#------------------------------------------------------------------------------ #$Date: 2024-11-21 01:10:52 +0200 (Thu, 21 Nov 2024) $ #$Revision: 296021 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/32/1573233.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573233 loop_ _publ_author_name 'Sumida, Akifumi' 'Saeki, Akinori' 'Matsuo, Kyohei' 'Naka, Kensuke' 'Imoto, Hiroaki' _publ_section_title ; Dithienoarsinines: Stable and Planer \p-Extended Arsabenzenes ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC06590E _journal_year 2024 _chemical_formula_moiety 'C14 H5 As O5 S2 W' _chemical_formula_sum 'C14 H5 As O5 S2 W' _chemical_formula_weight 576.07 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-04-10 _audit_creation_method ; Olex2 1.5-ac5-024 (compiled 2022.04.12 svn.rca3783a0 for Rigaku Oxford Diffraction, GUI svn.r6498) ; _audit_update_record ; 2024-09-20 deposited with the CCDC. 2024-11-18 downloaded from the CCDC. ; _cell_angle_alpha 92.355(6) _cell_angle_beta 106.909(6) _cell_angle_gamma 100.480(6) _cell_formula_units_Z 2 _cell_length_a 7.3120(5) _cell_length_b 10.1653(8) _cell_length_c 11.2954(8) _cell_measurement_reflns_used 2534 _cell_measurement_temperature 256.00 _cell_measurement_theta_max 32.7370 _cell_measurement_theta_min 3.1370 _cell_volume 785.92(10) _computing_cell_refinement 'CrysAlisPro 1.171.42.91a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.42.91a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.42.91a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5-ac5-024 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-ac5-024 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 256.00 _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -73.00 -48.00 0.10 0.50 -- 30.00 54.00 -90.00 250 2 \w 5.00 32.00 0.10 0.50 -- 30.00 54.00 -90.00 270 3 \w -70.00 31.00 0.10 0.50 -- 30.00 54.00 150.00 1010 4 \w -74.00 110.00 0.10 0.50 -- 30.00 54.00 30.00 1840 ; _diffrn_measurement_device 'two-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Mini (JP)' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0455688000 _diffrn_orient_matrix_UB_12 0.0016118000 _diffrn_orient_matrix_UB_13 0.0648637000 _diffrn_orient_matrix_UB_21 0.0494456000 _diffrn_orient_matrix_UB_22 0.0671154000 _diffrn_orient_matrix_UB_23 0.0011660000 _diffrn_orient_matrix_UB_31 -0.0787330000 _diffrn_orient_matrix_UB_32 0.0240645000 _diffrn_orient_matrix_UB_33 0.0119345000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0937 _diffrn_reflns_av_unetI/netI 0.1174 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 4555 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.372 _diffrn_reflns_theta_min 2.925 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 9.724 _exptl_absorpt_correction_T_max 0.264 _exptl_absorpt_correction_T_min 0.024 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.91a (Rigaku Oxford Diffraction, 2023) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour pink _exptl_crystal_colour_primary pink _exptl_crystal_density_diffrn 2.434 _exptl_crystal_description plate _exptl_crystal_F_000 536 _exptl_crystal_size_max 0.95 _exptl_crystal_size_mid 0.47 _exptl_crystal_size_min 0.15 _refine_diff_density_max 6.699 _refine_diff_density_min -5.056 _refine_diff_density_rms 0.533 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.105 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 208 _refine_ls_number_reflns 3210 _refine_ls_number_restraints 18 _refine_ls_restrained_S_all 1.104 _refine_ls_R_factor_all 0.1186 _refine_ls_R_factor_gt 0.0985 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1871P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2590 _refine_ls_wR_factor_ref 0.2985 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2385 _reflns_number_total 3210 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 3a-W(CO)5_a.res in P-1 3a-W(CO)5.res created by SHELXL-2018/3 at 09:33:26 on 10-Apr-2024 REM Old TITL 3a-W(CO)5 in P-1 REM SHELXT solution in P-1: R1 0.170, Rweak 0.007, Alpha 0.069 REM 0.000 for 0 systematic absences, Orientation As input REM Formula found by SHELXT: C16 O3 S2 As W CELL 0.71073 7.312 10.1653 11.2954 92.355 106.909 100.48 ZERR 2 0.0005 0.0008 0.0008 0.006 0.006 0.006 LATT 1 SFAC C H As O S W UNIT 28 10 2 10 4 2 SIMU 0.002 0.004 2 C009 O007 SIMU 0.002 0.004 2 O008 C00B SIMU 0.002 0.004 2 C00D O006 L.S. 20 0 0 PLAN 5 SIZE 0.15 0.47 0.95 TEMP -17.15 BOND list 4 fmap 2 53 acta REM REM REM WGHT 0.187100 FVAR 0.35437 W001 6 0.700102 0.201329 0.779070 11.00000 0.03535 0.03840 = 0.02951 0.01111 0.02078 0.01491 S003 5 0.539730 0.243520 0.367024 11.00000 0.03560 0.05255 = 0.03238 0.00842 0.01947 0.00882 S004 5 0.927317 0.644007 0.825585 11.00000 0.03289 0.06041 = 0.03853 0.01324 0.01722 0.01768 O005 4 0.237017 0.096221 0.690110 11.00000 0.02615 0.04100 = 0.06295 -0.00537 0.02052 0.00043 O006 4 1.163652 0.290300 0.891970 11.00000 0.03777 0.05091 = 0.04668 0.00560 0.01999 0.02064 O007 4 0.755701 0.022672 0.559309 11.00000 0.05049 0.03183 = 0.04010 0.01082 0.02421 0.01759 O008 4 0.629214 0.401001 0.974494 11.00000 0.04149 0.06025 = 0.01988 0.00374 0.01162 0.02037 C009 1 0.727061 0.083158 0.633740 11.00000 0.04842 0.02336 = 0.04013 0.01957 0.02102 0.01933 O00A 4 0.723406 -0.029802 0.950531 11.00000 0.06924 0.03904 = 0.05145 0.00516 0.01348 -0.01658 C00B 1 0.662660 0.329556 0.915649 11.00000 0.04302 0.05541 = 0.02085 0.00643 0.01239 0.01750 C00C 1 0.400707 0.135070 0.718726 11.00000 0.04563 0.02239 = 0.04577 0.00908 0.02862 0.01531 C00D 1 0.995081 0.263191 0.850912 11.00000 0.03773 0.04887 = 0.04703 0.00547 0.02043 0.02371 C00E 1 0.662494 0.379174 0.466971 11.00000 0.03486 0.05112 = 0.04319 0.01705 0.02753 0.02111 C00F 1 0.883026 0.657109 0.589780 11.00000 0.05668 0.04201 = 0.05576 0.02564 0.03090 0.03462 C00G 1 0.826593 0.618456 0.463763 11.00000 0.04755 0.03232 = 0.05181 0.02366 0.02627 0.03096 AFIX 43 H00G 2 0.859687 0.682976 0.413428 11.00000 -1.20000 AFIX 0 C00H 1 0.990585 0.786039 0.654527 11.00000 0.04107 0.05365 = 0.05277 0.01846 0.03052 0.01921 AFIX 43 H00H 2 1.035758 0.857447 0.614664 11.00000 -1.20000 AFIX 0 C00I 1 0.710328 0.052367 0.887543 11.00000 0.04703 0.06831 = 0.03553 -0.01123 -0.00378 0.04235 C00J 1 0.724549 0.491781 0.404443 11.00000 0.04949 0.04699 = 0.04753 0.02161 0.03918 0.02632 C00K 1 0.568217 0.325055 0.241254 11.00000 0.03712 0.07014 = 0.03434 0.01798 0.02484 0.01308 AFIX 43 H00K 2 0.525033 0.283582 0.160334 11.00000 -1.20000 AFIX 0 C00L 1 0.655295 0.449286 0.270166 11.00000 0.04542 0.05393 = 0.03247 0.02405 0.02627 0.02645 AFIX 43 H00L 2 0.672906 0.507285 0.211044 11.00000 -1.20000 AFIX 0 C00M 1 0.841689 0.566459 0.677015 11.00000 0.03462 0.04199 = 0.05208 0.01448 0.02746 0.02343 C00N 1 1.018355 0.792935 0.773772 11.00000 0.02498 0.04530 = 0.05115 0.01688 0.01454 0.00700 AFIX 43 H00N 2 1.081466 0.870831 0.826684 11.00000 -1.20000 AFIX 0 AS 3 0.706180 0.392838 0.637963 11.00000 0.04750 0.04146 = 0.03012 0.01031 0.02362 0.01807 HKLF 4 REM 3a-W(CO)5_a.res in P-1 REM wR2 = 0.2985, GooF = S = 1.105, Restrained GooF = 1.104 for all data REM R1 = 0.0985 for 2385 Fo > 4sig(Fo) and 0.1186 for all 3210 data REM 208 parameters refined using 18 restraints END WGHT 0.1872 0.0000 REM Highest difference peak 6.699, deepest hole -5.056, 1-sigma level 0.533 Q1 1 0.5794 0.3633 0.6005 11.00000 0.05 6.70 Q2 1 0.6656 0.1139 0.7475 11.00000 0.05 4.05 Q3 1 0.6766 0.1002 0.7067 11.00000 0.05 4.05 Q4 1 0.7311 0.3012 0.8384 11.00000 0.05 3.95 Q5 1 0.8795 0.3858 0.6556 11.00000 0.05 2.65 REM The information below was added by Olex2. REM REM R1 = 0.0985 for 2385 Fo > 4sig(Fo) and 0.1186 for all 4555 data REM 208 parameters refined using n/a restraints REM Highest difference peak 6.70, deepest hole -5.06 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1186 REM R1_gt = 0.0985 REM wR_ref = 0.2985 REM GOOF = 1.105 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 4555 REM Reflections_gt = 2385 REM Parameters = 208 REM Hole = -5.06 REM Peak = 6.70 REM Flack = n/a ; _cod_data_source_file d4sc06590e2.cif _cod_data_source_block 3a-W(CO)5 _cod_database_code 1573233 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula C14H5O5AsS2W _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.323 _shelx_estimated_absorpt_t_min 0.039 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2. Uiso/Uaniso restraints and constraints C009 \\sim O007: within 2A with sigma of 0.002 and sigma for terminal atoms of 0.004 within 2A O008 \\sim C00B: within 2A with sigma of 0.002 and sigma for terminal atoms of 0.004 within 2A C00D \\sim O006: within 2A with sigma of 0.002 and sigma for terminal atoms of 0.004 within 2A 3.a Aromatic/amide H refined with riding coordinates: C00G(H00G), C00H(H00H), C00K(H00K), C00L(H00L), C00N(H00N) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.306 _oxdiff_exptl_absorpt_empirical_full_min 0.343 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group W001 W 0.70010(10) 0.20133(7) 0.77907(7) 0.0308(4) Uani 1 1 d . . . . . S003 S 0.5397(8) 0.2435(6) 0.3670(5) 0.0381(11) Uani 1 1 d . . . . . S004 S 0.9273(7) 0.6440(6) 0.8256(5) 0.0412(12) Uani 1 1 d . . . . . O005 O 0.237(2) 0.0962(15) 0.6901(16) 0.043(4) Uani 1 1 d . . . . . O006 O 1.164(2) 0.2903(16) 0.8920(15) 0.042(3) Uani 1 1 d . U . . . O007 O 0.756(2) 0.0227(14) 0.5593(14) 0.037(3) Uani 1 1 d . U . . . O008 O 0.629(2) 0.4010(16) 0.9745(12) 0.039(3) Uani 1 1 d . U . . . C009 C 0.727(3) 0.0832(18) 0.634(2) 0.034(3) Uani 1 1 d . U . . . O00A O 0.723(3) -0.0298(17) 0.9505(18) 0.058(5) Uani 1 1 d . . . . . C00B C 0.663(3) 0.330(2) 0.9156(19) 0.038(3) Uani 1 1 d . U . . . C00C C 0.401(3) 0.1351(18) 0.719(2) 0.033(4) Uani 1 1 d . . . . . C00D C 0.995(3) 0.263(2) 0.851(2) 0.041(3) Uani 1 1 d . U . . . C00E C 0.662(3) 0.379(2) 0.467(2) 0.038(5) Uani 1 1 d . . . . . C00F C 0.883(3) 0.657(2) 0.590(2) 0.045(5) Uani 1 1 d . . . . . C00G C 0.827(3) 0.618(2) 0.464(2) 0.038(5) Uani 1 1 d . . . . . H00G H 0.859687 0.682976 0.413428 0.045 Uiso 1 1 calc R U . . . C00H C 0.991(3) 0.786(2) 0.655(2) 0.044(5) Uani 1 1 d . . . . . H00H H 1.035758 0.857447 0.614664 0.053 Uiso 1 1 calc R U . . . C00I C 0.710(3) 0.052(3) 0.888(2) 0.050(7) Uani 1 1 d . . . . . C00J C 0.725(3) 0.492(2) 0.404(2) 0.040(5) Uani 1 1 d . . . . . C00K C 0.568(3) 0.325(2) 0.241(2) 0.043(5) Uani 1 1 d . . . . . H00K H 0.525033 0.283582 0.160334 0.052 Uiso 1 1 calc R U . . . C00L C 0.655(3) 0.449(2) 0.270(2) 0.038(5) Uani 1 1 d . . . . . H00L H 0.672906 0.507285 0.211044 0.046 Uiso 1 1 calc R U . . . C00M C 0.842(3) 0.566(2) 0.677(2) 0.037(5) Uani 1 1 d . . . . . C00N C 1.018(3) 0.793(2) 0.774(2) 0.039(5) Uani 1 1 d . . . . . H00N H 1.081466 0.870831 0.826684 0.047 Uiso 1 1 calc R U . . . As As 0.7062(3) 0.3928(2) 0.6380(2) 0.0357(6) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W001 0.0353(5) 0.0384(5) 0.0295(5) 0.0111(4) 0.0208(4) 0.0149(4) S003 0.036(3) 0.053(3) 0.032(3) 0.008(2) 0.019(2) 0.009(2) S004 0.033(3) 0.060(3) 0.039(3) 0.013(3) 0.017(2) 0.018(2) O005 0.026(7) 0.041(8) 0.063(11) -0.005(7) 0.021(7) 0.000(6) O006 0.038(6) 0.051(7) 0.047(7) 0.006(6) 0.020(6) 0.021(6) O007 0.050(7) 0.032(6) 0.040(7) 0.011(5) 0.024(6) 0.018(5) O008 0.041(7) 0.060(8) 0.020(6) 0.004(5) 0.012(5) 0.020(6) C009 0.048(7) 0.023(6) 0.040(7) 0.020(5) 0.021(6) 0.019(5) O00A 0.069(12) 0.039(8) 0.051(11) 0.005(8) 0.013(10) -0.017(8) C00B 0.043(7) 0.055(8) 0.021(6) 0.006(6) 0.012(5) 0.018(6) C00C 0.046(12) 0.022(8) 0.046(12) 0.009(8) 0.029(10) 0.015(8) C00D 0.038(6) 0.049(7) 0.047(8) 0.005(6) 0.020(6) 0.024(6) C00E 0.035(10) 0.051(11) 0.043(12) 0.017(10) 0.028(10) 0.021(9) C00F 0.057(13) 0.042(11) 0.056(14) 0.026(10) 0.031(12) 0.035(11) C00G 0.048(11) 0.032(10) 0.052(13) 0.024(9) 0.026(10) 0.031(9) C00H 0.041(11) 0.054(13) 0.053(14) 0.018(11) 0.031(11) 0.019(10) C00I 0.047(13) 0.068(16) 0.036(12) -0.011(11) -0.004(10) 0.042(12) C00J 0.049(12) 0.047(11) 0.048(13) 0.022(10) 0.039(11) 0.026(10) C00K 0.037(11) 0.070(15) 0.034(12) 0.018(11) 0.025(10) 0.013(11) C00L 0.045(11) 0.054(12) 0.032(11) 0.024(10) 0.026(10) 0.026(10) C00M 0.035(10) 0.042(10) 0.052(13) 0.014(9) 0.027(10) 0.023(9) C00N 0.025(9) 0.045(11) 0.051(14) 0.017(10) 0.015(9) 0.007(8) As 0.0475(13) 0.0415(11) 0.0301(11) 0.0103(9) 0.0236(10) 0.0181(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 -2 3410.47 61.81 0 0 -3 5.22 2.74 0 0 4 10.41 2.29 0 0 -4 17.6 5.84 0 0 -5 1849.35 71.57 0 0 5 1707.9 34.03 0 0 -6 91.77 18.49 0 0 6 60.34 6.54 0 0 7 2005.25 42.2 0 0 -7 1903.31 92.22 0 0 -8 181.56 31.42 0 0 -9 494.97 57.07 0 0 -10 6 9.75 0 0 -11 30.37 15.98 0 0 -12 139.29 35.25 0 0 -13 48.29 23.68 0 1 -13 169.93 44.09 0 1 -12 33.77 16.83 0 1 -11 437.49 64.19 0 1 -10 281.39 46.63 0 -1 9 98.03 11.74 0 1 -9 88.33 23.8 0 1 -8 514.05 51.82 0 1 -7 142.49 24.35 0 1 -6 1325.2 66.22 0 1 -5 543.21 37.43 0 -1 5 462.16 29.35 0 1 -4 1194.01 47.93 0 -1 4 1058.97 39.84 0 -1 3 165.46 13.39 0 1 -3 211.68 17.42 0 1 -2 897.27 25.97 0 -1 2 879.86 25.25 0 -1 -1 3919.5 71.18 0 -1 -2 90.09 12.54 0 -1 -3 1521.63 60.56 0 -1 -4 47.66 11.52 0 -1 -5 332.18 33.6 0 -1 -6 179.88 27.92 0 -1 -7 202.07 31.68 0 -1 -8 1230.76 84.02 0 -1 -9 115.8 28.72 0 -1 -10 507.21 61.39 0 -1 -11 0.33 4.73 0 -1 -12 125.87 33.71 0 -1 -13 37.17 17.57 0 2 -13 56.77 24.48 0 2 -12 311.91 57.53 0 2 -11 60.4 22.94 0 2 -10 340.99 51.02 0 2 -9 46.41 16.8 0 2 -8 7.34 6.28 0 -2 7 762.34 47.55 0 2 -7 764.52 55.56 0 -2 6 110.66 16.55 0 2 -6 122.96 20.01 0 2 -5 2468.6 78.63 0 -2 5 2317.21 66.05 0 2 -4 105.09 14.65 0 -2 4 85.68 10.9 0 -2 3 4711.47 75.19 0 2 -3 4731.52 74.91 0 -2 2 594.31 23.82 0 2 -2 612.91 21.52 0 -2 1 1780.67 43.13 0 2 -1 1765.24 34.11 0 -2 0 1620.6 85.67 0 -2 0 1529.98 76.16 0 2 0 1696.81 62.19 0 2 1 507.65 30.26 0 -2 -1 500.51 33.31 0 -2 -2 5236.85 109.45 0 -2 -3 313.58 31.36 0 -2 -4 1944.34 85.17 0 -2 -5 11.92 7.05 0 -2 -6 135.28 26.5 0 -2 -7 843.42 68.25 0 -2 -8 181.78 33.57 0 -2 -9 783.72 72.01 0 -2 -10 53.26 18.48 0 -2 -11 128.87 31.77 0 -2 -12 8.15 9.84 0 -2 -13 51.32 25.25 0 3 -13 -12.52 20.69 0 3 -12 34.89 21.57 0 3 -11 351.16 59.09 0 3 -10 92.52 26.64 0 3 -9 1044.26 81.44 0 -3 9 1243.24 71.85 0 3 -8 101.35 22.85 0 -3 8 115.15 21.45 0 -3 7 342.41 31.07 0 3 -7 329.34 36.97 0 -3 6 201.16 21.61 0 3 -6 202.49 25.44 0 3 -5 114.73 17.88 0 -3 5 103.55 14.49 0 -3 4 3112.59 71.72 0 3 -4 3210.5 75.17 0 -3 3 543.31 28.19 0 3 -3 575.69 27.48 0 -3 2 7119.9 99.41 0 3 -2 7428.61 86.78 0 -3 1 9.03 3.85 0 3 -1 4.37 5.43 0 -3 1 13.03 5.07 0 -3 0 28.25 11.33 0 3 0 39.99 3.21 0 3 1 77.15 14.94 0 -3 -1 126.36 28.76 0 -3 -2 3.2 3.14 0 3 2 -7.3 8.45 0 -3 -3 1588.53 72.61 0 -3 -4 39.45 12.14 0 -3 -5 1566.28 83.04 0 -3 -6 96.61 21.4 0 -3 -7 278.47 38.75 0 -3 -8 19.65 11.38 0 -3 -9 21.63 12.73 0 -3 -10 349.22 50.74 0 -3 -11 119.62 32.14 0 -3 -12 281.18 52.47 0 4 -13 -5.48 13.15 0 4 -12 71.86 29.26 0 4 -11 17.44 15.52 0 4 -10 199.54 40.18 0 -4 10 407.82 43.87 0 4 -9 96.86 24.92 0 -4 9 187.35 28.48 0 4 -8 324.37 41.08 0 -4 8 433.79 37.38 0 -4 7 74.11 14.3 0 4 -7 58.17 16.11 0 -4 6 463.7 34.19 0 4 -6 450.57 39.31 0 -4 5 639.31 37.57 0 4 -5 662.93 41.69 0 -4 4 189.04 18.71 0 4 -4 204.14 20.22 0 -4 3 1838.36 59.88 0 4 -3 1864 51.36 0 -4 2 56.52 8.91 0 -4 2 25.16 7.51 0 4 -1 1345.97 62.52 0 -4 1 1325.64 58.69 0 -4 0 8.18 7.47 0 -4 0 2.08 2.58 0 4 0 8.34 3.82 0 -4 -1 495.03 64.75 0 4 1 424.27 36.94 0 -4 -2 498.66 55.73 0 4 2 351.93 38.41 0 -4 -3 326.57 39.38 0 4 3 295.91 29.92 0 4 4 1374.38 57.48 0 -4 -4 1191.08 74.6 0 -4 -5 134.77 26.63 0 -4 -6 1614.78 95.12 0 -4 -7 1.89 2.78 0 -4 -8 172.65 33.91 0 -4 -9 30.25 16.26 0 -4 -10 45.15 19.08 0 -4 -11 128.47 34.94 0 -4 -12 24.04 18.57 0 5 -12 32.41 19.77 0 5 -11 7.61 5.98 0 -5 11 47.09 15.95 0 5 -10 12.91 10.55 0 -5 10 68.65 18.83 0 5 -9 323.18 46.69 0 -5 9 757 54.1 0 -5 8 43.57 12.26 0 5 -8 17.76 9.22 0 -5 7 1547.53 66.54 0 5 -7 1081.12 69.81 0 -5 6 3.34 3.48 0 5 -6 -1.38 2.45 0 5 -5 862.34 46.81 0 -5 5 987.29 50.46 0 5 -4 1082.78 47.89 0 -5 4 1087.09 52.27 0 -5 3 17.82 7.22 0 5 -3 11.84 5.26 0 -5 2 1971.32 59.24 0 -5 2 1603.57 73.22 0 -5 1 2.9 4.41 0 -5 1 -1.68 4.13 0 5 -1 10.13 3.48 0 5 0 2911.09 85.42 0 -5 0 2848.98 106.09 0 -5 0 3106.17 122.16 0 -5 -1 31.64 17.69 0 5 1 30.69 7.84 0 -5 -1 24.14 16.6 0 -5 -2 111.37 36.43 0 -5 -2 130.35 28.53 0 5 2 132.28 18.94 0 5 3 59.76 12.57 0 -5 -3 77.29 25.79 0 5 4 0.89 9.53 0 -5 -4 23.35 11.85 0 -5 -5 971.09 80.71 0 5 5 927.81 63.36 0 5 6 61.58 11.78 0 -5 -6 73.76 23.28 0 -5 -7 559.85 64.28 0 5 7 710.77 55.68 0 -5 -8 44.88 18.74 0 -5 -9 132.88 34.15 0 -5 -10 6.79 11.08 0 -5 -11 51.22 24.54 0 -6 12 171.36 33.21 0 -6 11 317.25 43.76 0 6 -11 120.28 30.79 0 6 -10 32.24 16.58 0 -6 10 93.5 21.55 0 -6 9 -1.6 2.34 0 6 -9 -10.36 9.06 0 6 -8 107.53 21.96 0 -6 8 258.99 29.84 0 6 -7 86.78 19.35 0 -6 7 203.7 26.18 0 6 -6 941.43 60.56 0 -6 6 1423.67 65.36 0 -6 5 39.83 10.88 0 6 -5 20.67 7.57 0 6 -4 874.59 45.34 0 -6 4 1001.34 56.81 0 -6 3 3.06 4.8 0 6 -3 1.75 1.86 0 -6 2 3.11 3.32 0 -6 2 6.03 5.41 0 -6 1 399.44 45.75 0 -6 1 313.51 37.09 0 -6 0 5.18 4.59 0 -6 0 8.99 5.63 0 6 0 -3.34 5.68 0 -6 -1 1695.24 111.42 0 6 1 1544.72 63.89 0 -6 -1 1505.18 96.76 0 -6 -2 61.15 24.67 0 -6 -2 40.3 28.53 0 6 2 42.15 5.74 0 -6 -3 1398.01 94.01 0 6 3 1205.72 59.96 0 6 4 -4.18 7.58 0 -6 -4 8.11 8.42 0 -6 -5 198.5 43.49 0 6 5 241.52 31.68 0 -6 -6 130.18 35.89 0 6 6 174.54 26.31 0 -6 -7 17.95 14.09 0 6 7 18.74 14.38 0 -6 -8 538.43 75.93 0 -6 -9 13.31 15.83 0 -6 -10 160.4 45.49 0 -6 -11 9.68 16.23 0 -7 11 29.37 13.11 0 -7 10 228.67 33.89 0 -7 9 43.52 13.87 0 -7 8 72.3 17.25 0 -7 7 700.75 53.59 0 -7 6 12.44 6.9 0 -7 5 1311.83 72.54 0 -7 4 7.53 5.85 0 7 -3 394.2 34 0 -7 3 456.7 46.75 0 -7 2 26.33 12.18 0 -7 2 7.15 3.57 0 -7 1 20.04 10.06 0 -7 1 25.38 11.41 0 -7 0 802.81 56.47 0 -7 0 1041.83 71.16 0 -7 -1 17.01 11.03 0 -7 -1 24.32 14.12 0 7 1 -1.68 7.65 0 -7 -2 1189.7 111.25 0 7 2 1182.34 55.29 0 -7 -2 1069.13 102.56 0 -7 -3 -6.03 18.14 0 7 3 5.61 3.44 0 -7 -3 2.24 7.88 0 -7 -4 493.86 56.62 0 7 4 523.22 38.93 0 -7 -5 22.68 16.26 0 7 5 33.78 8.61 0 7 6 68.14 13.79 0 -7 -6 48.35 28.12 0 -7 -7 87.7 35.25 0 7 7 151.52 21.05 0 -7 -8 38.83 21.01 0 -7 -9 107.22 39.85 0 -7 -10 15.42 19.57 0 -8 11 450.47 52.73 0 -8 10 40.1 15.11 0 -8 9 547.2 51.55 0 -8 8 65.96 18.39 0 -8 7 59.89 16.57 0 -8 6 357.6 40.42 0 -8 5 61.4 17.16 0 -8 4 508.81 54.06 0 -8 3 6.64 5.58 0 -8 2 674.71 60.53 0 -8 1 45.6 15.47 0 -8 1 10.94 7.24 0 -8 0 32.18 12.56 0 -8 0 49.78 15.9 0 -8 -1 279.41 39.59 0 -8 -1 207.12 35.58 0 -8 -2 33.12 16.68 0 -8 -2 39.21 15.71 0 8 2 28.32 8.29 0 -8 -3 709.52 91.96 0 8 3 765.56 44.02 0 8 4 133.22 18.11 0 -8 -4 109.15 32.71 0 -8 -4 70.92 39.83 0 -8 -5 283.99 45.36 0 8 5 361.84 30.05 0 -8 -6 3.36 15.49 0 8 6 16.69 6.4 0 -8 -7 49.01 33.71 0 8 7 85.83 15.56 0 -8 -8 37.36 29.82 0 -8 -9 21.8 24.89 0 -9 10 179.23 33.19 0 -9 9 49.74 18.51 0 -9 8 385.11 48.36 0 -9 7 34.27 14.07 0 -9 6 156.25 29.21 0 -9 5 53.42 19.38 0 -9 4 2.24 3.97 0 -9 3 241.76 38.68 0 -9 2 31.48 13.2 0 -9 1 982.74 73.07 0 -9 0 7.74 5.91 0 -9 0 5.32 5.74 0 -9 -1 214.8 34.43 0 -9 -1 359.32 45.13 0 -9 -2 242.99 40.85 0 -9 -2 149.07 33.59 0 -9 -3 2.05 8.43 0 -9 -3 14.04 12.61 0 -9 -4 313.02 60.81 0 -9 -4 204.48 49.58 0 -9 -5 8.19 10.29 0 -9 -5 2.67 12.15 0 -9 -6 156.33 56.89 0 -9 -6 359.78 55.94 0 -9 -7 30.29 31.39 0 -9 -7 -4.29 8.3 0 -9 -8 12.24 21.73 0 -10 9 456.91 59.97 0 -10 8 14.17 11.25 0 -10 7 299.45 48.01 0 -10 6 7.93 8.5 0 -10 5 31.13 17.74 0 -10 4 122.29 30.26 0 -10 3 -5.33 7.16 0 -10 2 479.41 53.26 0 -10 1 -2.38 4.9 0 -10 0 481.61 53.09 0 -10 -1 6.88 8.47 0 -10 -2 84.15 21.67 0 -10 -2 46.38 17.15 0 -10 -3 31.29 15.8 0 -10 -3 19.39 11.41 0 -10 -4 24.87 15.08 0 -10 -4 16.29 11.75 0 -10 -5 152.94 41.22 0 -10 -5 94.89 35.75 0 -10 -6 6.91 9.41 0 -10 -6 8.32 5.87 0 -11 7 -2.38 5.78 0 -11 6 79.67 27.32 0 -11 5 8.03 10.44 0 -11 4 167.7 34.22 0 -11 3 10.39 9.62 0 -11 2 9.54 9.25 0 -11 1 447.13 50.89 0 -11 0 0.53 4.81 0 -11 -1 567.14 58.96 0 -11 -2 28.12 11.93 0 -11 -3 162.79 31.01 0 -11 -4 18.96 10.68 0 -11 -5 12.68 10.83 0 -12 5 208.17 39.97 0 -12 4 27.23 14.12 0 -12 3 222.8 38.43 0 -12 2 29.73 13.77 0 -12 1 27.93 13.75 0 -12 0 129.75 27.69 0 -12 -1 16.34 11.28 0 -12 -2 180.37 32.98 1 -12 -3 172.34 33.88 1 -12 -2 1.08 3.35 1 -12 -1 270.92 43.26 1 -12 0 4.14 6.76 1 -12 1 164.53 32.45 1 -12 2 31.24 14.92 1 -12 3 38.37 16.95 1 -12 4 335.5 52.8 1 -12 5 25.06 14.67 1 -11 -5 64.28 24.81 1 -11 -4 94.36 28.83 1 -11 -3 13.3 10.63 1 -11 -2 328.21 47.26 1 -11 -1 4.4 6.04 1 -11 0 344.65 47.77 1 -11 1 58.83 18.99 1 -11 2 160.4 33.13 1 -11 3 16.36 10.36 1 -11 4 22.76 12.04 1 -11 5 171.2 39.14 1 -11 6 18.23 16.7 1 -11 7 37.79 19.61 1 -10 -7 21.75 15.63 1 -10 -7 -7.54 23.2 1 -10 -6 133.45 51.35 1 -10 -6 275.6 57.02 1 -10 -5 -3.49 10.37 1 -10 -5 5.66 12.59 1 -10 -4 158.22 41.89 1 -10 -4 102.87 37.26 1 -10 -3 -0.76 4.28 1 -10 -2 1.11 4.31 1 -10 -1 220.35 36.48 1 -10 0 28.72 13.53 1 -10 1 768.66 70.03 1 -10 2 56.85 19.28 1 -10 3 560.89 63.82 1 -10 4 -1.43 5.02 1 -10 5 14.87 13.15 1 -10 6 166.44 37.77 1 -10 7 52.64 21.08 1 -10 8 316.48 50.13 1 -9 -8 48.75 30.76 1 -9 -7 125.75 43.73 1 -9 -6 3.85 11.27 1 -9 -6 12.09 7.72 1 -9 -5 481.8 70.89 1 -9 -5 312.08 69.1 1 -9 -4 11.85 19.18 1 -9 -4 0.98 8.56 1 -9 -3 111.83 35.44 1 -9 -3 219.38 47.67 1 -9 -2 25.59 13.65 1 -9 -2 40.89 17.96 1 -9 -1 153.24 30.54 1 -9 0 500.29 54.24 1 -9 1 37.14 14.1 1 -9 2 583.75 60.45 1 -9 3 9.67 8.18 1 -9 4 103.16 30.79 1 -9 5 5.24 7.3 1 -9 6 52.85 18.86 1 -9 7 203.55 37.2 1 -9 8 174.38 33.5 1 -9 9 195.02 36.32 1 -8 -10 0.48 9.08 1 -8 -9 88.24 32.87 1 -8 -8 10.88 12.24 1 -8 -7 15.39 12.52 1 -8 -6 201.69 44.98 1 -8 -5 7.85 8.83 1 -8 -5 6.37 9.72 1 -8 -4 496.04 66.9 1 -8 -4 469.4 73.62 1 -8 -3 58.65 23.81 1 -8 -3 37.52 25.84 1 -8 -2 332.95 60.48 1 -8 -2 443.92 63.58 1 -8 -1 23.65 9.2 1 -8 -1 36.2 14.88 1 -8 0 129.69 26.87 1 -8 1 654.43 62.97 1 -8 2 174.56 33.89 1 -8 3 330.58 52.42 1 -8 4 191.57 34.09 1 -8 5 408.89 46.72 1 -8 6 45.54 14.83 1 -8 7 177.66 29.79 1 -8 8 189.59 31.62 1 -8 9 169.97 29.57 1 -8 10 259.04 38.67 1 -7 -10 120.86 34.67 1 -7 -9 7.86 8.84 1 -7 -8 442.33 57.42 1 -7 -7 0.39 5.36 1 -7 -6 86.33 23.5 1 -7 -5 61.55 21.05 1 -7 -4 1.98 6.92 1 -7 -3 1115.69 100.62 1 -7 -3 1180.93 95.71 1 -7 -2 12.86 13.9 1 -7 -2 18.21 13.64 1 -7 -1 1724.2 120.19 1 -7 -1 1325.06 94.77 1 -7 0 4.98 4.24 1 -7 0 1.05 2.55 1 -7 1 561.22 58.48 1 -7 2 239.78 41.88 1 -7 3 6.44 4.93 1 -7 4 1164.64 74.5 1 -7 5 88.91 19.8 1 -7 6 654.97 50.77 1 -7 7 233.52 31.23 1 -7 8 121.57 23.64 1 -7 9 35.51 12.37 1 -7 10 31.88 12.48 1 -7 11 177.91 33.67 1 -6 -11 86.05 29.39 1 -6 -10 4.85 6.39 1 -6 -9 533.29 59.67 1 -6 -8 6.42 7.45 1 -6 -7 508.54 52.38 1 -6 -6 5.86 6.82 1 -6 -5 26.62 10.39 1 -6 -4 218.69 29.25 1 -6 -3 70.62 16.46 1 -6 -2 1478.42 87.29 1 -6 -2 1371.76 119.37 1 -6 -1 205.52 43.1 1 -6 -1 128.74 33.11 1 -6 0 1780.79 68.97 1 -6 0 1642.56 95.18 1 -6 1 96.73 24.67 1 -6 2 327.84 44 1 -6 3 141.45 24.51 1 -6 4 276.79 31.41 -1 6 -5 619.52 36.63 1 -6 5 661.05 47.56 -1 6 -6 486.43 38.69 1 -6 6 665.71 49.53 1 -6 7 459.7 40.75 -1 6 -7 323.73 34.89 -1 6 -8 47.46 15.6 1 -6 8 92.11 18.27 1 -6 9 332.08 37.57 -1 6 -9 187.44 31.15 1 -6 10 14.64 7.71 1 -6 11 210.02 36.21 1 -6 12 146.32 30.58 1 -5 -12 4.87 11.38 1 -5 -11 35.92 19.67 1 -5 -10 32.62 15.72 1 -5 -9 -0.03 4.42 1 -5 -8 318.47 41.83 1 -5 -7 7.9 5.91 1 -5 -6 1281.78 76.03 1 -5 -5 66.92 15.84 1 -5 -4 431.81 38.1 1 -5 -3 52.55 12.71 1 -5 -2 39.61 9.94 1 -5 -2 35.31 15.19 1 -5 -1 4745.54 241.34 1 -5 -1 4950 130.21 1 -5 0 342.58 45.73 1 -5 0 242.38 28.95 1 -5 1 1595.6 102.16 1 -5 2 63.41 15.9 1 -5 3 413.18 34.64 -1 5 -3 336.42 16.23 -1 5 -4 142.52 19.44 1 -5 4 155 20.6 1 -5 5 169.42 21.09 -1 5 -5 151.16 24.49 -1 5 -6 638.96 55.88 1 -5 6 1018.01 54.14 1 -5 7 189.38 25.02 -1 5 -7 111.75 25.13 1 -5 8 209.41 26.75 -1 5 -8 97.85 24.16 1 -5 9 88.08 18.56 -1 5 -9 34.37 16.07 1 -5 10 117.33 24.82 -1 5 -10 35.06 16.33 -1 5 -11 -7.53 11.65 1 -5 11 12.66 9.36 1 -4 -12 285.14 47.93 1 -4 -11 23.9 13.5 1 -4 -10 329.58 46.6 1 -4 -9 89.97 23.83 1 -4 -8 38.02 14 1 -4 -7 346.51 40.23 1 -4 -6 55.86 15.84 1 -4 -5 2373.22 89.2 1 -4 -4 83.08 15.33 1 -4 -3 1309.78 55.81 1 -4 -2 122.87 14.95 1 -4 -1 664.25 31.22 1 -4 -1 711.46 80.34 1 -4 0 2532.94 83.22 1 -4 0 2161.84 120.36 1 -4 1 21.75 10.21 1 -4 2 2002.72 73.03 -1 4 -3 362.57 27.73 1 -4 3 593.65 35.37 -1 4 -4 853.27 65.92 1 -4 4 1134.77 49.43 -1 4 -5 62.59 21.01 1 -4 5 114.3 15.8 1 -4 6 160.79 20.66 -1 4 -6 102.86 26.73 -1 4 -7 212.13 39.4 1 -4 7 466.07 36.2 1 -4 8 436.96 38.37 -1 4 -8 164.92 38.48 -1 4 -9 126.64 33.47 1 -4 9 459.95 45.29 1 -4 10 347.3 41.54 -1 4 -10 95.9 32.6 -1 4 -11 53.76 26.61 -1 4 -12 -6.33 14.07 1 -3 -13 164.17 38.29 1 -3 -12 17.58 15.9 1 -3 -11 508.12 62.16 1 -3 -10 2.97 6.13 1 -3 -9 103.01 25.6 1 -3 -8 7.23 5.33 1 -3 -7 17.97 9.44 1 -3 -6 644.28 45.31 1 -3 -5 183.72 21.66 1 -3 -4 2089.15 66.23 1 -3 -3 95.86 12.19 1 -3 -2 2920.04 60.41 1 -3 -1 99.87 23.48 1 -3 -1 99.22 9.13 1 -3 0 499.16 54.75 1 -3 1 1189.2 57.64 1 -3 2 633.43 32.2 -1 3 -2 549.85 30.6 1 -3 3 2450.11 61.41 -1 3 -3 2272.62 84.68 -1 3 -4 464.69 47.15 1 -3 4 418.7 28 -1 3 -5 507.63 58.04 1 -3 5 394.06 28.62 -1 3 -6 23.07 10.9 1 -3 6 24.78 7.5 1 -3 7 193.66 23.83 -1 3 -7 165.9 35.99 -1 3 -8 511.23 64.76 1 -3 8 824.25 55.66 1 -3 9 275.28 34.25 -1 3 -9 126.39 34.22 -1 3 -10 148.74 38.97 -1 3 -11 10.28 9.74 -1 3 -12 8.64 13.71 1 -2 -13 19.78 12.4 1 -2 -12 202.58 43.12 1 -2 -11 18.11 11.62 1 -2 -10 692.53 65.92 1 -2 -9 11.13 8.47 1 -2 -8 1036.31 66.39 1 -2 -7 58.67 14.45 1 -2 -6 53.53 11.94 1 -2 -5 1419.97 57.42 1 -2 -4 157.33 16.78 1 -2 -3 8987.12 115.52 1 -2 -2 29.43 5.75 1 -2 -1 2110.39 35.68 1 -2 0 8.44 9.72 1 -2 1 204.89 16.86 -1 2 -1 202.89 14.66 1 -2 2 642.36 27.12 -1 2 -2 554.01 46.06 -1 2 -3 362.52 34.51 1 -2 3 296.9 19.85 -1 2 -4 2238.17 100.51 1 -2 4 1778.25 55.86 -1 2 -5 853.93 72.36 1 -2 5 572.03 33.69 -1 2 -6 623.35 64.01 1 -2 6 492.75 34.8 -1 2 -7 285.27 44.19 1 -2 7 309.05 32.22 -1 2 -8 149.62 32.88 1 -2 8 179.19 25.84 1 -2 9 245.66 22.69 -1 2 -9 130.47 32.87 1 -2 10 287.4 26 -1 2 -10 122.63 34.12 -1 2 -11 206.68 48.38 -1 2 -12 156.16 46.7 1 -1 -13 79.67 28.05 1 -1 -12 46.41 20.21 1 -1 -11 162.45 34.36 1 -1 -10 2.89 3.53 1 -1 -9 501.55 49.68 1 -1 -8 59.92 16.26 1 -1 -7 1055.52 59.84 1 -1 -6 4.72 3.94 1 -1 -5 288.21 26 1 -1 -4 898.37 39.6 1 -1 -3 819.98 32.14 1 -1 -2 3303.59 55.35 1 -1 -1 311.88 14.42 1 -1 0 1530.3 96.52 -1 1 0 1659.17 32.86 -1 1 -1 95.01 22.03 1 -1 1 85.82 7.56 1 -1 2 1199.3 34.19 -1 1 -2 1206.53 74 1 -1 3 73.87 9.27 -1 1 -3 116.73 20.37 -1 1 -4 248.51 32.97 1 -1 4 155.02 15.5 -1 1 -5 3097.33 131.44 1 -1 5 2525.17 74.69 1 -1 6 505.47 35.76 -1 1 -6 671.57 65.33 1 -1 7 1866.21 55.13 -1 1 -7 1668.06 107.31 1 -1 8 59.4 10.85 -1 1 -8 33.05 13.59 1 -1 9 644.3 35.03 -1 1 -9 455.95 61.93 -1 1 -10 11.41 8.81 -1 1 -11 72.72 26.56 -1 1 -12 90.65 34.46 1 0 -13 299.25 54.9 1 0 -12 -2.53 7.77 1 0 -11 33.57 14.97 1 0 -10 328.52 43.52 1 0 -9 -2.8 2.83 1 0 -8 1945.55 89.67 1 0 -7 81.64 15.92 1 0 -6 4148.98 113.46 1 0 -5 1.12 1.61 1 0 -4 1116.16 44.08 1 0 -3 1050.67 37.88 1 0 -2 254.91 16.58 -1 0 1 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-6 1 4 20.24 9.66 -6 1 3 41.92 18.01 6 -1 -3 -6.19 23.84 6 -1 -2 996.09 64.03 -6 1 2 856.55 64.47 -6 1 1 10.27 6.18 6 -1 0 810.77 49.38 -6 1 0 801.13 68 -6 1 -1 17.72 11.53 6 -1 1 12.73 5.96 6 -1 2 475.64 40.21 -6 1 -2 499 64.65 -6 1 -3 66.13 22.23 -6 1 -4 8.07 10.12 -6 1 -5 382.51 68.82 -6 1 -6 25.93 26.6 -6 1 -7 114.76 43.47 6 0 -12 39.72 19.67 6 0 -11 166.46 37.88 6 0 -10 323.51 50.27 6 0 -9 83.46 23.86 6 0 -8 1043.93 83.97 6 0 -7 2.51 6.19 -6 0 6 835.17 69.66 -6 0 5 130.83 27.17 -6 0 4 305.07 37.55 -6 0 3 199.27 31.12 -6 0 2 47.45 16.89 -6 0 1 435.19 49.08 -6 0 0 16.95 11.25 -6 0 -1 528.29 66.85 -6 0 -2 6.77 11.9 -6 0 -3 145.63 38.55 -6 0 -4 -2.34 8.88 -6 0 -5 2.88 7.62 -6 0 -6 14.57 15.2 -6 0 -7 -9.02 21.5 6 1 -12 817.8 90.03 6 1 -11 8.07 9.52 6 1 -10 146.38 34.71 6 1 -9 131 33.03 6 1 -8 6.5 5.58 6 1 -7 876.81 82.52 -6 -1 7 874.86 77.5 -6 -1 6 17.36 9.98 -6 -1 5 677.06 62.16 -6 -1 4 58.42 18.64 -6 -1 3 150.35 31.15 -6 -1 2 3.14 4.87 -6 -1 1 44.71 18.06 -6 -1 0 735.24 80.83 -6 -1 -1 121.35 35.26 -6 -1 -2 572.86 79.8 -6 -1 -3 22.06 16.24 -6 -1 -4 41.96 26.43 -6 -1 -5 -11.5 21.82 -6 -1 -6 -6.56 21.96 6 2 -12 13.18 11.99 6 2 -11 661.34 80.18 6 2 -10 9.25 8.66 6 2 -9 747.84 77 6 2 -8 56.8 22.31 -6 -2 7 137.59 33.92 -6 -2 6 415.45 53.94 -6 -2 5 6.48 6.52 -6 -2 4 874.43 76.06 -6 -2 3 7.5 7.21 -6 -2 2 487.17 62.17 -6 -2 1 18.37 13.02 -6 -2 0 116.03 34.79 -6 -2 -1 144.28 44.22 -6 -2 -2 -9.02 16.62 -6 -2 -3 68.73 34.5 -6 -2 -4 -6.92 15.36 -6 -2 -5 31.69 24.44 -6 -2 -6 -10.98 14.12 6 3 -12 406.14 71.18 6 3 -11 -5.04 10.38 6 3 -10 625.28 77.23 6 3 -9 2.55 4.25 6 3 -8 292.72 52.57 -6 -3 7 86.71 27.26 -6 -3 6 25.28 14.3 -6 -3 5 197.55 37.99 -6 -3 4 9.74 7.29 -6 -3 3 403.93 59.81 -6 -3 2 42.69 18.36 -6 -3 1 224.23 50.97 -6 -3 0 -2.11 10.68 -6 -3 -1 44.08 28.61 -6 -3 -2 21.98 18.23 -6 -3 -3 20.81 16.72 -6 -3 -4 75.32 29.63 -6 -3 -5 19.96 16.74 6 4 -11 99.61 34.6 6 4 -10 8.57 15 6 4 -9 475.71 57.54 6 4 -9 450.33 70.63 -6 -4 8 10.97 14.78 6 4 -8 4.93 9.8 -6 -4 7 464.57 63.56 -6 -4 6 2.37 4.88 -6 -4 5 78.7 29.24 -6 -4 4 41.56 18.99 -6 -4 3 -1.8 6.15 -6 -4 2 438.67 75.26 -6 -4 1 -6.71 18.76 -6 -4 0 204.05 54.6 -6 -4 -1 21.82 20.89 -6 -4 -2 1.74 8.64 -6 -4 -3 39.27 20.12 -6 -4 -4 -6.18 9.31 6 5 -10 126.59 40.98 6 5 -9 20.93 24.58 6 5 -9 -0.31 10.3 6 5 -8 289.36 39.67 -6 -5 8 214.3 53.08 6 5 -8 219.91 55.81 -6 -5 7 7.1 10.58 -6 -5 6 225.44 55.84 -6 -5 5 13.29 15.12 -6 -5 4 85.79 39.74 -6 -5 3 22.39 18.95 -6 -5 2 19.65 18.24 -6 -5 1 115.53 35.48 -6 -5 0 16.98 18.18 -6 -5 -1 102.83 33.24 -6 -5 -2 9.62 12.18 -6 -5 -3 23.54 14.98 6 6 -9 46.45 20.29 6 6 -9 27.04 21.64 6 6 -8 7.51 13.15 6 6 -8 -2.63 20.88 -6 -6 8 -18.49 21.93 -6 -6 7 55.51 30.26 6 6 -7 190.74 29.07 -6 -6 6 -5.15 11.36 -6 -6 5 166.97 54.06 -6 -6 4 -0.02 8.43 -6 -6 3 120.12 40.82 -6 -6 2 22.54 17.82 -6 -6 1 9.12 14.7 -6 -6 0 262.32 54.59 -6 -6 -1 13.15 12.86 -6 -6 -2 123.35 38.58 -6 -7 7 34.19 22.48 6 7 -7 22.51 20.08 -6 -7 6 101 35.57 6 7 -6 171.01 28.73 -6 -7 5 -13.61 18.84 -6 -7 4 486.57 79.41 -6 -7 3 10.1 10.78 -6 -7 2 102.55 34.38 -6 -7 1 -5.48 11.21 -6 -7 0 2.28 10.98 7 -9 -6 138.95 40.9 7 -9 -5 10.04 12.8 7 -9 -4 395.81 65.55 7 -9 -3 19.28 11.8 7 -9 -2 44.7 19.34 7 -9 -1 2.63 6.63 7 -9 0 12.29 11.96 7 -9 1 7.25 8.04 7 -8 -7 9.6 12.35 7 -8 -6 40.24 19.18 7 -8 -5 115.57 38.76 7 -8 -4 59.16 25.87 7 -8 -3 296.43 53.36 7 -8 -2 17.7 11.82 7 -8 -1 165.43 44.05 7 -8 0 3.3 7.41 7 -8 1 30.22 16.77 7 -8 2 111.73 30.57 7 -7 -9 405.2 48.11 7 -7 -8 8.06 7.22 7 -7 -7 107.88 28.33 7 -7 -7 252.73 36.13 7 -7 -6 31.43 18.81 7 -7 -6 68.04 15.29 7 -7 -6 62.12 17.29 7 -7 -5 75.38 37.47 7 -7 -5 111.95 23.43 7 -7 -4 341.07 38.24 7 -7 -4 239.22 54.67 7 -7 -3 37.42 25.13 7 -7 -2 243.04 49.12 7 -7 -1 7.89 5.41 7 -7 0 72.88 26.97 7 -7 1 3.77 6.38 7 -7 2 58.35 18.61 7 -7 3 89.51 23.65 7 -6 -10 94.56 24.78 7 -6 -9 -0.85 7.43 7 -6 -8 599.62 59.85 7 -6 -7 78 21.31 7 -6 -6 321.69 40.4 7 -6 -6 366.88 36.26 7 -6 -5 12.86 8.1 7 -6 -5 2.58 4.06 7 -6 -4 32.42 21.57 7 -6 -4 37.92 10.15 7 -6 -4 51.66 15.56 7 -6 -3 67.17 14.51 7 -6 -3 71.4 31.47 7 -6 -3 67.68 18.76 7 -6 -2 64.23 29.01 7 -6 -2 95.67 17 7 -6 -2 109.09 23.32 7 -6 -1 420.59 36.66 -7 6 1 351.59 39.17 7 -6 0 126.44 30.05 7 -6 0 155.81 22.11 -7 6 0 105.42 21.88 7 -6 1 315.45 31.43 7 -6 1 372.99 46.68 7 -6 2 24.98 9.36 7 -6 2 20.83 10.04 7 -6 3 80.06 16.78 7 -6 3 76.88 18.75 7 -6 4 145.1 22.68 7 -5 -10 136.51 30.31 7 -5 -9 318.78 45.99 7 -5 -8 131.07 27.77 7 -5 -7 974.51 73.85 7 -5 -7 1200.25 65.12 7 -5 -6 51.19 14.02 7 -5 -6 43.62 15.82 7 -5 -5 317.15 32.24 7 -5 -5 289.3 38.4 7 -5 -5 236.7 55.46 7 -5 -4 5.79 6.78 7 -5 -4 -17.4 27 7 -5 -4 3.62 4.79 7 -5 -3 186.17 52.95 7 -5 -3 170.33 22.9 -7 5 3 178.64 32.64 7 -5 -2 27.55 18.24 -7 5 2 62.5 17.13 -7 5 1 23.75 9.46 7 -5 -1 39.77 17.82 7 -5 -1 49.02 11.93 7 -5 0 345.62 41.78 -7 5 0 296.71 38.06 7 -5 0 331.45 32.3 -7 5 -1 36.64 12.07 7 -5 1 74.49 17.06 7 -5 1 82.33 16.67 7 -5 2 287.92 33.16 7 -5 2 289.91 31 -7 5 -2 271.14 36.61 -7 5 -3 21.41 9.86 7 -5 3 28.85 10.19 7 -5 4 44.84 12.86 7 -5 5 10.31 5.78 7 -4 -11 276.91 45.54 7 -4 -10 3.44 7.33 7 -4 -9 108.81 26.72 7 -4 -8 166.96 31.12 7 -4 -7 15.1 10.27 7 -4 -6 457.09 48.23 7 -4 -6 600.03 44.21 7 -4 -5 110.32 18.71 7 -4 -5 86.34 30 7 -4 -5 98.28 22.33 7 -4 -4 318.86 30.85 7 -4 -4 232.81 75.46 -7 4 4 284.96 40.08 -7 4 3 27.14 11.5 7 -4 -3 65.35 14.06 7 -4 -3 21.55 17.11 7 -4 -2 106.01 30.39 7 -4 -2 158.6 23.6 -7 4 2 146.2 27.2 -7 4 1 25.4 11.85 7 -4 -1 24.48 9.46 7 -4 -1 51.5 13.36 7 -4 0 250.66 31.33 7 -4 0 233.53 28.06 -7 4 0 201.5 31.92 7 -4 1 467.59 41.03 -7 4 -1 346.56 42.14 7 -4 2 256.7 31.1 -7 4 -2 174.38 30.72 7 -4 3 373.46 36.83 -7 4 -3 323.34 43.62 -7 4 -4 68.51 20.64 7 -4 4 80.75 17.23 7 -4 5 99.36 19.71 -7 4 -5 82.44 24.02 7 -3 -11 12.48 7.18 7 -3 -10 950.93 84 7 -3 -9 28.75 12.36 7 -3 -8 308.35 43.67 7 -3 -7 15.05 11.57 7 -3 -6 61.72 19 -7 3 5 525.72 53.81 7 -3 -5 642.21 46.04 7 -3 -5 614.5 59.53 -7 3 4 39.77 13.77 7 -3 -4 37.58 34.59 7 -3 -4 77.69 16.13 -7 3 3 598.18 54.61 7 -3 -3 741.39 50.01 -7 3 2 22.67 11.03 7 -3 -2 34.5 14.74 7 -3 -2 35.32 11.99 7 -3 -1 290.58 30.22 -7 3 1 276.42 37.83 7 -3 0 17.79 7.76 -7 3 0 10.21 8.47 7 -3 1 48.92 12.53 -7 3 -1 34.17 14.64 7 -3 2 284.87 32.21 -7 3 -2 228.64 37.56 -7 3 -3 17.22 7.17 7 -3 3 44.07 13.78 7 -3 4 262.53 33.27 -7 3 -4 239.22 42.56 -7 3 -5 112.8 32.49 7 -3 5 124.7 22.77 7 -2 -11 570.45 68.2 7 -2 -10 2.3 3.9 7 -2 -9 621.72 65.45 7 -2 -8 1.78 3.45 7 -2 -7 86.9 23.65 -7 2 6 53.15 18.14 7 -2 -6 62.06 20.21 -7 2 5 108.09 24.01 7 -2 -4 284.56 85.47 -7 2 4 258.49 36.01 -7 2 3 72.41 17.58 7 -2 -2 534.57 43.01 -7 2 2 445.96 47.45 7 -2 -1 125.45 20.83 -7 2 1 86.58 21.23 7 -2 0 292.9 32.65 -7 2 0 267.68 40.99 -7 2 -1 2.32 4.46 7 -2 1 6.85 5.99 7 -2 2 219.05 29.17 -7 2 -2 171.4 34.83 -7 2 -3 89.2 27.24 7 -2 3 100.65 19.97 7 -2 4 269.16 33.86 -7 2 -4 213.78 45.66 -7 2 -5 92.41 27.66 7 -1 -11 109.89 31.04 7 -1 -10 191.97 39.17 7 -1 -9 19.36 11.45 7 -1 -8 564.65 62.95 7 -1 -7 122.92 28.59 -7 1 6 375.12 48.56 -7 1 5 1.69 2.81 -7 1 4 161.5 29.42 -7 1 3 583.86 66.75 -7 1 2 222.34 35.59 -7 1 1 888.18 74.03 -7 1 0 134.98 28.22 -7 1 -1 146.2 33.21 -7 1 -2 3.47 7.34 -7 1 -3 8.4 6.13 -7 1 -4 110.92 32.35 -7 1 -5 34.56 19.78 7 0 -11 70.6 26.06 7 0 -10 124.3 33.56 7 0 -9 175.94 36.88 7 0 -8 -0.82 6.01 -7 0 7 727.04 70.56 7 0 -7 743.88 75.73 -7 0 6 1.9 4.49 -7 0 5 462.85 53.62 -7 0 4 0.65 4.02 -7 0 3 167.7 32.14 -7 0 2 76.62 20.33 -7 0 1 6.86 7.89 -7 0 0 468.68 62.1 -7 0 -1 92.46 28.37 -7 0 -2 275.09 57.29 -7 0 -3 100.81 36.77 -7 0 -4 14.01 16.73 -7 0 -5 13.81 16.61 7 1 -11 162.33 38.3 7 1 -10 -3.13 6.88 7 1 -9 69.81 24.67 7 1 -8 208.26 43.44 -7 -1 7 155.61 35.39 -7 -1 6 456.77 54.59 -7 -1 5 183.83 33.08 -7 -1 4 716.37 76.9 -7 -1 3 43.02 17.01 -7 -1 2 262.07 45.37 -7 -1 1 44.05 17.66 -7 -1 0 163.08 39.11 -7 -1 -1 259.88 54.96 -7 -1 -2 49.16 27.63 -7 -1 -3 58.7 34.63 -7 -1 -4 -2.64 12.51 7 2 -11 10.89 12.95 7 2 -10 548 74.39 7 2 -9 3.61 6.85 -7 -2 8 122.6 32.61 7 2 -8 106.86 32.5 -7 -2 7 140.23 32.58 -7 -2 6 14.23 10.86 -7 -2 5 632.99 66.16 -7 -2 4 31.07 15.5 -7 -2 3 484.71 65.89 -7 -2 2 45.33 21.13 -7 -2 1 31.85 18.59 -7 -2 0 9.82 10.18 -7 -2 -1 -3.1 10.68 -7 -2 -2 69.57 33.39 -7 -2 -3 12.96 18.85 -7 -2 -4 7.82 18.47 7 3 -10 11.12 14.06 7 3 -9 413.22 68 -7 -3 8 24.86 15.37 7 3 -8 15.5 13.93 -7 -3 7 259.64 46.05 -7 -3 6 5.57 10.75 -7 -3 5 127.74 33.23 -7 -3 4 96.69 30.62 -7 -3 3 29.46 16.28 -7 -3 2 262.6 55.13 -7 -3 1 42.05 23.32 -7 -3 0 39.62 23.15 -7 -3 -1 -0.74 14.96 -7 -3 -2 15.59 21.55 -7 -3 -3 51.09 31.03 7 4 -9 30.69 22.99 -7 -4 8 507.71 79.91 -7 -4 7 14.13 11.53 -7 -4 6 193.08 48.53 -7 -4 5 31.11 18.92 -7 -4 4 27.17 13.4 -7 -4 3 87.49 32.03 -7 -4 2 17.09 18.37 -7 -4 1 52.62 28.18 -7 -4 0 5.62 12.16 -7 -4 -1 5.33 10.02 -7 -4 -2 -0.32 10.35 -7 -5 8 3.59 12.56 -7 -5 7 181.77 52.07 -7 -5 6 13.14 11.78 -7 -5 5 49.34 29.85 -7 -5 4 6.9 12.56 -7 -5 3 -8.18 13.58 -7 -5 2 35.01 22.42 -7 -5 1 3.53 9.91 -7 -5 0 120.63 38.9 -7 -6 6 80.9 40.05 -7 -6 5 23.41 20.52 -7 -6 4 126.12 41.3 -7 -6 3 -3.89 6.83 -7 -6 2 27.74 18.09 8 -8 -3 64.07 24.03 8 -8 -3 94.83 19.28 8 -8 -2 98.55 35.36 8 -7 -6 37.94 23.56 8 -7 -6 106.68 21.26 8 -7 -5 18.85 11.21 8 -7 -5 6.56 10.01 8 -7 -4 68.76 31.13 8 -7 -4 78.3 17.45 8 -7 -3 36.5 20.17 8 -7 -3 74.05 16.13 8 -7 -2 179.12 26.27 8 -7 -2 48.21 28.95 8 -7 -1 83.98 19.26 8 -7 -1 39.38 21.19 8 -7 0 72.52 16.54 8 -6 -8 147.95 32.06 8 -6 -7 316.92 45.32 8 -6 -7 179.15 44.93 8 -6 -6 133.83 21.95 8 -6 -6 65.57 33.61 8 -6 -6 100.68 24.68 8 -6 -5 79.52 17.68 8 -6 -5 58.66 33.04 8 -6 -5 91.11 23.77 8 -6 -4 12.04 14 8 -6 -4 25.24 9.58 8 -6 -4 10.48 7.9 8 -6 -3 51.12 28.56 8 -6 -3 125.67 23.6 8 -6 -3 122.76 27.61 8 -6 -2 516.89 45.95 -8 6 2 364.33 45.94 8 -6 -1 552.57 47.7 8 -6 0 242.53 31.68 8 -6 1 102.56 20.82 8 -5 -8 197.4 36.6 8 -5 -7 22.8 15.31 8 -5 -7 48.91 17.26 8 -5 -6 220.21 60.75 8 -5 -6 305.08 42.08 8 -5 -5 16.15 23.37 8 -5 -5 67.28 16.15 8 -5 -5 55.76 18.79 8 -5 -4 145.56 23.01 8 -5 -4 119.64 45.52 8 -5 -4 132.95 28.6 8 -5 -3 45.24 13.55 8 -5 -3 12.14 15.91 -8 5 3 32.36 12.85 -8 5 2 16 8.08 8 -5 -2 34.72 12.19 -8 5 1 72.2 19.03 8 -5 -1 138.14 24.1 -8 5 0 82.44 21.64 8 -5 0 134.85 23.23 8 -5 1 145.62 24.12 8 -5 2 183.83 27.11 8 -4 -9 11.21 10.94 8 -4 -8 155.68 31.4 8 -4 -7 116.75 27.53 8 -4 -6 143.2 44.79 8 -4 -6 166.99 31.67 8 -4 -5 313.6 36.02 8 -4 -5 265.14 41.42 -8 4 4 150.09 30.74 8 -4 -4 215.17 29.11 -8 4 3 400.08 47.97 8 -4 -3 486.27 44.84 -8 4 2 9.51 3.18 8 -4 -2 11.59 6.92 8 -4 -1 279.1 33.02 -8 4 1 266.23 39.29 -8 4 0 41.75 17.21 8 -4 0 70.2 16.85 8 -4 1 251.22 31.95 -8 4 -1 174.03 32.46 8 -4 2 102.48 21.58 -8 4 -2 61.54 18.22 8 -3 -9 280.84 44.74 8 -3 -8 15.99 11.66 8 -3 -7 28.57 14.31 8 -3 -6 150.2 43.09 8 -3 -6 164.5 32.57 -8 3 5 127.51 29.15 -8 3 4 456.83 49.7 -8 3 3 183.11 32.48 8 -3 -2 142.85 23.96 -8 3 2 114.18 24.52 -8 3 1 33.5 15.82 8 -3 -1 25.45 9.57 -8 3 0 12.22 7.33 8 -3 0 26.93 10.97 -8 3 -1 14.41 5.49 8 -3 1 39.7 13.27 -8 3 -2 52.1 19.05 8 -3 2 90.76 20.17 8 -2 -10 268.5 47.01 8 -2 -9 15.44 8.85 8 -2 -8 224.68 40.52 8 -2 -7 50.75 19.02 8 -2 -6 275.23 46.06 -8 2 6 294.35 45.22 -8 2 5 -1.87 5.05 -8 2 4 147.22 29.93 -8 2 3 223.76 34.68 -8 2 2 194.24 35 -8 2 1 216.33 38.2 -8 2 0 97.84 27.15 -8 2 -1 51.36 20.63 -8 2 -2 -0.93 10.56 8 -1 -10 177.69 40.15 8 -1 -9 254.35 43.94 8 -1 -8 180.19 36.97 -8 1 7 336.84 48.52 8 -1 -7 300.86 48.95 -8 1 6 23.22 12.95 -8 1 5 346.17 47.45 -8 1 4 36.53 14.65 -8 1 3 213.33 40.89 -8 1 2 227.31 39.29 -8 1 1 149.13 33.04 -8 1 0 52.15 19.58 -8 1 -1 21 15.1 -8 1 -2 3.08 10.84 8 0 -9 10.94 9.1 8 0 -8 326.43 53.61 -8 0 7 185.23 36.81 -8 0 6 344.26 46.4 -8 0 5 197.26 37.01 -8 0 4 56.57 18.63 -8 0 3 12.58 11.24 -8 0 2 32.81 17.08 -8 0 1 128.44 32.76 -8 0 0 157.26 37.02 -8 0 -1 114.33 33.97 -8 0 -2 180.48 45.79 8 1 -9 2.6 6.5 -8 -1 8 277.58 48.6 8 1 -8 250.56 49.42 -8 -1 7 168.78 36.32 -8 -1 6 141.67 32.15 -8 -1 5 377.89 52.53 -8 -1 4 103.53 29.35 -8 -1 3 156.93 35.64 -8 -1 2 12.76 15.16 -8 -1 1 32.11 14.6 -8 -1 0 51.16 21.58 -8 -1 -1 65.34 30.12 -8 -2 8 10.85 14.67 8 2 -8 -12.67 17.18 -8 -2 7 65.11 22.82 -8 -2 6 135.58 33.01 -8 -2 5 68.59 22.93 -8 -2 4 264.67 57.64 -8 -2 3 145.77 38.39 -8 -2 2 1.32 9.25 -8 -2 1 15.66 14.85 -8 -2 0 19.34 14.38 -8 -3 7 44.23 20.84 -8 -3 6 55.73 23.97 -8 -3 5 22.42 16.19 -8 -3 4 6.99 6.76 -8 -3 3 186.29 47.38 -8 -3 2 50.95 26.12 -8 -3 1 48.54 27.38 -8 -4 4 3.24 7.23 9 -4 -5 180.82 36.2 -9 4 4 120.58 28.22 -9 4 3 93.91 23.6 9 -3 -6 88.16 25.47 -9 3 5 66.2 22.14 -9 3 4 150.34 29.06 -9 3 3 40.92 17.95 -9 3 2 89.49 23.94 -9 2 6 30.04 15.46 -9 2 5 84.93 21.95 -9 2 4 54.97 20.03 -9 2 3 203.17 35.63 -9 2 2 119.01 33.5 -9 1 6 99.06 27.93 -9 1 5 6.68 5.43 -9 1 4 29.22 13.42 -9 1 3 9.59 4.68 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 0 1 0.1794 0 0 -1 0.2688 0 1 0 0.0629 0 -1 0 0.0835 -1 1 0 0.2156 1 -1 0 0.4137 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C009 W001 C00B 175.6(7) . . ? C009 W001 As 85.8(5) . . ? C00B W001 As 90.3(6) . . ? C00C W001 C009 90.6(8) . . ? C00C W001 C00B 87.8(8) . . ? C00C W001 As 95.8(5) . . ? C00D W001 C009 92.0(8) . . ? C00D W001 C00B 89.8(9) . . ? C00D W001 C00C 175.9(8) . . ? C00D W001 As 87.6(7) . . ? C00I W001 C009 92.6(8) . . ? C00I W001 C00B 91.4(8) . . ? C00I W001 C00C 87.0(9) . . ? C00I W001 C00D 89.7(10) . . ? C00I W001 As 176.7(6) . . ? C00E S003 C00K 92.3(11) . . ? C00M S004 C00N 91.1(11) . . ? O007 C009 W001 174.9(19) . . ? O008 C00B W001 171.5(18) . . ? O005 C00C W001 177.1(19) . . ? O006 C00D W001 175.9(19) . . ? S003 C00E As 126.0(12) . . ? C00J C00E S003 112.1(16) . . ? C00J C00E As 121.9(17) . . ? C00G C00F C00H 128(2) . . ? C00G C00F C00M 122(2) . . ? C00M C00F C00H 110(2) . . ? C00F C00G C00J 126(2) . . ? C00N C00H C00F 114(2) . . ? O00A C00I W001 177(2) . . ? C00E C00J C00L 108(2) . . ? C00G C00J C00E 125(2) . . ? C00G C00J C00L 127.6(18) . . ? C00L C00K S003 113.3(18) . . ? C00K C00L C00J 114.4(19) . . ? S004 C00M As 123.1(12) . . ? C00F C00M S004 111.1(17) . . ? C00F C00M As 125.7(18) . . ? C00H C00N S004 114.1(19) . . ? C00E As W001 127.9(6) . . ? C00M As W001 128.9(7) . . ? C00M As C00E 99.3(10) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag W001 C009 2.07(2) . ? W001 C00B 2.09(2) . ? W001 C00C 2.07(2) . ? W001 C00D 2.04(2) . ? W001 C00I 1.98(3) . ? W001 As 2.568(2) . ? S003 C00E 1.68(2) . ? S003 C00K 1.72(2) . ? S004 C00M 1.71(2) . ? S004 C00N 1.74(2) . ? O005 C00C 1.13(3) . ? O006 C00D 1.16(3) . ? O007 C009 1.11(2) . ? O008 C00B 1.07(2) . ? O00A C00I 1.12(3) . ? C00E C00J 1.44(3) . ? C00E As 1.86(2) . ? C00F C00G 1.38(3) . ? C00F C00H 1.44(3) . ? C00F C00M 1.43(3) . ? C00G C00J 1.40(3) . ? C00H C00N 1.30(3) . ? C00J C00L 1.47(3) . ? C00K C00L 1.29(3) . ? C00M As 1.83(2) . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -0.0006 0.0014 0.9983 0.0647 0.0012 0.0120 0.0006 -0.0014 -0.9983 -0.0647 -0.0012 -0.0120 0.0018 0.9958 -0.0001 0.0017 0.0669 0.0238 -0.0018 -0.9958 0.0001 -0.0017 -0.0669 -0.0238 -0.9951 0.9947 0.0014 -0.0436 0.0176 0.1023 0.9951 -0.9947 -0.0014 0.0436 -0.0176 -0.1023