#------------------------------------------------------------------------------ #$Date: 2024-11-20 04:49:53 +0200 (Wed, 20 Nov 2024) $ #$Revision: 296005 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/32/1573202.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1573202 loop_ _publ_author_name 'Zwolenik, A.' 'Makal, A.' _publ_section_title ; Tracking anharmonic oscillations in the structure of β-1,3-diacetylpyrene. ; _journal_issue 1 _journal_name_full IUCrJ _journal_paper_doi 10.1107/S2052252524010443 _journal_volume 12 _journal_year 2025 _chemical_formula_moiety 'C20 H14 O2' _chemical_formula_sum 'C20 H14 O2' _chemical_formula_weight 286.333 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_Int_Tables_number 14 _atom_sites_solution_primary direct _audit_creation_date 2024-08-11 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _cell_angle_alpha 90 _cell_angle_beta 102.742(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.17156(18) _cell_length_b 10.9455(3) _cell_length_c 17.7694(5) _cell_measurement_reflns_used 5075 _cell_measurement_temperature 150.06(10) _cell_measurement_theta_max 76.3150 _cell_measurement_theta_min 4.7690 _cell_volume 1360.48(7) _computing_cell_refinement 'CrysAlisPro 1.171.39.43d (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.43d (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.43d (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.06(10) _diffrn_detector 'CCD plate' _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.9992 _diffrn_measured_fraction_theta_max 0.9931 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -22.00 32.00 0.50 0.10 -- 0.00 52.00 -16.00 108 2 \w 39.00 65.00 0.50 0.10 -- 0.00 52.00 -16.00 52 3 \w -1.00 25.00 0.50 0.30 -- 66.60 -52.00-161.00 52 4 \w 29.00 124.00 0.50 0.30 -- 66.60 52.00 -16.00 190 5 \w 61.00 94.00 0.50 0.30 -- 66.60 -52.00-161.00 66 6 \w 45.00 74.00 0.50 0.30 -- 121.75 -52.00-161.00 58 7 \w -43.00 20.00 0.50 0.10 -- 0.00 77.00-180.00 126 8 \w -37.00 40.00 0.50 0.10 -- 0.00 -77.00 -30.00 154 9 \w -77.00 -45.00 0.50 0.10 -- 0.00 -77.00 -30.00 64 10 \w -8.00 33.00 0.50 0.10 -- 0.00 -52.00-161.00 82 11 \w 0.00 54.00 0.50 0.10 -- 0.00 -99.00-180.00 108 12 \w -78.00 -21.00 0.50 0.10 -- 0.00 -52.00-161.00 114 13 \w 11.00 53.00 0.50 0.10 -- 0.00 -99.00-120.00 84 14 \w 24.00 149.00 0.50 0.30 -- 66.60 77.00 60.00 250 15 \w 24.00 150.00 0.50 0.30 -- 66.60 77.00-150.00 252 16 \w 34.00 109.00 0.50 0.30 -- 66.60-125.00 -90.00 150 17 \w 115.00 141.00 0.50 0.30 -- 66.60 77.00 114.06 52 18 \w 25.00 79.00 0.50 0.30 -- 66.60 77.00-180.00 108 19 \w 97.00 150.00 0.50 0.30 -- 66.60 125.00 -90.00 106 20 \w 118.00 150.00 0.50 0.30 -- 66.60 125.00-180.00 64 21 \w 108.00 152.00 0.50 0.30 -- 66.60 77.00 -30.00 88 22 \w 24.00 150.00 0.50 0.30 -- 66.60 77.00 150.00 252 23 \w 24.00 59.00 0.50 0.30 -- 66.60 77.00 -60.00 70 24 \w 81.00 141.00 0.50 0.30 -- 66.60 77.00 30.00 120 25 \w 97.00 148.00 0.50 0.30 -- 66.60 125.00 120.00 102 26 \w 24.00 69.00 0.50 0.30 -- 66.60 77.00 0.00 90 27 \w 107.00 146.00 0.50 0.30 -- 66.60 77.00-180.00 78 28 \w 24.00 69.00 0.50 0.30 -- 66.60 77.00 114.06 90 29 \w 25.00 78.00 0.50 0.30 -- 66.60 77.00 30.00 106 30 \w 26.00 70.00 0.50 0.30 -- 66.60 77.00 -90.00 88 31 \w 24.00 60.00 0.50 0.30 -- 66.60 77.00 90.00 72 32 \w 24.00 57.00 0.50 0.30 -- 66.60 77.00 -30.00 66 33 \w 24.00 71.00 0.50 0.30 -- 66.60 77.00-120.00 94 34 \w 88.00 152.00 0.50 0.30 -- 66.60 77.00-120.00 128 35 \w 66.00 108.00 0.50 0.30 -- 66.60-125.00 150.00 84 36 \w 88.00 146.00 0.50 0.30 -- 66.60 77.00 90.00 116 37 \w 112.00 138.00 0.50 0.30 -- 66.60 77.00 -90.00 52 38 \w 84.00 152.00 0.50 0.30 -- 66.60 77.00 -60.00 136 39 \w 79.00 105.00 0.50 0.30 -- 121.75 76.00 -66.31 52 40 \w 83.00 113.00 0.50 0.30 -- 121.75 68.00 55.50 60 41 \w 84.00 113.00 0.50 0.30 -- 121.75 67.00 173.08 58 42 \w 138.00 178.00 0.50 0.30 -- 121.75 63.00 150.00 80 43 \w 85.00 110.00 0.50 0.30 -- 121.75 63.00 150.00 50 44 \w 53.00 108.00 0.50 0.30 -- 121.75-111.00 -60.00 110 45 \w 32.00 83.00 0.50 0.30 -- 121.75 -91.00-150.00 102 46 \w 145.00 176.00 0.50 0.30 -- 121.75 77.00 -60.00 62 47 \w 85.00 175.00 0.50 0.30 -- 121.75 63.00 0.00 180 48 \w 79.00 139.00 0.50 0.30 -- 121.75 77.00 -60.00 120 49 \w 145.00 178.00 0.50 0.30 -- 121.75 63.00-120.00 66 50 \w 86.00 142.00 0.50 0.30 -- 121.75 63.00-120.00 112 51 \w 82.00 108.00 0.50 0.30 -- 121.75 70.00-107.63 52 52 \w 46.00 106.00 0.50 0.30 -- 121.75-111.00 30.00 120 53 \w 79.00 132.00 0.50 0.30 -- 121.75 77.00 30.00 106 54 \w 133.00 159.00 0.50 0.30 -- 121.75 77.00 0.00 52 55 \w 80.00 177.00 0.50 0.30 -- 121.75 77.00 60.00 194 56 \w 79.00 174.00 0.50 0.30 -- 121.75 77.00 120.00 190 57 \w 34.00 95.00 0.50 0.30 -- 121.75 -91.00 150.00 122 58 \w 79.00 115.00 0.50 0.30 -- 121.75 77.00 0.00 72 59 \w 79.00 114.00 0.50 0.30 -- 121.75 77.00 90.00 70 60 \w 118.00 147.00 0.50 0.30 -- 121.75 77.00 90.00 58 61 \w 121.00 178.00 0.50 0.30 -- 121.75 72.00-140.82 114 62 \w 80.00 113.00 0.50 0.30 -- 121.75 72.00-140.82 66 63 \w 119.00 145.00 0.50 0.30 -- 121.75 77.00 -30.00 52 64 \w 85.00 163.00 0.50 0.30 -- 121.75 63.00-150.00 156 65 \w 49.00 108.00 0.50 0.30 -- 121.75-111.00 90.00 118 66 \w 132.00 172.00 0.50 0.30 -- 121.75 68.00 55.50 80 67 \w 80.00 109.00 0.50 0.30 -- 121.75 77.00 -30.00 58 68 \w 115.00 158.00 0.50 0.30 -- 121.75 76.00 -66.31 86 69 \w 44.00 108.00 0.50 0.30 -- 121.75-111.00-150.00 128 70 \w 38.00 86.00 0.50 0.30 -- 121.75 -91.00 120.00 96 71 \w 141.00 172.00 0.50 0.30 -- 121.75 77.00 -90.00 62 72 \w 144.00 177.00 0.50 0.30 -- 121.75 77.00 100.66 66 73 \w 86.00 170.00 0.50 0.30 -- 121.75 60.00 26.94 168 74 \w 79.00 116.00 0.50 0.30 -- 121.75 77.00 -90.00 74 75 \w 79.00 139.00 0.50 0.30 -- 121.75 77.00 100.66 120 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0717853764 _diffrn_orient_matrix_UB_12 -0.1325410748 _diffrn_orient_matrix_UB_13 0.0007272754 _diffrn_orient_matrix_UB_21 0.1894399882 _diffrn_orient_matrix_UB_22 -0.0365512367 _diffrn_orient_matrix_UB_23 0.0548699639 _diffrn_orient_matrix_UB_31 -0.0862114016 _diffrn_orient_matrix_UB_32 0.0301451940 _diffrn_orient_matrix_UB_33 0.0699509074 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0417 _diffrn_reflns_av_unetI/netI 0.0241 _diffrn_reflns_Laue_measured_fraction_full 0.9992 _diffrn_reflns_Laue_measured_fraction_max 0.9931 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 20905 _diffrn_reflns_point_group_measured_fraction_full 0.9992 _diffrn_reflns_point_group_measured_fraction_max 0.9931 _diffrn_reflns_theta_full 67.6840 _diffrn_reflns_theta_max 77.58 _diffrn_reflns_theta_min 4.78 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.710 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.735 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.43d (Rigaku Oxford Diffraction, 2018) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.398 _exptl_crystal_description irregular _exptl_crystal_F_000 601.956 _exptl_crystal_size_max 0.175 _exptl_crystal_size_mid 0.135 _exptl_crystal_size_min 0.093 _refine_diff_density_max 0.1206 _refine_diff_density_min -0.1223 _refine_diff_density_rms 0.0310 _refine_ls_d_res_high 0.7894 _refine_ls_d_res_low 9.2545 _refine_ls_goodness_of_fit_ref 1.0910 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_constraints 0 _refine_ls_number_parameters 325 _refine_ls_number_reflns 2867 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0910 _refine_ls_R_factor_all 0.0318 _refine_ls_R_factor_gt 0.0251 _refine_ls_shift/su_max -0.0005 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0080P)^2^+0.1256P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0499 _refine_ls_wR_factor_ref 0.0522 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 8 _reflns_limit_h_min -9 _reflns_limit_k_max 13 _reflns_limit_k_min 0 _reflns_limit_l_max 22 _reflns_limit_l_min 0 _reflns_number_gt 2405 _reflns_number_total 2867 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL 2oAPb_multiT_05_150_00_smart3_abs in P21/c #14 REM reset to P21/c #14 CELL 1.54184 7.171557 10.945478 17.769409 90 102.742 90 ZERR 4 0.000181 0.00027 0.000503 0 0.0025 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H O UNIT 80 56 8 L.S. 10 PLAN 5 TEMP -123 CONF BOND MORE -1 BOND $H fmap 2 53 acta WGHT 0.008011 0.125621 FVAR 3.898289 REM REM REM C1 1 0.29960 0.97085 0.07029 11.00000 0.02267 0.02653 0.02537 = 0.00313 0.00540 -0.00056 C2 1 0.21234 1.14176 -0.02351 11.00000 0.02388 0.02923 0.02533 = 0.00457 0.00520 -0.00023 C3 1 0.24497 1.01468 -0.00723 11.00000 0.02180 0.02813 0.02429 = 0.00121 0.00553 -0.00170 O4 3 0.46935 0.92768 0.23597 11.00000 0.04897 0.03736 0.02802 = 0.00847 0.00389 0.00663 C5 1 0.31921 1.05635 0.13172 11.00000 0.02515 0.02677 0.02377 = 0.00349 0.00623 -0.00007 C6 1 0.23550 1.22468 0.03897 11.00000 0.02698 0.02647 0.02678 = 0.00482 0.00554 0.00045 C7 1 0.26738 0.80433 -0.05566 11.00000 0.02584 0.03180 0.03434 = -0.00488 0.00775 -0.00327 C8 1 0.22874 0.93027 -0.06999 11.00000 0.02113 0.03383 0.02690 = -0.00231 0.00578 -0.00307 C9 1 0.28357 1.17957 0.11413 11.00000 0.02832 0.02733 0.02581 = 0.00249 0.00622 -0.00019 C10 1 0.17182 0.88884 -0.20805 11.00000 0.03063 0.05484 0.02995 = -0.00980 0.00657 -0.00749 C11 1 0.17914 0.97188 -0.14751 11.00000 0.02539 0.04299 0.02525 = -0.00227 0.00452 -0.00424 O12 3 0.25430 1.41090 -0.02805 11.00000 0.06982 0.03172 0.04418 = 0.01211 0.02176 0.00214 C13 1 0.33110 0.84221 0.08233 11.00000 0.03330 0.02768 0.03143 = 0.00350 0.00784 0.00081 C14 1 0.14088 1.09880 -0.16142 11.00000 0.03262 0.04693 0.02379 = 0.00364 0.00420 -0.00116 C15 1 0.31681 0.76307 0.02238 11.00000 0.03438 0.02789 0.03984 = 0.00038 0.00957 0.00094 C16 1 0.15525 1.17991 -0.10265 11.00000 0.03299 0.03754 0.02668 = 0.00724 0.00547 0.00217 C17 1 0.25967 0.72360 -0.11762 11.00000 0.03205 0.03924 0.04402 = -0.01318 0.01031 -0.00460 C18 1 0.22392 1.36048 0.02915 11.00000 0.03371 0.02796 0.03380 = 0.00582 0.00776 0.00078 C19 1 0.38552 1.02303 0.21500 11.00000 0.02891 0.03195 0.02497 = 0.00456 0.00568 -0.00096 C20 1 0.21282 0.76595 -0.19328 11.00000 0.03378 0.05171 0.03857 = -0.01691 0.00945 -0.00833 C21 1 0.17929 1.43629 0.09383 11.00000 0.04368 0.02854 0.04165 = 0.00008 0.00833 -0.00060 C22 1 0.35001 1.11170 0.27514 11.00000 0.04194 0.04475 0.02668 = -0.00075 0.00622 0.00132 H9 2 0.30012 1.24435 0.16101 11.00000 0.05732 0.04900 0.04297 = -0.00905 0.01060 -0.00115 H20 2 0.21201 0.70350 -0.24057 11.00000 0.08086 0.08024 0.05513 = -0.04299 0.01744 -0.00612 H10 2 0.13653 0.92274 -0.26789 11.00000 0.07440 0.10705 0.02804 = 0.00179 0.01379 -0.00564 H16 2 0.12785 1.27740 -0.11400 11.00000 0.08081 0.04577 0.05899 = 0.02163 0.01922 0.01093 H13 2 0.36964 0.80928 0.14148 11.00000 0.08130 0.06240 0.03232 = 0.01330 0.01311 0.00593 H14 2 0.10154 1.12859 -0.22176 11.00000 0.08330 0.08091 0.03101 = 0.00969 0.01124 0.01001 H22a 2 0.38080 1.06792 0.33158 11.00000 0.13149 0.08287 0.01736 = 0.01757 0.00939 0.01524 H15 2 0.34623 0.66603 0.03348 11.00000 0.08384 0.04105 0.07143 = -0.00065 0.02096 0.00714 H22b 2 0.43815 1.19140 0.27709 11.00000 0.09561 0.07451 0.06251 = -0.01979 0.02453 -0.02646 H21a 2 0.06718 1.39806 0.11553 11.00000 0.09155 0.07661 0.09919 = -0.02561 0.05515 -0.02648 H21b 2 0.14422 1.52783 0.07224 11.00000 0.13817 0.03573 0.07488 = 0.01799 0.02009 0.01763 H21c 2 0.30342 1.44095 0.14147 11.00000 0.06923 0.08113 0.06859 = -0.02071 -0.01696 0.00107 H22c 2 0.20436 1.14305 0.26294 11.00000 0.06809 0.10005 0.05647 = -0.00773 0.00498 0.02647 H17 2 0.29085 0.62671 -0.10538 11.00000 0.06734 0.04524 0.09932 = -0.01408 0.02287 -0.00075 HKLF 4 END Q2 1 0.5 0.825 0.05 11 0.05 0.12 Q3 1 0.208333 1.075 -0.083333 11 0.05 0.12 Q4 1 0.291667 0.875 0.016667 11 0.05 0.11 Q1 1 0.25 1.1 0.05 11 0.05 0.12 Q5 1 -0.041667 1.05 -0.066667 11 0.05 0.11 REM The information below was added by Olex2. REM REM R1 = 0.0251 for 2405 Fo > 4sig(Fo) and 0.0318 for all 2867 data REM 325 parameters refined using 0 restraints REM Highest difference peak 0.1206, deepest hole -0.1223 REM Mean Shift 0.0000, Max Shift -0.0005. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0318 REM R1_gt = 0.0251 REM wR_ref = 0.0522 REM GOOF = 1.0910 REM Shift_max = -0.0005 REM Shift_mean = 0.0000 REM Reflections_all = 2867 REM Reflections_gt = 2405 REM Parameters = 325 REM Hole = -0.1223 REM Peak = 0.1206 REM Flack = n/a ; _cod_data_source_file pen5002.cif _cod_data_source_block 150K _cod_original_cell_volume 1360.48(6) _cod_database_code 1573202 _chemical_oxdiff_formula 'C20 H14 O2' _olex2_refinement_description ; ; _olex2_refine_details ; Refinement using NoSpherA2, an implementation of NOn-SPHERical Atom-form-factors in Olex2. Please cite: F. Kleemiss et al. Chem. Sci. DOI 10.1039/D0SC05526C - 2021 NoSpherA2 implementation of HAR makes use of tailor-made aspherical atomic form factors calculated on-the-fly from a Hirshfeld-partitioned electron density (ED) - not from spherical-atom form factors. The ED is calculated from a gaussian basis set single determinant SCF wavefunction - either Hartree-Fock or DFT using selected funtionals - for a fragment of the crystal. This fragment can be embedded in an electrostatic crystal field by employing cluster charges or modelled using implicit solvation models, depending on the software used. The following options were used: SOFTWARE: ORCA 5.0 PARTITIONING: NoSpherA2 INT ACCURACY: Normal METHOD: B3LYP BASIS SET: 6-31G(d,p) CHARGE: 0 MULTIPLICITY: 1 DATE: 2024-03-29_19-17-36 ; _iucr_refine_fcf_details ; data_150K _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_Int_Tables_number 14 _cell_length_a 7.17156(18) _cell_length_b 10.9455(3) _cell_length_c 17.7694(5) _cell_angle_alpha 90 _cell_angle_beta 102.742(3) _cell_angle_gamma 90 _cell_volume 1360.48(6) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -9 0 4 1.198 2.646 1.254 179.093 o -9 0 6 77.003 62.795 9.731 3.070 o -9 1 3 2.697 2.812 1.775 91.421 o -9 1 4 31.043 21.112 2.907 26.666 o -9 1 5 16.862 11.785 1.267 90.627 o -9 1 6 9.199 5.137 1.327 116.174 o -9 1 7 1.676 1.442 0.807 374.906 o -8 0 2 0.060 0.930 1.328 176.881 o -8 0 4 72.462 76.954 5.023 9.163 o -8 0 10 18.049 25.730 4.099 16.455 o -8 0 12 0.746 4.459 2.063 70.956 o -8 1 1 45.730 50.118 2.273 28.443 o -8 1 2 87.783 94.592 3.589 12.932 o -8 1 3 141.961 147.135 4.989 7.220 o -8 1 4 504.432 514.039 13.337 1.238 o -8 1 5 121.221 123.284 4.902 7.931 o -8 1 6 103.316 105.129 4.824 8.632 o -8 1 7 8.307 9.859 1.842 70.900 o -8 1 8 11.588 12.706 2.810 33.978 o -8 1 9 4.119 3.119 1.885 79.323 o -8 1 10 35.805 38.163 5.449 9.296 o -8 1 11 125.810 120.747 9.923 2.778 o -8 1 12 41.100 39.278 4.856 11.108 o -8 1 13 11.548 15.639 3.246 26.263 o -8 1 14 0.218 3.180 1.757 98.706 o -8 2 1 38.139 36.480 2.204 33.043 o -8 2 2 14.150 12.001 1.444 84.439 o -8 2 3 132.204 144.279 4.380 8.525 o -8 2 4 827.212 854.390 13.683 0.948 o -8 2 5 353.238 343.022 7.536 2.943 o -8 2 6 154.556 150.467 4.793 7.310 o -8 2 7 28.608 31.320 2.095 39.194 o -8 2 8 1.762 2.293 1.112 215.770 o -8 2 9 65.681 72.121 5.316 8.620 o -8 2 10 50.191 46.379 5.310 9.266 o -8 2 11 14.599 12.295 3.548 22.294 o -8 2 12 8.179 7.580 2.699 38.541 o -8 2 13 0.419 0.904 1.689 109.287 o -8 2 14 5.872 2.725 1.546 106.647 o -8 3 1 19.854 18.085 1.342 75.281 o -8 3 2 154.797 162.370 4.864 7.100 o -8 3 3 26.896 26.272 1.727 50.098 o -8 3 4 4.589 4.670 1.206 157.002 o -8 3 5 210.561 223.696 5.996 4.848 o -8 3 6 63.373 61.285 2.855 19.636 o -8 3 7 10.125 10.406 1.434 95.451 o -8 3 8 31.156 28.115 3.079 23.979 o -8 3 9 1.751 2.177 1.127 211.753 o -8 3 10 10.125 6.937 2.866 34.142 o -8 3 11 2.472 2.265 2.514 48.238 o -8 3 12 74.004 64.361 6.062 6.953 o -8 3 13 26.770 24.850 6.117 7.843 o -8 4 1 4.334 4.705 1.441 121.185 o -8 4 2 6.529 6.853 1.385 116.020 o -8 4 3 41.981 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87.701 3.037 15.697 o 2 6 5 61.437 64.515 3.214 17.345 o 2 6 6 18.502 20.513 1.708 59.727 o 2 6 7 326.931 345.815 7.750 2.931 o 2 6 8 888.179 911.334 16.615 0.726 o 2 6 9 456.604 489.268 10.828 1.682 o 2 6 10 4.417 6.080 1.240 147.730 o 2 6 11 53.445 52.679 2.364 25.667 o 2 6 12 43.742 44.516 2.080 32.028 o 2 6 13 28.050 34.750 2.182 37.059 o 2 6 14 1.756 1.628 1.026 252.175 o 2 6 15 19.922 22.391 1.961 49.327 o 2 6 16 6.911 7.302 1.122 148.864 o 2 6 17 0.197 0.032 0.687 653.070 o 2 6 18 90.696 67.057 8.926 3.530 o 2 7 0 0.007 0.068 0.770 536.481 o 2 7 1 40.586 41.346 2.289 30.505 o 2 7 2 2.913 2.586 1.028 226.569 o 2 7 3 1.490 2.439 1.113 218.107 o 2 7 4 0.023 0.599 0.990 317.265 o 2 7 5 25.794 22.835 1.971 45.386 o 2 7 6 126.784 129.478 5.056 7.492 o 2 7 7 0.506 1.466 1.094 245.636 o 2 7 8 328.459 324.906 8.760 2.562 o 2 7 9 404.107 414.288 6.675 3.004 o 2 7 10 0.041 0.497 0.764 525.127 o 2 7 11 33.514 30.017 1.477 50.631 o 2 7 12 15.729 18.199 2.478 38.806 o 2 7 13 113.689 116.721 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201.410 4.993 6.128 o 4 4 1 0.914 1.036 0.762 456.476 o 4 4 2 62.183 57.510 2.825 20.188 o 4 4 3 15.294 14.061 1.595 72.154 o 4 4 4 25.113 29.411 2.351 35.872 o 4 4 5 308.867 302.593 8.373 2.787 o 4 4 6 0.000 0.527 1.003 310.751 o 4 4 7 69.776 69.904 3.565 14.665 o 4 4 8 48.638 51.586 3.992 14.315 o 4 4 9 11.181 10.335 1.145 118.939 o 4 4 10 2.550 3.178 0.842 302.845 o 4 4 11 30.894 28.325 1.891 43.146 o 4 4 12 71.476 72.730 2.929 17.809 o 4 4 13 110.028 121.060 3.438 11.867 o 4 4 14 0.035 -0.581 0.740 581.221 o 4 4 15 2.770 1.772 0.690 408.263 o 4 4 16 12.631 10.777 1.596 78.607 o 4 5 0 274.395 274.790 6.107 4.171 o 4 5 1 275.979 275.955 6.218 4.086 o 4 5 2 67.471 69.910 3.461 15.324 o 4 5 3 100.632 98.293 3.761 11.695 o 4 5 4 12.339 11.616 1.434 89.139 o 4 5 5 286.237 298.904 7.289 3.363 o 4 5 6 13.176 20.095 2.146 48.677 o 4 5 7 418.110 429.872 9.440 2.081 o 4 5 8 177.292 181.147 4.062 7.798 o 4 5 9 163.039 161.748 3.778 8.781 o 4 5 10 173.244 183.899 6.423 4.881 o 4 5 11 9.548 8.666 1.480 95.196 o 4 5 12 7.832 6.504 1.594 92.015 o 4 5 13 88.641 93.278 3.708 12.485 o 4 5 14 33.202 33.457 1.954 39.595 o 4 5 15 15.439 14.368 1.167 97.729 o 4 6 0 84.141 86.630 3.759 12.648 o 4 6 1 0.051 -0.410 1.050 288.858 o 4 6 2 26.792 25.941 2.319 36.513 o 4 6 3 34.441 34.556 2.463 30.505 o 4 6 4 97.163 94.709 4.393 9.988 o 4 6 5 34.878 36.896 2.641 27.740 o 4 6 6 328.304 332.449 5.023 4.341 o 4 6 7 359.488 375.857 5.701 3.678 o 4 6 8 255.202 266.087 4.584 5.527 o 4 6 9 36.162 37.169 2.141 34.536 o 4 6 10 1.405 1.070 0.991 278.988 o 4 6 11 7.049 10.758 1.211 127.248 o 4 6 12 15.690 19.498 1.439 75.728 o 4 6 13 6.892 6.520 1.023 168.151 o 4 6 14 22.912 20.091 1.381 68.039 o 4 6 15 7.648 1.790 1.554 102.046 o 4 7 0 37.525 38.448 2.468 29.225 o 4 7 1 6.348 9.979 1.616 89.641 o 4 7 2 9.806 9.360 1.857 68.482 o 4 7 3 18.618 21.049 1.627 62.499 o 4 7 4 34.884 35.798 1.931 38.839 o 4 7 5 92.523 91.037 2.802 16.013 o 4 7 6 75.737 79.463 2.405 20.185 o 4 7 7 139.523 135.849 3.481 10.403 o 4 7 8 100.001 108.201 3.386 12.759 o 4 7 9 1.730 1.626 0.923 299.862 o 4 7 10 106.894 114.602 3.210 12.875 o 4 7 11 79.500 84.716 2.829 17.150 o 4 7 12 3.684 4.710 0.871 252.449 o 4 7 13 15.021 14.967 1.385 83.698 o 4 7 14 61.251 39.996 18.314 0.933 o 4 8 0 14.665 12.760 1.117 105.710 o 4 8 1 22.941 23.503 1.398 65.309 o 4 8 2 150.409 144.738 3.365 10.178 o 4 8 3 33.269 34.719 1.634 45.758 o 4 8 4 0.402 1.091 0.686 581.084 o 4 8 5 49.422 54.556 2.714 22.899 o 4 8 6 0.065 0.167 1.012 308.498 o 4 8 7 28.998 30.260 1.975 41.766 o 4 8 8 3.656 2.136 1.022 221.855 o 4 8 9 107.147 102.309 3.013 13.865 o 4 8 10 62.421 64.662 2.198 24.540 o 4 8 11 55.701 53.526 1.780 31.121 o 4 8 12 9.923 7.305 0.898 163.978 o 4 9 0 120.684 126.415 4.442 8.853 o 4 9 1 4.664 4.793 1.222 153.115 o 4 9 2 253.437 262.223 5.927 4.466 o 4 9 3 589.896 603.194 9.212 1.754 o 4 9 4 188.619 199.600 4.924 6.294 o 4 9 5 8.038 9.277 1.175 130.639 o 4 9 6 19.430 18.195 1.931 52.051 o 4 9 7 53.283 63.342 2.793 21.132 o 4 9 8 2.373 1.523 0.849 324.708 o 4 9 9 0.102 -0.329 0.745 566.397 o 4 9 10 9.893 9.517 0.833 165.824 o 4 9 11 0.135 0.734 1.010 300.647 o 4 10 0 1.059 1.308 1.112 231.655 o 4 10 1 243.311 244.093 5.966 4.566 o 4 10 2 186.309 192.167 4.486 6.940 o 4 10 3 268.054 269.753 6.235 4.137 o 4 10 4 9.508 9.158 1.510 92.214 o 4 10 5 0.000 0.011 0.951 353.230 o 4 10 6 0.008 0.538 1.026 297.279 o 4 10 7 44.526 40.748 2.326 29.147 o 4 10 8 16.232 14.278 1.231 91.639 o 4 10 9 0.001 -0.104 0.668 715.537 o 4 11 0 0.885 -0.207 0.903 359.007 o 4 11 1 9.444 11.581 1.409 97.759 o 4 11 2 2.624 3.128 1.010 233.150 o 4 11 3 0.838 0.681 0.684 563.922 o 4 11 4 0.090 -0.097 0.620 815.511 o 4 11 5 0.098 -0.415 0.649 743.723 o 4 11 6 0.670 -0.854 0.874 389.833 o 4 11 7 43.484 31.302 2.422 29.275 o 4 12 0 1.572 1.622 0.682 480.348 o 4 12 1 6.882 4.998 0.733 241.157 o 4 12 2 16.200 12.897 2.556 37.849 o 5 0 0 22.295 22.760 2.887 28.565 o 5 0 2 3.362 3.121 1.260 159.738 o 5 0 4 1570.520 1637.300 40.184 0.162 o 5 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32.327 1.879 40.850 o 5 2 8 12.673 10.072 1.414 91.532 o 5 2 9 0.818 1.316 0.812 408.465 o 5 2 10 40.446 42.492 2.519 27.499 o 5 2 11 60.085 61.716 3.328 16.886 o 5 2 12 38.073 42.576 2.131 33.252 o 5 2 13 44.835 45.692 2.043 32.039 o 5 2 14 13.447 11.961 0.953 125.566 o 5 2 15 38.775 24.711 3.448 19.674 o 5 3 0 54.536 50.592 3.003 20.118 o 5 3 1 39.704 42.936 2.643 26.163 o 5 3 2 372.666 380.188 11.871 1.622 o 5 3 3 14.629 14.743 2.317 44.233 o 5 3 4 9.402 11.230 2.182 53.029 o 5 3 5 62.828 64.234 4.548 11.060 o 5 3 6 81.724 80.773 2.846 17.043 o 5 3 7 20.743 19.175 1.664 59.889 o 5 3 8 140.422 146.880 4.101 8.868 o 5 3 9 0.022 -0.174 1.151 240.766 o 5 3 10 9.965 10.482 1.419 97.054 o 5 3 11 45.950 54.623 2.575 24.732 o 5 3 12 229.578 241.064 5.762 4.841 o 5 3 13 8.030 7.350 0.984 163.761 o 5 3 14 5.278 4.270 0.756 267.752 o 5 4 0 17.908 13.684 1.823 59.052 o 5 4 1 0.809 2.917 1.328 163.476 o 5 4 2 97.731 93.468 4.448 9.839 o 5 4 3 10.865 11.450 1.751 71.584 o 5 4 4 449.763 459.053 11.398 1.598 o 5 4 5 77.050 77.784 2.505 19.522 o 5 4 6 20.535 21.009 1.530 64.311 o 5 4 7 1.055 0.020 0.948 323.216 o 5 4 8 58.673 66.688 3.574 15.425 o 5 4 9 4.685 4.475 1.360 131.527 o 5 4 10 90.408 91.661 3.588 12.879 o 5 4 11 0.029 1.721 0.942 332.033 o 5 4 12 6.977 8.538 1.172 137.801 o 5 4 13 13.035 11.682 1.138 110.723 o 5 4 14 14.728 12.656 0.948 119.452 o 5 5 0 217.179 210.612 6.973 4.066 o 5 5 1 5.404 5.451 1.413 119.252 o 5 5 2 307.743 310.069 8.702 2.650 o 5 5 3 278.414 286.748 5.120 4.798 o 5 5 4 126.695 132.047 3.278 11.435 o 5 5 5 119.802 117.800 3.287 11.978 o 5 5 6 401.357 400.190 7.072 2.887 o 5 5 7 213.780 231.161 6.226 4.602 o 5 5 8 0.344 1.890 1.134 229.415 o 5 5 9 8.512 8.970 1.283 116.642 o 5 5 10 3.538 2.098 1.003 229.808 o 5 5 11 25.264 29.432 1.697 50.947 o 5 5 12 0.322 0.183 0.859 413.571 o 5 5 13 2.745 1.446 0.623 470.936 o 5 6 0 2.280 2.887 0.833 317.652 o 5 6 1 89.650 86.792 2.803 16.384 o 5 6 2 62.688 64.691 2.302 23.644 o 5 6 3 35.059 36.011 1.967 38.079 o 5 6 4 12.371 15.065 1.256 98.184 o 5 6 5 93.915 90.856 2.945 15.295 o 5 6 6 495.151 508.711 9.042 1.991 o 5 6 7 567.261 601.815 10.457 1.570 o 5 6 8 94.024 105.466 3.544 12.550 o 5 6 9 2.097 2.683 0.898 291.850 o 5 6 10 28.949 32.945 1.734 46.526 o 5 6 11 6.342 5.510 0.826 220.871 o 5 6 12 97.565 85.128 3.596 12.667 o 5 7 0 0.610 0.414 0.784 467.603 o 5 7 1 87.177 88.713 3.065 15.290 o 5 7 2 88.840 91.272 2.923 15.726 o 5 7 3 0.462 -0.687 1.085 262.687 o 5 7 4 3.495 3.230 1.104 193.967 o 5 7 5 138.816 145.411 4.502 8.140 o 5 7 6 31.706 34.719 2.002 39.041 o 5 7 7 24.334 25.244 1.461 60.663 o 5 7 8 0.730 0.882 0.739 495.753 o 5 7 9 142.017 150.101 3.269 10.580 o 5 7 10 56.059 53.829 1.779 30.995 o 5 7 11 14.262 14.718 1.450 81.382 o 5 8 0 125.714 124.458 4.131 9.450 o 5 8 1 18.229 17.148 1.599 66.289 o 5 8 2 70.570 71.369 3.020 17.423 o 5 8 3 7.626 7.349 1.257 126.340 o 5 8 4 1.379 1.160 1.243 187.030 o 5 8 5 0.004 0.059 0.984 328.826 o 5 8 6 4.337 4.397 1.000 206.257 o 5 8 7 1.133 1.427 0.845 367.779 o 5 8 8 3.262 2.278 0.711 365.106 o 5 8 9 158.209 132.433 4.835 7.329 o 5 8 10 5.484 3.547 0.658 306.665 o 5 9 0 214.712 213.546 5.195 5.620 o 5 9 1 10.200 11.139 1.333 102.912 o 5 9 2 295.775 296.998 6.534 3.737 o 5 9 3 208.329 206.337 5.020 5.912 o 5 9 4 8.711 9.065 1.494 95.546 o 5 9 5 0.799 1.169 0.874 363.066 o 5 9 6 0.988 -0.062 0.809 433.011 o 5 9 7 61.695 55.666 3.236 17.561 o 5 9 8 0.650 0.660 0.667 605.668 o 5 10 0 7.818 8.950 1.202 128.934 o 5 10 1 425.752 429.990 7.697 2.564 o 5 10 2 113.437 114.219 2.690 14.299 o 5 10 3 55.115 61.450 2.528 23.172 o 5 10 4 11.133 12.608 1.447 89.709 o 5 10 5 0.095 0.792 0.686 623.913 o 5 10 6 1.088 1.253 0.702 501.796 o 5 11 0 5.730 4.195 1.223 148.420 o 5 11 1 17.253 12.496 1.666 67.165 o 5 11 2 0.321 0.341 1.348 172.068 o 6 0 0 38.628 42.053 3.632 17.474 o 6 0 2 171.474 183.870 7.740 3.807 o 6 0 4 229.905 233.573 7.237 3.767 o 6 0 6 23.039 29.061 2.261 38.508 o 6 0 8 1.695 1.812 1.527 125.353 o 6 0 10 15.893 15.194 1.907 56.885 o 6 0 12 10.172 5.897 1.618 85.887 o 6 1 0 38.079 32.554 2.290 32.350 o 6 1 1 97.993 102.851 4.091 10.694 o 6 1 2 11.414 11.553 1.234 107.606 o 6 1 3 3.676 4.942 0.884 246.364 o 6 1 4 6.090 4.474 0.960 197.143 o 6 1 5 25.225 24.155 1.535 57.895 o 6 1 6 31.007 34.310 1.940 40.648 o 6 1 7 17.876 20.247 1.825 56.087 o 6 1 8 3.356 3.049 1.146 185.529 o 6 1 9 0.149 0.363 1.061 277.060 o 6 1 10 65.732 61.444 2.923 18.928 o 6 1 11 54.861 51.100 5.424 8.795 o 6 1 12 12.851 11.973 1.344 94.150 o 6 1 13 0.047 0.312 1.164 233.089 o 6 2 0 99.352 104.995 3.639 12.006 o 6 2 1 40.599 42.915 3.156 20.932 o 6 2 2 8.693 8.795 1.031 147.664 o 6 2 3 14.782 15.037 1.490 77.936 o 6 2 4 0.101 0.390 0.845 432.491 o 6 2 5 0.254 0.565 0.953 335.000 o 6 2 6 23.062 27.740 2.360 36.731 o 6 2 7 0.688 -0.315 1.277 189.234 o 6 2 8 5.696 5.505 1.454 113.170 o 6 2 9 25.600 25.810 2.434 34.773 o 6 2 10 206.197 200.640 6.619 4.429 o 6 2 11 37.225 40.490 2.283 31.586 o 6 2 12 297.876 266.557 5.404 4.526 o 6 3 0 16.731 16.423 1.233 88.138 o 6 3 1 69.118 67.448 2.247 22.886 o 6 3 2 5.764 5.094 0.981 192.463 o 6 3 3 0.419 1.017 0.818 427.455 o 6 3 4 218.354 225.928 4.694 6.040 o 6 3 5 1.592 1.971 1.154 206.378 o 6 3 6 60.622 69.371 3.580 15.177 o 6 3 7 0.252 0.151 1.305 184.707 o 6 3 8 52.661 53.817 2.687 22.722 o 6 3 9 172.116 174.777 5.205 6.297 o 6 3 10 292.254 289.733 8.085 2.975 o 6 3 11 673.181 664.324 15.633 0.894 o 6 3 12 63.732 53.967 3.410 16.423 o 6 4 0 127.376 138.403 3.862 9.840 o 6 4 1 1.610 0.180 0.776 428.879 o 6 4 2 103.531 110.325 2.872 14.358 o 6 4 3 1.201 1.128 0.803 403.097 o 6 4 4 8.270 8.721 1.622 86.547 o 6 4 5 7.501 5.414 1.274 128.864 o 6 4 6 0.001 0.091 1.093 266.646 o 6 4 7 20.439 18.639 2.383 38.999 o 6 4 8 45.582 46.241 2.638 24.870 o 6 4 9 198.449 195.121 4.916 6.210 o 6 4 10 247.205 249.884 5.860 4.601 o 6 4 11 18.390 17.934 1.423 73.681 o 6 5 0 0.132 0.995 0.769 496.601 o 6 5 1 14.116 13.948 1.203 99.050 o 6 5 2 8.905 8.781 1.149 131.043 o 6 5 3 37.882 37.544 2.143 33.890 o 6 5 4 2.680 2.216 1.103 208.260 o 6 5 5 597.682 624.769 10.401 1.536 o 6 5 6 382.989 386.820 7.839 2.681 o 6 5 7 12.735 13.778 1.447 85.242 o 6 5 8 0.198 -0.326 0.814 470.666 o 6 5 9 0.154 0.634 0.748 533.158 o 6 5 10 5.668 5.186 0.824 232.825 o 6 5 11 3.017 0.869 0.661 440.140 o 6 6 0 5.106 5.256 1.125 166.963 o 6 6 1 3.498 2.533 1.050 212.783 o 6 6 2 23.037 27.291 1.906 47.390 o 6 6 3 27.176 27.364 2.083 40.937 o 6 6 4 29.271 28.731 1.871 44.333 o 6 6 5 92.063 88.385 2.779 16.251 o 6 6 6 194.843 196.076 4.286 7.048 o 6 6 7 138.916 141.141 4.335 8.502 o 6 6 8 1.413 2.432 0.742 414.740 o 6 6 9 0.722 0.507 0.654 628.112 o 6 6 10 15.362 12.219 1.308 90.734 o 6 7 0 1.294 0.353 1.398 153.902 o 6 7 1 15.125 14.651 1.480 78.225 o 6 7 2 4.053 2.832 1.014 214.976 o 6 7 3 55.838 55.685 2.756 21.587 o 6 7 4 2.684 4.151 0.922 255.630 o 6 7 5 13.931 15.508 1.224 96.046 o 6 7 6 11.616 11.074 1.031 127.433 o 6 7 7 0.052 -0.174 0.552 1032.890 o 6 7 8 0.166 0.967 0.602 767.169 o 6 8 0 17.527 19.129 1.463 72.132 o 6 8 1 0.021 -0.274 1.154 239.618 o 6 8 2 12.999 13.609 1.959 58.033 o 6 8 3 0.015 1.160 0.970 322.494 o 6 8 4 12.223 12.319 1.298 98.795 o 6 8 5 13.338 13.154 1.233 99.917 o 6 8 6 11.522 11.816 1.061 123.185 o 6 8 7 32.899 31.453 3.494 19.551 o 6 9 0 116.150 115.719 3.644 11.130 o 6 9 1 57.563 57.811 2.870 20.368 o 6 9 2 129.070 131.553 4.135 9.264 o 6 9 3 37.086 36.469 1.763 40.828 o 6 9 4 3.372 2.541 0.695 366.297 o 6 9 5 8.462 6.325 1.722 81.076 o 6 10 0 49.338 46.361 3.202 19.393 o 6 10 1 227.963 193.493 25.573 0.467 o 7 0 0 10.959 9.922 1.966 61.390 o 7 0 2 122.545 115.942 4.761 8.255 o 7 0 4 1282.620 1322.480 25.342 0.350 o 7 0 6 0.001 -0.020 1.351 174.988 o 7 0 8 9.527 6.269 1.899 68.425 o 7 1 0 42.312 45.479 2.307 29.338 o 7 1 1 14.230 15.607 1.430 81.852 o 7 1 2 8.639 9.378 1.131 133.170 o 7 1 3 127.722 129.220 3.554 10.726 o 7 1 4 88.307 92.229 2.889 15.883 o 7 1 5 76.084 75.174 2.978 17.038 o 7 1 6 62.149 59.683 2.646 21.383 o 7 1 7 1.585 1.446 1.143 213.125 o 7 1 8 2.452 1.262 0.978 262.840 o 7 1 9 12.022 11.841 1.655 75.181 o 7 2 0 1.534 1.324 1.003 268.604 o 7 2 1 19.546 20.380 1.772 56.509 o 7 2 2 1.111 1.737 1.072 243.026 o 7 2 3 89.351 94.274 3.357 13.757 o 7 2 4 17.879 17.896 1.695 62.154 o 7 2 5 0.548 1.094 1.474 141.105 o 7 2 6 21.692 24.596 2.102 43.801 o 7 2 7 85.800 86.711 4.580 9.904 o 7 2 8 33.029 29.507 2.398 32.549 o 7 2 9 0.387 0.286 0.765 507.409 o 7 3 0 24.536 25.762 2.198 39.916 o 7 3 1 2.362 1.836 1.348 152.719 o 7 3 2 13.563 14.408 1.601 74.069 o 7 3 3 8.317 9.265 1.620 86.041 o 7 3 4 92.582 93.123 4.819 9.021 o 7 3 5 5.255 4.992 1.156 160.872 o 7 3 6 28.306 24.175 1.715 50.170 o 7 3 7 2.438 1.876 0.954 267.813 o 7 3 8 11.213 11.597 1.234 108.131 o 7 3 9 30.869 24.113 1.858 45.021 o 7 4 0 15.981 18.069 1.755 61.553 o 7 4 1 14.042 12.101 1.515 80.089 o 7 4 2 77.397 75.897 3.330 15.126 o 7 4 3 37.180 36.022 2.265 32.478 o 7 4 4 7.204 4.565 1.297 128.924 o 7 4 5 60.733 60.517 2.407 23.410 o 7 4 6 27.399 26.736 1.589 53.372 o 7 4 7 4.676 2.835 1.268 150.885 o 7 4 8 2.038 1.292 0.734 418.545 o 7 5 0 6.618 7.134 1.297 125.932 o 7 5 1 91.445 91.879 3.223 14.246 o 7 5 2 65.693 66.002 2.534 21.353 o 7 5 3 7.072 5.594 0.991 176.409 o 7 5 4 243.179 246.656 5.347 5.064 o 7 5 5 201.054 196.301 4.564 6.597 o 7 5 6 122.226 114.814 5.100 7.613 o 7 5 7 47.602 41.601 1.750 35.804 o 7 6 0 18.297 18.231 1.860 55.339 o 7 6 1 71.441 77.676 2.572 19.729 o 7 6 2 29.992 25.755 1.696 49.014 o 7 6 3 96.493 92.701 4.486 9.782 o 7 6 4 48.824 45.662 2.603 24.733 o 7 6 5 80.498 67.634 4.229 11.484 o 7 6 6 123.534 96.872 3.796 10.776 o 7 7 0 0.283 0.423 0.768 506.497 o 7 7 1 19.540 19.240 1.237 79.964 o 7 7 2 28.085 26.322 1.561 53.813 o 7 7 3 49.557 46.495 3.674 16.184 o 7 7 4 0.186 0.801 0.665 649.563 o 7 8 0 73.418 55.299 5.134 9.102 o 7 8 1 0.751 0.492 0.646 637.950 o 7 8 2 12.638 12.152 2.343 45.235 o 8 0 0 0.252 0.812 1.232 203.192 o 8 0 2 37.664 37.758 2.660 26.853 o 8 0 4 88.434 89.838 3.943 11.739 o 8 1 0 0.281 2.109 0.872 366.347 o 8 1 1 11.552 10.255 1.079 124.447 o 8 1 2 10.156 12.009 1.132 120.922 o 8 1 3 1.248 1.686 1.186 202.155 o 8 1 4 1.032 1.306 0.956 302.978 o 8 1 5 0.467 0.857 0.830 418.616 o 8 2 0 7.844 5.203 0.921 185.145 o 8 2 1 3.521 2.766 0.896 263.017 o 8 2 2 14.278 13.046 1.715 68.080 o 8 2 3 0.275 0.815 0.899 369.268 o 8 2 4 0.200 -0.133 0.779 512.882 o 8 2 5 22.960 17.207 1.924 50.155 o 8 3 0 0.031 -0.436 1.176 230.645 o 8 3 1 0.099 -0.411 1.136 246.207 o 8 3 2 36.954 33.006 2.451 30.241 o 8 3 3 3.415 1.657 0.807 317.316 o 8 3 4 1.539 0.766 0.854 358.599 o 8 4 0 3.272 3.798 1.094 195.867 o 8 4 1 13.444 17.648 1.531 75.673 o 8 4 2 4.411 3.683 0.850 256.322 o 8 4 3 15.355 12.168 2.187 48.468 o 8 5 0 12.344 10.538 1.127 116.086 o 8 5 1 24.375 19.766 1.404 65.578 o 8 5 2 8.458 3.947 1.767 79.949 o ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.160 _oxdiff_exptl_absorpt_empirical_full_min 0.880 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn C1 C 0.29960(11) 0.97085(7) 0.07029(5) 0.02484(18) Uani 1.000000 . C2 C 0.21234(11) 1.14176(8) -0.02351(5) 0.02619(18) Uani 1.000000 . C3 C 0.24497(11) 1.01468(7) -0.00723(5) 0.02467(17) Uani 1.000000 . O4 O 0.46935(9) 0.92768(6) 0.23597(4) 0.03883(17) Uani 1.000000 . C5 C 0.31921(11) 1.05635(7) 0.13172(5) 0.02510(18) Uani 1.000000 . C6 C 0.23550(11) 1.22468(7) 0.03897(5) 0.02680(18) Uani 1.000000 . C7 C 0.26738(11) 0.80433(8) -0.05566(5) 0.03049(19) Uani 1.000000 . C8 C 0.22874(11) 0.93027(8) -0.06999(5) 0.02721(18) Uani 1.000000 . C9 C 0.28357(12) 1.17957(8) 0.11413(5) 0.02711(18) Uani 1.000000 . C10 C 0.17182(13) 0.88884(10) -0.20805(6) 0.0385(2) Uani 1.000000 . C11 C 0.17914(11) 0.97188(8) -0.14751(5) 0.0314(2) Uani 1.000000 . O12 O 0.25430(11) 1.41090(6) -0.02805(4) 0.04715(19) Uani 1.000000 . C13 C 0.33110(12) 0.84221(8) 0.08233(6) 0.03070(19) Uani 1.000000 . C14 C 0.14088(13) 1.09880(9) -0.16142(5) 0.0348(2) Uani 1.000000 . C15 C 0.31681(13) 0.76307(9) 0.02238(6) 0.0338(2) Uani 1.000000 . C16 C 0.15525(12) 1.17991(9) -0.10265(5) 0.0326(2) Uani 1.000000 . C17 C 0.25967(13) 0.72360(10) -0.11762(6) 0.0381(2) Uani 1.000000 . C18 C 0.22392(12) 1.36048(8) 0.02915(5) 0.0318(2) Uani 1.000000 . C19 C 0.38552(12) 1.02303(8) 0.21500(5) 0.02865(19) Uani 1.000000 . C20 C 0.21282(13) 0.76595(10) -0.19328(6) 0.0411(2) Uani 1.000000 . C21 C 0.17929(17) 1.43629(9) 0.09383(6) 0.0381(2) Uani 1.000000 . C22 C 0.35001(17) 1.11170(10) 0.27514(6) 0.0380(2) Uani 1.000000 . H9 H 0.3001(13) 1.2443(9) 0.1610(5) 0.050(3) Uani 1.000000 . H20 H 0.2120(16) 0.7035(10) -0.2406(6) 0.072(4) Uani 1.000000 . H10 H 0.1365(16) 0.9227(11) -0.2679(6) 0.069(4) Uani 1.000000 . H16 H 0.1278(15) 1.2774(9) -0.1140(6) 0.061(3) Uani 1.000000 . H13 H 0.3696(15) 0.8093(9) 0.1415(5) 0.059(3) Uani 1.000000 . H14 H 0.1015(16) 1.1286(10) -0.2218(6) 0.065(3) Uani 1.000000 . H22a H 0.3808(19) 1.0679(11) 0.3316(6) 0.078(4) Uani 1.000000 . H15 H 0.3462(16) 0.6660(9) 0.0335(6) 0.065(3) Uani 1.000000 . H22b H 0.4382(19) 1.1914(11) 0.2771(7) 0.076(4) Uani 1.000000 . H21a H 0.0672(19) 1.3981(11) 0.1155(7) 0.084(4) Uani 1.000000 . H21b H 0.144(2) 1.5278(10) 0.0722(7) 0.083(4) Uani 1.000000 . H21c H 0.3034(18) 1.4410(11) 0.1415(7) 0.078(4) Uani 1.000000 . H22c H 0.2044(18) 1.1431(11) 0.2629(6) 0.076(4) Uani 1.000000 . H17 H 0.2909(16) 0.6267(10) -0.1054(7) 0.070(3) Uani 1.000000 . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0227(4) 0.0265(4) 0.0254(4) -0.0006(3) 0.0054(3) 0.0031(3) C2 0.0239(4) 0.0292(4) 0.0253(4) -0.0002(3) 0.0052(3) 0.0046(3) C3 0.0218(4) 0.0281(4) 0.0243(4) -0.0017(3) 0.0055(3) 0.0012(3) O4 0.0490(4) 0.0374(4) 0.0280(3) 0.0066(3) 0.0039(3) 0.0085(3) C5 0.0251(4) 0.0268(4) 0.0238(4) -0.0001(3) 0.0062(3) 0.0035(3) C6 0.0270(4) 0.0265(4) 0.0268(4) 0.0004(3) 0.0055(3) 0.0048(3) C7 0.0258(4) 0.0318(4) 0.0343(5) -0.0033(3) 0.0078(4) -0.0049(4) C8 0.0211(4) 0.0338(5) 0.0269(4) -0.0031(3) 0.0058(3) -0.0023(3) C9 0.0283(4) 0.0273(4) 0.0258(5) -0.0002(3) 0.0062(3) 0.0025(4) C10 0.0306(5) 0.0548(6) 0.0299(5) -0.0075(4) 0.0066(4) -0.0098(4) C11 0.0254(4) 0.0430(5) 0.0252(4) -0.0042(4) 0.0045(3) -0.0023(4) O12 0.0698(5) 0.0317(4) 0.0442(4) 0.0021(3) 0.0218(4) 0.0121(3) C13 0.0333(5) 0.0277(4) 0.0314(5) 0.0008(3) 0.0078(4) 0.0035(4) C14 0.0326(5) 0.0469(6) 0.0238(5) -0.0012(4) 0.0042(4) 0.0036(4) C15 0.0344(5) 0.0279(5) 0.0398(5) 0.0009(4) 0.0096(4) 0.0004(4) C16 0.0330(5) 0.0375(5) 0.0267(5) 0.0022(4) 0.0055(4) 0.0072(4) C17 0.0321(5) 0.0392(5) 0.0440(6) -0.0046(4) 0.0103(4) -0.0132(5) C18 0.0337(5) 0.0280(4) 0.0338(5) 0.0008(3) 0.0078(4) 0.0058(4) C19 0.0289(4) 0.0319(4) 0.0250(4) -0.0010(3) 0.0057(3) 0.0046(3) C20 0.0338(5) 0.0517(6) 0.0386(6) -0.0083(4) 0.0095(4) -0.0169(5) C21 0.0437(6) 0.0285(5) 0.0417(6) -0.0006(4) 0.0083(5) 0.0001(4) C22 0.0419(6) 0.0447(6) 0.0267(5) 0.0013(5) 0.0062(4) -0.0007(4) H9 0.057(7) 0.049(7) 0.043(6) -0.001(5) 0.011(5) -0.009(5) H20 0.081(9) 0.080(8) 0.055(8) -0.006(7) 0.017(6) -0.043(7) H10 0.074(9) 0.107(10) 0.028(6) -0.006(7) 0.014(6) 0.002(7) H16 0.081(8) 0.046(7) 0.059(8) 0.011(6) 0.019(6) 0.022(6) H13 0.081(8) 0.062(7) 0.032(6) 0.006(6) 0.013(6) 0.013(6) H14 0.083(9) 0.081(8) 0.031(6) 0.010(7) 0.011(6) 0.010(6) H22a 0.131(12) 0.083(9) 0.017(6) 0.015(8) 0.009(6) 0.018(6) H15 0.084(9) 0.041(7) 0.071(8) 0.007(6) 0.021(6) -0.001(6) H22b 0.096(10) 0.075(9) 0.063(9) -0.026(8) 0.025(7) -0.020(7) H21a 0.092(10) 0.077(9) 0.099(11) -0.026(8) 0.055(9) -0.026(8) H21b 0.138(12) 0.036(7) 0.075(9) 0.018(7) 0.020(8) 0.018(6) H21c 0.069(9) 0.081(10) 0.069(9) 0.001(7) -0.017(7) -0.021(7) H22c 0.068(9) 0.100(10) 0.056(8) 0.026(8) 0.005(7) -0.008(7) H17 0.067(8) 0.045(7) 0.099(10) -0.001(6) 0.023(7) -0.014(7) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source _atom_type_scat_dispersion_source C 0.01788 0.00908 'NoSpherA2: Chem.Sci. 2021, DOI:10.1039/D0SC05526C' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' H 0.00000 0.00000 'NoSpherA2: Chem.Sci. 2021, DOI:10.1039/D0SC05526C' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' O 0.04960 0.03234 'NoSpherA2: Chem.Sci. 2021, DOI:10.1039/D0SC05526C' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code 0 0 2 80825.7 2842.27 11 0 0 3 -5.97715 22.3278 11 0 0 -3 -15.8399 18.5282 13 0 0 -4 15183.8 623.62 13 0 0 4 16362.8 638.187 11 0 0 -5 9.00743 25.8068 13 0 0 5 20.3205 31.8862 11 0 0 -6 17071.3 767.139 7 0 0 6 16178.8 691.51 11 0 0 -6 15449.3 672.521 13 0 0 7 20.9051 20.9388 34 0 0 -7 -6.68206 23.446 14 0 0 -7 7.21783 24.4669 31 0 0 -7 64.8058 33.2106 13 0 0 7 -14.5833 29.5416 11 0 0 -8 9806.94 433.918 31 0 0 8 9712.06 416.16 19 0 0 8 9401.7 420.733 16 0 0 8 9347.75 429.255 20 0 0 8 10083.6 431.66 34 0 0 -8 10574.6 432.944 14 0 0 8 10386.5 516.221 11 0 0 9 8.00742 25.1289 19 0 0 9 19.3696 27.7444 20 0 0 -9 46.157 32.3886 14 0 0 -9 -20.1317 35.316 31 0 0 9 8.60322 28.1007 16 0 0 9 -31.0588 37.5144 15 0 0 9 9.5379 28.6572 34 0 0 -10 138.573 46.7156 14 0 0 -10 151.949 48.9091 31 0 0 10 239.856 56.7845 15 0 0 10 210.307 45.7833 19 0 0 10 175.522 48.0536 34 0 0 10 168.088 46.9227 20 0 0 11 25.6413 36.7264 20 0 0 -11 -13.7426 32.9372 28 0 0 -11 26.8431 36.4747 31 0 0 -11 -12.1564 29.1356 14 0 0 11 -12.4632 27.6552 34 0 0 11 -10.3191 20.9029 19 0 0 -12 4029.89 277.067 28 0 0 12 3969.53 266.473 34 0 0 -12 4427.11 272.271 14 0 0 12 4388.69 275.575 20 0 0 12 4298.82 252.917 19 0 0 -12 3745.48 265.591 31 0 0 -13 60.2623 40.9485 14 0 0 -13 -17.455 38.7379 28 0 0 -13 -16.958 37.6351 31 0 0 13 -46.1542 44.0769 34 0 0 13 -16.086 38.5599 20 0 0 -14 92.2534 50.2958 31 0 0 14 122.056 54.8577 20 0 0 -14 133.448 57.4111 28 0 0 -15 -19.477 43.2186 31 0 0 15 18.3315 37.1331 20 0 0 -15 20.2048 36.6069 28 0 0 16 4525.29 307.32 70 0 0 16 4524.01 315.365 61 0 0 -16 4122.77 315.016 28 0 0 -16 4851.66 333.472 31 0 0 16 4465.01 315.66 65 0 0 16 5016.92 325.943 20 0 0 17 51.8661 51.9465 61 0 0 -17 -57.5092 54.9174 31 0 0 17 -17.4207 49.9075 65 0 0 17 16.3025 46.7046 70 0 0 -17 20.0445 44.4818 28 0 0 18 123.814 59.559 61 0 0 18 125.428 56.8917 65 0 0 18 43.5207 45.6244 70 0 0 19 11.9296 26.4763 70 0 0 19 26.2083 42.8035 65 0 0 20 1719.38 136.173 70 0 0 20 2098.17 152.308 65 0 0 21 -6.04643 23.2405 65 0 0 21 18.9494 16.624 70 0 1 0 -3.64072 9.03195 8 0 -1 0 14.2009 16.6075 12 0 -1 0 5.51509 9.8521 8 0 1 -1 129208 4343.34 12 0 -1 -1 123311 4340.52 12 0 1 1 124481 4351.03 7 0 -1 -1 123799 4318.47 9 0 -1 1 120154 4330.4 8 0 1 -2 30206.8 1106.55 12 0 -1 -2 30368.9 1104.84 12 0 1 2 31009.1 1142.19 7 0 1 2 30442.6 1104.97 12 0 -1 2 30021.3 1106.78 12 0 -1 -3 47341.3 1709.5 12 0 1 3 47374 1707.75 12 0 1 -3 47983.5 1713.83 12 0 -1 3 48108.3 1713.82 12 0 1 3 47284.3 1725.65 13 0 1 3 51084.9 1783.57 7 0 -1 4 178.273 31.2234 2 0 -1 4 151.751 28.7781 11 0 -1 -4 189.001 31.7569 2 0 1 -4 186.74 32.601 12 0 1 4 243.493 45.788 13 0 1 4 273.161 64.8594 7 0 1 4 188.354 55.7841 11 0 1 5 1169.69 67.4858 10 0 -1 5 1147.06 90.193 11 0 1 5 1332.36 146.463 7 0 -1 -5 1188.73 71.0015 2 0 -1 6 2146.21 133.429 27 0 -1 -6 2546.79 228.615 7 0 1 -6 2499.6 224.004 7 0 -1 6 1972.92 143.18 11 0 1 6 2579.76 209.296 11 0 1 -7 1710.67 116.959 29 0 1 -7 1536.98 159.501 13 0 -1 -7 1711.27 119.404 31 0 1 7 1953.77 192.237 11 0 1 -7 1609.56 121.58 14 0 1 7 1773.86 120.89 19 0 -1 7 1577.7 132.283 11 0 1 7 1603.13 120.522 34 0 1 7 1934.32 122.76 20 0 -1 7 1697.57 121.265 15 0 1 7 1883.71 120.652 37 0 -1 7 1772.47 125.342 27 0 -1 7 1658.52 114.908 34 0 -1 -8 76.9545 31.7479 14 0 -1 -8 41.4004 28.1341 31 0 1 8 49.3506 25.6218 16 0 -1 8 35.7541 26.9275 15 0 -1 8 38.8617 29.0965 34 0 1 -8 122.476 37.3938 29 0 1 8 72.5604 33.5262 20 0 1 -8 79.5858 34.0426 14 0 1 8 40.1846 27.3121 19 0 1 8 45.9367 29.4905 37 0 -1 8 82.6371 28.3624 19 0 1 8 44.3475 30.1273 34 0 1 -9 199.812 51.6459 31 0 1 9 155.975 40.4868 16 0 -1 -9 223.696 50.1935 31 0 -1 -9 205.796 44.5159 14 0 -1 9 117.117 32.9702 19 0 1 -9 191.635 43.6275 29 0 -1 -9 268.508 56.4453 28 0 1 -9 215.258 50.357 14 0 1 9 216.834 47.9207 20 0 1 9 137.935 43.6918 19 0 -1 9 108.586 39.7602 34 0 -1 9 250.448 55.4408 15 0 1 9 123.065 42.9866 34 0 1 10 479.336 70.8308 19 0 1 -10 523.629 79.8674 31 0 1 10 657.956 88.1525 34 0 -1 10 447.362 70.0939 34 0 1 10 556.298 71.48 16 0 1 -10 553.503 84.3978 14 0 1 10 436.189 73.2711 20 0 -1 10 397.949 74.4655 15 0 -1 -10 575.03 83.0031 28 0 -1 -10 429.463 72.2546 31 0 -1 -11 1632.82 148.323 31 0 1 11 1644.08 146.065 20 0 -1 11 1697.19 156.045 15 0 -1 -11 1843.05 162.446 28 0 1 -11 1744.77 159.127 31 0 -1 11 1653.31 145.69 34 0 1 11 1384.01 144.873 34 0 1 11 1611.91 138.402 16 0 1 11 1519.35 138.068 19 0 1 -11 1927.2 161.37 14 0 -1 11 1667.7 153.117 20 0 1 12 12.9411 28.7168 19 0 -1 12 26.4022 26.7416 34 0 -1 12 46.7604 39.9372 15 0 -1 12 -15.1346 30.6579 20 0 1 -12 15.7972 42.9314 31 0 1 12 14.0478 31.1722 20 0 -1 -12 14.6787 29.7344 31 0 1 -12 45.0316 38.4608 14 0 -1 -12 -15.5754 42.3286 28 0 1 12 -14.8803 35.6647 34 0 -1 -13 12435 602.144 31 0 -1 -13 12395.1 610.067 28 0 -1 13 11771.8 578.275 34 0 1 13 12337.2 580.718 19 0 1 -13 12315.3 611.721 31 0 1 13 13190.1 600.19 20 0 -1 13 12341.2 603.32 20 0 1 -13 12853.5 609.738 14 0 1 14 25698.8 1065.6 20 0 1 -14 25487.9 1089.26 31 0 -1 -14 26846.9 1096.09 28 0 -1 14 24227.8 1072.58 20 0 1 -14 26305.1 1084.03 14 0 -1 -14 26985.1 1085.06 31 0 1 14 23948.5 1036.46 19 0 -1 14 24014.8 1041.4 34 0 1 -15 6531.26 412.543 14 0 -1 -15 7630.73 434.184 31 0 -1 15 7608.33 437.566 20 0 1 -15 7589.71 445.186 31 0 -1 -15 7165.88 433.656 28 0 -1 16 316.515 81.1065 65 0 -1 16 192.071 65.3751 20 0 -1 16 159.082 68.1949 61 0 -1 -16 182.545 71.4105 28 0 -1 -16 75.2594 54.2275 31 0 1 16 240.703 75.2475 61 0 1 -16 183.354 76.3259 31 0 -1 16 145.705 62.5067 70 0 1 16 265.309 77.0722 65 0 1 16 125.281 58.7598 70 0 1 17 419.476 92.6606 65 0 1 -17 590.839 114.02 31 0 -1 17 607.93 105.499 20 0 -1 17 355.44 91.124 65 0 -1 17 450.688 92.1959 61 0 -1 -17 452.916 95.806 28 0 1 17 422.409 90.2728 61 0 1 17 492.833 97.5278 70 0 -1 17 560.319 95.4668 70 0 1 18 403.892 82.487 65 0 -1 18 303.779 83.1032 65 0 -1 18 428.893 83.7502 61 0 -1 18 423.042 77.008 70 0 1 18 456.145 88.2159 70 0 1 19 240.429 68.7973 70 0 -1 19 401.986 77.637 65 0 1 19 419.026 77.4085 65 0 -1 19 315.274 63.4907 70 0 1 20 63.1547 35.6463 65 0 1 20 57.2445 32.3618 70 0 -1 20 -10.2194 38.1895 65 0 1 21 282.357 44.8037 70 0 -1 21 376.576 51.9548 65 0 -1 -21 252.757 44.4943 59 0 2 0 7268.3 290.685 8 0 -2 0 7445.49 293.496 8 0 -2 0 6623.56 344.172 12 0 -2 -1 1815.6 98.7583 8 0 -2 1 1581.95 107.918 8 0 2 1 1704.26 98.5663 9 0 2 -1 1975.41 112.939 8 0 2 -1 1784.18 140.338 12 0 -2 -1 1728.6 137.875 12 0 2 -2 26107.6 988.154 8 0 2 2 26264.4 1010.04 12 0 -2 -2 25200.1 1007.4 12 0 -2 2 25797.6 1011.37 12 0 2 2 27056.2 1036.4 7 0 -2 -2 26218.7 968.867 9 0 2 -2 25346.1 1009.46 12 0 2 -3 19060.8 768.95 12 0 2 3 19254.3 764.991 12 0 2 3 19252.2 810.164 7 0 -2 3 18168.7 762.991 12 0 -2 -3 18962.5 765.307 12 0 2 -3 19001.2 774.359 8 0 2 -4 3336.47 206.128 12 0 -2 -4 3229.38 199.461 12 0 -2 4 3477.69 208.558 12 0 2 4 3477.24 211.053 13 0 2 -4 3178.41 225.287 8 0 2 4 3327.63 199.471 12 0 2 4 3270.69 245.287 7 0 2 5 656.994 86.5475 13 0 -2 -5 754.877 85.5793 2 0 2 5 549.034 103.491 11 0 2 -5 691.86 84.1811 12 0 -2 5 720.69 84.5685 2 0 2 -5 704.115 107.756 8 0 -2 -5 542.454 103.464 7 0 2 5 704.706 114.208 7 0 -2 -6 589.543 64.2947 28 0 2 6 532.562 62.4262 37 0 -2 6 412.467 62.1253 2 0 2 -6 421.389 58.5624 14 0 -2 6 474.185 60.0418 15 0 2 -6 693.446 118.172 8 0 2 6 337.951 69.3576 13 0 2 6 546.102 110.713 11 0 -2 6 622.476 65.8061 22 0 2 -6 495.409 61.3466 29 0 -2 6 527.415 64.3877 27 0 2 6 655.802 68.0021 34 0 -2 -7 7170.26 309.488 28 0 -2 -7 6212.51 290.888 31 0 2 7 6112.76 291.211 20 0 2 -7 6092.14 302.435 29 0 2 7 6659.75 305.593 37 0 2 -7 6387.18 307.942 14 0 -2 7 6381.62 304.782 15 0 2 7 6048.31 301.489 19 0 2 7 6260.46 291.536 38 0 -2 7 6370.95 306.503 27 0 2 -8 1599.3 132.454 14 0 2 8 1540.33 122.494 20 0 -2 -8 1550.78 120.466 31 0 2 -8 1699.62 130.61 29 0 -2 8 1489.54 126.977 15 0 2 8 1513.76 115.151 38 0 -2 -8 1714.01 129.754 28 0 -2 8 1674.92 132.152 27 0 2 8 1712.27 131.14 19 0 -2 8 1517.72 115.186 34 0 2 8 1691.79 117.152 16 0 -2 9 -11.2722 30.6334 27 0 2 9 10.4874 31.5087 19 0 2 -9 11.3569 30.8637 14 0 2 9 9.45767 22.6673 20 0 -2 9 52.4826 27.4486 34 0 2 9 -7.92427 20.3036 38 0 2 9 -11.212 30.4698 34 0 -2 -9 -21.1234 30.2551 28 0 -2 9 21.797 26.1205 15 0 2 9 16.3441 19.5862 16 0 -2 -9 -9.43726 31.9871 31 0 2 -9 -10.355 28.1409 29 0 -2 -10 2314.9 173.618 28 0 2 10 2202.37 151.118 16 0 2 -10 1954.34 158.185 29 0 -2 -10 1856.25 152.473 31 0 2 10 1946.35 158.936 19 0 2 -10 1984.11 169.257 14 0 -2 10 2084.88 167.164 15 0 -2 10 2010.31 153.36 34 0 2 10 2237.66 162.331 20 0 2 10 2025.7 166.812 34 0 -2 11 2125.81 176.389 15 0 2 -11 1837.79 158.329 29 0 -2 11 1747.63 146.646 34 0 -2 -11 1652.73 159.537 28 0 2 11 1760.71 158.277 19 0 2 11 1900.24 157.952 20 0 -2 -11 2012.27 162.839 31 0 2 -11 1845.82 169.003 14 0 -2 -12 9123.67 467.667 31 0 -2 12 9639.89 487.871 15 0 2 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35 1 4 -10 2193.06 174.406 26 -1 4 10 2073.07 175.171 19 1 4 -10 1994.13 175.91 14 1 -4 -10 1961.49 170.658 22 -1 -4 10 1955.89 171.25 27 -1 4 10 1557.43 147.064 16 -1 -4 10 1994.15 158.676 15 1 4 -10 1833.93 171.165 29 -1 -4 9 8734.13 421.004 25 1 -4 -9 9027.59 441.053 22 -1 -4 9 8865.85 444.393 27 1 4 -9 9060.87 456.432 29 -1 -4 9 8844.25 420.748 15 1 4 -9 9664.48 446.768 26 -1 4 9 9451.5 438.44 35 1 4 -9 9667.98 458.379 14 -1 -4 9 9412.23 451.896 22 -1 4 9 8482.78 437.077 19 -1 4 9 7940.98 417.886 16 -1 -4 8 1414.97 121.906 25 -1 4 8 1197.57 123.655 19 1 4 -8 1239.68 129.054 29 -1 4 8 1533.13 130.31 35 -1 -4 8 1293.07 117.464 15 1 4 -8 1502.06 137.06 14 -1 4 8 1519.47 126.186 21 1 4 -8 1363.76 128.458 26 -1 4 8 1658.16 131.625 16 -1 4 8 1347.93 127.436 38 1 -4 -8 1380.65 126.639 22 -1 -4 8 1514.93 135.275 22 -1 -4 8 1321.01 127.381 27 1 -4 -7 7574.2 369.593 18 -1 4 7 7913.6 359.207 35 -1 4 7 7174.42 352.927 21 -1 -4 7 7546.42 353.568 25 -1 -4 7 7557.51 347.071 15 -1 -4 7 7506.44 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-2 432.691 57.5012 33 2 -3 -1 1858.85 121.774 15 2 -3 -1 1548.46 163.044 11 2 3 -1 1622.45 182.311 9 2 -3 -1 1553.61 116.934 33 -2 -3 1 2042.69 196.282 8 -2 -3 1 1778.55 115.413 22 2 3 -1 1677.41 122.286 4 -2 3 1 1661.68 117.687 21 -2 3 1 1885.63 121.843 24 -2 -3 1 1625 113.04 36 -2 3 1 1658.08 117.132 3 -2 3 1 1810.97 107.48 8 2 -3 0 4206.72 221.087 15 2 -3 0 4881.91 293.577 11 -2 3 0 4195.39 219.118 3 -2 -3 0 4397.9 217.025 36 2 3 0 4786.22 333.708 9 -2 -3 0 4772.99 222.628 22 -2 -3 0 4394.16 311.378 8 -2 3 0 4537.78 226.962 8 2 3 0 4331.49 227.256 4 2 3 0 4874.49 294.47 7 -2 3 0 4288.68 217.741 21 2 -3 0 4115.23 217.728 30 2 3 1 176.973 40.344 4 -2 -3 -1 134.905 34.7803 36 2 -3 1 144.059 49.1632 11 -2 3 -1 212.637 43.788 24 2 -3 1 214.35 45.6796 15 -2 3 -1 118.322 36.0067 3 -2 -3 -1 166.404 37.0077 22 -2 3 -1 164.47 40.8883 9 2 -3 1 107.001 31.8639 30 -2 3 -1 98.6303 34.5716 14 2 3 1 113.262 51.0137 7 2 3 1 108.988 56.0672 9 2 -3 2 1896.71 135.193 15 -2 -3 -2 2182.38 136.209 22 2 -3 2 1971.42 154.934 11 -2 3 -2 1867.13 163.485 9 -2 3 -2 1954.28 138.124 24 -2 -3 -2 2082.61 132.533 36 2 3 2 2230.55 200.234 7 2 3 2 2008.79 137.961 4 -2 3 -2 2061.45 135.609 14 2 -3 2 1791.02 124.999 30 2 -3 2 2082.1 140.068 33 -2 3 -2 2014.39 131.571 3 2 3 3 4562.28 229.971 34 -2 -3 -3 4505.86 230.713 36 -2 -3 -3 4711.19 236.417 22 -2 3 -3 4189.9 235.556 14 2 -3 3 4634 226.354 27 -2 3 -3 4373.38 241.61 24 2 -3 3 4303.11 225.193 30 -2 3 -3 4782.2 310.887 9 2 3 3 4524.97 232.801 4 -2 3 -3 4505.63 228.405 3 2 3 3 4330.96 320.458 7 2 3 3 4157.86 241.462 38 -2 -3 -3 4645.12 220.851 18 2 -3 3 4532.85 242.092 33 2 -3 3 4538.28 242.613 15 2 3 4 23.1824 22.1387 4 2 -3 4 45.9917 25.9832 27 -2 -3 -4 7.16397 20.5247 18 -2 3 -4 7.1131 26.5694 3 -2 3 -4 -9.43743 28.356 24 2 -3 4 29.4761 22.1422 30 2 -3 4 48.2505 32.7102 15 2 3 4 -19.7041 34.5666 38 2 3 4 16.8246 25.2764 34 -2 -3 -4 17.2163 30.2028 22 -2 3 -4 9.28656 34.6867 14 -2 -3 -5 1456.02 133.719 28 2 -3 5 1646.53 130.069 27 -2 -3 -5 1934.91 143.447 22 -2 3 -5 1732.09 143.895 14 -2 3 -5 1877.98 136.467 31 2 -3 5 1980.56 153.482 15 2 3 5 1986.18 146.671 34 2 3 5 2049.02 132.882 4 2 3 5 2050.23 154.962 37 2 3 5 2027.45 151.106 38 -2 3 -5 1773.04 142.754 24 2 -3 6 2725.73 179.178 27 2 -3 6 2638.33 194.012 15 -2 3 -6 2831.16 194.856 24 -2 -3 -6 2569.32 183.324 22 2 3 6 2978.16 201.935 37 2 3 6 2936.83 191.961 38 2 3 6 2564.43 181.907 34 -2 -3 -6 2765.08 189.812 28 2 -3 6 2168.43 178.313 34 -2 3 -6 2539.44 173.873 31 2 -3 7 2328.07 169.608 27 2 -3 7 2089.15 177.437 15 -2 3 -7 2337.33 171.553 31 -2 3 -7 2204.27 172.32 24 -2 -3 -7 2264.84 174.662 28 2 -3 7 2015.03 168.256 34 -2 -3 -7 2153.7 168.555 22 -2 3 -7 2132.56 152.542 28 2 3 7 1968.55 164.142 38 2 3 7 2242.69 175.825 34 -2 -3 -8 1954.72 172.935 28 2 -3 8 1969.33 164.839 27 2 3 8 2183.81 180.09 34 -2 3 -8 2398.95 181.168 24 2 3 8 2020.68 177.27 37 2 -3 8 2197.63 180.766 34 -2 -3 -8 2175.2 176.206 22 2 3 8 1919.19 163.772 38 -2 3 -8 2012.62 179.058 14 2 3 8 2168.2 181.204 19 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15597.8 741.018 28 -2 3 -12 14196 698.14 28 2 -3 12 15926.5 751.959 15 -2 3 -12 15119 745.022 14 -2 -3 -12 15804.9 732.888 22 2 3 12 16768.8 759.52 34 2 3 12 15663.3 722.578 19 -2 -3 -13 8208.57 476.79 28 -2 3 -13 8861.3 467.047 28 2 -3 13 8917.08 499.882 15 -2 3 -13 8457.14 491.737 14 2 -3 13 8890.89 470.304 50 -2 -3 -13 8412.92 477.905 22 2 3 13 7830.91 457.176 71 2 -3 13 9090.16 483.32 20 2 -3 13 7950.59 465.492 34 -2 3 -13 8646.41 475.419 40 2 3 13 7940.93 458.534 19 2 3 13 8936.68 482.829 61 2 -3 13 8531.96 481.656 61 2 -3 14 3852.97 281.546 34 2 3 14 4170.23 283.261 19 -2 3 -14 3899.12 297.65 55 2 -3 14 3983.74 307.04 15 2 -3 14 3794.14 276.724 50 2 3 14 4082.77 297.305 61 -2 -3 -14 3744.31 286.278 22 -2 -3 -14 3717.4 291.198 28 -2 3 -14 4019.73 288.006 40 2 3 14 3944.14 280.716 71 -2 3 -14 4186.69 306.208 14 2 -3 14 3734.28 290.156 61 -2 -3 -14 4096.03 280.354 59 -2 3 -15 387.221 94.7895 55 2 3 15 535.237 91.6296 71 2 -3 15 463.99 86.6341 49 2 3 15 628.264 109.92 70 2 3 15 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170.937 18 2 -4 7 2233.53 184.537 15 -2 4 -7 2052.47 175.894 24 2 -4 7 2027.78 173.352 34 -2 4 -7 1892.7 154.214 31 -2 -4 -7 1967.66 170.296 22 2 4 7 2042.32 178.697 37 2 4 7 2404.85 186.061 38 2 4 7 1913.66 169.769 34 -2 4 -7 2073.59 178.819 14 2 -4 8 297.63 68.5251 27 2 4 8 325.001 74.1459 37 -2 4 -8 182.6 57.5369 24 -2 4 -8 309.036 64.5145 31 2 -4 8 146.4 57.7699 15 2 4 8 301.511 70.2092 34 -2 -4 -8 163.669 59.4312 22 2 4 8 232.925 62.5009 38 2 4 8 301.95 71.0939 19 -2 -4 -8 306.942 66.8187 18 -2 4 -8 332.154 74.9881 14 2 -4 8 366.929 75.7434 34 -2 -4 -9 10117.7 539.211 28 2 -4 9 10742.4 539.143 27 2 -4 9 10955.7 545.092 34 2 4 9 11221.7 554.603 34 2 -4 9 12452.6 580.827 15 -2 4 -9 11467 553.379 24 -2 -4 -9 10477.3 547.49 22 2 4 9 10726.2 536.946 38 -2 -4 -9 12076.8 546.571 18 -2 4 -9 11196.7 537.312 31 2 4 9 10565.2 554.16 19 -2 -4 -10 1987.9 194.15 28 -2 -4 -10 2519.48 212.779 22 2 4 10 2244.84 208.718 37 2 4 10 2029.22 194.669 19 2 -4 10 2425.52 214.683 15 -2 4 -10 2390.07 203.557 24 2 4 10 2038.5 180.607 38 2 -4 10 1829.89 181.073 34 -2 4 -10 1685.96 177.333 31 -2 -4 -10 1885.11 178.576 18 -2 4 -11 87.9198 55.3268 24 -2 -4 -11 102.381 53.698 18 2 -4 11 202.306 68.6895 15 -2 -4 -11 167.139 60.7903 22 2 -4 11 34.6167 38.6184 34 2 4 11 224.065 69.8571 19 -2 4 -11 219.885 74.7701 14 -2 4 -12 1370.33 171.391 14 2 -4 12 1237.1 162.219 15 2 -4 12 1085.62 141.058 34 -2 -4 -12 1425.68 163.581 22 -2 -4 -12 1369.59 157.761 18 2 4 12 985.739 141.652 19 2 4 13 483.357 97.5203 71 -2 4 -13 560.326 107.173 40 2 4 13 404.371 94.7354 49 -2 -4 -13 310.257 81.4299 22 2 4 13 279.575 81.9002 19 -2 -4 -13 485.241 94.3268 18 2 4 13 233.361 75.525 70 2 -4 13 367.27 90.1284 61 -2 4 -13 272.034 81.3575 14 2 4 14 365.158 93.4285 70 -2 4 -14 255.203 79.8101 55 2 4 14 259.437 79.0217 49 -2 -4 -14 209.882 65.7477 75 2 -4 14 129.462 65.232 61 -2 4 -14 401.838 90.8733 40 -2 -4 -14 206.868 70.5599 22 2 -4 14 126.898 54.8761 20 2 4 14 105.449 55.5559 19 -2 4 -14 182.405 66.5344 14 -2 -4 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19 4.52328 18.7776 61 -2 4 -19 17.7034 21.5908 59 2 5 -20 1282.98 99.5729 40 -2 -5 20 1317.63 105.073 65 -2 -5 19 155.645 47.4141 65 -2 5 19 173.787 48.0085 57 -2 5 19 230.426 57.2717 70 -2 5 18 408.757 80.3908 65 -2 -5 18 558.022 94.9205 65 -2 5 18 450.495 74.0589 69 -2 5 18 552.063 91.569 70 -2 5 18 613.149 89.877 57 -2 5 17 409.657 87.2866 65 -2 5 17 496.215 84.3095 69 -2 5 17 400.52 85.217 70 -2 -5 17 378.074 88.083 65 -2 5 17 668.848 102.883 57 -2 5 16 46.0891 44.0089 69 -2 -5 16 -33.3567 54.4738 65 -2 5 16 -16.9971 43.5497 65 -2 5 16 50.5858 43.2033 57 -2 5 15 1624.92 166.295 69 -2 -5 15 1251.84 159.878 20 -2 5 15 1489.07 167.031 57 -2 5 15 1573.61 170.612 35 -2 5 15 1270.92 158.698 65 2 -5 -15 1606.75 172.496 18 2 5 -15 1832.73 186.87 31 2 5 -15 1598.53 180.882 29 -2 5 14 480.511 92.7273 16 -2 -5 14 636.875 112.282 20 2 5 -14 632.208 117.751 29 -2 -5 14 707.408 121.639 42 -2 5 14 497.491 97.2028 69 -2 5 14 596.673 111.195 65 2 -5 -14 677.616 119.259 18 2 5 -14 542.914 110.404 14 -2 5 14 552.908 100.685 35 2 5 -14 456.057 98.6816 31 -2 5 14 581.474 106.549 57 -2 5 13 17.3588 31.4826 16 2 -5 -13 56.9838 45.5471 18 2 5 -13 20.9278 46.4593 29 -2 -5 13 37.4463 44.8968 20 -2 5 13 108.091 54.1442 35 2 5 -13 61.1586 52.2529 14 2 5 -12 444.865 101.828 29 -2 -5 12 492.644 97.2002 27 -2 5 12 460.69 89.1502 16 -2 -5 12 475.001 89.4888 25 -2 5 12 420.224 90.812 19 -2 -5 12 637.015 105.329 20 2 5 -12 543.374 102.475 14 -2 5 12 566.146 101.021 35 2 -5 -12 545.474 100.346 18 2 5 -11 19.1459 42.4836 29 -2 -5 11 16.4608 33.3435 27 2 5 -11 -17.609 35.6691 26 -2 -5 11 31.4787 34.925 25 2 5 -11 -18.1267 36.7178 14 -2 -5 11 16.4009 42.0227 20 -2 5 11 64.1043 48.1495 35 -2 5 11 16.4368 29.78 16 -2 5 11 -17.1112 46.5018 19 2 -5 -11 17.0976 34.6334 18 2 5 -10 17.872 36.2117 29 -2 5 10 15.6503 37.5193 16 2 5 -10 33.9326 43.4794 26 -2 -5 10 14.9369 38.281 25 -2 -5 10 15.2125 33.7667 27 -2 5 10 31.5553 35.0202 19 -2 -5 10 14.9584 35.8614 20 2 -5 -10 31.7634 38.0736 18 2 5 -10 16.6754 37.0116 14 -2 5 10 147.75 53.5438 35 -2 5 9 251.244 65.8857 16 2 5 -9 210.194 62.4564 26 -2 5 9 283.188 67.2013 35 -2 -5 9 154.938 51.4213 25 -2 -5 9 223.239 55.4479 27 2 -5 -9 190.389 56.6339 18 2 -5 -9 125.506 51.6224 15 -2 5 9 115.183 41.7183 19 2 5 -9 212.508 66.2412 14 -2 5 8 1851.72 152.597 35 -2 5 8 1754.07 160.257 16 -2 -5 8 1632.05 148.643 27 -2 -5 8 1747.2 154.845 25 2 5 -8 1604.41 159.535 26 2 -5 -8 1705.73 159.355 15 2 -5 -8 1684.9 153.93 18 -2 5 8 1719.35 153.186 19 2 5 -8 1515.42 157.801 29 -2 5 7 1049.68 118.339 16 -2 -5 7 1085.73 115.891 25 2 5 -7 1067.21 114.001 4 2 5 -7 1036.39 123.416 26 2 -5 -7 936.673 114.388 15 -2 5 7 831.841 109.633 21 -2 5 7 1216.37 122.867 19 -2 5 7 1235.09 117.846 35 2 -5 -7 930.293 110.787 18 2 5 -7 1134.62 126.098 29 -2 5 7 1020.05 105.405 3 -2 -5 7 1014.47 111.566 27 -2 -5 6 3989.68 237.425 25 2 -5 -6 3238.7 229.135 15 2 5 -6 3362.46 226.834 4 -2 5 6 3345.56 216.624 3 2 5 -6 3588.27 233.652 29 2 5 -6 3530.76 240.702 26 -2 5 6 3815.65 224.501 19 -2 5 6 3690.68 239.886 21 2 -5 -6 3575.71 228.457 18 -2 5 6 3616.59 218.36 35 -2 -5 6 3642.9 223.599 27 -2 5 6 3847.26 238.791 16 2 5 -5 1575.26 136.812 29 -2 -5 5 1314.52 124.025 17 -2 5 5 1565.71 137.749 16 -2 5 5 1344.88 116.644 19 2 5 -5 1272.04 130.386 4 -2 5 5 1640.12 125.586 35 2 -5 -5 1622.21 133.393 18 2 -5 -5 1473.37 135.502 15 -2 5 5 1233.19 119.733 3 2 5 -4 1016.52 115.096 26 -2 5 4 948.838 95.7497 24 -2 5 4 867.288 100.114 3 2 -5 -4 1153.31 115.662 15 2 5 -4 1222.84 121.223 4 2 5 -4 999.85 105.222 29 -2 5 4 1135.75 115.407 21 -2 -5 4 1105.71 109.632 17 -2 5 3 29565.3 1155.58 24 -2 -5 3 28969.7 1171.23 22 -2 5 3 31737.1 1191.87 21 2 -5 -3 30043.2 1182.28 33 2 5 -3 31191.9 1165.76 29 2 5 -3 31011.4 1193.24 4 2 5 -3 30715.7 1188.66 26 2 5 -3 29399.5 1163.72 38 2 -5 -3 31157.3 1170.14 18 2 -5 -3 31056.6 1185.05 15 -2 5 3 29820.6 1176.17 3 -2 -5 3 32252 1179.83 17 2 5 -2 14707.5 633.522 26 2 5 -2 14720.8 607.201 29 -2 5 2 14903.8 618.795 24 2 -5 -2 14930.3 635.05 15 2 5 -2 14653.1 642.811 4 -2 -5 2 15586.6 635.092 22 2 5 -2 13746.2 620.845 38 -2 5 2 15033.4 637.042 21 2 -5 -2 15324.4 623.199 18 -2 -5 2 15387.4 611.159 36 2 -5 -2 15075.5 634.632 33 -2 -5 2 14898.4 624.641 17 2 5 -1 23331.1 910.385 26 2 5 -1 22114.8 923.952 4 -2 5 1 23422.1 916.428 21 -2 5 1 23327.4 907.132 24 2 -5 -1 23679.8 920.629 15 -2 -5 1 22795.5 891.576 18 -2 -5 1 22665 911.164 22 2 5 -1 23027.2 915.987 38 2 -5 -1 23715.4 917.746 33 2 -5 -1 21987.6 897.411 18 -2 5 1 22647.9 913.544 3 2 5 0 5247.25 281.578 26 -2 5 0 5396.94 294.814 3 -2 5 0 5922.89 300.577 24 2 5 0 5205.99 300.535 4 -2 -5 0 5709.35 298.266 22 2 5 0 5253.72 298.525 38 -2 5 0 6176.36 301.645 21 -2 -5 0 5883.39 285.308 18 2 -5 0 5266.43 299.012 15 2 -5 0 5739.35 299.436 33 2 5 1 51614.4 1868.56 4 -2 5 -1 50127.7 1854.32 3 2 -5 1 51484.1 1866.97 15 -2 5 -1 49567.1 1860.13 24 2 5 1 49096.6 1836.25 37 -2 -5 -1 49636.6 1855.05 22 -2 5 -1 50347.5 1825.3 14 2 5 1 49185.2 1865.23 38 -2 5 -1 48262.4 1843.67 21 2 -5 1 50732.3 1855.84 33 2 -5 1 50037.8 1833.01 30 -2 -5 -1 50333.3 1834.22 18 -2 5 -2 9958.2 437.483 3 -2 -5 -2 9353.13 417.8 18 -2 5 -2 9003.13 412.251 14 2 -5 2 9868.03 448.366 15 -2 5 -2 9936.81 445.179 24 2 5 2 8386.45 432.532 4 2 5 2 8748.69 441.669 38 -2 5 -2 9347.81 420.865 21 -2 -5 -2 9837.63 441.289 22 2 5 2 8859.82 423.982 37 2 -5 2 8481.47 426.286 33 2 -5 2 8607.17 407.283 30 2 -5 3 1102.68 121.952 15 -2 5 -3 1128.64 109.496 3 2 5 3 802.61 101.497 4 2 5 3 886.366 101.514 37 -2 -5 -3 846.172 102.801 22 2 5 3 1114.82 120.983 38 -2 5 -3 897.133 97.9329 14 2 -5 3 903.608 106.024 33 -2 -5 -3 1029.6 103.117 18 2 5 4 5477.97 302.741 37 -2 5 -4 5024.14 285.425 3 2 -5 4 5690.65 297.938 27 -2 5 -4 4955.1 299.39 24 2 5 4 5365.83 293.632 4 -2 -5 -4 4745.74 275.61 18 -2 -5 -4 5231.25 297.128 22 -2 5 -4 5412.02 292.651 14 2 -5 4 5060.49 302.646 15 2 5 5 5667.45 329.512 37 2 -5 5 5366.74 329.5 15 -2 5 -5 5635.61 332.717 24 2 5 5 6159.9 316.73 4 -2 -5 -5 6416.12 334.381 22 -2 -5 -5 5648.2 309.826 18 2 5 5 5348.1 329.914 38 -2 5 -5 5678.24 320.215 14 2 -5 5 5773.84 322.691 27 2 -5 6 -13.423 42.1222 27 -2 -5 -6 -12.5118 27.7633 18 -2 5 -6 15.2421 43.6629 24 2 5 6 -15.1376 38.7857 37 2 5 6 -15.4279 27.9522 38 -2 -5 -6 14.2536 38.7362 22 -2 5 -6 28.0422 35.9252 14 2 5 7 279.895 78.8211 37 -2 5 -7 603.673 96.1807 14 -2 -5 -7 463.742 78.4887 18 -2 5 -7 522.2 92.2536 24 -2 -5 -7 353.889 75.1423 22 2 -5 7 283.819 79.8897 15 2 5 7 496.91 95.9798 19 2 5 7 388.022 81.4962 38 2 -5 7 511.661 87.0191 27 2 -5 7 392.169 80.244 34 -2 -5 -8 916.892 116.873 18 2 -5 8 720.848 106.494 34 2 -5 8 1112.58 138.385 15 2 5 8 728.521 114.431 37 2 5 8 936.415 127.621 19 -2 -5 -8 894.052 121.916 22 2 5 8 738.638 111.714 38 2 -5 8 949.886 122.917 27 -2 5 -8 937.686 127.507 24 -2 5 -8 1017.49 130.247 14 2 -5 9 1176.45 141.095 27 -2 -5 -9 1162.05 136.995 18 2 5 9 985.732 135.66 37 -2 5 -9 841.217 133.291 24 2 5 9 1066.4 134.357 38 -2 5 -9 1230.32 148.505 14 2 -5 9 979.853 125.295 34 -2 -5 -9 973.163 134.163 22 2 5 10 97.1329 58.3952 19 2 -5 10 90.5395 51.9054 27 -2 -5 -10 37.3556 41.4863 22 2 5 10 51.7496 41.3848 38 2 -5 10 49.5564 39.6345 34 -2 5 -10 78.3553 53.2671 14 -2 -5 -10 33.8005 37.5466 18 -2 5 -10 37.9445 51.5926 24 -2 5 -11 1964.68 206.328 14 -2 -5 -11 1934.99 189.967 18 -2 5 -11 1999.13 199.945 24 -2 -5 -11 2109.96 201.934 22 2 5 11 2420.89 222.207 19 2 5 12 2284.18 212.006 49 -2 5 -12 1862.96 187.916 53 -2 -5 -12 1995.64 198.439 22 -2 5 -12 2097.17 199.152 24 -2 5 -12 1718.33 193.903 40 2 5 12 1725.34 176.188 70 2 5 12 2211.45 208.666 19 -2 -5 -12 2032.46 190.611 18 2 -5 12 1901.76 197.563 61 2 5 12 1783.82 191.298 71 2 5 13 -18.5544 50.4243 71 2 -5 13 41.2907 45.8111 15 -2 5 -13 -57.8858 57.9717 40 -2 -5 -13 57.4726 42.5098 22 2 5 13 18.9849 29.7889 19 2 5 13 -33.2322 54.2713 70 2 5 13 37.1916 53.2702 49 2 -5 13 39.1051 50.0979 64 -2 -5 -13 17.4879 38.8051 18 2 -5 13 37.0631 60.5273 61 2 5 14 298.103 78.8971 57 -2 5 -14 391.034 90.1973 55 -2 5 -14 356.927 88.0234 40 2 5 14 339.713 88.0055 71 2 5 14 422.856 84.9321 70 2 -5 14 492.19 101.283 64 2 -5 14 377.333 87.4768 61 -2 5 -15 431.879 89.1566 55 2 5 15 562.497 93.215 70 2 5 15 397.466 80.4661 71 -2 5 -15 422.692 82.992 40 2 -5 15 422.736 86.8655 61 2 -5 15 615.552 104.962 64 2 5 15 432.849 86.6407 57 -2 5 -16 115.645 45.3591 40 -2 -5 -16 63.6241 47.7909 56 2 5 16 274.003 63.1256 70 2 -5 16 162.992 56.607 64 2 5 16 166.141 50.6714 71 -2 5 -16 111.929 52.4965 55 2 -5 16 162.199 55.5968 61 2 5 16 179.529 57.129 57 -2 5 -17 47.8119 40.6485 40 2 5 17 8.48391 27.7377 71 -2 5 -17 98.3855 48.5289 55 2 5 17 37.4364 33.9352 70 2 5 17 29.2691 38.5439 57 2 -5 17 26.4564 26.5247 65 -2 -5 -17 39.653 35.9419 56 2 -5 17 56.4972 38.1668 61 -2 5 -17 62.9491 37.0587 59 2 -5 18 132.651 34.194 65 -2 5 -18 165.513 42.1986 55 -2 5 -18 123.148 28.6028 59 2 5 18 205.869 40.9877 70 2 -5 18 152.054 37.6706 61 2 5 18 99.4092 31.5875 57 2 6 -20 175.922 32.229 40 2 6 -19 445.235 60.4282 53 -2 -6 19 351.855 59.0099 65 -2 6 19 500.806 66.7488 57 2 6 -18 56.3493 35.4228 53 -2 -6 18 41.6047 41.1196 65 -2 6 18 56.4186 40.9361 70 -2 6 18 54.2521 35.4967 57 -2 6 18 77.4217 34.0275 69 -2 -6 17 408.4 80.2662 65 -2 6 17 393.751 77.8494 57 -2 6 17 307.348 66.3581 69 -2 6 17 383.948 76.6137 70 -2 -6 16 234.76 68.8227 65 -2 6 16 330.372 83.9558 70 -2 6 16 418.184 78.2024 69 -2 6 16 459.605 88.1448 57 -2 6 15 82.0233 53.6649 69 -2 6 15 137.874 58.4921 70 -2 6 15 83.7833 50.4344 65 -2 6 15 52.6929 55.1995 57 -2 -6 14 404.852 90.8996 20 -2 -6 14 338.487 93.0712 42 2 -6 -14 419.073 89.7041 15 -2 6 14 428.509 89.731 65 -2 6 14 417.465 94.1 70 2 6 -14 482.982 102.499 14 -2 6 14 372.512 89.1635 69 2 -6 -14 381.235 85.7892 18 2 6 -14 540.442 99.4661 31 2 6 -14 379.429 96.5372 29 -2 6 13 830.6 120.359 46 -2 -6 13 1151.89 148.608 42 -2 6 13 811.406 125.547 69 -2 -6 13 845.496 126.262 20 -2 6 13 955.446 136.756 65 -2 6 13 850.854 129.205 70 2 -6 -13 750.634 125.827 15 2 -6 -13 888.392 131.125 18 2 6 -13 1049.31 143.826 14 -2 6 13 898.274 132.128 57 2 6 -13 1074.58 153.991 29 -2 -6 12 3365.73 271.079 27 2 -6 -12 4240.58 303.296 15 -2 -6 12 3708.86 278.715 20 2 6 -12 3999.18 306.441 29 -2 6 12 3668.88 279.945 19 2 6 -12 3655.82 284.28 14 2 -6 -12 4057.13 295.596 18 -2 6 12 4033.16 280.419 16 -2 -6 11 405.858 81.7112 20 -2 -6 11 442.51 88.4244 27 -2 6 11 258.071 70.4557 16 -2 -6 11 310.12 86.63 22 2 -6 -11 234.211 71.4669 15 -2 6 11 375.462 87.8242 19 2 -6 -11 294.49 77.0961 18 2 6 -11 187.237 66.4925 14 -2 6 10 16.8299 43.1343 16 -2 -6 10 47.9357 40.9538 25 -2 -6 10 55.1206 47.0883 22 2 -6 -10 18.6968 37.8869 15 -2 -6 10 78.6656 42.7696 20 -2 6 10 50.3077 48.0489 19 2 -6 -10 -17.5254 38.9019 18 -2 -6 10 67.0647 42.9711 27 2 6 -10 52.5882 42.0262 14 -2 6 9 1220.22 141.305 16 -2 -6 9 1103.55 133.59 27 2 -6 -9 1257.01 146.521 18 -2 -6 9 1249.14 138.247 25 2 -6 -9 1349.69 154.715 15 -2 -6 9 1174.94 145.077 22 2 6 -9 1292.98 144.228 14 -2 6 9 1440.65 148.404 19 2 6 -9 1482.89 162.53 29 2 6 -8 560.995 97.0878 29 -2 -6 8 264.908 67.9759 27 -2 6 8 453.562 82.47 16 -2 6 8 438.813 80.1587 19 -2 -6 8 444.386 82.7006 25 -2 6 8 300.077 66.4131 3 -2 -6 8 421.337 82.8114 22 2 -6 -8 319.08 78.7051 15 2 6 -8 511.62 95.4799 26 2 -6 -8 574.603 93.2057 18 2 6 -8 265.545 65.4593 14 -2 6 7 1967.08 174.079 16 2 6 -7 2049.76 186.027 26 -2 -6 7 1635.98 158.495 25 2 6 -7 2053.72 182.411 29 2 6 -7 2010.63 173.078 4 2 6 -7 1828.87 159.312 14 -2 -6 7 1840.15 162.691 27 2 -6 -7 2065.68 182.328 15 -2 6 7 1789.26 168.71 21 2 -6 -7 1545.89 156.365 18 -2 6 7 1946.09 160.27 19 -2 6 7 1646.82 152.602 3 -2 -6 7 1765.85 167.302 22 -2 -6 6 5034.02 293.604 27 2 -6 -6 4974.15 309.168 15 2 -6 -6 4776.36 296.732 18 2 6 -6 4577.82 307.396 26 -2 -6 6 5057.53 304.892 22 2 6 -6 5555.67 315.754 4 -2 6 6 5355.3 315.911 21 2 6 -6 4637.59 280.701 14 2 6 -6 5335.02 310.579 29 -2 6 6 4787.73 291.242 3 -2 6 6 5080.65 308.067 16 -2 6 5 760.384 98.3809 3 -2 6 5 671.628 100.686 16 2 6 -5 747.878 100.713 29 2 -6 -5 1021.09 122.091 15 2 -6 -5 910.159 109.802 18 2 6 -5 969.332 119.952 4 2 -6 -5 848.36 108.678 33 -2 6 4 6167.91 324.824 3 2 -6 -4 5430.15 309.222 18 2 -6 -4 5342.46 318.013 33 2 6 -4 5363.82 321.252 26 2 6 -4 5790.59 330.984 4 2 -6 -4 5449.31 321.67 15 -2 -6 4 5538.4 308.999 17 -2 6 4 5526.01 327.158 21 2 6 -4 5677.62 309.895 29 -2 6 3 15644.4 686.849 3 2 6 -3 16597.9 702.281 26 2 -6 -3 16160.3 697.617 15 2 6 -3 15323.6 701.417 4 2 -6 -3 16183.1 682.978 18 2 6 -3 15139.4 663.319 29 -2 6 3 15944.8 700 21 -2 6 3 15325.5 661.628 24 2 -6 -3 16548.5 695.968 33 -2 -6 3 15913.8 677.93 17 2 -6 -2 1110.04 120.13 33 -2 6 2 1029 109.075 24 2 -6 -2 1079.17 121.614 15 2 6 -2 1023.11 123.805 4 2 6 -2 916.869 105.515 38 -2 6 2 1300.55 129.257 21 2 -6 -2 1026.09 110.977 18 -2 -6 2 838.086 101.985 17 2 6 -1 127.382 51.4214 4 -2 6 1 141.432 50.9068 3 -2 6 1 90.687 39.947 24 2 -6 -1 132.931 46.7878 15 -2 6 1 128.918 45.3846 21 2 -6 -1 99.1197 40.6406 33 2 6 -1 125.671 45.6902 38 2 -6 -1 140.621 52.1388 18 -2 -6 1 67.4695 30.7882 17 -2 6 0 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57 -2 -6 -18 1141.91 79.8786 43 -2 6 -18 870.61 76.6624 55 2 7 -19 14.6228 20.7109 53 2 7 -19 -6.02562 21.8342 40 -2 7 19 5.41196 21.9253 57 2 7 -18 8.92031 28.0068 53 -2 7 18 45.304 26.2348 69 -2 -7 18 35.3828 30.0812 65 -2 7 18 8.66942 33.3312 57 2 7 -17 -12.216 39.9005 53 -2 -7 17 -9.66219 29.0313 65 -2 7 17 -9.8778 28.2981 69 -2 7 16 114.14 52.7924 69 -2 7 16 121.324 53.373 70 -2 -7 16 106.55 50.4551 65 2 7 -15 14.5798 41.7653 73 -2 7 15 61.3636 46.0904 70 -2 7 15 -15.0073 57.677 69 -2 7 15 -15.9167 49.9467 57 2 7 -14 -16.9023 34.2617 73 -2 7 14 16.8114 50.525 69 -2 7 14 87.3078 52.4779 57 -2 7 13 791.144 110.121 45 2 -7 -13 698.287 118.611 15 2 7 -13 608.749 110.825 29 2 7 -13 639.9 102.901 58 -2 -7 13 546.638 97.2078 20 -2 7 13 388.04 92.3002 70 -2 7 13 559.775 105.132 69 2 7 -13 356.546 87.0304 14 2 -7 -13 564.711 102.6 18 -2 7 13 461.422 99.2692 57 2 7 -12 381.273 92.2342 58 -2 -7 12 388.537 92.4598 27 2 7 -12 425.35 85.1353 31 -2 7 12 368.128 85.7329 46 -2 7 12 330.504 75.6573 45 -2 -7 12 300.557 91.423 42 2 -7 -12 204.223 74.8177 15 -2 7 12 415.144 90.2334 70 -2 -7 12 188.252 64.8654 20 2 -7 -12 365.285 84.2488 18 2 7 -12 319.958 80.7264 14 -2 7 12 302.337 84.5802 57 -2 7 11 1978.63 190.467 16 2 7 -11 2099.52 212.68 29 -2 -7 11 1877.32 189.128 27 -2 7 11 1856.64 192.444 46 -2 -7 11 1994.48 204.789 22 2 -7 -11 1803.5 190.666 18 -2 -7 11 1996.71 204.774 42 -2 -7 11 2120.64 191.489 20 -2 -7 11 2031.39 197.963 56 -2 7 11 1876.55 191.563 70 2 7 -11 1856.06 187.403 14 -2 7 11 1877.9 195.693 69 -2 7 11 2004.89 190.415 45 2 -7 -11 2144.26 208.104 15 -2 7 11 2000.62 200.015 57 2 7 -11 2094.74 202.895 58 -2 -7 10 8227.68 455.205 27 2 -7 -10 9004.66 486.12 15 -2 7 10 7655.06 444.23 16 -2 -7 10 7816.78 459.431 22 2 7 -10 8544.21 458.583 14 -2 7 10 7319.44 434.212 19 2 -7 -10 8125.91 458.748 18 2 7 -10 7950.47 472.281 29 -2 7 9 4925.49 332.587 16 -2 -7 9 5153.99 339.236 27 -2 -7 9 5353.99 335.799 25 2 -7 -9 5464.83 349.852 18 2 -7 -9 5629.81 361.801 15 -2 -7 9 6153.7 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95.7388 15 -2 -8 -6 156.194 66.9337 22 2 8 6 253.189 81.7085 38 -2 8 -6 244.852 81.1912 24 2 8 6 267.737 71.1903 21 2 -8 7 1013.57 143.792 27 -2 8 -7 1476.01 177.495 53 2 8 7 1301.43 153.152 71 -2 8 -7 1415.7 174.708 24 2 -8 7 1246.41 160.608 15 -2 -8 -7 1616.42 176.312 22 -2 -8 -7 1466.04 164.986 43 -2 8 -7 944.785 136.557 40 -2 8 -7 1387.42 171.099 73 2 8 7 1350.79 165.306 68 2 8 7 1535.34 168.565 19 2 -8 7 1336.7 163.326 62 -2 -8 -7 1420.69 158.244 18 2 -8 8 19.8201 53.8675 64 2 -8 8 38.2274 38.7227 27 2 8 8 39.921 44.2961 48 2 -8 8 62.0272 52.9794 15 -2 -8 -8 36.8222 47.1777 43 -2 8 -8 35.7919 48.639 40 2 8 8 20.7765 46.1065 38 -2 8 -8 39.5871 56.7048 73 2 8 8 126.818 56.8553 71 2 8 8 -19.5853 50.1859 19 2 -8 8 91.4736 62.0127 62 -2 -8 -8 -17.4869 44.81 18 2 -8 9 37.5641 45.0221 27 -2 8 -9 40.6785 52.119 53 2 8 9 36.039 43.1949 71 -2 8 -9 -20.6112 52.8157 24 2 -8 9 20.2207 44.8752 15 -2 -8 -9 53.8835 48.818 43 -2 8 -9 -17.9051 45.883 40 2 8 9 40.0591 44.4511 38 -2 8 -9 19.0485 45.6607 73 2 8 9 19.0229 54.499 68 2 -8 9 38.7058 63.2145 64 2 8 9 96.848 49.6349 19 -2 -8 -9 68.4883 43.8773 18 2 8 9 50.3541 48.0882 57 -2 8 -10 185.188 64.3669 55 -2 8 -10 77.6289 58.6417 53 -2 -8 -10 68.5649 54.1516 43 -2 8 -10 226.897 72.7226 40 -2 8 -10 355.718 85.4836 73 2 8 10 244.451 74.4518 71 2 8 10 250.75 72.828 68 2 -8 10 314.052 80.4995 64 2 8 10 147.427 57.8096 57 -2 -8 -11 2664.73 216.851 56 -2 8 -11 3294 237.088 55 -2 8 -11 3499.28 263.953 53 2 8 11 3366.83 245.612 46 -2 8 -11 3019.31 239.165 73 -2 -8 -11 3469.32 248.693 43 -2 8 -11 3465.7 251.648 40 2 -8 11 3527.95 260.209 64 2 8 11 3712 259.369 71 2 8 11 3404.66 253.812 68 2 -8 11 2939.91 233.115 61 2 8 11 3084.97 237.431 57 -2 -8 -12 276.312 65.8539 56 -2 8 -12 267.059 67.8884 55 2 8 12 240.805 65.9851 68 2 8 12 213.215 62.1442 46 2 -8 12 260.524 69.9367 64 -2 8 -12 159.49 63.5541 53 -2 -8 -12 228.595 67.7916 43 -2 8 -12 526.666 92.8453 40 2 8 12 283.291 73.2358 71 -2 8 -12 353.799 75.4666 73 2 8 12 198.157 63.393 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57.8358 53 2 9 -14 120.527 50.3188 73 -2 9 14 149.316 44.6223 45 -2 -9 14 219.835 58.8152 42 -2 9 14 161.5 53.5523 57 2 9 -14 120.545 46.7082 58 2 9 -13 51.1856 40.4351 58 2 9 -13 89.1364 52.3369 53 -2 9 13 158.025 56.1535 57 -2 -9 13 193.026 61.8202 42 2 9 -13 186.976 62.6641 73 -2 9 13 287.76 63.6017 45 -2 9 12 1181.42 130.08 45 2 9 -12 1208.28 143.385 53 2 9 -12 1189.58 143.124 73 -2 -9 12 1428.06 153.73 42 -2 9 12 1388.33 143.606 57 -2 9 12 1266.11 143.266 69 2 9 -12 933.446 125.279 58 2 9 -11 505.561 100.323 58 -2 9 11 683.63 109.143 69 -2 9 11 356.742 78.7369 45 -2 -9 11 405.123 94.5155 42 2 9 -11 604.145 106.855 73 2 9 -11 555.634 94.6731 47 -2 9 11 415.051 86.3235 57 -2 9 10 54.5872 57.3383 46 -2 9 10 174.901 63.0011 57 -2 9 10 253.046 70.2253 45 -2 -9 10 147.592 64.9381 42 -2 9 10 227.761 72.9179 69 2 9 -10 106.025 60.123 47 2 9 -10 163.732 70.1145 58 -2 -9 9 -17.6713 39.212 27 -2 9 9 53.9644 58.7524 69 2 -9 -9 -38.3689 49.1546 33 2 9 -9 18.9696 48.6041 47 -2 9 9 18.8834 41.9015 46 -2 9 9 89.2142 53.608 45 -2 -9 9 -18.9638 48.5894 42 2 -9 -9 18.7609 41.6296 18 2 9 -9 19.1083 54.7381 58 2 9 -9 37.3631 44.7748 29 -2 9 8 1955.3 189.981 16 -2 -9 8 1990.44 192.923 27 2 9 -8 2258.12 213.368 58 2 -9 -8 1719.88 189.456 18 -2 9 8 2342.88 213.494 46 -2 -9 8 2012.34 203.377 22 -2 -9 8 2229.42 210.788 42 2 9 -8 1647.77 190.786 47 2 -9 -8 2512.89 221.073 33 -2 9 8 2084.58 202.209 69 2 9 -8 2108.33 198.756 29 -2 9 7 1954.66 194.804 16 -2 -9 7 1816.61 185.127 27 -2 9 7 1901.47 196.072 46 -2 9 7 2180.07 204.056 45 -2 -9 7 1899.11 195.439 22 -2 -9 7 2119.69 209.398 42 -2 9 7 1653.79 179.95 69 2 9 -7 2097.43 209.789 47 -2 9 7 1670.99 174.221 3 2 -9 -7 2230.62 209.728 33 2 -9 -7 2250.91 210.54 18 -2 -9 6 304.595 79.9986 27 -2 9 6 187.235 64.0686 16 -2 -9 6 105.139 53.3763 25 2 9 -6 226.389 79.5846 47 2 -9 -6 250.19 72.4169 18 -2 9 6 265.388 79.181 46 -2 9 6 308.733 82.7247 3 -2 -9 6 351.265 87.048 22 2 9 -6 368.47 86.5111 67 2 -9 -6 265.873 75.501 33 2 9 -6 260.923 79.738 4 -2 9 6 351.841 86.2673 69 2 9 -6 375.766 95.2065 58 -2 9 5 6015.21 375.759 16 2 9 -5 5546.36 378.416 67 -2 9 5 5826.88 363.407 46 -2 -9 5 5452.64 353.857 27 2 9 -5 5526.26 374.187 4 -2 -9 5 5431.08 362.307 22 -2 -9 5 4927.88 344.315 25 -2 9 5 5731.73 381.373 21 2 -9 -5 5400.31 355.671 33 2 -9 -5 5596.98 368.379 18 -2 9 5 5966.55 372.674 3 2 9 -5 6301.11 383.025 58 -2 9 4 482.256 99.2812 3 2 -9 -4 510.202 106.43 15 -2 -9 4 693.879 114.868 22 -2 9 4 770.302 125.238 21 -2 9 4 464.229 106.975 16 2 9 -4 464.303 106.563 4 2 -9 -4 727.723 114.701 33 -2 9 3 1296.65 165.676 21 2 9 -3 1280.23 166.887 4 -2 9 3 1332.88 167.11 3 2 -9 -3 1503.98 172.823 15 -2 -9 3 1207.68 156.164 22 2 -9 -3 1314.88 153.548 33 2 -9 -2 1054.64 149.577 15 -2 -9 2 993.677 138.155 22 -2 9 2 890.195 137.514 21 2 9 -2 793.069 134.437 4 2 -9 -2 1108.29 138.988 33 2 -9 -1 -20.2639 44.9772 15 -2 -9 1 19.0895 48.923 22 -2 9 1 39.7048 47.5929 3 -2 9 1 19.7689 43.8792 21 2 9 -1 64.2569 51.3465 4 2 -9 -1 67.4504 40.4296 33 2 9 0 106.839 67.3844 21 2 -9 0 284.233 76.1224 15 -2 9 0 198.293 67.5413 3 -2 -9 0 267.88 77.8032 22 -2 9 0 134.307 58.0306 21 2 9 0 234.267 72.4931 4 2 9 1 21.2972 54.5961 21 -2 9 -1 16.7055 33.8852 24 2 -9 1 81.5605 61.2863 15 -2 9 -1 59.1482 47.287 3 -2 9 -1 36.9286 44.2891 21 2 9 1 75.7763 51.5131 38 2 9 1 84.2228 63.2851 4 -2 -9 -1 153.858 65.2107 22 2 -9 2 6479.06 418.35 15 -2 9 -2 6024.78 388.062 24 2 9 2 6708.16 424.997 21 -2 -9 -2 6598.06 409.442 22 2 9 2 7375.41 426.529 38 -2 9 -2 7083.26 417.399 3 2 9 2 7191.76 431.742 4 2 -9 3 10081.4 566.231 15 -2 9 -3 9817.39 547.697 73 2 -9 3 9818.9 550.229 27 2 9 3 9301.71 551.69 4 2 9 3 11300.4 584.024 21 2 9 3 11451.5 577.878 48 -2 9 -3 11316.4 564.623 24 -2 -9 -3 10658.8 566.415 22 2 9 3 10826.3 553.41 68 -2 -9 -3 10817.7 557.755 43 -2 9 -3 10517.4 550.873 53 -2 -9 -3 10744.9 554.194 41 2 9 3 11345.6 580.432 38 -2 9 -3 11784.4 586.105 47 2 -9 3 10531.6 555.119 62 -2 9 -3 11225 567.235 3 -2 -9 -3 10568.3 548.71 18 -2 9 -4 4333.51 312.75 53 2 -9 4 4695.24 320.723 27 2 -9 4 4007.7 312.393 15 -2 9 -4 3839.76 306.303 24 -2 9 -4 4338.24 315.694 47 -2 -9 -4 4332.77 307.295 43 -2 -9 -4 4302.98 300.35 18 -2 -9 -4 4612.02 319.877 22 2 9 4 4633.37 326.315 48 2 -9 4 4994.92 324.937 62 2 9 4 4594.68 322.996 21 2 9 4 4747.33 332.876 38 -2 9 -4 5100.54 333.849 73 2 9 4 3740.48 295.667 68 -2 9 -4 4964.73 321.331 3 2 9 4 4003.95 305.424 4 2 -9 5 4031.02 307.13 27 -2 9 -5 4561.01 321.341 47 2 9 5 4600 321.669 68 -2 9 -5 3786.73 302.411 53 2 -9 5 5064.65 344.177 15 2 9 5 4806.11 335.877 48 -2 9 -5 4846.27 331.987 24 2 9 5 4709.3 322.997 21 2 9 5 4542.92 317.4 63 -2 -9 -5 4256.68 314.655 22 -2 -9 -5 4723.81 319.483 43 2 9 5 4544.2 330.864 38 -2 9 -5 4673.78 327.995 73 -2 -9 -5 4481.37 309.454 18 2 -9 5 4740.9 320.702 62 2 -9 6 341.212 83.0949 27 -2 9 -6 256.051 76.5044 53 2 9 6 325.449 77.6169 21 -2 9 -6 422.216 94.7189 47 2 -9 6 447.62 98.1552 15 -2 -9 -6 359.369 86.8394 43 -2 -9 -6 368.422 88.5226 22 2 9 6 395.685 91.1498 38 2 9 6 299.421 87.4248 48 2 -9 6 429.491 97.4941 64 2 9 6 210.195 74.2706 68 -2 9 -6 279.35 77.483 24 2 9 6 230.106 68.9238 63 -2 -9 -6 243.12 72.935 18 2 -9 6 464.631 96.4093 62 2 9 7 2331 214.045 68 2 9 7 2200.17 202.878 19 2 -9 7 2381.51 214.113 27 -2 9 -7 2345.07 217.948 53 2 -9 7 2123.6 209.695 15 -2 9 -7 1988.09 204.534 24 -2 9 -7 2218.28 200.978 47 2 -9 7 1951.73 189.376 62 -2 -9 -7 1749.78 192.283 22 -2 -9 -7 2082.61 196.042 43 2 9 7 1998.75 206.675 38 -2 9 -7 1948.61 200.82 73 2 -9 7 2440.05 222.803 64 -2 -9 -7 2545.49 210.388 18 -2 9 -8 2319.06 210.842 53 -2 -9 -8 1979.47 185.596 43 -2 9 -8 1687.36 167.719 40 -2 9 -8 2475.3 214.821 73 2 9 8 1666.08 183.006 68 2 9 8 1820.36 177.671 71 2 -9 8 1866.71 194.119 64 2 9 9 183.619 59.067 71 -2 -9 -9 267.775 70.1202 43 -2 9 -9 147.903 55.5173 40 -2 9 -9 51.6762 49.6524 73 2 9 9 221.163 78.7752 68 2 -9 9 206.448 69.9148 64 -2 9 -10 77.6517 50.8045 73 -2 9 -10 66.6177 62.2692 53 2 9 10 46.0149 41.7809 46 -2 -9 -10 100.891 48.9353 43 -2 9 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37.7574 49 5 -1 14 28.7027 32.4948 49 -5 1 -14 86.6209 34.2072 75 -5 -1 -14 108.268 40.6802 75 5 -1 14 58.6764 35.2184 61 -5 -1 -14 34.5231 39.9196 59 -5 1 -14 66.3197 41.1839 59 5 1 15 254.721 46.4055 49 5 -1 15 292.765 49.1674 49 -5 -1 -15 314.099 45.3745 75 5 1 15 248.111 43.7814 70 -5 1 -15 269.639 44.4839 59 -5 -2 20 68.1146 31.5054 52 -5 -2 19 63.3468 35.8518 52 -5 2 18 1164.89 125.009 52 -5 2 18 1398.37 145.761 44 -5 2 18 1367.21 127.1 65 -5 2 17 112.781 52.9341 52 -5 2 17 242.266 75.3236 44 -5 2 17 140.033 55.5597 69 -5 2 17 177.937 55.4831 65 -5 2 16 1947.12 180.319 52 -5 -2 16 1898.74 186.414 52 -5 -2 16 2063.49 196.218 44 -5 2 16 1950.94 186.949 44 -5 2 16 1699.77 172.394 69 -5 2 16 1760.29 165.981 65 -5 2 15 16.7573 45.5396 52 -5 -2 15 18.5029 41.0564 52 -5 -2 15 17.861 51.1645 44 -5 2 15 18.5703 47.5804 44 -5 2 15 -17.5354 47.6543 69 -5 2 15 -15.4245 41.9178 65 5 2 -14 101.126 51.8583 29 -5 2 14 119.505 57.0899 16 -5 2 14 138.048 64.4811 52 5 2 -14 19.3348 35.0855 26 -5 -2 14 57.5374 46.0093 52 -5 -2 14 -18.5377 50.4169 44 -5 2 14 77.9297 55.8444 44 -5 2 14 80.1926 52.4216 65 5 2 -13 1243.76 161.079 29 -5 2 13 981.651 147.488 16 5 2 -13 1414.19 173.552 26 -5 2 13 1549.93 164.017 52 -5 -2 13 1430.82 169.425 52 -5 -2 13 1497.44 173.809 44 -5 2 13 1391.85 171.023 44 -5 2 13 1418.5 166.029 69 -5 2 13 1749.52 167.172 65 -5 -2 12 1349.95 169.008 56 5 2 -12 1931.04 201.473 26 -5 -2 12 1830.36 192.341 52 -5 -2 12 1751.39 187.314 25 -5 -2 12 2052.27 197.351 44 -5 -2 12 1963.58 192.641 72 -5 2 12 1663.54 181.424 69 5 2 -12 2024.29 196.465 32 5 -2 -12 1766.02 187.52 32 -5 2 12 1932.08 194.965 16 -5 2 11 7248.74 424.45 16 5 2 -11 6604.43 423.637 26 -5 -2 11 7789.84 438.723 25 5 -2 -11 7289.46 425.623 23 5 2 -11 6707.79 420.911 32 -5 2 10 18.219 33.0093 16 5 2 -10 -40.0935 48.0468 26 -5 -2 10 36.6705 40.6853 25 5 -2 -10 18.8461 34.1454 23 5 2 -10 39.2966 43.5987 32 -5 2 9 13758.1 666.637 16 5 2 -9 14784.8 702.687 26 -5 -2 9 16130.4 693.297 25 5 -2 -9 14489.9 692.59 23 5 2 -9 13799.3 667.682 4 5 2 -9 13984.8 693.315 32 5 -2 -9 13361.4 662.441 30 -5 2 9 13813.2 655.339 5 -5 2 8 777.978 111.875 16 -5 2 8 741.44 108.108 5 -5 -2 8 618.894 107.439 25 5 2 -8 787.807 116.131 4 5 2 -8 753.43 111.317 23 5 -2 -8 886.144 124.429 23 5 2 -8 574.612 111.358 32 5 -2 -8 896.876 120.283 30 -5 -2 8 719.529 108.531 5 -5 2 7 182.076 56.743 16 5 2 -7 53.8826 43.1418 26 -5 -2 7 122 47.94 25 5 2 -7 88.1061 47.9728 4 5 2 -7 16.9135 40.6373 23 5 -2 -7 108.821 52.0336 23 5 2 -7 112.427 56.3686 32 5 -2 -7 99.3615 49.8361 30 -5 -2 7 48.3089 41.3577 5 -5 -2 6 80.5993 46.2866 5 -5 2 6 127.481 44.5625 16 5 2 -6 102.99 46.7562 26 -5 -2 6 85.4546 40.923 25 5 2 -6 102.156 48.8764 23 5 2 -6 70.5154 53.06 4 5 -2 -6 142.362 60.3997 23 5 2 -6 54.86 46.9617 32 5 -2 -6 82.6243 45.0207 30 -5 -2 6 87.9176 46.0912 17 -5 -2 5 321.826 77.5339 5 -5 -2 5 292.732 63.1261 25 5 -2 -5 331.845 74.6268 23 5 2 -5 87.9468 48.447 4 -5 -2 5 205.644 64.5678 36 -5 2 5 198.29 62.2938 14 5 -2 -5 247.996 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17.4205 41.7547 36 5 -2 9 42.1 42.6414 34 -5 2 -9 19.1648 42.5279 14 -5 -2 -9 17.0336 40.8274 59 -5 2 -9 31.2913 44.8214 59 5 2 9 -18.5589 44.4829 34 -5 -2 -10 611.354 97.1545 56 -5 2 -10 631.842 111.565 55 5 -2 10 699.126 120.241 50 5 2 10 679.851 111.903 49 -5 -2 -10 628.779 106.584 75 5 -2 10 716.043 111.409 61 -5 -2 -10 719.196 116.091 59 -5 2 -10 472.258 97.9635 59 -5 -2 -11 910.821 110.206 56 -5 2 -11 992.089 123.776 55 5 -2 11 896.176 124.821 50 5 2 11 1146.18 134.443 49 -5 -2 -11 732.32 113.037 75 5 -2 11 1062.26 125.692 61 -5 2 -11 1045.85 121.864 59 -5 -2 -11 636.682 107.87 59 -5 -2 -12 606.209 86.3291 56 -5 2 -12 752.596 100.812 55 5 2 12 628.824 96.7674 49 -5 -2 -12 663.225 94.3464 75 -5 2 -12 573.179 78.3757 75 5 -2 12 712.718 95.0858 61 -5 -2 -12 640.062 96.3353 59 -5 2 -12 616.226 90.8665 59 -5 -2 -13 736.93 81.6921 56 -5 2 -13 647.783 87.6403 55 5 2 13 588.972 86.0232 49 5 -2 13 820.135 100.704 49 5 2 13 667.905 85.1679 71 5 -2 13 689.808 86.821 61 -5 -2 -13 670.003 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46.8219 39 8 -1 0 36.3839 41.1162 39 8 1 0 48.6021 39.695 74 8 -1 0 39.3622 44.4805 74 -8 1 0 12.1908 42.779 66 -8 -1 0 38.2657 46.6754 60 -8 -1 -1 143.331 49.3405 55 -8 1 -1 235.277 58.5258 55 8 1 1 137.083 51.6942 48 8 -1 1 106.087 41.9264 48 8 1 1 93.8428 48.9631 39 8 -1 1 127.616 52.13 39 8 1 1 139.747 54.0341 74 8 -1 1 185.827 57.4509 74 -8 1 -1 214.287 58.0198 66 -8 -1 -1 170.358 53.5059 60 -8 -1 -2 198.085 51.2804 55 -8 1 -2 244.387 59.3612 55 8 1 2 119.897 40.7456 48 8 1 2 152.866 55.7072 39 8 -1 2 164.841 48.1723 39 8 1 2 206.512 58.5505 74 8 -1 2 136.642 53.9255 74 -8 1 -2 253.396 56.1645 66 -8 -1 -2 139.491 49.6605 60 -8 -1 -3 7.51007 30.4344 55 -8 1 -3 17.9059 37.1735 55 -8 1 -3 61.2054 39.6104 66 -8 -1 -3 21.8142 39.5291 60 -8 -1 -4 -5.64687 26.5845 55 -8 1 -4 44.929 30.3397 55 -8 1 -4 35.2677 27.8558 66 -8 -1 -4 6.14363 32.4547 60 -8 1 -5 -5.70999 21.3302 55 -8 1 -5 14.6423 19.7766 66 -8 -1 -5 33.3281 25.5188 60 -8 2 14 41.4125 23.4899 44 -8 2 13 13.7384 25.6606 44 -8 2 12 115.192 41.0179 44 -8 2 11 186.842 53.9107 44 8 2 -10 627.281 79.8376 48 -8 2 10 788.656 93.0972 44 8 2 -9 1032.42 110.903 48 -8 2 9 1159.97 117.911 44 8 2 -8 47.7631 43.2836 48 -8 2 8 68.7312 45.2476 44 8 2 -8 -21.6271 40.4062 39 8 -2 -8 30.9753 33.7447 74 -8 -2 8 49.6609 31.8327 72 -8 2 7 501.969 80.3164 55 8 2 -7 413.307 77.4962 48 -8 2 7 494.728 82.1349 44 8 2 -7 602.3 92.045 39 8 -2 -7 495.944 81.8327 74 -8 -2 7 373.221 63.3605 72 -8 2 6 2394 181.103 55 8 2 -6 2297.93 188.03 48 -8 2 6 2362.32 181.59 44 8 2 -6 2150.13 182.612 39 8 -2 -6 2265.86 179.721 74 -8 -2 6 2243.15 161.212 72 -8 -2 5 5109.98 303.1 55 -8 2 5 5290.43 303.703 55 8 2 -5 5347.48 320.321 48 -8 2 5 5275.48 300.284 44 8 2 -5 5154.21 311.365 39 8 -2 -5 5358.64 310.978 74 -8 -2 5 4991.55 277.045 72 -8 -2 4 13186.5 587.782 55 -8 2 4 13696.1 592.23 55 8 2 -4 13377.8 607.496 48 -8 2 4 12675.1 578.324 44 8 2 -4 13130.7 603.476 39 8 -2 -4 12842.1 598.13 74 -8 -2 4 12253.3 552.558 72 -8 2 4 12737.1 590.65 66 -8 -2 3 2047.59 169.289 55 -8 2 3 2226.79 180.342 55 -8 2 3 2191.57 172.341 44 8 2 -3 2483.8 196.868 39 8 -2 -3 2267.44 186.473 74 -8 -2 3 2102.16 157.518 72 -8 2 3 2073.36 177.977 66 -8 -2 2 195.457 59.2345 55 -8 2 2 135.611 57.2729 55 8 2 -2 203.302 65.2549 48 -8 2 2 140.653 53.1338 44 8 2 -2 206.032 63.7393 39 8 -2 -2 244.383 66.5133 74 -8 -2 2 159.601 48.497 72 -8 -2 1 645.168 87.4803 55 8 2 -1 526.155 87.4341 48 8 -2 -1 457.582 81.1223 48 8 -2 -1 714.866 97.4818 39 8 2 -1 474.04 74.7377 74 8 -2 -1 595.841 94.7586 74 -8 -2 1 478.079 72.2584 72 -8 -2 0 78.473 41.7563 55 8 2 0 82.6009 42.8338 48 8 -2 0 91.7045 35.3373 48 8 2 0 99.6572 50.5306 39 8 -2 0 64.8531 40.4519 39 8 2 0 117.469 47.4605 74 8 -2 0 -12.6547 41.4112 74 -8 -2 0 93.2805 36.9294 72 -8 2 0 105.337 48.6533 66 -8 -2 -1 51.8184 36.7151 55 -8 2 -1 10.6671 39.8599 55 8 2 1 52.102 42.232 48 8 2 1 -11.3701 41.2168 39 8 -2 1 117.808 45.7225 39 8 -2 1 59.0323 44.1135 74 -8 -2 -1 15.5163 32.9857 72 -8 2 -1 54.4208 47.3004 66 -8 -2 -1 45.4101 44.3208 60 -8 -2 -2 222.724 46.9046 55 -8 2 -2 213.932 56.7551 55 8 2 2 103.488 43.951 48 -8 2 -2 147.606 53.1123 66 -8 -2 -2 273.248 59.3969 60 -8 2 -3 25.722 33.8551 55 8 2 3 -18.5812 25.0918 48 8 -2 3 9.25591 32.4735 74 -8 2 -3 8.55841 29.0083 66 -8 -2 -3 51.1857 36.2807 60 -8 2 -4 -7.19314 31.2499 55 8 -2 4 -7.49562 27.1604 74 8 2 4 -5.51471 18.6923 68 -8 2 -4 -20.9893 29.0439 66 -8 -2 -4 43.1079 37.4223 60 -8 2 -5 220.3 41.4755 55 -8 2 -5 316.02 44.4639 66 -8 -2 -5 233.187 43.7867 60 -8 3 13 468.979 57.2 44 8 3 -13 283.058 45.2162 67 -8 3 12 978.075 92.1206 44 -8 3 11 34.4256 38.212 44 -8 3 10 105.422 43.5606 44 8 3 -9 70.5255 41.5097 48 -8 3 9 10.3596 32.5265 44 8 -3 -9 35.3854 32.0728 74 -8 -3 9 23.9595 33.1713 72 8 3 -8 556.944 80.5185 48 -8 3 8 306.331 66.4965 44 8 -3 -8 449.527 74.221 74 -8 -3 8 375.921 64.902 72 -8 3 7 139.889 44.1962 55 8 3 -7 194.389 56.0162 48 -8 3 7 124.742 53.6243 44 8 3 -7 91.9598 52.6101 39 8 -3 -7 112.725 50.2879 74 -8 -3 7 251.113 56.1199 72 -8 3 6 964.805 103.889 55 8 3 -6 844.207 107.595 48 -8 3 6 971.546 111.486 44 8 3 -6 802.064 100.093 39 8 -3 -6 867.998 107.828 74 -8 -3 6 1093.86 107.815 72 -8 3 5 3111.91 210.233 55 8 3 -5 3286.79 227.862 48 -8 3 5 3369.01 225.141 44 8 3 -5 3372.21 226.256 39 8 -3 -5 3649.82 237.344 74 -8 -3 5 3592.83 215.445 72 -8 3 4 108.491 49.182 55 8 3 -4 155.511 56.3372 48 -8 3 4 68.9715 52.1061 44 8 3 -4 74.9345 53.1043 39 8 -3 -4 90.0835 49.5017 74 -8 -3 4 -9.95731 37.247 72 -8 3 4 45.1841 50.1716 66 -8 -3 3 459.074 73.9801 55 -8 3 3 350.313 68.5701 55 8 3 -3 451.469 86.1076 48 -8 3 3 459.421 76.4526 44 8 3 -3 303.512 74.5577 39 8 -3 -3 296.948 72.3817 74 -8 -3 3 345.089 66.3784 72 -8 3 3 480.374 80.6943 66 -8 -3 2 2417.14 169.89 55 -8 3 2 2399.56 176.991 55 8 3 -2 2278.76 186.803 39 8 -3 -2 2579.07 194.169 74 -8 -3 2 2508.46 173.794 72 -8 3 2 2612.97 188.455 66 -8 -3 1 309.846 57.4677 55 -8 3 1 359.75 68.3685 55 8 3 -1 262.26 68.8862 48 8 -3 -1 255.609 56.043 48 8 3 -1 278.612 69.9807 39 8 -3 -1 216.971 58.3908 39 8 -3 -1 183.833 58.3832 74 -8 -3 1 193.246 52.1663 72 -8 3 1 365.364 70.7789 66 -8 3 0 10.1064 33.0104 55 8 3 0 -32.9306 39.7754 48 8 -3 0 8.75117 34.5561 39 -8 -3 0 -17.2591 36.6672 72 -8 3 -1 -28.3072 36.2651 55 8 3 1 29.0976 34.0298 48 8 -3 1 -21.1179 39.4385 74 -8 -3 -1 -7.87863 30.281 72 -8 3 -2 496.61 71.4029 55 8 3 2 417.296 64.369 48 8 -3 2 630.499 80.5838 74 -8 3 -2 461.67 72.1212 66 8 3 3 23.0365 21.5253 48 8 -3 3 7.65766 30.2476 74 -8 -3 -3 -5.76014 25.5752 72 8 3 3 64.4299 29.7288 68 -8 3 -3 46.0853 36.8262 66 8 -3 4 -5.57335 24.7356 74 8 3 4 19.7245 18.9544 68 -8 3 -4 18.5763 25.7066 66 8 4 -12 61.9262 29.3736 67 -8 4 11 868.968 86.6011 44 8 4 -11 1015.85 93.2351 67 -8 4 10 90.1839 39.3494 44 8 -4 -10 26.0281 27.0856 74 8 4 -10 96.9649 40.7656 67 -8 4 9 18.1112 36.6899 44 8 -4 -9 24.416 27.5911 74 -8 -4 9 7.57831 31.464 72 8 4 -8 143.833 39.0638 48 -8 4 8 87.4517 43.1968 44 8 -4 -8 84.4015 44.2156 74 -8 -4 8 16.6247 37.7355 72 8 4 -7 9.32924 33.8062 48 -8 4 7 -10.1879 34.5334 44 8 -4 -7 51.5746 37.3776 74 -8 -4 7 8.85093 36.7439 72 -8 4 6 42.4197 32.7429 55 8 4 -6 133.648 48.4494 48 -8 4 6 41.9291 41.4585 44 8 4 -6 125.257 43.7099 39 8 -4 -6 54.9232 42.2839 74 -8 -4 6 55.2665 40.0872 72 -8 4 5 219.056 47.755 55 8 4 -5 163.555 51.0608 48 -8 4 5 275.571 65.6583 44 8 4 -5 247.027 56.5267 39 8 -4 -5 273.647 64.2223 74 -8 -4 5 357.421 65.4314 72 8 4 -5 239.469 62.4155 67 -8 4 4 24.9172 33.6504 55 8 4 -4 22.4505 43.1435 48 -8 4 4 -10.5392 31.667 44 8 4 -4 -10.4689 37.936 39 8 -4 -4 23.1506 39.236 74 -8 -4 4 9.43668 35.2483 72 8 4 -4 48.3817 41.1158 67 -8 4 3 539.152 72.8189 55 8 4 -3 528.741 85.6305 48 -8 4 3 608.206 84.196 44 8 4 -3 623.047 88.0933 39 8 -4 -3 552.063 85.566 74 -8 -4 3 419.075 74.1524 72 8 4 -3 542.541 72.9929 67 -8 4 3 731.362 84.8317 66 -8 4 2 145.985 40.6284 55 8 4 -2 76.9363 41.2552 48 -8 -4 2 63.2152 42.7053 72 -8 4 2 121.049 44.0207 66 -8 4 1 92.4985 37.3909 55 8 -4 -1 131.156 41.4126 39 -8 -4 1 17.1718 33.081 72 -8 4 1 54.7881 37.9783 66 -8 4 0 48.1426 32.5652 55 8 4 0 76.6237 39.8088 48 8 -4 0 68.1753 41.4281 74 -8 -4 0 63.7979 36.1739 72 -8 4 0 34.8967 37.9523 66 -8 4 -1 289.57 52.7921 55 8 4 1 310.164 56.4498 48 8 -4 1 283.102 56.1493 74 -8 -4 -1 136.591 42.5619 72 -8 4 -1 290.999 53.9855 66 -8 4 -2 19.7948 29.3409 55 8 4 2 94.9045 32.5471 48 8 -4 2 84.7657 35.0973 74 -8 -4 -2 24.8056 28.1498 72 8 4 2 51.7701 31.4786 68 -8 4 -2 72.0081 35.1765 66 -8 4 -3 209.492 39.0971 55 8 -4 3 120.715 31.0868 74 -8 -4 -3 119.038 34.6849 72 8 4 3 260.569 42.0184 68 -8 5 10 11.9575 22.9862 44 8 -5 -10 -25.1813 22.8191 74 8 5 -10 -26.2843 29.1677 67 8 -5 -9 59.8337 30.2179 74 8 5 -9 91.8967 35.4631 67 8 -5 -8 7.81193 30.8578 74 -8 -5 8 42.4679 31.4224 72 8 5 -7 659.617 69.7298 48 8 -5 -7 753.103 87.518 74 -8 -5 7 784.663 83.4846 72 8 5 -7 637.35 83.1016 67 8 5 -6 259.504 48.4508 48 -8 5 6 130.083 47.0415 44 8 -5 -6 184.534 52.034 74 -8 -5 6 207.3 47.9167 72 8 5 -6 297.595 57.6367 67 8 5 -5 379.386 63.2382 48 -8 5 5 336.516 60.7368 44 8 -5 -5 333.86 65.8087 74 -8 -5 5 350.615 60.7926 72 8 5 -5 369.932 65.7715 67 8 -5 -4 955.486 91.9818 51 8 5 -4 1527.44 121.456 48 -8 5 4 1470.5 119.319 44 8 -5 -4 1459.04 125.641 74 -8 -5 4 1601.29 120.523 72 8 5 -4 963.872 101.139 67 8 -5 -3 69.171 31.3592 51 8 5 -3 63.1013 39.1858 48 -8 5 3 43.4031 35.1928 44 -8 -5 3 8.01942 32.5163 72 8 5 -3 25.3884 27.0023 67 -8 5 2 10.0129 21.272 55 8 5 -2 17.6831 35.8186 48 -8 5 2 8.32446 30.1634 44 8 -5 -2 -11.617 29.7649 39 8 -5 -2 -8.93563 32.378 74 -8 -5 2 7.70826 33.4876 72 -8 5 2 12.5919 23.5154 66 -8 5 1 560.311 64.2897 55 8 5 -1 878.761 93.0136 48 -8 5 1 801.37 85.548 44 8 -5 -1 875.701 89.2883 74 -8 -5 1 845.598 85.726 72 -8 5 1 727.987 75.0962 66 -8 5 0 145.962 30.9371 55 8 -5 0 191.951 44.4814 74 -8 -5 0 131.413 38.0318 72 8 5 0 189.924 45.2049 68 -8 5 0 149.55 38.3166 66 8 5 1 372.402 54.2739 48 8 -5 1 263.872 43.4592 74 -8 -5 -1 314.52 49.9229 72 8 5 1 259.165 48.4055 68 -8 5 -1 291.965 44.711 66 -8 -5 -2 59.9867 26.8451 72 -8 6 8 593.821 61.4329 44 8 -6 -8 834.297 72.6463 74 -8 6 7 358.224 50.8733 44 8 -6 -7 365.809 53.1687 74 8 6 -7 324.713 51.0716 67 -8 6 6 144.265 37.2029 44 8 -6 -6 174.073 42.2577 74 8 6 -6 90.741 33.6341 67 8 6 -5 968.802 78.2099 48 -8 6 5 1188.52 92.0515 44 8 6 -5 939.607 84.5725 67 8 6 -4 91.8801 29.493 48 8 -6 -4 34.1083 24.0146 74 8 6 -3 193.436 39.145 48 8 -6 -3 141.883 37.394 74 8 6 -2 35.9247 27.1199 48 8 -6 -2 -5.74451 21.4566 74 8 6 -2 -19.0732 19.3183 68 8 6 -1 122.7 33.2946 48 -8 6 1 96.8018 30.6027 44 8 6 -1 79.7011 25.3423 68 9 0 -7 11.0695 19.4183 48 9 0 -7 -5.01922 24.0592 39 9 0 -6 797.551 78.6463 48 9 0 -6 1093.31 86.7314 39 9 0 -5 5.98689 24.2546 39 9 0 -4 39.0606 25.3119 48 9 0 -4 41.5195 28.9676 39 9 1 -7 20.324 20.5974 48 9 -1 -7 15.9254 20.4154 48 9 -1 -7 30.452 22.9999 39 9 1 -6 39.2093 25.4981 48 9 1 -6 96.4267 29.9032 39 9 -1 -6 106.41 34.1282 39 9 1 -5 143.648 35.423 48 9 -1 -5 146.831 37.6685 48 9 1 -5 193.629 39.2752 39 9 -1 -5 224.495 42.7807 39 9 1 -4 276.634 45.3012 48 9 1 -4 364.991 52.014 39 9 1 -3 42.7274 26.9781 39 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 5 1 -4 0.0501 3 -1 -10 0.0831 -1 -3 -9 0.0742 -3 0 5 0.0393 1 4 -5 0.0530 -1 3 5 0.0650 -2 -4 9 0.0253 1 -4 -5 0.0612 0 -5 -1 0.0471 -2 0 -5 0.0764 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C5 C1 C3 118.61(7) . . ? C13 C1 C3 118.28(8) . . ? C13 C1 C5 123.10(8) . . ? C6 C2 C3 118.67(7) . . ? C16 C2 C3 118.63(8) . . ? C16 C2 C6 122.70(8) . . ? C2 C3 C1 121.29(7) . . ? C8 C3 C1 119.44(7) . . ? C8 C3 C2 119.23(7) . . ? C9 C5 C1 118.83(7) . . ? C19 C5 C1 123.73(7) . . ? C19 C5 C9 117.37(8) . . ? C9 C6 C2 119.07(8) . . ? C18 C6 C2 123.48(7) . . ? C18 C6 C9 117.33(8) . . ? C15 C7 C8 118.63(8) . . ? C17 C7 C8 119.93(9) . . ? C17 C7 C15 121.44(9) . . ? C7 C8 C3 120.52(8) . . ? C11 C8 C3 120.55(8) . . ? C11 C8 C7 118.91(8) . . ? C6 C9 C5 123.46(8) . . ? H9 C9 C5 118.6(5) . . ? H9 C9 C6 117.9(5) . . ? C20 C10 C11 120.84(10) . . ? H10 C10 C11 119.0(6) . . ? H10 C10 C20 120.2(6) . . ? C10 C11 C8 119.74(9) . . ? C14 C11 C8 118.54(8) . . ? C14 C11 C10 121.71(9) . . ? C15 C13 C1 121.77(9) . . ? H13 C13 C1 117.9(5) . . ? H13 C13 C15 120.4(5) . . ? C16 C14 C11 121.63(9) . . ? H14 C14 C11 117.2(6) . . ? H14 C14 C16 121.2(6) . . ? C13 C15 C7 121.30(9) . . ? H15 C15 C7 118.7(6) . . ? H15 C15 C13 120.0(6) . . ? C14 C16 C2 121.32(9) . . ? H16 C16 C2 117.6(6) . . ? H16 C16 C14 121.0(6) . . ? C20 C17 C7 120.51(10) . . ? H17 C17 C7 118.9(6) . . ? H17 C17 C20 120.6(6) . . ? O12 C18 C6 122.13(9) . . ? C21 C18 C6 118.25(8) . . ? C21 C18 O12 119.59(9) . . ? C5 C19 O4 122.54(8) . . ? C22 C19 O4 118.90(8) . . ? C22 C19 C5 118.56(8) . . ? C17 C20 C10 120.07(10) . . ? H20 C20 C10 120.0(6) . . ? H20 C20 C17 119.9(6) . . ? H21a C21 C18 111.6(6) . . ? H21b C21 C18 108.1(6) . . ? H21b C21 H21a 111.2(10) . . ? H21c C21 C18 110.2(7) . . ? H21c C21 H21a 107.1(10) . . ? H21c C21 H21b 108.6(9) . . ? H22a C22 C19 109.8(6) . . ? H22b C22 C19 110.9(6) . . ? H22b C22 H22a 109.2(9) . . ? H22c C22 C19 111.8(6) . . ? H22c C22 H22a 108.5(9) . . ? H22c C22 H22b 106.6(9) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C3 1.4294(11) . ? C1 C5 1.4210(11) . ? C1 C13 1.4346(11) . ? C2 C3 1.4295(11) . ? C2 C6 1.4150(11) . ? C2 C16 1.4372(11) . ? C3 C8 1.4330(11) . ? O4 C19 1.2209(10) . ? C5 C9 1.3953(11) . ? C5 C19 1.4962(11) . ? C6 C9 1.3940(11) . ? C6 C18 1.4967(11) . ? C7 C8 1.4180(12) . ? C7 C15 1.4269(13) . ? C7 C17 1.4034(12) . ? C8 C11 1.4197(12) . ? C9 H9 1.080(9) . ? C10 C11 1.4004(13) . ? C10 C20 1.3895(15) . ? C10 H10 1.102(10) . ? C11 C14 1.4270(13) . ? O12 C18 1.2177(10) . ? C13 C15 1.3592(13) . ? C13 H13 1.088(9) . ? C14 C16 1.3572(13) . ? C14 H14 1.096(10) . ? C15 H15 1.092(10) . ? C16 H16 1.096(10) . ? C17 C20 1.3913(15) . ? C17 H17 1.096(11) . ? C18 C21 1.5079(13) . ? C19 C22 1.5063(13) . ? C20 H20 1.082(9) . ? C21 H21a 1.052(12) . ? C21 H21b 1.082(11) . ? C21 H21c 1.086(12) . ? C22 H22a 1.089(10) . ? C22 H22b 1.073(12) . ? C22 H22c 1.075(12) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 C3 C2 C6 0.12(9) . . . . ? C1 C3 C2 C16 -179.19(8) . . . . ? C1 C3 C8 C7 -0.34(9) . . . . ? C1 C3 C8 C11 -178.50(7) . . . . ? C1 C5 C9 C6 -2.23(9) . . . . ? C1 C5 C19 O4 17.54(9) . . . . ? C1 C5 C19 C22 -163.47(9) . . . . ? C1 C13 C15 C7 -0.75(10) . . . . ? C2 C3 C8 C7 177.59(7) . . . . ? C2 C3 C8 C11 -0.57(9) . . . . ? C2 C6 C9 C5 3.05(9) . . . . ? C2 C6 C18 O12 -23.89(9) . . . . ? C2 C6 C18 C21 158.12(9) . . . . ? C2 C16 C14 C11 0.85(10) . . . . ? C3 C8 C7 C15 1.92(9) . . . . ? C3 C8 C7 C17 -177.01(8) . . . . ? C3 C8 C11 C10 177.32(8) . . . . ? C3 C8 C11 C14 -1.68(9) . . . . ? O4 C19 C5 C9 -159.43(8) . . . . ? C5 C9 C6 C18 -173.00(8) . . . . ? C7 C8 C11 C10 -0.87(9) . . . . ? C7 C8 C11 C14 -179.87(8) . . . . ? C7 C17 C20 C10 -0.47(10) . . . . ? C8 C11 C10 C20 -0.10(9) . . . . ? C8 C11 C14 C16 1.57(9) . . . . ? C10 C11 C14 C16 -177.41(9) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 4.9993 1.0061 -3.9967 -0.4951 0.6910 -0.6802 2.9988 -0.9970 -9.9956 -0.0904 0.0561 -0.9878 -1.0007 -3.0023 -8.9975 0.4632 -0.5735 -0.6336 -2.9993 -0.0034 4.9972 0.2194 -0.2939 0.6080 0.9987 4.0020 -4.9978 -0.6058 -0.2313 -0.3151 -0.9998 2.9997 4.9981 -0.3222 -0.0248 0.5262 -1.9982 -4.0031 8.9961 0.6806 0.2614 0.6809 1.0000 -3.9999 -4.9981 0.4547 0.0614 -0.5564 0.0007 -5.0012 -0.9999 0.6621 0.1281 -0.2208 -2.0006 -0.0026 -4.9991 0.1403 -0.6532 -0.1773