#------------------------------------------------------------------------------ #$Date: 2024-12-24 03:06:49 +0200 (Tue, 24 Dec 2024) $ #$Revision: 296954 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/35/1573527.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573527 loop_ _publ_author_name 'Bouzid, Moad' 'Hierso, Jean-Cyrille' 'Mboyi, Cl\`eve D.' 'Poinsot, Didier' 'Domenichini, Bruno' 'Schreiner, Peter Richard' 'Ochmann, Lukas' _publ_section_title ; Sulfur functionalized diamondoid phosphines enable building nanocomposites interfacing sp3-carbon and gold nanolayer ; _journal_name_full Nanoscale _journal_paper_doi 10.1039/D4NR03511A _journal_year 2025 _chemical_formula_moiety 'C16 H21 Cl2 O2 P S' _chemical_formula_sum 'C16 H21 Cl2 O2 P S' _chemical_formula_weight 379.26 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_method ;FinalCif V139 by Daniel Kratzert, Freiburg 2024, https://dkratzert.de/finalcif.html ; _audit_update_record ; 2024-08-06 deposited with the CCDC. 2024-12-20 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 103.068(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.6911(2) _cell_length_b 21.7491(8) _cell_length_c 12.1069(5) _cell_measurement_reflns_used 2502 _cell_measurement_temperature 110(2) _cell_measurement_theta_max 27.485 _cell_measurement_theta_min 0.998 _cell_volume 1716.23(11) _computing_cell_refinement 'SAINT V8.40B (Bruker, 2016)' _computing_data_collection 'APEX5 (Bruker, 2023)' _computing_data_reduction SAINT _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2019/2 (Sheldrick, 2019)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 110(2) _diffrn_detector 'CCD Plate' _diffrn_detector_area_resol_mean 8.3 _diffrn_detector_type APEX2 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Nonius Kappa Apex II' _diffrn_measurement_method '\f and \w scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_radiation_collimation '0.6 mm' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a~1~' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_xray_symbol K-L~3~ _diffrn_reflns_av_R_equivalents 0.0618 _diffrn_reflns_av_unetI/netI 0.0322 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 44968 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.533 _diffrn_reflns_theta_min 3.211 _diffrn_source 'X-ray tube' _diffrn_source_target Mo _diffrn_source_type 'Siemens KFF Mo 2K-180' _exptl_absorpt_coefficient_mu 0.597 _exptl_absorpt_correction_T_max 0.8746 _exptl_absorpt_correction_T_min 0.8069 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016) was used for absorption correction.' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.468 _exptl_crystal_description prism _exptl_crystal_F_000 792 _exptl_crystal_recrystallization_method Sublimation _exptl_crystal_size_max 0.660 _exptl_crystal_size_mid 0.083 _exptl_crystal_size_min 0.077 _refine_diff_density_max 0.457 _refine_diff_density_min -0.263 _refine_diff_density_rms 0.065 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.080 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 200 _refine_ls_number_reflns 3950 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.080 _refine_ls_R_factor_all 0.0556 _refine_ls_R_factor_gt 0.0363 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0287P)^2^+1.4085P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0754 _refine_ls_wR_factor_ref 0.0834 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3103 _reflns_number_total 3950 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4nr03511a2.cif _cod_data_source_block Compound_1b _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1573527 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.694 _shelx_estimated_absorpt_t_max 0.955 _diffrn_measurement_ambient_temperature_device_make 'Oxford Cryostream 600' _shelx_res_file ; TITL 20220512mblo_diampocl2_0m_a.res in P2(1)/n 20220512mblo_diampocl2_0m.res created by SHELXL-2019/3 at 11:36:25 on 06-Aug-2024 REM Old TITL 20220512MBLO_diamPOCl2_0m in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.126, Rweak 0.006, Alpha 0.021 REM 0.364 for 112 systematic absences, Orientation as input REM Formula found by SHELXT: C16 O2 P S Cl2 CELL 0.71073 6.6911 21.7491 12.1069 90 103.068 90 ZERR 4 0.0002 0.0008 0.0005 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl O P S UNIT 64 84 8 8 4 4 L.S. 10 PLAN 10 SIZE 0.077 0.083 0.66 TEMP -163.15(10) CONF BOND list 4 MORE -1 BOND $H fmap 2 acta OMIT 0 1 1 OMIT 0 2 0 OMIT 0 2 1 REM REM REM WGHT 0.028700 1.408500 FVAR 0.40864 CL1 3 0.789945 0.230244 0.490548 11.00000 0.02270 0.02478 = 0.01971 -0.00378 0.00579 0.00215 CL2 3 0.542703 0.305835 0.283974 11.00000 0.05747 0.04167 = 0.01280 0.00156 0.00924 0.00998 S1 6 0.256348 0.519091 0.876387 11.00000 0.02427 0.02243 = 0.01712 -0.00450 -0.00006 0.00446 P1 5 0.503288 0.261420 0.424110 11.00000 0.02317 0.02070 = 0.01423 -0.00464 0.00048 -0.00072 O1 4 0.354254 0.211569 0.397250 11.00000 0.02975 0.02653 = 0.03334 -0.01520 -0.00251 -0.00481 O2 4 -0.101267 0.538996 0.732201 11.00000 0.02267 0.02079 = 0.02448 -0.00111 -0.00052 0.00249 C1 1 0.453919 0.319741 0.520811 11.00000 0.01536 0.01469 = 0.01247 -0.00093 0.00113 -0.00229 C2 1 0.612955 0.371730 0.538329 11.00000 0.01285 0.01721 = 0.01258 0.00262 0.00156 -0.00293 AFIX 23 H2A 2 0.751577 0.354784 0.569455 11.00000 -1.20000 H2B 2 0.613121 0.391596 0.464777 11.00000 -1.20000 AFIX 0 C3 1 0.559722 0.419102 0.620533 11.00000 0.01329 0.01360 = 0.01329 0.00107 0.00024 -0.00498 AFIX 13 H3 2 0.663311 0.453002 0.631557 11.00000 -1.20000 AFIX 0 C4 1 0.562680 0.388976 0.735591 11.00000 0.01133 0.01590 = 0.01083 0.00110 -0.00053 -0.00060 AFIX 13 H4 2 0.702485 0.371779 0.767317 11.00000 -1.20000 AFIX 0 C5 1 0.405298 0.336361 0.717817 11.00000 0.01508 0.01379 = 0.01081 0.00393 0.00212 -0.00163 AFIX 13 H5 2 0.408268 0.316232 0.792432 11.00000 -1.20000 AFIX 0 C6 1 0.456675 0.288394 0.635692 11.00000 0.01494 0.01388 = 0.01525 0.00105 0.00258 -0.00173 AFIX 23 H6A 2 0.354622 0.254697 0.624898 11.00000 -1.20000 H6B 2 0.593950 0.270626 0.667205 11.00000 -1.20000 AFIX 0 C7 1 0.237654 0.346442 0.471723 11.00000 0.01542 0.01756 = 0.01274 0.00039 -0.00216 -0.00335 AFIX 23 H7A 2 0.234126 0.366409 0.397822 11.00000 -1.20000 H7B 2 0.134599 0.313005 0.459564 11.00000 -1.20000 AFIX 0 C8 1 0.190827 0.363589 0.671222 11.00000 0.01210 0.01416 = 0.01630 0.00207 0.00214 -0.00363 AFIX 13 H8 2 0.087082 0.329738 0.660506 11.00000 -1.20000 AFIX 0 C9 1 0.187535 0.393600 0.555533 11.00000 0.01132 0.01467 = 0.01366 0.00292 -0.00262 -0.00087 AFIX 13 H9 2 0.047767 0.410890 0.524077 11.00000 -1.20000 AFIX 0 C10 1 0.345027 0.446269 0.573362 11.00000 0.01468 0.01356 = 0.01005 0.00374 -0.00079 -0.00139 AFIX 13 H10 2 0.342310 0.466482 0.498848 11.00000 -1.20000 AFIX 0 C11 1 0.511603 0.436505 0.818941 11.00000 0.01644 0.01892 = 0.01103 0.00061 -0.00066 -0.00063 AFIX 23 H11A 2 0.614906 0.469873 0.831103 11.00000 -1.20000 H11B 2 0.514649 0.416698 0.892928 11.00000 -1.20000 AFIX 0 C12 1 0.138719 0.411124 0.754102 11.00000 0.01510 0.01828 = 0.01484 0.00331 0.00376 0.00051 AFIX 23 H12A 2 -0.000618 0.427789 0.723909 11.00000 -1.20000 H12B 2 0.141006 0.391364 0.828042 11.00000 -1.20000 AFIX 0 C13 1 0.296479 0.463328 0.769896 11.00000 0.01641 0.01453 = 0.01260 -0.00194 0.00127 0.00099 C14 1 0.295213 0.494205 0.656206 11.00000 0.01714 0.01241 = 0.01647 0.00266 -0.00082 -0.00050 AFIX 23 H14A 2 0.398389 0.527595 0.667247 11.00000 -1.20000 H14B 2 0.158622 0.512434 0.624753 11.00000 -1.20000 AFIX 0 C15 1 0.010476 0.551440 0.822441 11.00000 0.02495 0.01555 = 0.02528 0.00073 0.00757 0.00251 C16 1 -0.047019 0.597350 0.903311 11.00000 0.03778 0.03125 = 0.03575 -0.00902 0.00666 0.01049 AFIX 137 H16A 2 -0.151903 0.579508 0.938543 11.00000 -1.50000 H16B 2 -0.101198 0.634642 0.861707 11.00000 -1.50000 H16C 2 0.074681 0.607736 0.962240 11.00000 -1.50000 AFIX 0 HKLF 4 REM 20220512mblo_diampocl2_0m_a.res in P2(1)/n REM wR2 = 0.0834, GooF = S = 1.080, Restrained GooF = 1.080 for all data REM R1 = 0.0363 for 3103 Fo > 4sig(Fo) and 0.0556 for all 3950 data REM 200 parameters refined using 0 restraints END WGHT 0.0287 1.4085 REM Highest difference peak 0.457, deepest hole -0.263, 1-sigma level 0.065 Q1 1 0.4810 0.2946 0.4752 11.00000 0.05 0.46 Q2 1 0.5607 0.3987 0.6769 11.00000 0.05 0.41 Q3 1 0.4268 0.3131 0.6802 11.00000 0.05 0.39 Q4 1 0.5479 0.4115 0.7707 11.00000 0.05 0.39 Q5 1 0.4853 0.3634 0.7222 11.00000 0.05 0.37 Q6 1 0.4041 0.4550 0.7983 11.00000 0.05 0.37 Q7 1 0.6524 0.2365 0.4537 11.00000 0.05 0.36 Q8 1 0.1781 0.3780 0.6083 11.00000 0.05 0.36 Q9 1 0.5345 0.3420 0.5274 11.00000 0.05 0.36 Q10 1 0.4605 0.4289 0.5979 11.00000 0.05 0.36 ; _shelx_res_checksum 1972 _shelx_hkl_file ; -1 0 0 -1.90 2.40 1 0 0 0.30 0.90 1 0 0 -1.30 2.10 -1 0 0 0.00 1.00 -2 0 0 96.99 4.00 -2 0 0 97.69 3.80 -2 0 0 90.69 6.70 2 0 0 93.09 3.50 -2 0 0 87.59 6.90 -3 0 0 -5.10 4.10 3 0 0 -1.90 3.10 3 0 0 0.90 4.20 -3 0 0 0.50 1.90 -3 0 0 -1.50 1.80 -3 0 0 1.60 3.60 4 0 0 901.11 31.00 -4 0 0 922.81 25.80 4 0 0 883.61 30.50 -4 0 0 898.51 30.70 -4 0 0 957.60 26.10 5 0 0 2.80 4.70 -5 0 0 -1.90 2.20 -5 0 0 -2.90 1.60 5 0 0 4.70 6.20 -5 0 0 -0.90 4.20 5 0 0 1.00 5.40 -6 0 0 0.30 2.70 -6 0 0 -11.80 6.00 6 0 0 -0.50 7.00 6 0 0 3.50 5.10 6 0 0 -0.20 5.20 -7 0 0 8.30 8.20 -7 0 0 0.30 2.60 7 0 0 3.20 8.50 7 0 0 -6.10 5.70 7 0 0 -5.00 6.10 -8 0 0 1.20 8.80 8 0 0 22.50 11.10 8 0 0 11.90 10.30 0 -1 0 0.10 0.20 0 -1 0 0.00 0.20 0 -1 0 -0.40 0.20 0 -1 0 -0.10 0.30 0 1 0 0.00 0.20 0 1 0 -0.20 0.20 0 1 0 0.20 0.30 0 1 0 -0.10 0.20 -1 -1 0 390.66 10.00 -1 -1 0 375.06 11.40 -1 -1 0 382.96 10.20 -1 -1 0 387.06 10.00 -1 -1 0 371.76 10.90 1 -1 0 297.47 10.10 1 1 0 303.97 10.00 -1 1 0 385.16 10.40 -1 1 0 375.06 11.70 1 1 0 299.97 9.60 -1 1 0 384.86 10.20 1 1 0 293.77 9.60 -2 -1 0 31.80 2.40 2 -1 0 24.20 5.20 -2 -1 0 30.60 4.10 -2 -1 0 35.50 2.50 2 -1 0 25.60 2.30 -2 -1 0 22.00 3.90 -2 1 0 25.20 2.60 -2 1 0 23.70 4.10 2 1 0 28.10 5.40 2 1 0 27.40 2.20 -2 1 0 25.70 2.30 3 -1 0 24.50 3.30 -3 -1 0 16.30 2.30 3 -1 0 18.70 1.90 -3 -1 0 19.40 4.50 3 -1 0 16.70 4.70 3 -1 0 21.60 4.70 -3 -1 0 18.70 4.80 -3 -1 0 17.30 2.40 3 1 0 19.60 4.70 -3 1 0 19.10 4.40 -3 1 0 15.50 2.50 -3 1 0 17.90 2.70 3 1 0 25.50 5.40 -3 1 0 14.60 4.30 3 1 0 17.70 5.10 -4 -1 0 271.07 9.20 -4 -1 0 277.87 13.50 -4 -1 0 270.97 8.90 4 -1 0 270.87 14.00 4 -1 0 262.67 13.20 4 -1 0 258.17 9.50 -4 1 0 277.37 9.50 4 1 0 283.37 13.80 4 1 0 272.07 13.60 -4 1 0 253.67 13.00 -4 1 0 256.87 9.20 5 -1 0 31.80 6.40 -5 -1 0 28.10 3.30 5 -1 0 23.70 7.20 5 -1 0 43.30 8.00 -5 -1 0 40.20 6.50 -5 -1 0 27.90 2.50 5 -1 0 33.70 3.40 -5 1 0 32.70 3.00 -5 1 0 31.70 6.50 5 1 0 23.50 6.10 5 1 0 26.80 7.20 -5 1 0 30.20 3.50 -5 1 0 32.80 3.00 5 1 0 30.50 6.10 6 -1 0 6.00 5.90 -6 -1 0 3.80 6.60 -6 -1 0 -0.10 2.50 6 -1 0 11.10 8.10 6 -1 0 1.00 6.80 -6 1 0 -5.80 5.10 -6 1 0 6.50 3.20 6 1 0 0.80 5.20 6 1 0 -6.10 6.80 6 1 0 5.10 5.30 7 -1 0 54.49 11.90 7 -1 0 46.20 8.70 -7 -1 0 50.39 4.20 7 -1 0 52.89 11.30 -7 -1 0 46.60 10.40 -7 1 0 45.20 10.20 7 1 0 56.19 10.00 7 1 0 36.40 10.80 -7 1 0 46.40 4.80 7 1 0 62.29 11.80 8 -1 0 23.40 10.40 -8 -1 0 26.40 9.70 8 -1 0 12.50 8.80 8 1 0 4.20 9.50 -8 1 0 18.60 2.30 -8 1 0 17.00 2.20 -8 1 0 9.30 9.30 -8 1 0 35.30 8.60 8 1 0 26.10 11.20 0 -2 0 0.50 1.00 0 -2 0 0.90 0.70 0 -2 0 -0.60 0.80 0 -2 0 0.20 1.20 0 2 0 0.10 0.70 0 2 0 -0.20 1.10 0 2 0 -0.30 0.80 0 2 0 0.00 1.00 -1 -2 0 991.80 27.20 -1 -2 0 979.50 27.10 1 -2 0 973.10 27.00 -1 -2 0 1016.80 27.00 -1 -2 0 1001.80 26.80 -1 -2 0 989.60 26.90 1 -2 0 973.10 27.20 1 2 0 955.30 27.10 1 2 0 931.51 26.70 -1 2 0 972.90 27.80 1 2 0 962.90 26.70 1 2 0 939.61 26.90 1 2 0 996.10 27.10 -1 2 0 1017.60 27.10 -1 2 0 967.70 27.20 2 -2 0 1009.30 31.40 -2 -2 0 1058.09 28.80 2 -2 0 1032.40 28.80 2 -2 0 1028.60 28.10 -2 -2 0 1024.70 28.40 -2 -2 0 1001.00 31.00 -2 -2 0 1014.10 29.90 2 2 0 1135.29 27.50 2 2 0 961.00 27.40 2 2 0 1006.00 30.60 -2 2 0 1036.20 29.00 -2 2 0 1051.29 28.80 -2 2 0 1016.70 31.10 2 2 0 1043.70 28.40 3 -2 0 155.28 9.00 -3 -2 0 144.79 6.10 -3 -2 0 154.98 6.40 3 -2 0 165.88 7.40 3 -2 0 150.58 8.40 -3 -2 0 147.89 8.80 -3 -2 0 152.98 8.70 3 -2 0 140.69 9.60 3 -2 0 153.08 6.10 3 2 0 150.38 5.20 -3 2 0 163.68 6.90 3 2 0 149.99 8.50 -3 2 0 150.58 6.60 -3 2 0 137.69 8.90 3 2 0 152.08 5.30 3 2 0 158.28 9.20 -3 2 0 141.59 8.90 4 -2 0 76.29 7.90 4 -2 0 74.59 7.80 -4 -2 0 60.09 7.00 -4 -2 0 70.29 4.40 -4 -2 0 68.59 4.30 4 -2 0 71.79 5.40 4 -2 0 62.39 7.50 -4 2 0 63.19 4.90 -4 2 0 59.09 7.10 -4 2 0 71.59 4.90 4 2 0 68.99 7.90 4 2 0 75.39 8.20 5 -2 0 41.70 8.40 -5 -2 0 49.40 3.50 5 -2 0 45.40 4.60 5 -2 0 51.59 7.80 -5 -2 0 51.09 4.00 -5 -2 0 47.00 7.60 5 -2 0 51.29 8.30 -5 2 0 56.39 4.30 -5 2 0 52.39 4.50 5 2 0 56.19 6.70 5 2 0 43.90 8.10 -5 2 0 38.80 8.30 5 2 0 52.29 7.70 -5 2 0 50.89 4.20 6 -2 0 130.79 12.10 6 -2 0 123.39 12.70 -6 -2 0 121.79 6.60 -6 -2 0 116.39 11.70 6 -2 0 146.89 14.50 -6 2 0 128.69 7.10 6 2 0 123.99 13.00 -6 2 0 111.29 12.50 6 2 0 113.19 9.40 6 2 0 135.89 13.50 -6 2 0 122.89 4.70 -6 2 0 126.59 4.80 7 -2 0 -4.90 8.90 -7 -2 0 3.20 7.30 -7 -2 0 6.50 2.80 7 -2 0 3.70 6.60 7 -2 0 -2.50 7.90 -7 2 0 10.00 9.00 -7 2 0 5.10 3.60 7 2 0 14.80 9.30 7 2 0 7.50 7.00 8 -2 0 6.20 9.80 8 -2 0 17.70 10.10 -8 -2 0 -1.50 8.00 8 -2 0 -9.20 9.20 -8 2 0 9.20 2.50 8 2 0 1.90 9.60 -8 2 0 3.60 10.10 -8 2 0 6.60 2.40 8 2 0 -3.40 9.80 -8 2 0 21.70 9.80 0 -3 0 -0.80 2.00 0 -3 0 0.50 2.30 0 -3 0 0.30 1.50 0 -3 0 -0.50 1.80 0 3 0 -1.10 1.90 0 3 0 4.80 2.50 0 3 0 2.20 1.60 0 3 0 -0.50 2.20 -1 -3 0 1627.94 44.70 -1 -3 0 1667.33 44.70 1 -3 0 1652.13 45.10 -1 -3 0 1637.34 45.00 1 -3 0 1676.83 44.80 -1 -3 0 1657.03 43.90 -1 -3 0 1567.44 44.90 1 -3 0 1586.44 45.10 -1 3 0 1651.13 45.10 1 3 0 1658.63 45.00 1 3 0 1654.83 44.50 1 3 0 1587.04 43.90 -1 3 0 1643.54 45.10 1 3 0 1641.84 45.00 -1 3 0 1623.04 45.00 -1 3 0 1625.44 44.80 2 -3 0 2364.36 62.29 2 -3 0 2242.38 64.19 2 -3 0 2374.76 61.69 -2 -3 0 2281.17 63.99 -2 -3 0 2272.47 62.09 -2 -3 0 2315.77 62.59 -2 -3 0 2301.87 61.89 -2 -3 0 2266.37 61.69 -2 3 0 2218.68 62.29 2 3 0 2288.37 61.79 2 3 0 2199.18 63.39 2 3 0 2341.67 61.19 2 3 0 2277.57 61.19 -2 3 0 2241.78 62.09 -2 3 0 2276.47 63.89 3 -3 0 1072.79 30.80 -3 -3 0 1013.80 33.10 3 -3 0 1049.89 31.90 -3 -3 0 1058.79 29.80 -3 -3 0 1058.49 31.70 3 -3 0 1020.60 33.00 3 -3 0 1076.99 29.80 3 -3 0 1026.10 33.40 3 -3 0 1060.39 30.80 -3 -3 0 1038.10 29.30 -3 3 0 1022.10 33.00 3 3 0 1018.90 29.00 -3 3 0 1022.40 30.00 3 3 0 1004.30 32.50 3 3 0 998.40 31.90 -3 3 0 1036.00 33.00 3 3 0 1031.80 28.90 -3 3 0 1071.89 29.90 4 -3 0 29.20 5.00 -4 -3 0 24.10 5.20 -4 -3 0 34.10 3.40 4 -3 0 21.40 6.20 4 -3 0 40.50 4.90 4 -3 0 40.80 6.50 -4 -3 0 21.60 3.20 4 -3 0 30.70 3.10 4 -3 0 32.10 4.80 -4 3 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23.30 4 5 0 605.64 18.20 -4 5 0 618.64 19.90 -4 5 0 609.84 19.70 -4 5 0 579.94 19.80 4 5 0 597.84 22.80 4 5 0 596.64 21.80 5 -5 0 432.26 17.70 -5 -5 0 464.85 16.10 5 -5 0 489.25 21.50 5 -5 0 480.05 17.80 -5 -5 0 470.55 16.30 -5 -5 0 495.05 19.20 5 -5 0 470.75 21.30 5 -5 0 451.95 19.80 5 5 0 476.55 16.70 -5 5 0 483.95 22.70 -5 5 0 478.45 17.00 -5 5 0 483.15 17.10 5 5 0 489.05 20.60 -5 5 0 486.75 16.80 5 5 0 470.25 21.20 6 -5 0 103.49 9.40 -6 -5 0 90.79 7.10 6 -5 0 107.89 12.40 -6 -5 0 96.79 5.30 6 -5 0 98.79 11.30 6 -5 0 83.89 11.20 -6 -5 0 93.39 9.90 -6 5 0 109.99 8.70 6 5 0 97.19 12.10 -6 5 0 85.09 12.30 6 5 0 89.59 11.30 -6 5 0 103.29 8.20 -6 5 0 103.39 7.30 -6 5 0 94.79 7.30 -7 -5 0 51.29 5.20 7 -5 0 48.10 10.50 7 -5 0 63.49 13.20 -7 -5 0 36.40 8.90 7 -5 0 45.80 10.20 7 5 0 47.00 9.70 7 5 0 40.70 10.00 -7 5 0 49.90 7.50 -7 5 0 41.80 5.80 -7 5 0 40.90 6.70 -7 5 0 38.80 11.20 -8 -5 0 5.10 2.70 8 -5 0 3.70 9.60 8 -5 0 11.20 8.70 8 -5 0 1.50 8.80 -8 -5 0 7.30 7.50 -8 5 0 19.30 10.00 8 5 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15.90 4.70 5 6 0 19.10 7.50 5 6 0 24.40 6.50 -5 6 0 16.20 4.90 -5 6 0 18.60 6.60 5 6 0 25.50 2.10 6 -6 0 348.77 18.40 -6 -6 0 348.37 16.80 6 -6 0 391.56 15.90 -6 -6 0 356.96 14.10 -6 -6 0 359.76 12.80 6 -6 0 348.27 19.90 6 -6 0 354.16 20.90 -6 6 0 358.56 15.20 -6 6 0 353.06 15.10 -6 6 0 356.56 14.60 -6 6 0 328.97 19.40 -6 6 0 349.77 14.80 6 6 0 349.17 20.00 6 6 0 361.66 18.80 7 -6 0 -6.90 7.80 7 -6 0 -5.60 7.20 7 -6 0 -2.00 7.10 -7 -6 0 3.50 3.80 -7 -6 0 -2.70 5.60 -7 6 0 14.10 9.70 7 6 0 8.60 7.60 -7 6 0 -1.00 4.80 -7 6 0 4.60 4.30 -7 6 0 2.00 3.40 7 6 0 -5.80 8.50 8 -6 0 -2.20 8.40 8 -6 0 7.40 11.40 -8 -6 0 -5.70 7.60 8 -6 0 26.10 10.70 -8 -6 0 -6.60 2.90 -8 6 0 16.50 11.30 8 6 0 13.90 10.60 -8 6 0 8.20 4.30 8 6 0 -10.20 7.60 -8 6 0 -2.60 3.90 0 -7 0 2.40 4.10 0 -7 0 0.80 3.40 0 -7 0 1.10 4.00 0 -7 0 3.60 4.80 0 7 0 8.30 4.00 0 7 0 -4.50 3.00 0 7 0 -3.40 3.00 0 7 0 9.20 5.10 1 -7 0 427.46 14.10 -1 -7 0 432.76 15.30 1 -7 0 425.46 16.20 -1 -7 0 427.26 15.20 -1 -7 0 402.36 15.70 -1 -7 0 442.06 16.00 1 -7 0 451.55 15.90 1 -7 0 434.06 16.70 1 -7 0 438.96 16.50 1 7 0 434.36 15.80 1 7 0 454.25 16.30 1 7 0 424.86 15.50 -1 7 0 442.76 15.60 1 7 0 434.16 16.40 -1 7 0 453.85 16.50 -1 7 0 437.46 15.20 -1 7 0 414.26 16.50 1 7 0 417.16 15.30 1 7 0 450.05 12.70 2 -7 0 227.08 11.30 -2 -7 0 225.98 10.20 -2 -7 0 214.58 10.70 2 -7 0 214.68 10.40 -2 -7 0 210.78 7.60 2 -7 0 223.18 10.60 2 -7 0 207.48 10.80 -2 -7 0 232.98 10.70 2 -7 0 224.08 10.70 -2 -7 0 223.98 11.40 2 7 0 218.48 10.40 2 7 0 210.68 11.00 -2 7 0 212.68 10.50 2 7 0 219.98 10.40 -2 7 0 219.28 10.80 2 7 0 220.88 9.60 2 7 0 231.28 9.50 2 7 0 220.68 8.00 2 7 0 222.08 10.70 -2 7 0 219.68 10.20 2 7 0 232.88 11.60 -2 7 0 219.98 9.90 -2 7 0 219.18 11.20 3 -7 0 249.28 10.90 3 -7 0 255.97 11.50 -3 -7 0 253.37 11.40 3 -7 0 268.17 13.10 3 -7 0 253.27 11.90 -3 -7 0 255.67 11.30 3 -7 0 276.37 10.90 -3 -7 0 244.38 12.40 3 -7 0 238.08 12.90 3 -7 0 236.98 12.70 -3 -7 0 253.67 9.80 -3 -7 0 243.98 11.10 -3 7 0 266.07 12.40 -3 7 0 265.37 8.00 3 7 0 272.07 12.80 -3 7 0 242.28 11.70 3 7 0 255.97 11.10 3 7 0 254.57 10.10 3 7 0 247.98 9.80 3 7 0 266.97 13.00 -3 7 0 264.97 11.20 -3 7 0 246.48 11.70 -3 7 0 253.87 11.60 3 7 0 244.28 11.10 4 -7 0 9.60 4.10 4 -7 0 4.30 5.10 4 -7 0 7.60 6.10 4 -7 0 1.00 4.20 -4 -7 0 1.30 3.60 4 -7 0 11.90 4.70 4 -7 0 7.80 6.20 -4 -7 0 2.90 3.10 -4 -7 0 7.80 4.20 -4 7 0 2.70 3.60 4 7 0 6.20 4.20 -4 7 0 -2.20 4.00 4 7 0 4.20 5.40 -4 7 0 4.60 4.00 4 7 0 2.90 5.50 4 7 0 1.40 1.80 -4 7 0 -0.20 5.90 4 7 0 2.70 3.90 -4 7 0 7.60 2.50 -4 7 0 4.20 3.70 4 7 0 4.80 3.20 4 7 0 -0.60 1.40 -5 -7 0 343.37 13.70 5 -7 0 319.87 15.40 5 -7 0 317.87 14.80 5 -7 0 325.67 18.20 5 -7 0 352.56 17.80 -5 -7 0 324.27 13.60 -5 -7 0 338.37 14.80 5 -7 0 308.87 15.80 -5 7 0 338.17 14.30 5 7 0 337.27 16.60 -5 7 0 323.67 14.50 5 7 0 321.27 11.50 -5 7 0 338.47 19.30 5 7 0 311.17 11.30 -5 7 0 351.06 14.20 5 7 0 300.97 15.00 -5 7 0 338.97 14.00 -5 7 0 331.27 12.70 5 7 0 332.47 17.70 -6 -7 0 4.80 3.80 6 -7 0 4.30 5.40 -6 -7 0 5.90 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12 0 276.67 13.20 3 12 0 265.37 15.50 -4 -12 0 92.99 10.00 4 -12 0 122.09 12.40 -4 -12 0 89.09 7.20 4 -12 0 101.49 8.60 -4 -12 0 102.09 6.20 4 -12 0 87.49 10.60 4 -12 0 103.69 12.70 4 -12 0 116.99 10.90 -4 -12 0 94.99 9.30 4 12 0 90.89 11.50 -4 12 0 106.09 10.40 -4 12 0 100.29 10.40 -4 12 0 97.19 9.80 4 12 0 105.69 7.90 -4 12 0 106.19 9.60 4 12 0 100.29 9.30 4 12 0 99.29 7.90 5 -12 0 190.58 17.80 -5 -12 0 194.28 12.90 -5 -12 0 194.98 10.00 5 -12 0 189.68 11.70 5 -12 0 212.38 14.90 5 -12 0 200.78 13.20 5 -12 0 188.28 15.40 -5 -12 0 212.48 13.70 -5 12 0 208.88 13.00 5 12 0 179.88 11.50 5 12 0 161.38 12.70 -5 12 0 184.28 16.60 5 12 0 205.58 15.20 -5 12 0 172.18 13.30 -5 12 0 180.58 13.60 5 12 0 182.48 14.00 6 -12 0 4.30 7.80 6 -12 0 7.60 6.30 -6 -12 0 5.40 5.60 6 -12 0 5.70 6.00 6 -12 0 8.20 7.30 6 -12 0 0.90 9.90 -6 -12 0 12.20 6.10 6 12 0 8.90 6.30 -6 12 0 21.00 9.60 -6 12 0 3.20 6.70 6 12 0 3.40 5.40 6 12 0 8.00 8.50 -6 12 0 4.30 6.20 7 -12 0 41.60 10.10 7 -12 0 40.70 10.80 7 -12 0 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-14 0.70 9.30 0 -3 14 7.70 9.80 0 3 14 9.10 10.10 0 3 -14 2.00 8.40 1 -3 14 -4.10 11.80 -1 -3 -14 3.60 9.90 -1 -3 -14 13.00 12.40 1 -3 14 -5.00 8.90 -1 3 -14 -4.20 9.70 1 3 14 1.90 10.50 -1 3 -14 0.70 12.40 -2 -3 -14 42.90 15.40 -2 3 -14 19.20 14.10 -5 -4 14 40.10 13.40 5 -4 -14 41.70 11.50 5 -4 -14 54.49 14.10 -5 4 14 75.19 14.00 5 4 -14 34.70 11.70 5 4 -14 44.70 12.70 4 -4 -14 -1.50 9.40 -4 -4 14 -1.00 7.70 -4 4 14 7.00 9.70 4 4 -14 -5.80 8.40 4 4 -14 -4.50 7.90 -3 -4 14 11.90 10.70 3 -4 -14 32.50 11.50 3 4 -14 7.20 10.60 3 4 -14 20.10 8.60 -3 4 14 26.10 11.00 -2 -4 14 13.50 10.20 2 -4 -14 32.70 12.70 2 4 -14 31.90 9.40 -2 4 14 24.50 9.20 2 4 -14 26.50 12.10 2 4 -14 26.70 9.10 1 -4 -14 9.10 7.30 -1 -4 14 14.90 10.00 1 4 -14 32.10 13.60 -1 4 14 12.40 10.50 1 4 -14 12.30 6.90 1 4 -14 13.60 7.00 0 -4 14 245.28 20.10 0 -4 -14 236.88 18.50 0 -4 -14 370.46 26.90 0 4 -14 342.17 26.70 0 4 14 270.87 19.80 0 4 -14 235.08 19.40 1 -4 14 -5.20 8.80 -1 -4 -14 -6.80 9.60 1 -4 14 -15.70 11.30 -1 4 -14 4.90 7.40 -5 -5 14 9.00 11.20 5 -5 -14 16.00 9.50 5 -5 -14 -1.50 8.10 5 5 -14 6.10 9.30 -5 5 14 11.90 10.90 5 5 -14 14.70 9.30 -4 -5 14 51.69 13.50 4 -5 -14 72.19 14.00 4 5 -14 55.79 11.70 4 5 -14 74.89 13.20 -4 5 14 66.29 11.90 -3 -5 14 53.69 12.70 3 -5 -14 74.89 14.50 3 5 -14 67.89 14.30 -3 5 14 71.49 13.20 3 5 -14 74.49 11.60 2 -5 -14 40.00 12.90 -2 -5 14 27.40 11.00 2 5 -14 21.10 12.40 2 5 -14 17.90 7.50 -2 5 14 26.70 11.70 2 5 -14 18.80 8.90 1 -5 -14 37.80 11.80 -1 -5 14 52.79 12.10 -1 5 14 78.59 14.10 1 5 -14 56.39 10.00 1 5 -14 75.59 12.40 1 5 -14 62.79 15.40 0 -5 14 187.28 19.80 0 -5 14 211.38 19.50 0 -5 -14 199.88 22.40 0 -5 -14 206.78 19.70 0 5 14 200.68 20.10 0 5 -14 201.88 22.40 0 5 -14 194.38 18.20 1 -5 14 294.07 23.90 -1 -5 -14 290.27 21.90 -1 -5 -14 269.37 26.10 1 -5 14 269.77 20.80 -1 5 -14 271.17 24.90 -1 5 -14 246.78 21.00 -5 -6 14 61.59 13.90 5 -6 -14 75.19 15.20 5 -6 -14 69.69 13.90 5 6 -14 96.69 14.60 5 6 -14 112.99 15.60 -5 6 14 87.49 14.40 4 -6 -14 42.70 10.90 -4 -6 14 45.20 11.00 4 6 -14 27.80 9.70 4 6 -14 37.50 11.10 -4 6 14 38.00 10.00 3 -6 -14 44.90 13.30 -3 -6 14 42.30 12.20 -3 6 14 46.10 12.40 3 6 -14 95.39 15.50 3 6 -14 52.69 10.90 -3 6 14 48.60 11.60 -2 -6 14 7.60 7.60 2 -6 -14 14.90 9.30 2 6 -14 4.40 7.30 -2 6 14 18.60 10.70 2 6 -14 17.40 12.40 -2 6 14 -2.40 9.70 2 6 -14 18.60 8.20 1 -6 -14 9.70 9.70 -1 -6 14 17.40 10.10 1 6 -14 6.50 9.00 1 6 -14 37.30 12.70 1 6 -14 10.90 8.40 -1 6 14 -1.60 10.20 0 -6 -14 6.40 9.50 0 -6 14 1.80 9.20 0 -6 -14 49.60 15.30 0 -6 14 -5.80 10.60 0 6 -14 -1.70 6.30 0 6 14 4.50 10.30 0 6 -14 -1.00 12.20 -1 -6 -14 56.19 11.80 1 -6 14 64.99 13.00 1 -6 14 72.89 15.70 -1 -6 -14 165.98 21.00 -1 6 -14 41.60 13.00 -1 6 -14 62.89 13.30 -4 -7 14 28.30 12.10 4 -7 -14 30.50 12.70 4 7 -14 9.10 9.50 -4 7 14 12.00 8.30 4 7 -14 25.70 10.40 -3 -7 14 56.89 13.00 3 -7 -14 53.89 13.60 3 7 -14 42.00 9.40 -3 7 14 50.99 11.90 3 7 -14 23.90 11.50 -3 7 14 60.99 13.10 -2 -7 14 -8.30 8.80 2 -7 -14 6.70 11.50 2 7 -14 3.60 11.50 -2 7 14 9.80 10.40 2 7 -14 7.10 6.60 -2 7 14 -9.70 9.90 2 7 -14 4.00 7.00 -1 -7 14 324.17 21.80 -1 -7 14 349.17 23.10 1 -7 -14 265.47 25.50 1 7 -14 301.77 19.90 -1 7 14 340.17 23.70 1 7 -14 338.77 26.00 -1 7 14 343.67 23.80 0 -7 -14 0.30 11.80 0 -7 14 -10.30 10.80 0 -7 -14 0.00 6.90 0 -7 14 -2.80 9.10 0 7 -14 11.10 12.60 0 7 14 -2.10 12.60 0 7 -14 -7.40 8.20 0 7 14 -2.80 7.50 1 -7 14 6.60 12.40 -1 -7 -14 48.40 15.20 1 -7 14 -9.50 9.40 1 -7 14 19.60 10.00 -1 -7 -14 -5.70 9.90 -1 7 -14 6.10 9.40 -1 7 -14 4.10 9.80 -4 -8 14 77.39 13.10 4 -8 -14 99.19 14.50 4 8 -14 78.89 12.50 -4 8 14 87.39 13.90 4 8 -14 124.29 14.90 -3 -8 14 99.39 15.70 3 -8 -14 75.69 13.90 -3 8 14 117.29 15.60 3 8 -14 91.99 12.50 -3 8 14 88.99 14.40 3 8 -14 95.39 19.60 2 -8 -14 14.90 12.30 -2 -8 14 3.30 7.70 2 8 -14 22.40 12.70 2 8 -14 21.90 8.50 -2 8 14 2.10 9.90 -2 8 14 9.70 10.60 1 -8 -14 -1.60 12.60 -1 -8 14 5.80 10.70 -1 -8 14 -2.40 9.10 -1 8 14 4.20 12.00 -1 8 14 13.00 8.50 1 8 -14 5.30 9.30 1 8 -14 9.30 8.30 0 -8 14 4.50 11.60 0 -8 14 -7.70 5.80 0 -8 -14 4.50 9.50 0 -8 -14 8.90 10.30 0 8 -14 16.80 10.90 0 8 -14 -11.80 8.00 0 8 14 2.50 8.00 0 8 14 21.90 13.60 1 -8 14 17.20 13.90 1 -8 14 57.69 12.90 1 -8 14 37.70 11.30 -1 -8 -14 74.09 15.90 -1 -8 -14 79.39 15.10 -1 8 -14 44.80 12.60 -1 8 -14 57.09 15.90 4 -9 -14 36.10 13.30 -4 -9 14 67.19 15.00 -4 9 14 16.50 10.50 -4 9 14 48.80 11.60 4 9 -14 31.50 10.70 4 9 -14 41.40 10.50 3 -9 -14 28.60 13.50 -3 -9 14 13.60 10.80 -3 9 14 44.60 12.90 3 9 -14 58.99 11.90 -3 9 14 63.49 13.00 -2 -9 14 121.89 15.90 2 -9 -14 136.09 19.30 -2 -9 14 116.29 15.90 -2 9 14 121.39 17.20 2 9 -14 138.29 19.10 2 9 -14 134.69 14.10 -2 9 14 135.39 17.60 -1 -9 14 24.00 11.70 1 -9 -14 0.10 12.50 -1 -9 14 21.50 10.50 -1 9 14 32.20 14.50 -1 9 14 15.80 9.00 1 9 -14 12.50 8.50 1 9 -14 5.60 9.60 0 -9 14 61.39 12.70 0 -9 14 33.70 13.30 0 -9 -14 60.19 16.30 0 9 14 64.49 16.90 0 9 -14 57.59 13.90 0 9 -14 60.59 12.00 1 -9 14 4.70 12.80 1 -9 14 11.80 9.60 1 -9 14 5.60 9.40 -1 -9 -14 6.70 8.40 -1 -9 -14 9.50 10.60 -1 9 -14 41.80 14.90 -1 9 -14 9.60 9.90 4 -10 -14 119.09 17.90 -4 -10 14 114.79 16.70 -4 10 14 113.19 15.30 4 10 -14 96.49 14.00 -4 10 14 131.19 16.50 4 10 -14 104.39 13.30 -3 -10 14 -7.00 8.40 3 -10 -14 8.30 12.70 -3 -10 14 -13.10 9.20 -3 10 14 16.20 10.40 3 10 -14 0.60 8.20 -3 10 14 11.50 11.10 2 -10 -14 13.10 12.30 -2 -10 14 -0.90 10.10 -2 -10 14 5.30 9.30 -2 10 14 7.00 10.80 2 10 -14 4.50 12.30 2 10 -14 7.10 7.00 -2 10 14 24.80 12.20 -1 -10 14 -0.80 9.50 -1 -10 14 18.00 11.70 1 -10 -14 0.20 12.50 -1 10 14 8.20 11.60 -1 10 14 2.60 8.10 1 10 -14 7.70 8.20 1 10 -14 16.30 13.30 0 -10 14 3.80 12.20 0 -10 14 -0.50 8.90 0 -10 -14 10.80 13.80 0 10 14 -4.60 12.90 0 10 -14 -2.60 12.80 0 10 -14 -6.20 8.20 -3 -11 14 -0.10 9.90 -3 -11 14 5.20 10.20 -3 11 14 29.40 12.00 -3 11 14 8.90 10.90 -2 -11 14 2.70 9.40 -2 -11 14 -22.30 10.60 2 -11 -14 -16.10 8.00 -2 11 14 19.40 11.80 2 11 -14 13.50 7.50 -2 11 14 -2.00 10.30 2 11 -14 2.20 12.20 1 -11 -14 90.49 16.40 -1 -11 14 83.19 14.00 -1 -11 14 69.99 15.20 -1 11 14 88.09 17.60 -1 11 14 60.69 14.20 1 11 -14 66.09 16.60 1 11 -14 81.19 11.90 0 -11 14 23.20 10.90 0 -11 14 33.60 11.80 0 -11 -14 21.20 15.20 0 -11 14 35.50 13.30 0 11 -14 24.90 10.30 0 11 -14 24.00 15.30 0 11 14 4.80 14.10 -3 -12 14 56.49 13.40 -3 12 14 59.69 13.60 -3 12 14 54.29 14.20 -2 -12 14 1.10 9.80 2 -12 -14 -27.40 11.10 -2 -12 14 -0.70 11.70 -2 12 14 -6.10 11.40 -2 12 14 -2.70 10.60 2 12 -14 13.70 12.80 -1 -12 14 10.40 9.40 1 -12 -14 -7.80 12.80 -1 -12 14 12.20 12.60 -1 12 14 13.20 13.20 1 12 -14 -7.10 12.80 1 12 -14 -14.50 7.20 -4 0 15 13.60 11.20 4 0 -15 -3.80 9.60 3 0 -15 21.20 12.10 -3 0 15 27.90 12.00 3 0 -15 42.90 11.20 2 0 -15 -1.10 11.50 -2 0 15 -15.00 6.50 1 0 -15 -8.90 8.50 1 0 -15 -13.40 8.30 -1 0 15 -0.40 8.00 0 0 15 4.10 10.50 0 0 -15 22.60 14.20 0 0 -15 -6.20 9.70 4 -1 -15 5.80 10.20 -4 -1 15 4.10 11.40 4 1 -15 2.30 9.60 4 1 -15 13.90 8.50 -4 1 15 5.60 8.30 -3 -1 15 81.89 13.40 3 -1 -15 64.09 12.80 -3 1 15 61.69 13.80 3 1 -15 76.59 12.50 3 1 -15 111.59 23.60 -2 -1 15 29.00 11.60 2 -1 -15 16.60 13.20 2 1 -15 31.40 13.80 -2 1 15 20.50 11.50 2 1 -15 29.10 10.40 -1 -1 15 108.99 16.80 1 -1 -15 141.29 15.50 1 -1 -15 131.89 18.00 1 1 -15 131.49 18.20 -1 1 15 146.09 18.40 1 1 -15 127.49 14.80 0 -1 15 -1.30 10.20 0 -1 -15 25.10 14.50 0 -1 -15 20.30 9.10 0 1 -15 2.50 9.30 0 1 15 7.40 11.60 0 1 -15 43.80 15.30 -4 -2 15 -6.60 7.70 4 -2 -15 13.50 10.00 4 2 -15 4.50 10.00 -4 2 15 -0.60 10.80 4 2 -15 -5.80 8.70 -3 -2 15 109.09 16.20 3 -2 -15 67.59 13.10 -3 2 15 97.19 14.10 3 2 -15 95.29 13.20 -2 -2 15 2.70 10.40 2 -2 -15 -1.40 8.30 2 2 -15 14.10 12.90 -2 2 15 -1.00 10.40 2 2 -15 -2.90 8.50 -1 -2 15 27.10 12.30 1 -2 -15 46.10 12.60 1 -2 -15 120.89 17.80 -1 2 15 54.29 14.00 1 2 -15 38.70 11.70 1 2 -15 33.10 11.80 0 -2 15 35.40 10.50 0 -2 -15 52.09 16.10 0 -2 -15 23.70 11.90 0 2 -15 24.10 14.50 0 2 15 42.00 13.60 0 2 -15 34.40 11.70 -4 -3 15 34.70 13.10 4 -3 -15 12.30 11.20 4 3 -15 16.20 10.90 4 3 -15 -2.30 9.20 -4 3 15 13.10 11.60 -3 -3 15 -3.90 10.30 3 -3 -15 14.10 9.50 -3 3 15 3.80 10.50 3 3 -15 17.20 9.30 2 -3 -15 32.30 11.50 -2 -3 15 30.00 12.20 2 3 -15 36.00 14.10 -2 3 15 20.80 11.70 2 3 -15 37.80 10.60 1 -3 -15 118.99 14.90 -1 -3 15 175.08 18.70 1 -3 -15 123.69 19.00 1 3 -15 109.29 16.80 -1 3 15 124.99 15.90 1 3 -15 103.59 14.80 0 -3 -15 2.80 10.30 0 -3 15 -1.40 10.00 0 -3 -15 -6.20 8.80 0 3 15 -6.30 7.90 0 3 -15 -3.50 12.80 0 3 -15 5.70 9.90 4 -4 -15 1.30 10.40 -4 -4 15 17.90 11.50 -4 4 15 10.20 11.30 4 4 -15 0.10 9.00 4 4 -15 5.70 9.50 -3 -4 15 75.29 13.20 3 -4 -15 92.69 15.10 -3 4 15 98.59 16.00 -2 -4 15 9.70 11.50 2 -4 -15 34.00 14.20 -2 4 15 12.20 9.30 2 4 -15 14.80 8.40 2 4 -15 41.90 14.70 1 -4 -15 36.00 14.80 -1 -4 15 8.40 10.70 1 4 -15 -4.40 6.70 -1 4 15 7.60 10.90 1 4 -15 12.20 10.90 1 4 -15 22.50 10.00 0 -4 15 11.30 8.30 0 -4 -15 22.40 11.00 0 -4 -15 7.90 9.70 0 4 15 14.20 11.90 0 4 -15 -12.10 12.20 0 4 -15 -3.20 9.10 -3 -5 15 191.58 20.20 -3 5 15 244.88 22.50 3 5 -15 182.38 16.70 -2 -5 15 24.50 11.50 -2 5 15 24.20 12.10 2 5 -15 34.20 10.90 -1 -5 15 12.20 10.30 1 -5 -15 0.60 13.30 1 5 -15 -5.40 8.70 -1 5 15 8.70 11.30 1 5 -15 -4.90 8.60 0 -5 -15 -3.40 9.50 0 -5 15 -10.80 9.80 0 -5 -15 18.40 10.80 0 -5 15 0.00 11.60 0 5 -15 7.70 10.80 0 5 -15 2.50 9.80 0 5 15 22.00 12.40 -3 -6 15 237.38 20.90 -3 6 15 212.58 21.10 3 6 -15 220.28 17.60 2 -6 -15 177.88 21.80 -2 -6 15 195.58 19.80 -2 6 15 174.78 20.00 2 6 -15 199.18 22.50 1 -6 -15 -16.60 11.50 -1 -6 15 -4.90 9.30 1 6 -15 -11.90 7.90 1 6 -15 20.80 11.20 -1 6 15 -11.10 9.80 -3 -7 15 34.50 12.60 3 7 -15 63.79 11.40 -3 7 15 46.90 12.90 -2 -7 15 8.60 10.50 2 -7 -15 40.90 14.60 -2 7 15 7.10 11.60 2 7 -15 -1.20 7.70 2 7 -15 36.20 14.30 -1 -7 15 16.30 10.50 1 -7 -15 28.30 14.00 -1 -7 15 6.00 13.30 1 7 -15 -0.10 8.20 1 7 -15 -5.20 12.40 -1 7 15 5.00 8.70 -2 -8 15 81.29 14.80 -2 -8 15 94.79 15.50 2 -8 -15 88.59 18.00 -2 8 15 99.79 17.30 -2 8 15 117.79 17.60 2 8 -15 92.09 13.00 2 8 -15 128.19 19.70 -1 -8 15 -10.80 8.70 1 -8 -15 35.10 14.50 1 8 -15 -7.00 13.10 -1 8 15 -1.40 10.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 99079 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.78995(7) 0.23024(2) 0.49055(4) 0.02224(12) Uani 1 1 d . . . . . Cl2 Cl 0.54270(10) 0.30584(3) 0.28397(5) 0.03711(16) Uani 1 1 d . . . . . S1 S 0.25635(8) 0.51909(2) 0.87639(4) 0.02203(13) Uani 1 1 d . . . . . P1 P 0.50329(8) 0.26142(2) 0.42411(5) 0.01996(13) Uani 1 1 d . . . . . O1 O 0.3543(2) 0.21157(7) 0.39725(14) 0.0314(4) Uani 1 1 d . . . . . O2 O -0.1013(2) 0.53900(7) 0.73220(13) 0.0236(3) Uani 1 1 d . . . . . C1 C 0.4539(3) 0.31974(9) 0.52081(16) 0.0145(4) Uani 1 1 d . . . . . C2 C 0.6130(3) 0.37173(9) 0.53833(16) 0.0144(4) Uani 1 1 d . . . . . H2A H 0.751577 0.354784 0.569455 0.017 Uiso 1 1 calc R U . . . H2B H 0.613121 0.391596 0.464777 0.017 Uiso 1 1 calc R U . . . C3 C 0.5597(3) 0.41910(9) 0.62053(16) 0.0138(4) Uani 1 1 d . . . . . H3 H 0.663311 0.453002 0.631557 0.017 Uiso 1 1 calc R U . . . C4 C 0.5627(3) 0.38898(9) 0.73559(16) 0.0132(4) Uani 1 1 d . . . . . H4 H 0.702485 0.371779 0.767317 0.016 Uiso 1 1 calc R U . . . C5 C 0.4053(3) 0.33636(8) 0.71782(16) 0.0134(4) Uani 1 1 d . . . . . H5 H 0.408268 0.316232 0.792432 0.016 Uiso 1 1 calc R U . . . C6 C 0.4567(3) 0.28839(8) 0.63569(16) 0.0148(4) Uani 1 1 d . . . . . H6A H 0.354622 0.254697 0.624898 0.018 Uiso 1 1 calc R U . . . H6B H 0.593950 0.270626 0.667205 0.018 Uiso 1 1 calc R U . . . C7 C 0.2377(3) 0.34644(9) 0.47172(16) 0.0161(4) Uani 1 1 d . . . . . H7A H 0.234126 0.366409 0.397822 0.019 Uiso 1 1 calc R U . . . H7B H 0.134599 0.313005 0.459564 0.019 Uiso 1 1 calc R U . . . C8 C 0.1908(3) 0.36359(9) 0.67122(16) 0.0144(4) Uani 1 1 d . . . . . H8 H 0.087082 0.329738 0.660506 0.017 Uiso 1 1 calc R U . . . C9 C 0.1875(3) 0.39360(9) 0.55553(16) 0.0141(4) Uani 1 1 d . . . . . H9 H 0.047767 0.410890 0.524077 0.017 Uiso 1 1 calc R U . . . C10 C 0.3450(3) 0.44627(8) 0.57336(16) 0.0133(4) Uani 1 1 d . . . . . H10 H 0.342310 0.466482 0.498848 0.016 Uiso 1 1 calc R U . . . C11 C 0.5116(3) 0.43650(9) 0.81894(16) 0.0161(4) Uani 1 1 d . . . . . H11A H 0.614906 0.469873 0.831103 0.019 Uiso 1 1 calc R U . . . H11B H 0.514649 0.416698 0.892928 0.019 Uiso 1 1 calc R U . . . C12 C 0.1387(3) 0.41112(9) 0.75410(17) 0.0160(4) Uani 1 1 d . . . . . H12A H -0.000618 0.427789 0.723909 0.019 Uiso 1 1 calc R U . . . H12B H 0.141006 0.391364 0.828042 0.019 Uiso 1 1 calc R U . . . C13 C 0.2965(3) 0.46333(9) 0.76990(16) 0.0148(4) Uani 1 1 d . . . . . C14 C 0.2952(3) 0.49421(9) 0.65621(16) 0.0161(4) Uani 1 1 d . . . . . H14A H 0.398389 0.527595 0.667247 0.019 Uiso 1 1 calc R U . . . H14B H 0.158622 0.512434 0.624753 0.019 Uiso 1 1 calc R U . . . C15 C 0.0105(3) 0.55144(9) 0.82244(19) 0.0216(4) Uani 1 1 d . . . . . C16 C -0.0470(4) 0.59735(11) 0.9033(2) 0.0352(6) Uani 1 1 d . . . . . H16A H -0.151903 0.579508 0.938543 0.053 Uiso 1 1 calc R U . . . H16B H -0.101198 0.634642 0.861707 0.053 Uiso 1 1 calc R U . . . H16C H 0.074681 0.607736 0.962240 0.053 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0227(2) 0.0248(3) 0.0197(3) -0.0038(2) 0.0058(2) 0.0021(2) Cl2 0.0575(4) 0.0417(4) 0.0128(3) 0.0016(2) 0.0092(3) 0.0100(3) S1 0.0243(3) 0.0224(3) 0.0171(3) -0.0045(2) -0.0001(2) 0.0045(2) P1 0.0232(3) 0.0207(3) 0.0142(3) -0.0046(2) 0.0005(2) -0.0007(2) O1 0.0297(8) 0.0265(8) 0.0333(10) -0.0152(7) -0.0025(7) -0.0048(7) O2 0.0227(7) 0.0208(8) 0.0245(8) -0.0011(6) -0.0005(6) 0.0025(6) C1 0.0154(9) 0.0147(9) 0.0125(9) -0.0009(7) 0.0011(7) -0.0023(7) C2 0.0128(8) 0.0172(10) 0.0126(10) 0.0026(8) 0.0016(7) -0.0029(7) C3 0.0133(9) 0.0136(9) 0.0133(10) 0.0011(7) 0.0002(7) -0.0050(7) C4 0.0113(8) 0.0159(9) 0.0108(9) 0.0011(7) -0.0005(7) -0.0006(7) C5 0.0151(8) 0.0138(9) 0.0108(9) 0.0039(7) 0.0021(7) -0.0016(7) C6 0.0149(9) 0.0139(9) 0.0152(10) 0.0011(7) 0.0026(8) -0.0017(7) C7 0.0154(9) 0.0176(10) 0.0127(10) 0.0004(8) -0.0022(7) -0.0033(7) C8 0.0121(8) 0.0142(9) 0.0163(10) 0.0021(8) 0.0021(7) -0.0036(7) C9 0.0113(8) 0.0147(9) 0.0137(10) 0.0029(7) -0.0026(7) -0.0009(7) C10 0.0147(8) 0.0136(9) 0.0100(9) 0.0037(7) -0.0008(7) -0.0014(7) C11 0.0164(9) 0.0189(10) 0.0110(9) 0.0006(8) -0.0007(7) -0.0006(8) C12 0.0151(9) 0.0183(10) 0.0148(10) 0.0033(8) 0.0038(8) 0.0005(7) C13 0.0164(9) 0.0145(9) 0.0126(9) -0.0019(7) 0.0013(7) 0.0010(7) C14 0.0171(9) 0.0124(9) 0.0165(10) 0.0027(8) -0.0008(7) -0.0005(7) C15 0.0250(10) 0.0156(10) 0.0253(12) 0.0007(9) 0.0076(9) 0.0025(8) C16 0.0378(13) 0.0313(13) 0.0357(14) -0.0090(11) 0.0067(11) 0.0105(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C15 S1 C13 105.95(9) . . ? O1 P1 C1 116.76(9) . . ? O1 P1 Cl2 112.36(8) . . ? C1 P1 Cl2 106.63(7) . . ? O1 P1 Cl1 112.24(7) . . ? C1 P1 Cl1 105.88(7) . . ? Cl2 P1 Cl1 101.66(3) . . ? C2 C1 C6 109.51(15) . . ? C2 C1 C7 109.61(15) . . ? C6 C1 C7 109.33(15) . . ? C2 C1 P1 112.60(13) . . ? C6 C1 P1 107.87(13) . . ? C7 C1 P1 107.86(13) . . ? C3 C2 C1 109.28(15) . . ? C3 C2 H2A 109.8 . . ? C1 C2 H2A 109.8 . . ? C3 C2 H2B 109.8 . . ? C1 C2 H2B 109.8 . . ? H2A C2 H2B 108.3 . . ? C2 C3 C4 110.23(15) . . ? C2 C3 C10 110.63(15) . . ? C4 C3 C10 108.66(15) . . ? C2 C3 H3 109.1 . . ? C4 C3 H3 109.1 . . ? C10 C3 H3 109.1 . . ? C3 C4 C11 110.47(15) . . ? C3 C4 C5 108.83(15) . . ? C11 C4 C5 110.23(15) . . ? C3 C4 H4 109.1 . . ? C11 C4 H4 109.1 . . ? C5 C4 H4 109.1 . . ? C6 C5 C8 110.60(15) . . ? C6 C5 C4 110.52(15) . . ? C8 C5 C4 108.53(15) . . ? C6 C5 H5 109.1 . . ? C8 C5 H5 109.1 . . ? C4 C5 H5 109.1 . . ? C5 C6 C1 108.95(15) . . ? C5 C6 H6A 109.9 . . ? C1 C6 H6A 109.9 . . ? C5 C6 H6B 109.9 . . ? C1 C6 H6B 109.9 . . ? H6A C6 H6B 108.3 . . ? C9 C7 C1 108.81(15) . . ? C9 C7 H7A 109.9 . . ? C1 C7 H7A 109.9 . . ? C9 C7 H7B 109.9 . . ? C1 C7 H7B 109.9 . . ? H7A C7 H7B 108.3 . . ? C12 C8 C5 110.54(15) . . ? C12 C8 C9 110.50(15) . . ? C5 C8 C9 108.49(15) . . ? C12 C8 H8 109.1 . . ? C5 C8 H8 109.1 . . ? C9 C8 H8 109.1 . . ? C7 C9 C10 110.23(15) . . ? C7 C9 C8 110.98(15) . . ? C10 C9 C8 108.62(15) . . ? C7 C9 H9 109.0 . . ? C10 C9 H9 109.0 . . ? C8 C9 H9 109.0 . . ? C14 C10 C9 110.76(15) . . ? C14 C10 C3 109.92(15) . . ? C9 C10 C3 108.58(15) . . ? C14 C10 H10 109.2 . . ? C9 C10 H10 109.2 . . ? C3 C10 H10 109.2 . . ? C4 C11 C13 109.18(15) . . ? C4 C11 H11A 109.8 . . ? C13 C11 H11A 109.8 . . ? C4 C11 H11B 109.8 . . ? C13 C11 H11B 109.8 . . ? H11A C11 H11B 108.3 . . ? C13 C12 C8 109.19(15) . . ? C13 C12 H12A 109.8 . . ? C8 C12 H12A 109.8 . . ? C13 C12 H12B 109.8 . . ? C8 C12 H12B 109.8 . . ? H12A C12 H12B 108.3 . . ? C14 C13 C12 110.45(16) . . ? C14 C13 C11 109.10(16) . . ? C12 C13 C11 108.93(15) . . ? C14 C13 S1 111.74(13) . . ? C12 C13 S1 111.81(13) . . ? C11 C13 S1 104.59(13) . . ? C13 C14 C10 109.39(15) . . ? C13 C14 H14A 109.8 . . ? C10 C14 H14A 109.8 . . ? C13 C14 H14B 109.8 . . ? C10 C14 H14B 109.8 . . ? H14A C14 H14B 108.2 . . ? O2 C15 C16 122.6(2) . . ? O2 C15 S1 125.31(16) . . ? C16 C15 S1 112.05(16) . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 P1 2.0219(7) . ? Cl2 P1 2.0208(8) . ? S1 C15 1.773(2) . ? S1 C13 1.834(2) . ? P1 O1 1.4591(16) . ? P1 C1 1.807(2) . ? O2 C15 1.207(3) . ? C1 C2 1.534(2) . ? C1 C6 1.545(3) . ? C1 C7 1.548(3) . ? C2 C3 1.529(3) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.535(3) . ? C3 C10 1.539(2) . ? C3 H3 1.0000 . ? C4 C11 1.536(3) . ? C4 C5 1.537(2) . ? C4 H4 1.0000 . ? C5 C6 1.533(3) . ? C5 C8 1.537(2) . ? C5 H5 1.0000 . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C7 C9 1.532(3) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C8 C12 1.535(3) . ? C8 C9 1.541(3) . ? C8 H8 1.0000 . ? C9 C10 1.538(2) . ? C9 H9 1.0000 . ? C10 C14 1.535(3) . ? C10 H10 1.0000 . ? C11 C13 1.542(3) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C12 C13 1.533(3) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 C14 1.530(3) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 C16 1.508(3) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 P1 C1 C2 -176.89(13) . . . . ? Cl2 P1 C1 C2 -50.36(14) . . . . ? Cl1 P1 C1 C2 57.36(14) . . . . ? O1 P1 C1 C6 62.16(15) . . . . ? Cl2 P1 C1 C6 -171.31(10) . . . . ? Cl1 P1 C1 C6 -63.59(12) . . . . ? O1 P1 C1 C7 -55.83(16) . . . . ? Cl2 P1 C1 C7 70.71(13) . . . . ? Cl1 P1 C1 C7 178.43(11) . . . . ? C6 C1 C2 C3 -60.24(19) . . . . ? C7 C1 C2 C3 59.7(2) . . . . ? P1 C1 C2 C3 179.75(12) . . . . ? C1 C2 C3 C4 60.44(19) . . . . ? C1 C2 C3 C10 -59.77(19) . . . . ? C2 C3 C4 C11 179.39(14) . . . . ? C10 C3 C4 C11 -59.22(19) . . . . ? C2 C3 C4 C5 -59.46(18) . . . . ? C10 C3 C4 C5 61.93(19) . . . . ? C3 C4 C5 C6 59.31(19) . . . . ? C11 C4 C5 C6 -179.39(15) . . . . ? C3 C4 C5 C8 -62.13(19) . . . . ? C11 C4 C5 C8 59.16(19) . . . . ? C8 C5 C6 C1 60.59(19) . . . . ? C4 C5 C6 C1 -59.62(19) . . . . ? C2 C1 C6 C5 59.72(19) . . . . ? C7 C1 C6 C5 -60.38(19) . . . . ? P1 C1 C6 C5 -177.41(12) . . . . ? C2 C1 C7 C9 -60.1(2) . . . . ? C6 C1 C7 C9 59.93(19) . . . . ? P1 C1 C7 C9 176.97(12) . . . . ? C6 C5 C8 C12 179.42(15) . . . . ? C4 C5 C8 C12 -59.18(19) . . . . ? C6 C5 C8 C9 -59.27(19) . . . . ? C4 C5 C8 C9 62.13(19) . . . . ? C1 C7 C9 C10 60.50(19) . . . . ? C1 C7 C9 C8 -59.89(19) . . . . ? C12 C8 C9 C7 -179.54(14) . . . . ? C5 C8 C9 C7 59.13(19) . . . . ? C12 C8 C9 C10 59.12(18) . . . . ? C5 C8 C9 C10 -62.21(19) . . . . ? C7 C9 C10 C14 179.39(15) . . . . ? C8 C9 C10 C14 -58.81(19) . . . . ? C7 C9 C10 C3 -59.82(19) . . . . ? C8 C9 C10 C3 61.98(19) . . . . ? C2 C3 C10 C14 -179.35(15) . . . . ? C4 C3 C10 C14 59.51(19) . . . . ? C2 C3 C10 C9 59.35(19) . . . . ? C4 C3 C10 C9 -61.79(19) . . . . ? C3 C4 C11 C13 59.80(19) . . . . ? C5 C4 C11 C13 -60.5(2) . . . . ? C5 C8 C12 C13 60.51(19) . . . . ? C9 C8 C12 C13 -59.60(19) . . . . ? C8 C12 C13 C14 59.32(19) . . . . ? C8 C12 C13 C11 -60.5(2) . . . . ? C8 C12 C13 S1 -175.58(12) . . . . ? C4 C11 C13 C14 -60.0(2) . . . . ? C4 C11 C13 C12 60.7(2) . . . . ? C4 C11 C13 S1 -179.67(13) . . . . ? C15 S1 C13 C14 61.70(15) . . . . ? C15 S1 C13 C12 -62.68(15) . . . . ? C15 S1 C13 C11 179.60(13) . . . . ? C12 C13 C14 C10 -58.97(19) . . . . ? C11 C13 C14 C10 60.73(19) . . . . ? S1 C13 C14 C10 175.89(12) . . . . ? C9 C10 C14 C13 59.02(19) . . . . ? C3 C10 C14 C13 -60.97(19) . . . . ? C13 S1 C15 O2 -1.5(2) . . . . ? C13 S1 C15 C16 178.35(16) . . . . ?