43 0 0 6 900.35 27.14 0 0 6 1000.07 27.06 0 0 7 328.45 10.19 0 0 7 339.96 10.35 0 0 8 1887.39 53.39 0 0 8 1907.94 53.48 0 0 9 2707.04 76.02 0 0 10 124.40 4.95 0 0 11 591.09 18.16 0 0 12 15.23 1.70 0 0 -12 16.17 1.44 0 0 -12 14.77 1.34 0 0 13 55.58 3.32 0 0 -13 56.54 3.00 0 0 -13 55.26 2.81 0 0 -14 125.91 4.97 0 0 -15 103.24 4.39 0 0 -16 183.31 6.73 0 0 17 1.01 0.83 0 0 -17 2.17 0.92 0 0 -18 25.22 1.86 0 0 18 26.61 1.91 0 0 19 37.56 2.16 0 0 -19 34.76 2.06 0 0 -20 196.32 6.50 0 0 20 199.10 6.55 0 -1 20 166.85 5.52 0 1 -20 158.85 5.61 0 1 -19 143.42 5.37 0 -1 19 151.33 5.30 0 1 -18 63.82 3.15 0 1 -17 32.29 2.21 0 1 -16 128.05 5.14 0 1 -15 58.54 3.03 0 1 -14 156.45 5.83 0 1 -13 306.19 9.87 0 1 -13 287.86 10.00 0 -1 12 96.04 4.38 0 1 -12 99.02 4.08 0 1 -12 99.03 3.95 0 1 -11 20.79 1.53 0 -1 11 19.28 1.74 0 -1 10 52.76 2.74 0 1 -10 52.16 2.48 0 -1 9 20.77 1.58 0 1 -9 20.53 1.39 0 1 -8 800.37 22.92 0 1 -7 22.07 1.28 0 1 -6 188.74 5.83 0 1 -5 88.83 2.95 0 1 -4 129.33 3.97 0 1 -3 98.93 3.03 0 1 -2 214.55 6.12 0 1 -1 0.37 0.22 0 -1 1 0.34 0.13 0 1 0 82.88 2.56 0 1 0 84.94 2.51 0 1 1 1.54 0.31 0 1 2 107.20 3.32 0 1 3 0.68 0.55 0 1 4 611.10 17.47 0 1 5 86.77 3.14 0 1 6 715.94 20.67 0 1 7 52.25 2.46 0 1 8 46.18 2.41 0 1 9 202.01 6.96 0 1 9 192.12 7.08 0 1 10 1.78 1.03 0 1 10 1.54 0.88 0 1 11 235.44 8.65 0 1 11 247.06 8.77 0 -1 -12 148.00 5.38 0 1 12 136.57 6.10 0 -1 -13 25.09 1.89 0 -1 -14 104.63 4.43 0 -1 -15 5.83 1.15 0 -1 -16 2.52 1.00 0 -1 -16 2.95 0.95 0 -1 -17 100.53 4.13 0 -1 -17 87.33 3.67 0 -1 -18 17.87 1.51 0 -1 -19 25.81 1.65 0 1 19 25.03 1.62 0 1 20 116.16 4.10 0 -2 20 2.34 0.78 0 -2 20 2.60 0.79 0 2 -20 1.42 0.73 0 2 -19 77.89 3.52 0 -2 19 87.62 3.60 0 -2 18 8.76 1.20 0 2 -18 7.67 1.19 0 -2 17 3.96 1.03 0 2 -17 6.45 1.12 0 -2 16 165.05 6.07 0 2 -16 153.98 6.00 0 2 -15 29.05 2.09 0 -2 15 27.00 2.02 0 2 -14 295.65 9.77 0 2 -13 249.15 8.55 0 2 -13 249.41 8.35 0 2 -12 19.12 1.57 0 2 -12 18.79 1.55 0 2 -11 77.47 3.34 0 2 -10 9.20 1.04 0 2 -9 277.39 8.70 0 2 -8 6782.44 187.31 0 2 -7 294.02 8.91 0 2 -6 0.70 0.45 0 2 -5 427.39 12.33 0 2 -4 1108.64 30.96 0 2 -3 137.36 4.23 0 2 -2 1072.29 28.22 0 -2 2 993.20 27.90 0 2 -1 1292.16 35.83 0 2 -1 1280.58 35.70 0 2 0 4617.00 127.84 0 2 0 4668.93 127.96 0 2 2 50.83 2.00 0 2 3 1643.52 45.89 0 2 4 410.68 12.13 0 2 5 288.96 8.98 0 2 6 499.02 14.96 0 2 7 595.71 17.86 0 2 8 54.42 2.87 0 2 9 647.10 19.66 0 2 10 402.05 14.01 0 2 10 445.37 13.97 0 2 11 9.19 1.66 0 -2 -11 13.40 1.32 0 2 11 13.95 1.94 0 -2 -12 2048.26 57.99 0 -2 -13 469.76 14.70 0 -2 -14 103.42 4.39 0 -2 -14 117.38 4.72 0 -2 -15 55.45 2.86 0 -2 -15 61.11 3.11 0 -2 -16 9.76 1.28 0 -2 -16 8.88 1.26 0 -2 -17 150.10 5.62 0 -2 -17 154.94 5.41 0 -2 -18 116.86 4.16 0 -2 -18 122.91 4.41 0 2 19 10.70 0.96 0 -2 -19 11.43 0.97 0 -2 -19 10.57 0.97 0 -3 20 1.28 0.67 0 3 -20 1.81 0.69 0 -3 20 1.70 0.71 0 -3 19 102.88 4.04 0 3 -19 106.70 4.18 0 3 -18 206.63 7.14 0 -3 18 199.91 6.99 0 -3 17 220.14 7.58 0 3 -17 218.76 7.70 0 3 -16 10.09 1.38 0 -3 16 10.24 1.31 0 -3 15 3.37 1.05 0 3 -15 3.29 1.14 0 -3 14 5.95 1.12 0 -3 14 5.91 0.98 0 3 -14 6.37 1.25 0 3 -14 6.49 1.12 0 -3 13 190.20 6.91 0 3 -13 190.49 7.17 0 3 -13 219.54 7.24 0 3 -13 192.11 6.87 0 -3 13 210.66 6.79 0 3 -12 65.85 3.08 0 3 -12 65.83 3.22 0 -3 12 68.41 3.10 0 3 -12 66.12 3.24 0 -3 12 77.83 3.74 0 3 -11 29.36 1.86 0 -3 11 29.55 2.20 0 3 -11 23.56 1.78 0 3 -10 1.59 0.61 0 -3 10 1.87 0.91 0 3 -9 11.86 1.12 0 -3 9 15.55 1.49 0 -3 8 218.85 7.18 0 3 -8 199.75 6.72 0 -3 7 793.30 23.12 0 3 -6 4.13 0.72 0 3 -5 32.84 1.61 0 3 -4 614.01 17.60 0 3 -3 65.57 2.71 0 3 -3 76.59 2.63 0 3 -2 973.18 27.07 0 -3 2 945.28 26.70 0 3 -2 1023.10 27.33 0 3 -1 41.40 1.71 0 3 -1 45.55 1.89 0 3 0 29.47 1.34 0 3 0 29.83 1.52 0 3 1 38.36 1.84 0 3 2 40.05 1.94 0 3 3 75.33 3.05 0 3 4 138.66 4.94 0 3 5 89.88 3.72 0 3 6 9.12 1.24 0 3 7 43.49 2.68 0 3 8 1.13 0.91 0 -3 -9 38.00 2.16 0 3 9 38.02 2.86 0 -3 -10 42.65 2.42 0 3 10 40.52 3.18 0 -3 -10 42.19 2.16 0 -3 -11 20.34 1.67 0 -3 -11 18.33 1.66 0 -3 -11 16.52 1.40 0 -3 -12 396.25 12.87 0 -3 -12 409.83 12.72 0 -3 -13 38.49 2.45 0 3 13 42.26 2.81 0 -3 -13 39.11 2.43 0 -3 -14 52.98 2.91 0 -3 -14 48.67 2.70 0 -3 -15 69.40 3.30 0 -3 -15 75.57 3.49 0 -3 -16 0.17 0.72 0 -3 -16 0.51 0.88 0 -3 -17 70.80 3.05 0 -3 -17 68.32 3.09 0 -3 -17 73.64 3.04 0 -3 -18 95.96 3.77 0 -3 -18 113.73 3.79 0 4 -20 33.59 1.78 0 4 -19 0.85 0.71 0 4 -18 85.84 3.70 0 -4 18 86.89 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104.43 4.36 0 -4 -10 373.35 12.00 0 -4 -10 373.06 11.66 0 -4 -11 2.08 0.96 0 -4 -11 2.39 0.91 0 -4 -12 622.58 18.54 0 -4 -12 633.08 19.07 0 -4 -13 640.59 19.19 0 -4 -13 612.29 19.35 0 4 13 651.63 19.59 0 -4 -13 642.95 19.28 0 -4 -14 766.05 22.42 0 4 14 742.09 22.54 0 -4 -14 725.03 22.14 0 -4 -14 769.52 22.27 0 -4 -15 10.33 1.23 0 -4 -15 13.74 1.40 0 4 15 10.19 1.46 0 -4 -16 37.99 2.05 0 -4 -16 37.96 2.04 0 5 -19 25.88 1.54 0 -5 18 24.26 1.47 0 5 -18 24.21 1.64 0 5 -17 96.10 4.01 0 -5 17 96.38 3.80 0 -5 16 166.34 5.89 0 5 -16 165.11 5.90 0 -5 15 25.05 1.83 0 5 -15 27.60 1.98 0 5 -14 43.20 2.61 0 -5 14 47.79 2.55 0 -5 13 45.69 2.56 0 5 -13 46.52 2.71 0 5 -12 481.09 14.99 0 5 -11 99.41 4.27 0 5 -10 221.05 7.64 0 5 -9 42.86 2.44 0 5 -8 0.89 0.81 0 5 -8 0.34 0.82 0 -5 8 0.58 0.62 0 5 -7 137.04 5.38 0 5 -7 145.92 5.05 0 5 -6 439.45 13.79 0 5 -5 166.62 6.08 0 5 -4 310.11 10.03 0 5 -3 53.60 2.66 0 5 -2 6.81 0.96 0 5 -1 385.85 12.16 0 5 0 4.84 0.96 0 5 1 28.30 1.94 0 5 2 9.66 1.25 0 5 3 63.16 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357.70 11.52 0 -6 8 49.32 2.55 0 6 -8 59.90 2.97 0 -6 7 11.23 1.46 0 -6 7 13.62 1.38 0 -6 7 14.71 1.33 0 6 -7 12.10 1.45 0 -6 6 401.72 12.11 0 -6 6 369.19 12.08 0 -6 5 33.33 2.11 0 -6 4 10.12 1.19 0 6 -4 10.88 1.38 0 -6 4 9.68 1.26 0 -6 3 27.66 1.95 0 6 -3 29.72 2.13 0 6 -2 399.85 13.13 0 -6 2 414.29 12.78 0 6 -1 152.03 5.96 0 -6 1 148.67 5.38 0 -6 0 1303.33 35.73 0 -6 0 1249.22 35.70 0 -6 0 1215.27 35.93 0 6 0 1215.85 36.53 0 -6 -1 2.05 0.91 0 -6 -1 1.92 0.85 0 -6 -1 1.94 0.92 0 -6 -2 295.60 9.32 0 -6 -2 277.37 9.36 0 -6 -2 281.64 9.19 0 -6 -2 275.22 9.11 0 -6 -3 29.55 1.99 0 -6 -3 25.07 1.82 0 -6 -3 28.06 2.00 0 -6 -3 25.97 1.74 0 -6 -4 344.26 11.14 0 -6 -4 340.25 11.00 0 -6 -5 1205.55 35.70 0 -6 -5 1279.39 35.98 0 -6 -6 152.14 5.73 0 -6 -6 148.68 5.84 0 -6 -7 1.46 0.84 0 -6 -8 1.43 0.97 0 -6 -8 1.02 0.80 0 -6 -9 26.78 1.92 0 -6 -9 24.67 1.92 0 -6 -10 28.65 2.01 0 -6 -10 30.33 1.97 0 -6 -11 167.15 5.63 0 -6 -11 145.58 5.68 0 6 12 27.28 1.99 0 -6 -12 25.16 1.73 0 -6 -12 26.24 1.65 0 6 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237.53 7.35 0 -9 7 59.32 2.47 0 -9 6 44.08 2.06 0 9 -6 40.89 2.03 0 9 -5 0.71 0.65 0 -9 5 -0.29 0.65 0 9 -4 17.08 1.27 0 -9 3 59.09 2.66 0 9 -3 64.23 2.68 0 9 -2 206.05 6.63 0 -9 2 203.14 6.70 0 -9 1 33.21 1.80 0 9 -1 31.32 1.71 0 -9 0 73.96 2.80 0 9 0 57.33 2.58 0 -9 -1 25.42 1.48 0 -9 -2 7.91 0.82 1 -9 -2 37.78 1.75 1 -9 -1 2.25 0.78 1 -9 -1 3.26 0.71 1 -9 0 5.03 0.82 1 -9 0 5.17 0.94 1 -9 1 109.80 4.11 1 -9 1 103.22 3.96 1 -9 2 14.60 1.24 1 -9 3 16.44 1.31 -1 9 -3 14.96 1.23 1 -9 3 16.63 1.41 1 -9 4 6.35 1.06 -1 9 -4 6.31 0.87 1 -9 5 14.57 1.19 1 -9 5 14.06 1.30 -1 9 -5 14.57 1.14 1 -9 6 168.95 5.52 -1 9 -6 162.42 5.43 1 -9 6 164.06 5.59 -1 9 -7 40.80 1.84 1 -9 7 34.63 1.85 1 -9 7 39.41 1.84 -1 9 -8 22.84 1.33 1 -8 -8 22.86 1.46 1 -8 -7 34.30 1.92 1 -8 -6 102.47 4.01 1 -8 -5 92.00 3.79 1 -8 -4 21.19 1.67 1 -8 -3 1.87 0.90 1 -8 -3 1.42 0.96 1 -8 -3 1.83 0.71 1 -8 -2 99.22 3.97 1 -8 -2 96.45 3.99 1 -8 -2 96.17 4.10 1 -8 -1 492.91 14.63 1 -8 -1 460.49 14.44 1 -8 0 6.89 1.16 1 -8 1 122.00 4.83 1 -8 2 44.07 2.53 1 -8 3 93.27 3.85 1 -8 4 56.40 2.98 1 -8 4 61.50 2.86 1 -8 5 31.64 1.96 1 -8 5 33.59 2.10 1 -8 6 1.38 0.80 -1 8 -6 1.08 0.79 1 -8 6 1.32 0.87 1 -8 7 16.32 1.46 1 -8 7 19.02 1.56 -1 8 -7 17.73 1.48 1 -8 7 20.26 1.68 1 -8 8 59.34 2.72 1 -8 8 55.11 2.72 -1 8 -8 60.03 2.78 1 -8 8 54.72 2.77 1 -8 9 34.69 2.00 -1 8 -9 33.65 1.93 -1 8 -10 2.28 0.80 1 -8 10 2.81 0.80 1 -8 11 8.90 0.97 -1 8 -11 9.94 1.02 -1 8 -12 129.33 4.55 1 -8 12 123.45 4.39 -1 8 -12 129.98 4.33 1 -8 13 27.32 1.43 -1 8 -13 29.57 1.58 -1 7 12 129.11 4.40 1 -7 -11 65.68 2.77 1 -7 -11 65.65 2.70 1 -7 -10 1.27 0.66 1 -7 -10 0.86 0.77 1 -7 -9 0.39 0.69 1 -7 -9 1.23 0.86 1 -7 -8 1.34 0.78 1 -7 -7 4.15 0.93 1 -7 -7 3.80 1.15 1 -7 -6 322.85 10.63 1 -7 -5 0.76 1.09 1 -7 -4 19.38 1.56 1 -7 -4 17.96 1.76 1 -7 -3 76.05 3.74 1 -7 -3 79.19 3.50 1 -7 -2 138.15 5.45 1 -7 -2 134.77 5.22 1 -7 -1 6.02 1.24 1 -7 -1 6.15 1.14 1 -7 0 6.62 1.22 1 -7 0 8.71 1.34 1 -7 1 108.55 4.73 1 -7 1 121.26 4.69 1 -7 2 480.64 14.26 1 -7 2 430.38 14.21 1 -7 3 1.26 0.89 1 -7 4 134.34 5.30 1 -7 4 133.09 5.33 1 -7 5 16.34 1.59 1 -7 5 13.54 1.52 1 -7 6 3.13 1.02 1 -7 6 2.98 0.88 1 -7 6 3.78 1.10 1 -7 7 288.98 9.64 -1 7 -7 292.90 9.40 1 -7 7 293.85 9.40 1 -7 8 148.78 5.88 1 -7 8 135.14 5.45 1 -7 8 154.82 5.55 -1 7 -8 155.65 5.66 1 -7 9 255.90 9.01 1 -7 9 247.32 8.67 1 -7 9 252.64 8.49 1 -7 10 89.83 3.91 -1 7 -10 94.42 3.88 1 -7 10 85.72 4.06 -1 7 -11 523.93 15.89 1 -7 11 522.18 15.77 -1 7 -11 509.89 15.62 1 -7 11 508.01 15.99 1 -7 12 6.98 1.12 1 -7 12 5.93 1.14 -1 7 -12 5.74 1.24 -1 7 -12 6.97 1.07 1 -7 13 204.01 7.20 -1 7 -13 213.49 7.19 1 -7 13 211.07 7.06 1 -7 14 3.86 0.89 -1 7 -14 5.03 1.00 1 -7 15 41.40 2.10 -1 7 -15 47.51 2.17 1 -7 16 5.68 0.71 -1 6 13 169.35 5.75 1 -6 -13 164.09 5.77 1 -6 -12 30.17 1.82 1 -6 -12 34.77 2.08 1 -6 -11 44.69 2.58 1 -6 -11 49.86 2.51 1 -6 -10 88.53 3.81 1 -6 -10 85.69 3.92 1 -6 -9 0.44 0.82 1 -6 -9 -0.13 0.98 1 -6 -8 1.50 0.86 1 -6 -8 1.23 1.07 1 -6 -7 71.58 3.11 1 -6 -6 43.56 2.65 1 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1.54 2 -8 11 1.28 0.58 2 -8 12 308.78 9.21 2 -7 -10 37.63 1.95 2 -7 -9 38.66 2.15 2 -7 -8 10.53 1.00 2 -7 -7 57.11 2.57 2 -7 -6 198.05 6.56 2 -7 -6 190.62 7.03 2 -7 -5 1.70 0.86 2 -7 -5 1.87 1.18 2 -7 -5 2.34 0.82 2 -7 -4 14.67 1.69 2 -7 -4 16.40 1.40 2 -7 -4 16.04 1.58 2 -7 -4 14.96 1.40 2 -7 -3 1.66 0.84 2 -7 -3 0.69 0.74 2 -7 -3 1.07 1.07 2 -7 -3 0.22 1.11 2 -7 -2 1.74 0.96 2 -7 -2 1.22 1.15 2 -7 -2 1.74 1.10 2 -7 -2 2.02 0.82 2 -7 -1 390.14 12.69 2 -7 -1 392.45 12.80 2 -7 -1 397.55 12.68 2 -7 0 0.93 0.96 2 -7 0 -0.07 0.99 2 -7 0 0.24 1.17 2 -7 1 42.07 2.43 2 -7 1 52.58 2.75 2 -7 1 42.46 2.77 2 -7 1 48.65 2.70 2 -7 2 55.84 2.82 2 -7 2 60.00 3.44 2 -7 3 0.67 1.03 2 -7 3 0.65 0.87 2 -7 3 0.83 1.13 2 -7 3 0.41 0.87 2 -7 4 42.09 2.53 2 -7 4 42.39 2.68 2 -7 4 42.16 2.83 2 -7 5 2.81 1.12 2 -7 5 1.56 1.21 2 -7 5 2.54 1.03 2 -7 6 0.46 0.88 2 -7 6 1.42 0.94 -2 7 -6 0.98 0.82 2 -7 6 1.32 1.08 -2 7 -7 35.63 2.10 2 -7 7 32.24 2.25 2 -7 7 31.62 2.24 2 -7 7 34.31 2.22 2 -7 8 72.11 3.57 2 -7 8 77.16 3.50 2 -7 8 74.57 3.39 2 -7 9 41.13 2.52 2 -7 10 29.18 2.05 -2 7 -11 29.71 1.89 2 -7 11 26.85 1.90 -2 7 -12 24.48 1.64 2 -7 12 22.76 1.66 -2 7 -13 140.05 4.87 2 -7 13 143.90 5.07 2 -6 -13 9.15 0.97 2 -6 -12 141.20 5.10 2 -6 -11 141.51 5.18 2 -6 -11 144.17 5.30 2 -6 -10 -0.45 0.91 2 -6 -10 0.20 0.58 2 -6 -10 0.12 0.71 2 -6 -9 11.49 1.16 2 -6 -9 9.76 1.41 2 -6 -9 11.27 1.31 2 -6 -8 22.98 1.80 2 -6 -8 23.91 1.99 2 -6 -8 21.94 1.60 2 -6 -7 13.21 1.34 2 -6 -7 13.98 1.45 2 -6 -6 103.30 4.26 2 -6 -6 114.57 4.62 2 -6 -5 1.18 0.81 2 -6 -5 1.49 1.14 2 -6 -5 1.00 0.93 2 -6 -5 1.71 0.86 2 -6 -4 135.36 5.84 2 -6 -4 145.72 5.69 2 -6 -4 159.58 5.76 2 -6 -4 144.27 5.52 2 -6 -4 152.94 5.48 2 -6 -3 20.17 1.88 2 -6 -3 18.30 1.98 2 -6 -3 17.86 1.65 2 -6 -3 22.30 1.75 2 -6 -3 17.58 1.53 2 -6 -2 1492.01 43.35 2 -6 -2 1434.43 43.09 2 -6 -2 1581.96 43.44 2 -6 -2 1518.86 42.81 2 -6 -1 745.39 21.98 2 -6 -1 755.38 22.13 2 -6 -1 711.60 21.99 2 -6 -1 727.86 21.51 2 -6 -1 734.54 22.29 2 -6 0 243.27 8.24 2 -6 0 224.67 8.17 2 -6 0 236.17 8.10 2 -6 0 222.06 8.39 2 -6 0 232.01 7.71 2 -6 0 245.28 7.81 2 -6 1 21.42 1.89 2 -6 1 24.18 1.64 2 -6 1 20.37 1.86 2 -6 1 23.32 1.87 2 -6 1 25.85 1.69 2 -6 2 135.91 5.35 2 -6 2 150.92 5.69 2 -6 2 151.24 5.35 2 -6 2 150.31 5.30 2 -6 2 141.75 5.92 2 -6 3 103.24 4.40 2 -6 3 118.93 4.80 2 -6 3 124.57 5.11 2 -6 3 107.28 4.81 2 -6 3 116.36 4.44 2 -6 4 193.62 6.74 2 -6 4 182.19 6.66 2 -6 4 188.80 7.12 2 -6 4 203.78 7.19 2 -6 4 205.07 7.36 2 -6 5 267.28 9.28 2 -6 5 255.70 8.73 2 -6 5 280.97 9.39 2 -6 5 276.09 9.23 2 -6 5 263.68 8.84 2 -6 6 139.85 5.43 2 -6 6 141.13 5.55 2 -6 6 131.56 5.20 2 -6 7 28.55 1.96 2 -6 7 27.33 2.03 2 -6 7 31.49 2.21 2 -6 8 595.08 18.07 2 -6 8 605.54 18.22 2 -6 9 2.65 0.85 2 -6 10 441.84 13.81 2 -6 11 105.03 4.36 -2 6 -11 112.29 4.52 -2 6 -12 0.17 0.89 2 -6 12 0.06 0.74 -2 6 -13 132.03 4.77 2 -6 13 117.77 4.60 -2 6 -14 67.54 2.85 2 -6 14 72.33 3.22 2 -6 15 4.80 0.95 -2 6 -15 5.34 0.80 2 -6 16 7.81 0.89 2 -5 -15 30.99 1.76 2 -5 -14 297.14 9.51 2 -5 -13 71.36 3.33 2 -5 -12 20.14 1.69 2 -5 -12 21.91 1.66 2 -5 -11 91.66 3.66 2 -5 -11 94.90 4.00 2 -5 -11 93.09 4.16 2 -5 -10 142.14 5.56 2 -5 -10 133.13 5.04 2 -5 -10 140.05 5.39 2 -5 -9 140.02 5.39 2 -5 -9 132.37 5.38 2 -5 -9 129.75 5.01 2 -5 -8 0.73 1.04 2 -5 -8 0.51 0.75 2 -5 -8 0.87 0.76 2 -5 -7 1.26 1.13 2 -5 -7 0.91 0.84 2 -5 -7 1.30 0.80 2 -5 -6 57.86 2.96 2 -5 -6 54.43 2.78 2 -5 -5 70.43 3.37 2 -5 -5 77.47 3.47 2 -5 -5 72.57 3.28 2 -5 -4 13.42 1.33 2 -5 -4 9.96 1.57 2 -5 -4 14.02 1.54 2 -5 -4 12.17 1.29 2 -5 -4 11.39 1.24 2 -5 -3 260.79 8.89 2 -5 -3 250.07 8.75 2 -5 -3 241.31 8.37 2 -5 -3 264.56 8.72 2 -5 -3 262.94 8.63 2 -5 -3 247.06 8.27 2 -5 -3 269.79 8.57 2 -5 -3 252.80 8.49 2 -5 -3 257.43 8.33 2 -5 -2 2.12 1.01 2 -5 -2 1.67 0.74 2 -5 -2 0.45 0.78 2 -5 -2 1.31 1.06 2 -5 -2 0.11 0.71 2 -5 -1 172.42 6.30 2 -5 -1 176.27 5.95 2 -5 -1 168.13 5.97 2 -5 -1 177.81 6.16 2 -5 -1 174.57 6.45 2 -5 0 102.00 4.24 2 -5 0 93.51 4.02 2 -5 0 91.14 3.74 2 -5 0 99.28 3.74 2 -5 1 279.65 9.85 2 -5 1 292.08 9.50 2 -5 1 318.22 9.43 2 -5 1 303.07 9.71 2 -5 2 267.48 9.15 2 -5 2 285.49 9.13 2 -5 2 294.34 8.94 2 -5 3 56.79 3.02 2 -5 3 52.96 2.67 2 -5 3 58.61 2.57 2 -5 4 4.78 1.21 2 -5 4 6.22 1.05 2 -5 4 3.50 0.77 2 -5 4 5.25 0.96 2 -5 5 157.49 5.98 2 -5 5 140.48 5.44 2 -5 5 157.57 5.80 2 -5 5 141.86 5.52 2 -5 5 159.41 5.75 2 -5 5 147.74 5.84 2 -5 6 43.32 2.48 2 -5 6 52.62 2.65 2 -5 6 42.64 2.51 2 -5 6 47.78 2.82 2 -5 6 43.37 2.62 2 -5 6 47.72 2.58 2 -5 6 45.91 2.54 2 -5 7 13.57 1.60 2 -5 7 12.22 1.38 2 -5 7 12.94 1.45 2 -5 7 12.84 1.46 2 -5 7 12.29 1.34 2 -5 8 121.56 4.85 2 -5 8 106.41 4.68 2 -5 9 229.46 8.17 2 -5 9 230.40 8.11 2 -5 10 67.75 3.46 2 -5 11 98.70 4.41 -2 5 -11 99.08 4.25 -2 5 -12 3.48 1.11 2 -5 12 3.51 1.07 -2 5 -13 15.04 1.48 2 -5 13 15.29 1.54 -2 5 -14 91.22 3.74 2 -5 14 89.99 3.93 -2 5 -15 16.66 1.32 2 -5 15 18.18 1.44 2 -5 16 18.80 1.36 2 -5 17 0.46 0.49 2 -5 17 0.74 0.64 2 -5 18 56.25 2.31 2 -4 -17 7.99 0.85 2 -4 -16 36.72 2.04 2 -4 -15 2.35 0.80 2 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2 -4 5 101.61 3.93 2 -4 6 389.81 11.79 2 -4 6 351.31 11.64 2 -4 6 373.80 11.54 2 -4 6 381.82 11.82 2 -4 7 92.52 3.84 2 -4 7 87.16 3.44 2 -4 8 48.56 2.70 2 -4 9 136.40 5.36 2 -4 9 139.49 5.08 2 -4 10 175.83 6.36 -2 4 -10 165.50 6.10 -2 4 -11 2554.75 72.28 2 -4 11 2587.48 72.08 -2 4 -12 194.76 6.89 -2 4 -13 13.74 1.41 -2 4 -14 5.47 1.03 2 -4 14 6.84 1.20 2 -4 15 56.12 2.86 2 -4 16 232.48 8.06 2 -4 16 242.06 7.90 2 -4 17 137.48 5.11 2 -4 17 142.96 5.01 2 -4 18 21.04 1.38 2 -4 18 20.96 1.37 2 -3 -18 26.61 1.58 2 -3 -18 25.98 1.50 2 -3 -17 2.31 0.77 2 -3 -15 240.77 8.35 2 -3 -14 1.40 0.90 2 -3 -13 114.83 4.90 2 -3 -12 7.66 1.24 2 -3 -12 6.72 1.01 2 -3 -11 163.34 6.24 2 -3 -10 147.84 5.69 2 -3 -10 141.87 5.63 2 -3 -10 148.84 5.41 2 -3 -9 218.78 7.86 2 -3 -9 216.84 7.84 2 -3 -8 118.26 4.70 2 -3 -8 119.23 4.65 2 -3 -8 127.51 4.94 2 -3 -7 1.25 0.81 2 -3 -6 127.86 4.65 2 -3 -6 134.26 4.91 2 -3 -5 200.68 6.52 2 -3 -5 195.49 6.40 2 -3 -5 181.75 6.16 2 -3 -4 2.35 0.71 2 -3 -4 2.32 0.65 2 -3 -4 2.73 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7.67 1.28 2 -2 -13 833.22 24.85 2 -2 -13 833.91 24.85 2 -2 -12 17.31 1.61 2 -2 -12 16.64 1.40 2 -2 -12 17.67 1.66 2 -2 -11 427.19 13.64 2 -2 -11 460.23 13.69 2 -2 -11 421.46 13.19 2 -2 -10 22.59 1.77 2 -2 -10 22.64 1.57 2 -2 -10 23.10 1.74 2 -2 -9 277.57 8.84 2 -2 -9 264.14 8.52 2 -2 -8 396.34 12.30 2 -2 -7 1.59 0.72 2 -2 -6 133.71 4.49 2 -2 -6 125.84 4.30 2 -2 -5 628.45 18.38 2 -2 -5 640.17 18.24 2 -2 -4 494.19 14.33 2 -2 -4 481.45 14.12 2 -2 -4 482.10 14.26 2 -2 -3 2.18 0.70 2 -2 -3 1.72 0.55 2 -2 -3 1.79 0.63 2 -2 -2 636.56 17.85 2 -2 -2 595.47 17.63 2 -2 -2 615.28 17.67 2 -2 -1 2.25 0.64 2 -2 -1 3.01 0.64 2 -2 0 1.16 0.57 2 -2 0 0.51 0.49 2 -2 0 0.80 0.60 2 -2 0 1.06 0.59 2 -2 1 989.96 27.66 2 -2 1 967.85 27.88 2 -2 2 863.72 25.30 2 -2 2 900.55 25.28 2 -2 2 917.39 25.50 2 -2 3 2477.07 69.56 -2 2 -3 2460.20 69.26 2 -2 3 2558.29 69.40 2 -2 4 498.05 14.53 2 -2 4 490.64 14.35 2 -2 5 39.56 1.81 2 -2 5 38.29 1.93 2 -2 5 43.20 1.83 2 -2 6 130.62 4.64 2 -2 6 137.95 4.66 2 -2 6 136.17 4.47 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7.32 2 2 -9 641.20 19.20 2 2 -8 44.13 2.34 2 2 -7 189.53 6.42 2 2 -6 118.46 4.37 2 2 -5 26.52 1.56 2 2 -5 23.45 1.20 2 2 -4 4.29 0.72 2 2 -4 4.11 0.49 2 2 -3 2277.68 60.62 2 2 -3 2114.81 60.18 2 2 -2 47.62 2.09 2 2 -2 43.40 1.68 2 2 -1 458.76 13.84 2 2 -1 475.77 13.45 2 2 0 367.05 10.67 2 2 0 364.92 11.05 2 2 1 3.09 0.57 2 2 2 568.44 16.48 2 2 3 4.04 0.78 2 2 4 2.79 0.75 2 2 5 1027.85 29.60 2 2 6 0.81 0.73 2 2 7 0.92 0.78 2 2 8 108.28 4.87 2 2 8 117.19 4.50 2 2 9 0.49 0.88 2 2 9 1.00 0.91 2 2 10 182.58 6.90 2 2 10 165.21 6.31 2 2 11 606.92 19.02 2 2 11 607.09 18.50 2 2 12 2.28 0.98 2 2 12 0.43 1.37 2 2 13 172.99 6.53 2 2 13 186.44 7.03 2 2 14 67.48 3.26 2 2 15 10.23 1.30 -2 -2 -16 809.35 22.61 2 2 16 741.80 22.66 2 2 17 32.66 1.82 -2 -2 -17 36.31 1.85 -2 -2 -18 1.97 0.62 2 3 -20 1.50 0.59 2 3 -19 140.91 4.96 2 3 -19 142.83 5.04 2 3 -18 111.77 4.32 2 3 -18 118.07 4.47 2 3 -17 32.98 2.04 2 3 -17 35.41 2.17 2 3 -16 1.18 0.76 2 3 -16 0.86 0.85 2 3 -15 37.13 2.24 2 3 -15 39.76 2.39 2 3 -14 139.80 5.46 2 3 -14 151.40 5.69 2 3 -14 150.86 5.38 -2 -3 14 153.30 5.09 2 3 -13 41.95 2.30 -2 -3 13 43.00 2.01 2 3 -13 38.91 2.26 2 3 -12 2.22 0.84 -2 -3 12 1.89 0.69 2 3 -12 2.59 0.99 2 3 -11 197.68 6.72 2 3 -11 207.21 7.01 -2 -3 11 193.39 6.43 2 3 -11 213.84 7.60 2 3 -10 754.82 22.19 2 3 -9 253.43 8.25 2 3 -8 71.91 3.07 2 3 -7 2.56 0.63 2 3 -6 45.44 2.06 2 3 -5 331.68 9.96 2 3 -4 137.89 4.55 2 3 -3 458.96 13.42 2 3 -2 1507.85 42.25 2 3 -1 239.71 7.42 2 3 0 1427.98 40.19 2 3 1 104.06 3.81 2 3 2 198.49 6.56 2 3 3 232.69 7.70 2 3 4 8.58 1.13 2 3 5 -0.13 0.79 2 3 6 164.18 6.42 2 3 6 175.34 6.12 2 3 7 47.07 2.53 2 3 7 41.36 2.77 2 3 8 303.70 11.00 2 3 8 326.23 10.44 2 3 9 122.85 5.21 2 3 9 102.75 4.57 2 3 10 8.33 1.32 2 3 10 8.56 1.71 2 3 11 117.68 5.08 2 3 11 132.92 5.60 2 3 12 16.08 1.65 2 3 12 19.03 2.09 2 3 13 12.26 1.39 2 3 13 10.61 1.69 -2 -3 -14 10.77 1.29 2 3 14 9.67 1.20 2 3 15 163.81 5.76 -2 -3 -15 167.45 5.74 2 3 16 32.58 1.72 2 4 -19 140.94 4.86 2 4 -18 101.72 3.85 2 4 -18 106.68 4.03 2 4 -17 145.40 5.18 2 4 -17 146.55 5.36 2 4 -16 35.63 2.04 2 4 -16 36.23 2.23 2 4 -15 10.46 1.20 2 4 -15 10.52 1.39 -2 -4 15 11.65 1.10 2 4 -15 9.72 1.17 2 4 -14 96.26 3.89 -2 -4 14 94.21 3.63 2 4 -14 89.96 3.82 2 4 -13 8.24 1.15 -2 -4 13 11.63 1.11 2 4 -13 9.96 1.29 2 4 -12 19.58 1.51 -2 -4 12 18.09 1.34 2 4 -12 17.77 1.71 2 4 -11 1277.81 38.22 -2 -4 11 1370.66 37.72 2 4 -10 16.33 1.55 -2 -4 10 17.53 1.31 2 4 -9 18.73 1.55 2 4 -9 17.88 1.71 2 4 -8 332.53 10.73 2 4 -8 348.00 10.89 2 4 -8 356.83 11.33 2 4 -7 75.81 3.23 2 4 -7 75.56 3.22 2 4 -7 83.62 3.62 2 4 -6 162.89 5.99 2 4 -6 164.25 5.64 2 4 -5 8.96 1.13 2 4 -5 8.79 0.91 2 4 -4 5.45 0.89 2 4 -4 5.87 0.77 2 4 -3 6.01 0.78 2 4 -3 5.97 0.92 2 4 -2 56.43 2.54 2 4 -2 57.23 2.81 2 4 -1 202.06 6.58 2 4 -1 188.97 6.82 2 4 0 1445.32 41.05 2 4 1 14.37 1.28 2 4 2 562.24 16.97 2 4 3 584.95 17.80 2 4 4 52.43 2.53 2 4 4 51.79 2.96 2 4 5 85.24 4.27 2 4 5 93.51 3.77 2 4 6 131.76 5.95 2 4 6 140.82 5.34 2 4 7 26.78 1.92 2 4 7 28.07 2.46 2 4 8 0.09 1.41 2 4 8 0.97 0.79 2 4 9 169.08 6.27 -2 -4 -10 168.16 5.98 2 4 10 156.20 6.02 -2 -4 -11 18.97 1.68 2 4 11 19.52 1.62 2 4 11 17.01 1.97 -2 -4 -12 299.60 9.32 2 4 12 297.94 10.09 2 4 12 282.37 9.50 -2 -4 -12 300.23 9.56 2 4 13 27.76 2.14 -2 -4 -13 31.28 1.93 -2 -4 -14 56.16 2.57 -2 -4 -15 0.36 0.68 -2 -4 -16 69.74 2.55 2 5 -18 23.72 1.47 -2 -5 17 107.61 3.73 2 5 -17 86.41 3.72 2 5 -16 147.17 5.39 2 5 -15 0.50 0.63 2 5 -15 0.43 0.84 2 5 -14 141.07 5.32 -2 -5 14 158.37 5.25 2 5 -14 153.20 5.55 2 5 -13 43.25 2.32 2 5 -13 51.43 2.74 -2 -5 13 47.73 2.29 2 5 -12 3.02 1.03 -2 -5 12 1.52 0.70 2 5 -11 170.07 6.58 -2 -5 11 198.43 6.24 2 5 -10 710.17 21.18 2 5 -9 465.07 14.35 -2 -5 8 211.53 7.23 2 5 -8 228.34 7.60 -2 -5 8 230.89 7.21 2 5 -7 136.74 5.09 2 5 -6 172.70 6.08 2 5 -6 173.22 6.29 2 5 -6 184.11 6.71 2 5 -5 18.10 1.43 2 5 -5 19.80 1.72 2 5 -5 18.57 1.47 2 5 -4 6.36 0.96 2 5 -4 5.39 1.02 2 5 -4 5.62 0.93 2 5 -3 0.21 0.70 2 5 -3 2.21 0.78 2 5 -2 96.45 4.01 2 5 -1 1222.24 35.28 2 5 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3 -7 3 112.02 4.11 3 -7 3 112.91 4.38 3 -7 3 110.63 4.71 3 -7 4 16.37 1.54 3 -7 4 20.12 1.63 3 -7 4 19.54 1.42 3 -7 5 124.49 4.78 3 -7 5 119.67 4.52 3 -7 5 135.41 5.16 3 -7 6 19.10 1.55 3 -7 6 18.69 1.37 3 -7 6 20.65 1.76 3 -7 7 422.19 12.92 3 -7 7 430.09 12.94 3 -7 7 407.38 12.61 3 -7 8 20.92 1.37 3 -7 8 23.80 1.64 3 -7 9 24.63 1.57 3 -7 9 21.11 1.33 3 -7 10 0.58 0.65 3 -7 11 2.26 0.64 3 -7 12 51.38 2.12 3 -6 -11 55.74 2.26 3 -6 -10 18.22 1.29 3 -6 -9 15.15 1.26 3 -6 -8 41.85 2.21 3 -6 -7 16.69 1.40 3 -6 -7 18.33 1.46 3 -6 -6 101.45 4.05 3 -6 -5 2.58 1.26 3 -6 -5 1.26 0.90 3 -6 -5 1.97 0.88 3 -6 -4 3.14 1.09 3 -6 -3 -0.05 0.72 3 -6 -3 0.44 1.13 3 -6 -2 3.64 1.25 3 -6 -2 2.88 0.82 3 -6 -1 218.63 8.14 3 -6 -1 212.60 7.36 3 -6 -1 237.32 7.63 3 -6 0 44.48 2.66 3 -6 0 46.90 2.64 3 -6 0 50.26 2.53 3 -6 0 47.09 2.40 3 -6 1 0.32 1.05 3 -6 1 0.77 0.85 3 -6 1 1.23 0.72 3 -6 1 0.74 0.73 3 -6 2 52.97 2.88 3 -6 2 55.20 2.76 3 -6 2 54.91 2.85 3 -6 2 47.55 3.05 3 -6 2 54.78 2.55 3 -6 3 33.94 2.27 3 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4.20 3 -5 -4 83.82 3.93 3 -5 -4 82.42 3.60 3 -5 -3 727.39 22.61 3 -5 -3 725.35 22.37 3 -5 -3 768.07 22.06 3 -5 -3 746.15 21.89 3 -5 -2 717.41 20.68 3 -5 -2 671.87 20.49 3 -5 -2 672.15 20.00 3 -5 -2 643.34 19.76 3 -5 -1 1571.05 45.91 3 -5 -1 1639.26 45.66 3 -5 -1 1586.08 46.39 3 -5 -1 1640.98 45.91 3 -5 0 19.37 1.63 3 -5 0 20.09 1.59 3 -5 0 17.77 1.46 3 -5 1 57.25 2.79 3 -5 1 51.99 2.86 3 -5 1 53.54 2.76 3 -5 1 54.02 2.51 3 -5 2 -0.06 1.09 3 -5 2 0.73 0.69 3 -5 2 0.16 1.18 3 -5 2 0.56 0.77 3 -5 2 0.76 0.80 3 -5 3 14.45 1.63 3 -5 3 13.38 1.45 3 -5 3 14.92 1.81 3 -5 3 13.82 1.39 3 -5 3 12.42 1.16 3 -5 4 61.38 3.09 3 -5 4 63.09 3.12 3 -5 4 60.36 3.30 3 -5 4 56.56 2.99 3 -5 5 30.84 2.21 3 -5 5 31.89 2.25 3 -5 5 38.11 2.49 3 -5 5 33.15 2.24 3 -5 6 271.32 9.33 3 -5 6 284.04 9.59 3 -5 6 274.60 9.46 3 -5 6 288.32 9.06 3 -5 6 274.73 9.46 3 -5 7 10.07 1.28 3 -5 7 10.02 1.48 3 -5 7 9.84 1.36 3 -5 7 11.74 1.40 3 -5 7 10.83 1.38 3 -5 8 84.83 3.94 3 -5 8 76.19 3.74 3 -5 9 23.95 2.00 3 -5 9 22.57 1.87 3 -5 10 340.24 11.15 3 -5 10 336.59 11.20 3 -5 11 4.71 1.19 3 -5 11 5.06 1.02 3 -5 12 81.87 3.73 3 -5 12 84.41 3.71 3 -5 13 26.16 1.83 3 -5 13 26.20 1.78 3 -5 14 14.97 1.27 3 -5 15 132.53 4.60 3 -4 -15 27.25 1.65 3 -4 -14 215.12 6.84 3 -4 -14 190.74 6.39 3 -4 -13 5.03 0.83 3 -4 -13 5.46 0.94 3 -4 -12 0.95 0.73 3 -4 -12 -0.05 0.69 3 -4 -11 0.32 0.70 3 -4 -11 1.12 0.79 3 -4 -10 140.28 5.37 3 -4 -10 143.63 5.48 3 -4 -9 49.15 2.92 3 -4 -9 50.82 2.73 3 -4 -9 47.86 2.66 3 -4 -8 3.48 1.24 3 -4 -8 4.14 0.91 3 -4 -8 2.71 0.87 3 -4 -7 10.48 1.29 3 -4 -7 11.66 1.73 3 -4 -7 12.32 1.34 3 -4 -6 14.98 1.45 3 -4 -6 12.93 1.49 3 -4 -6 15.43 1.82 3 -4 -5 193.77 6.46 3 -4 -5 195.62 6.60 3 -4 -5 189.07 6.72 3 -4 -5 195.71 6.80 3 -4 -4 1.78 0.98 3 -4 -4 0.72 0.99 3 -4 -4 1.61 0.78 3 -4 -4 4.26 1.28 3 -4 -3 77.72 3.24 3 -4 -3 79.30 3.60 3 -4 -3 78.76 3.71 3 -4 -3 73.38 3.55 3 -4 -3 66.19 3.37 3 -4 -3 72.78 3.19 3 -4 -2 177.20 5.78 3 -4 -2 154.44 5.84 3 -4 -2 184.34 6.24 3 -4 -2 158.96 6.34 3 -4 -2 161.19 6.20 3 -4 -2 161.13 5.68 3 -4 -2 153.64 6.04 3 -4 -1 17.00 1.44 3 -4 -1 16.40 1.72 3 -4 -1 18.17 1.81 3 -4 -1 14.71 1.52 3 -4 -1 17.63 1.32 3 -4 0 221.86 7.25 3 -4 0 222.18 7.01 3 -4 1 7.67 1.04 3 -4 1 7.03 1.31 3 -4 1 7.15 1.32 3 -4 1 8.38 0.93 3 -4 2 15.93 1.47 3 -4 2 17.19 1.73 3 -4 2 14.98 1.63 3 -4 2 15.79 1.63 3 -4 2 14.04 1.46 3 -4 3 203.09 7.20 3 -4 3 228.35 7.40 3 -4 3 209.00 7.68 3 -4 3 214.31 7.55 3 -4 3 200.59 7.38 3 -4 4 131.16 5.05 3 -4 4 133.81 5.11 3 -4 4 127.06 5.03 3 -4 4 135.23 5.28 3 -4 5 55.37 2.85 3 -4 5 50.58 2.78 3 -4 5 52.10 2.85 3 -4 5 49.40 2.85 3 -4 5 56.30 2.67 3 -4 6 138.72 5.23 3 -4 6 149.79 5.66 3 -4 6 143.24 5.42 3 -4 6 154.91 5.30 3 -4 7 15.82 1.67 3 -4 7 18.35 1.68 3 -4 8 9.40 1.40 3 -4 8 11.10 1.42 3 -4 9 79.79 3.94 3 -4 9 79.35 3.90 3 -4 9 84.04 3.64 3 -4 10 89.06 4.33 3 -4 10 100.58 4.01 3 -4 11 199.01 7.39 3 -4 12 63.18 3.31 3 -4 13 104.47 4.44 3 -4 13 109.77 4.57 3 -4 14 45.14 2.50 3 -4 15 40.41 2.18 3 -4 16 56.20 2.48 3 -3 -17 128.51 4.42 3 -3 -16 29.52 1.76 3 -3 -15 206.27 7.01 3 -3 -15 210.02 6.98 3 -3 -15 202.97 6.66 3 -3 -14 21.08 1.62 3 -3 -14 19.15 1.46 3 -3 -13 49.87 2.73 3 -3 -13 46.38 2.48 3 -3 -13 48.38 2.63 3 -3 -12 5.61 1.12 3 -3 -12 6.69 1.07 3 -3 -11 57.56 3.07 3 -3 -10 646.12 19.61 3 -3 -9 365.13 11.77 3 -3 -8 136.94 5.04 3 -3 -8 151.45 5.72 3 -3 -7 6.62 1.10 3 -3 -7 6.43 1.33 3 -3 -6 2.74 0.91 3 -3 -6 2.33 1.08 3 -3 -6 2.94 0.95 3 -3 -5 41.93 2.36 3 -3 -5 33.50 2.29 3 -3 -5 40.39 2.27 3 -3 -5 34.99 2.08 3 -3 -4 250.97 8.06 3 -3 -4 236.82 8.12 3 -3 -4 225.50 8.06 3 -3 -4 235.04 7.92 3 -3 -4 241.36 7.84 3 -3 -4 225.15 7.77 3 -3 -3 206.64 6.89 3 -3 -3 200.88 7.09 3 -3 -3 200.73 6.97 3 -3 -3 196.68 6.72 3 -3 -3 190.46 6.79 3 -3 -2 706.23 20.76 3 -3 -2 728.45 21.26 3 -3 -2 690.72 21.01 3 -3 -2 719.71 20.79 3 -3 -2 697.20 20.90 3 -3 -1 30.11 1.81 3 -3 -1 31.51 1.83 3 -3 -1 30.08 2.02 3 -3 -1 31.92 1.94 3 -3 0 201.38 6.40 3 -3 0 189.59 6.38 3 -3 1 175.37 5.80 3 -3 1 165.01 6.15 3 -3 1 160.13 5.97 3 -3 1 173.77 5.83 3 -3 1 151.57 5.83 3 -3 2 734.75 21.40 3 -3 2 684.51 21.17 3 -3 2 717.69 21.00 3 -3 2 721.94 21.07 3 -3 3 12.00 1.38 3 -3 3 11.04 1.33 3 -3 3 12.59 1.21 3 -3 3 10.99 1.17 3 -3 4 84.36 3.79 3 -3 4 84.26 3.65 3 -3 4 86.43 3.64 3 -3 4 83.29 3.55 3 -3 5 30.70 1.95 3 -3 5 32.72 2.05 3 -3 5 28.83 1.84 3 -3 6 43.24 2.46 3 -3 6 37.50 2.13 3 -3 6 43.81 2.38 3 -3 6 36.88 2.44 3 -3 7 328.54 10.48 3 -3 7 320.20 10.11 3 -3 7 307.26 10.37 3 -3 7 304.65 9.93 3 -3 8 44.27 2.69 3 -3 8 42.34 2.66 3 -3 8 42.37 2.40 3 -3 9 39.77 2.59 3 -3 9 38.06 2.34 3 -3 9 35.99 2.46 3 -3 10 2.43 1.10 3 -3 10 2.41 1.14 3 -3 10 2.86 1.13 3 -3 10 2.06 1.00 3 -3 10 1.78 1.17 3 -3 11 1319.20 39.05 3 -3 11 1340.86 38.42 3 -3 11 1312.89 38.58 3 -3 11 1408.83 38.37 3 -3 11 1306.39 38.61 3 -3 12 116.57 5.06 3 -3 12 114.89 4.70 3 -3 12 112.52 4.53 3 -3 12 117.37 4.80 3 -3 13 28.39 2.17 3 -3 13 27.48 1.92 3 -3 13 31.48 2.13 3 -3 14 0.65 0.85 3 -3 14 0.07 0.81 3 -3 15 11.63 1.29 3 -3 15 11.64 1.26 3 -3 16 104.17 4.07 3 -3 16 106.53 3.96 3 -2 -18 168.06 5.46 3 -2 -17 26.62 1.62 3 -2 -17 26.84 1.70 3 -2 -16 233.06 7.79 3 -2 -16 236.01 7.81 3 -2 -15 149.09 5.38 3 -2 -15 129.22 5.23 3 -2 -14 6.92 1.14 3 -2 -14 6.16 1.25 3 -2 -13 307.29 10.22 3 -2 -12 2.01 0.89 3 -2 -12 0.29 0.99 3 -2 -11 -0.20 0.86 3 -2 -11 1.19 0.88 3 -2 -11 0.51 0.78 3 -2 -10 13.55 1.41 3 -2 -10 10.89 1.36 3 -2 -10 12.12 1.34 3 -2 -9 143.32 5.68 3 -2 -9 145.52 5.45 3 -2 -8 59.94 3.01 3 -2 -8 65.92 3.20 3 -2 -8 67.29 2.99 3 -2 -7 99.81 4.21 3 -2 -7 112.04 4.35 3 -2 -6 93.34 3.81 3 -2 -6 100.19 3.82 3 -2 -5 33.17 1.93 3 -2 -5 27.13 1.72 3 -2 -4 480.17 14.45 3 -2 -3 371.23 11.40 3 -2 -2 30.27 1.69 3 -2 -2 29.04 1.76 3 -2 -2 28.91 1.75 3 -2 -1 218.43 7.06 3 -2 -1 228.77 7.18 3 -2 -1 208.58 7.14 3 -2 0 54.61 2.44 3 -2 1 115.87 4.28 3 -2 1 117.92 4.36 3 -2 2 5.73 0.86 3 -2 2 5.82 0.84 3 -2 3 92.07 3.64 3 -2 4 92.44 3.63 3 -2 5 97.45 3.78 3 -2 5 82.88 3.52 3 -2 6 2.01 0.79 3 -2 7 139.45 5.33 3 -2 7 134.37 5.08 3 -2 8 4.39 1.02 3 -2 8 4.95 1.09 3 -2 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5.11 1.10 4 0 -5 8.08 1.11 4 0 -5 6.62 1.06 4 0 -5 6.88 0.98 4 0 -5 6.97 1.20 4 0 -5 7.15 1.09 4 0 -4 -0.33 0.80 4 0 -4 0.35 0.72 4 0 -4 0.36 0.70 4 0 -4 0.11 0.72 4 0 -4 0.50 0.59 4 0 -4 0.22 0.84 4 0 -4 0.78 0.75 4 0 -3 3.12 0.88 4 0 -3 3.19 0.93 4 0 -3 1.86 0.82 4 0 -3 3.26 0.88 4 0 -2 40.08 2.34 4 0 -2 37.66 2.20 4 0 -2 42.25 2.25 4 0 -1 209.77 7.32 4 0 -1 202.49 6.66 4 0 0 717.10 21.64 4 0 0 723.20 21.79 4 0 0 729.79 21.46 4 0 0 741.90 21.18 4 0 0 732.15 21.45 4 0 1 38.69 2.26 4 0 1 34.25 2.29 4 0 1 37.30 2.13 4 0 1 35.37 1.89 4 0 1 36.94 2.12 4 0 2 1.43 0.81 4 0 2 1.59 1.00 4 0 2 1.63 0.61 4 0 2 1.86 0.83 4 0 3 92.63 3.88 4 0 3 97.21 4.27 4 0 3 104.15 4.01 4 0 3 98.83 3.80 4 0 3 97.02 3.89 4 0 4 34.46 2.43 4 0 4 37.21 2.18 4 0 4 36.43 2.01 4 0 4 40.20 2.17 4 0 5 55.01 3.22 4 0 5 65.66 3.10 4 0 5 61.13 3.05 4 0 5 64.79 2.89 4 0 5 57.95 2.75 4 0 6 9.78 1.56 4 0 6 9.32 1.29 4 0 6 9.90 1.44 4 0 7 1.63 1.25 4 0 7 1.24 0.86 4 0 7 1.29 1.18 4 0 8 0.22 0.84 4 0 8 1.00 1.16 4 0 9 64.91 3.25 4 0 9 72.04 3.45 4 0 10 14.53 1.58 4 0 10 14.82 1.77 4 0 10 13.71 1.61 4 0 10 13.76 1.49 4 0 11 100.09 4.00 4 0 11 99.15 4.31 4 0 11 91.96 3.84 4 0 11 91.78 4.04 4 0 12 45.57 2.41 4 0 12 48.92 2.67 4 0 12 46.48 2.35 4 0 12 51.69 2.59 4 0 13 8.46 1.07 4 0 13 9.56 1.21 4 0 13 11.40 1.13 4 0 14 58.82 2.54 4 0 14 66.22 2.70 4 0 15 0.24 0.56 4 1 -18 0.59 0.50 4 1 -17 311.65 9.54 4 1 -17 304.79 9.62 4 1 -17 321.09 9.44 4 1 -16 88.21 3.53 4 1 -16 92.08 3.58 4 1 -16 90.05 3.46 4 1 -15 48.37 2.50 4 1 -15 50.54 2.40 4 1 -14 8.27 1.15 4 1 -14 9.04 1.13 4 1 -13 45.72 2.46 4 1 -13 41.25 2.35 4 1 -12 2.82 0.89 4 1 -12 1.60 0.97 4 1 -11 601.46 18.17 4 1 -11 619.68 18.15 4 1 -11 592.95 18.23 4 1 -10 55.67 2.89 4 1 -10 49.12 2.65 4 1 -10 55.24 2.76 4 1 -10 53.56 2.87 4 1 -9 0.89 0.92 4 1 -9 0.62 0.89 4 1 -8 5.99 1.08 4 1 -8 3.57 0.89 4 1 -7 126.15 4.74 4 1 -7 120.80 4.78 4 1 -7 117.03 4.55 4 1 -7 123.58 4.83 4 1 -7 116.29 4.51 4 1 -6 24.57 1.75 4 1 -6 25.50 1.93 4 1 -6 26.34 1.77 4 1 -6 25.59 1.93 4 1 -6 27.70 1.81 4 1 -5 77.06 3.32 4 1 -5 77.98 3.59 4 1 -5 72.58 3.34 4 1 -5 83.65 3.55 4 1 -5 77.50 3.35 4 1 -4 18.20 1.42 4 1 -4 15.92 1.62 4 1 -4 16.25 1.48 4 1 -4 20.82 1.59 4 1 -4 15.74 1.60 4 1 -3 1.92 0.78 4 1 -3 2.18 1.01 4 1 -3 1.21 0.85 4 1 -3 1.75 0.66 4 1 -3 2.60 0.97 4 1 -2 141.80 4.99 4 1 -2 134.44 5.19 4 1 -2 146.45 5.07 4 1 -1 69.40 3.53 4 1 -1 73.17 3.03 4 1 -1 73.26 3.47 4 1 -1 76.01 3.08 4 1 0 74.39 3.08 4 1 0 72.39 3.52 4 1 0 76.03 3.35 4 1 0 76.88 3.15 4 1 0 75.14 3.70 4 1 1 187.58 6.22 4 1 1 186.29 6.72 4 1 1 189.28 6.53 4 1 1 185.51 6.35 4 1 1 187.63 6.49 4 1 2 1573.01 44.18 4 1 2 1567.71 44.64 4 1 2 1590.93 44.43 4 1 2 1513.23 44.56 4 1 2 1574.56 44.37 4 1 2 1563.18 44.40 4 1 3 26.50 1.66 4 1 3 22.85 1.82 4 1 3 22.77 1.69 4 1 3 25.39 2.03 4 1 3 26.10 1.83 4 1 3 26.48 1.76 4 1 3 23.83 1.67 4 1 4 69.63 3.20 4 1 4 77.92 3.73 4 1 4 83.77 3.59 4 1 4 80.69 3.45 4 1 4 71.72 3.23 4 1 5 11.86 1.17 4 1 5 9.41 1.56 4 1 5 12.67 1.41 4 1 5 11.44 1.25 4 1 5 9.56 1.09 4 1 6 82.82 3.74 4 1 6 79.01 3.55 4 1 6 79.39 3.55 4 1 7 18.49 1.97 4 1 7 24.08 1.91 4 1 7 18.71 1.78 4 1 7 19.79 1.71 4 1 8 9.85 1.68 4 1 8 8.49 1.30 4 1 8 7.77 1.16 4 1 8 9.37 1.45 4 1 9 178.31 6.42 4 1 9 163.14 6.00 4 1 10 744.03 21.01 4 1 10 718.50 21.43 4 1 10 679.09 21.15 4 1 11 118.20 4.49 4 1 11 125.68 4.89 4 1 11 122.43 4.73 4 1 11 114.46 4.40 4 1 12 88.43 3.78 4 1 12 92.88 3.66 4 1 13 5.55 0.88 4 1 13 5.90 1.05 4 1 13 5.73 0.88 4 1 14 1.62 0.72 4 1 14 1.67 0.58 4 2 -18 62.27 2.29 4 2 -17 4.98 0.76 4 2 -17 6.11 0.78 4 2 -17 4.83 0.71 4 2 -16 126.15 4.40 4 2 -16 124.02 4.42 4 2 -16 118.60 4.30 4 2 -15 1.41 0.69 4 2 -15 0.24 0.74 4 2 -15 0.93 0.69 4 2 -15 0.20 0.68 4 2 -14 0.90 0.74 4 2 -14 2.19 0.89 4 2 -14 0.28 0.77 4 2 -14 1.72 0.78 4 2 -13 1.80 0.72 4 2 -13 2.60 0.91 4 2 -13 1.88 0.90 4 2 -12 18.66 1.67 4 2 -12 24.18 1.69 4 2 -12 24.18 1.80 4 2 -11 107.15 4.37 4 2 -11 104.44 4.23 4 2 -11 106.43 4.39 4 2 -10 213.18 7.38 4 2 -9 59.06 2.88 4 2 -9 53.98 2.79 4 2 -8 111.78 4.30 4 2 -8 98.73 4.28 4 2 -8 104.12 4.12 4 2 -8 107.66 4.47 4 2 -7 202.60 6.85 4 2 -7 205.84 7.05 4 2 -7 198.13 6.81 4 2 -7 191.29 7.02 4 2 -6 72.72 3.13 4 2 -6 69.07 3.40 4 2 -6 70.01 3.19 4 2 -6 70.58 3.39 4 2 -5 24.61 1.69 4 2 -5 26.20 2.02 4 2 -5 24.98 1.83 4 2 -5 28.85 1.96 4 2 -4 82.96 3.40 4 2 -4 82.96 3.85 4 2 -4 77.85 3.62 4 2 -3 45.92 2.26 4 2 -3 42.95 2.47 4 2 -3 50.53 2.51 4 2 -3 46.81 2.37 4 2 -2 7.46 0.96 4 2 -2 6.42 1.22 4 2 -2 6.46 0.91 4 2 -1 4.81 0.86 4 2 -1 3.15 1.08 4 2 -1 4.27 0.84 4 2 0 2.86 0.77 4 2 0 4.74 1.10 4 2 0 4.98 1.06 4 2 0 3.74 0.81 4 2 1 516.68 15.54 4 2 1 538.57 16.28 4 2 1 540.24 16.04 4 2 1 518.21 15.91 4 2 2 4.57 0.89 4 2 2 5.52 1.20 4 2 2 4.68 1.09 4 2 2 4.59 0.93 4 2 3 3.43 0.97 4 2 3 5.02 0.96 4 2 3 2.91 1.19 4 2 3 3.23 0.86 4 2 4 33.07 1.99 4 2 4 31.38 2.34 4 2 4 39.29 2.34 4 2 4 38.46 2.25 4 2 4 30.62 1.93 4 2 5 4.82 1.38 4 2 5 6.91 1.18 4 2 5 6.04 1.07 4 2 6 38.12 2.73 4 2 6 47.05 2.68 4 2 6 45.09 2.51 4 2 6 45.70 2.60 4 2 7 5.66 1.38 4 2 7 5.93 1.06 4 2 7 6.90 1.28 4 2 8 8.58 1.60 4 2 8 6.97 1.15 4 2 8 6.82 1.27 4 2 9 19.01 1.58 4 2 9 16.75 1.55 4 2 10 16.31 1.69 4 2 10 10.62 1.23 4 2 11 14.81 1.40 4 2 11 18.62 1.38 4 2 12 302.11 9.24 4 2 12 302.93 9.35 4 2 13 2.63 0.83 4 2 14 38.39 1.74 4 3 -17 47.41 1.89 4 3 -17 49.43 2.01 4 3 -16 7.47 0.82 4 3 -16 6.84 0.81 4 3 -16 7.45 0.81 4 3 -15 1.18 0.62 4 3 -15 0.34 0.66 4 3 -15 0.92 0.63 4 3 -15 0.72 0.68 4 3 -14 404.48 11.90 4 3 -14 411.12 11.92 4 3 -13 20.68 1.55 4 3 -13 23.89 1.61 -4 -3 13 21.29 1.39 4 3 -13 23.72 1.66 4 3 -12 3.18 0.78 4 3 -12 1.63 0.82 4 3 -12 2.55 0.92 4 3 -11 -0.10 0.77 4 3 -10 63.73 2.94 4 3 -9 24.39 1.68 4 3 -9 21.56 1.69 4 3 -9 24.27 1.90 4 3 -8 53.42 2.55 4 3 -8 49.77 2.70 4 3 -8 52.18 2.59 4 3 -8 50.36 2.79 4 3 -7 18.56 1.43 4 3 -7 18.16 1.64 4 3 -7 19.15 1.55 4 3 -7 15.15 1.63 4 3 -6 28.30 1.73 4 3 -6 26.78 2.02 4 3 -6 27.11 1.94 4 3 -6 30.28 2.06 4 3 -5 105.99 3.98 4 3 -5 101.35 4.45 4 3 -5 101.66 4.30 4 3 -5 113.93 4.44 4 3 -4 364.30 11.38 4 3 -4 359.85 12.07 4 3 -4 359.23 11.86 4 3 -3 0.69 0.62 4 3 -3 0.89 0.90 4 3 -3 0.65 0.67 4 3 -2 9.00 0.99 4 3 -2 7.25 1.34 4 3 -2 11.26 1.19 4 3 -1 0.65 0.62 4 3 -1 1.01 1.01 4 3 -1 0.19 0.84 4 3 0 0.92 0.65 4 3 0 3.19 1.13 4 3 0 0.88 0.87 4 3 1 477.46 14.85 4 3 1 485.11 14.66 4 3 1 466.37 14.07 4 3 2 810.10 23.96 4 3 2 806.69 23.77 4 3 3 611.29 18.66 4 3 3 626.73 18.50 4 3 4 0.96 0.72 4 3 5 46.07 2.63 4 3 6 4.95 1.08 4 3 6 3.66 0.95 4 3 6 5.27 1.15 4 3 7 20.21 1.68 4 3 7 19.61 1.63 4 3 8 0.48 0.79 4 3 8 0.06 0.62 4 3 9 20.52 1.80 4 3 9 20.63 1.58 4 3 9 17.35 1.49 4 3 10 29.08 1.99 4 3 10 28.61 1.76 4 3 10 28.09 1.71 4 3 11 536.97 15.83 4 3 11 571.21 16.26 4 3 11 533.72 15.98 4 4 -16 0.05 0.51 -4 -4 15 204.83 6.31 4 4 -15 211.35 6.61 -4 -4 14 8.73 0.85 4 4 -14 10.19 1.07 -4 -4 13 10.48 0.96 4 4 -13 10.39 1.17 -4 -4 12 63.82 2.65 4 4 -11 21.63 1.67 4 4 -10 6.95 1.02 4 4 -10 9.93 1.29 4 4 -9 11.31 1.30 4 4 -9 14.29 1.24 4 4 -9 12.22 1.47 4 4 -8 46.14 2.52 4 4 -8 42.97 2.30 4 4 -8 41.35 2.51 4 4 -7 294.48 9.23 4 4 -7 286.66 8.99 4 4 -6 149.52 5.60 4 4 -6 138.11 5.30 4 4 -6 136.44 5.33 4 4 -5 60.85 3.21 4 4 -5 62.30 3.07 4 4 -5 65.84 3.09 4 4 -4 2.50 0.99 4 4 -3 11.65 1.41 4 4 -3 13.79 1.29 4 4 -2 16.39 1.72 4 4 -2 21.98 1.56 4 4 -1 0.36 0.98 4 4 -1 0.65 0.81 4 4 -1 0.06 0.65 4 4 0 12.22 1.50 4 4 0 12.28 1.42 4 4 0 12.54 1.23 4 4 1 1.87 1.07 4 4 1 1.98 0.94 4 4 1 1.89 0.75 4 4 2 222.46 7.88 4 4 2 226.53 7.74 4 4 2 240.20 7.83 4 4 3 3.43 0.97 4 4 3 3.99 0.89 4 4 3 3.78 0.88 4 4 4 58.25 2.72 4 4 4 67.68 3.06 4 4 5 17.27 1.48 4 4 6 28.73 1.86 4 4 7 26.28 1.72 4 4 8 24.12 1.73 4 4 8 19.95 1.44 4 4 9 7.02 1.05 4 4 9 7.13 0.84 4 4 10 2.66 0.78 4 4 11 1.72 0.62 4 5 -15 11.72 0.90 -4 -5 14 130.70 4.20 4 5 -14 129.17 4.41 -4 -5 13 591.09 16.97 -4 -5 12 224.88 7.11 4 5 -12 237.96 7.50 -4 -5 11 0.81 0.62 4 5 -11 2.05 0.80 -4 -5 10 0.98 0.67 4 5 -10 0.47 0.85 4 5 -9 5.51 0.97 4 5 -9 6.46 0.90 4 5 -9 4.65 1.10 4 5 -8 14.35 1.38 4 5 -8 12.53 1.22 4 5 -8 12.76 1.36 4 5 -7 167.47 5.72 4 5 -7 154.50 5.42 4 5 -6 96.41 4.14 4 5 -6 97.99 3.97 4 5 -6 93.39 3.91 4 5 -5 24.91 1.97 4 5 -5 25.74 1.85 4 5 -5 25.54 1.74 4 5 -4 1.70 0.89 4 5 -3 100.29 4.35 4 5 -2 11.16 1.45 4 5 -2 15.14 1.27 4 5 -1 17.31 1.66 4 5 -1 16.63 1.47 4 5 -1 16.49 1.32 4 5 0 3.20 1.00 4 5 0 4.30 0.97 4 5 0 4.38 0.79 4 5 1 6.17 1.11 4 5 1 7.66 1.04 4 5 1 6.63 0.92 4 5 2 55.17 2.73 4 5 2 52.35 2.56 4 5 2 59.28 2.65 4 5 3 285.19 9.16 4 5 3 278.46 9.02 4 5 3 307.53 9.26 4 5 4 64.75 2.84 4 5 5 9.10 0.99 4 5 6 121.38 4.33 4 5 7 20.11 1.28 4 5 8 25.94 1.36 4 6 -13 19.03 1.16 -4 -6 12 2.09 0.50 4 6 -12 2.14 0.64 4 6 -11 15.30 1.17 -4 -6 10 1.07 0.53 4 6 -10 1.17 0.65 -4 -6 9 3.38 0.64 4 6 -9 3.16 0.64 4 6 -9 2.92 0.79 -4 -6 8 8.99 0.96 -4 -6 8 6.49 0.91 4 6 -8 7.87 1.03 -4 -6 8 9.46 0.87 4 6 -8 9.79 0.97 4 6 -8 7.77 0.97 -4 -6 7 23.71 1.56 -4 -6 7 22.27 1.58 4 6 -7 26.51 1.72 -4 -6 7 25.94 1.43 4 6 -7 26.45 1.58 4 6 -7 23.09 1.52 -4 -6 6 270.46 8.50 4 6 -6 269.26 8.72 -4 -6 6 263.87 8.15 4 6 -6 266.08 8.54 -4 -6 5 24.88 1.68 4 6 -5 26.28 1.82 -4 -6 5 20.27 1.32 4 6 -5 22.31 1.60 -4 -6 4 32.80 1.68 4 6 -4 36.52 2.03 -4 -6 3 4.39 0.99 4 6 -3 2.81 0.95 -4 -6 2 26.01 1.78 4 6 -2 25.21 1.77 4 6 -2 23.85 1.66 -4 -6 1 27.71 1.86 4 6 -1 29.99 1.89 4 6 -1 29.69 1.79 -4 -6 0 35.28 1.98 -4 -6 0 31.36 2.03 4 6 0 38.37 2.07 4 6 0 36.34 1.94 -4 -6 -1 3.26 0.79 -4 -6 -1 1.52 0.77 4 6 1 2.90 0.77 4 6 1 2.27 0.67 4 6 1 2.05 0.59 -4 -6 -2 1.43 0.65 4 6 2 1.90 0.66 -4 -6 -2 1.79 0.71 4 6 2 1.88 0.60 4 6 2 1.36 0.52 4 6 3 17.03 1.08 4 6 4 0.17 0.42 -4 -6 -5 84.86 3.31 -4 -7 7 0.34 0.51 4 7 -7 0.94 0.61 -4 -7 7 1.03 0.55 4 7 -7 1.45 0.52 4 7 -6 25.36 1.44 -4 -7 6 21.69 1.36 4 7 -6 23.20 1.31 -4 -7 5 16.86 1.17 -4 -7 5 15.48 1.21 4 7 -5 18.98 1.19 -4 -7 4 7.82 0.96 4 7 -4 7.42 0.86 -4 -7 3 0.18 0.57 4 7 -3 0.63 0.63 -4 -7 2 2.12 0.63 4 7 -2 2.43 0.65 -4 -7 2 2.25 0.66 4 7 -2 2.40 0.59 -4 -7 1 9.19 0.87 4 7 -1 8.18 0.88 -4 -7 1 8.04 0.91 4 7 -1 8.16 0.81 -4 -7 0 240.38 7.13 4 7 0 229.11 7.20 5 -5 -6 86.70 3.17 5 -5 -5 55.90 2.43 5 -5 -4 -0.50 0.96 5 -5 -3 213.41 6.98 5 -5 -2 0.69 0.83 5 -5 -1 65.06 3.02 5 -5 1 37.04 2.28 5 -5 2 138.50 5.24 5 -5 2 155.21 5.12 5 -5 3 106.78 3.89 5 -5 4 0.27 0.55 5 -5 5 23.99 1.40 5 -5 6 2.55 0.61 5 -4 -9 15.55 1.14 5 -4 -8 3.95 0.72 5 -4 -7 33.31 1.85 5 -4 -7 30.12 1.70 5 -4 -6 64.49 2.88 5 -4 -6 67.10 2.80 5 -4 -5 1.42 0.92 5 -4 -5 1.56 0.93 5 -4 -5 0.45 0.61 5 -4 -4 190.75 6.48 5 -4 -3 279.67 9.15 5 -4 -3 277.26 9.46 5 -4 -2 1.77 1.07 5 -4 -2 -1.31 1.35 5 -4 -2 1.09 0.97 5 -4 -2 -0.82 1.47 5 -4 -1 153.51 5.73 5 -4 0 14.71 1.68 5 -4 0 17.43 1.37 5 -4 1 0.70 1.00 5 -4 1 0.70 1.04 5 -4 1 0.28 0.62 5 -4 1 0.86 1.02 5 -4 2 1.08 0.66 5 -4 2 -0.22 1.10 5 -4 3 59.01 2.66 5 -4 4 22.07 1.49 5 -4 5 90.46 3.55 5 -4 6 0.81 0.60 5 -4 7 8.50 0.90 5 -4 8 25.10 1.43 5 -3 -11 220.97 7.01 5 -3 -10 4.80 0.82 5 -3 -9 106.01 3.77 5 -3 -9 94.12 3.79 5 -3 -8 7.19 1.11 5 -3 -8 7.32 0.95 5 -3 -7 1.26 0.90 5 -3 -7 1.27 0.67 5 -3 -6 5.88 1.15 5 -3 -6 7.56 0.97 5 -3 -6 6.13 1.22 5 -3 -5 24.27 1.94 5 -3 -5 21.56 1.54 5 -3 -4 1.87 1.14 5 -3 -4 3.32 1.06 5 -3 -3 134.68 5.00 5 -3 -3 134.16 5.32 5 -3 -2 2.93 1.36 5 -3 -2 3.22 1.12 5 -3 -1 1.82 1.04 5 -3 -1 1.20 0.69 5 -3 0 219.46 7.47 5 -3 0 219.12 7.86 5 -3 0 240.63 7.55 5 -3 1 0.68 1.21 5 -3 1 2.11 1.04 5 -3 1 2.86 0.74 5 -3 2 3.24 1.13 5 -3 2 4.27 0.81 5 -3 3 21.89 1.88 5 -3 3 25.16 1.61 5 -3 4 81.04 3.27 5 -3 4 77.52 3.28 5 -3 5 2.24 0.71 5 -3 5 1.31 1.00 5 -3 5 3.06 0.99 5 -3 6 21.85 1.51 5 -3 6 26.45 1.71 5 -3 7 67.21 2.88 5 -3 7 74.53 3.03 5 -3 8 3.45 0.69 5 -3 8 4.93 1.01 5 -3 9 242.70 7.56 5 -3 10 68.50 2.64 5 -2 -12 78.11 3.09 5 -2 -11 380.81 11.65 5 -2 -11 410.01 11.97 5 -2 -10 12.80 1.25 5 -2 -10 10.50 1.16 5 -2 -9 93.40 3.59 5 -2 -9 88.74 3.76 5 -2 -8 37.18 1.97 5 -2 -8 39.23 2.16 5 -2 -8 34.22 2.07 5 -2 -7 10.72 1.11 5 -2 -7 11.94 1.40 5 -2 -7 10.82 1.17 5 -2 -6 3.27 1.15 5 -2 -6 2.83 0.82 5 -2 -6 2.93 0.78 5 -2 -5 117.70 4.25 5 -2 -5 118.89 4.50 5 -2 -5 113.99 4.71 5 -2 -5 106.99 4.29 5 -2 -4 158.25 5.49 5 -2 -4 159.33 5.75 5 -2 -4 163.96 6.12 5 -2 -3 606.86 17.86 5 -2 -3 623.23 18.12 5 -2 -3 593.36 18.46 5 -2 -2 212.55 6.97 5 -2 -2 216.85 7.25 5 -2 -1 66.92 2.81 5 -2 -1 61.74 2.97 5 -2 -1 66.95 3.50 5 -2 0 228.63 7.30 5 -2 0 226.04 7.45 5 -2 0 223.00 7.94 5 -2 1 104.77 4.04 5 -2 1 107.34 4.54 5 -2 1 115.26 4.00 5 -2 2 2.82 1.20 5 -2 2 0.29 1.02 5 -2 3 17.31 1.69 5 -2 3 14.61 1.42 5 -2 3 18.55 1.61 5 -2 4 4.07 1.17 5 -2 4 4.07 1.00 5 -2 4 4.78 1.17 5 -2 5 -0.29 0.99 5 -2 5 0.82 0.86 5 -2 5 -0.10 0.98 5 -2 6 185.87 6.60 5 -2 6 200.39 6.61 5 -2 7 1.11 0.86 5 -2 7 0.26 0.94 5 -2 8 11.16 1.29 5 -2 8 11.55 1.29 5 -2 9 24.90 1.66 5 -2 11 17.17 1.19 5 -1 -13 54.32 2.27 5 -1 -12 66.34 2.81 5 -1 -12 72.43 2.77 5 -1 -11 142.93 5.37 5 -1 -11 173.94 5.43 5 -1 -10 25.76 1.71 5 -1 -10 25.37 1.73 5 -1 -9 1.21 0.95 5 -1 -9 1.02 0.77 5 -1 -8 148.48 5.18 5 -1 -8 128.95 5.03 5 -1 -7 3.22 1.05 5 -1 -7 2.48 0.89 5 -1 -6 2.61 0.84 5 -1 -5 42.11 2.25 5 -1 -4 31.65 1.89 5 -1 -4 29.62 2.01 5 -1 -3 251.38 8.20 5 -1 -3 256.77 8.33 5 -1 -2 74.23 3.08 5 -1 -2 67.11 3.13 5 -1 -1 255.27 8.09 5 -1 -1 256.98 8.17 5 -1 -1 241.77 8.22 5 -1 0 1.21 0.76 5 -1 0 0.40 0.92 5 -1 0 -0.05 1.34 5 -1 1 750.96 21.90 5 -1 1 755.63 22.15 5 -1 2 1.25 0.80 5 -1 2 1.55 0.90 5 -1 2 3.16 1.13 5 -1 2 1.74 1.16 5 -1 3 0.43 0.91 5 -1 3 2.48 1.08 5 -1 3 2.08 1.14 5 -1 4 6.43 1.25 5 -1 4 5.18 1.11 5 -1 4 4.55 1.19 5 -1 4 5.14 1.27 5 -1 5 19.92 1.72 5 -1 5 17.15 1.64 5 -1 5 23.05 1.96 5 -1 5 21.05 1.77 5 -1 6 1.34 0.92 5 -1 6 0.07 1.02 5 -1 6 0.36 1.07 5 -1 7 3.35 1.02 5 -1 7 3.29 1.12 5 -1 8 125.41 4.64 5 -1 8 118.68 4.87 5 -1 9 77.58 3.18 5 -1 10 61.08 2.59 5 -1 11 24.12 1.48 5 -1 11 22.92 1.60 5 -1 11 22.76 1.38 5 0 -15 38.13 1.63 5 0 -14 1.07 0.61 5 0 -13 60.30 2.58 5 0 -13 60.36 2.44 5 0 -12 137.92 4.92 5 0 -11 133.26 5.31 5 0 -11 177.04 5.55 5 0 -10 107.92 4.23 5 0 -10 105.51 4.14 5 0 -9 1.70 0.90 5 0 -9 2.03 0.79 5 0 -8 275.31 8.63 5 0 -8 247.61 8.41 5 0 -7 116.32 4.46 5 0 -7 109.52 4.29 5 0 -6 1.29 0.83 5 0 -6 0.22 0.88 5 0 -5 84.74 3.55 5 0 -5 84.82 3.77 5 0 -4 4.74 0.97 5 0 -4 3.48 1.08 5 0 -3 56.72 3.00 5 0 -2 547.57 16.71 5 0 -1 90.75 3.64 5 0 0 250.80 8.50 5 0 1 300.99 9.82 5 0 1 305.91 9.91 5 0 2 176.41 6.61 5 0 2 188.84 6.60 5 0 2 189.01 6.58 5 0 3 3.14 1.12 5 0 3 2.55 1.18 5 0 3 1.28 0.88 5 0 4 17.77 1.68 5 0 4 20.59 1.81 5 0 4 15.25 1.70 5 0 5 7.14 1.24 5 0 5 8.27 1.33 5 0 6 0.67 0.93 5 0 6 1.47 1.16 5 0 6 1.24 1.11 5 0 7 222.22 7.08 5 0 7 204.15 6.89 5 0 8 21.80 1.77 5 0 8 21.76 1.68 5 0 9 156.28 5.60 5 0 9 148.88 5.18 5 0 10 0.82 0.71 5 0 10 0.18 0.86 5 0 10 -0.49 0.83 5 0 11 3.90 0.79 5 0 11 4.55 0.76 5 1 -15 47.79 1.94 5 1 -14 0.52 0.57 5 1 -14 1.25 0.60 5 1 -13 10.14 1.03 5 1 -13 10.19 1.01 5 1 -12 11.29 1.13 5 1 -12 13.57 1.20 5 1 -11 9.59 1.13 5 1 -11 12.91 1.22 5 1 -10 142.99 5.14 5 1 -10 137.31 5.03 5 1 -9 3.02 0.89 5 1 -9 1.69 0.84 5 1 -8 1.01 0.82 5 1 -8 1.16 0.73 5 1 -8 1.37 0.81 5 1 -7 254.32 8.41 5 1 -7 263.32 8.34 5 1 -7 254.98 8.43 5 1 -6 12.25 1.28 5 1 -6 10.84 1.32 5 1 -5 71.58 3.15 5 1 -5 74.15 3.42 5 1 -4 40.11 2.14 5 1 -4 38.26 2.41 5 1 -4 40.27 2.43 5 1 -3 76.47 3.18 5 1 -3 74.84 3.51 5 1 -3 70.15 3.45 5 1 -2 259.28 8.31 5 1 -1 6.28 0.98 5 1 -1 7.21 1.21 5 1 0 289.25 9.30 5 1 0 299.39 9.78 5 1 0 306.50 9.82 5 1 1 131.19 4.80 5 1 1 134.97 4.90 5 1 1 139.91 5.22 5 1 2 259.51 8.28 5 1 2 252.05 8.50 5 1 3 0.94 0.97 5 1 3 0.52 0.64 5 1 3 0.93 0.79 5 1 4 5.72 1.18 5 1 4 5.97 0.86 5 1 4 5.04 1.22 5 1 4 4.92 0.93 5 1 5 2.04 1.05 5 1 5 1.91 0.65 5 1 5 1.82 1.12 5 1 6 29.05 2.15 5 1 6 40.16 2.20 5 1 7 1.67 0.98 5 1 7 1.75 1.00 5 1 7 2.48 0.97 5 1 8 2.72 0.96 5 1 8 2.45 0.93 5 1 9 8.26 1.09 5 1 9 10.19 1.20 5 1 9 9.89 1.09 5 1 10 2.09 0.71 5 1 10 1.10 0.78 5 1 10 0.81 0.66 5 1 11 1.98 0.58 5 1 11 2.26 0.70 5 2 -15 50.02 1.91 5 2 -14 20.68 1.19 5 2 -14 19.29 1.21 5 2 -13 31.42 1.63 5 2 -13 32.56 1.70 5 2 -12 49.31 2.33 5 2 -12 61.37 2.52 5 2 -11 33.37 1.89 5 2 -11 41.23 2.03 5 2 -10 91.79 3.63 5 2 -10 89.87 3.64 5 2 -10 101.46 4.02 5 2 -9 4.14 0.88 5 2 -9 4.40 0.87 5 2 -9 2.59 0.89 5 2 -8 50.66 2.50 5 2 -8 51.52 2.83 5 2 -8 55.85 2.65 5 2 -7 172.71 5.77 5 2 -7 164.73 5.88 5 2 -7 157.69 6.10 5 2 -7 167.75 5.89 5 2 -6 97.03 3.81 5 2 -6 98.97 4.06 5 2 -6 103.80 4.28 5 2 -6 96.56 4.05 5 2 -5 0.04 0.69 5 2 -5 0.23 0.75 5 2 -5 0.06 0.89 5 2 -4 57.15 2.55 5 2 -4 56.94 2.91 5 2 -4 54.32 2.86 5 2 -3 2.75 0.79 5 2 -3 1.69 0.87 5 2 -3 1.11 0.87 5 2 -2 10.62 1.09 5 2 -2 9.35 1.48 5 2 -1 489.72 14.86 5 2 -1 499.03 15.45 5 2 -1 524.64 15.46 5 2 0 0.88 0.69 5 2 0 0.91 0.98 5 2 0 0.45 0.62 5 2 0 0.12 0.88 5 2 1 546.28 16.48 5 2 1 546.97 16.27 5 2 1 538.93 16.43 5 2 2 91.59 3.98 5 2 2 103.83 3.97 5 2 2 100.32 4.03 5 2 3 66.07 2.91 5 2 3 65.81 3.00 5 2 4 38.99 2.24 5 2 4 40.19 2.06 5 2 4 34.20 1.96 5 2 5 99.18 3.94 5 2 5 100.24 3.83 5 2 6 6.77 0.87 5 2 6 7.73 1.15 5 2 7 29.68 1.73 5 2 7 25.47 1.49 5 2 8 7.60 1.03 5 2 8 5.98 1.00 5 2 8 5.32 0.89 5 2 9 3.84 0.76 5 2 9 2.31 0.78 5 2 9 1.72 0.63 5 2 10 201.42 6.30 5 2 10 208.10 6.45 5 3 -13 41.31 1.73 5 3 -13 43.02 1.90 5 3 -12 22.25 1.22 -5 -3 12 18.96 1.11 5 3 -12 22.44 1.37 5 3 -11 40.57 1.94 5 3 -11 42.19 2.15 5 3 -10 8.66 0.92 5 3 -10 8.08 0.94 5 3 -10 10.93 1.23 5 3 -9 114.61 4.05 5 3 -9 120.97 4.51 5 3 -9 109.19 4.09 5 3 -8 63.31 2.59 5 3 -8 65.63 2.76 5 3 -8 62.85 2.73 5 3 -7 40.21 1.92 5 3 -7 34.54 2.07 5 3 -7 38.25 2.26 5 3 -7 41.02 2.16 5 3 -6 151.53 5.10 5 3 -6 148.45 5.68 5 3 -6 145.67 5.45 5 3 -6 154.14 5.57 5 3 -6 155.91 5.52 5 3 -5 2.70 0.72 5 3 -5 1.76 0.97 5 3 -5 3.00 0.90 5 3 -5 4.00 0.96 5 3 -5 3.05 0.94 5 3 -4 28.93 1.57 5 3 -4 26.51 1.93 5 3 -4 27.30 1.95 5 3 -3 0.42 0.59 5 3 -3 0.30 0.84 5 3 -3 -0.30 0.89 5 3 -2 12.10 1.05 5 3 -2 10.15 1.45 5 3 -1 29.02 2.20 5 3 -1 30.49 2.05 5 3 -1 31.95 2.04 5 3 -1 29.31 1.64 5 3 0 8.13 1.33 5 3 0 7.10 1.16 5 3 0 8.09 0.99 5 3 0 7.44 1.12 5 3 1 0.71 0.87 5 3 1 0.68 0.73 5 3 1 0.44 0.64 5 3 1 0.61 0.80 5 3 2 23.91 1.64 5 3 2 24.14 1.56 5 3 2 21.73 1.59 5 3 3 4.74 0.87 5 3 3 4.15 0.78 5 3 3 3.95 0.81 5 3 4 0.48 0.55 5 3 4 0.04 0.88 5 3 5 114.68 4.11 5 3 5 112.49 4.10 5 3 6 14.46 1.19 5 3 6 15.08 1.11 5 3 7 8.28 0.85 5 3 7 8.78 0.81 5 3 8 1.45 0.66 5 4 -12 19.52 1.28 -5 -4 11 35.09 1.63 5 4 -11 43.54 2.02 -5 -4 10 7.41 0.81 5 4 -10 7.88 1.03 5 4 -9 112.80 4.18 5 4 -9 111.10 3.91 5 4 -8 1.75 0.76 5 4 -8 1.77 0.64 5 4 -8 1.30 0.77 5 4 -8 1.86 0.68 5 4 -7 70.99 3.17 5 4 -7 75.85 3.08 5 4 -7 71.45 3.08 5 4 -7 70.13 3.00 5 4 -6 12.23 1.37 5 4 -6 12.41 1.19 5 4 -6 11.74 1.22 5 4 -6 14.23 1.29 5 4 -5 46.62 2.60 5 4 -5 46.91 2.42 5 4 -5 47.45 2.42 5 4 -4 37.45 2.13 5 4 -3 73.41 3.43 5 4 -2 9.94 1.37 5 4 -1 59.07 2.98 5 4 -1 60.79 2.81 5 4 -1 57.61 2.76 5 4 0 160.09 5.85 5 4 0 162.93 5.72 5 4 0 166.12 5.69 5 4 1 1.04 0.83 5 4 1 2.02 0.72 5 4 1 1.99 0.72 5 4 2 300.21 9.43 5 4 2 313.76 9.41 5 4 3 6.12 0.95 5 4 4 4.20 0.82 5 4 5 22.00 1.22 5 5 -11 8.59 0.81 5 5 -10 0.58 0.52 5 5 -9 0.50 0.56 -5 -5 8 43.45 1.82 5 5 -8 44.09 1.92 5 5 -8 47.12 1.95 5 5 -7 16.98 1.31 5 5 -7 18.49 1.19 5 5 -7 16.32 1.17 5 5 -6 18.99 1.45 5 5 -6 19.51 1.32 5 5 -6 19.36 1.31 5 5 -5 165.50 5.68 5 5 -5 162.25 5.51 5 5 -5 160.74 5.47 5 5 -4 0.92 0.64 5 5 -3 1.47 0.77 5 5 -2 13.79 1.29 5 5 -2 12.82 1.16 5 5 -2 16.01 1.23 5 5 -1 41.64 2.18 5 5 -1 45.87 2.09 5 5 -1 42.88 2.05 5 5 0 8.80 0.99 5 5 0 8.50 0.89 5 5 0 9.06 0.88 -5 -5 -1 110.19 4.02 5 5 1 136.48 4.20 -5 -5 -2 16.28 1.04 5 5 2 21.19 1.17 -5 -6 6 7.37 0.73 5 6 -6 8.75 0.84 -5 -6 5 12.92 0.94 5 6 -5 14.32 1.06 -5 -6 3 7.13 0.73 5 6 -3 7.90 0.82 -5 -6 2 12.83 0.94 5 6 -2 16.90 1.06 6 -3 0 267.65 8.49 6 -2 -7 53.15 2.29 6 -2 -6 24.37 1.48 6 -2 -5 20.06 1.43 6 -2 -5 23.22 1.54 6 -2 -4 0.35 0.79 6 -2 -4 1.36 0.91 6 -2 -3 -0.16 0.78 6 -2 -3 0.08 0.89 6 -2 -2 9.28 1.06 6 -2 -1 2.50 1.16 6 -2 0 85.61 3.63 6 -2 1 113.40 4.33 6 -2 2 6.00 1.08 6 -2 3 0.91 0.79 6 -1 -10 -0.21 0.57 6 -1 -8 97.33 3.33 6 -1 -8 101.71 3.56 6 -1 -7 39.47 1.65 6 -1 -7 31.38 1.78 6 -1 -6 0.24 0.80 6 -1 -6 0.25 0.55 6 -1 -6 0.03 0.78 6 -1 -5 12.46 0.97 6 -1 -5 10.42 1.25 6 -1 -5 9.77 1.11 6 -1 -4 30.96 1.83 6 -1 -4 33.87 2.08 6 -1 -3 85.98 3.37 6 -1 -3 81.54 3.67 6 -1 -2 1.37 0.80 6 -1 -2 0.36 0.84 6 -1 -1 75.07 3.34 6 -1 0 6.75 1.28 6 -1 1 171.90 5.93 6 -1 2 3.51 0.96 6 -1 3 38.28 1.96 6 -1 4 19.42 1.31 6 -1 5 31.79 1.62 6 -1 6 7.23 0.83 6 0 -10 2.90 0.52 6 0 -9 0.79 0.63 6 0 -9 0.19 0.47 6 0 -8 99.74 3.33 6 0 -8 89.18 3.41 6 0 -7 20.06 1.18 6 0 -7 14.25 1.23 6 0 -6 37.86 2.03 6 0 -6 42.38 2.16 6 0 -5 1.18 0.91 6 0 -5 0.91 0.61 6 0 -5 -0.39 0.90 6 0 -4 180.58 5.55 6 0 -4 170.50 5.93 6 0 -3 13.21 1.14 6 0 -3 7.48 1.06 6 0 -2 1.18 0.68 6 0 -2 2.03 0.98 6 0 -1 69.92 3.22 6 0 0 28.54 1.94 6 0 1 43.62 2.40 6 0 1 44.25 2.18 6 0 2 103.84 3.93 6 0 2 103.22 3.82 6 0 3 7.80 0.99 6 0 3 8.08 1.08 6 0 4 50.27 2.25 6 0 5 47.52 2.07 6 1 -10 1.04 0.58 6 1 -10 -0.20 0.44 6 1 -9 20.18 1.12 6 1 -9 23.63 1.31 6 1 -8 23.58 1.24 6 1 -8 19.30 1.30 6 1 -7 86.60 2.85 6 1 -7 63.27 2.79 6 1 -6 9.20 0.87 6 1 -6 6.57 0.93 6 1 -5 0.15 0.53 6 1 -5 0.44 0.68 6 1 -4 70.08 2.70 6 1 -3 2.42 0.79 6 1 -1 8.45 1.24 6 1 0 1.00 0.88 6 1 1 3.21 0.93 6 1 2 12.88 1.20 6 1 2 14.96 1.26 6 1 3 46.33 2.10 6 1 3 54.00 2.27 6 2 -9 4.77 0.53 6 2 -9 3.38 0.67 6 2 -8 0.53 0.43 6 2 -8 0.40 0.59 6 2 -7 32.06 1.39 6 2 -7 24.32 1.40 6 2 -6 71.67 2.47 6 2 -6 59.28 2.43 6 2 -5 7.92 0.76 6 2 -5 5.59 0.91 6 2 -4 2.52 0.61 6 2 -4 1.41 0.66 6 2 -3 150.40 4.74 6 2 -3 122.89 4.76 6 2 -2 40.95 2.05 6 2 -1 0.72 0.86 6 2 -1 0.18 0.68 6 2 0 20.40 1.42 6 2 1 0.57 0.78 6 2 3 7.13 0.91 6 2 4 23.03 1.25 6 3 -4 1.88 0.73 6 3 -4 1.29 0.63 6 3 -3 151.48 4.96 6 3 -2 104.21 3.66 6 3 1 2.36 0.71 0 0 0 0.00 0.00 TITL form_I in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 5.289773 7.866891 17.558989 99.1613 96.1868 90.6921 ZERR 3.00 0.000236 0.000267 0.000593 0.0028 0.0034 0.0032 LATT 1 SFAC C H N O UNIT 33.00 30.00 3.00 3.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0 TEMP -173 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 99695 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.880 _oxdiff_exptl_absorpt_empirical_full_min 0.567 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl01 Cl 0.04434(7) 0.91069(4) 0.10013(2) 0.02569(15) Uani 1 1 d . . . . . O002 O -0.23773(19) 0.78059(14) 0.44882(6) 0.0255(3) Uani 1 1 d . . . . . N003 N 0.1944(2) 0.76549(15) 0.46938(7) 0.0198(3) Uani 1 1 d . . . . . H003 H 0.338775 0.764651 0.448673 0.024 Uiso 1 1 calc R U . . . N004 N 0.1937(2) 0.74344(15) 0.54596(7) 0.0205(3) Uani 1 1 d . . . . . N005 N 0.5382(2) 0.62613(15) 0.89686(7) 0.0211(3) Uani 1 1 d . . . . . C006 C 0.4349(3) 0.67323(17) 0.65864(8) 0.0176(3) Uani 1 1 d . . . . . C007 C 0.6815(3) 0.57312(17) 0.76688(8) 0.0190(3) Uani 1 1 d . . . . . H007 H 0.824463 0.513683 0.785630 0.023 Uiso 1 1 calc R U . . . C008 C 0.5096(3) 0.64275(17) 0.81816(8) 0.0179(3) Uani 1 1 d . . . . . C009 C 0.4037(3) 0.69271(17) 0.57683(8) 0.0193(3) Uani 1 1 d . . . . . H009 H 0.540443 0.667529 0.546308 0.023 Uiso 1 1 calc R U . . . C00A C 0.0031(3) 0.81967(17) 0.34566(8) 0.0178(3) Uani 1 1 d . . . . . C00B C 0.2620(3) 0.74139(17) 0.70967(8) 0.0187(3) Uani 1 1 d . . . . . H00B H 0.116866 0.797984 0.690385 0.022 Uiso 1 1 calc R U . . . C00C C -0.1868(3) 0.75254(18) 0.28690(8) 0.0202(3) Uani 1 1 d . . . . . H00C H -0.326428 0.688581 0.298994 0.024 Uiso 1 1 calc R U . . . C00D C 0.2078(3) 0.91426(18) 0.32789(8) 0.0201(3) Uani 1 1 d . . . . . H00D H 0.338816 0.959244 0.367582 0.024 Uiso 1 1 calc R U . . . C00E C 0.2987(3) 0.72779(18) 0.78728(8) 0.0189(3) Uani 1 1 d . . . . . H00E H 0.179567 0.776668 0.820679 0.023 Uiso 1 1 calc R U . . . C00F C -0.0271(3) 0.78839(18) 0.42624(8) 0.0194(3) Uani 1 1 d . . . . . C00G C 0.0297(3) 0.87380(17) 0.19529(8) 0.0190(3) Uani 1 1 d . . . . . C00H C 0.6448(3) 0.59030(17) 0.68902(8) 0.0185(3) Uani 1 1 d . . . . . H00H H 0.765659 0.544388 0.655607 0.022 Uiso 1 1 calc R U . . . C00I C -0.1746(3) 0.77791(18) 0.21111(8) 0.0215(3) Uani 1 1 d . . . . . H00I H -0.302876 0.730845 0.170943 0.026 Uiso 1 1 calc R U . . . C00J C 0.2202(3) 0.94265(18) 0.25229(9) 0.0205(3) Uani 1 1 d . . . . . H00J H 0.357515 1.008418 0.239985 0.025 Uiso 1 1 calc R U . . . C00K C 0.4655(3) 0.7719(2) 0.95158(9) 0.0263(3) Uani 1 1 d . . . . . H00A H 0.574770 0.872445 0.949954 0.039 Uiso 1 1 calc R U . . . H00F H 0.485158 0.742924 1.004107 0.039 Uiso 1 1 calc R U . . . H00G H 0.287658 0.798294 0.937445 0.039 Uiso 1 1 calc R U . . . C00L C 0.7677(3) 0.5473(2) 0.92599(9) 0.0316(4) Uani 1 1 d . . . . . H00K H 0.781194 0.432556 0.895609 0.047 Uiso 1 1 calc R U . . . H00L H 0.760630 0.536961 0.980613 0.047 Uiso 1 1 calc R U . . . H00M H 0.916333 0.619009 0.921409 0.047 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl01 0.0383(2) 0.0241(2) 0.0160(2) 0.00506(14) 0.00563(15) 0.00554(15) O002 0.0236(5) 0.0335(6) 0.0212(5) 0.0080(4) 0.0047(4) 0.0019(4) N003 0.0234(6) 0.0230(6) 0.0135(6) 0.0034(5) 0.0033(5) 0.0013(5) N004 0.0270(6) 0.0203(6) 0.0141(6) 0.0023(5) 0.0026(5) 0.0002(5) N005 0.0288(6) 0.0180(6) 0.0159(6) 0.0026(5) 0.0004(5) 0.0025(5) C006 0.0219(7) 0.0138(6) 0.0164(7) 0.0008(5) 0.0009(5) -0.0026(5) C007 0.0215(7) 0.0141(6) 0.0205(7) 0.0020(5) -0.0002(5) 0.0013(5) C008 0.0233(7) 0.0127(6) 0.0170(7) 0.0018(5) 0.0005(5) -0.0030(5) C009 0.0244(7) 0.0159(7) 0.0174(7) 0.0008(5) 0.0035(5) -0.0001(5) C00A 0.0217(7) 0.0139(6) 0.0177(7) 0.0020(5) 0.0024(5) 0.0038(5) C00B 0.0202(7) 0.0161(7) 0.0189(7) 0.0019(5) 0.0003(5) 0.0006(5) C00C 0.0215(7) 0.0185(7) 0.0205(7) 0.0024(5) 0.0023(5) 0.0003(5) C00D 0.0212(7) 0.0171(7) 0.0207(7) 0.0012(5) -0.0006(5) 0.0013(5) C00E 0.0210(7) 0.0172(7) 0.0181(7) 0.0010(5) 0.0036(5) 0.0014(5) C00F 0.0240(7) 0.0158(6) 0.0178(7) 0.0010(5) 0.0022(5) 0.0012(5) C00G 0.0273(7) 0.0147(6) 0.0157(7) 0.0028(5) 0.0042(5) 0.0055(5) C00H 0.0218(7) 0.0143(6) 0.0185(7) -0.0003(5) 0.0033(5) -0.0001(5) C00I 0.0244(7) 0.0197(7) 0.0188(7) 0.0006(5) -0.0008(5) 0.0022(5) C00J 0.0234(7) 0.0163(7) 0.0228(7) 0.0039(6) 0.0053(6) 0.0014(5) C00K 0.0363(8) 0.0256(8) 0.0165(7) 0.0018(6) 0.0035(6) 0.0041(6) C00L 0.0410(9) 0.0340(9) 0.0208(8) 0.0094(7) -0.0001(7) 0.0127(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N004 N003 H003 120.0 . . ? C00F N003 H003 120.0 . . ? C00F N003 N004 120.00(11) . . ? C009 N004 N003 114.55(12) . . ? C008 N005 C00K 116.96(11) . . ? C008 N005 C00L 117.31(12) . . ? C00L N005 C00K 112.51(12) . . ? C00B C006 C009 121.72(13) . . ? C00H C006 C009 120.51(13) . . ? C00H C006 C00B 117.73(13) . . ? C008 C007 H007 119.7 . . ? C00H C007 H007 119.7 . . ? C00H C007 C008 120.62(13) . . ? N005 C008 C007 122.33(13) . . ? N005 C008 C00E 120.15(12) . . ? C007 C008 C00E 117.50(13) . . ? N004 C009 C006 120.50(13) . . ? N004 C009 H009 119.7 . . ? C006 C009 H009 119.7 . . ? C00C C00A C00D 119.56(13) . . ? C00C C00A C00F 117.33(12) . . ? C00D C00A C00F 123.10(12) . . ? C006 C00B H00B 119.4 . . ? C00E C00B C006 121.16(13) . . ? C00E C00B H00B 119.4 . . ? C00A C00C H00C 119.6 . . ? C00I C00C C00A 120.84(13) . . ? C00I C00C H00C 119.6 . . ? C00A C00D H00D 119.9 . . ? C00J C00D C00A 120.10(13) . . ? C00J C00D H00D 119.9 . . ? C008 C00E H00E 119.3 . . ? C00B C00E C008 121.31(13) . . ? C00B C00E H00E 119.3 . . ? O002 C00F N003 124.29(13) . . ? O002 C00F C00A 121.38(13) . . ? N003 C00F C00A 114.30(12) . . ? C00I C00G Cl01 118.86(11) . . ? C00J C00G Cl01 118.96(11) . . ? C00J C00G C00I 122.18(13) . . ? C006 C00H H00H 119.2 . . ? C007 C00H C006 121.65(13) . . ? C007 C00H H00H 119.2 . . ? C00C C00I C00G 118.34(13) . . ? C00C C00I H00I 120.8 . . ? C00G C00I H00I 120.8 . . ? C00D C00J H00J 120.5 . . ? C00G C00J C00D 118.97(13) . . ? C00G C00J H00J 120.5 . . ? N005 C00K H00A 109.5 . . ? N005 C00K H00F 109.5 . . ? N005 C00K H00G 109.5 . . ? H00A C00K H00F 109.5 . . ? H00A C00K H00G 109.5 . . ? H00F C00K H00G 109.5 . . ? N005 C00L H00K 109.5 . . ? N005 C00L H00L 109.5 . . ? N005 C00L H00M 109.5 . . ? H00K C00L H00L 109.5 . . ? H00K C00L H00M 109.5 . . ? H00L C00L H00M 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl01 C00G 1.7505(14) . ? O002 C00F 1.2260(18) . ? N003 H003 0.8800 . ? N003 N004 1.3833(16) . ? N003 C00F 1.3554(19) . ? N004 C009 1.2798(19) . ? N005 C008 1.4009(18) . ? N005 C00K 1.4578(19) . ? N005 C00L 1.451(2) . ? C006 C009 1.4608(19) . ? C006 C00B 1.401(2) . ? C006 C00H 1.394(2) . ? C007 H007 0.9500 . ? C007 C008 1.404(2) . ? C007 C00H 1.388(2) . ? C008 C00E 1.410(2) . ? C009 H009 0.9500 . ? C00A C00C 1.394(2) . ? C00A C00D 1.397(2) . ? C00A C00F 1.4990(19) . ? C00B H00B 0.9500 . ? C00B C00E 1.377(2) . ? C00C H00C 0.9500 . ? C00C C00I 1.385(2) . ? C00D H00D 0.9500 . ? C00D C00J 1.389(2) . ? C00E H00E 0.9500 . ? C00G C00I 1.388(2) . ? C00G C00J 1.381(2) . ? C00H H00H 0.9500 . ? C00I H00I 0.9500 . ? C00J H00J 0.9500 . ? C00K H00A 0.9800 . ? C00K H00F 0.9800 . ? C00K H00G 0.9800 . ? C00L H00K 0.9800 . ? C00L H00L 0.9800 . ? C00L H00M 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl01 C00G C00I C00C -178.70(10) . . . . ? Cl01 C00G C00J C00D 179.62(10) . . . . ? N003 N004 C009 C006 176.59(11) . . . . ? N004 N003 C00F O002 -4.8(2) . . . . ? N004 N003 C00F C00A 177.02(11) . . . . ? N005 C008 C00E C00B -178.04(12) . . . . ? C006 C00B C00E C008 -0.9(2) . . . . ? C007 C008 C00E C00B 0.3(2) . . . . ? C008 C007 C00H C006 -1.4(2) . . . . ? C009 C006 C00B C00E -177.53(12) . . . . ? C009 C006 C00H C007 178.69(12) . . . . ? C00A C00C C00I C00G -0.9(2) . . . . ? C00A C00D C00J C00G -1.0(2) . . . . ? C00B C006 C009 N004 -13.4(2) . . . . ? C00B C006 C00H C007 0.8(2) . . . . ? C00C C00A C00D C00J 0.7(2) . . . . ? C00C C00A C00F O002 -33.12(19) . . . . ? C00C C00A C00F N003 145.14(13) . . . . ? C00D C00A C00C C00I 0.2(2) . . . . ? C00D C00A C00F O002 145.69(14) . . . . ? C00D C00A C00F N003 -36.05(18) . . . . ? C00F N003 N004 C009 168.13(13) . . . . ? C00F C00A C00C C00I 179.10(12) . . . . ? C00F C00A C00D C00J -178.09(12) . . . . ? C00H C006 C009 N004 168.79(13) . . . . ? C00H C006 C00B C00E 0.3(2) . . . . ? C00H C007 C008 N005 179.12(12) . . . . ? C00H C007 C008 C00E 0.8(2) . . . . ? C00I C00G C00J C00D 0.4(2) . . . . ? C00J C00G C00I C00C 0.5(2) . . . . ? C00K N005 C008 C007 143.91(14) . . . . ? C00K N005 C008 C00E -37.83(18) . . . . ? C00L N005 C008 C007 5.7(2) . . . . ? C00L N005 C008 C00E -176.08(13) . . . . ?