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Information card for entry 1572874
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Coordinates | 1572874.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H20 O4 |
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Calculated formula | C24 H20 O4 |
Title of publication | Three-component modular synthesis of chiral 1,3-dioxoles via Rh-catalyzed carbenic olefination cascade |
Authors of publication | Huang, Shisheng; Luo, Jilong; Chen, Ping; Chen, Jiean; Wang, Zhaofeng |
Journal of publication | Chemical Science |
Year of publication | 2024 |
a | 5.57076 ± 0.00008 Å |
b | 7.79768 ± 0.00012 Å |
c | 42.0452 ± 0.0006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1826.4 ± 0.05 Å3 |
Cell temperature | 105 ± 2 K |
Ambient diffraction temperature | 105 ± 2 K |
Number of distinct elements | 3 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0334 |
Residual factor for significantly intense reflections | 0.0317 |
Weighted residual factors for significantly intense reflections | 0.0792 |
Weighted residual factors for all reflections included in the refinement | 0.0803 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
295497 (current) | 2024-10-16 | cif/ Adding structures of 1572874 via cif-deposit CGI script. |
1572874.cif |
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Users of the data should acknowledge the original authors of the
structural data.