Crystallography Open Database

Information card for entry 1573692

Preview

Coordinates	1573692.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H45 N O5 Si2
Calculated formula	C24 H45 N O5 Si2
Title of publication	Total synthesis of (-)-flueggenine A and (-)-15'-<i>epi</i>-flueggenine D.
Authors of publication	Seo, Seung Mo; Kim, Dongwook; Kim, Taewan; Han, Sunkyu
Journal of publication	Chemical science
Year of publication	2025
Journal volume	16
Journal issue	3
Pages of publication	1216 - 1221
a	6.8112 ± 0.0003 Å
b	9.0531 ± 0.0004 Å
c	23.2935 ± 0.001 Å
α	90°
β	95.8682 ± 0.0016°
γ	90°
Cell volume	1428.81 ± 0.11 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0423
Residual factor for significantly intense reflections	0.0372
Weighted residual factors for significantly intense reflections	0.0882
Weighted residual factors for all reflections included in the refinement	0.0902
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
298163 (current)	2025-03-04	cif/ Updating files of 1573690, 1573691, 1573692, 1573693, 1573694 Original log message: Adding full bibliography for 1573690--1573694.cif.	1573692.cif
297334	2025-01-16	cif/ Adding structures of 1573690, 1573691, 1573692, 1573693, 1573694 via cif-deposit CGI script.	1573692.cif