#------------------------------------------------------------------------------ #$Date: 2024-10-20 01:11:33 +0300 (Sun, 20 Oct 2024) $ #$Revision: 295552 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/29/1572906.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572906 loop_ _publ_author_name 'Kage, Mirai' 'Yamakoshi, Hiroyuki' 'Tabata, Manami' 'Ohashi, Eisaku' 'Noguchi, Kimihiro' 'Watanabe, Takeshi' 'Uchida, Manato' 'Takada, Minetatsu' 'Ikeuchi, Kazutada' 'Nakamura, Seiichi' _publ_section_title ; Oxidative generation of isobenzofurans from phthalans: application to the formal synthesis of (+-)-morphine ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC05890A _journal_year 2024 _chemical_formula_moiety 'C21 H29 N O5' _chemical_formula_sum 'C21 H29 N O5' _chemical_formula_weight 375.45 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2023-01-20 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 89.490(9) _cell_angle_beta 98.254(7) _cell_angle_gamma 89.986(6) _cell_formula_units_Z 2 _cell_length_a 7.6082(4) _cell_length_b 11.0116(11) _cell_length_c 10.8744(13) _cell_measurement_reflns_used 6935 _cell_measurement_temperature 103(2) _cell_measurement_theta_max 30.8580 _cell_measurement_theta_min 2.6220 _cell_volume 901.57(15) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection CrystalClear _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Yadokari-XG 2011 (Wakita Nemoto et al., 2011)' _computing_publication_material 'Yadokari-XG 2011 (Wakita,Nemoto et al., 2011)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 103(2) _diffrn_detector_area_resol_mean 28.5714 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measurement_device_type 'Rigaku VariMax Saturn' _diffrn_measurement_method \w _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1089 _diffrn_reflns_av_unetI/netI 0.0590 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.982 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 14919 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.982 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.500 _diffrn_reflns_theta_min 1.849 _diffrn_source 'rotating-anode X-ray tube' _exptl_absorpt_coefficient_mu 0.098 _exptl_absorpt_correction_T_max 0.997 _exptl_absorpt_correction_T_min 0.985 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.383 _exptl_crystal_description platelet _exptl_crystal_F_000 404 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.030 _refine_diff_density_max 0.525 _refine_diff_density_min -0.578 _refine_diff_density_rms 0.097 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.322 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 245 _refine_ls_number_reflns 3335 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.322 _refine_ls_R_factor_all 0.1234 _refine_ls_R_factor_gt 0.1083 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2898 _refine_ls_wR_factor_ref 0.3177 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2740 _reflns_number_total 3335 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05890a2.cif _cod_data_source_block samp2 _cod_database_code 1572906 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.985 _shelx_estimated_absorpt_t_max 0.997 _shelx_res_file ; samp2.res created by SHELXL-2014/7 TITL REM Yadorkari-X generated CELL 0.71073 7.6082 11.0116 10.8744 89.4900 98.2540 89.9860 ZERR 2.0 0.0004 0.0011 0.0013 0.0090 0.0070 0.0060 LATT 1 REM SPGR P-1 triclinic SFAC C H N O UNIT 42 58 2 10 SIZE 0.15 0.10 0.03 TEMP -170.0 L.S. 10 FMAP 2 PLAN -25 ACTA CONF LIST 4 OMIT -10.000000 51.000000 OMIT 0 0 1 OMIT -1 -7 8 OMIT -3 -5 10 TWIN 1 0 0 0 -1 0 0 0 1 WGHT 0.200000 BASF 0.37507 FVAR 8.70130 O1 4 0.424638 0.947973 0.265938 11.00000 0.00897 0.05717 = 0.04735 0.01268 0.00191 -0.00019 O2 4 0.927141 0.551286 0.769023 11.00000 0.01718 0.04750 = 0.04081 0.00663 0.00001 -0.00029 C1 1 0.839611 0.646183 0.530210 11.00000 0.01226 0.04536 = 0.04212 0.00914 -0.00081 -0.00136 AFIX 13 H1 2 0.904073 0.568211 0.552939 11.00000 -1.20000 AFIX 0 O3 4 0.622959 1.121178 0.183848 11.00000 0.01946 0.04875 = 0.05645 0.01533 0.00237 -0.00224 O4 4 0.807284 0.713019 0.847196 11.00000 0.02105 0.06748 = 0.03573 0.00805 -0.00012 0.00175 C2 1 0.439823 0.643691 0.201971 11.00000 0.01575 0.05065 = 0.04009 0.00621 -0.00407 -0.01296 AFIX 13 H2 2 0.512711 0.703816 0.161914 11.00000 -1.20000 AFIX 0 O5 4 0.280600 0.621299 0.117595 11.00000 0.02020 0.05153 = 0.04502 0.01101 -0.00705 -0.00462 AFIX 83 H3 2 0.221871 0.685958 0.105199 11.00000 -1.50000 AFIX 0 C4 1 0.672793 0.619433 0.438782 11.00000 0.01257 0.04722 = 0.03975 0.01289 -0.00140 -0.00596 AFIX 13 H4 2 0.597757 0.562438 0.480925 11.00000 -1.20000 AFIX 0 N1 3 0.787342 0.698818 0.642160 11.00000 0.01546 0.05154 = 0.04099 0.00767 -0.00124 0.00160 C6 1 0.395931 0.698356 0.320202 11.00000 0.01494 0.04170 = 0.04685 0.01537 -0.00061 -0.00302 AFIX 23 H5 2 0.329021 0.638475 0.363587 11.00000 -1.20000 H6 2 0.318960 0.770340 0.299701 11.00000 -1.20000 AFIX 0 C7 1 0.513695 0.782567 0.527903 11.00000 0.01141 0.04836 = 0.04182 0.01274 -0.00232 -0.00147 AFIX 23 H7 2 0.435718 0.722141 0.560856 11.00000 -1.20000 H8 2 0.445290 0.858892 0.511227 11.00000 -1.20000 AFIX 0 C8 1 0.895990 1.021838 0.279068 11.00000 0.02002 0.03750 = 0.05039 0.00531 0.00596 -0.00788 AFIX 43 H20 2 0.969273 1.083291 0.251589 11.00000 -1.20000 AFIX 0 C9 1 0.549201 0.531260 0.231050 11.00000 0.01750 0.04847 = 0.04516 0.00560 -0.00171 -0.00306 AFIX 23 H9 2 0.583978 0.498871 0.153378 11.00000 -1.20000 H10 2 0.477205 0.468705 0.266588 11.00000 -1.20000 AFIX 0 C10 1 0.674572 0.805945 0.625705 11.00000 0.01560 0.05566 = 0.04096 0.01020 -0.00144 0.00077 AFIX 23 H11 2 0.742968 0.875586 0.599351 11.00000 -1.20000 H12 2 0.634438 0.826650 0.705619 11.00000 -1.20000 AFIX 0 C11 1 0.865444 0.770266 1.056218 11.00000 0.02839 0.07064 = 0.04038 0.00594 0.00305 -0.00458 AFIX 33 H13 2 0.906451 0.743190 1.141613 11.00000 -1.50000 H14 2 0.943641 0.834732 1.033190 11.00000 -1.50000 H15 2 0.743848 0.801440 1.050434 11.00000 -1.50000 AFIX 0 C12 1 0.962082 0.731935 0.468850 11.00000 0.01004 0.05582 = 0.04040 0.00590 -0.00084 -0.00591 AFIX 23 H21 2 1.047625 0.769386 0.534855 11.00000 -1.20000 H22 2 1.031000 0.683162 0.416385 11.00000 -1.20000 AFIX 0 C13 1 0.716666 0.557318 0.323541 11.00000 0.01356 0.05327 = 0.04061 0.00842 0.00186 0.00095 AFIX 23 H16 2 0.779176 0.479980 0.347627 11.00000 -1.20000 H17 2 0.797590 0.609625 0.282883 11.00000 -1.20000 AFIX 0 C14 1 0.608272 0.933721 0.287771 11.00000 0.00756 0.05048 = 0.04429 0.00808 -0.00060 -0.00211 C15 1 0.866996 0.831309 0.390191 11.00000 0.01273 0.04798 = 0.03763 0.00534 0.00004 -0.00398 C16 1 0.712160 1.027489 0.248569 11.00000 0.01702 0.04722 = 0.04143 0.00764 0.00096 -0.00132 C17 1 0.680041 0.834990 0.356013 11.00000 0.01114 0.04540 = 0.03801 0.00913 0.00165 -0.00416 C18 1 0.969357 0.925570 0.349735 11.00000 0.01339 0.06152 = 0.04123 0.01169 0.00108 -0.00697 AFIX 43 H23 2 1.094671 0.922721 0.372141 11.00000 -1.20000 AFIX 0 C19 1 0.847545 0.646196 0.752180 11.00000 0.01028 0.05633 = 0.04123 0.00470 0.00150 -0.00756 C20 1 0.565200 0.736575 0.407774 11.00000 0.01346 0.04642 = 0.04369 0.01443 0.00126 -0.00485 C21 1 0.723891 1.223553 0.151990 11.00000 0.02900 0.05194 = 0.05166 0.01204 0.00596 -0.00500 AFIX 33 H24 2 0.644023 1.283481 0.106124 11.00000 -1.50000 H25 2 0.785234 1.260322 0.228010 11.00000 -1.50000 H26 2 0.811493 1.196923 0.100034 11.00000 -1.50000 AFIX 0 C22 1 0.341844 0.952107 0.139975 11.00000 0.01980 0.05759 = 0.04704 0.01302 -0.00155 -0.00006 AFIX 33 H27 2 0.213379 0.962325 0.137256 11.00000 -1.50000 H28 2 0.389451 1.020608 0.097055 11.00000 -1.50000 H29 2 0.365700 0.876235 0.098892 11.00000 -1.50000 AFIX 0 C23 1 0.869080 0.666011 0.970178 11.00000 0.02519 0.05620 = 0.03707 0.00873 -0.00249 -0.00001 AFIX 23 H18 2 0.991215 0.633550 0.974679 11.00000 -1.20000 H19 2 0.790363 0.600081 0.992015 11.00000 -1.20000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM REM R1 = 0.1083 for 2740 Fo > 4sig(Fo) and 0.1234 for all 3335 data REM 245 parameters refined using 0 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 0.525, deepest hole -0.578, 1-sigma level 0.097 Q1 1 0.7890 0.8218 0.3522 11.00000 0.05 0.52 Q2 1 0.4937 0.7222 0.3850 11.00000 0.05 0.49 Q3 1 0.2813 1.0402 0.1196 11.00000 0.05 0.47 Q4 1 0.5672 1.1133 0.1703 11.00000 0.05 0.45 Q5 1 0.7616 0.6309 0.4715 11.00000 0.05 0.44 Q6 1 0.8529 0.7200 0.8582 11.00000 0.05 0.41 Q7 1 0.6231 0.5472 0.2578 11.00000 0.05 0.40 Q8 1 0.2603 0.5417 0.1327 11.00000 0.05 0.39 Q9 1 0.6471 0.5551 0.2952 11.00000 0.05 0.39 Q10 1 0.5992 0.7952 0.5743 11.00000 0.05 0.39 Q11 1 0.9344 0.8401 0.4578 11.00000 0.05 0.37 Q12 1 0.2511 0.8836 0.1252 11.00000 0.05 0.37 Q13 1 0.3987 0.8575 0.2626 11.00000 0.05 0.37 Q14 1 0.7778 1.0400 0.2820 11.00000 0.05 0.36 Q15 1 0.3683 0.6328 0.1920 11.00000 0.05 0.36 Q16 1 0.4875 0.9542 0.2830 11.00000 0.05 0.35 Q17 1 0.9158 0.9234 0.2760 11.00000 0.05 0.35 Q18 1 0.3615 0.6222 0.1242 11.00000 0.05 0.34 Q19 1 0.8536 0.6129 0.8642 11.00000 0.05 0.34 Q20 1 0.7367 0.6781 0.6237 11.00000 0.05 0.33 Q21 1 0.8911 0.6581 0.7688 11.00000 0.05 0.31 Q22 1 0.9089 0.8581 0.3654 11.00000 0.05 0.31 Q23 1 0.7411 0.6377 0.8468 11.00000 0.05 0.30 Q24 1 0.6878 0.9371 0.3465 11.00000 0.05 0.30 Q25 1 0.5298 0.9362 0.2638 11.00000 0.05 0.30 ; _shelx_res_checksum 82883 _shelx_hkl_file ; 0 0 -1-64.9149 53.6705 1 0 0 1-49.4754 77.7115 1 0 0 -1-88.1677 65.7709 1 0 0 2 289919. 1607.70 1 0 0 2 273233. 1687.73 1 0 0 -2 234085. 1352.19 1 0 0 2 289994. 1795.82 1 0 0 -2 324015. 2291.28 1 0 0 -2 300686. 1780.33 1 0 0 -2 256892. 2080.85 1 0 0 2 268755. 1533.99 1 0 0 2 266381. 2026.52 1 0 0 -3 6045.38 503.484 1 0 0 -3 6602.60 401.521 1 0 0 3 5879.27 326.559 1 0 0 3 6182.61 395.479 1 0 0 -3 5892.34 545.879 1 0 0 3 6011.08 340.397 1 0 0 4 75.0309 223.435 1 0 0 -4 369.350 422.508 1 0 0 4 461.266 237.107 1 0 0 4 111.821 266.440 1 0 0 -4 162.331 303.831 1 0 0 -4 390.046 227.357 1 0 0 5 389.077 229.611 1 0 0 5 160.637 287.320 1 0 0 -5-320.509 332.811 1 0 0 -5-23.5387 234.671 1 0 0 5-24.1036 240.048 1 0 0 -5 137.410 456.849 1 0 0 -6 1061.10 396.965 1 0 0 -6 1897.75 575.358 1 0 0 6 1713.77 287.167 1 0 0 6 1505.29 351.090 1 0 0 -6 1851.03 343.227 1 0 0 6 1536.54 395.673 1 0 0 7 562.814 387.614 1 0 0 7 103.646 252.845 1 0 0 -7 96.9451 233.420 1 0 0 -7 343.636 374.450 1 0 0 -7 548.645 497.979 1 0 0 7 347.924 248.903 1 0 0 -8 22482.3 1245.81 1 0 0 8 17301.9 1024.36 1 0 0 8 18040.3 857.883 1 0 0 -8 21643.4 949.108 1 0 0 -8 19031.2 1199.99 1 0 0 8 16278.1 786.997 1 0 0 -9 770.135 649.514 1 0 0 -9 200.217 401.814 1 0 0 -9 249.971 249.669 1 0 0 9-28.5649 430.449 1 0 0 9-111.151 318.595 1 0 0 9 225.208 286.084 1 0 0 10 14977.1 923.391 1 0 0 10 17671.7 1203.88 1 0 0 -10 17048.1 1304.46 1 0 0 -10 15365.0 1260.86 1 0 0 10 18927.5 1006.36 1 0 0 -10 19595.0 1022.58 1 0 0 11-9.83622 357.491 1 0 0 -11 147.689 319.484 1 0 0 -11 0.85059 531.271 1 0 0 -11-380.510 577.393 1 0 0 11-229.222 400.625 1 0 0 11 817.148 549.230 1 0 0 12 866.347 455.106 1 0 0 -12 1018.97 661.202 1 0 0 12 1170.93 647.361 1 0 0 -12 856.216 492.555 1 0 0 13-474.793 453.234 1 0 0 -13 287.309 412.220 1 0 0 13 281.367 648.374 1 0 0 -13-647.375 673.814 1 0 0 14 825.858 522.764 1 0 0 -14 48.3326 697.051 1 0 0 14 220.096 701.610 1 0 0 15 448.217 749.218 1 0 -1 15 1493.27 798.961 1 0 1 -14 3164.50 1013.45 1 0 -1 14 5572.41 922.327 1 0 -1 14 6293.27 1097.13 1 0 1 -13 597.444 724.995 1 0 -1 13 579.339 634.977 1 0 -1 13 2239.50 601.899 1 0 1 -13 1179.85 555.061 1 0 -1 12 351.665 544.761 1 0 1 -12 189.323 578.675 1 0 -1 12-346.346 426.000 1 0 1 -12-787.135 406.065 1 0 -1 12-481.279 382.427 1 0 -1 11 7273.92 953.581 1 0 -1 11 8844.25 784.026 1 0 1 -11 9210.43 1133.76 1 0 1 -11 10140.0 845.962 1 0 1 -10 3069.76 697.672 1 0 -1 10 2524.26 481.178 1 0 1 -10 3056.12 715.006 1 0 -1 10 4626.93 770.284 1 0 -1 10 3132.43 570.915 1 0 1 -10 3766.01 564.695 1 0 1 -9 53918.4 1642.71 1 0 -1 9 24053.9 1049.12 1 0 -1 9 33847.1 1499.24 1 0 -1 9 35247.5 1236.99 1 0 1 -9 65308.0 2296.85 1 0 1 -9 49820.9 1846.59 1 0 -1 8 2525.00 398.539 1 0 -1 8 2130.35 409.409 1 0 1 -8 1694.82 381.362 1 0 -1 8 1935.31 516.032 1 0 1 -8 1655.60 526.709 1 0 1 -8 1857.92 616.702 1 0 -1 7 11336.2 643.296 1 0 1 -7 9065.80 662.898 1 0 -1 7 12257.2 654.231 1 0 -1 7 12300.4 831.669 1 0 1 -7 8693.40 831.422 1 0 1 -7 8810.22 799.651 1 0 1 -6 925.111 461.648 1 0 1 -6 852.620 313.639 1 0 -1 6 693.989 347.387 1 0 -1 6 1190.54 293.226 1 0 -1 6 516.586 236.358 1 0 1 -6 504.346 376.127 1 0 -1 5 9317.41 506.711 1 0 1 -5 5351.15 642.935 1 0 1 -5 6465.17 609.654 1 0 1 -5 7177.27 536.739 1 0 -1 5 9931.98 542.020 1 0 -1 5 9309.95 680.113 1 0 1 -4 44023.1 1038.55 1 0 -1 4 59619.6 1347.76 1 0 -1 4 54332.2 1109.47 1 0 -1 4 53665.2 1033.18 1 0 1 -4 41205.5 1210.86 1 0 1 -4 35491.8 1099.10 1 0 -1 3 42940.6 882.522 1 0 -1 3 52030.7 951.571 1 0 1 -3 63608.0 1268.91 1 0 -1 3 41912.7 780.997 1 0 1 -3 57738.9 974.590 1 0 1 -3 62391.9 1100.65 1 0 -1 3 43174.3 1006.52 1 0 1 -2 121192. 1313.38 1 0 -1 2 84284.5 1016.86 1 0 -1 2 89704.0 1185.10 1 0 -1 2 104980. 883.586 1 0 1 -2 99170.7 1099.67 1 0 -1 2 90687.2 929.556 1 0 1 -1 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632.736 1 -1 -1 -1 45690.7 855.468 1 -1 -1 -2 75195.8 1074.11 1 1 1 2 61421.0 720.779 1 -1 -1 -2 84316.6 1409.70 1 -1 -1 -2 64373.4 747.760 1 1 1 3 7683.82 436.254 1 1 1 3 9322.88 334.810 1 -1 -1 -3 9746.37 644.234 1 -1 -1 -3 8761.22 353.912 1 -1 -1 -3 9398.23 498.789 1 1 1 3 8048.23 519.616 1 -1 -1 -4 27521.1 625.103 1 -1 -1 -4 26581.0 1040.85 1 1 1 4 26253.0 778.260 1 1 1 4 27495.7 898.486 1 -1 -1 -4 25785.0 1029.75 1 -1 -1 -4 28472.8 885.317 1 -1 -1 -5 28408.3 1148.79 1 -1 -1 -5 27469.0 929.955 1 -1 -1 -5 28794.2 1121.77 1 1 1 5 14577.2 666.156 1 1 1 5 14206.0 771.140 1 1 1 6 5500.72 574.857 1 -1 -1 -6 5664.37 653.631 1 -1 -1 -6 6801.35 562.920 1 1 1 6 5101.09 469.838 1 -1 -1 -7 21692.0 1150.99 1 1 1 7 11582.0 820.138 1 -1 -1 -7 26232.7 1059.86 1 -1 -1 -7 26159.8 1264.72 1 1 1 7 12435.0 697.151 1 -1 -1 -8 10041.8 710.669 1 -1 -1 -8 8033.63 828.269 1 1 1 8 11095.7 742.258 1 1 1 8 11574.6 881.485 1 -1 -1 -8 7724.21 793.624 1 1 1 9 14674.9 907.804 1 -1 -1 -9 12220.9 821.821 1 1 1 9 14418.7 1025.66 1 -1 -1 -9 7812.44 847.388 1 -1 -1 -9 9525.50 950.562 1 1 1 10 184.971 399.544 1 1 1 10-216.184 443.116 1 -1 -1 -10 22.3295 233.153 1 -1 -1 -10-982.589 539.788 1 -1 -1 -10 510.633 359.455 1 -1 -1 -11-29.9574 368.457 1 1 1 11-79.2166 507.878 1 -1 -1 -11 312.676 522.831 1 1 1 11 363.463 378.993 1 1 1 12 621.566 609.484 1 -1 -1 -12-456.247 634.625 1 1 1 12 654.336 447.062 1 -1 -1 -12-212.112 406.979 1 -1 -1 -13 920.865 739.066 1 -1 -1 -13 2465.82 621.591 1 1 1 13 1366.86 547.255 1 1 1 13 395.241 569.620 1 1 1 14 988.753 700.015 1 -1 -1 -14 30.5450 676.009 1 1 1 14 690.398 586.437 1 -1 -2 15 680.983 529.470 1 -1 -2 14 1080.87 766.217 1 -1 -2 14 1225.24 588.872 1 1 2 -14 871.280 748.278 1 1 2 -13 541.094 458.061 1 -1 -2 13 103.832 411.663 1 -1 -2 13 1160.67 744.002 1 1 2 -13-231.198 611.375 1 -1 -2 13 470.549 477.206 1 1 2 -12 2535.40 596.764 1 1 2 -12 2188.36 816.730 1 -1 -2 12 1578.90 491.489 1 -1 -2 12 2592.34 578.907 1 -1 -2 12 2407.30 757.250 1 1 2 -11 548.024 603.512 1 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822.391 395.914 1 -2 10 -5 1024.48 451.574 1 -2 10 -5 1018.94 415.720 1 2 -10 5 2224.02 598.797 1 2 -10 5 2118.63 629.511 1 2 -10 5 2820.74 592.345 1 -2 10 -6 881.576 430.651 1 2 -10 6 1873.19 608.099 1 -2 10 -6 282.436 406.446 1 2 -10 6 338.372 486.433 1 2 -10 7 1073.25 608.179 1 2 -10 7 1024.01 605.281 1 -2 10 -7-307.324 434.198 1 2 -10 8 9622.11 1163.46 1 -2 10 -8 1996.41 729.809 1 -2 10 -8 1572.66 718.205 1 2 -10 8 7129.16 1044.43 1 2 -10 9 221.456 623.072 1 -2 10 -9-874.392 574.168 1 2 -10 9 273.704 611.678 1 -2 10 -9-237.373 656.335 1 2 -10 10-519.499 704.576 1 2 -10 10 922.931 670.411 1 -2 10 -10 615.566 513.240 1 -2 9 12 868.166 520.039 1 2 -9 -11 1187.72 1043.94 1 -2 9 11 893.473 463.906 1 -2 9 10-306.549 375.533 1 2 -9 -10-274.351 902.559 1 2 -9 -9 345.502 830.386 1 2 -9 -9 1034.82 493.601 1 -2 9 8 256.342 372.876 1 2 -9 -8-468.773 785.608 1 2 -9 -8 494.647 415.955 1 2 -9 -7 1093.56 861.492 1 -2 9 7 1519.13 374.835 1 2 -9 -7 405.971 348.489 1 2 -9 -6-70.7122 310.996 1 2 -9 -6 351.251 711.708 1 -2 9 6-128.236 288.619 1 2 -9 -5 6438.47 1052.02 1 2 -9 -5 6258.35 608.272 1 2 -9 -4 1676.00 344.392 1 2 -9 -4 953.026 701.748 1 -2 9 4 2159.58 385.754 1 -2 9 4 1247.73 333.139 1 -2 9 3 19818.1 954.736 1 2 -9 -3 20278.7 849.755 1 -2 9 2 2710.95 364.047 1 -2 9 2 1499.90 288.599 1 2 -9 -2 1300.10 640.902 1 -2 9 2 3200.27 426.476 1 2 -9 -2 3363.21 441.837 1 -2 9 1 6657.90 535.219 1 -2 9 1 5505.60 440.050 1 2 -9 -1 6716.98 518.187 1 -2 9 1 4961.15 505.791 1 -2 9 0 4031.84 479.443 1 2 -9 0 3473.83 573.753 1 2 -9 1 1266.57 544.805 1 -2 9 -1 858.219 215.790 1 -2 9 -1 1786.67 371.908 1 -2 9 -1 1185.59 323.192 1 2 -9 1-28.1933 330.408 1 2 -9 1 426.197 392.686 1 2 -9 2 2613.80 525.508 1 2 -9 2 2084.26 504.378 1 -2 9 -2 1876.27 425.393 1 -2 9 -2 1367.62 367.205 1 2 -9 2 2699.78 540.340 1 2 -9 3 124.606 397.299 1 -2 9 -3-325.157 320.482 1 -2 9 -3-107.907 314.244 1 2 -9 3-115.090 393.711 1 2 -9 3 60.3797 406.571 1 2 -9 4 6003.94 690.249 1 2 -9 4 7161.18 714.746 1 -2 9 -4 3781.38 593.898 1 2 -9 4 5819.42 707.425 1 -2 9 -4 3430.82 496.174 1 -2 9 -5 2207.72 477.686 1 2 -9 5 5150.86 663.788 1 2 -9 5 3419.10 632.659 1 2 -9 5 4789.84 699.255 1 -2 9 -5 3035.84 597.866 1 2 -9 6 1159.31 516.916 1 2 -9 6 80.6670 452.766 1 -2 9 -6 949.934 468.189 1 2 -9 6 1199.31 557.649 1 -2 9 -6 209.637 388.937 1 2 -9 7 275.743 455.010 1 2 -9 7 234.792 500.773 1 -2 9 -7 555.814 474.599 1 -2 9 -7 249.436 451.740 1 2 -9 7 1151.10 508.924 1 2 -9 8 2509.13 713.189 1 2 -9 8 3343.08 769.804 1 -2 9 -8 206.540 484.434 1 -2 9 -8 1072.45 631.261 1 2 -9 8 1954.37 565.297 1 2 -9 9-352.253 612.172 1 2 -9 9 446.714 552.136 1 -2 9 -9 152.904 540.782 1 2 -9 10 958.698 676.175 1 -2 9 -10 116.522 550.684 1 2 -9 10 381.488 632.105 1 -2 9 -10-584.114 644.367 1 -2 9 -11 1272.06 744.471 1 -2 8 12 20.0931 408.815 1 2 -8 -12 693.899 943.389 1 2 -8 -11-469.767 493.576 1 2 -8 -11 1077.39 896.119 1 -2 8 11 731.609 419.450 1 -2 8 10-344.731 379.869 1 2 -8 -10-787.491 486.295 1 2 -8 -9-558.182 843.279 1 -2 8 9 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707.877 1 -2 8 -1 6594.90 508.011 1 2 -8 1 8487.83 713.236 1 2 -8 2 2592.72 483.930 1 -2 8 -2 1677.06 201.646 1 -2 8 -2 2348.59 409.074 1 2 -8 2 1874.60 470.354 1 -2 8 -2 2634.93 426.767 1 2 -8 2 2133.29 508.203 1 -2 8 -3-283.349 283.975 1 2 -8 3 148.896 346.821 1 2 -8 3 48.8236 358.396 1 -2 8 -3 355.074 313.036 1 2 -8 3 68.9156 343.068 1 2 -8 4 298.748 399.730 1 2 -8 4 1332.12 458.003 1 2 -8 4 1107.67 420.556 1 -2 8 -4 1115.68 406.610 1 -2 8 -4 1253.88 357.720 1 2 -8 5 108.714 455.052 1 2 -8 5-167.541 414.022 1 2 -8 5 1079.01 495.233 1 -2 8 -5 1789.63 532.799 1 -2 8 -5 1926.60 445.839 1 2 -8 6 7359.99 817.409 1 2 -8 6 7339.83 761.372 1 2 -8 6 8943.32 888.178 1 -2 8 -7-107.032 431.183 1 2 -8 7 67.3577 390.473 1 2 -8 7 104.957 478.710 1 -2 8 -7 20.6830 402.609 1 2 -8 7-839.200 507.538 1 2 -8 8-56.7449 504.366 1 -2 8 -8 127.614 412.207 1 -2 8 -8 1.23750 516.216 1 2 -8 8 39.4485 402.082 1 2 -8 8-335.031 511.016 1 2 -8 9 195.606 534.249 1 2 -8 9 952.191 603.384 1 -2 8 -9 63.4498 521.797 1 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2935.62 477.257 1 2 -7 -5 10259.0 1110.15 1 -2 7 5 4419.90 506.681 1 2 -7 -5 8304.42 670.157 1 2 -7 -4 2830.24 420.411 1 -2 7 4 3083.29 288.614 1 2 -7 -4 4569.04 848.601 1 -2 7 4 3816.60 412.381 1 2 -7 -4 2138.95 222.512 1 -2 7 4 2025.80 353.386 1 -2 7 3 1265.50 208.741 1 2 -7 -3 1421.78 274.516 1 -2 7 3 1026.85 288.342 1 -2 7 3 1511.57 274.603 1 2 -7 -2 21758.4 754.731 1 -2 7 2 18864.7 634.661 1 2 -7 -2 18678.9 1340.16 1 -2 7 2 22509.2 796.286 1 -2 7 2 21670.7 833.829 1 -2 7 1 11318.3 523.544 1 2 -7 -1 14031.1 867.232 1 -2 7 1 9936.89 543.538 1 2 -7 -1 9675.49 1050.89 1 -2 7 1 11710.0 603.027 1 2 -7 -1 12797.3 623.831 1 -2 7 0 1172.39 272.823 1 2 -7 0 1015.22 483.921 1 2 -7 0 467.261 338.612 1 -2 7 0 2047.72 316.744 1 2 -7 0 1144.31 454.163 1 -2 7 -1 8866.70 603.755 1 2 -7 1 17537.8 849.523 1 2 -7 1 16230.7 848.653 1 2 -7 1 21068.7 964.819 1 2 -7 1 9716.04 793.608 1 -2 7 -1 14093.0 652.824 1 2 -7 2 24.8054 338.254 1 2 -7 2-366.742 308.500 1 -2 7 -2 132.880 126.675 1 -2 7 -2 126.735 240.251 1 -2 7 -2 86.7558 257.747 1 2 -7 2 4.14376 323.577 1 -2 7 -3 5903.64 541.599 1 -2 7 -3 5470.41 573.420 1 2 -7 3 5800.75 626.929 1 2 -7 3 2686.40 525.521 1 2 -7 3 3269.34 526.454 1 -2 7 -3 2019.99 166.336 1 2 -7 4 2342.97 521.418 1 2 -7 4 1994.97 482.881 1 -2 7 -4 1019.42 355.280 1 -2 7 -4 1131.92 335.241 1 2 -7 4 1290.53 432.622 1 2 -7 5 3899.04 556.176 1 -2 7 -5 1817.25 402.254 1 2 -7 5 2697.66 555.739 1 2 -7 5 3818.98 590.655 1 -2 7 -5 3151.33 528.662 1 -2 7 -6 10017.6 870.129 1 2 -7 6 17593.8 1025.03 1 2 -7 6 18824.2 1198.86 1 2 -7 6 17150.2 1126.82 1 -2 7 -6 11694.0 935.310 1 2 -7 7 10383.7 999.740 1 2 -7 7 10579.3 974.010 1 -2 7 -7 4142.44 752.805 1 -2 7 -7 6562.40 792.952 1 2 -7 7 14202.9 971.531 1 2 -7 8 1928.29 510.163 1 2 -7 8 1907.33 665.374 1 -2 7 -8 557.793 467.385 1 2 -7 8 1810.12 577.733 1 -2 7 -8 185.357 461.902 1 2 -7 9-803.040 548.328 1 -2 7 -9 268.749 421.990 1 2 -7 9 955.430 585.929 1 -2 7 -9 685.447 588.691 1 2 -7 9-227.407 438.639 1 2 -7 10 1101.70 698.472 1 2 -7 10-31.1687 421.900 1 2 -7 10-370.744 590.393 1 -2 7 -10 714.142 510.271 1 -2 7 -10-687.772 639.048 1 2 -7 11 1180.28 689.305 1 2 -7 11 903.895 544.490 1 -2 7 -11-99.0687 609.903 1 2 -7 11 1690.95 743.033 1 -2 7 -11 315.916 550.523 1 2 -7 12-163.353 679.213 1 -2 7 -12-176.924 526.613 1 2 -7 12 597.937 635.619 1 2 -7 12 19.1287 471.104 1 -2 7 -12-381.760 740.041 1 2 -7 13 1967.58 742.174 1 2 -6 -14 374.886 1008.09 1 2 -6 -14-119.045 552.669 1 2 -6 -13 1077.25 984.114 1 -2 6 13 959.996 495.356 1 2 -6 -13 699.805 635.647 1 2 -6 -12-721.107 576.928 1 -2 6 12-11.7484 395.724 1 2 -6 -12-435.330 1006.91 1 2 -6 -11 3055.18 1184.21 1 2 -6 -11 204.956 502.750 1 2 -6 -10 2180.90 1058.84 1 -2 6 10 234.326 359.226 1 -2 6 10 336.772 407.813 1 2 -6 -10 1454.97 514.291 1 2 -6 -9 3590.04 701.802 1 -2 6 9 3515.15 527.106 1 -2 6 9 1928.38 484.028 1 2 -6 -9 2341.68 996.862 1 2 -6 -8 10577.7 911.789 1 -2 6 8 1342.02 480.530 1 -2 6 8 2485.36 521.227 1 2 -6 -8 11299.1 1424.98 1 -2 6 7 2736.05 424.042 1 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31425.5 1209.78 1 2 -6 1 48155.9 1378.35 1 -2 6 -1 30691.9 1056.42 1 2 -6 2 3387.23 488.072 1 -2 6 -2 7775.52 577.026 1 -2 6 -2 7963.44 514.884 1 2 -6 2 5324.38 564.918 1 2 -6 2 3240.97 554.783 1 -2 6 -3 17623.0 766.763 1 -2 6 -3 6689.78 289.511 1 -2 6 -3 18166.3 956.381 1 2 -6 3 16237.5 967.015 1 2 -6 3 13663.3 846.894 1 2 -6 3 12051.5 882.986 1 2 -6 4 1930.91 441.746 1 2 -6 4 1538.65 371.621 1 -2 6 -4 1601.94 393.149 1 -2 6 -4 1274.36 352.671 1 2 -6 4 1802.41 453.340 1 -2 6 -5 7846.05 707.812 1 -2 6 -5 6288.29 596.173 1 2 -6 5 12413.7 891.797 1 2 -6 5 12292.9 845.715 1 2 -6 5 14374.4 961.965 1 2 -6 6 10715.3 816.216 1 -2 6 -6 6622.89 739.864 1 -2 6 -6 7113.88 800.133 1 2 -6 6 9682.16 863.055 1 2 -6 6 9791.77 885.281 1 2 -6 7 195.364 462.580 1 2 -6 7 199.501 424.905 1 -2 6 -7 340.023 442.957 1 2 -6 7 795.334 416.947 1 -2 6 -7 243.807 432.334 1 2 -6 8-99.6102 506.017 1 2 -6 8 974.415 494.888 1 -2 6 -8 181.319 433.673 1 2 -6 8 1218.36 420.857 1 -2 6 -8 510.756 418.010 1 2 -6 9 1642.68 580.349 1 2 -6 9 1749.66 662.627 1 -2 6 -9 2562.69 689.557 1 -2 6 -9 1301.12 656.117 1 2 -6 9 2982.92 613.168 1 2 -6 10-123.361 426.997 1 2 -6 10 638.379 604.580 1 -2 6 -10 293.280 518.660 1 -2 6 -10 292.891 545.127 1 2 -6 10-789.492 597.665 1 -2 6 -11-614.886 674.084 1 2 -6 11-545.522 601.880 1 2 -6 11-734.673 669.668 1 2 -6 11 689.370 486.308 1 -2 6 -11 809.493 548.662 1 -2 6 -12 409.222 544.875 1 2 -6 12-943.174 735.224 1 2 -6 12-295.768 578.976 1 2 -6 12 118.884 477.523 1 -2 6 -12-444.086 694.903 1 2 -6 13 1165.78 593.627 1 2 -5 -14-252.957 592.790 1 2 -5 -14-1292.15 1075.68 1 -2 5 14 559.131 590.389 1 2 -5 -13 45.2553 519.123 1 2 -5 -13-796.061 1006.54 1 -2 5 13 91.2220 455.914 1 -2 5 12 444.150 434.661 1 -2 5 12 211.387 569.280 1 2 -5 -12 1593.93 651.541 1 -2 5 11 1145.81 555.164 1 2 -5 -11-164.807 472.682 1 -2 5 11 814.065 404.361 1 2 -5 -11-217.569 910.330 1 2 -5 -10 9122.79 1534.93 1 -2 5 10 5087.98 580.013 1 2 -5 -10 11325.7 1045.08 1 -2 5 10 2534.71 497.499 1 -2 5 9 459.660 386.249 1 2 -5 -9 5502.02 1073.04 1 2 -5 -9 4490.89 651.927 1 -2 5 9 915.493 354.977 1 -2 5 8 2737.52 485.776 1 2 -5 -8 8961.83 1221.07 1 2 -5 -8 7550.40 784.638 1 -2 5 8 2776.91 538.923 1 2 -5 -7 2124.34 864.977 1 2 -5 -7 1786.44 497.148 1 -2 5 7 1897.17 364.194 1 -2 5 7 1650.22 359.339 1 2 -5 -6 935.255 334.413 1 -2 5 6 1436.28 302.995 1 2 -5 -6 1086.30 748.483 1 -2 5 6 1081.20 149.476 1 -2 5 6 2232.12 352.323 1 -2 5 5 2580.44 270.982 1 -2 5 5 3103.25 463.420 1 2 -5 -5 6627.12 578.012 1 2 -5 -5 6580.60 921.190 1 -2 5 5 2420.13 399.967 1 2 -5 -4 3596.88 470.953 1 -2 5 4 2299.31 388.480 1 -2 5 4 5756.78 321.701 1 2 -5 -4 7440.69 858.162 1 -2 5 4 1931.97 407.806 1 -2 5 3 3478.21 420.471 1 2 -5 -3 7140.45 812.802 1 -2 5 3 3495.89 469.157 1 -2 5 3 7073.11 327.488 1 -2 5 3 3934.36 206.164 1 -2 5 3 5836.11 249.621 1 2 -5 -3 6538.21 436.372 1 -2 5 2 1791.29 307.985 1 2 -5 -2 1573.53 612.498 1 -2 5 2 1375.02 208.234 1 -2 5 2 1607.75 228.662 1 -2 5 2 1560.05 286.340 1 2 -5 -2 1612.89 257.011 1 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860.021 1 -2 -7 -8 1214.81 497.622 1 2 7 8 348.945 267.510 1 2 7 8 385.481 386.995 1 -2 -7 -8 1451.48 380.364 1 -2 -7 -9 389.545 378.857 1 2 7 9 122.331 252.737 1 2 7 9 323.409 424.353 1 -2 -7 -9 472.728 466.053 1 -2 -7 -10 827.169 571.060 1 2 7 10-63.6064 268.559 1 2 7 10 190.873 415.558 1 -2 -7 -11 989.468 612.111 1 2 7 11 640.536 335.537 1 2 7 11 1201.42 529.974 1 2 7 12 15.2607 304.889 1 2 7 12 370.726 466.289 1 2 7 13 535.932 372.660 1 -2 -8 12-177.717 518.421 1 -2 -8 12 46.0045 657.252 1 2 8 -12 407.486 729.711 1 2 8 -12-244.972 510.542 1 -2 -8 11 110.605 518.255 1 -2 -8 11-661.416 705.920 1 2 8 -11 602.811 587.038 1 2 8 -11 488.186 533.360 1 -2 -8 10 253.542 467.765 1 2 8 -10 723.938 455.060 1 2 8 -10-545.027 545.498 1 -2 -8 10 122.371 587.025 1 -2 -8 9 942.683 512.222 1 2 8 -9 840.096 433.715 1 2 8 -9-220.790 419.243 1 -2 -8 8 184.389 364.012 1 -2 -8 8-11.0673 404.225 1 2 8 -8-125.959 386.908 1 -2 -8 8 390.469 504.860 1 -2 -8 7 1718.22 456.026 1 -2 -8 7 529.716 437.279 1 2 8 -7 726.517 457.111 1 -2 -8 6 2010.75 410.352 1 2 8 -6 4192.86 489.260 1 2 8 -6 2300.18 576.128 1 -2 -8 6 3562.84 630.872 1 -2 -8 6 2217.36 590.957 1 -2 -8 5-11.7598 322.512 1 -2 -8 5-164.125 388.925 1 2 8 -5 155.612 279.594 1 -2 -8 5 73.0039 329.058 1 2 8 -5 332.443 358.624 1 -2 -8 4 1784.22 483.198 1 2 8 -4 3472.79 575.834 1 2 8 -4 2292.17 366.077 1 -2 -8 4 3073.72 471.570 1 -2 -8 4 4012.25 690.627 1 -2 -8 3 4484.09 561.394 1 2 8 -3 4835.44 411.950 1 2 8 -3 4900.85 589.382 1 -2 -8 3 3544.98 532.198 1 -2 -8 2 644.216 308.435 1 -2 -8 2 1051.98 366.563 1 2 8 -2 833.551 244.135 1 -2 -8 2 692.999 288.591 1 -2 -8 2 643.591 324.212 1 -2 -8 1 74.9184 245.138 1 -2 -8 1 646.437 336.209 1 2 8 -1-152.907 211.691 1 -2 -8 1 462.499 275.866 1 -2 -8 1 307.636 243.567 1 -2 -8 0 286.387 194.058 1 -2 -8 0 1192.52 376.728 1 2 8 0 148.431 201.269 1 -2 -8 0 650.087 347.029 1 -2 -8 0 586.046 249.920 1 2 8 1 1971.10 345.433 1 -2 -8 -1 2264.71 332.713 1 -2 -8 -2 3275.55 497.484 1 2 8 2 3031.03 361.637 1 -2 -8 -2 1828.50 296.033 1 -2 -8 -2 2463.41 411.614 1 2 8 2 2557.27 278.267 1 -2 -8 -3 200.000 331.565 1 2 8 3-7.63499 213.200 1 -2 -8 -3 392.643 258.272 1 2 8 3-8.45737 225.475 1 -2 -8 -3 116.539 181.651 1 2 8 4 3387.13 457.114 1 -2 -8 -4 2500.23 533.316 1 -2 -8 -4 2167.45 400.712 1 -2 -8 -5 3759.62 533.578 1 2 8 5 7887.71 599.301 1 2 8 5 8478.85 618.107 1 -2 -8 -5 3450.27 596.468 1 -2 -8 -6 3838.84 651.847 1 2 8 6 16.1031 289.565 1 2 8 6 1330.03 329.394 1 -2 -8 -6 5163.24 710.523 1 -2 -8 -7 405.590 446.729 1 2 8 7 67.6366 247.790 1 2 8 7 474.781 431.402 1 -2 -8 -7 322.425 323.391 1 2 8 8 1233.20 331.126 1 2 8 8 846.759 428.809 1 -2 -8 -8-97.9804 427.914 1 -2 -8 -8 189.400 283.986 1 2 8 9 166.400 271.505 1 -2 -8 -9 604.818 505.323 1 2 8 9 80.8765 392.323 1 2 8 10 441.008 327.525 1 2 8 10-434.627 436.483 1 -2 -8 -10 1098.88 560.204 1 2 8 11 282.529 337.557 1 2 8 11 350.197 486.742 1 -2 -8 -11 607.970 560.297 1 2 8 12 698.290 406.365 1 2 8 12 18.9458 470.355 1 -2 -9 12 465.387 730.422 1 2 9 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1 -2 -9 2 1017.20 350.482 1 -2 -9 2 1330.98 377.657 1 2 9 -2 1105.43 276.148 1 -2 -9 2 1596.28 481.445 1 -2 -9 1 3421.05 537.877 1 -2 -9 1 2881.16 403.023 1 2 9 -1 4086.26 387.112 1 -2 -9 0 774.366 270.724 1 2 9 0 549.773 242.967 1 -2 -9 -1 2421.37 479.718 1 -2 -9 -1 2385.77 366.552 1 -2 -9 -1 1995.64 415.723 1 -2 -9 -2 1303.24 444.690 1 2 9 2 138.305 239.068 1 -2 -9 -2 981.779 350.463 1 -2 -9 -2 691.503 259.765 1 -2 -9 -3 324.986 378.980 1 2 9 3-164.255 247.995 1 -2 -9 -3 29.5530 253.487 1 -2 -9 -4 5998.76 737.823 1 -2 -9 -4 4660.61 597.472 1 2 9 4 5540.17 569.102 1 2 9 5 5720.39 550.782 1 -2 -9 -5 5919.75 778.958 1 -2 -9 -6 420.884 430.382 1 2 9 6 141.409 255.152 1 2 9 6 107.244 305.757 1 -2 -9 -6 233.687 299.672 1 -2 -9 -7-12.7102 409.106 1 2 9 7-138.589 277.515 1 -2 -9 -7 133.039 291.651 1 2 9 7-298.425 352.306 1 -2 -9 -8 176.357 465.983 1 2 9 8 98.1447 280.031 1 2 9 8-592.666 383.536 1 2 9 9 324.333 309.498 1 2 9 9 543.817 434.237 1 -2 -9 -9-479.780 499.625 1 -2 -9 -10-606.881 561.159 1 2 9 10-517.722 355.288 1 2 9 10-521.194 418.109 1 -2 -9 -11-412.157 545.873 1 2 9 11 192.846 336.476 1 2 9 11 287.632 461.006 1 -2 -10 11-906.572 724.850 1 2 10 -11-719.529 582.271 1 -2 -10 10 1046.08 589.141 1 2 10 -10 380.319 508.932 1 2 10 -10 570.309 569.437 1 -2 -10 10-151.048 614.056 1 -2 -10 9 705.149 531.901 1 -2 -10 9 549.250 586.703 1 2 10 -9 128.039 425.860 1 2 10 -9 388.017 455.475 1 -2 -10 8 449.602 561.866 1 -2 -10 8 67.9335 488.912 1 2 10 -8-134.346 469.207 1 -2 -10 8 737.926 480.036 1 2 10 -7 1047.35 489.517 1 -2 -10 7 1647.08 550.469 1 -2 -10 7 2127.75 633.754 1 -2 -10 7 1507.42 553.622 1 -2 -10 6 1154.01 480.628 1 -2 -10 6 1267.49 531.170 1 2 10 -6 91.0408 451.899 1 -2 -10 6 648.979 530.339 1 -2 -10 5 7392.71 761.424 1 -2 -10 5 5185.65 748.224 1 2 10 -5 7564.77 784.681 1 -2 -10 5 4389.81 613.793 1 -2 -10 4 2091.54 510.528 1 2 10 -4 2310.96 374.606 1 -2 -10 4 1644.90 470.779 1 2 10 -4 1828.26 495.714 1 -2 -10 4 1090.08 398.502 1 -2 -10 3 321.876 314.338 1 2 10 -3 631.344 308.465 1 2 10 -3-112.904 380.582 1 -2 -10 3 412.987 346.231 1 -2 -10 2 1960.69 418.725 1 2 10 -2 2555.69 363.257 1 -2 -10 2 3119.72 641.469 1 -2 -10 1 1023.72 331.378 1 2 10 -1 1948.70 324.620 1 -2 -10 1 1362.34 456.995 1 -2 -10 1 1163.29 409.952 1 -2 -10 0 4822.58 633.147 1 -2 -10 0 4746.87 491.442 1 -2 -10 0 3646.34 528.600 1 -2 -10 -1 414.047 261.589 1 -2 -10 -1 1355.97 418.234 1 -2 -10 -1 1243.20 391.354 1 2 10 1 181.982 266.716 1 -2 -10 -2 4257.85 612.868 1 -2 -10 -2 2373.55 490.835 1 -2 -10 -3 83.3140 339.282 1 2 10 3-254.520 266.175 1 -2 -10 -3 86.2549 298.033 1 -2 -10 -4 1448.66 474.837 1 -2 -10 -4 743.929 404.313 1 2 10 4 800.283 333.621 1 2 10 5 1992.25 427.187 1 -2 -10 -5 1568.42 464.096 1 -2 -10 -5 2604.65 610.595 1 -2 -10 -6 683.498 479.638 1 -2 -10 -6 1082.69 406.758 1 2 10 6 1028.10 332.988 1 -2 -10 -7 753.524 515.492 1 2 10 7 808.277 366.773 1 2 10 8 363.002 363.285 1 -2 -10 -8 3350.57 845.601 1 -2 -10 -9 518.281 534.105 1 2 10 9 149.632 317.939 1 2 10 10 864.052 376.504 1 -2 -10 -10 845.012 643.646 1 -2 -11 10-651.227 683.405 1 -2 -11 9-56.4430 478.648 1 -2 -11 9 899.323 645.838 1 2 11 -9-193.014 453.052 1 2 11 -9-58.8810 482.014 1 -2 -11 8 315.490 486.899 1 2 11 -8-437.372 505.444 1 -2 -11 8 175.806 556.895 1 -2 -11 7 213.697 506.767 1 -2 -11 7-53.9106 455.306 1 2 11 -7 219.112 513.595 1 -2 -11 7 18.6453 456.777 1 -2 -11 6 9152.38 952.558 1 2 11 -6 9303.37 1075.20 1 -2 -11 6 7836.69 962.360 1 -2 -11 5 11064.4 1061.85 1 -2 -11 5 10693.0 941.695 1 -2 -11 4 795.293 423.734 1 2 11 -4 2234.09 565.086 1 -2 -11 4 1608.81 518.917 1 -2 -11 3 301.753 373.416 1 -2 -11 3-196.408 376.053 1 2 11 -3 341.644 455.540 1 2 11 -3 760.465 329.036 1 -2 -11 2 964.648 428.554 1 -2 -11 2 258.807 372.512 1 2 11 -2 630.457 319.174 1 -2 -11 1 1015.64 392.253 1 -2 -11 1 2162.22 537.060 1 2 11 -1 549.149 267.629 1 -2 -11 1 1828.48 570.565 1 -2 -11 0 283.965 318.627 1 2 11 0 1206.64 367.553 1 -2 -11 0 533.063 351.138 1 -2 -11 0 621.761 442.053 1 2 11 1 292.997 260.933 1 -2 -11 -1 377.584 361.697 1 -2 -11 -1 697.926 316.880 1 2 11 2 19.2069 282.243 1 -2 -11 -2 758.198 359.848 1 2 11 3 1087.74 320.689 1 -2 -11 -3 868.055 435.588 1 -2 -11 -3 936.266 416.871 1 -2 -11 -4 2688.85 570.344 1 -2 -11 -4 4156.68 692.004 1 2 11 4 3507.03 491.460 1 -2 -11 -5 455.936 458.658 1 2 11 5 439.414 327.122 1 -2 -11 -5 314.260 334.263 1 -2 -11 -6 1194.38 508.590 1 2 11 6 199.054 331.131 1 -2 -11 -7 237.944 500.409 1 2 11 7 603.596 366.006 1 -2 -11 -8 821.102 552.654 1 2 11 8 250.474 346.286 1 -2 -11 -9 901.199 582.359 1 2 11 9 54.9692 347.696 1 -2 -12 8 275.088 527.125 1 2 12 -8 1092.90 635.674 1 -2 -12 7 1175.58 549.396 1 2 12 -7 909.277 584.520 1 -2 -12 7 613.280 522.398 1 -2 -12 6-630.715 545.562 1 2 12 -6 167.970 517.371 1 -2 -12 6-159.788 481.828 1 -2 -12 5 2151.10 558.307 1 2 12 -5 3431.12 678.319 1 -2 -12 5 2262.57 629.477 1 -2 -12 4 358.677 428.979 1 -2 -12 4-109.092 460.669 1 2 12 -4 300.395 462.861 1 -2 -12 3 148.471 413.770 1 -2 -12 3 630.029 423.448 1 2 12 -3 1049.81 502.887 1 2 12 -2 407.204 273.790 1 -2 -12 2 515.647 407.003 1 -2 -12 2-136.999 379.220 1 2 12 -1 676.744 317.893 1 -2 -12 1 772.756 469.309 1 -2 -12 1-215.694 401.047 1 -2 -12 1 330.214 396.535 1 -2 -12 0 1313.78 515.753 1 2 12 0 781.194 295.849 1 -2 -12 0 600.205 423.082 1 -2 -12 -1 931.829 459.952 1 2 12 1 314.834 321.135 1 -2 -12 -1 734.898 416.063 1 2 12 2 809.838 367.451 1 -2 -12 -2 343.129 405.455 1 -2 -12 -2 425.708 365.077 1 2 12 3 4850.85 571.513 1 -2 -12 -3 5806.81 726.281 1 -2 -12 -4 10057.3 1141.68 1 -2 -12 -4 14855.6 1100.35 1 -2 -12 -5 560.135 430.018 1 2 12 5 586.464 365.858 1 -2 -12 -6 749.267 478.484 1 2 12 6 724.546 370.605 1 -2 -12 -7-481.120 513.739 1 2 12 7 100.573 354.002 1 -2 -12 -8 813.084 591.026 1 2 12 8 157.699 360.300 1 -2 -13 7 338.081 496.719 1 2 13 -7 617.662 589.799 1 -2 -13 7 234.792 468.647 1 2 13 -6 896.794 627.551 1 -2 -13 6 492.566 485.559 1 -2 -13 6 249.455 564.519 1 -2 -13 5 603.231 540.691 1 -2 -13 5 889.166 500.576 1 2 13 -5 2006.94 676.200 1 -2 -13 4 718.436 462.753 1 2 13 -4 866.248 533.549 1 -2 -13 4 422.530 475.785 1 -2 -13 3 407.332 419.161 1 -2 -13 3 159.253 547.983 1 2 13 -3 876.940 548.335 1 2 13 -2 7408.62 922.587 1 -2 -13 2 4684.26 757.831 1 2 13 -1 253.945 272.961 1 -2 -13 1-137.387 451.782 1 -2 -13 0 3062.99 626.172 1 2 13 0 2065.04 419.390 1 -2 -13 0 1987.27 577.861 1 -2 -13 -1 425.377 424.954 1 2 13 1-110.046 340.872 1 -2 -13 -1 196.906 463.799 1 -2 -13 -2 2780.72 623.978 1 2 13 2 3164.05 523.022 1 -2 -13 -2 1982.69 520.993 1 -2 -13 -3 965.009 486.829 1 2 13 3 267.453 336.141 1 2 13 4 1376.82 410.226 1 -2 -13 -4 2561.01 613.914 1 -2 -13 -5 813.156 521.429 1 2 13 5 1573.39 437.503 1 -2 -13 -6-44.9647 446.063 1 2 13 6 75.8471 375.822 1 -2 -13 -7 215.427 469.570 1 -2 -14 6 400.152 491.638 1 -2 -14 5 216.270 516.325 1 2 14 -5-266.367 581.404 1 -2 -14 5-36.3968 511.489 1 -2 -14 4 1440.79 592.934 1 2 14 -4 2186.35 666.313 1 -2 -14 4 1439.04 565.710 1 2 14 -3 9.67512 467.529 1 -2 -14 3-145.153 517.627 1 2 14 -2 621.568 533.793 1 -2 -14 2-481.702 534.355 1 -2 -14 1 82.3671 454.768 1 2 14 0 22.7447 305.495 1 -2 -14 0-167.131 414.996 1 -2 -14 0 300.626 438.819 1 -2 -14 -1 1304.62 526.956 1 2 14 1 1853.42 449.822 1 -2 -14 -1 991.339 501.779 1 -2 -14 -2 1211.66 559.723 1 2 14 2 1471.34 432.217 1 -2 -14 -2 386.836 423.582 1 -2 -14 -3 3143.33 694.328 1 2 14 3 780.151 401.176 1 2 14 4 744.710 410.979 1 -2 -14 -4 1029.19 515.521 1 -2 -14 -5 2400.42 648.967 1 -2 -15 2 1450.17 606.588 1 2 15 -1 181.360 648.182 1 -2 -15 1 397.525 468.553 1 -2 -15 0 1935.96 582.304 1 -2 -15 -1 5796.29 899.023 1 2 15 2 718.893 429.458 1 2 15 3 457.910 393.540 1 -3 14 6 67.0153 337.619 1 -3 14 5 59.0922 320.771 1 -3 14 -4-296.266 365.809 1 3 -13 -7 156.982 898.603 1 -3 13 -2 86.3867 344.805 1 -3 13 -3-560.562 439.045 1 -3 13 -3-131.739 414.090 1 3 -13 4 626.869 527.792 1 -3 13 -4 67.9931 427.562 1 -3 13 -4-143.872 477.943 1 3 -13 5 615.848 570.430 1 -3 13 -5-443.536 472.165 1 -3 13 -5-140.926 409.743 1 3 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797.741 1 3 -7 7 12747.0 1169.91 1 -3 7 -8 1163.68 528.835 1 3 -7 8 202.402 505.692 1 3 -7 8 230.148 484.605 1 3 -7 9 3316.04 786.252 1 -3 7 -9 1018.18 578.479 1 3 -7 9 3782.82 756.044 1 -3 7 -9 576.455 564.384 1 -3 7 -10 964.301 459.863 1 3 -7 10 2444.60 743.796 1 3 -7 10 1423.16 597.380 1 -3 7 -10 532.739 541.559 1 -3 7 -10 380.829 604.579 1 3 -7 11 222.767 623.519 1 -3 7 -11 586.966 455.164 1 -3 7 -11 133.623 502.883 1 3 -7 11 460.391 572.202 1 -3 7 -11-13.9248 631.432 1 -3 7 -12 712.370 690.987 1 3 -7 12 818.549 610.765 1 -3 6 13-759.722 488.880 1 3 -6 -13-805.872 1146.47 1 -3 6 12 369.429 405.954 1 3 -6 -12 285.841 1034.35 1 -3 6 11 220.368 463.039 1 -3 6 11 286.385 382.769 1 3 -6 -11-372.247 446.548 1 3 -6 -11-432.209 1077.56 1 3 -6 -10 49.8942 410.173 1 3 -6 -10-1023.98 1021.71 1 -3 6 10 11.6489 382.526 1 -3 6 10 656.373 443.955 1 3 -6 -9 557.048 405.606 1 -3 6 9 106.872 329.838 1 3 -6 -9 112.072 885.231 1 -3 6 9 177.251 377.289 1 -3 6 8 2702.25 479.932 1 3 -6 -8 1866.72 457.589 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481.556 281.687 1 3 -6 1 199.336 433.239 1 3 -6 1 660.367 355.463 1 -3 6 -1 310.189 243.513 1 -3 6 -1 457.436 189.868 1 3 -6 2 122.156 329.047 1 3 -6 2 8.02384 342.755 1 -3 6 -2 260.953 256.995 1 -3 6 -2 309.044 284.978 1 3 -6 2 258.714 362.868 1 -3 6 -2 449.433 244.010 1 3 -6 3 356.522 355.759 1 -3 6 -3 135.036 262.103 1 3 -6 3 308.349 355.152 1 3 -6 3-0.29089 241.312 1 -3 6 -3 781.777 357.530 1 -3 6 -3 149.030 254.900 1 -3 6 -4 5803.96 538.901 1 3 -6 4 6505.58 711.092 1 -3 6 -4 5101.89 568.295 1 -3 6 -4 4707.65 567.359 1 3 -6 5 16154.1 1038.59 1 3 -6 5 15973.9 1016.64 1 -3 6 -5 12693.1 1002.39 1 -3 6 -5 11458.0 886.619 1 3 -6 6 22341.6 1327.65 1 3 -6 6 25360.3 1268.99 1 -3 6 -6 16475.0 1154.79 1 -3 6 -6 19993.0 1294.72 1 3 -6 7 1052.61 537.971 1 -3 6 -7 1677.67 569.217 1 -3 6 -7 936.112 535.929 1 3 -6 7 1314.85 454.858 1 3 -6 8-91.2957 496.649 1 3 -6 8 225.994 448.475 1 -3 6 -8 32.3318 524.333 1 -3 6 -8-565.541 436.881 1 -3 6 -9 588.975 459.894 1 3 -6 9-77.7350 539.597 1 -3 6 -9 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13976.1 532.948 1 -3 0 2 16434.4 575.353 1 3 0 -2 17697.9 517.315 1 3 0 -2 16170.5 780.242 1 -3 0 2 15051.6 596.097 1 -3 0 1 4859.14 292.105 1 3 0 -1 4968.71 465.992 1 3 0 -1 5042.83 417.584 1 -3 0 1 4894.40 360.286 1 -3 0 1 4642.97 344.728 1 -3 0 1 4773.12 360.960 1 3 0 0 3503.80 328.485 1 -3 0 0 3740.89 353.945 1 -3 0 0 3823.81 346.064 1 3 0 0 4181.48 443.305 1 -3 0 0 4176.32 308.337 1 -3 0 0 4229.61 379.967 1 3 0 1 4664.81 403.435 1 3 0 1 4325.39 311.893 1 -3 0 -1 4198.04 363.208 1 3 0 1 4632.56 453.552 1 -3 0 -1 4627.52 388.549 1 -3 0 -1 4622.94 406.752 1 3 0 2 11920.8 465.203 1 3 0 2 11613.4 663.506 1 -3 0 -2 10624.9 601.325 1 -3 0 -2 11006.4 525.855 1 3 0 2 11363.7 604.297 1 -3 0 -2 12059.8 652.992 1 3 0 3 114388. 1827.29 1 3 0 3 111546. 1896.31 1 -3 0 -3 114364. 1681.05 1 3 0 3 115080. 1304.76 1 -3 0 -3 115120. 2072.03 1 3 0 4 62981.9 1506.86 1 3 0 4 60687.0 1453.09 1 -3 0 -4 60395.8 1643.71 1 3 0 4 60408.9 959.288 1 -3 0 -4 64175.7 1293.74 1 -3 0 -4 61702.6 1559.74 1 3 0 5 28083.6 1061.57 1 3 0 5 28328.1 1119.66 1 -3 0 -5 29966.8 943.449 1 -3 0 -5 29544.9 1300.99 1 3 0 5 32672.4 731.566 1 -3 0 -5 27933.9 1111.84 1 3 0 6 1237.79 390.432 1 -3 0 -6 889.144 360.226 1 -3 0 -6 684.069 258.378 1 3 0 6 1074.59 194.870 1 -3 0 -6 104.267 376.712 1 3 0 6 505.809 338.855 1 3 0 7 23.1188 355.923 1 3 0 7 172.280 167.292 1 -3 0 -7 235.781 257.326 1 3 0 7 492.886 361.317 1 -3 0 -7 66.6974 293.698 1 -3 0 -7 53.8014 411.206 1 3 0 8 619.272 431.032 1 3 0 8 1162.88 236.508 1 -3 0 -8 578.178 287.540 1 -3 0 -8 352.277 353.176 1 3 0 8 376.252 355.898 1 -3 0 -8 23.2650 452.335 1 3 0 9 3543.25 646.552 1 -3 0 -9 3757.22 477.359 1 -3 0 -9 3218.77 602.139 1 -3 0 -9 3036.60 722.770 1 3 0 9 3489.08 550.213 1 3 0 10 4196.20 742.322 1 -3 0 -10 5164.12 567.528 1 -3 0 -10 5062.19 705.586 1 -3 0 -10 4312.06 847.873 1 3 0 10 4400.85 659.005 1 -3 0 -11 4797.24 943.255 1 -3 0 -11 4683.26 729.897 1 -3 0 -11 4860.01 600.479 1 3 0 11 5187.48 810.470 1 3 0 11 4392.75 673.367 1 3 0 12 263.606 579.456 1 -3 0 -12-51.0304 448.392 1 3 0 12-139.839 446.071 1 -3 0 -12 599.937 658.962 1 3 0 13 4364.51 857.545 1 -3 0 -13 4089.60 759.525 1 -3 0 -13 3708.47 992.889 1 3 0 13 5407.18 836.937 1 3 0 14-231.562 635.412 1 -3 0 -14 529.161 493.627 1 -3 -1 15 1815.91 602.198 1 3 1 -15 1355.40 820.636 1 -3 -1 14 150.117 661.027 1 -3 -1 14 9.96210 434.390 1 3 1 -14-325.857 667.862 1 -3 -1 13 1272.46 713.267 1 -3 -1 13 364.331 478.436 1 3 1 -13 715.728 666.790 1 -3 -1 12 156.424 450.364 1 -3 -1 12 221.780 411.739 1 3 1 -12 1258.38 859.293 1 3 1 -12-359.552 555.467 1 -3 -1 12-1182.29 556.442 1 -3 -1 11 2073.04 428.941 1 3 1 -11 3040.95 526.978 1 -3 -1 11 2280.61 493.950 1 3 1 -11 3990.99 945.884 1 3 1 -11 4523.13 832.345 1 -3 -1 11 2204.16 607.000 1 -3 -1 10 2952.34 458.234 1 3 1 -10 3584.96 828.070 1 3 1 -10 3189.60 494.888 1 3 1 -10 4718.85 776.564 1 -3 -1 10 3663.98 513.027 1 -3 -1 10 3105.41 573.906 1 3 1 -9 19544.6 1413.83 1 -3 -1 9 9020.21 616.288 1 3 1 -9 15727.1 1070.80 1 3 1 -9 11498.8 728.919 1 -3 -1 9 7197.76 724.585 1 -3 -1 9 8656.48 654.102 1 3 1 -8 4918.65 750.786 1 -3 -1 8 4951.94 455.045 1 3 1 -8 3486.56 595.758 1 -3 -1 8 5531.59 528.294 1 3 1 -8 3414.69 413.110 1 -3 -1 8 3160.37 534.606 1 -3 -1 7 53824.7 1231.79 1 -3 -1 7 56518.9 1340.58 1 -3 -1 7 56457.4 1388.76 1 -3 -1 7 54611.9 1541.81 1 -3 -1 6 72634.3 1320.06 1 3 1 -6 76040.7 2132.87 1 3 1 -6 67881.3 1559.94 1 -3 -1 6 78427.3 1442.75 1 -3 -1 6 72455.5 1578.61 1 3 1 -5 4777.43 539.282 1 -3 -1 5 4495.84 375.781 1 3 1 -5 3355.54 387.059 1 -3 -1 5 5410.09 438.204 1 -3 -1 5 4051.16 347.119 1 -3 -1 5 3838.18 404.852 1 -3 -1 4 519.188 243.092 1 -3 -1 4 874.062 238.383 1 3 1 -4 773.828 365.892 1 -3 -1 4 700.783 221.152 1 3 1 -4 437.066 239.585 1 -3 -1 4 981.165 253.606 1 3 1 -3 2606.95 417.066 1 -3 -1 3 2519.58 409.952 1 -3 -1 3 1979.44 285.226 1 3 1 -3 2158.85 278.807 1 -3 -1 3 1841.41 270.200 1 -3 -1 3 1119.85 297.485 1 3 1 -2 10929.4 591.421 1 -3 -1 2 9718.36 439.978 1 -3 -1 2 10395.2 496.410 1 -3 -1 2 10062.9 499.174 1 -3 -1 1 41676.8 873.686 1 3 1 -1 41533.1 946.901 1 -3 -1 1 42961.7 910.235 1 -3 -1 1 44539.0 913.781 1 -3 -1 1 43181.1 968.100 1 3 1 0 70385.2 1141.24 1 -3 -1 0 61227.3 1125.39 1 3 1 0 68046.4 1319.53 1 -3 -1 0 69612.4 1308.60 1 -3 -1 0 65093.2 1070.38 1 -3 -1 0 62201.1 1165.83 1 3 1 1 40739.1 834.186 1 -3 -1 -1 40782.4 966.049 1 3 1 1 43116.9 1045.99 1 -3 -1 -1 37512.9 1077.69 1 -3 -1 -1 36181.1 825.826 1 -3 -1 -1 36278.6 960.403 1 3 1 2 146542. 1914.51 1 -3 -1 -2 144181. 1756.67 1 3 1 2 133360. 1436.34 1 -3 -1 -2 130270. 1993.07 1 3 1 2 140413. 1747.20 1 3 1 3 17044.3 838.497 1 3 1 3 23544.4 666.185 1 -3 -1 -3 23847.8 828.313 1 -3 -1 -3 26007.8 1006.67 1 3 1 3 20904.1 806.922 1 -3 -1 -3 31988.3 1210.77 1 3 1 4 956.199 308.712 1 3 1 4 1155.94 332.684 1 3 1 4 1473.26 213.227 1 -3 -1 -4 1445.61 263.480 1 -3 -1 -4 1565.65 352.908 1 -3 -1 -4 1510.68 406.642 1 3 1 5 2574.74 413.088 1 -3 -1 -5 2360.96 320.630 1 3 1 5 2576.88 270.156 1 -3 -1 -5 2117.04 459.589 1 -3 -1 -5 1994.71 378.066 1 3 1 5 2679.02 395.142 1 3 1 6 10474.1 721.279 1 -3 -1 -6 14700.8 699.825 1 3 1 6 15188.6 579.035 1 -3 -1 -6 15909.9 1061.14 1 3 1 6 9930.91 677.790 1 -3 -1 -6 15831.0 911.994 1 -3 -1 -7 3299.11 612.212 1 3 1 7 5717.82 632.517 1 3 1 7 4817.23 370.970 1 3 1 7 5751.91 596.171 1 -3 -1 -7 2683.19 510.274 1 -3 -1 -7 3470.06 454.403 1 3 1 8 12921.7 871.584 1 3 1 8 19901.9 704.232 1 -3 -1 -8 20777.8 898.239 1 -3 -1 -8 21282.8 1142.24 1 -3 -1 -8 20712.7 1353.92 1 3 1 8 14008.0 926.422 1 3 1 9 14167.9 1029.67 1 3 1 9 22334.8 777.158 1 -3 -1 -9 25121.6 987.099 1 -3 -1 -9 26316.2 1361.20 1 -3 -1 -9 23044.6 1519.62 1 3 1 9 14531.5 1004.42 1 -3 -1 -10 2957.45 425.031 1 3 1 10 1609.43 596.298 1 3 1 10 1856.41 502.181 1 -3 -1 -10 3259.24 596.551 1 -3 -1 -10 2302.16 696.276 1 3 1 11 2357.94 675.144 1 -3 -1 -11 1952.77 543.358 1 3 1 11 3709.93 672.571 1 -3 -1 -11 1419.95 669.252 1 3 1 12 963.726 588.283 1 3 1 12 552.411 470.440 1 -3 -1 -12 785.664 452.051 1 -3 -1 -12-561.805 575.096 1 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1 -3 -2 8 5015.01 590.078 1 3 2 -7 3861.78 614.624 1 -3 -2 7 1747.26 312.017 1 3 2 -7 2326.37 423.760 1 -3 -2 7 1635.06 332.079 1 -3 -2 7 3108.68 457.227 1 -3 -2 7 1521.89 416.414 1 3 2 -6 13776.8 723.213 1 3 2 -6 15825.8 836.154 1 -3 -2 6 9701.69 528.789 1 -3 -2 6 9749.96 646.555 1 -3 -2 6 12421.1 719.286 1 -3 -2 6 7885.08 645.705 1 -3 -2 5 11048.7 527.601 1 -3 -2 5 12163.8 680.668 1 -3 -2 5 13686.3 655.711 1 3 2 -5 11329.8 801.031 1 3 2 -5 8931.77 616.750 1 -3 -2 5 14756.5 741.544 1 -3 -2 4 8493.19 429.184 1 3 2 -4 10492.9 680.308 1 -3 -2 4 9764.62 547.334 1 -3 -2 4 9447.47 529.061 1 3 2 -4 8507.59 581.016 1 -3 -2 4 9011.73 540.799 1 -3 -2 3 911.379 251.597 1 -3 -2 3 1211.55 227.059 1 3 2 -3 1798.12 351.944 1 -3 -2 3 1167.53 276.390 1 3 2 -3 1684.69 300.463 1 -3 -2 3 1893.51 318.076 1 -3 -2 2 4164.99 381.078 1 -3 -2 2 4117.92 365.199 1 3 2 -2 4104.72 371.060 1 -3 -2 2 5132.45 438.327 1 -3 -2 2 4480.73 375.763 1 3 2 -1 119895. 1583.31 1 3 2 -1 120169. 1547.98 1 -3 -2 1 118187. 1464.18 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1276.25 404.879 1 -7 8 2 2031.48 542.098 1 7 -8 -1 804.547 759.435 1 -7 8 1 855.239 431.807 1 -7 8 1 489.238 487.735 1 7 -8 0 2160.95 807.180 1 -7 8 0 1355.02 441.451 1 -7 8 0 1132.47 526.538 1 -7 8 -1 424.381 426.608 1 -7 8 -1 704.724 495.514 1 7 -8 1-261.411 630.438 1 -7 8 -2 466.499 447.989 1 7 -8 2 1053.72 672.808 1 -7 8 -2 899.383 497.489 1 7 -8 3 155.452 604.045 1 -7 8 -3-75.6147 387.900 1 -7 8 -3 11.7174 367.992 1 -7 8 -3-302.933 415.697 1 7 -8 4 2514.14 736.481 1 -7 8 -4 2234.80 521.636 1 -7 8 -4 1540.97 552.959 1 7 -8 5 1808.83 683.037 1 -7 8 -5 1103.37 479.714 1 -7 8 -5 110.568 418.518 1 7 -8 5 1987.37 787.482 1 -7 8 -6 1947.43 601.310 1 -7 8 -6 1371.14 687.956 1 7 -8 6 1146.67 761.634 1 -7 7 10 625.914 510.067 1 -7 7 9 816.548 580.611 1 7 -7 -9-240.719 1106.51 1 -7 7 9-596.873 466.805 1 -7 7 8 610.961 539.816 1 7 -7 -8-372.911 976.479 1 -7 7 8-757.802 508.052 1 -7 7 7 1490.10 517.249 1 7 -7 -7 1365.20 1017.74 1 -7 7 7 343.086 427.701 1 -7 7 6 584.335 449.725 1 -7 7 6 1214.64 506.287 1 -7 7 5 2283.01 573.389 1 7 -7 -5 1034.87 811.102 1 -7 7 5 2960.93 603.622 1 -7 7 4 2273.23 502.645 1 -7 7 4 1617.11 512.677 1 7 -7 -4 397.808 730.565 1 -7 7 4 650.678 412.471 1 7 -7 -3 1276.69 736.815 1 -7 7 3 1157.47 403.455 1 -7 7 3 753.814 428.359 1 7 -7 -2 27852.5 1712.78 1 -7 7 2 24107.7 1190.56 1 -7 7 2 24503.7 1261.36 1 -7 7 1 5882.56 690.659 1 7 -7 -1 4981.85 901.927 1 7 -7 -1 7005.44 1002.96 1 -7 7 1 6513.26 727.044 1 -7 7 0 6792.45 736.440 1 -7 7 0 6839.59 789.521 1 7 -7 1 2892.73 891.280 1 -7 7 -1 2328.90 511.636 1 -7 7 -1 1407.11 520.072 1 7 -7 2 610.896 676.431 1 -7 7 -2 410.423 387.448 1 -7 7 -2-69.5773 378.881 1 -7 7 -2 298.277 388.759 1 7 -7 3 6371.22 1242.66 1 -7 7 -3 6159.56 773.225 1 -7 7 -3 5324.58 728.107 1 -7 7 -3 6008.83 742.333 1 -7 7 -4 191.159 377.763 1 -7 7 -4 206.706 398.538 1 7 -7 4 487.393 591.514 1 7 -7 5-736.204 585.846 1 -7 7 -5 512.022 445.455 1 -7 7 -5 258.841 434.785 1 7 -7 5 1084.59 675.694 1 7 -7 6 223.805 538.108 1 -7 7 -6 191.049 414.231 1 7 -7 6 1070.19 724.525 1 -7 7 -6 1203.54 554.063 1 7 -7 7 851.928 737.873 1 -7 7 -7 590.531 568.893 1 -7 6 11 2364.80 663.895 1 -7 6 10 1117.08 573.283 1 7 -6 -10 794.819 1181.55 1 -7 6 10 902.130 498.381 1 -7 6 9-332.794 510.590 1 7 -6 -9 247.059 994.080 1 -7 6 9 712.908 491.461 1 -7 6 8 193.813 485.970 1 7 -6 -8 712.357 944.229 1 -7 6 8 685.699 476.976 1 -7 6 7 1488.68 509.918 1 7 -6 -7 168.600 816.327 1 -7 6 7 610.510 435.399 1 -7 6 6 4339.03 685.245 1 -7 6 6 4466.22 668.485 1 -7 6 5 3019.50 558.358 1 -7 6 5 2893.55 488.507 1 7 -6 -5 2981.49 989.835 1 -7 6 5 3667.89 621.843 1 -7 6 4 2465.70 560.536 1 7 -6 -4 981.628 844.409 1 -7 6 4 2591.19 530.019 1 -7 6 4 2154.86 489.492 1 -7 6 3 3180.23 525.339 1 7 -6 -3 863.304 860.216 1 7 -6 -3 4530.28 834.050 1 -7 6 3 2245.76 579.483 1 -7 6 2 6193.64 640.651 1 -7 6 2 6673.61 708.792 1 -7 6 1 17553.2 1025.19 1 7 -6 -1 20445.2 1493.84 1 -7 6 1 17266.5 1082.60 1 -7 6 0 1803.33 499.173 1 7 -6 0 827.229 595.128 1 7 -6 0 2726.85 786.087 1 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623.602 420.965 1 -7 5 -4 7067.31 799.137 1 -7 5 -4 6711.62 784.375 1 7 -5 4 5875.19 1042.51 1 7 -5 5 5796.25 900.528 1 -7 5 -5 5688.40 710.641 1 -7 5 -5 3698.95 684.309 1 7 -5 5 4315.71 972.538 1 7 -5 6 513.093 542.593 1 -7 5 -6 211.967 375.960 1 7 -5 6-410.085 585.849 1 -7 5 -6 405.010 419.703 1 7 -5 7 896.577 602.776 1 -7 5 -7 540.809 456.576 1 7 -5 7-176.666 597.306 1 -7 5 -7 747.066 527.162 1 7 -5 8 2723.80 745.081 1 7 -5 8 2149.63 858.740 1 -7 5 -8 1692.90 554.193 1 -7 5 -8 1822.55 673.458 1 -7 4 11 2526.10 609.037 1 7 -4 -11 2887.98 1215.39 1 -7 4 11 2467.78 575.360 1 -7 4 10 1457.74 601.129 1 -7 4 10 242.066 440.855 1 -7 4 9 650.030 544.805 1 7 -4 -9-212.050 910.251 1 -7 4 9 1072.71 460.964 1 -7 4 8-147.380 456.901 1 7 -4 -8 469.353 876.068 1 -7 4 8 156.834 410.719 1 -7 4 7 1214.20 493.968 1 -7 4 7 49.7538 368.430 1 -7 4 7 331.345 442.516 1 -7 4 6 1773.15 514.088 1 7 -4 -6 1873.46 854.112 1 -7 4 6 2010.87 528.125 1 -7 4 6 702.201 341.406 1 -7 4 5 8764.50 777.268 1 7 -4 -5 8220.01 1151.76 1 -7 4 5 7188.90 648.674 1 -7 4 5 8420.73 820.650 1 -7 4 4 2143.20 451.773 1 7 -4 -4 2422.19 791.323 1 -7 4 4 3015.60 561.582 1 -7 4 3 5822.22 617.704 1 7 -4 -3 4453.05 831.895 1 -7 4 3 5437.42 668.215 1 7 -4 -2 936.564 584.590 1 -7 4 2 1343.64 389.698 1 7 -4 -2 575.547 590.208 1 -7 4 2 1031.52 407.619 1 7 -4 -1 2150.98 674.211 1 -7 4 1 1508.28 459.011 1 7 -4 -1 1551.27 559.101 1 -7 4 1 1670.97 397.477 1 -7 4 1 1859.26 475.522 1 -7 4 0 1710.53 475.803 1 7 -4 0 1313.61 545.251 1 7 -4 0 827.626 597.100 1 -7 4 0 803.560 362.348 1 -7 4 0 1374.56 467.565 1 7 -4 1 276.318 554.270 1 7 -4 1 691.191 478.086 1 -7 4 -1 252.625 380.885 1 -7 4 -1 149.354 322.884 1 -7 4 -1 831.845 455.499 1 -7 4 -2-137.487 337.727 1 -7 4 -2-294.426 350.672 1 -7 4 -2-0.24785 353.641 1 7 -4 2 351.030 543.039 1 -7 4 -3 280.246 393.793 1 -7 4 -3 134.853 324.867 1 7 -4 3 150.343 519.873 1 -7 4 -3 312.091 364.551 1 -7 4 -4 871.816 448.751 1 7 -4 4 1169.30 591.140 1 -7 4 -4 1146.52 464.644 1 7 -4 5 4790.36 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1234.84 424.656 1 7 4 -6 1857.81 596.691 1 -7 -4 6 1579.03 451.131 1 7 4 -6 969.553 449.427 1 -7 -4 6 2258.56 510.168 1 7 4 -5 7642.88 880.576 1 -7 -4 5 6935.32 687.898 1 7 4 -5 5653.92 645.704 1 -7 -4 5 7244.44 726.512 1 -7 -4 5 4897.93 629.257 1 -7 -4 4 949.671 372.143 1 7 4 -4 1622.00 524.625 1 7 4 -4 979.848 380.837 1 -7 -4 4 2253.18 497.970 1 -7 -4 4 1980.64 450.961 1 7 4 -3 5077.64 686.767 1 -7 -4 3 4808.06 651.083 1 -7 -4 3 3913.80 573.696 1 -7 -4 3 4582.74 560.214 1 -7 -4 2 323.544 316.510 1 -7 -4 2 252.556 312.364 1 7 4 -2 579.407 426.954 1 -7 -4 2 533.802 435.783 1 -7 -4 2 328.701 329.194 1 -7 -4 1 1330.96 341.525 1 7 4 -1 1004.08 493.820 1 -7 -4 1 1759.21 443.619 1 7 4 -1 1561.24 449.908 1 -7 -4 1 760.904 449.272 1 -7 -4 1 1153.05 473.200 1 -7 -4 0 1465.67 441.693 1 7 4 0 1483.27 481.333 1 7 4 0 621.417 359.050 1 -7 -4 0 568.967 337.222 1 -7 -4 0 692.099 420.846 1 -7 -4 0 999.661 338.277 1 -7 -4 -1 323.840 329.468 1 7 4 1 108.396 335.440 1 -7 -4 -1 310.055 286.576 1 -7 -4 -1 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1484.10 626.181 1 7 5 8 963.043 394.722 1 -7 -5 -8 1598.48 667.638 1 -7 -5 -8 1456.87 753.600 1 -7 -6 11 1572.59 738.196 1 7 6 -11 1481.35 630.439 1 -7 -6 10 1023.20 609.784 1 7 6 -10 1040.58 858.896 1 7 6 -10-413.541 537.440 1 -7 -6 10 357.536 510.729 1 -7 -6 10 96.6222 460.274 1 -7 -6 9 1025.03 511.622 1 7 6 -9 401.124 449.107 1 -7 -6 9-153.605 470.408 1 -7 -6 9 825.407 462.513 1 -7 -6 8 470.114 437.087 1 7 6 -8 846.547 663.880 1 7 6 -8 395.258 474.274 1 -7 -6 8 232.761 462.224 1 -7 -6 8 524.358 453.527 1 -7 -6 7 972.652 498.549 1 7 6 -7 438.789 550.561 1 7 6 -7-334.511 485.482 1 -7 -6 7 576.548 491.198 1 -7 -6 7 507.696 408.742 1 -7 -6 6 885.841 461.055 1 7 6 -6 2548.46 690.780 1 -7 -6 6 2265.70 529.652 1 7 6 -6 1489.31 528.508 1 -7 -6 6 2344.99 519.180 1 -7 -6 5 773.172 473.234 1 7 6 -5 1789.22 605.727 1 7 6 -5 845.470 472.589 1 -7 -6 5 1639.51 542.717 1 -7 -6 5 1093.36 428.641 1 -7 -6 4 870.760 392.000 1 7 6 -4 851.199 507.231 1 7 6 -4 1138.56 482.550 1 -7 -6 4 769.079 363.825 1 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416.280 434.332 1 -7 -6 -7 39.8326 497.758 1 7 6 7 387.026 389.943 1 -7 -6 -7 141.369 502.928 1 -7 -6 -8 1460.40 696.490 1 7 6 8 1522.66 446.069 1 7 7 -11 332.171 513.317 1 -7 -7 10 1821.52 573.786 1 7 7 -10 2485.72 659.535 1 -7 -7 10 946.168 621.198 1 -7 -7 9-337.334 524.945 1 7 7 -9-394.157 604.354 1 -7 -7 9-569.730 534.898 1 -7 -7 9 211.392 445.473 1 -7 -7 8 862.252 529.703 1 7 7 -8 80.8494 617.689 1 7 7 -8 144.360 475.096 1 -7 -7 8-214.510 548.179 1 -7 -7 8 383.989 427.495 1 -7 -7 7 570.731 426.821 1 7 7 -7 606.365 602.945 1 7 7 -7 1289.09 598.927 1 -7 -7 7 901.097 472.762 1 -7 -7 7 187.481 420.529 1 -7 -7 6 210.212 420.710 1 7 7 -6 61.5980 568.942 1 7 7 -6 77.4811 415.567 1 -7 -7 6 576.582 423.909 1 -7 -7 6 597.857 442.122 1 7 7 -5 435.448 520.723 1 7 7 -5 96.4453 421.179 1 -7 -7 5 810.663 479.521 1 -7 -7 5 160.050 366.435 1 7 7 -4 1063.83 522.837 1 7 7 -4 1324.54 522.834 1 -7 -7 4 801.702 433.108 1 -7 -7 4 825.843 398.834 1 -7 -7 3 364.636 381.107 1 7 7 -3 290.681 381.532 1 -7 -7 3 585.358 365.839 1 -7 -7 3 1163.66 485.906 1 -7 -7 2 22190.7 1276.55 1 7 7 -2 23769.6 1256.55 1 -7 -7 2 12428.5 941.307 1 -7 -7 2 11706.0 1032.85 1 -7 -7 1 5242.63 693.847 1 7 7 -1 5251.97 629.859 1 -7 -7 1 3570.40 532.481 1 -7 -7 0 6677.16 777.297 1 7 7 0 5657.12 632.202 1 -7 -7 0 5036.99 613.003 1 -7 -7 0 5743.57 722.917 1 -7 -7 -1 2673.44 587.686 1 7 7 1 1123.10 393.621 1 -7 -7 -1 2201.52 554.524 1 -7 -7 -1 1680.25 450.236 1 -7 -7 -2 1105.05 495.161 1 7 7 2 279.299 342.028 1 -7 -7 -2 1310.37 448.215 1 -7 -7 -2 690.025 468.826 1 -7 -7 -3 10063.5 1002.79 1 -7 -7 -3 10814.1 1075.62 1 -7 -7 -3 9753.77 1081.54 1 -7 -7 -4 631.879 462.536 1 7 7 4 437.954 411.413 1 -7 -7 -4 986.683 537.243 1 -7 -7 -5-194.536 474.576 1 7 7 5 403.760 406.984 1 -7 -7 -5 138.689 414.983 1 -7 -7 -6 493.806 527.853 1 7 7 6 131.952 368.815 1 -7 -7 -6 353.197 506.033 1 -7 -7 -7 999.566 637.808 1 7 7 7 2266.39 522.593 1 -7 -7 -7 1155.05 562.042 1 -7 -8 10 1107.75 588.078 1 7 8 -10-484.189 510.847 1 -7 -8 10 381.523 560.515 1 -7 -8 9 612.966 561.179 1 7 8 -9 628.421 680.500 1 7 8 -9-1267.08 642.064 1 -7 -8 9 556.544 581.603 1 7 8 -8 274.628 629.750 1 7 8 -8-559.041 574.674 1 -7 -8 8-442.850 560.121 1 -7 -8 8-238.569 446.509 1 7 8 -7-152.770 586.392 1 7 8 -7 163.398 510.232 1 -7 -8 7 411.505 542.277 1 -7 -8 7 178.624 433.866 1 7 8 -6-166.685 575.094 1 7 8 -6 799.358 512.637 1 -7 -8 6 259.733 459.091 1 -7 -8 6 11.3877 437.210 1 7 8 -5 1579.84 620.016 1 7 8 -5 625.934 507.862 1 -7 -8 5 348.489 392.995 1 -7 -8 5 730.091 453.013 1 7 8 -4 238.095 484.521 1 7 8 -4 28.7124 434.281 1 -7 -8 4-118.844 489.076 1 -7 -8 4-194.563 377.777 1 -7 -8 3 7014.34 749.300 1 -7 -8 3 6221.10 836.300 1 -7 -8 2 1480.63 519.811 1 7 8 -2 1686.86 471.796 1 -7 -8 2 574.820 434.818 1 -7 -8 2 1012.66 397.677 1 -7 -8 1 575.924 476.939 1 7 8 -1 1629.46 503.197 1 -7 -8 1 108.485 329.636 1 -7 -8 1 231.270 396.517 1 -7 -8 0 1611.55 587.537 1 7 8 0 557.667 393.080 1 -7 -8 0 957.385 376.605 1 -7 -8 0 1252.15 527.087 1 -7 -8 -1-22.4501 395.306 1 7 8 1-81.3480 369.876 1 -7 -8 -1-69.0973 340.893 1 -7 -8 -1 354.949 455.489 1 -7 -8 -2 253.944 450.048 1 7 8 2 674.279 411.648 1 -7 -8 -2 743.147 427.931 1 -7 -8 -2-223.546 389.750 1 -7 -8 -3 701.250 607.176 1 7 8 3 152.770 371.330 1 -7 -8 -3 4.09858 444.414 1 -7 -8 -4 2856.12 660.998 1 7 8 4 1540.83 496.094 1 -7 -8 -4 2514.93 656.522 1 -7 -8 -5 1184.36 520.905 1 7 8 5 28.2971 394.540 1 -7 -8 -5 1447.19 610.689 1 7 8 6 3082.15 588.816 1 -7 -8 -6 1802.39 617.797 1 -7 -8 -6 2123.62 717.840 1 7 9 -8 4754.35 933.219 1 7 9 -8 3874.66 841.327 1 -7 -9 8 2506.90 700.454 1 7 9 -7-487.725 652.913 1 7 9 -7-853.727 588.440 1 -7 -9 7-100.481 539.450 1 -7 -9 7 354.623 494.064 1 7 9 -6 4704.43 840.570 1 7 9 -6 4203.93 757.926 1 -7 -9 6 557.777 481.659 1 -7 -9 6 1477.17 558.845 1 7 9 -5 462.383 645.611 1 7 9 -5 427.900 537.667 1 -7 -9 5-72.0563 448.977 1 -7 -9 5 464.303 431.385 1 7 9 -4 5325.44 757.051 1 7 9 -4 4752.86 756.502 1 -7 -9 4 2264.58 558.991 1 -7 -9 4 1903.43 652.085 1 -7 -9 3 2785.61 716.400 1 -7 -9 3 1465.47 428.947 1 -7 -9 2 668.739 454.344 1 7 9 -2 1422.04 466.344 1 -7 -9 2 978.146 448.565 1 -7 -9 2 531.522 380.757 1 -7 -9 1 3498.19 693.514 1 -7 -9 1 2171.31 490.489 1 -7 -9 1 2492.69 558.656 1 -7 -9 0 769.147 485.479 1 7 9 0 538.166 402.288 1 -7 -9 0 135.586 427.060 1 -7 -9 0 361.570 368.495 1 -7 -9 -1 568.268 457.077 1 7 9 1 905.521 450.283 1 -7 -9 -1 385.378 375.871 1 -7 -9 -1 222.456 407.162 1 -7 -9 -2 2878.16 704.093 1 -7 -9 -2 1993.75 552.518 1 -7 -9 -3 1874.97 637.910 1 -7 -9 -3 1419.57 516.823 1 -7 -9 -4 5554.88 857.631 1 7 9 4 3242.30 635.366 1 -7 -9 -4 4921.07 815.846 1 -7 -9 -5 541.738 577.519 1 7 9 5 110.507 408.190 1 -7 -9 -5 948.612 548.444 1 7 10 -7 5361.10 992.584 1 7 10 -7 4154.07 867.400 1 7 10 -6 1797.97 706.048 1 7 10 -6 2137.91 705.642 1 -7 -10 6 174.034 598.484 1 -7 -10 6 491.212 540.976 1 7 10 -5 426.896 572.444 1 7 10 -5 722.007 554.542 1 -7 -10 5 147.539 510.570 1 -7 -10 5-470.191 451.139 1 7 10 -4 2925.72 712.329 1 -7 -10 4 1452.39 541.657 1 -7 -10 4 1288.28 460.121 1 7 10 -3 707.939 458.697 1 -7 -10 3 398.390 539.601 1 -7 -10 3 305.890 396.082 1 -7 -10 2 1447.62 532.029 1 -7 -10 2 1296.19 596.998 1 -7 -10 2 1118.81 434.003 1 -7 -10 1 1701.05 584.174 1 7 10 -1 2200.11 549.413 1 -7 -10 1 831.589 508.631 1 -7 -10 1 956.117 448.995 1 -7 -10 0 8788.79 987.238 1 7 10 0 2133.32 502.350 1 -7 -10 0 3899.72 604.433 1 -7 -10 0 7524.98 961.131 1 -7 -10 -1 7086.04 902.008 1 -7 -10 -1 5076.62 785.262 1 -7 -10 -2 572.609 457.378 1 7 10 2 951.160 439.636 1 -7 -10 -2 62.0553 451.481 1 -7 -10 -3 1769.52 611.079 1 7 10 3 1305.16 516.555 1 -7 -10 -3 1178.95 573.682 1 7 11 -6 1249.65 670.006 1 7 11 -5 62.6778 574.509 1 7 11 -4 160.370 485.558 1 7 11 -4 762.371 540.023 1 -7 -11 4 154.327 448.056 1 7 11 -3 1060.43 486.841 1 -7 -11 3 507.946 408.866 1 -7 -11 2 708.856 494.079 1 7 11 -2 21.1996 444.938 1 -7 -11 2 44.3016 520.666 1 -7 -11 2 293.015 436.670 1 -7 -11 1 1115.11 589.510 1 7 11 -1 2015.72 568.225 1 -7 -11 1 900.210 516.115 1 -7 -11 1 789.464 431.632 1 -7 -11 0 5564.06 941.830 1 -7 -11 0 4054.97 749.522 1 -7 -12 3 117.562 437.662 1 -8 10 3 252.424 479.922 1 -8 10 2 325.615 499.650 1 -8 10 0 1956.63 612.096 1 -8 10 -1 1245.26 529.951 1 8 -9 -6 347.200 1015.44 1 -8 9 6-145.666 497.953 1 -8 9 5-69.5248 518.528 1 8 -9 -5-594.608 1110.81 1 -8 9 5 832.949 529.954 1 -8 9 4 152.375 487.465 1 -8 9 4 429.774 475.512 1 -8 9 3 500.761 494.330 1 -8 9 3 215.307 505.538 1 -8 9 2 1223.80 526.300 1 -8 9 2 956.437 578.323 1 -8 9 1 7869.83 869.627 1 -8 9 1 7353.00 895.565 1 -8 9 0 3053.84 671.557 1 -8 9 0 2198.69 674.778 1 8 -9 1 2126.98 936.846 1 -8 9 -1 862.063 506.580 1 -8 9 -1 1099.91 590.072 1 -8 9 -2 1132.29 617.765 1 -8 8 7 1889.93 610.927 1 8 -8 -7 1020.05 1148.35 1 -8 8 6 155.270 452.855 1 8 -8 -6-159.646 962.043 1 -8 8 6 293.930 497.685 1 -8 8 5 767.155 567.604 1 8 -8 -5 1653.40 999.809 1 -8 8 5 420.907 487.061 1 -8 8 4 1975.44 583.762 1 8 -8 -4 615.487 891.524 1 -8 8 4 2464.51 650.346 1 -8 8 3 3254.58 549.541 1 -8 8 3 3706.30 688.359 1 8 -8 -2 10590.9 1311.78 1 -8 8 2 8742.26 811.378 1 -8 8 2 9897.74 932.441 1 -8 8 1 6826.13 783.031 1 -8 8 1 5637.34 820.324 1 -8 8 0 503.961 442.020 1 8 -8 0-469.649 825.967 1 -8 8 0 878.805 528.867 1 8 -8 1 1583.58 840.644 1 -8 8 -1 1051.64 519.875 1 -8 8 -1 946.497 566.109 1 -8 8 -2 327.030 459.820 1 8 -8 2 257.375 702.206 1 -8 8 -2-259.633 477.069 1 8 -8 3 1335.00 790.539 1 -8 8 -3 1192.43 531.413 1 -8 8 -3-68.7521 469.849 1 -8 8 -5 716.972 492.798 1 -8 7 8-387.265 608.242 1 8 -7 -8 291.684 1073.32 1 -8 7 8 593.487 525.273 1 -8 7 7 1927.13 584.684 1 8 -7 -7 2052.36 1103.57 1 -8 7 7 1740.96 579.393 1 -8 7 6 83.4148 481.825 1 8 -7 -6-7.52919 842.397 1 -8 7 6 620.858 524.172 1 -8 7 5 1739.10 543.694 1 8 -7 -5 335.392 811.592 1 -8 7 5 2160.78 612.576 1 -8 7 4 10652.6 1021.88 1 -8 7 4 11010.9 917.090 1 -8 7 4 10693.7 991.344 1 -8 7 3 292.086 359.016 1 -8 7 3-151.417 450.479 1 8 -7 -2 1123.57 738.070 1 -8 7 2 439.969 376.958 1 -8 7 2 1082.86 491.436 1 8 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2767.47 827.520 1 -8 6 3 2486.62 511.525 1 8 -6 -3 1296.45 873.861 1 -8 6 3 3230.85 607.342 1 8 -6 -2 911.023 692.465 1 8 -6 -2 1519.94 686.612 1 -8 6 2 1798.51 474.901 1 -8 6 2 2165.85 551.070 1 -8 6 1 3200.96 617.744 1 8 -6 -1 4030.20 851.390 1 -8 6 1 3254.57 633.958 1 8 -6 0 961.518 730.137 1 -8 6 0 59.5831 395.913 1 -8 6 0-87.0864 476.514 1 -8 6 -1 6371.43 772.242 1 -8 6 -1 6992.20 881.544 1 8 -6 2 4818.76 909.792 1 -8 6 -2 4015.21 682.276 1 -8 6 -2 3669.86 736.231 1 8 -6 3-484.869 666.566 1 -8 6 -3 760.554 525.835 1 -8 6 -3 586.485 407.825 1 -8 6 -3-24.9477 414.133 1 -8 6 -4 440.795 480.394 1 -8 6 -4 191.783 420.294 1 -8 6 -4-99.7791 413.977 1 8 -6 4 1050.40 701.677 1 -8 6 -5 487.664 448.431 1 -8 6 -5 758.876 467.216 1 8 -6 5 626.337 710.359 1 -8 6 -5 1028.05 519.292 1 -8 6 -6-95.1402 430.859 1 -8 5 9 204.152 504.989 1 8 -5 -9-686.704 980.885 1 -8 5 9-52.3393 431.088 1 -8 5 8 2644.13 703.172 1 8 -5 -8 2597.15 1207.27 1 -8 5 8 2463.32 609.795 1 -8 5 7 3872.02 703.154 1 8 -5 -7 3487.02 1192.25 1 -8 5 7 4056.56 706.308 1 -8 5 6 12392.5 1076.92 1 8 -5 -6 10117.7 1484.46 1 -8 5 6 8892.70 780.651 1 -8 5 6 9515.86 956.514 1 -8 5 5 3816.34 672.133 1 -8 5 5 3250.82 541.561 1 8 -5 -5 3386.74 976.507 1 -8 5 5 3784.33 652.176 1 8 -5 -4 5542.94 1040.55 1 -8 5 4 5788.86 679.582 1 -8 5 4 7479.65 827.535 1 8 -5 -3-248.345 637.904 1 8 -5 -3 994.668 769.173 1 -8 5 3 10.7353 366.826 1 -8 5 3 980.009 512.216 1 -8 5 2 4995.48 642.114 1 8 -5 -2 4303.99 869.049 1 -8 5 2 5180.84 685.066 1 8 -5 -2 7139.66 1073.45 1 8 -5 -1 537.593 625.872 1 8 -5 -1 156.165 610.507 1 -8 5 1 931.930 391.615 1 -8 5 1 288.466 387.595 1 -8 5 0 216.962 438.958 1 8 -5 0 325.541 642.282 1 -8 5 0 403.243 463.861 1 -8 5 -1 685.567 415.416 1 8 -5 1 682.014 666.990 1 -8 5 -1 1035.55 503.056 1 -8 5 -1 937.649 483.075 1 8 -5 2 1852.47 667.573 1 -8 5 -2 1871.62 592.716 1 -8 5 -2 1088.33 446.493 1 -8 5 -2 1323.55 541.018 1 8 -5 3 6794.16 1027.24 1 -8 5 -3 5652.82 756.783 1 -8 5 -3 5310.71 746.652 1 -8 5 -3 6383.66 800.574 1 8 -5 4 7105.09 1091.58 1 -8 5 -4 6309.06 857.613 1 -8 5 -4 4631.77 733.828 1 -8 5 -4 5245.67 746.750 1 -8 5 -5-92.9693 435.471 1 -8 5 -5 1036.94 536.793 1 8 -5 5 126.182 596.138 1 -8 5 -5 987.248 467.984 1 -8 5 -6 987.792 513.385 1 8 -5 6 334.803 604.948 1 -8 5 -6-200.020 426.021 1 -8 4 10 960.599 568.287 1 -8 4 10-120.889 475.600 1 -8 4 9-114.558 503.464 1 8 -4 -9 514.882 1028.80 1 -8 4 9 1167.10 487.621 1 -8 4 8 544.729 576.487 1 8 -4 -8 1566.90 998.900 1 -8 4 8 240.633 421.602 1 -8 4 7 1663.03 620.647 1 -8 4 7 2609.49 588.282 1 -8 4 7 2975.65 722.375 1 8 -4 -7 3036.03 1028.13 1 -8 4 6 7288.52 871.768 1 8 -4 -6 6111.31 1145.42 1 -8 4 6 4601.13 631.326 1 -8 4 6 3408.70 724.012 1 -8 4 5 8317.23 851.975 1 -8 4 5 7165.16 713.900 1 8 -4 -4 3566.60 925.506 1 -8 4 4 4459.02 634.685 1 -8 4 4 4708.69 660.040 1 8 -4 -3 3697.27 890.729 1 8 -4 -3 4090.74 874.808 1 -8 4 3 4754.49 623.914 1 -8 4 3 5436.09 676.555 1 8 -4 -2 1309.67 763.519 1 8 -4 -2-166.871 635.122 1 -8 4 2 538.770 365.849 1 -8 4 2 264.804 391.932 1 8 -4 -1 3369.52 798.904 1 -8 4 1 3618.48 584.804 1 8 -4 -1 2345.39 745.711 1 -8 4 1 3829.44 580.236 1 -8 4 0 4098.68 632.771 1 8 -4 0 2573.26 765.239 1 -8 4 0 3234.55 566.908 1 8 -4 0 2257.70 751.374 1 -8 4 0 2562.13 572.582 1 8 -4 1 2691.11 755.466 1 -8 4 -1 1551.85 498.016 1 -8 4 -1 1288.62 468.757 1 -8 4 -1 1240.77 488.504 1 8 -4 2 2193.64 740.349 1 -8 4 -2 2495.46 588.947 1 -8 4 -2 2089.16 534.767 1 -8 4 -2 1764.69 510.555 1 8 -4 3 6041.09 1006.26 1 -8 4 -3 5913.33 844.286 1 -8 4 -3 6802.02 839.379 1 -8 4 -3 5621.52 814.382 1 -8 4 -4 1170.66 459.067 1 -8 4 -4 748.136 499.847 1 8 -4 4-13.0199 572.521 1 -8 4 -4 303.359 403.807 1 -8 4 -5 1785.81 600.034 1 8 -4 5 1261.80 665.811 1 -8 4 -5 1025.65 523.364 1 -8 4 -5 1966.61 561.210 1 8 -4 6 1794.14 767.000 1 -8 4 -6 849.808 587.007 1 8 -4 7 898.008 619.546 1 -8 4 -7 840.038 569.654 1 -8 3 11 885.646 519.912 1 -8 3 10 631.333 527.903 1 -8 3 10-197.576 437.080 1 -8 3 9 1311.79 581.046 1 8 -3 -9 1031.69 946.999 1 -8 3 9 293.223 414.549 1 -8 3 8 1097.17 563.065 1 -8 3 8 1776.41 579.448 1 -8 3 8 1252.78 525.458 1 -8 3 7 297.680 475.383 1 8 -3 -7 1692.22 893.227 1 -8 3 7-150.549 429.749 1 -8 3 7 434.715 569.820 1 -8 3 6 5485.91 770.508 1 -8 3 6 4984.98 689.909 1 -8 3 6 4469.90 693.402 1 -8 3 5 349.284 365.971 1 8 -3 -5 793.373 692.527 1 -8 3 5 953.830 421.082 1 -8 3 5 374.423 420.815 1 8 -3 -4 5064.35 876.170 1 -8 3 4 3994.70 571.386 1 -8 3 4 4519.20 711.446 1 8 -3 -3 10795.6 1164.24 1 8 -3 -3 9221.89 1057.88 1 -8 3 3 13163.9 914.416 1 -8 3 3 14369.6 966.143 1 8 -3 -2 4975.30 835.975 1 -8 3 2 7495.90 786.965 1 8 -3 -2 7767.90 1067.72 1 -8 3 2 6847.41 724.609 1 8 -3 -1 5667.36 997.908 1 -8 3 1 7895.24 760.125 1 -8 3 1 7537.72 708.913 1 -8 3 1 6800.21 773.951 1 -8 3 0 2233.59 495.069 1 8 -3 0 4156.13 805.324 1 8 -3 0 2261.41 596.010 1 -8 3 0 3054.08 575.208 1 -8 3 0 3089.84 568.765 1 8 -3 1 1168.85 599.987 1 8 -3 1 1326.46 571.586 1 -8 3 -1 314.728 392.049 1 -8 3 -1 673.017 425.408 1 -8 3 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1697.52 804.936 1 -8 2 6 1763.50 521.595 1 -8 2 6 1645.82 527.750 1 -8 2 5 3057.22 557.635 1 8 -2 -5 1082.51 723.248 1 -8 2 5 1804.70 427.038 1 -8 2 5 2589.15 591.013 1 -8 2 4 22343.0 1128.83 1 -8 2 4 26853.2 1324.40 1 8 -2 -3 4006.82 824.764 1 8 -2 -3 4205.69 717.483 1 -8 2 3 5713.46 620.970 1 -8 2 3 5649.92 676.891 1 8 -2 -2 969.917 526.910 1 -8 2 2 848.966 408.159 1 8 -2 -2 1235.29 675.557 1 -8 2 2 1624.52 433.791 1 -8 2 2 1551.12 502.783 1 8 -2 -1 2534.59 721.443 1 8 -2 -1 1762.47 595.257 1 -8 2 1 1800.85 477.894 1 -8 2 1 2121.12 472.023 1 -8 2 1 1513.19 438.971 1 8 -2 0 450.671 506.494 1 -8 2 0 455.060 375.422 1 8 -2 0 109.343 554.841 1 -8 2 0 467.654 360.673 1 -8 2 0 682.561 393.859 1 8 -2 1 1675.58 608.568 1 8 -2 1 1088.84 539.056 1 -8 2 -1 1374.92 457.576 1 -8 2 -1 1557.41 499.405 1 -8 2 -1 1569.07 504.611 1 8 -2 2 899.873 502.100 1 -8 2 -2 108.097 397.812 1 -8 2 -2 541.337 441.972 1 -8 2 -2 455.942 425.455 1 8 -2 2 686.693 584.605 1 -8 2 -3 1470.23 521.300 1 -8 2 -3 879.367 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442.011 1 -8 1 5 3621.80 567.682 1 8 -1 -5 5062.48 878.326 1 -8 1 5 3729.88 573.811 1 -8 1 5 3552.93 616.689 1 -8 1 4 17685.8 982.975 1 -8 1 4 20032.8 1169.90 1 8 -1 -3 8771.02 1069.30 1 8 -1 -3 8135.47 919.055 1 -8 1 3 7667.26 722.426 1 -8 1 3 8765.98 793.260 1 -8 1 3 8523.28 823.879 1 8 -1 -2 4822.10 787.105 1 -8 1 2 5115.23 626.490 1 -8 1 2 4273.73 569.987 1 8 -1 -2 5752.87 907.580 1 -8 1 2 3370.12 581.304 1 8 -1 -1 3596.79 678.891 1 -8 1 1 2885.36 567.484 1 -8 1 1 2246.00 516.868 1 -8 1 1 3222.82 562.392 1 8 -1 -1 3865.87 755.875 1 8 -1 0 5536.12 849.924 1 8 -1 0 4236.14 766.358 1 -8 1 0 4691.42 610.972 1 -8 1 0 4447.00 636.165 1 -8 1 0 4987.07 626.650 1 8 -1 1 788.891 590.229 1 8 -1 1 1446.82 534.038 1 -8 1 -1 1107.94 434.160 1 -8 1 -1 1187.78 445.692 1 -8 1 -1 2018.40 502.432 1 8 -1 2 814.632 505.260 1 -8 1 -2 868.854 432.659 1 -8 1 -2 691.172 449.945 1 8 -1 2 998.574 614.224 1 -8 1 -2 368.503 426.308 1 8 -1 3 391.993 464.446 1 -8 1 -3 1123.57 458.187 1 8 -1 3 846.010 571.929 1 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-9 -1 0 576.971 420.567 1 -9 -1 0 1449.95 513.327 1 9 1 1 2300.05 699.745 1 9 1 1 1284.42 563.384 1 -9 -1 -1 1342.75 494.381 1 -9 -1 -1 1091.35 501.705 1 -9 -1 -1 1686.85 540.816 1 9 1 2 1810.54 627.855 1 9 1 2 693.377 499.040 1 -9 -1 -2 1094.58 519.628 1 -9 -1 -2 319.483 425.002 1 -9 -1 -2 1231.38 466.732 1 9 1 3 1623.32 591.331 1 -9 -1 -3 1327.76 550.838 1 -9 -1 -3 1002.66 499.376 1 9 1 3 1756.48 707.354 1 -9 -1 -3 1371.35 455.626 1 -9 -1 -4 22062.5 1374.87 1 -9 -1 -4 18712.5 1430.67 1 9 1 4 20142.4 1499.87 1 -9 -1 -5 6435.27 827.766 1 -9 -1 -5 6958.58 954.813 1 9 1 5 4470.17 926.463 1 9 1 6 1915.89 685.789 1 -9 -1 -6 1662.77 541.403 1 -9 -2 9-291.804 505.353 1 -9 -2 9-133.846 428.757 1 -9 -2 8-79.0387 489.844 1 9 2 -8 587.883 758.248 1 -9 -2 8-460.023 414.763 1 -9 -2 7 1518.81 575.386 1 -9 -2 7 1884.66 608.803 1 -9 -2 6 202.913 457.303 1 9 2 -6 100.169 601.906 1 -9 -2 6 861.182 500.503 1 -9 -2 5 9987.05 1063.27 1 -9 -2 5 7582.41 952.912 1 9 2 -4 3935.96 856.801 1 -9 -2 4 3560.69 781.699 1 -9 -2 4 2021.81 545.846 1 -9 -2 4 2619.35 601.786 1 9 2 -3 2909.06 758.828 1 -9 -2 3 3905.35 702.831 1 -9 -2 3 4996.13 682.834 1 -9 -2 3 3732.95 668.831 1 -9 -2 2-104.722 390.890 1 9 2 -2 747.070 546.369 1 9 2 -2 1590.68 676.788 1 -9 -2 2 623.704 393.344 1 -9 -2 2 748.533 457.262 1 9 2 -1 1140.14 629.702 1 9 2 -1 1221.75 562.219 1 -9 -2 1 816.863 415.988 1 -9 -2 1 1007.53 541.478 1 -9 -2 1 781.898 451.433 1 9 2 0 54.4455 475.161 1 -9 -2 0 246.334 380.433 1 -9 -2 0-270.435 411.446 1 9 2 0-140.698 577.173 1 -9 -2 0 17.2429 390.157 1 9 2 1 1251.97 659.720 1 9 2 1 1872.67 583.441 1 -9 -2 -1 1155.67 482.801 1 -9 -2 -1 1971.91 549.960 1 -9 -2 -1 1746.30 498.858 1 9 2 2 590.916 603.137 1 9 2 2 314.242 476.588 1 -9 -2 -2 356.416 465.728 1 -9 -2 -2 761.447 448.250 1 9 2 3 8149.81 1001.25 1 9 2 3 7681.41 894.870 1 -9 -2 -3 7333.42 835.162 1 -9 -2 -3 7295.44 944.989 1 9 2 4 5258.65 756.810 1 -9 -2 -4 4266.67 756.286 1 -9 -2 -4 3218.43 795.193 1 9 2 4 4281.57 829.542 1 -9 -2 -5 5797.93 909.305 1 -9 -2 -5 4301.08 856.671 1 9 2 5 4248.84 866.807 1 9 2 6 1675.22 698.047 1 -9 -2 -6 1075.16 572.414 1 -9 -3 9 409.697 530.247 1 -9 -3 9 705.596 493.006 1 -9 -3 8-742.422 536.110 1 9 3 -8 349.251 723.940 1 -9 -3 8 342.969 477.749 1 -9 -3 7 492.526 496.566 1 9 3 -7 335.089 664.245 1 -9 -3 7 321.397 434.315 1 -9 -3 6 892.591 481.044 1 9 3 -6 2373.23 811.434 1 -9 -3 6 1053.97 535.370 1 -9 -3 5 3462.88 699.372 1 -9 -3 5 4451.11 735.104 1 -9 -3 5 2469.67 641.650 1 9 3 -4 6442.73 926.941 1 -9 -3 4 5822.71 816.582 1 -9 -3 4 4639.21 728.563 1 -9 -3 4 4344.40 736.834 1 -9 -3 3 505.633 425.143 1 9 3 -3 530.716 611.300 1 -9 -3 3 1207.58 592.999 1 -9 -3 3 891.813 433.109 1 9 3 -2 803.654 565.528 1 -9 -3 2 1518.98 534.046 1 -9 -3 2 723.850 451.550 1 -9 -3 2 1833.83 531.545 1 -9 -3 1 1715.37 497.884 1 9 3 -1 1158.54 566.127 1 -9 -3 1 1760.73 512.483 1 -9 -3 1 1484.32 583.426 1 9 3 0 375.184 508.839 1 -9 -3 0 432.164 389.817 1 -9 -3 0 71.1390 405.326 1 9 3 1 900.523 542.579 1 -9 -3 -1-47.7738 382.347 1 -9 -3 -1 588.321 456.602 1 9 3 2 1376.94 546.818 1 -9 -3 -2 1673.91 477.302 1 -9 -3 -2 767.898 482.515 1 9 3 3 3131.30 604.688 1 -9 -3 -3 3176.37 623.513 1 -9 -3 -3 2145.59 695.691 1 9 3 4 49.6145 400.553 1 -9 -3 -4 331.518 440.292 1 -9 -3 -4 278.576 534.312 1 9 3 5 611.213 456.380 1 -9 -3 -5 983.712 516.461 1 -9 -3 -6 1172.02 528.505 1 -9 -4 9 2676.71 766.456 1 -9 -4 8-245.230 519.647 1 9 4 -8 728.896 698.223 1 -9 -4 8 1140.83 538.267 1 -9 -4 7 988.716 488.772 1 9 4 -7 1297.71 751.969 1 -9 -4 7 1186.48 550.665 1 -9 -4 6 115.781 448.529 1 9 4 -6 590.348 688.289 1 -9 -4 6 7.39358 410.920 1 -9 -4 5 591.974 450.551 1 9 4 -5 1585.63 708.175 1 -9 -4 5 185.059 413.056 1 -9 -4 5 1518.06 501.347 1 -9 -4 4 1591.03 528.812 1 9 4 -4 1344.66 757.476 1 -9 -4 4 1472.78 551.240 1 -9 -4 4 985.485 488.162 1 9 4 -3 1538.41 675.901 1 -9 -4 3 2234.20 628.441 1 -9 -4 3 1750.21 535.123 1 -9 -4 3 2221.09 592.752 1 9 4 -2 1343.38 645.138 1 -9 -4 2 541.596 553.009 1 -9 -4 2 716.944 465.509 1 9 4 -1 2156.03 645.422 1 -9 -4 1 1698.49 622.786 1 -9 -4 1 1331.08 491.901 1 9 4 0 2423.69 683.728 1 -9 -4 0 1436.23 500.599 1 -9 -4 0 1762.78 574.784 1 9 4 1 912.979 557.640 1 -9 -4 -1 976.106 429.529 1 -9 -4 -1 811.739 528.397 1 9 4 2 4086.32 655.730 1 -9 -4 -2 3359.05 614.139 1 -9 -4 -2 4019.15 771.127 1 9 4 3-17.2887 415.845 1 -9 -4 -3 925.241 433.637 1 -9 -4 -3 1141.91 571.703 1 9 4 4 3310.97 635.330 1 -9 -4 -4 2830.47 622.443 1 -9 -4 -4 3507.02 779.174 1 9 4 5 208.169 425.211 1 -9 -4 -5 328.050 398.587 1 -9 -5 8 3468.03 753.012 1 9 5 -7 8805.61 1286.40 1 -9 -5 7 7621.50 883.702 1 -9 -5 7 6420.93 860.281 1 -9 -5 6 317.540 448.163 1 9 5 -6 1634.56 767.144 1 -9 -5 6 858.515 476.498 1 -9 -5 6 483.898 474.133 1 9 5 -5 1226.27 763.688 1 -9 -5 5 445.649 455.810 1 -9 -5 5 818.357 500.708 1 9 5 -4 1406.43 674.764 1 -9 -5 4 254.943 473.853 1 -9 -5 4 400.750 452.997 1 9 5 -3 81.6448 557.242 1 -9 -5 3 335.426 443.941 1 -9 -5 3 1048.77 491.540 1 9 5 -2 3491.61 800.480 1 -9 -5 2 3005.96 661.005 1 -9 -5 2 3042.75 635.199 1 9 5 -1 1247.73 648.186 1 -9 -5 1 1920.49 712.553 1 -9 -5 1 1188.03 541.637 1 9 5 0-463.863 477.776 1 -9 -5 0 390.953 521.329 1 -9 -5 0 184.955 454.145 1 9 5 1 3451.90 670.810 1 -9 -5 -1 3998.10 735.851 1 -9 -5 -1 4262.95 840.160 1 9 5 2 2010.78 536.641 1 -9 -5 -2 1899.89 573.126 1 -9 -5 -2 1319.49 532.259 1 9 5 3 1677.46 560.071 1 -9 -5 -3 885.741 475.712 1 -9 -5 -3 1713.40 624.834 1 9 5 4 158.321 423.120 1 -9 -5 -4-153.173 357.727 1 9 5 5 1280.15 493.090 1 -9 -6 7 668.706 534.691 1 9 6 -6 4107.18 912.292 1 -9 -6 6 2183.24 613.412 1 -9 -6 6 2745.51 608.819 1 9 6 -5-1190.66 661.694 1 -9 -6 5 777.704 530.545 1 -9 -6 5-411.154 499.100 1 9 6 -4 1223.93 661.999 1 -9 -6 4 335.143 402.306 1 -9 -6 4 635.760 503.378 1 9 6 -3 149.981 555.046 1 -9 -6 3 583.046 473.602 1 -9 -6 3-366.604 446.992 1 9 6 -2 4325.58 812.403 1 -9 -6 2 3176.30 652.775 1 -9 -6 2 4005.98 789.831 1 9 6 -1 245.893 518.793 1 -9 -6 1 656.907 558.044 1 -9 -6 1 376.477 493.163 1 9 6 0 4343.88 711.024 1 -9 -6 0 5123.83 812.088 1 -9 -6 0 6031.58 884.058 1 9 6 1 628.341 459.695 1 -9 -6 -1 646.612 559.709 1 -9 -6 -1 1182.39 603.741 1 9 6 2-208.556 469.209 1 -9 -6 -2 1640.50 662.348 1 -9 -6 -2 954.491 570.245 1 9 6 3 2583.49 608.687 1 -9 -6 -3 1644.07 602.173 1 -9 -7 7 513.714 544.769 1 -9 -7 6 478.277 433.200 1 -9 -7 5 2073.84 656.460 1 9 7 -4 21.6038 618.116 1 -9 -7 4 412.669 426.030 1 -9 -7 4 865.797 521.182 1 9 7 -3 625.841 647.394 1 -9 -7 3 562.308 416.264 1 -9 -7 3 559.193 495.812 1 9 7 -2 783.342 590.603 1 -9 -7 2 667.710 482.701 1 -9 -7 2 1055.22 477.078 1 9 7 -1 574.378 564.460 1 -9 -7 1 746.939 519.812 1 -9 -7 1-449.082 546.751 1 9 7 0-232.316 516.072 1 -9 -7 0 238.787 427.765 1 -9 -7 0 552.652 530.615 1 -9 -7 -1-167.020 509.848 1 -9 -7 -1 282.039 442.527 1 -9 -7 -1 787.782 519.279 1 -9 -7 -2 3861.17 713.979 1 -9 -7 -2 2807.65 735.051 1 -9 -7 -3 1629.49 643.794 1 -9 -8 2 2001.23 542.465 1 -9 -8 2 1888.07 561.104 1 -9 -8 1 1248.52 519.890 1 -9 -8 1 493.766 459.874 1 -9 -8 0 1317.32 657.348 1 -9 -8 0 647.961 472.075 1 -9 -8 -1 2911.22 716.639 1 -9 -8 -1 2250.75 540.328 1 -9 -8 -2 376.322 481.409 1 10 -5 -5 1318.05 968.492 1 -10 5 5 1465.43 498.036 1 10 -5 -4 1104.11 883.337 1 -10 5 4 1947.33 511.928 1 10 -5 -3 2132.48 954.173 1 -10 5 3 2544.85 590.287 1 -10 5 2 720.175 461.562 1 -10 4 6 1145.60 657.933 1 10 -4 -5 2516.94 1009.45 1 -10 4 5 1544.71 525.992 1 -10 4 4 3484.00 688.296 1 -10 4 4 2971.45 621.990 1 10 -4 -4 1693.16 977.283 1 10 -4 -3 176.927 763.974 1 -10 4 3-90.9695 389.251 1 10 -4 -2 2144.91 830.660 1 -10 4 2 2945.87 673.676 1 10 -4 -2 1815.54 829.007 1 -10 4 2 2303.04 646.342 1 -10 4 1 1221.90 634.152 1 -10 4 1 456.216 524.153 1 -10 3 7 188.461 526.030 1 -10 3 6 1809.37 631.976 1 -10 3 6 236.797 509.718 1 -10 3 5 665.784 517.908 1 10 -3 -5 778.798 809.162 1 -10 3 5 969.645 460.821 1 -10 3 4 790.901 541.647 1 10 -3 -4 1615.84 872.603 1 -10 3 4 1037.24 460.754 1 -10 3 4 358.060 525.801 1 10 -3 -3-304.259 762.970 1 10 -3 -3 387.630 721.144 1 -10 3 3 1101.01 518.415 1 -10 3 3 316.103 504.937 1 10 -3 -2 4116.07 1078.20 1 -10 3 2 3268.76 639.178 1 10 -3 -2 2380.60 827.539 1 -10 3 2 3109.41 708.550 1 10 -3 -1 220.953 657.857 1 -10 3 1 269.863 441.612 1 10 -3 -1 977.114 905.169 1 -10 3 1 1517.38 586.908 1 10 -3 0 1438.24 836.978 1 -10 3 0 1689.39 548.017 1 -10 3 0 1035.88 530.946 1 10 -3 1 537.433 758.394 1 -10 3 -1 59.5106 466.712 1 -10 3 -3 5287.45 878.320 1 -10 2 7 2674.15 646.659 1 -10 2 7 3286.07 812.691 1 10 -2 -6 14545.2 1646.24 1 -10 2 6 11501.3 1239.66 1 -10 2 5 1833.15 607.403 1 -10 2 5 1675.95 542.071 1 10 -2 -5 1857.83 869.689 1 -10 2 5 2096.08 603.775 1 -10 2 4 1843.28 609.225 1 -10 2 4 2208.59 540.911 1 10 -2 -4 3048.28 919.805 1 -10 2 4 2256.72 726.629 1 10 -2 -3 1142.12 766.539 1 10 -2 -3 1039.58 803.115 1 -10 2 3 1548.53 516.798 1 -10 2 3 956.226 585.640 1 10 -2 -2 1428.82 736.402 1 -10 2 2 1393.20 514.207 1 10 -2 -2 246.265 737.653 1 -10 2 2 1841.42 621.807 1 10 -2 -1 1748.96 680.571 1 -10 2 1 1485.58 557.282 1 10 -2 -1 2656.34 847.821 1 -10 2 1 1651.47 553.843 1 10 -2 0 1996.48 907.075 1 10 -2 0 985.074 635.032 1 -10 2 0 1287.06 561.378 1 -10 2 0 1135.18 523.262 1 -10 2 -1 2366.46 685.698 1 10 -2 1 1117.32 794.390 1 -10 2 -1 2060.62 610.411 1 10 -2 2 3280.95 923.058 1 -10 2 -2 2629.25 636.244 1 -10 2 -2 2264.70 599.217 1 -10 2 -3 213.831 507.730 1 -10 2 -3-85.4685 473.657 1 -10 1 8 564.591 461.174 1 -10 1 7 1273.45 524.839 1 -10 1 7 1617.52 611.461 1 -10 1 6 8390.47 969.394 1 10 -1 -6 6917.81 1261.98 1 -10 1 6 10591.0 1279.42 1 -10 1 6 8494.16 1032.98 1 -10 1 5 8310.64 894.116 1 10 -1 -5 5180.77 1147.44 1 -10 1 5 7261.71 964.801 1 -10 1 5 7241.36 914.132 1 -10 1 4 1735.14 610.455 1 -10 1 4 1864.40 551.122 1 10 -1 -4 1278.67 673.771 1 -10 1 4 2211.92 552.678 1 10 -1 -3 2030.05 783.421 1 -10 1 3 1259.03 487.859 1 -10 1 3 1164.49 560.844 1 10 -1 -2 506.060 661.812 1 -10 1 2 823.145 463.652 1 10 -1 -2 1190.97 808.287 1 -10 1 2 1036.68 580.167 1 10 -1 -1 2072.82 735.107 1 -10 1 1 1015.80 471.375 1 10 -1 -1 2873.36 912.320 1 -10 1 1 1478.54 579.286 1 10 -1 0 6104.83 991.863 1 -10 1 0 6219.39 928.789 1 10 -1 0 7262.80 1273.39 1 -10 1 0 7617.03 912.728 1 -10 1 -1 3010.75 713.930 1 10 -1 1 1680.07 793.974 1 -10 1 -1 1546.32 562.246 1 -10 1 -1 2062.07 607.244 1 -10 1 -2 6096.64 864.019 1 -10 1 -2 6731.17 838.376 1 10 -1 3 6991.84 1098.97 1 -10 1 -3 5753.75 754.847 1 -10 1 -4 27162.4 1551.63 1 -10 0 7 1186.45 553.189 1 -10 0 6 2887.52 664.600 1 10 0 -6 3884.42 1129.22 1 -10 0 6 4696.54 827.496 1 -10 0 6 4734.86 850.020 1 -10 0 5 8327.60 906.913 1 10 0 -5 7303.26 1233.67 1 -10 0 5 10618.6 1165.47 1 -10 0 5 8703.32 1006.90 1 -10 0 4 189.507 454.073 1 -10 0 4 177.633 403.101 1 10 0 -4 1363.73 753.895 1 -10 0 4 882.118 521.477 1 -10 0 3 622.430 542.598 1 -10 0 3 212.310 391.106 1 10 0 -2-92.2289 612.550 1 -10 0 2 581.610 436.406 1 10 0 -2-249.299 640.071 1 -10 0 2-535.145 473.553 1 10 0 -1 793.751 701.009 1 -10 0 1-185.071 399.295 1 10 0 -1 1263.53 788.648 1 -10 0 1-135.972 462.103 1 10 0 0-69.5008 654.944 1 10 0 0 159.736 577.797 1 -10 0 0-43.0266 401.075 1 -10 0 0-140.907 410.493 1 -10 0 0 558.885 464.434 1 10 0 1 286.325 628.530 1 -10 0 -1 643.108 485.132 1 10 0 1 210.517 641.827 1 -10 0 -1 661.377 461.717 1 -10 0 -1 618.183 497.024 1 10 0 2 7488.40 1128.78 1 -10 0 -2 5794.96 829.027 1 -10 0 -2 5247.39 873.983 1 -10 0 -2 5485.02 779.427 1 10 0 3 14987.8 1490.90 1 -10 0 -3 15083.5 1339.13 1 -10 0 -3 14350.1 1128.28 1 -10 -1 6 5239.67 899.250 1 -10 -1 6 3563.49 777.010 1 10 1 -5 5925.95 1049.74 1 -10 -1 5 5946.05 926.194 1 -10 -1 5 3659.29 741.437 1 10 1 -4 2665.91 816.578 1 -10 -1 4 2322.92 685.454 1 -10 -1 4 2787.10 660.937 1 -10 -1 3 2026.91 585.736 1 10 1 -3 1398.60 712.877 1 -10 -1 3 740.035 497.961 1 -10 -1 2 393.747 406.832 1 -10 -1 2 701.921 496.574 1 10 1 -1 978.994 649.727 1 -10 -1 1 1788.30 534.637 1 10 1 -1 1694.18 865.826 1 -10 -1 1 2595.04 657.930 1 -10 -1 1 798.375 515.780 1 10 1 0 7936.93 1115.68 1 -10 -1 0 6156.71 792.803 1 10 1 0 8717.73 1309.92 1 -10 -1 0 6376.59 900.592 1 -10 -1 0 6529.41 906.073 1 10 1 1 2395.54 716.924 1 -10 -1 -1 1607.53 542.150 1 10 1 1 2489.91 794.103 1 -10 -1 -1 2381.38 627.898 1 -10 -1 -1 1729.64 541.616 1 10 1 2 5892.91 965.263 1 10 1 2 6442.71 946.254 1 -10 -1 -2 6255.32 851.394 1 -10 -1 -2 6159.03 915.270 1 10 1 3 4799.27 976.360 1 -10 -1 -3 4929.22 874.198 1 10 1 4 25071.4 1794.51 1 -10 -2 6 10934.9 1140.04 1 -10 -2 5 78.9753 521.910 1 10 2 -5 1274.24 780.306 1 -10 -2 5 1463.45 636.188 1 10 2 -4 1952.58 789.993 1 -10 -2 4 4846.67 996.429 1 -10 -2 4 3532.46 731.687 1 10 2 -3 1338.07 711.739 1 -10 -2 3-38.8242 490.602 1 -10 -2 3 1363.60 620.265 1 -10 -2 2 717.279 474.402 1 10 2 -2 1869.43 747.811 1 -10 -2 2 1431.87 549.814 1 -10 -2 2 73.4706 414.921 1 10 2 -1 674.946 654.752 1 -10 -2 1 925.376 471.756 1 -10 -2 1 1492.47 588.038 1 -10 -2 1 199.588 448.782 1 10 2 0 1979.43 685.640 1 -10 -2 0 776.099 453.348 1 -10 -2 0 1386.48 538.267 1 10 2 1 1926.84 669.089 1 -10 -2 -1 1117.48 507.148 1 -10 -2 -1 1600.21 606.837 1 10 2 2 2813.21 707.811 1 -10 -2 -2 2209.55 649.208 1 -10 -2 -2 1274.76 562.174 1 10 2 3-67.5965 494.904 1 -10 -3 6 1096.96 490.271 1 -10 -3 5 639.500 550.375 1 -10 -3 4 1647.13 599.812 1 10 3 -4 140.915 698.525 1 -10 -3 4 264.299 507.739 1 -10 -3 3-36.3970 473.895 1 10 3 -3-260.655 623.329 1 -10 -3 3 1011.24 707.281 1 -10 -3 3 325.929 438.253 1 10 3 -2 4083.65 883.251 1 -10 -3 2 2920.41 689.426 1 -10 -3 2 3298.11 676.154 1 10 3 -1 1642.38 707.930 1 -10 -3 1 534.804 518.144 1 -10 -3 1 1175.86 566.331 1 10 3 0 1779.78 683.636 1 -10 -3 0 2015.01 584.653 1 -10 -3 0 1305.03 572.798 1 10 3 1 466.400 531.453 1 -10 -3 -1 81.6450 392.615 1 -10 -3 -1 270.573 488.669 1 10 3 2 2043.17 660.961 1 10 3 3 6917.81 954.592 1 -10 -4 6-78.6773 423.532 1 -10 -4 4 2178.40 620.897 1 -10 -4 3-223.398 579.948 1 -10 -4 3-358.797 528.739 1 10 4 -2 2417.57 778.976 1 -10 -4 2 2164.92 741.624 1 -10 -4 2 2268.02 609.989 1 10 4 -1 640.769 632.594 1 -10 -4 1-200.014 593.046 1 -10 -4 1 90.3458 478.483 1 10 4 0 1365.95 655.805 1 -10 -4 0 824.629 497.634 1 -10 -4 0 1521.46 648.841 1 10 4 1 848.966 619.771 1 -10 -5 5 864.088 526.974 1 -10 -5 4 3113.22 675.063 1 -10 -5 3 1897.84 679.438 1 -10 -5 2 1445.59 576.218 1 -10 -5 1 1199.55 628.941 1 0 0 0 0.00 0.00 0 TITL 190225_sample2a in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 7.609974 11.009382 10.875369 90.0000 98.3157 90.0000 ZERR 2.00 0.000721 0.001362 0.001619 0.0000 0.0112 0.0000 LATT 1 SFAC C H N O UNIT 42.00 58.00 2.00 10.00 TREF HKLF 4 END ; _shelx_hkl_checksum 98320 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.4246(4) 0.9480(4) 0.2659(4) 0.0381(10) Uani 1 1 d . . . . . O2 O 0.9271(4) 0.5513(4) 0.7690(3) 0.0356(9) Uani 1 1 d . . . . . C1 C 0.8396(6) 0.6462(5) 0.5302(5) 0.0338(12) Uani 1 1 d . . . . . H1 H 0.9041 0.5682 0.5529 0.041 Uiso 1 1 calc R U . . . O3 O 0.6230(5) 1.1212(4) 0.1838(4) 0.0420(10) Uani 1 1 d . . . . . O4 O 0.8073(5) 0.7130(4) 0.8472(4) 0.0419(10) Uani 1 1 d . . . . . C2 C 0.4398(6) 0.6437(6) 0.2020(5) 0.0363(13) Uani 1 1 d . . . . . H2 H 0.5127 0.7038 0.1619 0.044 Uiso 1 1 calc R U . . . O5 O 0.2806(5) 0.6213(4) 0.1176(4) 0.0401(10) Uani 1 1 d . . . . . H3 H 0.2219 0.6860 0.1052 0.060 Uiso 1 1 calc R U . . . C4 C 0.6728(6) 0.6194(5) 0.4388(5) 0.0338(12) Uani 1 1 d . . . . . H4 H 0.5978 0.5624 0.4809 0.041 Uiso 1 1 calc R U . . . N1 N 0.7873(5) 0.6988(5) 0.6422(4) 0.0366(11) Uani 1 1 d . . . . . C6 C 0.3959(6) 0.6984(5) 0.3202(5) 0.0351(13) Uani 1 1 d . . . . . H5 H 0.3290 0.6385 0.3636 0.042 Uiso 1 1 calc R U . . . H6 H 0.3190 0.7703 0.2997 0.042 Uiso 1 1 calc R U . . . C7 C 0.5137(6) 0.7826(5) 0.5279(5) 0.0345(13) Uani 1 1 d . . . . . H7 H 0.4357 0.7221 0.5609 0.041 Uiso 1 1 calc R U . . . H8 H 0.4453 0.8589 0.5112 0.041 Uiso 1 1 calc R U . . . C8 C 0.8960(7) 1.0218(5) 0.2791(5) 0.0359(13) Uani 1 1 d . . . . . H20 H 0.9693 1.0833 0.2516 0.043 Uiso 1 1 calc R U . . . C9 C 0.5492(7) 0.5313(6) 0.2310(5) 0.0377(13) Uani 1 1 d . . . . . H9 H 0.5840 0.4989 0.1534 0.045 Uiso 1 1 calc R U . . . H10 H 0.4772 0.4687 0.2666 0.045 Uiso 1 1 calc R U . . . C10 C 0.6746(6) 0.8059(6) 0.6257(6) 0.0380(13) Uani 1 1 d . . . . . H11 H 0.7430 0.8756 0.5994 0.046 Uiso 1 1 calc R U . . . H12 H 0.6344 0.8267 0.7056 0.046 Uiso 1 1 calc R U . . . C11 C 0.8654(8) 0.7703(7) 1.0562(6) 0.0467(15) Uani 1 1 d . . . . . H13 H 0.9065 0.7432 1.1416 0.070 Uiso 1 1 calc R U . . . H14 H 0.9436 0.8347 1.0332 0.070 Uiso 1 1 calc R U . . . H15 H 0.7438 0.8014 1.0504 0.070 Uiso 1 1 calc R U . . . C12 C 0.9621(6) 0.7319(6) 0.4689(5) 0.0359(13) Uani 1 1 d . . . . . H21 H 1.0476 0.7694 0.5349 0.043 Uiso 1 1 calc R U . . . H22 H 1.0310 0.6832 0.4164 0.043 Uiso 1 1 calc R U . . . C13 C 0.7167(6) 0.5573(6) 0.3235(5) 0.0361(13) Uani 1 1 d . . . . . H16 H 0.7792 0.4800 0.3476 0.043 Uiso 1 1 calc R U . . . H17 H 0.7976 0.6096 0.2829 0.043 Uiso 1 1 calc R U . . . C14 C 0.6083(6) 0.9337(6) 0.2878(5) 0.0346(13) Uani 1 1 d . . . . . C15 C 0.8670(6) 0.8313(5) 0.3902(5) 0.0332(12) Uani 1 1 d . . . . . C16 C 0.7122(6) 1.0275(5) 0.2486(5) 0.0356(13) Uani 1 1 d . . . . . C17 C 0.6800(6) 0.8350(5) 0.3560(5) 0.0318(12) Uani 1 1 d . . . . . C18 C 0.9694(6) 0.9256(6) 0.3497(5) 0.0391(14) Uani 1 1 d . . . . . H23 H 1.0947 0.9227 0.3721 0.047 Uiso 1 1 calc R U . . . C19 C 0.8475(6) 0.6462(6) 0.7522(5) 0.0362(13) Uani 1 1 d . . . . . C20 C 0.5652(6) 0.7366(5) 0.4078(5) 0.0349(13) Uani 1 1 d . . . . . C21 C 0.7239(8) 1.2236(6) 0.1520(6) 0.0443(14) Uani 1 1 d . . . . . H24 H 0.6440 1.2835 0.1061 0.066 Uiso 1 1 calc R U . . . H25 H 0.7852 1.2603 0.2280 0.066 Uiso 1 1 calc R U . . . H26 H 0.8115 1.1969 0.1000 0.066 Uiso 1 1 calc R U . . . C22 C 0.3418(7) 0.9521(6) 0.1400(6) 0.0422(14) Uani 1 1 d . . . . . H27 H 0.2134 0.9623 0.1373 0.063 Uiso 1 1 calc R U . . . H28 H 0.3895 1.0206 0.0971 0.063 Uiso 1 1 calc R U . . . H29 H 0.3657 0.8762 0.0989 0.063 Uiso 1 1 calc R U . . . C23 C 0.8691(7) 0.6660(6) 0.9702(5) 0.0402(14) Uani 1 1 d . . . . . H18 H 0.9912 0.6335 0.9747 0.048 Uiso 1 1 calc R U . . . H19 H 0.7904 0.6001 0.9920 0.048 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0090(16) 0.057(2) 0.047(2) 0.0127(19) 0.0019(14) -0.0002(16) O2 0.0172(16) 0.047(2) 0.041(2) 0.0066(18) 0.0000(14) -0.0003(17) C1 0.012(2) 0.045(3) 0.042(3) 0.009(2) -0.001(2) -0.001(2) O3 0.0195(17) 0.049(2) 0.056(2) 0.015(2) 0.0024(15) -0.0022(17) O4 0.0211(18) 0.067(3) 0.036(2) 0.0080(19) -0.0001(15) 0.0018(18) C2 0.016(2) 0.051(3) 0.040(3) 0.006(3) -0.004(2) -0.013(2) O5 0.0202(17) 0.052(2) 0.045(2) 0.0110(19) -0.0071(15) -0.0046(17) C4 0.013(2) 0.047(3) 0.040(3) 0.013(2) -0.0014(19) -0.006(2) N1 0.0155(19) 0.052(3) 0.041(3) 0.008(2) -0.0012(17) 0.0016(19) C6 0.015(2) 0.042(3) 0.047(3) 0.015(2) -0.001(2) -0.003(2) C7 0.011(2) 0.048(3) 0.042(3) 0.013(2) -0.0023(19) -0.001(2) C8 0.020(2) 0.037(3) 0.050(3) 0.005(2) 0.006(2) -0.008(2) C9 0.018(2) 0.048(3) 0.045(3) 0.006(3) -0.002(2) -0.003(2) C10 0.016(2) 0.056(4) 0.041(3) 0.010(3) -0.0014(19) 0.001(2) C11 0.028(3) 0.071(4) 0.040(3) 0.006(3) 0.003(2) -0.005(3) C12 0.010(2) 0.056(3) 0.040(3) 0.006(3) -0.0008(19) -0.006(2) C13 0.014(2) 0.053(3) 0.041(3) 0.008(3) 0.002(2) 0.001(2) C14 0.008(2) 0.050(3) 0.044(3) 0.008(2) -0.0006(19) -0.002(2) C15 0.013(2) 0.048(3) 0.038(3) 0.005(2) 0.0000(19) -0.004(2) C16 0.017(2) 0.047(3) 0.041(3) 0.008(3) 0.001(2) -0.001(2) C17 0.011(2) 0.045(3) 0.038(3) 0.009(2) 0.0016(18) -0.004(2) C18 0.013(2) 0.062(4) 0.041(3) 0.012(3) 0.0011(19) -0.007(2) C19 0.0103(19) 0.056(4) 0.041(3) 0.005(3) 0.0015(19) -0.008(2) C20 0.013(2) 0.046(3) 0.044(3) 0.014(2) 0.001(2) -0.005(2) C21 0.029(3) 0.052(4) 0.052(4) 0.012(3) 0.006(2) -0.005(3) C22 0.020(2) 0.058(4) 0.047(3) 0.013(3) -0.002(2) 0.000(2) C23 0.025(3) 0.056(4) 0.037(3) 0.009(3) -0.002(2) 0.000(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C14 O1 C22 117.5(4) . . ? N1 C1 C4 108.9(4) . . ? N1 C1 C12 111.7(5) . . ? C4 C1 C12 109.7(4) . . ? C16 O3 C21 118.0(4) . . ? C19 O4 C23 116.0(5) . . ? O5 C2 C9 112.4(5) . . ? O5 C2 C6 110.4(4) . . ? C9 C2 C6 109.9(4) . . ? C13 C4 C1 111.7(4) . . ? C13 C4 C20 112.2(4) . . ? C1 C4 C20 110.1(5) . . ? C19 N1 C10 124.9(5) . . ? C19 N1 C1 118.2(5) . . ? C10 N1 C1 116.9(4) . . ? C2 C6 C20 111.8(4) . . ? C20 C7 C10 112.4(4) . . ? C18 C8 C16 118.7(5) . . ? C2 C9 C13 111.3(5) . . ? N1 C10 C7 110.1(5) . . ? C15 C12 C1 114.5(4) . . ? C4 C13 C9 111.8(4) . . ? C17 C14 O1 119.3(4) . . ? C17 C14 C16 122.9(4) . . ? O1 C14 C16 117.6(5) . . ? C18 C15 C17 118.7(5) . . ? C18 C15 C12 117.9(4) . . ? C17 C15 C12 123.4(5) . . ? O3 C16 C8 124.2(5) . . ? O3 C16 C14 116.6(4) . . ? C8 C16 C14 119.2(5) . . ? C14 C17 C15 117.8(5) . . ? C14 C17 C20 122.9(4) . . ? C15 C17 C20 119.0(5) . . ? C8 C18 C15 122.8(4) . . ? O2 C19 N1 126.9(6) . . ? O2 C19 O4 121.8(5) . . ? N1 C19 O4 111.3(5) . . ? C7 C20 C4 107.1(4) . . ? C7 C20 C17 107.9(5) . . ? C4 C20 C17 110.7(4) . . ? C7 C20 C6 109.3(4) . . ? C4 C20 C6 105.8(5) . . ? C17 C20 C6 115.7(4) . . ? O4 C23 C11 106.1(5) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C14 1.392(5) . ? O1 C22 1.423(7) . ? O2 C19 1.207(8) . ? C1 N1 1.459(7) . ? C1 C4 1.526(6) . ? C1 C12 1.540(7) . ? O3 C16 1.367(7) . ? O3 C21 1.432(7) . ? O4 C19 1.344(7) . ? O4 C23 1.444(7) . ? C2 O5 1.434(6) . ? C2 C9 1.497(8) . ? C2 C6 1.505(8) . ? C4 C13 1.512(8) . ? C4 C20 1.536(8) . ? N1 C19 1.344(7) . ? N1 C10 1.453(8) . ? C6 C20 1.548(7) . ? C7 C20 1.508(8) . ? C7 C10 1.525(7) . ? C8 C18 1.374(8) . ? C8 C16 1.392(7) . ? C9 C13 1.534(7) . ? C11 C23 1.490(10) . ? C12 C15 1.503(8) . ? C14 C17 1.378(8) . ? C14 C16 1.401(8) . ? C15 C18 1.403(8) . ? C15 C17 1.418(6) . ? C17 C20 1.544(7) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C1 C4 C13 -176.4(4) . . . . ? C12 C1 C4 C13 61.1(6) . . . . ? N1 C1 C4 C20 58.3(5) . . . . ? C12 C1 C4 C20 -64.2(6) . . . . ? C4 C1 N1 C19 125.8(5) . . . . ? C12 C1 N1 C19 -112.9(5) . . . . ? C4 C1 N1 C10 -54.8(6) . . . . ? C12 C1 N1 C10 66.5(5) . . . . ? O5 C2 C6 C20 -173.9(4) . . . . ? C9 C2 C6 C20 61.6(5) . . . . ? O5 C2 C9 C13 -178.8(4) . . . . ? C6 C2 C9 C13 -55.4(6) . . . . ? C19 N1 C10 C7 -129.1(5) . . . . ? C1 N1 C10 C7 51.5(6) . . . . ? C20 C7 C10 N1 -52.7(6) . . . . ? N1 C1 C12 C15 -80.6(5) . . . . ? C4 C1 C12 C15 40.2(7) . . . . ? C1 C4 C13 C9 -179.5(5) . . . . ? C20 C4 C13 C9 -55.4(6) . . . . ? C2 C9 C13 C4 53.0(6) . . . . ? C22 O1 C14 C17 -120.9(6) . . . . ? C22 O1 C14 C16 65.0(7) . . . . ? C1 C12 C15 C18 168.7(5) . . . . ? C1 C12 C15 C17 -10.8(8) . . . . ? C21 O3 C16 C8 -4.0(9) . . . . ? C21 O3 C16 C14 174.6(5) . . . . ? C18 C8 C16 O3 176.9(5) . . . . ? C18 C8 C16 C14 -1.7(9) . . . . ? C17 C14 C16 O3 -178.6(5) . . . . ? O1 C14 C16 O3 -4.7(8) . . . . ? C17 C14 C16 C8 0.1(9) . . . . ? O1 C14 C16 C8 174.0(5) . . . . ? O1 C14 C17 C15 -172.0(5) . . . . ? C16 C14 C17 C15 1.8(9) . . . . ? O1 C14 C17 C20 1.4(9) . . . . ? C16 C14 C17 C20 175.2(6) . . . . ? C18 C15 C17 C14 -2.0(9) . . . . ? C12 C15 C17 C14 177.4(5) . . . . ? C18 C15 C17 C20 -175.7(5) . . . . ? C12 C15 C17 C20 3.7(9) . . . . ? C16 C8 C18 C15 1.4(9) . . . . ? C17 C15 C18 C8 0.5(9) . . . . ? C12 C15 C18 C8 -179.0(6) . . . . ? C10 N1 C19 O2 172.5(5) . . . . ? C1 N1 C19 O2 -8.2(7) . . . . ? C10 N1 C19 O4 -7.1(7) . . . . ? C1 N1 C19 O4 172.2(4) . . . . ? C23 O4 C19 O2 1.6(7) . . . . ? C23 O4 C19 N1 -178.8(4) . . . . ? C10 C7 C20 C4 58.1(5) . . . . ? C10 C7 C20 C17 -61.1(6) . . . . ? C10 C7 C20 C6 172.3(5) . . . . ? C13 C4 C20 C7 174.2(4) . . . . ? C1 C4 C20 C7 -60.8(5) . . . . ? C13 C4 C20 C17 -68.5(5) . . . . ? C1 C4 C20 C17 56.6(6) . . . . ? C13 C4 C20 C6 57.6(5) . . . . ? C1 C4 C20 C6 -177.4(4) . . . . ? C14 C17 C20 C7 -82.7(6) . . . . ? C15 C17 C20 C7 90.6(6) . . . . ? C14 C17 C20 C4 160.4(5) . . . . ? C15 C17 C20 C4 -26.3(7) . . . . ? C14 C17 C20 C6 40.1(8) . . . . ? C15 C17 C20 C6 -146.6(6) . . . . ? C2 C6 C20 C7 -176.1(4) . . . . ? C2 C6 C20 C4 -61.1(5) . . . . ? C2 C6 C20 C17 61.9(6) . . . . ? C19 O4 C23 C11 161.3(4) . . . . ?