#------------------------------------------------------------------------------ #$Date: 2024-10-23 01:09:40 +0300 (Wed, 23 Oct 2024) $ #$Revision: 295580 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/29/1572918.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1572918 loop_ _publ_author_name 'Li, Can' 'Zhou, Wei' 'Liu, Zhaoxin' 'Gao, Rong' 'Mi, Qixi' 'Ning, Zhijun' 'Ren, Yi' _publ_section_title ; Non-innocent P-centers in nonbenzenoid polycyclic aromatic molecules with tunable structures and properties ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC05857G _journal_year 2024 _chemical_formula_moiety 'C38 H21 N2 O P S' _chemical_formula_sum 'C38 H21 N2 O P S' _chemical_formula_weight 584.60 _chemical_name_systematic ThBz-CPC-Ox _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2023-02-10 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _audit_update_record ; 2024-08-23 deposited with the CCDC. 2024-10-07 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 99.2710(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.0774(2) _cell_length_b 18.4805(5) _cell_length_c 17.7635(5) _cell_measurement_reflns_used 9859 _cell_measurement_temperature 150.00 _cell_measurement_theta_max 56.95 _cell_measurement_theta_min 4.71 _cell_volume 2617.00(12) _computing_cell_refinement 'SAINT V8.40A (Bruker, 2019)' _computing_data_reduction 'SAINT V8.40A (Bruker, 2019)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 150.00 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34138 _diffrn_reflns_av_R_equivalents 0.0515 _diffrn_reflns_av_unetI/netI 0.0325 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 32351 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 57.006 _diffrn_reflns_theta_min 4.162 _diffrn_source_current 2.5 _diffrn_source_power 0.17465 _diffrn_source_voltage 69.86 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.292 _exptl_absorpt_correction_T_max 0.7512 _exptl_absorpt_correction_T_min 0.6182 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1428 before and 0.0552 after correction. The Ratio of minimum to maximum transmission is 0.8229. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'metallic blackish' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier blackish _exptl_crystal_density_diffrn 1.484 _exptl_crystal_description block _exptl_crystal_F_000 1208 _exptl_crystal_preparation yellow _exptl_crystal_recrystallization_method transparent _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.292 _refine_diff_density_min -0.345 _refine_diff_density_rms 0.044 _refine_ls_extinction_coef 0.0010(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 405 _refine_ls_number_reflns 5338 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.035 _refine_ls_R_factor_all 0.0402 _refine_ls_R_factor_gt 0.0336 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0403P)^2^+1.1885P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0851 _refine_ls_wR_factor_ref 0.0880 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4718 _reflns_number_total 5338 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc05857g2.cif _cod_data_source_block thbz_cpc_ox_2_0m _cod_database_code 1572918 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Restrained distances H13-H4 2.2 with sigma of 0.01 H23-H29 2.2 with sigma of 0.01 2.a Aromatic/amide H refined with riding coordinates: C34(H34), C35(H35), C16(H16), C21(H21), C38(H38), C36(H36), C1(H1), C22(H22), C32(H32), C2(H2), C14(H14), C20(H20), C3(H3), C15(H15), C30(H30), C31(H31), C37(H37) ; _shelx_res_file ; TITL thbz_cpc_ox_2_0m_a.res in P2(1)/c thbz_cpc_ox_2_0m.res created by SHELXL-2018/3 at 14:35:56 on 10-Feb-2023 REM Old TITL ThBz_CPC_OX_2_0m in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.094, Rweak 0.005, Alpha 0.029 REM 0.912 for 184 systematic absences, Orientation as input REM Formula found by SHELXT: C38 N2 O P S CELL 1.34138 8.0774 18.4805 17.7635 90 99.271 90 ZERR 4 0.0002 0.0005 0.0005 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O P S DISP C 0.0137 0.0067 57.1 DISP H 0 0 0.6 DISP N 0.0241 0.0134 109.9 DISP O 0.0389 0.0241 193.4 DISP P 0.2543 0.3332 2560.5 DISP S 0.2925 0.4295 3294.4 UNIT 152 84 8 4 4 4 DFIX 2.2 0.01 H13 H4 DFIX 2.2 0.01 H23 H29 L.S. 4 0 0 PLAN 5 TEMP -123.15 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta OMIT -2 2 1 REM REM REM WGHT 0.040300 1.188500 EXTI 0.000998 FVAR 0.46829 S1 6 0.231442 0.568040 0.570991 11.00000 0.02689 0.02256 = 0.02633 -0.00247 0.00410 0.00192 P1 5 0.397395 0.298151 0.416419 11.00000 0.01581 0.02204 = 0.02541 -0.00261 0.00255 0.00080 O1 4 0.526250 0.260252 0.379820 11.00000 0.01992 0.02997 = 0.03246 -0.00451 0.00582 0.00331 N1 3 0.506464 0.361431 0.635633 11.00000 0.01962 0.02302 = 0.02429 0.00110 0.00062 -0.00112 N2 3 0.169922 0.480794 0.333113 11.00000 0.02095 0.02361 = 0.02363 -0.00013 0.00221 -0.00083 C12 1 0.597046 0.296151 0.637746 11.00000 0.01864 0.02360 = 0.03027 0.00227 0.00268 -0.00186 C11 1 0.572896 0.268016 0.563083 11.00000 0.01647 0.02408 = 0.03082 0.00136 0.00179 -0.00259 C33 1 0.215831 0.239889 0.415139 11.00000 0.01895 0.02665 = 0.02181 -0.00436 0.00252 -0.00034 C25 1 0.251888 0.439887 0.395037 11.00000 0.01557 0.02320 = 0.02519 0.00161 0.00205 -0.00221 C17 1 0.263501 0.469674 0.470267 11.00000 0.01655 0.02187 = 0.02547 0.00010 0.00360 -0.00098 C6 1 0.404442 0.474652 0.679237 11.00000 0.01898 0.02622 = 0.02581 -0.00165 0.00407 -0.00518 C7 1 0.338166 0.489584 0.601007 11.00000 0.01870 0.02166 = 0.02782 -0.00081 0.00456 -0.00166 C34 1 0.051797 0.265562 0.399974 11.00000 0.02047 0.03087 = 0.02874 -0.00482 0.00296 0.00114 AFIX 43 H34 2 0.032050 0.315485 0.389358 11.00000 -1.20000 AFIX 0 C28 1 0.187960 0.444284 0.265691 11.00000 0.02115 0.02635 = 0.02525 -0.00181 0.00291 -0.00439 C10 1 0.468287 0.317638 0.514079 11.00000 0.01737 0.02222 = 0.02733 -0.00012 0.00133 -0.00114 C8 1 0.345453 0.441535 0.542418 11.00000 0.01599 0.02267 = 0.02482 -0.00057 0.00344 -0.00290 C35 1 -0.083091 0.219226 0.400162 11.00000 0.01829 0.04634 = 0.03268 -0.00721 0.00375 -0.00131 AFIX 43 H35 2 -0.194443 0.237483 0.390557 11.00000 -1.20000 AFIX 0 C24 1 0.087415 0.546824 0.342290 11.00000 0.01795 0.02343 = 0.02982 0.00289 0.00505 -0.00166 C13 1 0.704760 0.262025 0.696733 11.00000 0.02545 0.03328 = 0.03047 0.00420 -0.00099 -0.00164 C16 1 0.653599 0.203644 0.547711 11.00000 0.02137 0.02591 = 0.03632 0.00031 0.00363 0.00000 AFIX 43 H16 2 0.637563 0.183882 0.497694 11.00000 -1.20000 AFIX 0 C9 1 0.432957 0.374447 0.559513 11.00000 0.01568 0.02369 = 0.02443 -0.00064 0.00185 -0.00328 C21 1 -0.064237 0.679370 0.365614 11.00000 0.02984 0.02553 = 0.04346 0.00708 0.00875 0.00605 AFIX 43 H21 2 -0.113048 0.725078 0.372952 11.00000 -1.20000 AFIX 0 C38 1 0.241195 0.166196 0.429405 11.00000 0.02266 0.02828 = 0.03256 -0.00167 0.00038 -0.00072 AFIX 43 H38 2 0.352255 0.147683 0.439788 11.00000 -1.20000 AFIX 0 C36 1 -0.054976 0.146444 0.414361 11.00000 0.02724 0.04242 = 0.02993 -0.00704 0.00642 -0.01388 AFIX 43 H36 2 -0.147321 0.114600 0.414315 11.00000 -1.20000 AFIX 0 C5 1 0.483191 0.407234 0.696590 11.00000 0.01925 0.02664 = 0.02586 -0.00082 0.00270 -0.00598 C27 1 0.275896 0.379639 0.286341 11.00000 0.02044 0.02554 = 0.02655 -0.00165 0.00353 -0.00421 C1 1 0.384330 0.522634 0.738295 11.00000 0.02510 0.02890 = 0.03094 -0.00379 0.00497 -0.00327 AFIX 43 H1 2 0.334918 0.568724 0.726352 11.00000 -1.20000 AFIX 0 C19 1 0.105783 0.577388 0.415660 11.00000 0.01958 0.02337 = 0.02843 0.00294 0.00517 -0.00121 C22 1 -0.087574 0.647545 0.294131 11.00000 0.02475 0.03356 = 0.03745 0.01093 0.00367 0.00372 AFIX 43 H22 2 -0.155164 0.671141 0.252609 11.00000 -1.20000 AFIX 0 C26 1 0.314898 0.377196 0.368127 11.00000 0.01834 0.02529 = 0.02557 -0.00148 0.00297 -0.00084 C32 1 0.318426 0.333021 0.229726 11.00000 0.02863 0.02705 = 0.03049 -0.00424 0.00675 -0.00485 AFIX 43 H32 2 0.377193 0.289194 0.243283 11.00000 -1.20000 AFIX 0 C18 1 0.196596 0.537347 0.478043 11.00000 0.02010 0.02363 = 0.02673 -0.00139 0.00490 -0.00157 C23 1 -0.014113 0.582141 0.282422 11.00000 0.02550 0.03235 = 0.02875 0.00479 0.00133 -0.00071 C2 1 0.435372 0.503655 0.813257 11.00000 0.03009 0.03868 = 0.02780 -0.00675 0.00541 -0.00529 AFIX 43 H2 2 0.423614 0.536658 0.853058 11.00000 -1.20000 AFIX 0 C29 1 0.143944 0.463371 0.188933 11.00000 0.03225 0.03351 = 0.02753 0.00279 0.00090 -0.00108 C4 1 0.527355 0.387489 0.773007 11.00000 0.02615 0.03153 = 0.02848 0.00363 0.00185 -0.00379 C14 1 0.782488 0.198912 0.679906 11.00000 0.02735 0.03274 = 0.04035 0.01064 -0.00143 0.00383 AFIX 43 H14 2 0.855492 0.174804 0.719278 11.00000 -1.20000 AFIX 0 C20 1 0.030422 0.644083 0.425920 11.00000 0.02904 0.02626 = 0.03455 0.00189 0.00812 0.00229 AFIX 43 H20 2 0.044833 0.665310 0.475252 11.00000 -1.20000 AFIX 0 C3 1 0.504395 0.435548 0.830028 11.00000 0.02898 0.04264 = 0.02419 0.00103 0.00235 -0.00598 AFIX 43 H3 2 0.536512 0.421714 0.881830 11.00000 -1.20000 AFIX 0 C15 1 0.756691 0.169652 0.606718 11.00000 0.02543 0.02657 = 0.04503 0.00433 0.00359 0.00478 AFIX 43 H15 2 0.810772 0.125697 0.597264 11.00000 -1.20000 AFIX 0 C30 1 0.186730 0.416562 0.134502 11.00000 0.03880 0.03839 = 0.02487 -0.00104 0.00317 -0.00639 AFIX 43 H30 2 0.156473 0.428506 0.082072 11.00000 -1.20000 AFIX 0 C31 1 0.273242 0.352184 0.154507 11.00000 0.03417 0.03367 = 0.02874 -0.00762 0.00885 -0.00931 AFIX 43 H31 2 0.301149 0.321305 0.115671 11.00000 -1.20000 AFIX 0 C37 1 0.106692 0.119680 0.428633 11.00000 0.03687 0.02855 = 0.03043 -0.00212 0.00298 -0.00575 AFIX 43 H37 2 0.125495 0.069487 0.437892 11.00000 -1.20000 AFIX 0 H13 2 0.739822 0.279726 0.743829 11.00000 0.03265 H4 2 0.557920 0.345422 0.789852 11.00000 0.03150 H23 2 -0.047426 0.564884 0.238675 11.00000 0.04200 H29 2 0.099351 0.504161 0.169269 11.00000 0.04252 HKLF 4 REM thbz_cpc_ox_2_0m_a.res in P2(1)/c REM wR2 = 0.0880, GooF = S = 1.032, Restrained GooF = 1.035 for all data REM R1 = 0.0336 for 4718 Fo > 4sig(Fo) and 0.0402 for all 5338 data REM 405 parameters refined using 2 restraints END WGHT 0.0405 1.1872 REM Highest difference peak 0.292, deepest hole -0.345, 1-sigma level 0.044 Q1 1 0.4439 0.3202 0.4678 11.00000 0.05 0.29 Q2 1 0.3494 0.3438 0.3879 11.00000 0.05 0.25 Q3 1 0.5794 0.2792 0.5993 11.00000 0.05 0.24 Q4 1 0.1716 0.5461 0.5181 11.00000 0.05 0.24 Q5 1 0.2780 0.5186 0.5938 11.00000 0.05 0.23 ; _shelx_res_checksum 28268 _shelx_hkl_file ; 2 0 0 58.59 3.00 2 0 0 60.49 2.90 2 0 0 59.09 2.70 2 0 0 57.29 2.90 5 0 0 29.70 2.50 5 0 0 34.40 4.30 5 0 0 30.70 1.90 5 0 0 31.20 2.60 6 0 0 554.54 23.40 6 0 0 539.75 23.50 6 0 0 447.56 22.60 6 0 0 510.45 21.90 6 0 0 508.55 22.90 7 0 0 315.97 16.30 7 0 0 354.66 17.10 7 0 0 342.07 16.50 7 0 0 358.66 17.20 8 0 0 26.70 4.10 8 0 0 20.80 3.50 8 0 0 34.50 4.90 8 0 0 24.40 3.80 9 0 0 17.90 5.90 9 0 0 7.50 3.40 9 0 0 7.80 2.80 0 -1 0 1.10 0.40 0 -1 0 1.80 0.90 0 -1 0 1.20 0.30 0 -1 0 1.60 0.20 0 1 0 0.90 0.10 0 1 0 0.90 0.70 0 1 0 2.00 0.50 -1 -1 0 553.44 24.40 1 -1 0 591.24 24.30 1 1 0 594.34 24.40 -1 1 0 578.74 24.30 2 -1 0 23.00 1.40 -2 -1 0 28.60 3.80 2 -1 0 21.90 1.40 2 -1 0 25.80 1.60 2 -1 0 22.70 1.20 2 1 0 29.30 4.90 2 1 0 21.50 1.60 2 1 0 21.60 1.50 2 1 0 22.70 1.50 2 1 0 22.50 1.20 2 1 0 21.60 1.70 2 1 0 24.40 1.80 3 -1 0 10.90 1.10 3 -1 0 16.40 1.40 3 -1 0 13.00 1.20 3 -1 0 13.30 0.90 3 -1 0 15.00 1.30 3 1 0 13.40 1.10 3 1 0 11.80 0.90 3 1 0 13.90 1.50 3 1 0 11.10 1.20 3 1 0 11.30 1.10 3 1 0 11.00 1.20 3 1 0 11.90 1.20 4 -1 0 62.19 3.60 4 -1 0 60.09 3.10 4 -1 0 60.29 3.50 4 -1 0 62.39 3.60 4 -1 0 62.49 3.60 4 1 0 63.49 3.50 4 1 0 61.49 3.70 4 1 0 59.99 3.60 4 1 0 62.79 3.60 4 1 0 61.79 3.00 5 -1 0 51.89 2.90 5 -1 0 50.89 3.60 5 -1 0 54.39 3.50 5 -1 0 48.50 3.50 5 -1 0 62.69 5.20 5 1 0 51.99 3.50 5 1 0 54.49 2.80 5 1 0 54.19 3.80 5 1 0 54.49 4.20 5 1 0 50.79 3.40 6 -1 0 8.70 1.80 6 -1 0 11.00 2.00 6 -1 0 11.80 1.30 6 -1 0 14.20 2.40 6 -1 0 11.50 2.40 6 1 0 11.60 2.10 6 1 0 11.30 1.30 6 1 0 11.30 2.20 6 1 0 12.20 2.10 6 1 0 13.00 2.10 7 -1 0 25.30 3.70 7 -1 0 25.80 3.40 7 -1 0 29.40 3.80 7 -1 0 39.30 4.70 7 -1 0 28.80 2.40 7 1 0 32.40 4.10 7 1 0 34.20 4.30 7 1 0 32.30 2.40 7 1 0 33.00 3.90 7 1 0 36.30 4.20 8 -1 0 148.19 9.40 8 -1 0 155.08 9.90 8 -1 0 169.68 10.60 8 -1 0 167.98 10.10 8 1 0 154.68 9.50 8 1 0 178.58 10.10 8 1 0 180.08 10.50 8 1 0 164.28 10.40 9 -1 0 21.00 4.40 9 1 0 31.50 5.40 9 1 0 22.90 4.80 9 1 0 26.00 4.70 0 -2 0 5.90 1.10 0 -2 0 4.10 0.30 0 -2 0 4.70 0.30 0 -2 0 5.70 2.20 0 2 0 3.50 1.50 0 2 0 6.80 0.90 0 2 0 5.50 0.50 0 2 0 8.00 1.20 0 2 0 4.00 0.30 1 -2 0 481.15 22.50 1 -2 0 441.56 19.70 -1 -2 0 488.25 23.50 1 2 0 392.06 19.10 1 2 0 477.45 19.80 -1 2 0 471.35 22.60 1 2 0 505.65 24.10 -1 2 0 450.25 19.80 2 -2 0 1380.36 58.39 2 2 0 1421.46 58.69 -3 -2 0 745.53 33.40 3 2 0 688.23 29.60 3 2 0 650.03 35.00 4 -2 0 12.00 1.70 4 -2 0 10.90 1.50 4 -2 0 10.60 1.40 4 -2 0 13.60 1.70 4 -2 0 9.30 1.00 4 2 0 9.40 1.50 4 2 0 6.80 1.20 4 2 0 10.50 1.60 4 2 0 10.00 1.40 4 2 0 8.70 1.00 5 -2 0 19.50 2.00 5 -2 0 24.00 2.50 5 -2 0 24.00 3.10 5 -2 0 19.80 2.00 5 2 0 19.50 2.40 5 2 0 19.40 1.40 5 2 0 20.30 2.10 -5 2 0 25.50 1.80 5 2 0 21.20 2.70 5 2 0 19.40 2.00 6 -2 0 194.68 10.20 6 -2 0 203.38 9.10 6 -2 0 211.08 10.20 6 -2 0 184.28 10.00 6 -2 0 185.88 9.90 6 2 0 189.48 8.90 6 2 0 207.08 10.70 6 2 0 189.48 9.70 6 2 0 201.98 10.50 6 2 0 196.58 10.00 7 -2 0 2.50 1.00 7 -2 0 1.70 2.10 7 -2 0 0.70 1.10 7 -2 0 1.20 2.70 7 -2 0 0.10 1.00 7 2 0 0.10 1.20 7 2 0 -0.30 1.10 7 2 0 1.10 2.00 7 2 0 3.20 1.00 7 2 0 4.90 2.30 8 -2 0 40.30 3.20 8 -2 0 37.40 4.80 8 -2 0 36.50 4.00 8 -2 0 36.70 4.80 8 -2 0 36.20 5.60 8 2 0 44.20 5.10 8 2 0 36.50 4.60 8 2 0 37.50 4.90 8 2 0 36.70 5.20 9 -2 0 55.39 10.10 9 -2 0 45.00 6.50 9 2 0 41.50 7.20 9 2 0 54.49 6.20 0 -3 0 -0.10 0.10 0 -3 0 2.00 2.30 0 -3 0 0.30 0.20 0 3 0 0.00 1.60 0 3 0 0.30 0.50 0 3 0 0.50 0.40 0 3 0 1.10 1.30 -1 -3 0 1397.66 63.19 1 3 0 1596.14 63.19 -1 3 0 1511.05 63.19 -2 -3 0 623.24 30.40 2 -3 0 529.25 24.20 2 -3 0 576.74 28.10 -2 3 0 540.75 23.50 2 3 0 573.84 24.50 -2 3 0 609.24 29.10 -2 3 0 512.95 24.50 2 3 0 576.54 31.30 3 -3 0 10.60 1.50 3 -3 0 9.40 1.10 3 -3 0 11.30 1.80 -3 -3 0 11.60 3.80 3 -3 0 11.50 3.00 3 -3 0 10.30 1.20 3 -3 0 9.30 1.20 3 -3 0 11.30 1.40 3 3 0 11.00 1.50 3 3 0 9.30 1.80 3 3 0 10.90 1.70 3 3 0 8.80 4.60 3 3 0 13.30 1.80 3 3 0 9.10 0.70 3 3 0 10.80 1.30 -3 3 0 16.80 3.80 4 -3 0 16.80 1.60 4 -3 0 18.50 1.60 4 -3 0 18.30 2.10 4 -3 0 18.70 2.20 4 -3 0 17.40 1.30 4 3 0 19.60 2.20 4 3 0 16.30 1.60 4 3 0 16.90 1.80 4 3 0 14.60 1.90 4 3 0 14.60 1.90 -4 3 0 18.50 1.50 4 3 0 15.00 1.10 5 -3 0 121.29 6.70 5 -3 0 119.49 6.60 5 -3 0 124.99 6.40 5 -3 0 122.29 6.50 5 -3 0 131.29 5.90 5 3 0 122.39 6.60 -5 3 0 120.79 6.30 5 3 0 124.79 7.10 5 3 0 120.19 5.60 5 3 0 117.09 6.30 6 -3 0 514.05 24.70 6 -3 0 568.34 23.80 6 -3 0 546.05 24.80 6 -3 0 551.14 24.90 6 -3 0 600.74 25.00 6 3 0 574.24 25.80 6 3 0 542.15 24.80 6 3 0 533.75 23.50 6 3 0 546.75 24.50 7 -3 0 223.18 11.70 7 -3 0 193.68 11.40 7 -3 0 236.38 12.40 7 -3 0 242.68 10.60 7 -3 0 227.88 11.90 7 3 0 217.68 11.50 7 3 0 231.78 12.80 7 3 0 226.18 12.50 7 3 0 214.68 11.30 8 -3 0 43.70 3.50 8 -3 0 38.50 4.90 8 -3 0 37.90 7.30 8 -3 0 34.30 5.30 8 3 0 39.10 4.70 8 3 0 37.00 6.90 8 3 0 40.70 7.20 8 3 0 41.30 4.90 9 -3 0 4.00 2.20 9 -3 0 0.60 1.90 9 3 0 8.70 3.90 0 -4 0 119.59 5.00 0 -4 0 114.79 5.10 0 -4 0 133.99 11.20 0 -4 0 114.79 6.70 0 4 0 125.99 6.80 0 4 0 122.19 5.80 0 4 0 118.39 5.30 0 4 0 106.79 11.10 -1 -4 0 662.33 34.90 1 -4 0 664.83 34.00 -1 4 0 627.14 27.30 -1 4 0 621.74 28.50 1 4 0 687.73 36.10 1 4 0 660.93 28.90 -1 4 0 673.93 34.80 2 -4 0 193.78 8.20 2 -4 0 186.38 8.80 2 -4 0 199.98 8.80 -2 -4 0 203.68 15.30 2 -4 0 195.58 13.70 -2 -4 0 181.48 8.30 2 -4 0 188.98 9.40 2 -4 0 192.38 8.70 2 -4 0 188.68 8.60 2 -4 0 198.88 8.40 2 4 0 189.98 9.10 2 4 0 188.48 8.90 -2 4 0 233.08 15.40 2 4 0 194.58 8.40 -2 4 0 187.98 10.10 2 4 0 205.78 8.90 2 4 0 194.38 9.70 -2 4 0 191.48 8.40 -2 4 0 193.48 8.90 2 4 0 202.28 9.30 2 4 0 217.78 16.90 3 -4 0 2.50 1.30 3 -4 0 2.60 2.10 -3 -4 0 3.00 0.50 3 -4 0 4.30 1.30 -3 -4 0 1.60 2.50 3 -4 0 3.20 0.70 3 -4 0 4.20 1.30 3 -4 0 3.40 0.60 3 -4 0 2.60 0.70 3 4 0 6.20 1.80 3 4 0 2.40 1.00 3 4 0 2.50 0.40 3 4 0 4.00 1.00 3 4 0 3.40 0.70 -3 4 0 4.00 0.90 3 4 0 6.10 4.40 3 4 0 3.00 0.90 3 4 0 3.90 1.10 -3 4 0 6.50 3.20 4 4 0 932.01 56.79 4 4 0 956.10 40.80 5 -4 0 792.52 33.80 5 4 0 743.63 32.90 5 4 0 806.22 34.60 5 4 0 809.92 35.00 -5 4 0 781.72 33.90 5 4 0 783.12 34.20 6 -4 0 26.70 2.70 6 -4 0 29.70 2.80 6 -4 0 27.40 4.10 6 -4 0 28.70 2.10 6 -4 0 27.30 3.50 6 4 0 27.70 2.80 6 4 0 26.60 2.60 6 4 0 27.00 3.50 6 4 0 29.30 3.60 7 -4 0 1.20 1.20 7 -4 0 1.60 1.20 7 -4 0 5.90 3.70 7 -4 0 0.40 0.90 7 -4 0 0.60 2.60 7 4 0 0.00 1.00 7 4 0 1.90 1.80 7 4 0 1.60 1.70 7 4 0 2.60 1.70 8 -4 0 44.20 7.00 8 -4 0 40.10 4.40 8 -4 0 44.10 3.80 8 4 0 34.90 5.40 9 -4 0 12.50 3.00 9 -4 0 11.10 2.90 9 4 0 14.10 4.20 0 -5 0 0.10 0.40 0 -5 0 4.20 3.50 0 -5 0 0.10 0.20 0 -5 0 2.90 2.70 0 5 0 0.30 0.60 0 5 0 0.30 2.10 0 5 0 -0.60 3.10 0 5 0 0.00 0.80 1 -5 0 617.14 28.70 1 -5 0 678.73 35.70 -1 -5 0 682.53 36.80 1 5 0 655.13 28.90 -1 5 0 685.63 36.90 -1 5 0 629.34 27.30 1 5 0 645.14 37.50 2 -5 0 340.87 21.30 -2 -5 0 359.16 23.20 2 -5 0 306.17 15.20 -2 -5 0 313.17 13.80 2 5 0 334.07 13.90 2 5 0 306.97 23.50 2 5 0 330.67 15.60 2 5 0 338.47 14.50 2 5 0 329.17 14.80 -2 5 0 329.07 14.60 -2 5 0 322.67 13.90 -2 5 0 339.47 22.60 2 5 0 313.77 14.50 3 -5 0 15.40 1.50 3 -5 0 18.30 4.90 3 -5 0 16.50 2.50 3 -5 0 19.10 2.10 3 -5 0 15.00 0.90 3 -5 0 15.10 1.20 -3 -5 0 13.60 1.00 3 -5 0 13.60 1.30 -3 -5 0 19.10 5.80 3 -5 0 15.40 2.00 3 5 0 17.90 2.20 3 5 0 15.00 1.30 -3 5 0 15.70 5.50 3 5 0 16.40 2.30 3 5 0 15.90 1.80 3 5 0 14.30 2.70 -3 5 0 15.30 1.70 3 5 0 19.40 7.50 3 5 0 17.00 2.00 4 -5 0 38.10 3.20 4 -5 0 38.50 3.30 4 -5 0 35.50 2.80 4 -5 0 40.30 2.60 -4 -5 0 49.99 9.10 4 -5 0 41.60 2.70 4 5 0 43.60 3.20 4 5 0 44.80 10.90 4 5 0 44.30 2.80 -4 5 0 38.80 2.90 4 5 0 39.90 3.80 4 5 0 40.40 3.40 4 5 0 35.40 2.00 4 5 0 39.60 3.10 5 -5 0 244.78 11.70 5 -5 0 243.48 11.40 5 -5 0 244.08 12.20 5 -5 0 234.18 11.80 5 -5 0 264.97 11.00 5 5 0 231.28 11.30 5 5 0 250.27 11.40 5 5 0 257.27 12.40 5 5 0 242.38 12.70 -5 5 0 248.68 11.80 5 5 0 243.98 11.50 5 5 0 230.18 11.80 6 -5 0 333.87 15.50 6 -5 0 319.77 15.20 6 -5 0 343.97 14.50 6 -5 0 331.67 16.10 6 -5 0 303.87 15.50 6 5 0 326.97 16.30 6 5 0 315.67 15.50 6 5 0 323.47 16.70 6 5 0 312.77 15.00 7 -5 0 113.39 7.20 7 -5 0 131.79 6.60 7 -5 0 125.19 7.60 7 -5 0 125.49 9.30 7 5 0 119.79 7.20 7 5 0 134.89 9.00 7 5 0 122.69 7.50 7 5 0 131.69 8.60 8 -5 0 220.98 10.20 8 -5 0 221.28 11.70 8 -5 0 189.08 11.20 8 5 0 202.68 11.10 8 5 0 189.88 10.90 8 5 0 215.58 12.70 9 -5 0 113.59 8.10 9 5 0 103.99 9.40 0 -6 0 18.50 4.40 0 -6 0 13.60 4.90 0 -6 0 14.60 0.80 0 -6 0 12.80 1.00 0 6 0 18.40 2.20 0 6 0 15.20 2.90 0 6 0 27.50 8.10 1 -6 0 50.89 5.20 1 -6 0 53.89 2.50 -1 -6 0 50.09 2.50 1 -6 0 73.19 11.80 1 -6 0 53.69 2.50 -1 -6 0 54.79 10.30 1 6 0 52.89 4.50 -1 6 0 55.19 11.10 1 6 0 53.49 3.50 1 6 0 50.59 3.20 1 6 0 39.00 8.40 -1 6 0 51.09 2.80 -1 6 0 53.69 3.40 -1 6 0 52.59 5.10 1 6 0 51.29 2.70 2 -6 0 -0.50 2.00 2 -6 0 1.90 0.40 2 -6 0 1.10 2.50 -2 -6 0 1.10 3.40 2 -6 0 1.60 0.40 -2 -6 0 1.30 0.40 2 -6 0 2.20 0.50 2 6 0 1.90 1.10 2 6 0 2.20 1.00 -2 6 0 0.30 3.20 2 6 0 -0.10 2.00 -2 6 0 0.70 0.80 -2 6 0 1.60 3.50 -2 6 0 1.30 0.70 -3 -6 0 746.23 33.40 3 -6 0 837.92 43.20 -3 -6 0 838.02 50.89 3 6 0 837.02 35.80 -3 6 0 814.32 45.50 3 6 0 737.13 54.39 4 -6 0 530.35 23.50 4 -6 0 517.45 23.20 -4 -6 0 525.15 33.20 4 -6 0 537.05 23.10 4 -6 0 537.05 22.70 4 -6 0 478.45 28.90 4 6 0 530.75 22.90 4 6 0 526.65 22.20 4 6 0 487.45 36.50 4 6 0 527.05 23.60 4 6 0 525.25 23.50 -4 6 0 540.25 23.40 -4 6 0 483.15 31.40 4 6 0 563.04 24.50 -5 -6 0 8.20 4.70 5 -6 0 8.60 1.50 5 -6 0 12.50 1.50 5 -6 0 13.50 1.80 5 -6 0 11.30 2.90 -5 6 0 10.50 1.90 5 6 0 8.00 2.00 5 6 0 9.10 1.80 5 6 0 9.70 1.90 5 6 0 9.70 2.10 6 -6 0 24.40 2.10 6 -6 0 25.10 4.40 6 -6 0 23.60 3.00 6 -6 0 23.30 2.40 6 6 0 30.40 3.70 6 6 0 22.40 2.40 6 6 0 24.60 3.80 7 -6 0 56.89 4.50 7 -6 0 55.09 3.60 7 -6 0 51.39 4.20 7 6 0 54.39 4.40 7 6 0 48.50 4.10 7 6 0 53.99 5.30 8 -6 0 21.10 3.20 8 -6 0 36.80 3.20 8 -6 0 21.80 3.40 8 6 0 28.70 4.80 8 6 0 24.90 3.90 8 6 0 25.40 3.50 9 -6 0 77.89 6.50 9 6 0 65.19 8.10 0 -7 0 0.70 0.40 0 -7 0 -1.10 1.70 0 -7 0 9.80 5.40 0 7 0 2.10 0.70 0 7 0 3.00 4.80 0 7 0 0.40 0.90 1 -7 0 118.89 5.30 -1 -7 0 117.59 13.70 -1 -7 0 115.29 5.20 1 -7 0 93.09 7.80 1 -7 0 119.19 5.10 1 7 0 115.99 6.40 -1 7 0 119.39 6.30 -1 7 0 115.39 14.30 1 7 0 120.49 7.60 1 7 0 116.19 14.80 1 7 0 119.99 5.50 -1 7 0 114.09 5.50 -1 7 0 121.99 8.10 -2 -7 0 334.27 25.60 -2 -7 0 320.57 14.10 2 -7 0 311.47 14.10 2 -7 0 343.07 14.00 2 -7 0 324.37 23.90 -2 7 0 335.67 14.30 -2 7 0 326.77 15.20 2 7 0 348.07 15.10 2 7 0 350.66 16.70 2 7 0 331.77 14.30 2 7 0 313.47 27.00 -2 7 0 292.97 17.10 2 7 0 352.86 15.90 -2 7 0 318.27 25.70 3 -7 0 146.29 6.50 -3 -7 0 136.59 6.40 3 -7 0 145.19 7.20 3 -7 0 138.09 6.60 3 -7 0 144.49 6.30 -3 -7 0 139.19 15.80 3 -7 0 139.59 14.10 3 -7 0 135.79 8.50 -3 7 0 153.88 7.70 3 7 0 148.79 7.60 -3 7 0 140.19 6.70 -3 7 0 136.09 15.90 3 7 0 143.89 7.70 3 7 0 142.19 6.60 3 7 0 152.68 9.10 3 7 0 145.59 7.30 3 7 0 159.68 19.20 4 -7 0 37.40 3.90 -4 -7 0 39.20 9.60 4 -7 0 42.50 2.60 4 -7 0 40.10 8.40 4 -7 0 41.20 3.80 4 -7 0 40.80 2.50 4 7 0 41.00 3.00 4 7 0 45.00 3.60 4 7 0 45.80 12.80 4 7 0 48.90 4.90 4 7 0 42.30 2.40 -4 7 0 42.90 3.40 -4 7 0 57.09 13.50 5 -7 0 3.00 0.80 5 -7 0 2.60 1.10 5 -7 0 1.90 0.90 5 -7 0 2.40 2.60 5 7 0 3.60 1.50 5 7 0 3.40 1.10 5 7 0 2.60 1.30 -5 7 0 3.70 1.30 5 7 0 4.30 2.30 6 -7 0 163.78 8.70 6 -7 0 154.68 8.20 6 -7 0 145.69 8.80 6 7 0 162.18 8.90 6 7 0 154.38 8.10 7 -7 0 11.30 2.20 7 -7 0 14.30 1.90 7 -7 0 14.40 2.70 7 7 0 13.40 2.60 7 7 0 15.80 2.50 7 7 0 10.40 3.10 8 -7 0 62.09 4.20 8 -7 0 53.69 4.80 8 7 0 49.40 6.50 8 7 0 55.29 4.70 9 -7 0 22.90 4.30 9 7 0 22.50 6.60 0 -8 0 428.66 31.00 0 -8 0 441.66 18.70 0 8 0 445.56 19.00 0 8 0 457.15 20.20 0 8 0 438.06 33.30 0 8 0 432.56 21.50 1 -8 0 205.08 8.70 1 -8 0 211.38 8.80 -1 -8 0 198.18 8.80 -1 -8 0 198.88 19.50 1 -8 0 181.68 12.80 1 -8 0 197.58 19.00 1 8 0 205.48 9.10 -1 8 0 213.28 10.30 1 8 0 197.88 11.60 1 8 0 218.78 22.10 1 8 0 210.28 10.40 -1 8 0 202.88 9.20 -1 8 0 209.38 21.10 -1 8 0 193.38 11.80 -2 -8 0 862.31 51.49 2 -8 0 865.71 49.70 2 8 0 857.21 39.10 -2 8 0 902.71 53.29 -2 8 0 888.01 36.50 -2 8 0 836.52 39.70 2 8 0 829.22 54.09 -2 8 0 864.71 37.60 3 -8 0 2.80 0.70 3 -8 0 2.70 0.60 3 -8 0 2.90 2.80 3 -8 0 0.40 1.00 -3 -8 0 7.30 0.90 3 -8 0 2.60 0.50 3 -8 0 5.50 3.10 -3 -8 0 3.40 3.40 3 8 0 1.40 1.10 3 8 0 2.00 1.10 3 8 0 1.40 2.40 -3 8 0 2.50 1.20 3 8 0 2.10 0.80 3 8 0 3.70 1.50 3 8 0 1.80 1.10 -3 8 0 4.00 1.00 3 8 0 -1.10 2.40 -3 8 0 6.30 5.00 4 -8 0 1.50 0.70 4 -8 0 0.20 2.20 4 -8 0 2.70 2.80 4 -8 0 0.80 0.50 4 -8 0 0.10 0.70 -4 -8 0 1.10 2.50 4 8 0 0.80 1.00 4 8 0 1.80 1.00 -4 8 0 4.80 4.80 4 8 0 3.90 4.20 -4 8 0 1.30 1.10 4 8 0 3.50 2.70 4 8 0 1.30 1.20 5 -8 0 493.45 22.90 5 -8 0 546.05 23.10 5 -8 0 548.65 23.90 5 8 0 562.34 24.60 5 8 0 521.35 23.50 5 8 0 534.55 25.00 6 -8 0 165.98 8.00 6 -8 0 158.78 8.40 6 -8 0 175.08 9.10 6 8 0 171.38 9.50 6 8 0 155.28 8.40 6 8 0 166.58 10.20 7 -8 0 270.17 11.90 7 -8 0 234.48 12.50 7 -8 0 274.77 13.30 7 8 0 228.48 12.10 7 8 0 252.47 13.20 7 8 0 247.08 14.50 8 -8 0 187.68 10.60 8 -8 0 183.38 9.20 8 8 0 170.08 10.20 8 8 0 205.48 13.00 9 -8 0 7.90 3.70 9 8 0 -6.30 6.20 0 -9 0 -1.00 2.90 0 -9 0 0.40 0.40 0 9 0 0.10 0.80 0 9 0 -1.20 0.90 0 9 0 0.20 2.70 0 9 0 2.10 3.80 1 -9 0 782.12 49.30 -1 -9 0 796.42 50.49 1 9 0 831.12 34.80 -1 9 0 812.92 37.90 1 9 0 868.71 38.00 1 9 0 776.62 52.79 -1 9 0 850.71 53.59 -1 9 0 818.12 36.10 2 -9 0 251.77 10.50 -2 -9 0 238.28 10.50 2 -9 0 233.18 26.50 2 -9 0 220.58 14.60 2 -9 0 240.28 10.40 -2 -9 0 219.88 27.70 -2 9 0 238.58 12.10 2 9 0 237.38 10.80 2 9 0 244.88 13.90 2 9 0 253.57 12.30 -2 9 0 251.07 10.90 2 9 0 228.48 11.70 2 9 0 235.08 27.00 -3 -9 0 867.71 53.69 3 -9 0 786.22 35.00 -3 -9 0 836.22 34.90 3 -9 0 780.92 37.80 3 -9 0 774.12 49.10 -3 9 0 830.02 35.30 -3 9 0 856.01 36.80 3 9 0 791.42 57.99 3 9 0 850.41 35.20 3 9 0 876.41 37.00 3 9 0 846.82 38.50 3 9 0 854.21 36.60 3 9 0 844.12 36.20 -3 9 0 810.72 53.69 4 -9 0 55.09 5.90 4 -9 0 54.79 3.90 4 -9 0 70.49 13.90 4 -9 0 54.29 3.20 4 -9 0 57.89 3.20 -4 9 0 69.89 16.50 -4 9 0 55.39 4.50 4 9 0 54.69 3.20 4 9 0 55.29 3.70 4 9 0 53.29 6.10 4 9 0 55.39 4.60 4 9 0 61.29 4.60 5 -9 0 12.30 1.50 5 -9 0 15.60 2.30 5 -9 0 10.40 2.20 5 -9 0 16.20 2.20 -5 9 0 16.30 2.50 5 9 0 15.30 2.70 5 9 0 14.10 3.90 5 9 0 15.10 2.10 5 9 0 12.00 2.70 6 -9 0 33.10 2.60 6 -9 0 36.50 3.40 6 -9 0 30.00 2.60 6 9 0 35.30 4.30 6 9 0 33.90 3.90 6 9 0 28.00 2.70 6 9 0 26.60 3.50 6 9 0 35.20 4.90 7 -9 0 110.89 7.10 7 -9 0 111.29 6.10 7 9 0 103.79 7.20 7 9 0 109.19 6.80 7 9 0 129.39 9.50 8 -9 0 72.99 5.70 8 9 0 94.79 10.00 8 9 0 64.69 5.50 9 -9 0 -0.30 3.40 0 -10 0 467.85 35.50 0 -10 0 435.36 19.20 0 10 0 449.36 19.60 0 10 0 457.15 37.90 0 10 0 459.65 23.20 0 10 0 451.55 21.20 -1 -10 0 879.41 55.99 1 -10 0 883.41 54.89 1 10 0 902.01 41.30 -1 10 0 892.41 43.50 -1 10 0 896.81 37.80 1 10 0 903.61 37.80 1 10 0 934.01 39.60 1 10 0 807.92 57.89 -1 10 0 840.82 57.79 -1 10 0 905.31 39.40 2 -10 0 271.97 11.80 -2 -10 0 269.57 11.90 2 -10 0 273.77 12.00 -2 -10 0 283.97 27.70 2 -10 0 265.57 25.00 -2 10 0 282.67 28.70 -2 10 0 259.97 12.20 2 10 0 264.67 12.20 -2 10 0 260.17 13.60 2 10 0 290.17 14.00 2 10 0 276.27 15.70 2 10 0 238.78 28.10 -2 10 0 287.77 18.10 -3 -10 0 80.09 17.40 3 -10 0 85.89 5.60 3 -10 0 87.59 9.70 3 -10 0 100.99 18.50 -3 -10 0 91.89 4.40 3 -10 0 89.09 4.20 3 -10 0 88.39 4.40 3 10 0 97.89 8.20 -3 10 0 93.59 19.00 3 10 0 89.09 6.30 3 10 0 88.89 6.10 -3 10 0 92.59 4.80 3 10 0 91.09 28.40 -3 10 0 89.19 6.10 3 10 0 85.29 4.70 3 10 0 86.59 5.50 4 -10 0 821.82 33.70 4 -10 0 729.93 36.20 4 -10 0 745.73 33.60 4 -10 0 697.03 48.50 4 10 0 793.72 33.80 -4 10 0 763.02 54.79 -4 10 0 819.92 35.80 4 10 0 869.01 35.80 4 10 0 823.72 37.80 4 10 0 818.62 35.40 4 10 0 800.52 35.70 5 -10 0 256.77 13.70 5 -10 0 298.97 13.90 5 -10 0 283.37 12.70 5 10 0 254.57 13.20 -5 10 0 297.27 14.70 5 10 0 281.27 15.10 5 10 0 289.47 14.60 5 10 0 306.37 16.50 6 -10 0 0.60 0.90 6 -10 0 2.60 1.10 6 10 0 4.90 3.00 6 10 0 1.00 1.00 6 10 0 -0.30 1.50 6 10 0 2.30 2.90 7 -10 0 71.89 4.50 7 -10 0 64.79 5.20 7 10 0 64.69 5.50 7 10 0 89.09 9.00 8 -10 0 5.20 2.00 8 10 0 8.00 2.70 0 -11 0 0.20 0.50 0 -11 0 2.70 3.70 0 11 0 0.80 0.90 0 11 0 -0.60 3.60 0 11 0 -1.10 3.60 0 11 0 -0.20 1.10 1 -11 0 228.18 10.40 -1 -11 0 220.28 28.80 -1 -11 0 240.68 10.50 1 -11 0 226.98 10.30 1 -11 0 240.48 25.60 -1 11 0 233.08 10.90 -1 11 0 348.17 51.79 -1 11 0 240.08 12.60 -1 11 0 235.08 15.90 1 11 0 245.38 12.60 1 11 0 247.68 15.60 1 11 0 237.08 10.90 1 11 0 213.68 27.00 2 -11 0 34.80 2.10 -2 -11 0 27.20 10.20 2 -11 0 36.50 2.10 -2 -11 0 34.10 2.20 2 -11 0 32.30 9.80 -2 11 0 33.70 2.60 -2 11 0 45.50 11.60 2 11 0 47.80 16.20 2 11 0 27.00 5.30 -2 11 0 34.20 11.80 -2 11 0 37.20 3.90 2 11 0 34.60 4.70 2 11 0 36.00 2.60 -3 -11 0 39.10 2.40 3 -11 0 39.50 2.40 3 -11 0 43.60 4.10 3 -11 0 29.30 9.60 3 -11 0 38.60 2.20 3 11 0 43.20 4.20 3 11 0 37.50 2.70 3 11 0 35.80 3.40 3 11 0 28.20 5.40 -3 11 0 39.40 14.30 -3 11 0 36.50 4.00 4 -11 0 73.89 3.90 4 -11 0 57.89 3.40 4 -11 0 57.29 17.20 4 -11 0 74.29 5.00 4 11 0 61.59 8.00 4 11 0 77.29 6.70 -4 11 0 96.49 23.60 4 11 0 75.09 5.60 4 11 0 76.89 4.20 -4 11 0 82.29 5.90 4 11 0 67.89 4.50 5 -11 0 88.19 5.70 5 -11 0 78.19 6.60 5 -11 0 90.49 4.80 5 11 0 89.09 6.40 5 11 0 86.39 8.80 5 11 0 82.89 5.10 -5 11 0 90.49 6.40 6 -11 0 19.80 2.20 6 -11 0 18.40 3.00 6 11 0 36.90 6.00 6 11 0 27.70 4.00 6 11 0 19.60 3.00 6 11 0 16.00 4.30 7 -11 0 168.08 8.60 7 -11 0 159.58 9.60 7 11 0 163.48 10.00 7 11 0 206.58 14.20 8 -11 0 62.09 5.80 8 11 0 75.09 6.00 0 -12 0 57.49 2.90 0 -12 0 34.00 11.10 0 12 0 47.50 4.60 0 12 0 34.90 13.90 0 12 0 53.29 3.70 0 12 0 45.30 7.30 1 -12 0 146.39 6.40 1 -12 0 126.99 23.10 1 -12 0 121.89 6.10 -1 -12 0 166.58 27.90 -1 12 0 137.19 6.90 1 12 0 125.69 26.80 -1 12 0 94.19 19.70 1 12 0 136.89 8.50 -1 12 0 145.39 13.20 -1 12 0 144.69 8.80 1 12 0 135.19 6.90 1 12 0 143.79 11.30 2 -12 0 0.10 3.20 2 -12 0 4.40 0.80 -2 -12 0 6.70 1.10 2 -12 0 6.90 0.90 -2 12 0 5.80 2.30 2 12 0 6.20 1.40 -2 12 0 5.40 1.30 2 12 0 5.60 1.90 2 12 0 7.30 4.50 -2 12 0 2.50 5.80 -3 -12 0 22.10 1.80 3 -12 0 24.70 3.40 3 -12 0 19.40 9.20 3 -12 0 23.60 1.80 3 -12 0 24.40 1.70 -3 12 0 24.10 3.70 -3 12 0 30.40 14.40 3 12 0 32.40 5.90 3 12 0 27.30 2.60 3 12 0 27.00 3.60 3 12 0 25.80 4.00 4 -12 0 595.14 27.60 4 -12 0 593.14 25.80 4 -12 0 624.54 26.30 4 12 0 644.64 31.40 4 12 0 640.14 28.60 4 12 0 575.24 27.00 -4 12 0 621.84 28.90 4 12 0 603.84 26.50 5 -12 0 67.89 4.00 5 -12 0 66.79 5.00 5 12 0 65.39 5.60 5 12 0 59.29 4.30 5 12 0 104.19 8.90 5 12 0 68.99 8.50 6 -12 0 41.50 4.00 6 -12 0 47.10 3.30 6 12 0 44.90 4.70 6 12 0 42.80 7.70 7 -12 0 20.30 3.00 7 12 0 28.90 4.20 8 -12 0 -0.30 2.40 8 12 0 0.60 2.80 0 -13 0 1.00 0.60 0 -13 0 3.20 5.20 0 13 0 -0.80 1.30 0 13 0 2.60 1.20 0 13 0 -0.50 3.30 0 13 0 -6.50 9.10 -1 -13 0 61.29 3.40 1 -13 0 61.19 3.30 -1 13 0 62.79 4.00 1 13 0 68.89 5.70 -1 13 0 60.89 5.60 1 13 0 55.99 8.20 -1 13 0 62.19 10.40 1 13 0 59.49 3.90 -1 13 0 54.99 29.80 2 -13 0 312.27 13.10 -2 -13 0 299.07 13.20 2 -13 0 294.97 12.90 2 13 0 306.27 13.70 -2 13 0 307.07 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45.40 2.30 2 -2 2 49.50 2.60 2 -2 2 45.70 3.50 -2 2 -2 50.29 2.50 2 2 2 46.70 2.40 -2 2 -2 43.60 4.20 2 2 2 77.49 12.20 2 2 2 49.40 2.80 2 2 2 49.50 2.60 2 2 2 55.99 3.50 -2 2 -2 50.39 6.10 2 2 2 46.30 2.70 2 2 2 47.70 2.30 -3 -2 -2 295.47 19.90 3 -2 2 276.67 12.30 3 -2 2 281.97 12.40 3 -2 2 285.47 11.90 3 -2 2 286.77 12.30 3 -2 2 261.87 12.10 3 -2 2 276.37 12.80 3 -2 2 282.57 12.70 -3 -2 -2 252.07 11.70 3 2 2 278.37 12.10 3 2 2 289.87 12.40 3 2 2 276.97 13.50 -3 2 -2 282.87 17.10 3 2 2 274.17 12.30 3 2 2 281.17 11.70 3 2 2 264.67 12.80 3 2 2 283.07 12.50 3 2 2 274.27 11.80 4 -2 2 845.92 35.90 -4 -2 -2 859.61 43.20 -4 -2 -2 911.01 44.80 4 -2 2 848.52 36.10 4 2 2 836.52 36.60 4 2 2 841.32 36.50 5 -2 2 131.09 6.70 5 -2 2 109.99 6.40 5 -2 2 124.49 6.00 5 -2 2 126.69 6.80 5 -2 2 117.79 6.80 5 2 2 124.29 6.40 5 2 2 132.79 6.90 5 2 2 139.49 7.20 5 2 2 124.09 5.80 5 2 2 124.29 6.50 6 -2 2 563.14 23.90 6 -2 2 517.55 24.40 6 -2 2 534.65 25.00 6 -2 2 608.84 25.30 6 -2 2 572.04 25.00 6 2 2 502.25 24.40 6 2 2 585.44 25.80 6 2 2 578.04 25.30 6 2 2 531.35 24.60 7 -2 2 52.99 5.80 7 -2 2 48.30 4.20 7 -2 2 53.79 4.50 7 2 2 50.49 4.90 7 2 2 50.89 6.70 7 2 2 47.50 4.80 7 2 2 51.79 4.60 8 -2 2 47.10 4.60 8 -2 2 52.09 4.80 8 2 2 42.00 5.30 8 2 2 48.40 5.80 8 2 2 43.90 4.80 9 -2 2 41.40 5.40 9 -2 2 58.49 6.60 9 2 2 40.60 5.70 9 2 2 33.90 5.20 9 -3 -2 56.09 6.70 9 -3 -2 70.79 7.70 9 3 -2 58.89 7.60 9 3 -2 69.19 7.50 8 -3 -2 2.80 1.50 8 -3 -2 15.00 4.20 8 -3 -2 2.20 1.60 8 -3 -2 8.80 3.40 8 -3 -2 4.50 1.30 8 3 -2 7.70 2.60 8 3 -2 6.70 2.50 8 3 -2 6.00 2.50 8 3 -2 8.80 2.90 7 -3 -2 36.50 4.50 7 -3 -2 22.10 3.00 7 -3 -2 30.50 4.30 7 -3 -2 33.20 5.20 7 -3 -2 29.90 2.30 7 3 -2 29.30 3.20 7 3 -2 33.80 4.80 7 3 -2 27.70 4.20 7 3 -2 29.10 3.70 7 3 -2 26.20 2.00 6 -3 -2 253.47 13.10 6 -3 -2 235.28 12.60 6 -3 -2 262.97 13.00 6 -3 -2 278.77 12.00 6 3 -2 280.97 13.80 -6 3 2 275.37 12.80 6 3 -2 247.98 11.60 6 3 -2 279.07 13.80 6 3 -2 271.27 12.80 6 3 -2 271.87 13.10 5 -3 -2 104.59 5.30 5 -3 -2 114.99 6.00 5 -3 -2 111.99 5.90 5 -3 -2 113.99 6.40 5 -3 -2 111.79 6.10 5 3 -2 93.59 7.30 5 3 -2 111.29 5.10 5 3 -2 117.39 6.70 5 3 -2 123.29 6.60 4 3 -2 715.43 30.40 -3 -3 2 1374.16 59.99 3 -3 -2 1211.78 54.09 3 3 -2 1346.87 61.39 3 3 -2 1287.07 54.89 -2 3 2 6171.68 255.97 -1 -3 2 1937.41 86.79 -1 3 2 2077.99 86.49 1 3 -2 2048.99 92.29 1 3 -2 2193.58 86.79 0 -3 -2 470.35 21.90 0 -3 2 473.75 22.30 0 -3 -2 487.95 30.50 0 3 -2 521.15 27.10 0 3 2 551.54 30.90 0 3 2 500.15 22.00 0 3 -2 531.25 22.30 1 -3 2 691.63 34.50 -1 -3 -2 732.43 37.90 -1 3 -2 684.03 34.50 1 3 2 634.44 37.60 -1 3 -2 642.14 29.40 2 -3 2 383.46 18.00 -2 -3 -2 393.06 16.70 -2 -3 -2 421.76 26.20 2 -3 2 419.26 23.30 -2 3 -2 433.76 23.50 2 3 2 382.76 16.80 -2 3 -2 369.96 18.30 2 3 2 413.76 18.00 -2 3 -2 404.56 17.10 2 3 2 375.46 26.70 3 -3 2 145.59 6.30 3 -3 2 141.29 6.90 3 -3 2 158.88 12.30 3 -3 2 149.29 7.00 3 -3 2 146.99 7.70 3 -3 2 155.68 7.30 -3 -3 -2 134.19 6.40 -3 -3 -2 166.88 14.70 3 -3 2 156.18 6.70 3 3 2 150.68 7.90 -3 3 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29.10 5.10 9 -4 -2 28.90 4.20 9 -4 -2 40.60 3.50 9 4 -2 37.10 5.00 9 4 -2 42.90 5.50 9 4 -2 49.40 9.20 8 -4 -2 58.09 3.80 8 -4 -2 59.19 8.20 8 -4 -2 45.10 4.40 8 -4 -2 46.80 4.60 8 4 -2 55.99 5.20 8 4 -2 65.59 8.30 8 4 -2 52.09 4.80 7 -4 -2 23.30 4.30 7 -4 -2 13.10 3.30 7 -4 -2 13.80 1.70 7 -4 -2 15.40 2.60 7 -4 -2 16.20 3.00 7 4 -2 12.00 3.00 7 4 -2 19.30 2.90 7 4 -2 21.60 3.00 7 4 -2 16.30 1.90 7 4 -2 12.20 3.00 6 -4 -2 39.20 2.50 6 -4 -2 36.80 4.10 6 -4 -2 38.60 4.10 6 -4 -2 37.10 3.20 6 -4 -2 36.60 3.10 6 4 -2 37.50 4.60 6 4 -2 34.40 3.10 -6 4 2 40.20 3.20 6 4 -2 37.50 3.90 6 4 -2 34.70 3.20 5 -4 -2 537.95 23.20 5 -4 -2 514.85 23.50 5 -4 -2 533.25 22.60 5 -4 -2 516.15 23.40 5 4 -2 543.65 24.20 5 4 -2 535.05 23.60 5 4 -2 537.35 23.40 5 4 -2 517.15 22.20 5 4 -2 503.55 24.00 -4 -4 2 1176.58 54.29 4 4 -2 1109.09 47.50 4 4 -2 1064.99 55.39 3 -4 -2 4.00 2.40 3 -4 -2 2.50 0.60 3 -4 -2 2.80 0.60 -3 -4 2 3.40 0.50 3 -4 -2 3.60 1.20 3 -4 -2 2.90 1.10 -3 -4 2 1.60 2.30 3 -4 -2 2.70 0.70 3 4 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24.90 2.90 -1 4 -2 25.60 6.20 1 4 2 19.20 1.30 1 4 2 19.60 1.30 -1 4 -2 19.90 1.90 1 4 2 14.50 5.60 2 -4 2 7.60 0.60 2 -4 2 7.20 1.00 -2 -4 -2 7.00 4.50 2 -4 2 3.30 2.00 2 -4 2 9.50 3.80 -2 -4 -2 7.30 0.70 2 -4 2 7.90 0.80 2 4 2 9.60 1.40 -2 4 -2 9.40 3.40 2 4 2 7.20 0.80 2 4 2 10.50 6.10 2 4 2 7.00 0.90 2 4 2 6.40 1.80 2 4 2 6.90 1.30 2 4 2 6.00 0.90 3 -4 2 32.30 1.60 3 -4 2 33.60 1.90 3 -4 2 30.00 2.70 3 -4 2 32.70 2.20 3 -4 2 46.60 8.30 3 -4 2 32.80 2.20 3 -4 2 30.20 2.20 -3 -4 -2 30.00 1.70 -3 -4 -2 33.50 8.30 3 4 2 36.60 2.40 -3 4 -2 38.90 11.20 3 4 2 33.80 2.70 3 4 2 31.70 2.50 3 4 2 30.90 2.00 -3 4 -2 34.50 2.20 3 4 2 31.20 3.40 3 4 2 58.79 13.00 3 4 2 33.30 1.90 -3 4 -2 39.50 7.90 4 -4 2 3.60 1.00 -4 -4 -2 5.90 3.60 4 -4 2 2.50 1.50 4 -4 2 3.20 1.10 4 -4 2 3.20 0.70 4 -4 2 2.70 1.70 4 -4 2 2.10 1.20 4 -4 2 2.10 0.80 -4 4 -2 2.90 2.30 4 4 2 2.00 1.00 4 4 2 3.50 0.90 4 4 2 2.10 1.70 4 4 2 3.60 1.10 4 4 2 3.10 1.20 5 -4 2 6.50 1.10 5 -4 2 5.20 1.20 5 -4 2 5.90 1.70 5 -4 2 7.20 2.50 5 -4 2 5.70 1.30 5 4 2 5.90 1.70 5 4 2 6.40 1.30 5 4 2 5.90 1.40 5 4 2 5.00 1.70 5 4 2 6.60 1.70 6 -4 2 198.08 8.80 6 -4 2 166.48 9.30 6 -4 2 181.88 10.50 6 -4 2 193.88 9.80 6 -4 2 184.78 9.50 6 4 2 194.08 10.20 6 4 2 176.18 9.20 6 4 2 186.28 10.70 6 4 2 176.58 9.40 7 -4 2 42.70 3.10 7 -4 2 36.30 3.50 7 -4 2 35.80 3.60 7 4 2 37.80 5.10 7 4 2 34.20 4.30 7 4 2 32.80 4.00 7 4 2 33.50 3.20 8 -4 2 91.99 6.50 8 -4 2 89.19 6.70 8 4 2 87.19 7.00 8 4 2 95.69 7.80 9 -4 2 57.59 8.40 9 -4 2 60.79 6.20 9 4 2 53.59 6.70 9 -5 -2 12.40 3.00 9 -5 -2 9.30 2.00 9 5 -2 13.10 4.20 9 5 -2 7.00 5.00 9 5 -2 6.90 3.50 8 -5 -2 188.28 12.00 8 -5 -2 195.78 9.50 8 -5 -2 196.68 12.50 8 5 -2 185.08 11.80 8 5 -2 187.58 12.40 7 -5 -2 203.68 10.80 7 -5 -2 197.98 11.60 7 -5 -2 220.88 9.90 7 -5 -2 186.58 10.80 7 -5 -2 200.88 11.90 7 5 -2 214.78 12.40 7 5 -2 208.68 11.10 7 5 -2 210.38 10.70 6 -5 -2 55.49 3.80 6 -5 -2 51.19 4.90 6 -5 -2 51.99 3.10 6 -5 -2 49.20 3.80 6 -5 -2 58.59 5.20 6 5 -2 51.29 4.90 -6 5 2 50.89 4.00 6 5 -2 44.70 2.70 6 5 -2 54.29 4.10 6 5 -2 50.69 3.80 6 5 -2 53.59 4.80 5 -5 -2 7.30 1.40 5 -5 -2 6.90 1.30 5 -5 -2 19.30 2.70 5 -5 -2 6.80 2.00 5 -5 -2 6.30 1.00 -5 5 2 8.20 1.60 5 5 -2 6.50 1.80 5 5 -2 5.40 0.70 5 5 -2 8.40 2.00 5 5 -2 6.70 1.50 5 5 -2 4.90 1.50 4 5 -2 6986.50 310.57 3 -5 -2 747.63 37.10 -3 -5 2 691.03 29.30 -3 -5 2 769.62 39.60 3 -5 -2 692.43 30.30 3 5 -2 704.03 31.20 -3 5 2 653.73 29.30 3 5 -2 739.53 41.30 3 5 -2 647.64 29.10 -3 5 2 737.53 40.60 2 -5 -2 291.87 12.30 -2 -5 2 277.67 12.20 2 -5 -2 295.37 12.70 2 -5 -2 275.97 19.50 -2 -5 2 289.47 20.40 2 -5 -2 284.87 12.20 2 -5 -2 275.77 13.60 2 5 -2 297.87 12.40 2 5 -2 284.87 14.10 -2 5 2 327.67 23.10 -2 5 2 289.07 12.40 -2 5 2 281.77 13.10 2 5 -2 305.47 13.40 2 5 -2 272.77 20.80 2 5 -2 294.27 13.10 1 -5 -2 46.10 2.20 1 -5 -2 47.50 8.60 1 -5 -2 43.20 4.10 1 -5 -2 47.30 2.20 -1 5 2 47.20 4.20 1 5 -2 55.09 9.70 -1 5 2 61.69 11.80 1 5 -2 48.00 2.50 1 5 -2 46.70 3.20 -1 5 2 45.80 2.90 -1 5 2 44.60 2.40 1 5 -2 51.99 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4 552.64 27.00 6 2 4 522.85 27.20 7 -2 4 2.70 1.50 7 -2 4 0.80 1.30 7 2 4 0.50 1.20 7 2 4 5.80 3.00 7 2 4 -0.50 1.20 8 -2 4 18.40 3.30 8 -2 4 13.60 2.90 8 2 4 18.10 3.50 8 2 4 16.10 3.50 9 -2 4 46.40 6.20 9 -2 4 48.90 6.50 9 2 4 47.90 6.40 10 3 -4 14.40 5.40 9 -3 -4 67.69 5.60 9 -3 -4 58.09 5.50 9 -3 -4 80.69 8.10 9 -3 -4 34.50 8.00 9 3 -4 75.29 9.00 9 3 -4 70.49 7.00 9 3 -4 75.19 9.50 8 -3 -4 173.78 8.30 8 -3 -4 176.48 10.60 8 -3 -4 162.38 9.70 8 -3 -4 152.08 10.30 8 -3 -4 168.28 10.60 8 3 -4 171.58 10.10 8 3 -4 187.28 12.20 8 3 -4 164.68 9.60 7 -3 -4 62.29 5.50 7 -3 -4 60.29 5.80 7 -3 -4 62.19 3.60 7 -3 -4 53.09 4.40 7 3 -4 57.69 5.90 7 3 -4 53.79 3.10 7 3 -4 54.29 5.20 7 3 -4 60.89 4.50 7 3 -4 53.09 4.60 6 -3 -4 4.30 1.20 6 -3 -4 9.00 2.20 6 -3 -4 8.60 2.10 6 -3 -4 3.60 2.30 6 -3 -4 3.20 0.80 6 3 -4 3.60 1.50 6 3 -4 4.60 0.80 6 3 -4 3.50 1.70 6 3 -4 6.00 1.70 6 3 -4 4.20 1.50 5 -3 -4 7.00 1.50 5 -3 -4 4.60 1.40 5 -3 -4 5.60 0.90 5 -3 -4 5.10 1.10 5 -3 -4 7.20 2.00 5 3 -4 4.50 1.30 5 3 -4 4.00 0.70 5 3 -4 4.90 1.40 5 3 -4 5.10 1.70 5 3 -4 5.50 1.50 4 3 -4 827.72 35.40 -3 -3 4 24.60 1.40 3 -3 -4 25.20 1.60 3 -3 -4 25.60 1.70 3 -3 -4 27.60 2.00 3 -3 -4 28.30 6.10 -3 -3 4 36.60 7.00 3 -3 -4 30.00 2.00 3 -3 -4 28.90 2.50 3 3 -4 24.20 2.60 3 3 -4 30.50 6.90 3 3 -4 25.80 2.30 3 3 -4 26.40 2.20 3 3 -4 23.00 2.90 3 3 -4 28.50 2.40 3 3 -4 23.00 1.50 -2 -3 4 86.39 3.90 2 -3 -4 97.19 4.70 2 -3 -4 86.99 3.90 2 -3 -4 81.89 4.00 2 -3 -4 72.59 4.40 2 -3 -4 93.49 4.30 -2 -3 4 98.19 9.80 2 -3 -4 85.19 4.80 2 3 -4 96.79 5.30 2 3 -4 92.29 9.60 -2 3 4 90.89 12.00 -2 3 4 93.79 5.70 2 3 -4 91.99 4.50 2 3 -4 99.39 5.80 1 -3 -4 245.68 10.40 1 -3 -4 238.28 19.60 -1 -3 4 239.28 10.30 1 -3 -4 218.78 11.30 -1 -3 4 253.67 17.70 1 -3 -4 247.48 10.50 -1 3 4 235.98 10.40 -1 3 4 274.87 21.90 1 3 -4 263.27 12.30 1 3 -4 255.77 17.60 0 -3 -4 61.19 12.10 0 -3 4 40.80 2.00 0 -3 4 43.30 8.40 0 -3 -4 38.80 3.70 0 3 4 33.10 9.90 0 3 4 43.90 3.50 0 3 4 39.90 2.10 0 3 -4 47.60 4.80 0 3 -4 38.40 2.10 1 -3 4 134.09 6.00 1 -3 4 133.89 5.70 1 -3 4 132.69 12.50 1 -3 4 115.29 7.70 -1 -3 -4 164.08 18.60 1 3 4 131.69 5.80 1 3 4 126.39 15.70 1 3 4 129.09 7.20 -1 3 -4 129.79 6.20 1 3 4 137.09 6.30 1 3 4 129.79 5.90 -1 3 -4 127.39 7.90 1 3 4 125.89 6.00 -1 3 -4 120.59 11.90 2 -3 4 270.27 19.70 -2 -3 -4 250.17 10.90 -2 -3 -4 247.98 22.60 2 -3 4 254.67 10.80 2 -3 4 205.58 14.90 2 -3 4 250.57 11.20 2 3 4 258.17 11.20 -2 3 -4 249.18 13.40 2 3 4 265.97 11.50 -2 3 -4 247.58 11.10 2 3 4 271.47 12.60 2 3 4 254.97 10.90 -2 3 -4 262.17 19.10 3 -3 4 123.29 6.00 3 -3 4 113.29 7.50 3 -3 4 125.19 5.30 -3 -3 -4 112.79 5.40 -3 -3 -4 131.19 25.10 3 -3 4 124.89 5.60 3 -3 4 125.49 6.10 3 3 4 123.99 6.00 3 3 4 110.39 5.50 -3 3 -4 124.69 12.70 3 3 4 127.99 5.50 3 3 4 105.19 7.70 3 3 4 129.79 6.30 3 3 4 118.49 6.00 3 3 4 115.49 7.10 4 -3 4 1.80 2.20 4 -3 4 1.40 0.80 4 -3 4 1.80 1.30 4 -3 4 3.00 0.80 -4 -3 -4 1.90 3.20 4 -3 4 1.30 0.70 -4 -3 -4 3.10 3.00 4 3 4 0.50 1.60 4 3 4 1.40 0.60 4 3 4 -0.30 0.90 4 3 4 0.20 2.30 4 3 4 1.10 0.70 4 3 4 1.20 0.90 4 3 4 1.70 0.90 -4 3 -4 2.10 2.40 -5 -3 -4 7.90 4.10 5 -3 4 11.70 1.90 -5 -3 -4 3.40 3.10 5 -3 4 10.40 1.60 5 -3 4 9.40 1.70 5 -3 4 10.50 1.80 5 3 4 9.80 2.40 5 3 4 11.00 1.80 5 3 4 13.10 2.00 5 3 4 10.90 2.00 5 3 4 9.20 1.90 5 3 4 11.60 2.80 6 -3 4 255.67 12.20 6 -3 4 261.87 13.50 6 3 4 255.87 13.80 6 3 4 252.77 13.60 6 3 4 209.78 11.50 6 3 4 217.08 11.30 7 -3 4 14.00 2.60 7 -3 4 22.90 3.40 7 3 4 21.70 4.30 7 3 4 22.30 3.50 7 3 4 13.40 3.00 8 -3 4 16.70 3.30 8 -3 4 16.70 3.10 8 3 4 9.50 3.00 8 3 4 20.30 3.70 9 -3 4 69.29 7.10 9 -3 4 74.99 7.30 9 3 4 64.19 7.50 9 -4 -4 11.30 6.30 9 -4 -4 1.90 1.50 9 -4 -4 2.60 1.60 9 4 -4 -3.70 3.60 9 4 -4 5.60 4.30 8 -4 -4 49.20 3.80 8 -4 -4 49.70 6.30 8 -4 -4 52.29 7.60 8 -4 -4 45.30 5.90 8 -4 -4 49.50 4.30 8 4 -4 50.29 5.10 8 4 -4 53.49 4.90 8 4 -4 55.19 9.20 7 -4 -4 83.59 5.60 7 -4 -4 98.79 6.90 7 -4 -4 87.29 4.70 7 -4 -4 95.29 7.10 7 4 -4 73.19 4.10 7 4 -4 76.19 5.70 7 4 -4 87.59 7.50 -7 4 4 83.79 5.70 7 4 -4 82.09 5.60 6 -4 -4 76.99 4.90 6 -4 -4 75.79 5.30 6 -4 -4 78.99 6.10 6 -4 -4 81.49 4.30 6 -4 -4 94.19 5.80 6 4 -4 83.69 6.40 6 4 -4 82.39 5.20 6 4 -4 80.09 5.40 6 4 -4 72.99 3.90 5 -4 -4 7.10 1.30 5 -4 -4 8.50 1.80 5 -4 -4 8.90 1.20 5 -4 -4 7.60 2.10 5 -4 -4 8.70 1.70 5 4 -4 10.00 1.00 5 4 -4 7.50 1.70 5 4 -4 5.60 1.80 5 4 -4 7.50 1.60 4 -4 -4 342.07 14.30 4 -4 -4 334.07 15.30 4 -4 -4 334.37 14.90 4 -4 -4 323.77 14.50 4 -4 -4 311.97 15.40 4 4 -4 333.57 15.80 4 4 -4 324.47 15.30 4 4 -4 317.97 14.10 4 4 -4 338.37 15.20 4 4 -4 323.27 15.10 4 4 -4 347.57 24.90 3 -4 -4 39.80 7.50 -3 -4 4 31.50 1.70 3 -4 -4 32.30 2.20 3 -4 -4 31.70 1.90 3 -4 -4 29.90 2.60 3 -4 -4 31.10 1.60 -3 -4 4 31.20 7.20 3 -4 -4 34.50 2.30 3 -4 -4 29.90 1.90 -3 4 4 29.70 8.20 -3 4 4 32.60 1.80 3 4 -4 35.60 2.90 3 4 -4 33.90 2.50 3 4 -4 42.20 8.60 3 4 -4 40.00 3.40 3 4 -4 30.70 3.60 2 -4 -4 15.00 1.10 2 -4 -4 15.20 1.10 2 -4 -4 15.90 1.30 2 -4 -4 19.80 2.20 2 -4 -4 14.70 1.00 -2 -4 4 10.70 4.20 2 -4 -4 14.00 2.10 -2 -4 4 12.70 0.90 2 -4 -4 11.00 4.80 -2 4 4 15.00 1.10 2 4 -4 14.00 1.50 -2 4 4 13.50 6.30 2 4 -4 10.20 2.50 2 4 -4 13.30 4.50 -2 4 4 15.30 3.30 1 -4 -4 83.59 3.80 -1 -4 4 89.29 10.20 1 -4 -4 82.89 5.40 -1 -4 4 82.99 3.80 1 -4 -4 87.49 11.60 1 -4 -4 79.29 3.90 1 -4 -4 82.79 4.00 1 4 -4 82.99 9.80 -1 4 4 117.19 18.10 -1 4 4 90.99 5.80 1 4 -4 88.89 5.90 -1 4 4 84.89 3.90 1 4 -4 84.19 4.20 0 -4 -4 121.49 5.40 0 -4 4 123.79 5.30 0 -4 -4 110.39 7.30 0 -4 -4 132.59 15.00 0 -4 4 92.39 8.60 0 4 -4 125.49 7.60 0 4 4 123.79 5.50 0 4 -4 130.09 12.40 0 4 4 132.79 15.90 0 4 4 125.09 7.10 0 4 -4 128.99 6.20 -1 -4 -4 0.90 0.40 1 -4 4 1.20 0.40 -1 -4 -4 2.30 4.00 1 -4 4 3.60 3.50 1 4 4 0.70 1.60 1 4 4 5.20 5.50 1 4 4 1.00 0.50 -1 4 -4 3.80 2.90 1 4 4 1.00 0.50 -1 4 -4 1.70 0.80 -1 4 -4 2.40 2.50 2 -4 4 1902.01 88.59 -2 -4 -4 1916.61 94.09 -2 4 -4 1731.33 78.89 -2 4 -4 1959.30 88.59 2 4 4 1762.62 78.29 3 -4 4 27.90 1.50 3 -4 4 27.80 2.10 3 -4 4 27.50 2.20 3 -4 4 27.00 1.80 -3 -4 -4 30.10 9.20 3 -4 4 27.90 4.20 3 4 4 26.20 2.20 3 4 4 27.40 2.50 3 4 4 27.00 3.40 3 4 4 27.20 1.70 -3 4 -4 30.70 9.50 3 4 4 26.50 2.10 4 -4 4 76.09 5.10 -4 -4 -4 70.99 14.90 4 -4 4 90.09 4.90 4 -4 4 87.69 6.30 4 -4 4 90.19 4.70 -4 -4 -4 98.39 15.60 4 4 4 88.19 4.80 4 4 4 86.49 4.90 -4 4 -4 96.19 11.30 4 4 4 85.49 4.10 4 4 4 83.09 6.00 4 4 4 82.39 6.60 4 4 4 74.19 5.90 5 -4 4 15.50 2.20 5 -4 4 12.50 2.20 5 -4 4 14.90 1.90 -5 -4 -4 15.20 6.10 5 -4 4 11.10 1.80 5 4 4 10.50 2.30 5 4 4 14.70 2.20 5 4 4 15.20 2.90 5 4 4 11.70 3.10 5 4 4 11.10 1.90 6 -4 4 129.99 7.30 6 -4 4 134.29 7.80 6 4 4 109.89 6.50 6 4 4 123.49 7.60 6 4 4 119.49 8.10 6 4 4 106.29 6.80 7 -4 4 39.90 3.80 7 -4 4 39.00 3.90 7 4 4 36.90 4.00 7 4 4 32.10 4.60 8 -4 4 121.29 8.00 8 -4 4 110.59 7.50 8 4 4 112.19 8.20 9 -4 4 12.00 3.60 9 -4 4 11.00 3.60 9 4 4 15.50 5.10 9 -5 -4 12.00 5.60 9 -5 -4 8.70 1.80 9 -5 -4 7.00 2.20 9 5 -4 6.50 3.50 9 5 -4 20.80 5.60 8 -5 -4 1.10 0.80 8 -5 -4 0.40 1.20 8 -5 -4 8.80 4.40 8 5 -4 2.90 1.90 8 5 -4 0.50 1.70 7 -5 -4 20.10 4.10 7 -5 -4 24.90 4.50 7 -5 -4 18.50 2.70 7 -5 -4 18.80 2.10 7 5 -4 19.80 3.20 -7 5 4 16.50 3.00 7 5 -4 20.80 4.80 7 5 -4 21.60 3.10 6 -5 -4 471.35 22.70 6 -5 -4 530.95 21.30 6 -5 -4 484.35 22.40 6 -5 -4 465.25 22.30 6 -5 -4 469.85 21.90 6 5 -4 442.06 20.70 6 5 -4 503.75 22.60 -6 5 4 519.05 22.90 6 5 -4 507.25 22.40 5 -5 -4 199.78 9.70 5 -5 -4 189.68 9.40 5 -5 -4 194.88 10.30 5 -5 -4 204.18 9.00 5 -5 -4 201.38 9.90 5 5 -4 194.18 9.90 5 5 -4 178.08 8.50 5 5 -4 207.08 11.10 5 5 -4 201.18 10.10 4 -5 -4 613.04 28.00 -4 -5 4 656.53 37.10 4 -5 -4 623.54 33.00 4 5 -4 627.64 27.30 4 5 -4 684.83 29.30 4 5 -4 689.53 28.80 4 5 -4 651.03 40.90 4 5 -4 666.93 28.60 3 -5 -4 90.99 4.10 3 -5 -4 96.09 4.40 -3 -5 4 86.79 4.20 3 -5 -4 96.89 4.90 3 -5 -4 89.69 4.50 3 -5 -4 88.69 5.50 3 -5 -4 90.59 6.90 3 -5 -4 91.79 10.50 -3 -5 4 92.99 11.20 3 5 -4 112.79 6.50 -3 5 4 86.59 14.80 3 5 -4 92.19 6.40 3 5 -4 89.89 5.10 3 5 -4 92.19 11.60 -3 5 4 87.99 4.30 3 5 -4 87.99 4.10 3 5 -4 96.79 5.70 2 -5 -4 150.68 6.60 2 -5 -4 154.18 7.00 2 -5 -4 158.38 15.20 2 -5 -4 147.19 6.90 -2 -5 4 158.88 14.80 2 -5 -4 154.18 6.80 2 -5 -4 141.69 8.00 2 5 -4 156.18 7.40 -2 5 4 168.48 18.00 -2 5 4 157.18 6.80 2 5 -4 155.78 8.80 -2 5 4 136.29 9.10 1 -5 -4 -1.70 2.50 -1 -5 4 5.60 3.80 1 -5 -4 4.10 0.60 1 -5 -4 5.00 4.70 1 -5 -4 2.90 0.50 -1 -5 4 4.30 0.60 1 -5 -4 1.70 0.60 -1 5 4 4.00 2.30 1 5 -4 0.20 2.00 -1 5 4 2.70 5.20 1 5 -4 3.50 1.00 1 5 -4 3.00 1.10 1 5 -4 5.20 3.90 -1 5 4 2.90 0.70 0 -5 4 394.46 26.30 0 -5 -4 394.26 16.30 0 -5 4 335.67 19.80 0 -5 -4 395.96 29.00 0 -5 -4 335.07 18.40 0 5 -4 374.46 25.80 0 5 -4 401.66 18.80 0 5 4 399.66 17.00 0 5 -4 396.66 17.30 0 5 4 404.36 31.10 0 5 4 401.06 16.40 0 5 4 395.96 18.30 1 -5 4 102.79 8.20 -1 -5 -4 113.39 5.30 1 -5 4 118.89 5.20 1 -5 4 120.09 13.00 -1 -5 -4 117.09 15.20 -1 5 -4 124.49 13.20 1 5 4 115.09 5.40 -1 5 -4 119.29 6.10 1 5 4 116.49 5.90 1 5 4 150.58 23.20 1 5 4 116.29 7.10 -1 5 -4 121.59 8.00 1 5 4 116.19 5.30 -2 -5 -4 175.58 7.90 2 -5 4 173.78 7.70 2 -5 4 180.98 8.40 -2 -5 -4 173.08 19.20 2 -5 4 174.78 16.60 2 5 4 158.98 20.10 2 5 4 176.78 8.20 2 5 4 174.18 9.90 -2 5 -4 183.58 8.60 -2 5 -4 195.78 17.30 -2 5 -4 184.08 11.40 2 5 4 176.48 8.00 2 5 4 192.58 9.10 2 5 4 175.58 8.60 -3 -5 -4 47.10 11.70 3 -5 4 42.90 9.90 3 -5 4 46.90 2.30 3 -5 4 47.20 3.10 3 -5 4 51.29 3.10 3 -5 4 46.20 5.40 -3 -5 -4 45.30 2.50 3 5 4 42.80 2.60 3 5 4 45.00 3.30 -3 5 -4 51.39 10.90 3 5 4 55.59 14.60 -3 5 -4 49.20 3.00 3 5 4 47.40 3.60 3 5 4 48.80 3.00 3 5 4 46.80 4.60 4 -5 4 300.87 13.80 4 -5 4 291.57 13.20 4 -5 4 292.57 12.70 4 -5 4 291.87 14.20 4 -5 4 285.37 15.20 4 5 4 317.27 15.00 -4 5 -4 309.97 25.60 4 5 4 298.47 15.40 4 5 4 297.27 13.00 4 5 4 312.07 14.80 4 5 4 303.57 13.90 5 -5 4 81.19 4.90 5 -5 4 80.89 4.70 5 -5 4 64.89 5.00 5 -5 4 85.99 4.90 -5 -5 -4 84.99 14.90 5 5 4 83.19 6.20 5 5 4 80.89 5.10 5 5 4 76.09 4.80 5 5 4 65.49 4.30 5 5 4 78.29 6.70 5 5 4 80.29 5.80 6 -5 4 24.60 3.10 6 -5 4 21.70 3.80 6 5 4 23.10 2.40 6 5 4 23.40 3.30 6 5 4 22.50 3.80 7 -5 4 31.70 4.10 7 -5 4 26.30 3.60 7 5 4 23.60 3.60 7 5 4 27.90 3.90 7 5 4 23.30 4.30 8 -5 4 70.79 5.90 8 -5 4 71.79 5.50 8 5 4 63.49 6.00 9 -5 4 6.70 3.10 9 -6 -4 5.70 1.60 9 -6 -4 3.90 1.70 9 6 -4 7.90 4.00 9 6 -4 -1.10 3.10 8 -6 -4 12.20 5.20 8 -6 -4 2.90 1.30 8 -6 -4 1.60 0.90 8 6 -4 2.40 1.80 8 6 -4 3.00 1.80 7 -6 -4 117.09 6.30 7 -6 -4 113.49 7.00 7 -6 -4 125.89 9.00 7 6 -4 118.99 7.30 7 6 -4 151.38 10.90 -7 6 4 122.79 7.90 7 6 -4 128.89 7.80 6 -6 -4 103.59 6.20 6 -6 -4 109.99 5.70 6 -6 -4 101.59 7.70 6 -6 -4 114.19 7.40 6 -6 -4 98.09 6.40 6 6 -4 131.89 8.90 6 6 -4 114.49 6.70 -6 6 4 117.49 7.10 6 6 -4 119.19 7.00 -5 -6 4 114.69 11.70 5 -6 -4 115.69 6.10 5 -6 -4 125.49 7.40 5 -6 -4 125.79 7.00 5 -6 -4 114.99 6.30 5 -6 -4 124.59 5.80 5 6 -4 107.09 5.20 5 6 -4 120.19 6.80 5 6 -4 88.29 8.30 -5 6 4 126.89 7.10 5 6 -4 125.89 8.10 5 6 -4 121.09 6.90 4 -6 -4 140.49 6.80 4 -6 -4 142.99 7.90 4 -6 -4 150.98 7.40 4 -6 -4 130.79 7.10 4 -6 -4 138.19 12.40 4 -6 -4 133.59 6.80 -4 -6 4 151.48 15.10 4 6 -4 152.28 8.80 4 6 -4 136.79 15.90 4 6 -4 148.39 7.80 4 6 -4 129.69 6.10 4 6 -4 138.59 7.50 3 -6 -4 45.10 2.80 3 -6 -4 41.70 4.20 -3 -6 4 75.99 14.80 3 -6 -4 52.09 3.30 3 -6 -4 49.30 2.70 3 -6 -4 49.10 2.40 -3 -6 4 51.29 2.60 3 6 -4 52.09 4.00 -3 6 4 50.59 2.70 3 6 -4 54.99 5.20 3 6 -4 46.70 2.30 -3 6 4 61.79 19.20 3 6 -4 63.49 5.00 3 6 -4 51.69 3.50 2 -6 -4 93.29 4.60 2 -6 -4 88.39 4.20 -2 -6 4 86.79 4.10 -2 -6 4 89.49 11.60 2 -6 -4 88.49 11.80 2 -6 -4 86.29 4.00 2 6 -4 97.49 12.40 -2 6 4 84.89 7.40 2 6 -4 89.39 6.80 2 6 -4 87.79 4.90 -2 6 4 97.79 17.10 -1 -6 4 1047.70 53.99 1 -6 -4 1029.10 63.59 1 -6 -4 853.21 42.50 1 6 -4 1016.20 53.89 -1 6 4 959.20 42.90 1 6 -4 1023.00 43.50 0 -6 -4 107.99 5.30 0 -6 4 131.39 11.90 0 -6 4 114.69 5.20 0 -6 -4 116.29 5.30 0 -6 -4 123.79 15.50 0 -6 4 114.79 13.30 0 6 4 120.09 6.20 0 6 -4 125.59 8.10 0 6 -4 121.59 13.80 0 6 4 141.29 18.10 0 6 4 117.89 7.60 0 6 4 114.89 5.40 1 -6 4 286.27 12.00 1 -6 4 288.77 22.80 -1 -6 -4 305.87 26.20 -1 -6 -4 286.47 12.00 1 -6 4 252.67 15.30 1 6 4 287.07 12.90 -1 6 -4 277.67 15.10 1 6 4 295.67 27.80 1 6 4 277.67 14.30 1 6 4 270.47 12.10 -1 6 -4 275.07 13.00 -1 6 -4 290.17 23.40 1 6 4 278.87 12.20 2 -6 4 49.10 2.40 -2 -6 -4 48.10 2.50 2 -6 4 32.60 8.20 2 -6 4 41.80 3.10 -2 -6 -4 46.60 12.40 2 6 4 50.39 3.40 2 6 4 40.70 12.40 -2 6 -4 47.30 6.80 -2 6 -4 47.70 3.30 -2 6 -4 67.59 12.60 2 6 4 51.59 4.70 2 6 4 46.50 2.80 2 6 4 48.70 2.70 3 -6 4 1389.36 64.99 3 -6 4 1501.95 77.29 -3 -6 -4 1544.05 82.59 3 6 4 1319.67 84.49 -3 6 -4 1517.05 63.19 3 6 4 1613.04 65.29 -3 6 -4 1545.75 77.79 4 -6 4 109.89 5.90 4 -6 4 103.29 5.30 -4 -6 -4 91.99 18.30 4 -6 4 111.19 5.90 4 -6 4 101.19 4.70 4 -6 4 89.89 7.50 4 6 4 120.09 5.50 4 6 4 102.29 6.00 4 6 4 106.99 5.90 -4 6 -4 97.09 16.30 4 6 4 104.89 7.60 4 6 4 108.49 6.80 5 -6 4 0.00 0.70 5 -6 4 0.20 0.70 5 -6 4 1.60 2.10 5 -6 4 -0.10 1.60 5 6 4 -0.10 3.40 5 6 4 0.00 1.50 5 6 4 0.20 0.90 5 6 4 1.70 1.10 5 6 4 2.80 3.30 -5 6 -4 0.30 2.70 6 -6 4 37.10 3.30 6 -6 4 35.90 3.40 6 6 4 34.40 3.20 6 6 4 29.40 4.30 6 6 4 35.40 3.70 7 -6 4 294.47 14.40 7 -6 4 304.87 14.80 7 6 4 248.88 13.60 7 6 4 291.47 15.30 8 -6 4 -0.70 1.40 8 -6 4 0.90 1.20 8 6 4 1.60 2.00 9 -6 4 9.30 3.40 9 6 4 15.10 5.20 9 -7 -4 9.80 2.10 9 7 -4 8.00 3.90 9 7 -4 -0.70 3.20 8 -7 -4 17.60 5.70 8 -7 -4 8.00 2.10 8 -7 -4 12.00 1.80 8 7 -4 10.70 2.50 8 7 -4 9.80 2.60 7 -7 -4 208.18 11.30 7 -7 -4 220.08 10.50 7 -7 -4 223.68 13.20 7 7 -4 215.78 12.00 -7 7 4 215.18 12.20 7 7 -4 263.07 15.40 7 7 -4 226.38 11.60 6 -7 -4 835.22 37.70 6 -7 -4 984.30 42.30 -6 7 4 870.81 38.90 6 7 -4 894.41 38.30 6 7 -4 735.13 44.30 5 -7 -4 109.49 6.10 5 -7 -4 110.89 7.00 5 -7 -4 115.29 5.70 5 7 -4 111.89 6.70 5 7 -4 117.59 7.30 5 7 -4 127.39 8.70 -5 7 4 117.59 7.10 5 7 -4 105.79 6.70 4 -7 -4 1.10 0.60 4 -7 -4 1.00 0.60 4 -7 -4 2.50 1.50 -4 -7 4 3.40 3.40 4 7 -4 1.80 3.40 4 7 -4 1.00 2.20 -4 7 4 1.10 1.00 4 7 -4 10.10 3.10 4 7 -4 1.50 1.30 4 7 -4 7.00 1.70 3 -7 -4 37.40 2.50 3 -7 -4 41.00 2.00 3 -7 -4 36.80 4.10 3 -7 -4 33.40 8.50 -3 -7 4 36.50 2.10 3 -7 -4 37.60 3.00 3 -7 -4 39.70 2.20 -3 -7 4 38.70 9.50 -3 7 4 39.20 2.30 3 7 -4 40.30 3.80 3 7 -4 35.20 9.80 3 7 -4 37.10 4.90 -3 7 4 42.30 3.30 3 7 -4 33.90 2.90 -3 7 4 51.59 13.80 -2 -7 4 2.20 0.60 -2 -7 4 6.10 4.90 2 -7 -4 2.20 3.70 2 -7 -4 3.90 0.60 2 -7 -4 3.20 0.60 2 -7 -4 3.20 1.40 -2 7 4 3.20 1.20 -2 7 4 5.00 5.40 2 7 -4 0.80 1.00 -2 7 4 4.80 4.00 2 7 -4 2.60 2.80 -2 7 4 2.90 0.70 2 7 -4 1.90 3.50 -1 -7 4 18.20 6.10 -1 -7 4 26.80 1.60 1 -7 -4 23.60 7.40 1 -7 -4 36.50 5.60 1 -7 -4 28.80 1.60 1 -7 -4 29.80 1.70 1 7 -4 33.90 8.30 -1 7 4 29.00 1.90 -1 7 4 26.30 4.40 1 7 -4 28.80 4.50 -1 7 4 39.00 12.90 1 7 -4 29.00 2.90 -1 7 4 28.30 2.60 0 -7 4 171.98 17.70 0 -7 -4 175.28 8.00 0 -7 4 190.38 8.20 0 -7 -4 183.48 8.20 0 -7 -4 188.88 20.30 0 7 -4 194.78 9.60 0 7 4 189.88 9.20 0 7 -4 194.98 11.50 0 7 -4 189.58 18.80 0 7 4 188.88 10.90 0 7 4 170.88 21.60 -1 -7 -4 310.67 27.40 1 -7 4 277.77 23.60 1 -7 4 246.48 17.50 1 -7 4 297.47 12.40 -1 -7 -4 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4 17.80 2.60 5 7 4 15.50 3.80 6 -7 4 276.37 13.40 6 -7 4 277.97 13.20 6 7 4 253.17 13.00 6 7 4 244.08 13.00 6 7 4 258.47 12.90 6 7 4 272.77 13.90 7 -7 4 22.40 3.70 7 -7 4 33.90 3.30 7 7 4 31.20 4.80 7 7 4 29.60 3.00 8 -7 4 47.70 4.90 8 -7 4 47.10 4.40 8 7 4 45.90 6.20 9 -7 4 4.00 3.00 9 7 4 -8.30 3.90 9 -8 -4 69.39 4.70 9 8 -4 60.99 6.30 9 8 -4 62.09 6.70 8 -8 -4 539.25 24.90 8 -8 -4 564.04 23.70 8 8 -4 534.85 25.40 8 8 -4 509.25 24.60 7 -8 -4 40.60 3.00 7 -8 -4 36.40 3.50 7 -8 -4 45.70 6.50 7 8 -4 38.70 3.70 -7 8 4 45.90 4.50 7 8 -4 42.80 4.20 -6 8 4 1439.56 62.49 6 8 -4 1464.15 62.09 6 8 -4 1387.06 63.29 5 -8 -4 1.00 0.60 5 -8 -4 0.60 0.70 5 -8 -4 -0.80 2.30 -5 8 4 0.80 1.20 5 8 -4 0.50 1.20 4 -8 -4 6.10 1.20 4 -8 -4 5.60 1.00 -4 -8 4 5.00 4.00 4 -8 -4 6.70 2.20 4 -8 -4 4.30 2.00 4 -8 -4 6.10 4.30 4 8 -4 5.20 3.10 -4 8 4 5.80 1.60 -4 8 4 6.40 5.10 4 8 -4 14.60 7.90 4 8 -4 4.60 1.70 4 8 -4 7.20 1.90 3 -8 -4 281.07 12.00 -3 -8 4 280.67 25.00 3 -8 -4 295.67 12.80 3 -8 -4 288.57 13.10 3 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570.84 26.90 -4 10 -4 576.74 26.60 4 10 4 578.04 25.00 5 -10 4 416.06 19.40 5 -10 4 449.66 20.20 5 10 4 439.96 23.00 5 10 4 438.86 18.80 5 10 4 429.46 20.80 5 10 4 400.86 20.50 6 -10 4 40.30 3.80 6 -10 4 38.60 3.20 6 10 4 38.40 4.90 6 10 4 34.20 3.70 6 10 4 26.60 7.40 7 -10 4 68.29 5.50 7 10 4 69.89 5.20 7 10 4 71.59 6.70 8 -10 4 34.00 4.60 8 10 4 29.90 6.50 8 -11 -4 104.79 5.80 8 -11 -4 100.49 8.60 8 11 -4 92.99 6.20 8 11 -4 95.69 7.50 7 -11 -4 5.70 1.60 7 -11 -4 1.20 0.90 7 11 -4 3.40 1.90 7 11 -4 2.60 1.40 6 -11 -4 44.70 3.10 6 -11 -4 39.20 3.50 6 11 -4 45.00 4.00 6 11 -4 45.90 4.50 -6 11 4 47.40 5.10 6 11 -4 47.20 5.70 5 -11 -4 135.79 7.50 5 -11 -4 124.49 8.70 5 -11 -4 142.49 6.90 -5 11 4 151.38 13.50 5 11 -4 144.69 8.50 5 11 -4 140.69 10.90 4 -11 -4 379.76 20.00 4 -11 -4 429.06 41.30 4 -11 -4 463.65 19.40 4 -11 -4 444.26 19.00 4 11 -4 455.05 21.70 4 11 -4 459.35 21.10 4 11 -4 467.65 24.10 -4 11 4 473.95 22.00 -3 -11 4 115.99 5.80 3 -11 -4 118.49 5.70 3 -11 -4 117.39 6.90 3 -11 -4 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1.40 2.80 -1 4 8 4.80 3.10 1 4 -8 5.00 4.70 1 4 -8 4.20 2.80 -1 4 8 3.30 0.80 1 4 -8 3.70 0.90 0 -4 8 6.10 0.80 0 -4 8 5.20 0.80 0 -4 8 10.60 7.00 0 4 8 5.30 0.90 0 4 -8 8.10 3.80 0 4 8 5.90 2.60 0 4 -8 4.50 3.80 -1 -4 -8 813.22 58.69 1 -4 8 822.52 52.49 1 4 8 808.62 34.80 1 4 8 872.41 37.70 -1 4 -8 792.22 50.49 1 4 8 785.52 35.20 -1 4 -8 868.81 38.90 -2 -4 -8 275.97 11.80 2 -4 8 265.07 12.10 -2 -4 -8 252.17 30.60 -2 -4 -8 277.47 27.20 2 -4 8 261.87 11.70 -2 4 -8 283.17 26.00 -2 4 -8 248.88 16.70 2 4 8 280.97 14.80 2 4 8 269.57 12.20 2 4 8 256.97 11.80 2 4 8 269.77 12.70 -3 -4 -8 95.69 5.00 -3 -4 -8 137.89 24.00 3 -4 8 101.09 6.00 3 -4 8 97.49 4.80 3 -4 8 102.89 7.10 -3 4 -8 117.49 20.90 3 4 8 106.19 5.60 3 4 8 106.39 6.20 3 4 8 102.99 8.10 3 4 8 102.99 5.10 3 4 8 92.69 5.20 4 -4 8 13.40 2.20 -4 -4 -8 18.60 9.90 4 -4 8 12.10 1.30 4 -4 8 11.20 1.70 4 4 8 12.20 1.50 4 4 8 12.90 2.30 4 4 8 12.40 2.00 -4 4 -8 4.30 4.90 4 4 8 11.00 4.10 5 -4 8 58.39 4.40 5 -4 8 56.19 5.00 5 -4 8 56.79 5.60 5 4 8 48.00 4.00 5 4 8 47.00 6.30 6 -4 8 100.49 6.40 6 -4 8 93.49 6.40 6 4 8 93.49 7.20 6 4 8 94.69 6.30 6 4 8 83.79 8.40 6 4 8 91.49 7.20 7 -4 8 81.29 6.10 7 -4 8 84.49 6.40 7 4 8 83.49 6.20 8 -4 8 21.00 4.00 8 -4 8 21.20 4.20 8 4 8 21.50 4.20 9 -5 -8 88.49 5.30 9 -5 -8 87.89 9.70 9 5 -8 101.29 9.50 9 5 -8 85.09 7.10 8 -5 -8 0.50 0.80 8 -5 -8 2.90 4.10 -8 5 8 0.90 1.40 8 5 -8 0.40 1.50 8 5 -8 7.10 3.20 7 -5 -8 10.00 4.60 7 -5 -8 5.60 3.30 7 5 -8 0.10 1.40 7 5 -8 0.70 1.70 6 -5 -8 60.99 6.10 6 -5 -8 48.00 3.10 6 -5 -8 49.90 5.80 6 5 -8 45.80 4.10 6 5 -8 44.10 4.10 6 5 -8 43.70 2.60 5 -5 -8 2.30 2.80 5 -5 -8 0.00 0.60 5 -5 -8 4.90 1.60 5 5 -8 -0.20 1.00 5 5 -8 0.10 1.20 5 5 -8 1.10 0.50 5 5 -8 3.70 5.00 4 -5 -8 2.70 3.40 4 -5 -8 4.30 2.40 -4 -5 8 12.40 6.80 4 -5 -8 7.30 4.40 4 -5 -8 3.80 0.90 4 -5 -8 4.40 0.60 4 5 -8 5.10 1.70 4 5 -8 4.90 1.40 4 5 -8 3.20 0.80 4 5 -8 7.50 5.40 4 5 -8 5.90 2.80 -3 -5 8 487.15 20.90 3 -5 -8 477.95 21.20 3 -5 -8 427.36 33.30 3 -5 -8 467.15 36.70 3 -5 -8 517.75 21.40 -3 -5 8 484.55 36.10 3 5 -8 516.55 24.30 3 5 -8 499.85 21.30 -3 5 8 478.05 21.10 3 5 -8 506.05 22.90 3 5 -8 445.26 34.30 3 5 -8 515.75 21.80 2 -5 -8 417.76 36.00 -2 -5 8 429.06 33.50 2 -5 -8 446.26 19.10 2 -5 -8 454.75 18.90 2 -5 -8 444.06 19.30 2 5 -8 449.76 19.50 2 5 -8 455.15 22.40 2 5 -8 401.06 32.00 -2 5 8 444.66 19.10 -1 -5 8 7.30 0.90 1 -5 -8 3.20 4.60 -1 -5 8 7.80 5.70 1 -5 -8 7.50 1.00 1 5 -8 12.40 3.60 -1 5 8 7.90 3.50 1 5 -8 7.30 1.10 -1 5 8 6.70 1.00 1 5 -8 7.00 4.40 0 -5 8 243.08 10.40 0 -5 -8 231.78 10.40 0 -5 -8 232.08 27.20 0 -5 8 243.48 29.40 0 5 8 230.78 10.50 0 5 8 227.78 10.30 0 5 8 241.18 13.30 0 5 -8 255.37 43.70 0 5 -8 249.28 14.40 1 -5 8 514.45 39.20 1 -5 8 556.84 23.00 -1 -5 -8 521.75 44.80 -1 -5 -8 552.94 22.80 1 -5 8 515.85 22.60 1 5 8 506.65 23.30 1 5 8 524.45 25.60 -1 5 -8 570.24 27.20 -1 5 -8 527.65 38.60 1 5 8 525.75 22.80 2 -5 8 60.99 3.60 -2 -5 -8 71.59 18.30 2 -5 8 98.99 20.10 -2 -5 -8 62.49 3.40 2 5 8 60.89 3.60 2 5 8 61.79 3.80 -2 5 -8 74.89 9.90 -2 5 -8 77.79 17.10 2 5 8 67.29 6.20 3 -5 8 210.68 9.50 3 -5 8 216.58 10.30 3 -5 8 227.08 10.90 -3 -5 -8 223.68 25.90 -3 -5 -8 213.28 9.70 -3 5 -8 200.68 23.30 3 5 8 229.18 13.30 3 5 8 194.28 11.90 3 5 8 212.58 9.80 3 5 8 217.48 10.20 3 5 8 202.78 10.20 4 -5 8 141.29 7.50 4 -5 8 134.09 6.50 4 -5 8 149.49 8.10 4 -5 8 151.48 9.30 4 5 8 147.59 7.60 4 5 8 135.49 8.40 -4 5 -8 150.78 26.40 4 5 8 152.98 10.50 4 5 8 132.49 6.80 4 5 8 128.69 7.00 5 -5 8 651.03 29.30 5 -5 8 656.33 30.10 5 -5 8 662.03 29.10 5 5 8 633.54 30.20 5 5 8 605.44 31.10 5 5 8 667.93 27.90 5 5 8 648.54 29.00 6 -5 8 20.10 3.00 6 -5 8 25.50 3.70 6 5 8 21.60 5.90 6 5 8 26.80 3.70 6 5 8 20.80 3.80 6 5 8 23.30 5.30 7 -5 8 431.96 21.70 7 -5 8 467.65 22.10 7 5 8 465.45 22.10 8 -5 8 62.19 6.40 8 -5 8 59.29 6.10 8 5 8 75.29 7.90 9 -6 -8 108.69 10.30 9 -6 -8 107.09 6.10 9 6 -8 131.39 10.00 9 6 -8 99.49 7.70 8 -6 -8 70.29 7.70 8 -6 -8 64.49 4.10 -8 6 8 61.79 5.80 8 6 -8 70.99 6.50 8 6 -8 67.59 5.40 7 -6 -8 180.88 8.70 7 -6 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263.47 13.30 6 -6 8 1.50 1.10 6 -6 8 -0.60 1.00 6 6 8 -3.20 6.20 6 6 8 -0.60 1.00 6 6 8 -0.90 5.40 7 -6 8 2.80 1.70 7 -6 8 0.90 1.40 7 6 8 -1.00 1.50 8 -6 8 10.90 3.40 8 -6 8 6.30 3.70 9 -7 -8 39.80 3.70 9 7 -8 47.90 6.50 8 -7 -8 204.38 9.90 8 -7 -8 205.08 13.50 -8 7 8 197.58 12.10 8 7 -8 200.78 11.70 8 7 -8 207.08 11.30 7 -7 -8 147.39 7.50 7 -7 -8 143.89 10.30 7 7 -8 159.78 9.10 -7 7 8 147.39 9.70 7 7 -8 135.99 8.80 6 -7 -8 2.50 1.00 6 -7 -8 3.60 3.10 6 7 -8 2.40 1.50 6 7 -8 1.20 1.50 -6 7 8 2.50 1.80 5 -7 -8 0.50 0.70 5 -7 -8 3.70 2.20 5 7 -8 -0.60 1.10 5 7 -8 2.00 2.80 5 7 -8 2.30 1.50 4 -7 -8 161.88 7.20 4 -7 -8 134.79 17.60 4 -7 -8 180.78 7.90 4 -7 -8 171.58 8.50 4 7 -8 169.68 11.10 4 7 -8 136.99 9.30 4 7 -8 158.98 7.40 4 7 -8 180.28 8.90 -3 -7 8 28.20 1.90 3 -7 -8 30.40 2.60 3 -7 -8 30.30 2.10 -3 -7 8 44.40 13.40 3 -7 -8 29.90 1.80 3 -7 -8 26.40 9.60 3 7 -8 25.80 4.90 3 7 -8 28.90 2.70 -3 7 8 30.70 2.20 3 7 -8 29.00 9.60 3 7 -8 32.00 4.30 3 7 -8 30.50 2.10 -2 -7 8 2.20 3.70 2 -7 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531.45 24.40 1 5 9 549.15 23.90 -1 5 -9 576.04 42.30 -2 -5 -9 47.90 14.40 -2 -5 -9 67.59 20.40 2 -5 9 45.50 3.00 -2 -5 -9 46.90 2.90 2 -5 9 50.39 2.80 2 5 9 48.90 3.10 -2 5 -9 36.90 11.50 2 5 9 48.70 3.00 -2 5 -9 49.50 9.50 2 5 9 49.70 6.20 -3 -5 -9 338.97 51.99 -3 -5 -9 254.57 11.60 3 -5 9 256.57 11.40 3 -5 9 269.37 12.20 3 -5 9 279.87 14.50 3 -5 9 241.38 12.70 3 5 9 261.77 12.10 3 5 9 230.78 11.80 3 5 9 269.57 15.60 -3 5 -9 232.58 38.50 4 -5 9 50.29 2.90 4 -5 9 44.80 5.40 4 -5 9 51.69 3.80 4 -5 9 49.20 4.20 4 5 9 51.49 3.80 4 5 9 54.99 7.30 4 5 9 49.80 3.20 4 5 9 51.59 4.70 5 -5 9 11.50 3.60 5 -5 9 11.60 2.20 5 -5 9 12.80 2.50 5 5 9 14.60 4.40 5 5 9 13.40 2.40 5 5 9 10.70 2.70 6 -5 9 11.40 2.30 6 -5 9 7.90 2.30 6 5 9 7.00 2.20 6 5 9 11.60 4.30 7 -5 9 36.80 4.70 7 -5 9 36.80 4.70 7 5 9 43.50 4.50 8 -5 9 4.00 3.30 8 -5 9 6.00 3.40 8 5 9 4.80 4.00 9 -6 -9 5.00 2.00 9 -6 -9 15.00 6.10 9 6 -9 2.70 3.30 9 6 -9 12.40 5.40 8 -6 -9 6.90 5.00 8 -6 -9 3.80 1.30 -8 6 9 3.70 2.40 8 6 -9 12.80 3.90 8 6 -9 3.30 2.00 7 -6 -9 7.90 1.50 7 -6 -9 8.70 4.10 7 6 -9 6.60 2.20 7 6 -9 10.10 2.70 -7 6 9 4.60 2.10 6 -6 -9 177.38 8.70 6 -6 -9 178.58 10.10 6 6 -9 180.38 10.10 6 6 -9 181.18 10.10 5 -6 -9 21.60 1.90 5 -6 -9 24.20 3.20 5 6 -9 20.80 3.30 5 6 -9 19.00 1.60 5 6 -9 23.00 3.20 4 -6 -9 49.30 2.60 4 -6 -9 55.49 14.00 4 -6 -9 53.19 3.70 4 -6 -9 41.70 2.90 4 6 -9 51.69 2.90 4 6 -9 50.69 3.80 4 6 -9 55.29 6.10 3 -6 -9 18.30 9.50 3 -6 -9 5.60 1.50 -3 -6 9 6.00 7.60 3 -6 -9 8.40 1.00 3 -6 -9 11.00 1.30 -3 -6 9 7.90 1.10 3 -6 -9 16.30 8.70 3 6 -9 10.40 1.50 3 6 -9 6.40 3.20 3 6 -9 8.90 2.40 3 6 -9 9.30 1.70 -3 6 9 10.20 1.40 3 6 -9 6.10 5.90 2 -6 -9 169.68 29.60 -2 -6 9 121.09 5.70 -2 -6 9 101.79 18.90 2 -6 -9 118.19 5.80 2 -6 -9 125.89 6.00 -2 6 9 121.49 11.70 2 6 -9 78.09 15.10 -2 6 9 123.39 5.90 2 6 -9 119.69 9.30 2 6 -9 120.39 6.20 -1 -6 9 227.48 25.20 1 -6 -9 216.68 10.40 -1 -6 9 220.98 10.00 1 -6 -9 229.68 10.10 1 6 -9 244.48 14.50 1 6 -9 224.38 23.80 1 6 -9 228.48 10.20 -1 6 9 213.28 14.00 -1 6 9 227.28 10.20 0 -6 -9 1003.70 69.99 0 6 -9 1042.60 47.40 0 6 9 1031.90 43.00 0 6 9 1039.70 46.50 0 6 9 1038.30 43.90 0 6 -9 887.71 60.49 -1 -6 -9 3.80 6.30 -1 -6 -9 3.10 0.90 1 -6 9 3.40 0.80 1 -6 9 6.10 6.10 1 -6 9 2.50 0.70 1 6 9 2.80 0.90 1 6 9 4.40 1.80 -1 6 -9 7.00 4.40 -1 6 -9 3.10 5.40 1 6 9 3.30 3.30 1 6 9 3.80 0.80 2 -6 9 94.89 22.00 2 -6 9 75.69 4.50 -2 -6 -9 85.69 20.90 -2 -6 -9 75.69 4.10 2 -6 9 82.59 4.10 2 6 9 78.59 4.30 2 6 9 76.59 4.30 -2 6 -9 72.99 18.10 2 6 9 77.39 7.80 -2 6 -9 87.89 12.10 -3 -6 -9 40.20 14.00 3 -6 9 41.90 3.70 3 -6 9 36.30 2.90 3 -6 9 35.90 2.30 -3 -6 -9 31.70 2.40 3 6 9 31.60 2.80 -3 6 -9 44.20 14.60 3 6 9 37.60 2.90 3 6 9 36.30 6.30 3 6 9 37.00 2.60 4 -6 9 186.98 9.40 4 -6 9 178.38 10.10 4 -6 9 173.18 11.10 4 -6 9 178.38 8.20 4 6 9 169.18 9.20 4 6 9 183.58 8.60 4 6 9 185.38 12.70 5 -6 9 466.15 22.70 5 -6 9 456.65 21.60 5 -6 9 451.55 21.20 5 6 9 474.75 21.30 5 6 9 444.76 19.80 5 6 9 435.16 24.00 6 -6 9 66.89 5.30 6 -6 9 63.69 5.30 6 6 9 74.89 6.40 6 6 9 69.59 7.60 7 -6 9 13.20 3.30 8 -6 9 2.90 3.20 8 -6 9 4.30 3.20 8 6 9 2.10 3.80 9 -7 -9 96.89 5.70 9 7 -9 79.19 7.20 9 7 -9 120.59 10.80 8 -7 -9 4.40 1.40 8 -7 -9 12.50 5.80 -8 7 9 4.40 2.80 8 7 -9 8.80 3.60 8 7 -9 4.40 2.20 7 -7 -9 7.00 1.80 7 -7 -9 8.20 4.40 7 7 -9 3.70 2.30 7 7 -9 4.20 2.30 -7 7 9 4.10 2.20 6 -7 -9 0.50 0.80 6 -7 -9 2.80 3.10 6 7 -9 0.60 1.40 6 7 -9 1.10 1.40 -6 7 9 0.80 1.90 5 -7 -9 7.50 2.60 5 -7 -9 6.60 1.20 5 7 -9 5.70 0.90 5 7 -9 4.30 1.80 5 7 -9 8.40 2.80 4 -7 -9 184.18 22.40 4 -7 -9 204.48 10.20 4 -7 -9 224.18 9.70 4 -7 -9 195.88 9.10 4 7 -9 196.28 9.30 4 7 -9 243.88 15.50 4 7 -9 226.78 11.80 4 7 -9 192.18 10.40 3 -7 -9 340.07 14.60 3 -7 -9 294.67 31.20 -3 -7 9 344.37 14.70 3 -7 -9 344.67 15.00 3 -7 -9 328.97 15.20 3 7 -9 336.57 15.00 -3 7 9 322.17 15.00 3 7 -9 359.56 19.10 3 7 -9 347.87 15.70 2 -7 -9 41.80 3.20 -2 -7 9 41.30 2.40 2 -7 -9 45.80 13.80 -2 -7 9 34.30 10.80 2 -7 -9 45.50 2.50 -2 7 9 37.50 12.20 2 7 -9 29.40 10.40 -2 7 9 40.90 2.70 2 7 -9 39.30 2.90 2 7 -9 32.20 5.50 -1 -7 9 35.70 12.30 1 -7 -9 22.00 1.70 1 -7 -9 20.70 2.10 1 -7 -9 16.90 9.70 -1 -7 9 20.10 1.60 -1 7 9 22.60 2.00 -1 7 9 25.70 5.70 1 7 -9 22.00 2.20 -1 7 9 18.70 2.80 1 7 -9 28.10 5.80 1 7 -9 22.60 9.30 -1 7 9 18.60 10.30 0 -7 9 2.40 3.50 0 -7 -9 0.20 3.10 0 -7 -9 1.40 0.70 0 7 -9 3.00 4.70 0 7 9 1.20 1.40 0 7 9 0.40 3.00 0 7 9 0.60 0.70 0 7 -9 1.60 3.90 0 7 9 7.30 3.70 1 -7 9 40.90 2.80 1 -7 9 47.20 13.70 1 -7 9 37.30 2.40 -1 -7 -9 47.30 17.50 1 7 9 32.70 3.80 1 7 9 41.20 6.30 1 7 9 42.70 2.70 -1 7 -9 34.20 7.40 1 7 9 38.40 2.40 -1 7 -9 64.19 17.40 2 -7 9 871.91 36.90 2 -7 9 735.33 58.49 -2 -7 -9 901.91 36.50 -2 7 -9 761.02 57.89 2 7 9 836.62 36.60 2 7 9 825.92 37.30 2 7 9 918.21 41.10 2 7 9 899.11 36.60 3 -7 9 682.63 28.20 -3 -7 -9 592.04 53.49 3 -7 9 631.24 29.60 3 -7 9 679.23 29.10 -3 -7 -9 630.34 28.30 -3 7 -9 607.54 74.49 3 7 9 633.44 28.80 3 7 9 770.02 37.10 3 7 9 676.33 28.60 4 -7 9 12.70 3.50 4 -7 9 13.90 2.70 4 -7 9 16.30 3.20 4 7 9 15.10 2.30 4 7 9 17.40 2.00 4 7 9 14.50 4.90 5 -7 9 97.89 8.00 5 -7 9 92.59 6.50 5 -7 9 101.59 6.40 5 7 9 110.39 10.00 5 7 9 99.99 6.40 5 7 9 103.69 5.30 6 -7 9 453.65 21.10 6 -7 9 416.26 21.00 6 7 9 456.85 21.20 6 7 9 432.36 22.40 7 -7 9 78.89 6.20 7 -7 9 78.39 6.00 7 7 9 73.89 6.40 9 -8 -9 16.00 2.60 9 8 -9 18.20 4.40 9 8 -9 29.70 6.00 8 -8 -9 -0.90 8.90 8 -8 -9 2.70 1.40 8 8 -9 -2.30 3.20 -8 8 9 -3.70 2.10 8 8 -9 0.80 3.00 7 -8 -9 6.90 4.90 7 -8 -9 7.10 1.30 7 8 -9 7.80 2.50 7 8 -9 4.30 2.10 -7 8 9 5.20 2.70 6 -8 -9 351.06 16.00 6 -8 -9 339.47 17.60 -6 8 9 368.26 18.90 6 8 -9 357.76 17.80 6 8 -9 357.06 17.50 5 -8 -9 221.78 12.00 5 -8 -9 243.18 10.80 5 8 -9 224.18 14.00 5 8 -9 239.68 12.30 5 8 -9 228.08 12.70 -5 8 9 232.98 13.20 4 -8 -9 1.70 0.80 4 -8 -9 1.70 4.70 4 -8 -9 0.50 0.50 4 -8 -9 -1.70 1.50 4 8 -9 2.30 1.80 4 8 -9 -0.20 1.00 4 8 -9 0.40 0.40 4 8 -9 2.20 3.40 3 -8 -9 223.08 43.30 3 -8 -9 219.98 10.40 3 -8 -9 214.78 9.70 -3 -8 9 217.58 9.80 3 -8 -9 224.48 10.00 3 8 -9 241.88 14.60 -3 8 9 220.48 10.20 3 8 -9 207.58 9.90 3 8 -9 219.08 10.80 3 8 -9 192.58 12.10 2 -8 -9 31.80 13.20 2 -8 -9 13.20 1.40 2 -8 -9 12.10 1.40 -2 -8 9 15.50 1.60 2 8 -9 15.90 5.20 -2 8 9 10.80 2.30 -2 8 9 14.90 1.80 -2 8 9 15.60 10.90 2 8 -9 13.00 1.80 -1 -8 9 43.30 2.60 1 -8 -9 73.89 21.30 1 -8 -9 41.20 2.60 1 -8 -9 39.10 2.50 -1 -8 9 34.10 12.40 -1 8 9 42.20 4.00 1 8 -9 40.20 12.10 1 8 -9 36.30 6.50 -1 8 9 43.60 7.60 -1 8 9 39.40 17.20 1 8 -9 41.10 2.70 -1 8 9 36.10 2.70 0 -8 -9 39.00 2.40 0 -8 9 36.40 2.30 0 -8 -9 37.10 2.60 0 -8 9 27.50 10.10 0 8 9 58.19 22.40 0 8 9 35.60 2.60 0 8 9 35.50 6.00 0 8 -9 45.00 13.90 0 8 9 42.60 4.20 1 -8 9 26.00 3.70 -1 -8 -9 37.10 16.50 1 -8 9 24.90 1.90 -1 -8 -9 27.00 2.00 1 -8 9 49.10 16.30 1 8 9 34.80 6.40 1 8 9 21.20 2.20 -1 8 -9 27.10 8.00 1 8 9 29.10 3.80 -1 8 -9 23.60 11.30 1 8 9 30.00 16.60 2 -8 9 35.70 2.80 2 -8 9 18.60 9.10 -2 -8 -9 34.40 2.40 2 -8 9 33.80 2.20 2 8 9 20.20 5.20 2 8 9 32.30 2.40 2 8 9 33.50 3.30 2 8 9 34.70 2.60 -2 8 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5 11 0.60 3.20 8 5 -11 -0.40 2.00 8 5 -11 15.50 5.00 7 -5 -11 5.80 4.10 7 -5 -11 1.60 0.90 7 5 -11 -0.30 1.40 7 5 -11 11.80 3.50 6 -5 -11 63.09 5.40 6 -5 -11 49.70 3.50 6 5 -11 47.50 3.00 6 5 -11 54.99 4.70 6 5 -11 55.99 5.20 5 -5 -11 63.19 3.90 5 -5 -11 63.99 4.70 5 5 -11 59.59 3.60 5 5 -11 69.29 5.20 5 5 -11 71.89 6.30 4 -5 -11 388.46 39.90 4 -5 -11 439.46 19.00 4 -5 -11 473.35 19.70 4 -5 -11 451.95 19.90 4 5 -11 442.06 19.60 4 5 -11 457.85 21.20 4 5 -11 456.75 20.40 4 5 -11 307.07 42.90 3 -5 -11 488.95 20.70 3 -5 -11 497.25 21.30 -3 -5 11 468.45 20.70 3 -5 -11 461.95 21.00 -3 5 11 487.55 21.00 3 5 -11 480.45 21.60 3 5 -11 496.25 22.90 -2 -5 11 75.79 4.00 2 -5 -11 78.39 4.60 2 -5 -11 80.49 4.10 2 -5 -11 99.99 24.10 -2 5 11 70.59 4.20 2 5 -11 84.49 8.40 2 5 -11 76.39 4.50 1 -5 -11 6.40 7.80 1 -5 -11 0.40 3.20 -1 -5 11 5.90 4.90 1 -5 -11 1.10 0.80 -1 5 11 6.90 5.20 1 5 -11 4.00 3.80 -1 5 11 1.50 0.80 1 5 -11 7.20 6.00 0 -5 -11 37.30 17.90 0 -5 11 30.10 2.00 0 -5 -11 29.50 2.10 0 -5 11 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11 328.67 19.80 5 6 11 328.57 14.90 5 6 11 334.87 16.20 6 -6 11 5.90 2.00 6 -6 11 3.70 1.80 6 6 11 4.90 1.90 6 6 11 7.10 5.40 7 -6 11 82.29 6.80 7 -6 11 81.79 10.60 8 -7 -11 85.59 8.70 8 -7 -11 80.19 5.00 8 7 -11 74.29 6.40 -8 7 11 78.29 7.50 8 7 -11 106.79 8.80 7 -7 -11 4.70 4.50 7 -7 -11 2.30 1.00 7 7 -11 2.60 2.60 7 7 -11 1.40 1.70 -7 7 11 -0.30 2.30 6 -7 -11 327.97 15.10 6 -7 -11 329.27 16.60 6 7 -11 328.57 16.70 6 7 -11 336.37 16.60 5 -7 -11 81.49 8.50 5 -7 -11 86.69 4.80 5 7 -11 87.69 6.40 5 7 -11 84.79 5.80 5 7 -11 77.59 4.20 4 -7 -11 88.79 4.20 4 -7 -11 86.89 4.70 4 -7 -11 74.89 5.20 4 7 -11 93.89 6.60 4 7 -11 81.49 4.50 4 7 -11 84.49 5.50 -3 -7 11 329.97 17.00 3 -7 -11 389.66 16.50 3 -7 -11 326.17 39.60 3 -7 -11 392.16 16.10 3 -7 -11 344.47 16.40 -3 7 11 366.36 16.50 3 7 -11 390.06 18.90 3 7 -11 380.86 17.10 2 -7 -11 104.99 5.50 -2 -7 11 101.09 5.20 2 -7 -11 108.99 5.20 2 -7 -11 90.99 24.30 2 7 -11 97.89 10.10 -2 7 11 97.79 6.00 2 7 -11 105.19 5.70 1 -7 -11 344.17 44.00 1 -7 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12 142.19 8.10 4 -12 12 142.79 8.40 4 -12 12 142.09 6.90 4 12 12 143.29 7.70 5 -12 12 58.69 8.00 5 -12 12 71.09 6.40 7 -13 -12 28.50 3.10 -7 13 12 21.70 6.10 7 13 -12 22.90 4.70 7 13 -12 20.10 5.10 6 -13 -12 0.70 1.30 -6 13 12 5.00 5.50 6 13 -12 -1.80 2.70 6 13 -12 -4.30 2.50 5 -13 -12 66.19 4.00 5 13 -12 69.69 5.40 -5 13 12 53.79 7.90 5 13 -12 62.89 6.10 4 -13 -12 16.30 1.60 4 -13 -12 11.20 1.60 4 13 -12 11.40 3.40 4 13 -12 17.40 2.80 -4 13 12 12.80 5.60 4 13 -12 12.20 7.60 3 -13 -12 89.39 4.70 3 -13 -12 87.89 4.60 -3 -13 12 88.19 4.90 -3 13 12 72.39 8.60 3 13 -12 98.39 13.40 3 13 -12 81.19 7.40 2 -13 -12 -0.20 0.70 -2 -13 12 0.60 0.80 2 -13 -12 1.50 0.80 -2 13 12 2.00 1.30 -2 13 12 -2.60 4.70 2 13 -12 15.00 9.50 1 -13 -12 275.87 12.40 -1 -13 12 271.67 12.40 -1 -13 12 265.07 13.10 -1 13 12 248.78 16.00 -1 13 12 281.57 13.20 1 13 -12 263.27 23.40 0 -13 12 58.99 3.70 0 -13 12 60.39 4.10 0 -13 -12 54.69 3.60 0 13 12 52.79 6.90 0 13 -12 65.19 17.50 0 13 12 56.29 4.30 -1 -13 -12 15.30 2.00 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2 -4 -14 61.19 4.30 -2 4 14 57.89 3.80 2 4 -14 57.39 4.80 2 4 -14 56.19 28.60 -1 -4 14 86.69 10.90 -1 -4 14 106.19 5.40 1 -4 -14 106.29 5.40 -1 4 14 75.99 11.00 1 4 -14 103.19 6.70 -1 4 14 101.49 5.50 0 -4 14 1173.48 53.09 0 -4 -14 1138.89 48.30 0 -4 14 1147.19 48.30 0 4 14 1097.19 48.40 0 4 14 1130.89 53.89 0 4 14 1156.08 48.50 -1 -4 -14 11.60 1.70 1 -4 14 17.40 5.80 1 -4 14 12.70 1.70 1 4 14 14.40 2.00 1 4 14 14.10 2.00 2 -4 14 17.00 5.20 2 -4 14 16.50 1.90 -2 -4 -14 12.90 1.90 2 4 14 19.30 5.70 2 4 14 15.30 2.80 2 4 14 13.50 2.00 -3 -4 -14 17.80 2.20 3 -4 14 10.80 5.10 3 -4 14 15.20 2.70 3 -4 14 15.10 1.90 3 4 14 14.70 2.30 3 4 14 17.30 2.30 3 4 14 12.10 6.00 4 -4 14 35.20 3.80 4 -4 14 38.10 2.80 4 -4 14 41.10 7.50 4 4 14 38.10 3.90 4 4 14 34.40 2.90 4 4 14 34.70 8.00 5 -4 14 53.59 4.80 5 4 14 50.29 4.30 6 -4 14 3.80 2.90 8 -5 -14 8.40 2.30 8 -5 -14 0.20 5.10 -8 5 14 0.90 7.10 8 5 -14 10.60 6.40 8 5 -14 2.30 3.10 7 -5 -14 282.87 13.00 7 -5 -14 252.47 17.10 7 5 -14 273.67 16.10 7 5 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5 14 222.38 10.50 2 5 14 190.28 10.70 3 -5 14 28.40 2.70 -3 -5 -14 31.00 3.00 3 -5 14 30.80 6.60 3 -5 14 30.00 3.80 3 5 14 21.10 6.90 3 5 14 29.00 2.90 3 5 14 24.80 2.70 4 -5 14 3.70 5.00 4 -5 14 4.00 1.90 4 -5 14 2.60 1.00 4 5 14 -1.70 5.60 4 5 14 3.00 1.30 4 5 14 1.70 1.20 5 -5 14 134.59 14.50 5 -5 14 122.09 8.00 5 5 14 155.68 19.60 6 -5 14 13.60 3.70 6 5 14 17.80 3.70 8 -6 -14 115.49 6.90 -8 6 14 120.29 10.10 8 6 -14 107.19 10.00 8 6 -14 131.29 10.10 7 -6 -14 2.60 4.60 7 -6 -14 12.80 2.00 -7 6 14 11.40 4.50 7 6 -14 14.60 3.30 6 -6 -14 0.30 3.90 6 -6 -14 8.00 1.60 6 6 -14 13.60 4.00 6 6 -14 7.70 2.20 5 -6 -14 79.19 4.60 5 6 -14 73.89 5.60 5 6 -14 68.69 6.30 5 6 -14 68.69 4.20 4 -6 -14 7.70 1.50 4 -6 -14 8.70 1.20 4 6 -14 11.50 2.90 4 6 -14 8.10 2.30 4 6 -14 9.00 1.70 3 -6 -14 17.60 1.90 -3 -6 14 18.50 2.10 3 -6 -14 15.60 2.10 3 6 -14 19.50 3.40 3 6 -14 23.90 3.10 -3 6 14 20.40 2.50 2 -6 -14 144.09 7.80 -2 -6 14 147.29 7.30 2 -6 -14 148.29 7.20 2 6 -14 151.98 9.30 -2 6 14 149.59 7.60 1 -6 -14 37.80 2.70 1 -6 -14 35.90 3.10 -1 -6 14 36.70 2.70 -1 -6 14 18.40 7.20 -1 6 14 34.90 2.80 -1 6 14 32.70 4.80 0 -6 -14 95.99 5.10 0 -6 14 90.79 10.40 0 -6 14 87.99 5.10 0 6 14 90.09 7.20 0 6 14 108.99 13.60 1 -6 14 61.69 3.70 -1 -6 -14 60.59 3.80 1 -6 14 47.80 7.60 1 6 14 56.69 9.40 1 6 14 57.69 3.90 2 -6 14 205.88 9.70 2 -6 14 215.38 14.70 -2 -6 -14 205.78 9.80 2 6 14 188.08 9.90 2 6 14 198.88 10.00 2 6 14 199.68 15.50 -3 -6 -14 4.70 1.30 3 -6 14 7.20 1.40 3 -6 14 5.00 2.30 3 6 14 7.90 1.60 3 6 14 10.20 10.60 3 6 14 8.70 1.80 4 -6 14 1.20 1.60 4 -6 14 8.40 4.80 4 -6 14 -1.10 0.80 4 6 14 1.10 6.00 4 6 14 1.00 1.10 4 6 14 1.20 1.10 5 -6 14 169.68 12.70 5 -6 14 160.08 12.50 5 6 14 152.98 14.20 5 6 14 152.68 9.00 6 -6 14 7.50 3.30 8 -7 -14 17.90 2.70 8 7 -14 11.80 5.30 8 7 -14 10.20 3.90 -8 7 14 11.00 4.80 7 -7 -14 12.30 2.00 -7 7 14 8.40 4.20 7 7 -14 12.30 4.80 7 7 -14 11.40 3.00 6 -7 -14 16.70 2.30 6 7 -14 16.50 4.20 -6 7 14 3.80 3.90 6 7 -14 16.90 3.20 5 -7 -14 77.49 4.60 5 7 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118.79 9.70 6 -5 -15 275.47 12.40 6 5 -15 262.07 13.40 6 5 -15 256.77 14.40 6 5 -15 246.38 11.90 5 -5 -15 2.40 1.10 5 5 -15 0.00 1.30 5 5 -15 3.10 1.00 5 5 -15 1.90 3.00 4 -5 -15 3.70 0.90 4 -5 -15 3.60 1.30 4 5 -15 3.50 1.80 4 5 -15 4.10 2.40 4 5 -15 6.90 1.60 3 -5 -15 19.70 2.40 3 -5 -15 19.80 2.00 -3 -5 15 20.80 2.80 3 5 -15 18.50 3.20 3 5 -15 20.70 2.70 -3 5 15 21.00 2.50 2 -5 -15 232.78 10.70 2 -5 -15 228.78 11.30 -2 5 15 221.78 11.00 1 -5 -15 5.80 1.30 -1 -5 15 5.60 1.30 1 5 -15 5.10 1.90 -1 5 15 3.70 1.40 0 -5 15 99.49 5.40 0 -5 15 115.69 11.90 0 -5 -15 98.99 5.40 0 5 15 90.09 7.40 0 5 15 97.29 5.60 1 -5 15 296.47 13.70 -1 -5 -15 299.47 13.80 1 -5 15 302.57 20.20 1 5 15 303.87 21.00 1 5 15 300.07 14.40 1 5 15 295.27 14.00 2 -5 15 106.99 11.20 -2 -5 -15 101.89 5.60 2 -5 15 103.79 5.60 2 5 15 108.09 13.50 2 5 15 98.89 5.70 2 5 15 89.59 5.70 -3 -5 -15 101.79 5.70 3 -5 15 102.89 6.10 3 -5 15 104.69 8.30 3 -5 15 104.49 11.10 3 5 15 101.59 12.40 3 5 15 91.19 6.00 3 5 15 106.19 6.40 4 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14.40 1 6 15 123.49 6.80 2 -6 15 23.20 2.40 2 -6 15 17.40 6.40 -2 -6 -15 19.60 2.30 2 6 15 20.90 2.60 2 6 15 19.00 8.40 -3 -6 -15 2.40 1.00 3 -6 15 0.90 1.50 3 -6 15 -1.10 5.10 3 -6 15 -0.70 0.80 3 6 15 1.80 6.80 3 6 15 0.80 1.00 3 6 15 1.80 1.30 4 -6 15 68.09 5.50 4 -6 15 69.19 4.10 4 -6 15 69.39 9.90 4 6 15 68.59 5.60 4 6 15 65.89 4.40 4 6 15 52.59 10.70 5 -6 15 70.49 9.80 5 -6 15 72.19 6.00 5 6 15 75.29 10.80 7 -7 -15 7.90 2.00 7 7 -15 9.70 3.30 -7 7 15 4.60 4.50 7 7 -15 14.00 4.90 6 -7 -15 66.69 4.40 -6 7 15 61.19 7.70 6 7 -15 87.49 7.60 6 7 -15 74.49 5.70 5 -7 -15 314.67 14.30 5 7 -15 287.57 15.50 5 7 -15 317.67 15.70 4 -7 -15 3.30 0.90 4 -7 -15 1.50 0.90 4 7 -15 2.60 1.10 4 7 -15 3.30 1.90 -3 -7 15 265.47 12.20 3 -7 -15 274.07 12.50 3 -7 -15 270.07 12.00 3 7 -15 254.27 14.00 3 7 -15 249.58 12.70 2 -7 -15 2.40 1.00 -2 -7 15 2.10 0.90 2 -7 -15 1.40 1.00 -2 7 15 1.40 1.10 -2 7 15 -2.40 3.20 2 7 -15 1.60 1.90 1 -7 -15 17.40 2.10 -1 -7 15 16.90 2.00 1 -7 -15 18.30 2.40 1 7 -15 20.40 3.80 -1 7 15 22.20 4.80 -1 7 15 23.70 2.70 0 -7 -15 34.60 3.20 0 -7 15 40.80 2.90 0 -7 15 25.20 7.60 0 -7 -15 43.30 3.00 0 7 15 42.40 11.10 0 7 15 34.90 3.50 0 7 15 37.90 5.50 1 -7 15 32.40 7.10 1 -7 15 36.00 2.80 -1 -7 -15 31.60 2.70 1 7 15 41.90 3.30 1 7 15 25.60 9.50 2 -7 15 109.89 17.20 2 -7 15 82.99 4.80 -2 -7 -15 77.79 4.80 2 7 15 81.39 5.10 3 -7 15 44.10 4.40 3 -7 15 49.50 3.40 -3 -7 -15 54.19 3.50 3 -7 15 53.79 9.00 3 7 15 39.70 9.60 3 7 15 46.10 3.60 4 -7 15 4.00 9.80 4 -7 15 2.10 1.10 4 -7 15 0.20 1.70 4 7 15 2.40 8.60 4 7 15 0.60 1.40 5 -7 15 45.80 11.50 5 -7 15 50.79 5.60 5 7 15 41.40 15.50 7 -8 -15 -0.30 1.70 7 8 -15 1.20 3.00 -7 8 15 2.30 4.80 7 8 -15 5.70 4.70 6 -8 -15 36.00 3.10 6 8 -15 43.00 5.80 -6 8 15 33.80 6.30 6 8 -15 36.00 4.60 5 -8 -15 3.40 1.30 -5 8 15 2.00 4.10 5 8 -15 2.60 2.80 5 8 -15 6.00 2.30 4 -8 -15 50.89 3.50 4 -8 -15 43.90 2.80 -4 8 15 39.40 6.80 4 8 -15 50.29 4.80 4 8 -15 47.30 3.20 -3 -8 15 95.69 5.40 3 -8 -15 97.79 5.50 3 -8 -15 101.09 5.10 3 8 -15 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34.50 4.70 4 -4 -19 29.60 2.30 4 4 -19 35.20 3.20 4 4 -19 35.20 2.70 3 -4 -19 1.10 1.10 3 -4 -19 1.20 1.00 3 4 -19 2.20 1.30 2 -4 -19 50.19 4.10 -2 -4 19 54.59 3.80 2 -4 -19 46.90 3.40 -2 4 19 59.29 4.20 -2 4 19 47.50 6.40 -1 -4 19 19.70 2.60 1 -4 -19 17.40 2.20 1 -4 -19 12.00 2.50 -1 4 19 21.70 2.80 0 -4 19 44.50 3.70 0 -4 -19 49.10 3.60 0 4 19 56.99 4.20 1 -4 19 134.19 9.10 1 -4 19 116.29 17.30 1 -4 19 144.99 7.50 -1 -4 -19 133.79 8.00 1 4 19 145.09 7.80 2 -4 19 23.20 3.00 2 -4 19 22.30 3.60 -2 -4 -19 19.00 2.60 2 4 19 21.40 3.20 3 -4 19 -24.40 14.20 3 -4 19 3.00 2.90 3 -4 19 0.70 2.30 3 4 19 0.20 2.70 3 4 19 18.80 20.70 6 -5 -19 27.90 3.00 -6 5 19 27.10 5.90 5 -5 -19 21.70 2.80 -5 5 19 15.30 5.40 5 5 -19 18.10 2.30 4 -5 -19 14.20 2.30 4 5 -19 16.40 2.30 -4 5 19 17.00 5.40 3 -5 -19 0.70 1.10 3 -5 -19 -0.70 1.20 -3 5 19 -1.90 4.80 3 5 -19 2.40 1.40 2 -5 -19 123.99 6.70 2 -5 -19 125.59 7.20 -2 -5 19 133.89 7.10 -2 5 19 126.59 10.50 -2 5 19 143.79 7.50 -1 -5 19 8.40 1.80 1 -5 -19 9.10 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19 0.70 17.50 5 -7 -19 -0.20 2.20 -5 7 19 1.30 5.30 4 -7 -19 45.30 3.90 -4 7 19 50.69 7.40 3 -7 -19 -0.20 1.50 3 -7 -19 0.10 1.10 -3 7 19 2.00 4.90 3 7 -19 0.60 1.30 -2 -7 19 2.60 1.50 2 -7 -19 0.70 1.40 2 -7 -19 -1.10 2.20 -2 7 19 3.50 1.70 2 7 -19 1.50 1.50 -1 -7 19 156.98 9.60 1 -7 -19 128.39 7.20 1 -7 -19 129.19 8.30 -1 7 19 152.48 8.70 0 -7 19 75.29 4.90 0 -7 -19 74.99 4.70 0 -7 -19 70.69 4.90 0 7 19 70.19 5.30 -1 -7 -19 12.90 2.50 -1 -7 -19 13.70 2.30 1 -7 19 15.10 2.60 1 -7 19 13.30 3.20 1 7 19 17.50 3.20 -2 -7 -19 5.80 2.20 2 -7 19 1.90 15.50 2 -7 19 5.90 2.40 2 -7 19 10.60 3.30 2 7 19 2.60 2.90 2 7 19 1.00 32.00 5 -8 -19 14.50 2.50 5 8 -19 15.90 4.40 -5 8 19 6.30 5.30 4 -8 -19 111.29 6.30 -4 8 19 97.09 10.90 4 8 -19 102.59 8.90 3 -8 -19 24.10 2.70 3 -8 -19 28.90 2.60 3 8 -19 31.90 2.80 -3 8 19 18.30 6.00 -2 -8 19 1.60 1.50 2 -8 -19 0.90 1.50 2 -8 -19 -0.60 1.30 2 8 -19 3.80 1.60 -2 8 19 1.30 1.90 1 -8 -19 -0.50 1.30 -1 -8 19 1.40 1.50 1 -8 -19 1.90 1.50 -1 8 19 1.00 1.90 0 -8 19 4.80 1.90 0 -8 -19 2.20 1.40 0 -8 -19 0.80 1.50 0 8 19 0.40 2.10 1 -8 19 1.90 2.60 1 -8 19 -0.80 1.90 -1 -8 -19 -3.50 1.60 1 8 19 0.20 2.50 2 -8 19 65.09 5.20 -2 -8 -19 65.99 5.00 2 -8 19 77.39 6.50 2 -8 19 70.49 17.00 2 8 19 64.09 5.40 4 -9 -19 173.98 8.50 4 9 -19 156.38 9.60 -4 9 19 154.48 12.70 3 -9 -19 3.40 1.90 3 -9 -19 -1.20 1.30 -3 9 19 -6.50 5.60 -2 -9 19 27.70 3.10 2 -9 -19 29.10 2.80 2 -9 -19 27.40 2.70 2 9 -19 23.80 3.10 1 -9 -19 0.90 1.50 -1 -9 19 1.40 1.70 1 -9 -19 1.00 1.40 -1 9 19 -1.00 2.20 0 -9 -19 21.30 2.70 0 -9 19 21.40 2.90 0 9 19 17.10 3.40 1 -9 19 19.20 3.10 1 -9 19 21.20 4.30 -1 -9 -19 16.80 2.80 2 -9 19 0.90 2.30 2 -9 19 5.60 3.20 2 9 19 3.70 3.10 4 -10 -19 4.10 2.20 -4 10 19 0.70 5.40 4 10 -19 0.20 3.20 3 -10 -19 43.90 3.90 3 -10 -19 32.10 2.80 -3 10 19 29.30 6.10 2 -10 -19 54.59 4.00 2 -10 -19 47.80 3.80 -2 -10 19 47.70 4.20 1 -10 -19 15.10 2.40 -1 -10 19 17.80 3.70 -1 10 19 20.30 3.90 0 -10 -19 38.50 4.30 0 -10 19 47.10 6.60 0 10 19 45.20 6.00 1 -10 19 14.20 3.70 1 -10 19 12.50 2.70 -1 -10 -19 12.50 2.60 1 10 19 17.90 3.70 3 -11 -19 0.90 1.50 2 -11 -19 11.70 2.10 -2 -11 19 5.30 2.40 1 -11 -19 18.10 2.80 -1 -11 19 16.10 2.80 -1 11 19 15.70 3.90 0 -11 19 4.90 2.40 0 -11 -19 3.20 2.00 0 11 19 2.30 3.50 5 0 -20 15.80 4.20 4 0 -20 231.58 10.90 4 0 -20 256.57 11.90 3 0 -20 134.09 8.30 2 0 -20 36.50 4.00 2 0 -20 35.50 3.20 -2 0 20 40.30 4.40 -1 0 20 30.40 4.10 1 0 -20 25.20 2.80 0 0 20 261.07 14.80 1 0 20 5.80 1.90 1 0 20 0.90 2.00 -1 0 -20 0.30 1.70 2 0 20 110.79 7.70 -2 0 -20 105.29 6.60 2 0 20 43.50 25.00 2 0 20 111.69 7.00 5 -1 -20 1.90 3.10 5 1 -20 1.10 2.80 4 -1 -20 4.20 2.10 4 -1 -20 3.20 1.10 4 1 -20 0.90 1.70 4 1 -20 2.30 1.10 3 -1 -20 24.30 3.70 3 -1 -20 19.20 2.20 3 1 -20 18.50 2.60 3 1 -20 26.30 4.10 2 -1 -20 -2.50 1.10 -2 -1 20 0.70 1.50 2 -1 -20 -1.10 1.50 2 1 -20 -0.30 1.30 2 1 -20 -1.50 1.60 -2 1 20 0.70 1.50 -1 -1 20 1.40 1.90 1 -1 -20 0.40 1.40 1 -1 -20 -0.40 1.60 1 1 -20 -0.10 1.40 -1 1 20 -0.40 1.90 0 -1 -20 3.50 2.00 0 -1 20 8.60 2.00 0 -1 20 7.80 2.40 0 1 -20 9.20 2.50 0 1 20 6.80 2.40 1 -1 20 25.60 3.30 1 -1 20 29.40 3.50 -1 -1 -20 25.30 3.00 -1 1 -20 23.00 2.90 1 1 20 26.00 3.30 2 -1 20 60.79 5.40 2 -1 20 52.79 4.80 2 -1 20 117.09 27.80 -2 -1 -20 57.79 4.80 2 1 20 44.30 27.20 -2 1 -20 52.79 4.70 2 1 20 66.19 5.20 5 -2 -20 14.20 3.70 5 2 -20 13.90 2.40 4 -2 -20 0.20 1.70 4 -2 -20 0.60 0.90 4 2 -20 -1.20 2.30 4 2 -20 -2.00 1.00 3 -2 -20 7.60 2.00 3 -2 -20 11.80 1.80 3 2 -20 11.80 1.90 3 2 -20 14.50 2.70 2 -2 -20 90.09 6.00 2 -2 -20 86.99 5.30 -2 -2 20 93.59 5.70 2 2 -20 94.49 6.40 -2 2 20 97.29 5.90 1 -2 -20 153.68 7.80 1 -2 -20 151.08 8.70 0 -2 20 29.80 3.40 0 -2 -20 30.50 3.20 0 -2 20 34.70 3.70 0 2 20 34.60 3.60 1 -2 20 -1.00 1.90 -1 -2 -20 0.00 1.70 1 -2 20 3.90 2.10 -1 2 -20 3.40 1.90 1 2 20 -0.10 2.20 -2 -2 -20 -1.30 2.00 2 -2 20 0.50 2.40 2 -2 20 -0.90 2.50 2 2 20 1.00 2.60 -2 2 -20 -4.10 2.10 5 -3 -20 41.90 5.20 5 3 -20 44.60 3.90 4 -3 -20 3.00 2.00 4 3 -20 3.00 1.30 4 3 -20 7.10 2.00 3 -3 -20 95.49 5.80 3 -3 -20 94.19 5.10 3 3 -20 92.99 6.00 3 3 -20 89.19 5.20 -2 -3 20 50.29 4.00 -2 3 20 59.19 4.40 -1 -3 20 16.80 2.50 -1 3 20 24.30 3.10 0 -3 -20 82.89 5.90 0 -3 20 84.99 5.40 0 -3 20 80.59 6.30 0 -3 -20 82.99 5.20 0 3 20 88.39 5.70 -1 -3 -20 150.18 8.10 1 -3 20 155.38 9.00 1 -3 20 154.88 8.40 1 3 20 156.88 8.70 2 -3 20 10.80 26.10 -2 -3 -20 1.30 2.10 2 -3 20 -1.10 2.70 2 3 20 -1.80 25.20 -2 3 -20 1.30 2.30 5 -4 -20 3.20 2.20 5 4 -20 3.10 1.80 -5 4 20 7.20 4.80 4 -4 -20 0.60 1.90 4 4 -20 -0.50 1.10 -4 4 20 4.10 4.40 4 4 -20 2.60 1.70 3 -4 -20 8.40 1.70 3 -4 -20 9.80 2.10 3 4 -20 8.90 2.30 -3 4 20 18.70 4.90 2 -4 -20 -0.20 1.30 2 -4 -20 -0.30 1.60 -2 -4 20 -0.20 1.40 2 4 -20 -0.10 1.70 -2 4 20 5.50 1.80 -1 -4 20 37.90 3.80 1 -4 -20 41.10 4.00 1 -4 -20 34.40 3.30 -1 4 20 38.10 5.60 0 -4 -20 11.90 2.70 0 -4 -20 11.80 2.20 0 -4 20 12.00 2.40 0 -4 20 7.90 2.80 0 4 20 9.30 2.50 1 -4 20 14.40 3.10 -1 -4 -20 7.40 2.50 -1 -4 -20 9.60 2.30 1 -4 20 13.30 2.70 1 4 20 10.60 2.80 2 -4 20 6.80 2.70 2 -4 20 28.80 17.10 2 -4 20 1.20 2.80 -2 -4 -20 6.40 2.40 2 4 20 32.20 28.10 2 4 20 6.80 3.00 5 -5 -20 -1.50 1.90 -5 5 20 6.70 5.10 4 -5 -20 1.40 1.90 -4 5 20 5.80 7.60 4 5 -20 4.30 1.80 3 -5 -20 59.39 4.00 3 -5 -20 67.99 4.70 3 5 -20 69.29 4.90 -3 5 20 62.39 7.40 -2 -5 20 -0.10 1.50 2 -5 -20 0.40 1.40 2 -5 -20 2.50 1.80 -2 5 20 2.90 1.90 2 5 -20 1.50 1.90 1 -5 -20 17.20 2.40 -1 -5 20 19.40 2.80 1 -5 -20 23.20 3.20 -1 5 20 21.10 3.00 0 -5 -20 21.80 3.10 0 -5 20 24.80 3.10 0 -5 20 23.50 4.00 0 -5 -20 31.70 3.10 0 5 20 22.70 3.20 1 -5 20 30.50 4.10 1 -5 20 29.30 3.50 -1 -5 -20 21.80 3.00 1 5 20 23.80 3.70 -2 -5 -20 2.20 3.40 2 -5 20 -3.10 2.20 2 -5 20 5.00 3.10 2 -5 20 -25.50 19.70 2 5 20 0.70 2.80 4 -6 -20 -0.20 2.80 4 6 -20 4.20 1.70 -4 6 20 1.10 4.90 4 6 -20 2.60 1.40 3 -6 -20 0.00 1.30 3 -6 -20 -0.70 1.70 -3 6 20 -4.60 5.10 3 6 -20 0.30 1.60 -2 -6 20 110.49 6.40 2 -6 -20 106.49 6.30 2 -6 -20 105.79 5.90 2 6 -20 103.19 6.70 1 -6 -20 23.10 3.10 1 -6 -20 17.60 2.50 -1 -6 20 21.70 2.90 -1 6 20 20.50 3.20 0 -6 20 -1.50 2.60 0 -6 20 4.20 2.20 0 -6 -20 4.80 2.00 0 -6 -20 5.00 2.20 0 6 20 4.30 2.50 1 -6 20 17.80 3.10 -1 -6 -20 17.10 3.20 -1 -6 -20 17.30 3.50 1 6 20 19.70 3.70 2 -6 20 14.00 3.60 2 -6 20 17.50 3.10 2 6 20 18.70 3.60 4 -7 -20 3.10 2.20 -4 7 20 -3.40 5.00 3 -7 -20 27.40 2.70 3 -7 -20 26.70 3.10 3 7 -20 27.30 3.00 2 -7 -20 5.20 1.80 2 -7 -20 3.70 1.90 2 7 -20 7.30 2.30 1 -7 -20 4.10 1.90 1 -7 -20 5.70 2.00 -1 -7 20 2.70 2.10 -1 7 20 5.80 2.70 0 -7 20 -0.10 2.20 0 -7 -20 5.80 2.60 0 -7 20 -6.90 2.90 0 -7 -20 0.30 1.90 0 7 20 3.10 2.90 -1 -7 -20 4.50 2.30 1 -7 20 3.60 2.90 1 -7 20 3.60 2.50 1 7 20 9.10 3.20 4 -8 -20 69.19 4.90 -4 8 20 46.80 7.50 3 -8 -20 4.70 1.60 3 -8 -20 3.70 2.00 2 -8 -20 14.00 2.20 2 -8 -20 18.70 2.90 -2 -8 20 24.00 3.20 2 8 -20 14.40 2.60 1 -8 -20 1.90 1.80 1 -8 -20 4.20 2.10 -1 -8 20 1.40 2.60 -1 8 20 7.70 2.90 0 -8 -20 35.20 4.10 0 -8 20 21.80 4.90 0 -8 20 40.40 4.00 0 8 20 35.70 4.50 -1 -8 -20 8.70 2.40 1 -8 20 3.20 2.50 1 -8 20 16.60 3.70 1 8 20 5.90 3.30 3 -9 -20 44.00 3.80 3 -9 -20 40.00 3.30 2 -9 -20 21.50 2.50 -2 -9 20 25.30 4.10 2 -9 -20 19.70 2.80 -1 -9 20 62.89 4.90 1 -9 -20 58.29 4.40 -1 9 20 53.49 5.30 0 -9 20 16.90 3.00 0 -9 -20 14.00 2.50 0 -9 20 6.90 3.70 0 9 20 10.30 3.60 4 0 -21 -2.60 2.00 3 0 -21 -1.30 1.90 3 0 -21 0.30 1.50 2 0 -21 1.50 2.20 2 0 -21 -0.60 1.70 -1 0 21 -0.70 2.00 1 0 -21 1.80 2.00 1 0 -21 2.00 2.40 0 0 21 -1.80 2.20 0 0 -21 0.70 2.10 1 0 21 2.20 2.80 -1 0 -21 -1.80 2.20 4 -1 -21 53.99 4.80 4 1 -21 55.09 4.80 3 -1 -21 19.80 3.10 3 -1 -21 24.20 2.50 3 1 -21 22.60 2.60 3 1 -21 26.30 3.30 2 -1 -21 55.59 4.20 2 -1 -21 50.09 4.60 2 1 -21 54.69 4.20 2 1 -21 55.69 5.10 1 -1 -21 14.40 3.10 -1 -1 21 15.80 2.80 1 -1 -21 9.70 2.30 1 1 -21 15.80 3.10 1 1 -21 10.70 2.40 -1 1 21 23.20 3.30 0 -1 -21 48.10 4.10 0 -1 21 52.79 4.60 0 1 21 52.19 4.70 0 1 -21 45.60 4.10 -1 -1 -21 125.39 7.20 1 -1 21 122.99 7.70 -1 1 -21 123.09 7.20 1 1 21 115.59 7.70 4 -2 -21 23.10 3.10 4 2 -21 27.20 3.30 3 -2 -21 4.20 2.20 3 -2 -21 3.20 1.70 3 2 -21 3.10 1.70 3 2 -21 4.70 2.40 2 -2 -21 15.60 3.00 -2 -2 21 22.00 3.80 2 -2 -21 15.00 2.40 2 2 -21 15.70 3.10 2 2 -21 18.30 2.60 1 -2 -21 90.79 5.60 -1 -2 21 99.09 6.10 1 -2 -21 91.19 6.50 1 2 -21 80.69 6.50 -1 2 21 90.19 6.20 1 2 -21 89.99 5.70 0 -2 -21 5.80 2.30 0 -2 21 15.50 2.70 0 -2 21 8.30 2.60 0 -2 -21 3.00 2.70 0 2 21 5.10 2.80 0 2 -21 4.20 2.30 -1 -2 -21 3.60 2.40 1 -2 21 6.50 2.80 1 -2 21 -0.60 2.60 1 2 21 5.30 3.00 -1 2 -21 2.20 2.40 4 -3 -21 1.30 2.10 -4 3 21 12.70 4.60 4 3 -21 6.00 2.30 3 -3 -21 4.70 2.10 3 -3 -21 1.40 2.20 3 3 -21 5.30 3.30 3 3 -21 7.70 2.20 2 -3 -21 99.79 6.50 -2 -3 21 101.09 6.40 2 -3 -21 106.09 5.90 2 3 -21 102.89 6.00 2 3 -21 100.69 6.80 -1 -3 21 40.00 4.70 -1 -3 21 51.29 4.50 1 -3 -21 43.70 4.30 1 -3 -21 41.50 3.80 -1 3 21 41.80 5.20 0 -3 -21 5.80 2.40 0 -3 -21 5.50 3.40 0 -3 21 5.20 4.70 0 -3 21 11.90 2.80 0 3 -21 5.10 2.80 1 -3 21 8.00 3.10 1 -3 21 4.50 2.80 -1 -3 -21 1.70 2.80 -1 -3 -21 6.60 2.50 -1 3 -21 10.20 2.80 1 3 21 12.50 3.30 4 -4 -21 75.49 5.10 4 4 -21 73.59 5.80 -4 4 21 68.69 8.70 3 -4 -21 15.00 4.70 3 -4 -21 10.00 2.10 3 4 -21 9.40 3.80 3 4 -21 11.90 2.70 2 -4 -21 3.70 1.90 2 -4 -21 7.10 2.70 -2 -4 21 1.30 2.00 2 4 -21 1.30 2.40 1 -4 -21 11.70 2.80 -1 -4 21 3.50 3.10 1 -4 -21 10.10 2.30 -1 -4 21 9.30 4.10 -1 4 21 7.10 2.80 0 -4 21 43.50 5.00 0 -4 -21 35.30 4.30 0 -4 21 52.49 5.10 0 4 21 38.20 4.40 1 -4 21 156.98 8.20 -1 -4 -21 136.59 7.70 1 -4 21 142.79 10.10 -1 -4 -21 123.69 8.40 -1 4 -21 132.29 7.90 1 4 21 138.59 8.50 3 -5 -21 37.00 3.10 3 -5 -21 43.60 4.00 3 5 -21 42.10 4.00 3 5 -21 37.00 3.30 2 -5 -21 132.09 9.00 -2 -5 21 146.59 8.00 2 -5 -21 137.19 10.70 2 5 -21 126.49 8.20 1 -5 -21 4.30 2.50 1 -5 -21 2.10 2.20 -1 -5 21 1.60 2.40 -1 5 21 2.80 2.80 0 -5 21 -2.10 2.40 0 -5 -21 -1.90 2.60 0 -5 -21 0.60 2.10 0 -5 21 4.00 2.70 0 5 21 2.00 3.10 3 -6 -21 9.30 2.30 3 -6 -21 8.30 1.80 2 -6 -21 5.40 2.00 2 -6 -21 6.40 2.40 2 6 -21 5.90 2.70 1 -6 -21 52.89 4.40 -1 -6 21 60.79 4.80 1 -6 -21 53.39 5.00 1 6 -21 63.19 5.50 -1 6 21 48.30 5.20 0 -6 21 51.59 4.50 0 -6 -21 64.69 7.70 0 -6 21 49.00 5.30 0 -6 -21 45.90 4.00 0 6 21 39.90 4.80 2 -7 -21 2.60 2.30 2 -7 -21 7.10 1.90 1 -7 -21 3.00 2.10 1 -7 -21 -1.80 4.20 -1 -7 21 2.20 2.80 1 7 -21 4.50 3.00 2 0 -22 5.00 2.10 2 0 -22 12.30 3.10 1 0 -22 0.30 2.80 1 0 -22 -1.20 2.10 -1 0 22 2.70 3.20 2 -1 -22 2.10 2.60 2 -1 -22 -0.80 1.80 2 1 -22 -2.90 1.90 2 1 -22 -0.90 2.50 1 -1 -22 249.18 12.10 -1 -1 22 216.28 13.10 1 -1 -22 227.18 11.10 1 1 -22 247.28 12.30 1 1 -22 228.78 11.20 -1 1 22 214.78 13.70 2 -2 -22 55.19 4.10 2 -2 -22 45.70 4.40 2 2 -22 44.40 4.50 2 2 -22 45.00 3.80 -1 -2 22 14.80 6.00 1 -2 -22 16.50 2.60 1 -2 -22 19.10 3.40 1 2 -22 13.50 2.70 1 2 -22 10.40 3.20 2 -3 -22 6.80 2.00 2 3 -22 5.00 2.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 8645 _olex2_exptl_crystal_mounting_method no _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.23144(5) 0.56804(2) 0.57099(2) 0.02528(11) Uani 1 1 d . . . . . P1 P 0.39739(4) 0.29815(2) 0.41642(2) 0.02117(11) Uani 1 1 d . . . . . O1 O 0.52625(12) 0.26025(6) 0.37982(6) 0.0273(2) Uani 1 1 d . . . . . N1 N 0.50646(15) 0.36143(7) 0.63563(7) 0.0226(3) Uani 1 1 d . . . . . N2 N 0.16992(15) 0.48079(7) 0.33311(7) 0.0229(3) Uani 1 1 d . . . . . C12 C 0.59705(18) 0.29615(8) 0.63775(9) 0.0243(3) Uani 1 1 d . . . . . C11 C 0.57290(18) 0.26802(8) 0.56308(9) 0.0240(3) Uani 1 1 d . . . . . C33 C 0.21583(18) 0.23989(8) 0.41514(8) 0.0226(3) Uani 1 1 d . . . . . C25 C 0.25189(17) 0.43989(8) 0.39504(8) 0.0215(3) Uani 1 1 d . . . . . C17 C 0.26350(17) 0.46967(8) 0.47027(8) 0.0213(3) Uani 1 1 d . . . . . C6 C 0.40444(18) 0.47465(8) 0.67924(8) 0.0236(3) Uani 1 1 d . . . . . C7 C 0.33817(18) 0.48958(8) 0.60101(8) 0.0226(3) Uani 1 1 d . . . . . C34 C 0.05180(18) 0.26556(9) 0.39997(9) 0.0268(3) Uani 1 1 d . . . . . H34 H 0.032050 0.315485 0.389358 0.032 Uiso 1 1 calc R U . . . C28 C 0.18796(18) 0.44428(8) 0.26569(9) 0.0243(3) Uani 1 1 d . . . . . C10 C 0.46829(18) 0.31764(8) 0.51408(8) 0.0226(3) Uani 1 1 d . . . . . C8 C 0.34545(17) 0.44153(8) 0.54242(8) 0.0211(3) Uani 1 1 d . . . . . C35 C -0.0831(2) 0.21923(10) 0.40016(9) 0.0325(4) Uani 1 1 d . . . . . H35 H -0.194443 0.237483 0.390557 0.039 Uiso 1 1 calc R U . . . C24 C 0.08741(18) 0.54682(8) 0.34229(9) 0.0236(3) Uani 1 1 d . . . . . C13 C 0.7048(2) 0.26203(9) 0.69673(10) 0.0303(4) Uani 1 1 d . . . . . C16 C 0.65360(19) 0.20364(8) 0.54771(10) 0.0280(3) Uani 1 1 d . . . . . H16 H 0.637563 0.183882 0.497694 0.034 Uiso 1 1 calc R U . . . C9 C 0.43296(17) 0.37445(8) 0.55951(8) 0.0214(3) Uani 1 1 d . . . . . C21 C -0.0642(2) 0.67937(9) 0.36561(10) 0.0326(4) Uani 1 1 d . . . . . H21 H -0.113048 0.725078 0.372952 0.039 Uiso 1 1 calc R U . . . C38 C 0.24119(19) 0.16620(9) 0.42940(9) 0.0283(3) Uani 1 1 d . . . . . H38 H 0.352255 0.147683 0.439788 0.034 Uiso 1 1 calc R U . . . C36 C -0.0550(2) 0.14644(10) 0.41436(9) 0.0330(4) Uani 1 1 d . . . . . H36 H -0.147321 0.114600 0.414315 0.040 Uiso 1 1 calc R U . . . C5 C 0.48319(18) 0.40723(8) 0.69659(8) 0.0240(3) Uani 1 1 d . . . . . C27 C 0.27590(18) 0.37964(8) 0.28634(9) 0.0242(3) Uani 1 1 d . . . . . C1 C 0.38433(19) 0.52263(9) 0.73830(9) 0.0283(3) Uani 1 1 d . . . . . H1 H 0.334918 0.568724 0.726352 0.034 Uiso 1 1 calc R U . . . C19 C 0.10578(18) 0.57739(8) 0.41566(9) 0.0237(3) Uani 1 1 d . . . . . C22 C -0.0876(2) 0.64754(9) 0.29413(10) 0.0321(4) Uani 1 1 d . . . . . H22 H -0.155164 0.671141 0.252609 0.038 Uiso 1 1 calc R U . . . C26 C 0.31490(18) 0.37720(8) 0.36813(8) 0.0231(3) Uani 1 1 d . . . . . C32 C 0.3184(2) 0.33302(9) 0.22973(9) 0.0285(3) Uani 1 1 d . . . . . H32 H 0.377193 0.289194 0.243283 0.034 Uiso 1 1 calc R U . . . C18 C 0.19660(18) 0.53735(8) 0.47804(9) 0.0234(3) Uani 1 1 d . . . . . C23 C -0.0141(2) 0.58214(9) 0.28242(10) 0.0292(3) Uani 1 1 d . . . . . C2 C 0.4354(2) 0.50366(9) 0.81326(9) 0.0321(4) Uani 1 1 d . . . . . H2 H 0.423614 0.536658 0.853058 0.039 Uiso 1 1 calc R U . . . C29 C 0.1439(2) 0.46337(10) 0.18893(9) 0.0315(4) Uani 1 1 d . . . . . C4 C 0.5274(2) 0.38749(9) 0.77301(9) 0.0290(3) Uani 1 1 d . . . . . C14 C 0.7825(2) 0.19891(9) 0.67991(10) 0.0342(4) Uani 1 1 d . . . . . H14 H 0.855492 0.174804 0.719278 0.041 Uiso 1 1 calc R U . . . C20 C 0.0304(2) 0.64408(9) 0.42592(10) 0.0296(3) Uani 1 1 d . . . . . H20 H 0.044833 0.665310 0.475252 0.036 Uiso 1 1 calc R U . . . C3 C 0.5044(2) 0.43555(9) 0.83003(9) 0.0322(4) Uani 1 1 d . . . . . H3 H 0.536512 0.421714 0.881830 0.039 Uiso 1 1 calc R U . . . C15 C 0.7567(2) 0.16965(9) 0.60672(10) 0.0326(4) Uani 1 1 d . . . . . H15 H 0.810772 0.125697 0.597264 0.039 Uiso 1 1 calc R U . . . C30 C 0.1867(2) 0.41656(10) 0.13450(9) 0.0342(4) Uani 1 1 d . . . . . H30 H 0.156473 0.428506 0.082072 0.041 Uiso 1 1 calc R U . . . C31 C 0.2732(2) 0.35218(9) 0.15451(9) 0.0318(4) Uani 1 1 d . . . . . H31 H 0.301149 0.321305 0.115671 0.038 Uiso 1 1 calc R U . . . C37 C 0.1067(2) 0.11968(9) 0.42863(9) 0.0322(4) Uani 1 1 d . . . . . H37 H 0.125495 0.069487 0.437892 0.039 Uiso 1 1 calc R U . . . H13 H 0.740(2) 0.2797(9) 0.7438(11) 0.033(5) Uiso 1 1 d D . . . . H4 H 0.558(2) 0.3454(10) 0.7899(10) 0.032(5) Uiso 1 1 d D . . . . H23 H -0.047(2) 0.5649(10) 0.2387(11) 0.042(6) Uiso 1 1 d D . . . . H29 H 0.099(2) 0.5042(11) 0.1693(11) 0.043(5) Uiso 1 1 d D . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0269(2) 0.02256(19) 0.0263(2) -0.00247(14) 0.00410(15) 0.00192(14) P1 0.01581(19) 0.02204(19) 0.02541(19) -0.00261(14) 0.00255(14) 0.00080(14) O1 0.0199(5) 0.0300(6) 0.0325(6) -0.0045(5) 0.0058(4) 0.0033(4) N1 0.0196(6) 0.0230(6) 0.0243(6) 0.0011(5) 0.0006(5) -0.0011(5) N2 0.0209(6) 0.0236(6) 0.0236(6) -0.0001(5) 0.0022(5) -0.0008(5) C12 0.0186(7) 0.0236(7) 0.0303(8) 0.0023(6) 0.0027(6) -0.0019(6) C11 0.0165(7) 0.0241(8) 0.0308(8) 0.0014(6) 0.0018(6) -0.0026(6) C33 0.0189(7) 0.0267(8) 0.0218(7) -0.0044(6) 0.0025(6) -0.0003(6) C25 0.0156(7) 0.0232(7) 0.0252(7) 0.0016(6) 0.0020(5) -0.0022(6) C17 0.0166(7) 0.0219(7) 0.0255(7) 0.0001(6) 0.0036(6) -0.0010(6) C6 0.0190(7) 0.0262(8) 0.0258(7) -0.0017(6) 0.0041(6) -0.0052(6) C7 0.0187(7) 0.0217(7) 0.0278(8) -0.0008(6) 0.0046(6) -0.0017(6) C34 0.0205(7) 0.0309(8) 0.0287(8) -0.0048(6) 0.0030(6) 0.0011(6) C28 0.0211(7) 0.0263(8) 0.0252(7) -0.0018(6) 0.0029(6) -0.0044(6) C10 0.0174(7) 0.0222(7) 0.0273(7) -0.0001(6) 0.0013(6) -0.0011(6) C8 0.0160(7) 0.0227(7) 0.0248(7) -0.0006(6) 0.0034(6) -0.0029(6) C35 0.0183(7) 0.0463(10) 0.0327(9) -0.0072(7) 0.0037(6) -0.0013(7) C24 0.0180(7) 0.0234(7) 0.0298(8) 0.0029(6) 0.0051(6) -0.0017(6) C13 0.0255(8) 0.0333(9) 0.0305(9) 0.0042(7) -0.0010(7) -0.0016(7) C16 0.0214(8) 0.0259(8) 0.0363(9) 0.0003(6) 0.0036(6) 0.0000(6) C9 0.0157(7) 0.0237(7) 0.0244(7) -0.0006(6) 0.0019(5) -0.0033(6) C21 0.0298(9) 0.0255(8) 0.0435(10) 0.0071(7) 0.0088(7) 0.0060(7) C38 0.0227(8) 0.0283(8) 0.0326(8) -0.0017(7) 0.0004(6) -0.0007(6) C36 0.0272(8) 0.0424(10) 0.0299(8) -0.0070(7) 0.0064(7) -0.0139(7) C5 0.0192(7) 0.0266(8) 0.0259(7) -0.0008(6) 0.0027(6) -0.0060(6) C27 0.0204(7) 0.0255(8) 0.0266(8) -0.0016(6) 0.0035(6) -0.0042(6) C1 0.0251(8) 0.0289(8) 0.0309(8) -0.0038(7) 0.0050(6) -0.0033(6) C19 0.0196(7) 0.0234(7) 0.0284(8) 0.0029(6) 0.0052(6) -0.0012(6) C22 0.0248(8) 0.0336(9) 0.0375(9) 0.0109(7) 0.0037(7) 0.0037(7) C26 0.0183(7) 0.0253(8) 0.0256(7) -0.0015(6) 0.0030(6) -0.0008(6) C32 0.0286(8) 0.0270(8) 0.0305(8) -0.0042(6) 0.0068(6) -0.0049(7) C18 0.0201(7) 0.0236(7) 0.0267(7) -0.0014(6) 0.0049(6) -0.0016(6) C23 0.0255(8) 0.0323(9) 0.0288(8) 0.0048(7) 0.0013(6) -0.0007(7) C2 0.0301(9) 0.0387(9) 0.0278(8) -0.0067(7) 0.0054(7) -0.0053(7) C29 0.0323(9) 0.0335(9) 0.0275(8) 0.0028(7) 0.0009(7) -0.0011(7) C4 0.0262(8) 0.0315(9) 0.0285(8) 0.0036(7) 0.0019(6) -0.0038(7) C14 0.0273(8) 0.0327(9) 0.0403(10) 0.0106(7) -0.0014(7) 0.0038(7) C20 0.0290(8) 0.0263(8) 0.0345(9) 0.0019(7) 0.0081(7) 0.0023(7) C3 0.0290(8) 0.0426(10) 0.0242(8) 0.0010(7) 0.0023(6) -0.0060(7) C15 0.0254(8) 0.0266(8) 0.0450(10) 0.0043(7) 0.0036(7) 0.0048(7) C30 0.0388(10) 0.0384(9) 0.0249(8) -0.0010(7) 0.0032(7) -0.0064(8) C31 0.0342(9) 0.0337(9) 0.0287(8) -0.0076(7) 0.0089(7) -0.0093(7) C37 0.0369(9) 0.0285(8) 0.0304(8) -0.0021(7) 0.0030(7) -0.0057(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2543 0.3332 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.2925 0.4295 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C18 S1 C7 90.91(7) . . ? O1 P1 C33 109.61(7) . . ? O1 P1 C10 112.61(6) . . ? O1 P1 C26 114.34(7) . . ? C10 P1 C33 105.39(7) . . ? C26 P1 C33 104.07(7) . . ? C26 P1 C10 110.10(7) . . ? C12 N1 C5 128.79(13) . . ? C9 N1 C12 108.00(12) . . ? C9 N1 C5 123.18(12) . . ? C25 N2 C24 123.00(12) . . ? C28 N2 C25 107.95(12) . . ? C28 N2 C24 129.06(13) . . ? N1 C12 C11 107.37(13) . . ? C13 C12 N1 131.57(15) . . ? C13 C12 C11 120.91(14) . . ? C12 C11 C10 108.22(13) . . ? C16 C11 C12 119.84(14) . . ? C16 C11 C10 131.85(15) . . ? C34 C33 P1 122.80(12) . . ? C34 C33 C38 118.39(14) . . ? C38 C33 P1 118.81(11) . . ? N2 C25 C17 118.26(13) . . ? C26 C25 N2 109.44(13) . . ? C26 C25 C17 132.21(14) . . ? C25 C17 C8 129.92(13) . . ? C18 C17 C25 118.28(13) . . ? C18 C17 C8 111.69(13) . . ? C5 C6 C7 117.83(13) . . ? C1 C6 C7 122.22(14) . . ? C1 C6 C5 119.83(14) . . ? C6 C7 S1 123.43(11) . . ? C8 C7 S1 112.84(11) . . ? C8 C7 C6 123.65(14) . . ? C33 C34 H34 119.6 . . ? C35 C34 C33 120.86(15) . . ? C35 C34 H34 119.6 . . ? N2 C28 C27 107.65(13) . . ? C29 C28 N2 131.80(15) . . ? C29 C28 C27 120.44(14) . . ? C11 C10 P1 121.81(11) . . ? C9 C10 P1 131.37(11) . . ? C9 C10 C11 106.67(13) . . ? C7 C8 C17 111.72(13) . . ? C7 C8 C9 118.48(13) . . ? C9 C8 C17 129.77(13) . . ? C34 C35 H35 120.1 . . ? C36 C35 C34 119.74(15) . . ? C36 C35 H35 120.1 . . ? C19 C24 N2 118.21(13) . . ? C23 C24 N2 123.11(14) . . ? C23 C24 C19 118.66(14) . . ? C12 C13 H13 126.6(10) . . ? C14 C13 C12 117.93(16) . . ? C14 C13 H13 115.0(10) . . ? C11 C16 H16 120.7 . . ? C15 C16 C11 118.69(15) . . ? C15 C16 H16 120.7 . . ? N1 C9 C8 117.92(13) . . ? C10 C9 N1 109.66(13) . . ? C10 C9 C8 132.36(14) . . ? C22 C21 H21 120.4 . . ? C20 C21 H21 120.4 . . ? C20 C21 C22 119.29(15) . . ? C33 C38 H38 119.6 . . ? C37 C38 C33 120.85(15) . . ? C37 C38 H38 119.6 . . ? C35 C36 H36 119.8 . . ? C35 C36 C37 120.35(15) . . ? C37 C36 H36 119.8 . . ? C6 C5 N1 118.27(13) . . ? C4 C5 N1 123.03(14) . . ? C4 C5 C6 118.64(14) . . ? C28 C27 C26 108.02(13) . . ? C28 C27 C32 120.26(14) . . ? C32 C27 C26 131.60(15) . . ? C6 C1 H1 119.7 . . ? C2 C1 C6 120.69(15) . . ? C2 C1 H1 119.7 . . ? C24 C19 C18 118.29(13) . . ? C20 C19 C24 119.43(14) . . ? C20 C19 C18 122.24(14) . . ? C21 C22 H22 119.6 . . ? C23 C22 C21 120.87(15) . . ? C23 C22 H22 119.6 . . ? C25 C26 P1 130.98(12) . . ? C25 C26 C27 106.89(13) . . ? C27 C26 P1 121.36(11) . . ? C27 C32 H32 120.7 . . ? C31 C32 C27 118.67(15) . . ? C31 C32 H32 120.7 . . ? C17 C18 S1 112.83(11) . . ? C17 C18 C19 123.47(14) . . ? C19 C18 S1 123.69(11) . . ? C24 C23 H23 125.9(13) . . ? C22 C23 C24 120.66(16) . . ? C22 C23 H23 113.0(12) . . ? C1 C2 H2 120.5 . . ? C1 C2 C3 119.10(15) . . ? C3 C2 H2 120.5 . . ? C28 C29 H29 128.7(11) . . ? C30 C29 C28 118.13(16) . . ? C30 C29 H29 112.9(11) . . ? C5 C4 H4 126.3(12) . . ? C3 C4 C5 120.10(16) . . ? C3 C4 H4 113.1(11) . . ? C13 C14 H14 119.1 . . ? C13 C14 C15 121.71(15) . . ? C15 C14 H14 119.1 . . ? C21 C20 C19 120.98(16) . . ? C21 C20 H20 119.5 . . ? C19 C20 H20 119.5 . . ? C2 C3 H3 119.3 . . ? C4 C3 C2 121.45(15) . . ? C4 C3 H3 119.3 . . ? C16 C15 C14 120.90(15) . . ? C16 C15 H15 119.6 . . ? C14 C15 H15 119.6 . . ? C29 C30 H30 119.1 . . ? C29 C30 C31 121.77(16) . . ? C31 C30 H30 119.1 . . ? C32 C31 C30 120.72(15) . . ? C32 C31 H31 119.6 . . ? C30 C31 H31 119.6 . . ? C38 C37 H37 120.1 . . ? C36 C37 C38 119.80(16) . . ? C36 C37 H37 120.1 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 C7 1.7267(15) . ? S1 C18 1.7255(15) . ? P1 O1 1.4881(10) . ? P1 C33 1.8166(15) . ? P1 C10 1.7740(15) . ? P1 C26 1.7691(15) . ? N1 C12 1.4083(19) . ? N1 C9 1.4071(18) . ? N1 C5 1.4106(19) . ? N2 C25 1.4090(18) . ? N2 C28 1.4025(19) . ? N2 C24 1.4124(19) . ? C12 C11 1.409(2) . ? C12 C13 1.400(2) . ? C11 C10 1.441(2) . ? C11 C16 1.404(2) . ? C33 C34 1.392(2) . ? C33 C38 1.394(2) . ? C25 C17 1.434(2) . ? C25 C26 1.381(2) . ? C17 C8 1.441(2) . ? C17 C18 1.378(2) . ? C6 C7 1.433(2) . ? C6 C5 1.410(2) . ? C6 C1 1.403(2) . ? C7 C8 1.377(2) . ? C34 H34 0.9500 . ? C34 C35 1.386(2) . ? C28 C27 1.408(2) . ? C28 C29 1.398(2) . ? C10 C9 1.382(2) . ? C8 C9 1.435(2) . ? C35 H35 0.9500 . ? C35 C36 1.381(3) . ? C24 C19 1.406(2) . ? C24 C23 1.396(2) . ? C13 C14 1.380(2) . ? C13 H13 0.900(18) . ? C16 H16 0.9500 . ? C16 C15 1.380(2) . ? C21 H21 0.9500 . ? C21 C22 1.384(2) . ? C21 C20 1.376(2) . ? C38 H38 0.9500 . ? C38 C37 1.384(2) . ? C36 H36 0.9500 . ? C36 C37 1.381(2) . ? C5 C4 1.395(2) . ? C27 C26 1.437(2) . ? C27 C32 1.408(2) . ? C1 H1 0.9500 . ? C1 C2 1.374(2) . ? C19 C18 1.432(2) . ? C19 C20 1.400(2) . ? C22 H22 0.9500 . ? C22 C23 1.377(2) . ? C32 H32 0.9500 . ? C32 C31 1.374(2) . ? C23 H23 0.843(19) . ? C2 H2 0.9500 . ? C2 C3 1.389(2) . ? C29 C30 1.382(2) . ? C29 H29 0.88(2) . ? C4 C3 1.382(2) . ? C4 H4 0.855(17) . ? C14 H14 0.9500 . ? C14 C15 1.392(3) . ? C20 H20 0.9500 . ? C3 H3 0.9500 . ? C15 H15 0.9500 . ? C30 H30 0.9500 . ? C30 C31 1.396(2) . ? C31 H31 0.9500 . ? C37 H37 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S1 C7 C8 C17 0.82(16) . . . . ? S1 C7 C8 C9 179.11(10) . . . . ? P1 C33 C34 C35 -179.50(12) . . . . ? P1 C33 C38 C37 -179.66(12) . . . . ? P1 C10 C9 N1 173.65(11) . . . . ? P1 C10 C9 C8 -9.3(3) . . . . ? O1 P1 C33 C34 -139.81(12) . . . . ? O1 P1 C33 C38 39.74(14) . . . . ? O1 P1 C10 C11 -37.58(14) . . . . ? O1 P1 C10 C9 147.38(14) . . . . ? O1 P1 C26 C25 -150.43(13) . . . . ? O1 P1 C26 C27 41.08(14) . . . . ? N1 C12 C11 C10 1.11(16) . . . . ? N1 C12 C11 C16 178.08(13) . . . . ? N1 C12 C13 C14 -176.90(15) . . . . ? N1 C5 C4 C3 178.65(14) . . . . ? N2 C25 C17 C8 -176.98(13) . . . . ? N2 C25 C17 C18 -1.2(2) . . . . ? N2 C25 C26 P1 -167.96(11) . . . . ? N2 C25 C26 C27 1.78(16) . . . . ? N2 C28 C27 C26 -0.98(16) . . . . ? N2 C28 C27 C32 -177.42(13) . . . . ? N2 C28 C29 C30 176.63(15) . . . . ? N2 C24 C19 C18 -4.6(2) . . . . ? N2 C24 C19 C20 177.70(13) . . . . ? N2 C24 C23 C22 -178.05(14) . . . . ? C12 N1 C9 C10 2.68(16) . . . . ? C12 N1 C9 C8 -174.87(12) . . . . ? C12 N1 C5 C6 172.16(13) . . . . ? C12 N1 C5 C4 -10.9(2) . . . . ? C12 C11 C10 P1 -175.61(11) . . . . ? C12 C11 C10 C9 0.51(16) . . . . ? C12 C11 C16 C15 -0.6(2) . . . . ? C12 C13 C14 C15 0.4(2) . . . . ? C11 C12 C13 C14 -1.9(2) . . . . ? C11 C10 C9 N1 -1.96(16) . . . . ? C11 C10 C9 C8 175.12(15) . . . . ? C11 C16 C15 C14 -0.9(2) . . . . ? C33 P1 C10 C11 81.87(13) . . . . ? C33 P1 C10 C9 -93.17(15) . . . . ? C33 P1 C26 C25 90.02(15) . . . . ? C33 P1 C26 C27 -78.47(13) . . . . ? C33 C34 C35 C36 -1.0(2) . . . . ? C33 C38 C37 C36 -0.7(2) . . . . ? C25 N2 C28 C27 2.06(16) . . . . ? C25 N2 C28 C29 -173.95(16) . . . . ? C25 N2 C24 C19 8.1(2) . . . . ? C25 N2 C24 C23 -170.41(14) . . . . ? C25 C17 C8 C7 175.36(14) . . . . ? C25 C17 C8 C9 -2.7(3) . . . . ? C25 C17 C18 S1 -176.30(11) . . . . ? C25 C17 C18 C19 4.5(2) . . . . ? C17 C25 C26 P1 15.7(3) . . . . ? C17 C25 C26 C27 -174.59(15) . . . . ? C17 C8 C9 N1 178.07(13) . . . . ? C17 C8 C9 C10 1.2(3) . . . . ? C6 C7 C8 C17 177.78(13) . . . . ? C6 C7 C8 C9 -3.9(2) . . . . ? C6 C5 C4 C3 -4.4(2) . . . . ? C6 C1 C2 C3 -1.3(2) . . . . ? C7 S1 C18 C17 0.17(12) . . . . ? C7 S1 C18 C19 179.34(13) . . . . ? C7 C6 C5 N1 5.9(2) . . . . ? C7 C6 C5 C4 -171.12(14) . . . . ? C7 C6 C1 C2 173.77(14) . . . . ? C7 C8 C9 N1 0.13(19) . . . . ? C7 C8 C9 C10 -176.75(15) . . . . ? C34 C33 C38 C37 -0.1(2) . . . . ? C34 C35 C36 C37 0.2(2) . . . . ? C28 N2 C25 C17 174.53(12) . . . . ? C28 N2 C25 C26 -2.42(16) . . . . ? C28 N2 C24 C19 -171.56(14) . . . . ? C28 N2 C24 C23 9.9(2) . . . . ? C28 C27 C26 P1 170.45(10) . . . . ? C28 C27 C26 C25 -0.49(16) . . . . ? C28 C27 C32 C31 0.4(2) . . . . ? C28 C29 C30 C31 -0.8(3) . . . . ? C10 P1 C33 C34 98.77(13) . . . . ? C10 P1 C33 C38 -81.69(13) . . . . ? C10 P1 C26 C25 -22.49(16) . . . . ? C10 P1 C26 C27 169.01(11) . . . . ? C10 C11 C16 C15 175.58(15) . . . . ? C8 C17 C18 S1 0.26(16) . . . . ? C8 C17 C18 C19 -178.92(13) . . . . ? C35 C36 C37 C38 0.6(2) . . . . ? C24 N2 C25 C17 -5.2(2) . . . . ? C24 N2 C25 C26 177.84(13) . . . . ? C24 N2 C28 C27 -178.22(13) . . . . ? C24 N2 C28 C29 5.8(3) . . . . ? C24 C19 C18 S1 179.31(11) . . . . ? C24 C19 C18 C17 -1.6(2) . . . . ? C24 C19 C20 C21 1.4(2) . . . . ? C13 C12 C11 C10 -175.00(14) . . . . ? C13 C12 C11 C16 2.0(2) . . . . ? C13 C14 C15 C16 1.0(3) . . . . ? C16 C11 C10 P1 7.9(2) . . . . ? C16 C11 C10 C9 -175.97(15) . . . . ? C9 N1 C12 C11 -2.29(15) . . . . ? C9 N1 C12 C13 173.24(16) . . . . ? C9 N1 C5 C6 -10.1(2) . . . . ? C9 N1 C5 C4 166.88(14) . . . . ? C21 C22 C23 C24 -0.8(2) . . . . ? C38 C33 C34 C35 1.0(2) . . . . ? C5 N1 C12 C11 175.76(13) . . . . ? C5 N1 C12 C13 -8.7(3) . . . . ? C5 N1 C9 C10 -175.50(13) . . . . ? C5 N1 C9 C8 6.9(2) . . . . ? C5 C6 C7 S1 177.48(11) . . . . ? C5 C6 C7 C8 0.8(2) . . . . ? C5 C6 C1 C2 -2.3(2) . . . . ? C5 C4 C3 C2 0.9(2) . . . . ? C27 C28 C29 C30 1.0(2) . . . . ? C27 C32 C31 C30 -0.1(2) . . . . ? C1 C6 C7 S1 1.4(2) . . . . ? C1 C6 C7 C8 -175.29(14) . . . . ? C1 C6 C5 N1 -177.84(13) . . . . ? C1 C6 C5 C4 5.1(2) . . . . ? C1 C2 C3 C4 2.0(2) . . . . ? C19 C24 C23 C22 3.4(2) . . . . ? C22 C21 C20 C19 1.3(2) . . . . ? C26 P1 C33 C34 -17.10(14) . . . . ? C26 P1 C33 C38 162.44(12) . . . . ? C26 P1 C10 C11 -166.46(11) . . . . ? C26 P1 C10 C9 18.49(17) . . . . ? C26 C25 C17 C8 -0.9(3) . . . . ? C26 C25 C17 C18 174.96(15) . . . . ? C26 C27 C32 C31 -175.11(15) . . . . ? C32 C27 C26 P1 -13.7(2) . . . . ? C32 C27 C26 C25 175.39(15) . . . . ? C18 S1 C7 C6 -177.55(13) . . . . ? C18 S1 C7 C8 -0.57(12) . . . . ? C18 C17 C8 C7 -0.68(17) . . . . ? C18 C17 C8 C9 -178.73(14) . . . . ? C18 C19 C20 C21 -176.20(15) . . . . ? C23 C24 C19 C18 174.00(14) . . . . ? C23 C24 C19 C20 -3.7(2) . . . . ? C29 C28 C27 C26 175.57(14) . . . . ? C29 C28 C27 C32 -0.9(2) . . . . ? C29 C30 C31 C32 0.3(3) . . . . ? C20 C21 C22 C23 -1.6(2) . . . . ? C20 C19 C18 S1 -3.1(2) . . . . ? C20 C19 C18 C17 176.02(14) . . . . ?