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Information card for entry 1572874
Preview
| Coordinates | 1572874.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H20 O4 |
|---|---|
| Calculated formula | C24 H20 O4 |
| Title of publication | Three-component modular synthesis of chiral 1,3-dioxoles via Rh-catalyzed carbenic olefination cascade |
| Authors of publication | Huang, Shisheng; Luo, Jilong; Chen, Ping; Chen, Jiean; Wang, Zhaofeng |
| Journal of publication | Chemical Science |
| Year of publication | 2024 |
| a | 5.57076 ± 0.00008 Å |
| b | 7.79768 ± 0.00012 Å |
| c | 42.0452 ± 0.0006 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1826.4 ± 0.05 Å3 |
| Cell temperature | 105 ± 2 K |
| Ambient diffraction temperature | 105 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0334 |
| Residual factor for significantly intense reflections | 0.0317 |
| Weighted residual factors for significantly intense reflections | 0.0792 |
| Weighted residual factors for all reflections included in the refinement | 0.0803 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 295497 (current) | 2024-10-16 | cif/ Adding structures of 1572874 via cif-deposit CGI script. |
1572874.cif |
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Users of the data should acknowledge the original authors of the
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