#------------------------------------------------------------------------------ #$Date: 2025-01-18 01:05:02 +0200 (Sat, 18 Jan 2025) $ #$Revision: 297368 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/37/1573706.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573706 _journal_paper_doi 10.1039/D4SC08530B _chemical_formula_moiety 'C15 H15 N3 O S' _chemical_formula_sum 'C15 H15 N3 O S' _chemical_formula_weight 285.36 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_method ;FinalCif V137 by Daniel Kratzert, Freiburg 2024, https://dkratzert.de/finalcif.html ; _audit_update_record ; 2024-05-24 deposited with the CCDC. 2025-01-09 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 98.52(2) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 9.889(8) _cell_length_b 23.89(2) _cell_length_c 12.335(10) _cell_measurement_reflns_used 9948 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.8315 _cell_measurement_theta_min 2.25 _cell_volume 2882(4) _computing_cell_refinement 'SAINT V8.40B' _computing_data_collection 'Bruker BIS 2018.9.0.3/05-Dec-2018 and APEX5_2023.9-2' _computing_data_reduction 'SAINT V8.40B' _computing_structure_refinement 'SHELXL-2019/2 (Sheldrick, 2019)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(2) _diffrn_detector CCD _diffrn_detector_area_resol_mean 8.3 _diffrn_detector_type 'Bruker APEXII' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker APEX2 QUAZAR' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0551 _diffrn_reflns_av_unetI/netI 0.0347 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 33 _diffrn_reflns_limit_k_min -33 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 62376 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.041 _diffrn_reflns_theta_min 1.705 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_current 0.6 _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 0.224 _exptl_absorpt_correction_T_max 0.746 _exptl_absorpt_correction_T_min 0.7051 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ;SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.315 _exptl_crystal_description block _exptl_crystal_F_000 1200 _exptl_crystal_recrystallization_method 'Crystals were obtained at room temperature from a mixture of dichloromethane and ethanol by slow solvent evaporation.' _exptl_crystal_size_max 0.777 _exptl_crystal_size_mid 0.534 _exptl_crystal_size_min 0.190 _refine_diff_density_max 0.450 _refine_diff_density_min -0.349 _refine_diff_density_rms 0.055 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 375 _refine_ls_number_reflns 8434 _refine_ls_number_restraints 12 _refine_ls_restrained_S_all 1.034 _refine_ls_R_factor_all 0.0503 _refine_ls_R_factor_gt 0.0400 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0377P)^2^+1.4959P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0919 _refine_ls_wR_factor_ref 0.0971 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7054 _reflns_number_total 8434 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc08530b2.cif _cod_data_source_block Eisenreich_TSC_4_a _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1573706 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.845 _shelx_estimated_absorpt_t_max 0.959 _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _shelx_res_file ; TITL Eisenreich_TSC_4_a.res in P2(1)/n Eisenreich_TSC_4_a.res created by SHELXL-2019/3 at 11:46:52 on 12-May-2024 REM Old TITL Eisenreich_TSC_4 in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.094, Rweak 0.004, Alpha 0.024 REM 0.869 for 164 systematic absences, Orientation as input REM Formula found by SHELXT: C30 N6 O2 S2 CELL 0.71073 9.8895 23.8880 12.3348 90.000 98.516 90.000 ZERR 8.000 0.0076 0.0196 0.0102 0.000 0.021 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O S UNIT 120 120 24 8 8 DFIX 0.90 N2 H2n DANG 1.86 N3 H2n DANG 1.84 C1 H2n DFIX 0.90 N1 H1n DANG 1.81 C1 H1n DANG 1.90 C2 H1n DFIX 0.90 N4 H4n DANG 1.82 C16 H4n DANG 1.91 C17 H4n DFIX 0.90 N5 H5n DANG 1.86 N6 H5n DANG 1.84 C16 H5n TEMP -173.150 SIZE 0.19 0.534 0.777 L.S. 10 BOND $H CONF MORE -1 HTAB LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.037700 1.495900 FVAR 0.33903 S1 5 0.838105 0.499300 0.650249 11.00000 0.01975 0.01465 = 0.01222 0.00160 0.00284 0.00164 S2 5 0.550758 0.875136 1.091344 11.00000 0.02063 0.01315 = 0.01150 -0.00163 0.00219 -0.00126 O1 4 0.442413 0.687965 0.813592 11.00000 0.01788 0.02281 = 0.02219 -0.01040 0.00486 -0.00077 O2 4 0.516908 0.636130 1.316193 11.00000 0.02450 0.02180 = 0.02137 0.00867 -0.00094 -0.00651 N1 3 0.689262 0.568079 0.507823 11.00000 0.01989 0.01910 = 0.01126 0.00026 0.00205 0.00568 REM HFIX R2N-H H1N 2 0.667595 0.579303 0.442038 11.00000 -1.20000 N2 3 0.822876 0.504606 0.434927 11.00000 0.01854 0.01545 = 0.01191 0.00086 0.00236 0.00453 REM HFIX R2N-H H2N 2 0.875240 0.475833 0.441906 11.00000 -1.20000 N3 3 0.764309 0.523085 0.332705 11.00000 0.01792 0.01488 = 0.01235 0.00115 0.00075 0.00084 N4 3 0.518838 0.783572 0.965353 11.00000 0.03021 0.01417 = 0.01184 -0.00223 0.00411 -0.00377 REM HFIX R2N-H H4N 2 0.508950 0.769553 0.901871 11.00000 -1.20000 N5 3 0.528516 0.867603 0.877399 11.00000 0.02649 0.01345 = 0.01092 -0.00124 0.00250 -0.00300 REM HFIX R2N-H H5N 2 0.544261 0.903096 0.879801 11.00000 -1.20000 N6 3 0.516268 0.839099 0.779342 11.00000 0.01962 0.01770 = 0.01201 -0.00300 0.00231 -0.00281 C1 1 0.779303 0.526055 0.525439 11.00000 0.01402 0.01295 = 0.01360 -0.00042 0.00252 -0.00167 C2 1 0.628369 0.596023 0.591469 11.00000 0.01662 0.01497 = 0.01325 0.00005 0.00147 0.00479 C3 1 0.499353 0.580478 0.610757 11.00000 0.01982 0.01782 = 0.02243 -0.00746 0.00362 -0.00256 AFIX 43 H3 2 0.455292 0.549223 0.573160 11.00000 -1.20000 AFIX 0 C4 1 0.433352 0.610225 0.684822 11.00000 0.01638 0.02014 = 0.02231 -0.00560 0.00495 -0.00325 AFIX 43 H4 2 0.344031 0.599817 0.696789 11.00000 -1.20000 AFIX 0 C5 1 0.499461 0.655245 0.740977 11.00000 0.01722 0.01457 = 0.01376 -0.00128 0.00206 0.00253 C6 1 0.631674 0.669522 0.725037 11.00000 0.01663 0.01544 = 0.01954 -0.00433 0.00055 -0.00204 AFIX 43 H6 2 0.678314 0.699247 0.765933 11.00000 -1.20000 AFIX 0 C7 1 0.695172 0.640347 0.649493 11.00000 0.01472 0.01819 = 0.02025 -0.00106 0.00289 -0.00056 AFIX 43 H7 2 0.784489 0.650679 0.637386 11.00000 -1.20000 AFIX 0 C8 1 0.305404 0.674535 0.829522 11.00000 0.01717 0.03626 = 0.02408 -0.01243 0.00451 0.00045 AFIX 137 H8A 2 0.246470 0.673161 0.758325 11.00000 -1.50000 H8B 2 0.271560 0.703247 0.875505 11.00000 -1.50000 H8C 2 0.304546 0.638018 0.865620 11.00000 -1.50000 AFIX 0 C9 1 0.800781 0.496524 0.251237 11.00000 0.01767 0.01263 = 0.01480 0.00106 0.00274 0.00045 AFIX 43 H9 2 0.865092 0.466907 0.265327 11.00000 -1.20000 AFIX 0 C10 1 0.746601 0.510330 0.137268 11.00000 0.01829 0.01331 = 0.01368 0.00151 0.00188 -0.00120 C11 1 0.791145 0.478619 0.054335 11.00000 0.02813 0.01815 = 0.01606 -0.00020 0.00427 0.00331 AFIX 43 H11 2 0.852927 0.448476 0.072806 11.00000 -1.20000 AFIX 0 C12 1 0.745586 0.490905 -0.055213 11.00000 0.03813 0.02486 = 0.01397 -0.00306 0.00477 -0.00174 AFIX 43 H12 2 0.776470 0.469200 -0.111255 11.00000 -1.20000 AFIX 0 C13 1 0.655513 0.534606 -0.082695 11.00000 0.03146 0.03068 = 0.01606 0.00377 -0.00319 -0.00488 AFIX 43 H13 2 0.625021 0.543171 -0.157533 11.00000 -1.20000 AFIX 0 C14 1 0.609687 0.565970 -0.000596 11.00000 0.02660 0.02780 = 0.02352 0.00584 -0.00267 0.00508 AFIX 43 H14 2 0.547294 0.595860 -0.019563 11.00000 -1.20000 AFIX 0 C15 1 0.654263 0.554008 0.108780 11.00000 0.02296 0.02071 = 0.01853 0.00103 0.00202 0.00436 AFIX 43 H15 2 0.621993 0.575532 0.164442 11.00000 -1.20000 AFIX 0 C16 1 0.532693 0.839295 0.973098 11.00000 0.01293 0.01394 = 0.01402 -0.00074 0.00184 -0.00093 C17 1 0.516956 0.747890 1.058711 11.00000 0.02381 0.01009 = 0.01380 -0.00075 0.00394 -0.00097 C18 1 0.638371 0.728249 1.117923 11.00000 0.01845 0.01910 = 0.02533 0.00195 0.00670 -0.00168 AFIX 43 H18 2 0.723610 0.739853 1.098740 11.00000 -1.20000 AFIX 0 C19 1 0.635099 0.691838 1.204701 11.00000 0.01716 0.01857 = 0.02530 0.00334 0.00148 0.00258 AFIX 43 H19 2 0.718086 0.679069 1.246023 11.00000 -1.20000 AFIX 0 C20 1 0.510031 0.673862 1.231568 11.00000 0.02224 0.01246 = 0.01517 0.00023 0.00154 -0.00132 C21 1 0.388333 0.693797 1.173517 11.00000 0.01730 0.02185 = 0.01641 0.00007 0.00280 -0.00401 AFIX 43 H21 2 0.302985 0.681995 1.192188 11.00000 -1.20000 AFIX 0 C22 1 0.393027 0.731278 1.087655 11.00000 0.01844 0.01797 = 0.01539 -0.00086 0.00011 0.00072 AFIX 43 H22 2 0.310289 0.745598 1.048529 11.00000 -1.20000 AFIX 0 C23 1 0.392850 0.608556 1.329232 11.00000 0.03829 0.06727 = 0.03988 0.03289 -0.01352 -0.03115 AFIX 137 H23A 2 0.347503 0.595462 1.257694 11.00000 -1.50000 H23B 2 0.332662 0.634710 1.360415 11.00000 -1.50000 H23C 2 0.412916 0.576499 1.378570 11.00000 -1.50000 AFIX 0 C24 1 0.497963 0.870250 0.693646 11.00000 0.01713 0.01721 = 0.01431 -0.00178 0.00257 -0.00109 AFIX 43 H24 2 0.491135 0.909631 0.702092 11.00000 -1.20000 AFIX 0 C25 1 0.487337 0.846606 0.583165 11.00000 0.01382 0.01780 = 0.01371 -0.00135 0.00144 -0.00191 C26 1 0.509646 0.789688 0.564526 11.00000 0.02041 0.01831 = 0.01621 -0.00010 0.00062 0.00021 AFIX 43 H26 2 0.530223 0.764732 0.624672 11.00000 -1.20000 AFIX 0 C27 1 0.501591 0.769883 0.457947 11.00000 0.02310 0.01927 = 0.02105 -0.00622 0.00143 0.00050 AFIX 43 H27 2 0.516543 0.731294 0.445363 11.00000 -1.20000 AFIX 0 C28 1 0.471672 0.806302 0.369203 11.00000 0.02029 0.02781 = 0.01533 -0.00589 0.00081 -0.00226 AFIX 43 H28 2 0.468184 0.792694 0.296473 11.00000 -1.20000 AFIX 0 C29 1 0.447045 0.862409 0.387445 11.00000 0.02292 0.02544 = 0.01289 0.00096 -0.00015 -0.00223 AFIX 43 H29 2 0.425185 0.887177 0.327138 11.00000 -1.20000 AFIX 0 C30 1 0.454340 0.882419 0.493978 11.00000 0.01888 0.01808 = 0.01599 -0.00023 0.00105 -0.00018 AFIX 43 H30 2 0.436684 0.920831 0.506090 11.00000 -1.20000 AFIX 0 HKLF 4 REM Eisenreich_TSC_4_a.res in P2(1)/n REM wR2 = 0.0971, GooF = S = 1.031, Restrained GooF = 1.034 for all data REM R1 = 0.0400 for 7054 Fo > 4sig(Fo) and 0.0503 for all 8434 data REM 375 parameters refined using 12 restraints END WGHT 0.0377 1.4960 REM Instructions for potential hydrogen bonds EQIV $1 x, y, z-1 HTAB N1 O2_$1 EQIV $2 -x+3/2, y-1/2, -z+3/2 HTAB N2 S2_$2 HTAB N4 O1 EQIV $3 -x+3/2, y+1/2, -z+3/2 HTAB N5 S1_$3 EQIV $4 x+1/2, -y+3/2, z-1/2 HTAB C7 S2_$4 EQIV $5 x-1/2, -y+3/2, z-1/2 HTAB C8 S2_$5 HTAB C9 S2_$2 REM Highest difference peak 0.450, deepest hole -0.349, 1-sigma level 0.055 Q1 1 0.4610 0.8726 0.4405 11.00000 0.05 0.42 Q2 1 0.4982 0.8578 0.6357 11.00000 0.05 0.39 Q3 1 0.7712 0.5093 0.1927 11.00000 0.05 0.37 Q4 1 0.7584 0.4842 0.0000 11.00000 0.05 0.36 Q5 1 0.5650 0.6613 0.7352 11.00000 0.05 0.36 Q6 1 0.4472 0.6823 1.1981 11.00000 0.05 0.35 Q7 1 0.7821 0.4988 0.0952 11.00000 0.05 0.35 Q8 1 0.4818 0.6285 0.7251 11.00000 0.05 0.35 Q9 1 0.4608 0.6393 0.6988 11.00000 0.05 0.35 Q10 1 0.5629 0.5888 0.6050 11.00000 0.05 0.35 Q11 1 0.5672 0.6783 1.2051 11.00000 0.05 0.34 Q12 1 0.5192 0.7649 1.0145 11.00000 0.05 0.34 Q13 1 0.4675 0.6028 0.6337 11.00000 0.05 0.33 Q14 1 0.7110 0.5347 0.1261 11.00000 0.05 0.32 Q15 1 0.5000 0.7786 0.5122 11.00000 0.05 0.32 Q16 1 0.4745 0.8648 0.5365 11.00000 0.05 0.32 Q17 1 0.3921 0.7154 1.1362 11.00000 0.05 0.31 Q18 1 0.4627 0.7864 0.4151 11.00000 0.05 0.31 Q19 1 0.6599 0.6167 0.6273 11.00000 0.05 0.31 Q20 1 0.6181 0.5561 0.0529 11.00000 0.05 0.31 ; _shelx_res_checksum 8047 _shelx_hkl_file ; -1 0 0 0.00 0.20 -1 0 0 0.30 0.10 1 0 0 0.10 0.10 1 0 0 0.30 0.20 1 0 0 0.20 0.20 2 0 0 4322.77 151.98 2 0 0 4114.39 152.38 2 0 0 4208.68 152.48 -2 0 0 4151.78 152.48 -2 0 0 4274.07 152.08 3 0 0 0.50 0.50 3 0 0 0.60 0.30 -3 0 0 0.00 0.40 -3 0 0 0.50 0.40 -4 0 0 2014.70 74.49 4 0 0 2099.49 75.29 -4 0 0 2064.99 75.39 -4 0 0 2041.20 75.59 4 0 0 2022.50 75.19 4 0 0 1994.40 74.19 -5 0 0 3.30 0.90 -5 0 0 4.10 1.30 5 0 0 8.30 1.20 -5 0 0 2.40 1.10 5 0 0 5.20 1.30 5 0 0 2.80 1.10 -6 0 0 1508.45 58.19 -6 0 0 1527.45 56.69 -6 0 0 1509.35 57.79 6 0 0 1503.05 56.09 6 0 0 1511.15 57.59 6 0 0 1573.44 57.79 7 0 0 10.10 2.20 -7 0 0 7.30 1.90 7 0 0 5.50 1.70 -7 0 0 2.70 1.10 8 0 0 97.49 6.70 -8 0 0 103.89 7.30 -8 0 0 102.79 6.90 -8 0 0 94.79 6.00 8 0 0 97.79 6.80 9 0 0 1.70 1.50 -9 0 0 1.00 1.40 -9 0 0 -0.80 1.40 9 0 0 4.10 1.90 -9 0 0 0.00 1.50 -10 0 0 6.80 2.70 -10 0 0 6.80 2.60 10 0 0 10.60 3.30 -10 0 0 9.50 2.60 11 0 0 3.20 2.10 -11 0 0 1.90 2.00 -11 0 0 5.00 2.70 -12 0 0 3.70 2.30 12 0 0 4.70 2.90 -13 0 0 4.30 3.10 13 0 0 4.80 3.30 0 -1 0 0.20 0.10 0 -1 0 0.20 0.10 0 1 0 0.00 0.10 -1 -1 0 97.09 4.00 1 -1 0 95.59 4.00 1 -1 0 93.19 4.00 -1 -1 0 98.89 4.10 1 -1 0 96.09 4.00 -1 -1 0 98.39 3.80 -1 1 0 94.59 4.10 1 1 0 102.49 3.90 1 1 0 96.39 3.90 -1 1 0 98.69 3.90 -2 -1 0 202.78 8.40 2 -1 0 209.08 8.40 -2 -1 0 209.58 8.50 2 -1 0 210.08 7.80 -2 -1 0 208.48 8.00 2 -1 0 200.98 8.40 -2 1 0 210.98 8.50 2 1 0 208.38 8.30 2 1 0 203.48 8.00 -2 1 0 215.28 8.10 2 1 0 199.28 8.40 3 -1 0 304.07 11.50 3 -1 0 297.57 12.30 -3 -1 0 312.17 12.60 -3 -1 0 301.07 12.40 3 -1 0 299.37 12.30 -3 -1 0 302.77 11.80 3 1 0 307.67 12.20 3 1 0 298.47 11.70 -3 1 0 307.67 11.80 3 1 0 303.07 12.30 -3 1 0 301.57 12.40 4 -1 0 13.10 1.20 -4 -1 0 13.30 1.90 -4 -1 0 9.90 1.80 -4 -1 0 9.50 1.30 4 -1 0 15.30 1.90 4 -1 0 11.30 1.80 4 1 0 10.00 1.70 4 1 0 10.50 1.60 4 1 0 10.70 1.30 -4 1 0 12.60 1.50 -4 1 0 14.20 1.90 -5 -1 0 577.84 23.40 -5 -1 0 614.74 24.30 5 -1 0 599.14 24.10 5 -1 0 625.54 24.30 -5 -1 0 598.74 24.60 5 -1 0 619.44 22.80 5 1 0 615.54 24.30 5 1 0 619.04 23.20 -5 1 0 606.04 23.40 5 1 0 591.74 24.10 -5 1 0 612.14 24.40 6 -1 0 14.70 2.50 -6 -1 0 9.30 2.30 -6 -1 0 11.70 2.20 -6 -1 0 17.00 2.10 6 -1 0 12.00 2.10 6 -1 0 15.30 1.50 -6 1 0 9.90 2.40 6 1 0 10.50 1.50 -6 1 0 15.60 2.10 6 1 0 9.30 2.10 6 1 0 14.20 2.40 -6 1 0 12.70 2.30 -7 -1 0 84.19 5.70 7 -1 0 71.39 5.20 -7 -1 0 67.49 5.50 7 -1 0 81.29 5.60 7 -1 0 80.59 4.10 -7 -1 0 76.09 4.80 7 1 0 79.69 5.50 -7 1 0 71.39 5.70 -7 1 0 70.59 5.30 7 1 0 78.09 5.50 7 1 0 75.89 4.30 -7 1 0 73.79 4.70 8 -1 0 278.77 13.70 8 -1 0 283.17 13.80 -8 -1 0 281.67 13.90 -8 -1 0 270.87 12.70 -8 -1 0 261.67 13.90 -8 1 0 292.97 12.90 8 1 0 298.37 14.00 8 1 0 269.37 11.90 -8 1 0 259.17 14.00 8 1 0 277.77 13.60 -8 1 0 279.87 13.80 -9 -1 0 131.99 8.70 -9 -1 0 132.29 8.60 9 -1 0 125.09 8.30 -9 -1 0 124.69 7.50 9 -1 0 133.99 8.70 -9 1 0 120.09 7.40 -9 1 0 127.39 8.90 -9 1 0 132.39 8.50 9 1 0 135.59 8.70 -10 -1 0 90.09 7.50 10 -1 0 100.29 7.40 10 -1 0 101.29 7.80 -10 -1 0 90.19 8.80 -10 -1 0 93.69 7.20 -10 1 0 92.19 7.40 -10 1 0 98.49 6.70 -10 1 0 102.89 8.00 10 1 0 94.99 7.60 -11 -1 0 34.90 5.60 11 -1 0 28.00 5.00 -11 -1 0 26.80 4.90 -11 1 0 26.70 5.30 11 1 0 35.30 5.60 -11 1 0 31.50 5.20 -12 -1 0 1.50 2.50 12 -1 0 4.70 2.60 12 1 0 -1.70 2.40 -12 1 0 3.00 2.60 -13 -1 0 0.30 2.60 13 -1 0 -0.10 2.70 13 1 0 0.90 2.50 -13 1 0 3.70 3.00 0 -2 0 87.19 3.80 0 -2 0 93.19 3.90 0 -2 0 88.39 3.60 0 2 0 89.69 3.60 0 2 0 89.99 3.50 -1 -2 0 212.58 8.60 1 -2 0 218.88 8.70 1 -2 0 217.48 8.70 1 -2 0 222.88 8.60 -1 -2 0 223.58 8.40 -1 -2 0 222.08 8.70 1 2 0 224.98 8.50 1 2 0 223.68 8.50 -1 2 0 218.28 8.50 -1 2 0 224.28 8.20 2 -2 0 9727.23 354.46 2 -2 0 9708.13 354.06 -2 -2 0 9999.00 354.36 3 -2 0 260.87 9.90 -3 -2 0 265.67 10.40 3 -2 0 264.77 10.90 3 -2 0 251.17 10.80 -3 -2 0 248.48 10.90 -3 -2 0 267.17 11.00 -3 2 0 268.37 10.50 3 2 0 261.47 10.70 3 2 0 268.07 10.40 3 2 0 266.87 10.80 -3 2 0 262.37 11.00 -4 -2 0 295.17 12.90 4 -2 0 296.17 11.60 -4 -2 0 305.97 12.20 -4 -2 0 308.27 13.10 4 -2 0 318.27 13.00 4 -2 0 297.37 12.80 -4 2 0 316.57 13.10 4 2 0 313.07 12.80 4 2 0 304.87 12.80 -4 2 0 305.27 12.30 4 2 0 303.37 12.20 5 -2 0 580.14 23.50 -5 -2 0 602.34 22.80 -5 -2 0 601.74 23.80 5 -2 0 599.04 22.00 5 -2 0 597.64 23.70 -5 -2 0 583.04 23.80 5 2 0 571.94 23.40 5 2 0 583.44 22.60 -5 2 0 577.74 23.70 -5 2 0 605.64 22.80 5 2 0 566.54 23.40 6 -2 0 34.80 3.60 -6 -2 0 27.70 3.70 -6 -2 0 32.50 3.70 6 -2 0 33.20 3.80 -6 -2 0 35.50 3.20 6 -2 0 33.00 2.10 -6 2 0 33.10 3.80 -6 2 0 30.80 3.00 6 2 0 32.70 2.50 6 2 0 29.20 3.30 6 2 0 39.10 4.00 -7 -2 0 34.70 4.20 7 -2 0 34.90 2.30 7 -2 0 29.50 3.60 -7 -2 0 34.00 3.50 -7 -2 0 24.20 3.50 7 -2 0 36.50 4.20 -7 2 0 37.00 3.60 -7 2 0 26.40 4.00 -7 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3.50 5 -4 0 24.60 1.40 -5 -4 0 23.40 3.00 -5 -4 0 19.00 2.20 5 -4 0 19.30 2.50 5 4 0 23.50 2.70 -5 4 0 24.70 3.00 5 4 0 23.80 2.30 -5 4 0 28.30 2.70 6 -4 0 15.40 1.20 6 -4 0 20.70 2.80 6 -4 0 22.80 3.10 -6 -4 0 17.90 2.30 -6 -4 0 11.70 2.30 -6 -4 0 16.70 2.80 6 4 0 17.30 2.60 6 4 0 17.10 2.10 -6 4 0 13.40 2.40 -6 4 0 14.40 2.00 -7 -4 0 15.10 2.30 -7 -4 0 5.60 1.80 7 -4 0 5.60 1.60 -7 -4 0 5.50 2.00 7 -4 0 9.70 2.30 -7 4 0 10.40 2.50 7 4 0 5.40 1.70 7 4 0 9.90 1.80 -7 4 0 7.00 1.70 -8 -4 0 67.99 4.90 8 -4 0 63.99 6.20 8 -4 0 60.99 6.10 -8 -4 0 72.79 5.90 -8 -4 0 68.59 6.70 8 4 0 70.09 5.70 8 4 0 61.19 4.40 -8 4 0 70.29 4.80 -8 4 0 73.39 5.70 9 -4 0 3.60 1.90 9 -4 0 -0.40 1.40 -9 -4 0 3.40 1.90 -9 -4 0 2.40 1.80 -9 -4 0 3.60 1.70 -9 4 0 9.00 2.70 9 4 0 4.90 1.80 -9 4 0 0.40 1.70 -9 4 0 0.50 1.30 9 4 0 6.00 2.50 10 -4 0 0.90 1.50 -10 -4 0 0.20 1.80 10 -4 0 -0.20 1.60 -10 -4 0 -0.50 1.60 -10 4 0 0.10 1.40 -10 4 0 -0.50 1.20 10 4 0 2.60 2.00 -10 4 0 -1.10 1.80 -11 -4 0 3.60 2.50 11 -4 0 2.60 2.40 11 -4 0 4.00 2.50 -11 -4 0 0.50 2.00 -11 4 0 4.30 2.10 -11 4 0 6.00 2.70 -11 4 0 2.90 2.10 11 4 0 4.30 2.80 -12 -4 0 120.89 11.70 12 -4 0 105.29 10.90 12 -4 0 116.09 9.20 12 4 0 139.19 10.70 -12 4 0 107.79 9.00 -13 -4 0 7.60 3.80 13 -4 0 4.30 2.50 13 4 0 7.40 3.90 -13 4 0 6.90 3.70 0 -5 0 0.70 0.50 0 -5 0 1.50 0.70 0 -5 0 -0.20 0.50 0 5 0 0.40 0.40 0 5 0 0.70 0.50 1 -5 0 206.18 8.30 1 -5 0 198.88 8.80 1 -5 0 197.08 8.80 -1 -5 0 198.68 8.10 -1 -5 0 191.28 8.70 -1 -5 0 207.08 8.80 1 5 0 200.98 8.20 1 5 0 204.38 8.20 1 5 0 200.38 8.10 -1 5 0 195.98 7.80 -1 5 0 200.68 8.20 2 -5 0 279.67 11.30 2 -5 0 272.47 11.70 2 -5 0 262.67 11.60 -2 -5 0 287.07 11.10 -2 -5 0 265.17 11.70 -2 -5 0 270.87 11.70 2 5 0 290.37 11.20 2 5 0 286.67 11.20 -2 5 0 282.57 10.70 -2 5 0 279.47 11.20 -3 -5 0 387.76 16.30 -3 -5 0 409.76 16.30 3 -5 0 392.96 15.80 3 -5 0 386.56 16.10 -3 -5 0 400.56 15.50 3 -5 0 388.96 16.10 -3 5 0 391.06 15.60 3 5 0 392.66 15.60 -3 5 0 395.46 14.80 -3 5 0 401.76 16.30 3 5 0 399.56 15.80 -4 -5 0 220.28 9.20 4 -5 0 202.38 9.60 4 -5 0 216.48 9.90 4 -5 0 210.98 8.10 -4 -5 0 219.08 10.00 4 -5 0 206.48 9.70 -4 -5 0 210.18 10.10 4 5 0 222.18 9.40 -4 5 0 215.58 9.90 4 5 0 217.18 9.60 -4 5 0 223.88 9.40 5 -5 0 749.23 30.20 -5 -5 0 766.22 30.80 5 -5 0 789.02 30.60 -5 -5 0 783.62 29.70 5 -5 0 773.42 28.20 -5 -5 0 758.92 30.60 5 5 0 762.12 30.30 5 5 0 764.32 29.70 -5 5 0 786.82 29.70 -5 5 0 787.22 30.70 -6 -5 0 74.39 5.40 6 -5 0 72.59 4.90 6 -5 0 78.69 5.30 -6 -5 0 74.79 5.20 -6 -5 0 74.79 4.50 6 -5 0 67.19 3.10 6 5 0 83.79 5.20 -6 5 0 80.39 5.30 6 5 0 65.09 4.30 -6 5 0 76.49 4.50 7 -5 0 80.59 5.60 -7 -5 0 79.19 5.10 -7 -5 0 79.69 6.00 -7 -5 0 78.39 5.80 7 -5 0 83.59 5.90 7 5 0 74.29 4.90 -7 5 0 81.89 5.10 -7 5 0 103.19 6.40 7 5 0 74.69 5.60 -8 -5 0 -0.80 1.20 -8 -5 0 -0.90 0.90 -8 -5 0 -0.10 1.20 8 -5 0 0.60 1.50 8 -5 0 -0.80 1.10 8 5 0 1.00 1.10 8 5 0 -0.50 1.00 -8 5 0 2.00 1.30 -8 5 0 -0.50 1.00 -9 -5 0 27.60 4.40 9 -5 0 15.20 3.20 9 -5 0 18.10 3.40 -9 -5 0 13.20 3.10 -9 5 0 16.90 3.70 9 5 0 18.50 2.80 -9 5 0 21.70 3.80 -9 5 0 17.80 3.00 9 5 0 15.00 3.30 10 -5 0 39.00 5.40 10 -5 0 30.40 5.00 -10 -5 0 19.80 4.50 -10 -5 0 28.10 4.70 -10 5 0 27.20 4.00 10 5 0 32.60 5.10 -10 5 0 30.50 4.70 -10 5 0 27.10 5.00 -11 -5 0 136.69 10.20 11 -5 0 112.69 8.90 11 -5 0 115.89 8.80 -11 -5 0 117.99 9.10 -11 5 0 115.69 8.00 -11 5 0 124.79 9.00 11 5 0 122.19 9.60 -11 5 0 104.89 10.40 -12 -5 0 -1.30 2.40 12 -5 0 -1.70 2.10 12 -5 0 -1.80 1.90 -12 5 0 0.30 2.00 12 5 0 0.30 2.60 13 -5 0 42.60 6.60 -13 -5 0 33.50 6.60 -13 5 0 42.30 6.70 13 5 0 32.50 6.30 0 -6 0 4420.26 162.78 0 -6 0 4564.84 163.68 0 -6 0 4469.15 163.68 0 6 0 4520.95 162.68 0 6 0 4506.05 162.78 -1 -6 0 390.86 15.80 1 -6 0 389.76 15.80 -1 -6 0 392.86 15.00 1 -6 0 401.06 16.00 1 -6 0 387.06 15.10 -1 -6 0 374.66 15.80 1 6 0 382.96 15.00 1 6 0 384.16 15.00 1 6 0 387.06 15.10 -1 6 0 371.86 15.00 -1 6 0 389.66 14.70 2 -6 0 671.93 26.20 2 -6 0 676.13 26.10 -2 -6 0 669.43 26.20 2 -6 0 666.03 25.50 -2 -6 0 664.73 25.20 -2 -6 0 662.13 26.10 -2 6 0 640.64 25.40 -2 6 0 677.03 24.80 2 6 0 698.73 25.50 2 6 0 661.23 25.40 3 -6 0 18.60 2.10 -3 -6 0 15.90 2.30 3 -6 0 20.40 2.30 3 -6 0 22.50 2.60 -3 -6 0 19.10 2.50 -3 -6 0 20.80 2.00 -3 6 0 23.20 1.40 3 6 0 19.60 2.20 -3 6 0 21.10 2.00 3 6 0 22.50 2.20 -4 -6 0 624.84 23.90 4 -6 0 627.54 24.60 4 -6 0 615.44 24.70 -4 -6 0 625.14 25.10 4 -6 0 618.14 22.70 4 -6 0 610.04 24.30 -4 -6 0 620.94 24.90 -4 6 0 621.64 24.10 -4 6 0 592.54 24.70 4 6 0 620.74 24.10 4 6 0 623.34 24.40 5 -6 0 15.10 2.40 -5 -6 0 6.40 1.60 -5 -6 0 8.30 1.50 5 -6 0 6.80 1.70 -5 -6 0 10.10 2.10 5 -6 0 11.50 2.00 -5 6 0 9.00 1.60 5 6 0 11.50 1.80 5 6 0 4.70 1.40 -5 6 0 11.80 2.10 -6 -6 0 200.18 9.30 -6 -6 0 197.78 10.20 6 -6 0 191.28 10.00 -6 -6 0 195.78 10.50 6 -6 0 207.68 10.00 6 6 0 194.88 9.30 -6 6 0 197.08 10.20 -6 6 0 191.28 9.30 6 6 0 204.08 10.00 7 -6 0 4.80 1.80 7 -6 0 3.30 1.80 -7 -6 0 3.20 1.60 -7 -6 0 2.70 1.70 -7 -6 0 4.30 1.40 -7 6 0 2.10 1.20 7 6 0 4.30 1.80 7 6 0 1.30 1.00 -7 6 0 4.80 1.70 8 -6 0 10.50 2.50 -8 -6 0 12.50 2.50 8 -6 0 12.40 2.80 -8 -6 0 6.50 2.60 -8 -6 0 5.90 2.30 -8 6 0 9.30 2.40 8 6 0 10.30 2.10 8 6 0 11.10 2.60 -8 6 0 7.40 1.80 9 -6 0 44.40 5.60 -9 -6 0 41.60 5.40 9 -6 0 41.80 5.20 -9 -6 0 40.60 5.70 9 6 0 41.20 4.40 -9 6 0 40.40 4.50 9 6 0 44.00 5.60 -9 6 0 35.50 4.80 -10 -6 0 34.70 5.70 10 -6 0 32.10 5.00 10 -6 0 41.30 5.50 -10 -6 0 21.10 4.30 -10 6 0 27.80 4.00 -10 6 0 30.00 4.80 -10 6 0 35.10 5.80 10 6 0 30.60 5.00 -11 -6 0 53.59 7.30 11 -6 0 59.89 7.10 11 -6 0 74.99 8.30 -11 -6 0 61.59 7.40 11 6 0 56.59 7.30 -11 6 0 55.49 7.00 -11 6 0 46.30 6.80 -11 6 0 59.19 6.30 12 -6 0 9.20 3.40 -12 -6 0 11.60 4.10 12 -6 0 10.30 3.50 -12 6 0 11.90 3.60 12 6 0 14.10 4.40 13 -6 0 12.60 3.50 -13 -6 0 8.90 3.70 13 6 0 10.40 4.30 -13 6 0 13.40 4.20 0 -7 0 1.60 0.90 0 -7 0 0.40 0.70 0 -7 0 1.90 0.70 0 7 0 0.60 0.50 0 7 0 0.50 0.50 -1 -7 0 2483.75 94.09 1 -7 0 2543.85 94.09 -1 -7 0 2580.44 93.99 1 -7 0 2542.75 94.09 1 -7 0 2530.65 93.09 -1 -7 0 2579.64 92.99 1 7 0 2578.04 93.09 -1 7 0 2516.35 92.69 -1 7 0 2574.24 93.09 1 7 0 2577.94 92.99 1 7 0 2543.45 93.09 2 -7 0 80.39 5.00 -2 -7 0 81.99 5.10 -2 -7 0 86.19 4.30 2 -7 0 86.89 4.50 2 -7 0 83.39 5.00 -2 -7 0 85.19 5.10 -2 7 0 86.99 4.00 2 7 0 92.39 4.60 2 7 0 86.49 4.50 -2 7 0 87.99 4.40 3 -7 0 1248.78 47.60 3 -7 0 1253.87 47.80 -3 -7 0 1258.07 46.70 -3 -7 0 1274.87 47.90 -3 -7 0 1243.08 48.00 3 -7 0 1241.08 47.00 -3 7 0 1264.77 47.00 3 7 0 1273.17 47.10 3 7 0 1241.68 47.00 -3 7 0 1268.67 46.10 -4 -7 0 73.79 5.00 -4 -7 0 70.69 4.00 4 -7 0 62.19 4.40 4 -7 0 71.99 4.30 4 -7 0 63.09 4.40 -4 -7 0 72.19 4.80 4 7 0 69.79 4.20 4 7 0 61.39 4.20 -4 7 0 68.89 4.10 -4 7 0 69.59 3.10 -4 7 0 77.69 4.80 5 -7 0 0.30 0.80 -5 -7 0 2.50 1.00 -5 -7 0 -0.20 1.00 -5 -7 0 0.80 1.10 5 -7 0 1.40 1.00 5 -7 0 0.40 0.90 -5 7 0 1.50 1.00 -5 7 0 1.40 1.00 5 7 0 0.60 0.90 5 7 0 2.20 1.00 -6 -7 0 255.67 11.70 6 -7 0 282.87 12.60 6 -7 0 248.28 12.60 -6 -7 0 277.07 13.40 -6 -7 0 282.37 13.20 -6 7 0 278.47 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343.97 14.30 3 10 0 351.76 15.30 3 10 0 349.17 15.20 3 10 0 349.17 14.70 -3 10 0 379.86 15.20 4 -10 0 242.38 12.10 4 -10 0 247.58 11.20 -4 -10 0 265.97 12.60 4 -10 0 254.67 12.00 -4 -10 0 223.48 10.60 -4 -10 0 264.27 12.90 -4 10 0 253.17 11.20 -4 10 0 249.48 10.20 4 10 0 240.28 11.40 4 10 0 238.78 11.20 5 -10 0 7.70 2.00 -5 -10 0 7.00 2.10 -5 -10 0 6.70 2.00 5 -10 0 5.80 1.60 5 10 0 6.10 1.70 5 10 0 5.70 1.50 -5 10 0 6.90 1.60 6 -10 0 49.80 4.10 6 -10 0 50.29 5.00 -6 -10 0 56.89 6.00 -6 -10 0 51.49 3.80 6 -10 0 48.00 5.20 -6 -10 0 54.49 6.00 6 10 0 59.09 4.40 -6 10 0 49.30 4.60 6 10 0 47.90 5.00 -6 10 0 49.40 5.10 -7 -10 0 4.80 2.20 -7 -10 0 2.90 2.00 7 -10 0 5.60 2.20 -7 -10 0 5.80 1.70 7 -10 0 8.00 2.10 -7 10 0 3.60 1.80 -7 10 0 2.30 1.30 7 10 0 4.30 1.70 7 10 0 4.20 1.70 8 -10 0 31.50 4.20 8 -10 0 34.40 4.80 -8 -10 0 27.80 5.00 -8 -10 0 35.70 5.30 -8 10 0 35.20 4.80 8 10 0 37.60 5.10 -8 10 0 34.60 4.20 8 10 0 39.10 4.60 -9 -10 0 2.40 2.10 -9 -10 0 -2.20 1.70 9 -10 0 -0.40 1.30 9 -10 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30.30 4.30 7 -11 0 40.70 4.60 -7 11 0 37.50 4.90 7 11 0 30.30 3.80 7 11 0 38.10 4.80 -7 11 0 30.80 3.80 -8 -11 0 11.50 3.30 8 -11 0 12.20 3.00 8 -11 0 5.90 2.00 -8 -11 0 8.60 3.10 8 11 0 8.20 2.30 -8 11 0 6.80 2.50 -8 11 0 9.60 2.40 8 11 0 4.70 2.10 -9 -11 0 60.59 7.90 9 -11 0 53.59 6.10 -9 -11 0 44.80 6.40 9 -11 0 48.10 6.20 -9 11 0 52.69 6.20 -9 11 0 53.79 5.70 9 11 0 51.59 5.80 9 11 0 53.69 6.60 10 -11 0 17.40 4.10 10 -11 0 18.70 3.80 -10 -11 0 20.10 4.60 -10 -11 0 7.90 3.50 10 11 0 12.50 3.60 10 11 0 16.20 3.50 -10 11 0 10.20 3.20 -10 11 0 17.10 3.40 -11 -11 0 44.50 7.40 -11 -11 0 49.80 7.50 11 -11 0 51.89 6.70 11 -11 0 42.80 6.50 11 11 0 41.60 7.00 -11 11 0 41.80 5.60 -11 11 0 51.29 6.40 12 -11 0 4.10 3.10 -12 -11 0 4.00 3.70 12 -11 0 7.30 3.60 -12 11 0 3.00 2.80 -12 11 0 6.70 2.90 12 11 0 11.30 4.30 13 -11 0 4.50 3.40 -13 -11 0 3.90 3.40 13 11 0 11.20 4.40 -13 11 0 5.60 3.30 0 -12 0 70.69 5.60 0 -12 0 89.59 6.00 0 -12 0 71.29 4.50 0 12 0 73.59 4.50 0 12 0 79.89 4.60 -1 -12 0 88.79 5.20 -1 -12 0 92.89 6.40 1 -12 0 78.99 6.00 1 -12 0 95.69 6.40 -1 -12 0 86.89 6.40 1 -12 0 100.79 5.30 1 12 0 90.79 5.10 -1 12 0 97.69 5.30 1 12 0 94.09 5.20 -1 12 0 98.29 5.10 1 12 0 93.09 5.30 2 -12 0 743.83 29.60 -2 -12 0 676.83 29.20 2 -12 0 705.53 29.20 2 -12 0 719.53 27.50 -2 -12 0 690.33 29.50 2 12 0 699.83 27.40 -2 12 0 706.33 27.70 2 12 0 717.63 27.90 2 12 0 685.93 27.80 -2 12 0 703.03 27.20 -3 -12 0 49.80 3.40 3 -12 0 48.10 5.20 -3 -12 0 46.60 5.30 3 -12 0 54.09 5.30 -3 -12 0 45.00 5.00 3 -12 0 47.80 3.40 -3 12 0 46.10 3.10 3 12 0 43.60 3.30 3 12 0 51.39 3.90 -3 12 0 49.00 3.60 3 12 0 36.00 3.70 -4 -12 0 15.70 2.10 4 -12 0 10.70 2.60 4 -12 0 9.10 1.80 4 -12 0 10.20 2.40 -4 -12 0 13.70 2.90 -4 -12 0 11.30 3.00 4 12 0 14.30 2.50 4 12 0 14.20 2.10 4 12 0 12.70 2.40 -4 12 0 10.30 2.00 -4 12 0 13.60 1.80 5 -12 0 7.90 2.10 -5 -12 0 5.10 2.20 5 -12 0 8.50 2.40 -5 -12 0 6.60 2.60 -5 -12 0 8.60 1.70 5 -12 0 8.70 1.90 -5 12 0 7.80 1.30 5 12 0 8.20 2.00 5 12 0 6.70 1.90 -5 12 0 6.40 1.70 -5 12 0 8.90 2.20 -6 -12 0 229.98 13.20 6 -12 0 225.08 11.20 -6 -12 0 228.68 10.50 6 -12 0 225.88 11.70 -6 -12 0 225.48 12.60 6 -12 0 255.77 12.50 -6 12 0 225.58 11.10 6 12 0 203.98 11.10 -6 12 0 245.08 12.30 6 12 0 213.08 11.70 7 -12 0 18.50 3.10 -7 -12 0 17.30 3.90 -7 -12 0 17.80 3.80 7 -12 0 15.90 3.10 7 -12 0 23.40 3.90 7 12 0 18.00 3.50 -7 12 0 13.50 2.70 7 12 0 16.20 3.00 -7 12 0 11.00 2.70 -8 -12 0 40.00 6.10 8 -12 0 46.10 5.30 8 -12 0 42.40 5.60 -8 -12 0 41.80 5.90 -8 12 0 39.70 5.50 8 12 0 33.00 5.00 8 12 0 43.60 5.00 -8 12 0 44.00 4.80 -9 -12 0 115.09 10.70 -9 -12 0 116.29 11.30 9 -12 0 111.59 7.90 9 -12 0 114.49 8.60 9 12 0 110.59 7.80 -9 12 0 119.09 8.50 -9 12 0 117.69 7.70 9 12 0 103.69 8.50 -10 -12 0 53.79 7.80 -10 -12 0 43.40 6.70 10 -12 0 48.40 6.00 10 -12 0 51.49 6.90 -10 12 0 45.20 5.50 10 12 0 54.89 6.30 -10 12 0 58.49 7.10 10 12 0 48.40 6.90 11 -12 0 0.40 1.90 11 -12 0 1.30 2.30 -11 -12 0 3.30 3.30 -11 -12 0 -1.20 2.20 11 12 0 1.20 2.50 -11 12 0 2.20 2.00 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0 92.39 9.10 6 -20 0 100.29 6.70 6 20 0 99.79 7.90 -6 20 0 91.79 7.00 7 -20 0 30.70 5.70 -7 -20 0 37.40 6.90 -7 -20 0 39.70 7.40 7 -20 0 46.70 6.20 7 -20 0 33.00 4.50 -7 20 0 33.40 5.60 7 20 0 35.50 5.60 -7 20 0 40.70 5.30 8 -20 0 1.90 1.70 -8 -20 0 2.40 3.40 8 -20 0 0.00 2.00 8 -20 0 0.40 2.30 -8 -20 0 6.50 3.30 -8 20 0 3.60 2.30 8 20 0 3.20 2.70 -8 20 0 -0.20 2.10 9 -20 0 11.60 4.10 -9 -20 0 6.90 4.10 9 -20 0 12.30 3.50 9 -20 0 10.80 3.20 -9 -20 0 12.20 5.10 -9 20 0 15.10 3.80 9 20 0 9.90 3.60 -9 20 0 17.80 4.00 -10 -20 0 -3.00 2.90 10 -20 0 0.90 2.60 -10 -20 0 4.40 4.00 10 -20 0 -0.40 2.20 -10 20 0 -0.20 2.00 10 20 0 0.20 2.10 -11 -20 0 22.20 6.90 11 -20 0 16.60 4.30 11 -20 0 23.50 5.60 11 20 0 13.00 4.20 -11 20 0 18.20 4.10 0 -21 0 18.30 4.20 0 21 0 7.80 2.20 1 -21 0 104.99 10.40 -1 -21 0 85.99 9.70 -1 -21 0 121.79 9.50 1 -21 0 97.29 10.00 1 21 0 111.99 7.50 1 21 0 109.59 6.80 -1 21 0 117.89 7.10 -1 21 0 96.89 6.90 2 -21 0 30.30 5.80 -2 -21 0 22.30 4.80 2 -21 0 14.80 3.90 -2 -21 0 23.70 5.00 -2 21 0 20.10 3.30 -2 21 0 16.10 3.10 2 21 0 19.00 3.50 2 21 0 16.70 2.80 3 -21 0 204.08 12.90 -3 -21 0 189.58 13.20 3 -21 0 185.08 12.30 -3 -21 0 183.38 12.80 3 21 0 181.48 10.80 -3 21 0 181.38 10.30 -3 21 0 175.98 9.90 3 21 0 182.08 9.60 4 -21 0 54.79 7.50 -4 -21 0 55.69 7.60 -4 -21 0 59.09 8.20 4 -21 0 61.39 7.60 4 21 0 44.90 5.80 -4 21 0 70.79 6.50 5 -21 0 1.80 2.20 -5 -21 0 3.70 2.90 -5 -21 0 0.70 2.60 5 -21 0 4.60 2.80 -5 21 0 6.00 2.30 5 21 0 4.70 2.40 6 -21 0 8.40 2.90 6 -21 0 7.00 3.30 -6 -21 0 4.40 2.70 -6 -21 0 6.20 3.20 -6 21 0 5.50 2.50 6 21 0 5.90 2.90 7 -21 0 31.50 5.80 -7 -21 0 37.10 7.20 -7 -21 0 39.20 7.70 7 -21 0 48.50 6.50 -7 21 0 35.50 5.30 7 21 0 41.40 6.00 -7 21 0 54.49 7.10 8 -21 0 28.10 5.40 -8 -21 0 25.40 6.20 -8 -21 0 17.70 5.80 8 -21 0 24.70 4.80 -8 21 0 21.10 4.40 -8 21 0 19.20 4.10 8 21 0 18.60 4.60 9 -21 0 43.50 6.20 -9 -21 0 45.70 9.00 9 -21 0 35.90 6.30 -9 -21 0 35.90 6.90 9 21 0 23.60 5.10 -9 21 0 33.70 5.30 -10 -21 0 0.70 3.30 -10 -21 0 0.60 3.20 10 -21 0 0.90 3.10 -10 21 0 2.50 2.50 10 21 0 0.10 2.70 0 -22 0 105.29 10.40 0 -22 0 85.49 9.70 0 22 0 88.09 6.70 0 22 0 91.49 6.30 1 -22 0 8.60 3.30 -1 -22 0 10.70 3.50 -1 -22 0 3.90 2.70 1 -22 0 10.00 3.50 1 22 0 6.40 2.40 -1 22 0 4.70 2.00 1 22 0 7.20 2.10 -1 22 0 8.40 2.30 -2 -22 0 11.60 3.90 2 -22 0 13.10 3.70 -2 -22 0 19.00 5.00 2 -22 0 7.50 3.10 -2 22 0 7.50 2.20 -2 22 0 12.90 2.80 2 22 0 10.90 3.00 2 22 0 8.70 2.30 3 -22 0 16.70 4.40 3 -22 0 8.70 3.50 -3 -22 0 17.60 4.50 -3 -22 0 10.20 3.90 3 22 0 14.70 3.20 -3 22 0 13.70 2.90 -3 22 0 23.70 3.70 3 22 0 16.80 2.80 4 -22 0 106.29 10.90 -4 -22 0 117.29 11.90 4 -22 0 126.69 9.60 -4 -22 0 115.19 12.20 4 22 0 124.39 8.80 -4 22 0 113.69 7.70 5 -22 0 29.50 5.40 -5 -22 0 27.50 5.80 -5 -22 0 41.90 7.30 5 -22 0 34.20 6.20 -5 22 0 33.00 4.50 5 22 0 32.30 5.00 -6 -22 0 65.79 9.20 6 -22 0 73.49 8.70 -6 -22 0 75.59 10.20 6 -22 0 79.79 8.40 -6 22 0 74.59 7.20 6 22 0 65.49 7.40 -7 -22 0 82.09 11.10 7 -22 0 80.29 8.50 -7 -22 0 99.49 11.60 7 -22 0 74.89 9.10 -7 22 0 78.29 7.80 7 22 0 85.69 9.20 -7 22 0 91.99 9.50 8 -22 0 5.50 3.40 -8 -22 0 6.30 4.40 8 -22 0 10.00 3.60 -8 -22 0 8.30 4.50 8 22 0 14.10 4.20 -8 22 0 4.00 2.80 -8 22 0 11.10 3.80 9 -22 0 33.90 5.50 9 -22 0 32.50 6.50 -9 -22 0 23.40 7.10 -9 -22 0 48.50 8.60 -9 22 0 35.40 5.50 9 22 0 30.00 5.50 10 -22 0 15.50 4.70 -10 -22 0 20.00 6.50 -10 -22 0 34.60 8.60 -10 22 0 14.70 3.60 10 22 0 8.90 3.30 0 -23 0 13.30 3.80 0 -23 0 18.00 4.40 0 23 0 7.90 2.50 0 23 0 7.20 2.20 -1 -23 0 205.88 14.20 -1 -23 0 212.08 14.30 1 -23 0 200.38 14.00 1 -23 0 186.28 13.50 1 23 0 209.08 11.10 -1 23 0 227.38 11.50 1 23 0 216.28 12.10 -1 23 0 217.38 11.80 2 -23 0 12.70 3.80 -2 -23 0 10.30 4.00 -2 -23 0 4.50 3.10 2 -23 0 13.00 3.90 2 23 0 12.10 2.50 2 23 0 7.20 2.70 -2 23 0 7.10 2.50 3 -23 0 24.70 5.20 -3 -23 0 26.30 5.90 3 -23 0 30.20 5.80 -3 -23 0 32.90 6.50 3 23 0 26.30 4.40 -3 23 0 27.40 4.10 -3 23 0 32.80 4.50 -4 -23 0 135.19 13.70 4 -23 0 101.09 10.30 -4 -23 0 113.99 12.20 4 -23 0 93.79 10.50 4 23 0 119.29 8.80 -4 23 0 136.89 8.40 5 -23 0 6.60 3.30 -5 -23 0 8.40 4.20 -5 -23 0 7.60 3.40 5 -23 0 3.00 2.40 -5 23 0 8.40 2.70 5 23 0 5.60 2.70 6 -23 0 40.20 6.80 -6 -23 0 34.70 6.80 -6 -23 0 57.89 9.70 6 -23 0 37.50 6.00 -6 23 0 49.80 5.80 6 23 0 47.30 6.70 -7 -23 0 3.00 3.70 7 -23 0 1.40 2.50 -7 -23 0 2.30 3.30 7 -23 0 4.50 2.90 -7 23 0 0.60 2.60 -7 23 0 4.20 2.30 7 23 0 -1.80 2.00 8 -23 0 15.90 4.60 -8 -23 0 9.80 5.20 8 -23 0 14.90 4.00 -8 -23 0 18.90 5.40 -8 23 0 19.70 4.40 8 23 0 18.60 4.70 9 -23 0 117.49 12.20 -9 -23 0 79.09 12.40 -9 -23 0 111.39 13.20 -9 23 0 100.39 9.50 9 23 0 117.69 11.70 10 -23 0 3.30 3.10 -10 -23 0 -0.10 3.40 -10 -23 0 3.50 4.10 -10 23 0 1.90 2.30 10 23 0 -0.80 2.60 0 -24 0 121.99 12.20 0 -24 0 105.89 11.00 0 24 0 107.09 7.30 0 24 0 106.99 7.90 1 -24 0 1.30 2.30 -1 -24 0 -1.30 1.50 1 -24 0 1.70 2.60 -1 -24 0 1.40 2.10 1 24 0 -0.70 1.70 -1 24 0 4.90 2.10 1 24 0 1.80 1.60 -1 24 0 0.20 1.30 -2 -24 0 105.69 11.40 2 -24 0 84.79 10.00 2 -24 0 89.59 10.20 -2 -24 0 87.79 10.80 2 24 0 122.09 7.30 -2 24 0 100.79 7.20 2 24 0 97.39 7.70 -2 24 0 114.29 7.70 3 -24 0 25.20 5.80 3 -24 0 33.10 6.30 -3 -24 0 30.80 6.20 -3 -24 0 27.20 6.20 -3 24 0 21.30 3.60 3 24 0 19.40 4.00 -4 -24 0 24.20 6.00 4 -24 0 23.60 5.40 -4 -24 0 30.20 6.30 4 -24 0 34.40 6.00 4 24 0 30.40 5.10 -4 24 0 20.20 3.80 5 -24 0 10.60 3.70 -5 -24 0 2.40 3.30 5 -24 0 4.00 3.10 -5 -24 0 -1.50 3.00 -5 24 0 1.80 2.00 5 24 0 3.30 2.50 6 -24 0 193.28 13.30 -6 -24 0 175.38 17.10 -6 -24 0 171.88 13.60 6 -24 0 150.98 11.30 -6 24 0 157.78 10.40 6 24 0 158.98 11.40 -7 -24 0 8.50 5.00 7 -24 0 14.00 4.10 -7 -24 0 5.80 3.90 7 -24 0 18.90 5.20 -7 24 0 17.30 3.60 -7 24 0 11.90 4.60 7 24 0 9.40 3.80 -8 -24 0 19.50 6.80 8 -24 0 15.20 4.60 8 -24 0 20.60 6.10 -8 -24 0 15.40 5.50 -8 24 0 12.80 3.70 8 24 0 12.30 4.10 9 -24 0 4.60 3.70 -9 -24 0 9.50 5.20 -9 -24 0 0.60 4.40 -9 24 0 2.50 2.50 9 24 0 1.60 2.40 0 -25 0 14.20 4.30 0 -25 0 8.40 3.10 0 25 0 4.00 1.80 0 25 0 5.20 2.40 -1 -25 0 142.49 11.80 1 -25 0 181.38 13.00 -1 -25 0 153.58 12.50 1 -25 0 197.18 13.20 1 25 0 138.19 9.00 -1 25 0 162.18 9.70 1 25 0 157.68 10.30 -1 25 0 162.38 10.10 2 -25 0 64.59 9.00 2 -25 0 79.19 9.60 -2 -25 0 67.89 9.30 -2 -25 0 67.09 9.40 -2 25 0 68.09 6.80 2 25 0 68.49 6.30 2 25 0 78.09 7.80 -2 25 0 71.99 7.20 3 -25 0 14.80 4.70 -3 -25 0 34.70 7.10 -3 -25 0 32.30 6.90 3 -25 0 25.30 5.80 3 25 0 27.30 4.80 -3 25 0 21.80 3.90 4 -25 0 190.98 13.10 -4 -25 0 183.38 13.90 4 -25 0 189.18 13.70 -4 -25 0 180.78 14.40 -4 25 0 176.08 10.70 4 25 0 165.78 11.50 5 -25 0 16.20 4.90 -5 -25 0 23.90 5.90 -5 -25 0 15.10 5.20 5 -25 0 20.10 4.90 5 25 0 11.40 3.80 -5 25 0 22.70 4.10 -6 -25 0 97.39 12.70 6 -25 0 89.29 10.60 6 -25 0 72.99 8.80 -6 -25 0 93.59 11.60 -6 25 0 90.79 8.70 6 25 0 91.99 9.60 7 -25 0 4.20 2.80 -7 -25 0 0.50 3.70 7 -25 0 5.50 3.30 -7 -25 0 3.00 3.80 7 25 0 0.70 2.40 -7 25 0 4.20 2.50 -8 -25 0 25.50 6.70 -8 -25 0 25.20 7.10 8 -25 0 15.20 5.10 8 25 0 13.20 4.20 -8 25 0 6.60 3.00 -9 -25 0 115.09 14.70 9 -25 0 100.59 11.70 -9 -25 0 107.09 13.20 -9 25 0 117.29 9.10 9 25 0 90.29 10.20 0 -26 0 63.59 8.60 0 -26 0 59.69 8.60 0 26 0 49.40 5.50 0 26 0 51.29 6.70 1 -26 0 51.09 8.20 -1 -26 0 29.70 6.40 -1 -26 0 27.80 5.80 1 -26 0 40.80 7.50 1 26 0 49.30 5.30 1 26 0 50.49 6.30 -1 26 0 34.80 4.80 -1 26 0 41.30 5.60 -2 -26 0 0.40 2.80 2 -26 0 -0.30 2.30 -2 -26 0 -0.40 2.70 2 -26 0 0.30 2.30 2 26 0 2.40 2.30 -2 26 0 2.30 2.10 -2 26 0 -0.30 1.50 3 -26 0 3.70 3.10 3 -26 0 7.60 3.80 -3 -26 0 8.70 4.30 -3 -26 0 2.10 3.10 -3 26 0 5.80 2.40 3 26 0 4.50 2.70 -4 -26 0 73.89 10.10 4 -26 0 59.89 8.80 4 -26 0 75.09 9.40 -4 -26 0 72.39 10.60 4 26 0 78.39 8.40 -4 26 0 81.99 7.80 5 -26 0 40.20 6.70 -5 -26 0 34.50 7.30 -5 -26 0 43.70 8.80 5 -26 0 29.30 6.20 5 26 0 29.40 5.70 -5 26 0 21.60 4.20 -6 -26 0 23.90 7.20 -6 -26 0 31.60 7.30 6 -26 0 18.50 5.50 6 -26 0 22.10 5.00 6 26 0 23.60 5.30 -6 26 0 17.90 3.80 -7 -26 0 36.10 8.60 7 -26 0 30.70 6.60 -7 -26 0 29.70 7.10 7 26 0 30.90 6.00 -7 26 0 22.40 4.40 8 -26 0 7.50 4.20 -8 -26 0 12.40 5.60 -8 -26 0 11.90 5.10 -8 26 0 4.90 2.60 8 26 0 8.80 3.10 0 -27 0 7.50 3.50 0 -27 0 5.60 3.40 0 27 0 3.30 1.80 0 27 0 4.90 2.60 -1 -27 0 26.40 6.30 1 -27 0 12.00 4.70 -1 -27 0 23.30 5.60 1 -27 0 33.00 7.00 -1 27 0 14.40 3.80 1 27 0 27.80 4.00 1 27 0 27.30 5.30 -1 27 0 15.10 3.30 -2 -27 0 4.90 3.60 -2 -27 0 3.40 3.40 2 -27 0 1.30 2.90 2 -27 0 6.40 3.90 2 27 0 4.00 2.60 -2 27 0 2.60 1.80 -2 27 0 3.00 2.50 3 -27 0 150.18 11.90 -3 -27 0 134.79 14.70 -3 -27 0 126.19 13.40 3 -27 0 117.49 12.60 3 27 0 131.99 10.00 -3 27 0 128.49 8.90 4 -27 0 -0.90 2.70 -4 -27 0 3.90 3.90 -4 -27 0 -2.10 2.40 4 -27 0 1.50 3.30 -4 27 0 -0.60 1.70 4 27 0 -2.20 1.90 5 -27 0 2.00 2.90 5 -27 0 2.80 2.90 -5 -27 0 -3.30 2.90 -5 -27 0 -1.80 3.30 5 27 0 -1.40 2.40 -5 27 0 1.20 2.00 6 -27 0 9.20 4.10 -6 -27 0 2.90 4.10 -6 -27 0 4.60 4.30 6 -27 0 5.70 3.90 -6 27 0 3.70 2.40 6 27 0 9.50 3.90 -7 -27 0 68.39 10.90 7 -27 0 69.69 9.70 -7 -27 0 63.39 11.00 -7 27 0 54.79 6.80 7 27 0 56.59 7.90 8 -27 0 5.90 3.30 -8 -27 0 2.50 3.90 -8 -27 0 6.00 4.40 8 27 0 4.20 2.40 -8 27 0 5.70 2.80 0 -28 0 14.10 4.90 0 -28 0 18.60 5.30 0 28 0 13.70 3.20 0 28 0 11.20 3.40 -1 -28 0 22.40 5.60 1 -28 0 15.40 5.30 -1 -28 0 34.50 7.20 1 -28 0 12.80 4.90 -1 28 0 24.20 4.20 1 28 0 30.60 5.50 1 28 0 22.60 3.90 -1 28 0 34.30 5.50 2 -28 0 103.09 11.80 2 -28 0 79.29 10.60 -2 -28 0 104.09 12.20 -2 -28 0 69.09 10.40 -2 28 0 99.29 7.60 2 28 0 103.19 9.90 -3 -28 0 4.90 3.40 3 -28 0 3.60 3.50 3 -28 0 6.30 3.70 -3 -28 0 2.60 3.60 -3 28 0 5.30 2.40 3 28 0 3.80 2.70 -4 -28 0 27.30 7.20 -4 -28 0 21.90 6.40 4 -28 0 23.30 5.70 4 -28 0 25.80 6.20 -4 28 0 17.10 3.90 4 28 0 16.50 4.90 -5 -28 0 3.00 3.90 5 -28 0 2.20 2.70 5 -28 0 6.60 3.80 -5 -28 0 0.10 3.90 5 28 0 3.60 3.30 -5 28 0 0.80 2.20 6 -28 0 70.39 10.20 -6 -28 0 54.29 9.60 -6 -28 0 64.89 11.30 -6 28 0 46.70 6.50 6 28 0 70.39 9.00 -7 -28 0 7.70 3.70 7 -28 0 -0.10 2.90 -7 -28 0 3.00 4.60 -7 28 0 3.30 2.60 7 28 0 2.70 3.70 0 -29 0 6.90 4.00 0 -29 0 8.80 4.30 0 29 0 1.90 2.30 0 29 0 5.40 2.40 1 -29 0 16.00 5.70 1 -29 0 18.10 5.50 -1 -29 0 19.00 5.90 -1 -29 0 11.90 5.20 1 29 0 14.50 3.90 -1 29 0 17.90 4.20 -1 29 0 19.60 3.80 -2 -29 0 41.20 8.30 2 -29 0 40.20 7.60 -2 -29 0 49.00 8.70 2 -29 0 30.60 6.90 2 29 0 42.60 6.50 -2 29 0 36.60 5.40 3 -29 0 86.29 11.30 3 -29 0 112.59 12.40 -3 -29 0 102.39 12.50 -3 -29 0 74.59 11.80 3 29 0 107.59 10.80 -3 29 0 97.39 9.00 4 -29 0 28.90 6.10 -4 -29 0 63.09 10.50 4 -29 0 33.20 7.30 -4 -29 0 35.40 8.00 4 29 0 37.00 6.50 -4 29 0 43.80 5.90 5 -29 0 10.10 4.70 -5 -29 0 24.10 6.90 -5 -29 0 11.00 5.60 -5 29 0 13.50 3.70 5 29 0 1.90 2.80 6 -29 0 -2.40 2.80 -6 -29 0 6.20 4.40 -6 -29 0 5.70 4.80 -6 29 0 4.30 2.70 6 29 0 2.10 2.70 0 -30 0 93.19 12.30 0 -30 0 146.59 15.00 0 30 0 119.79 8.60 0 30 0 112.99 10.90 1 -30 0 -0.70 2.90 -1 -30 0 1.60 3.20 -1 -30 0 3.50 3.70 1 -30 0 1.20 3.10 -1 30 0 0.80 2.30 1 30 0 0.60 2.40 -1 30 0 3.40 2.20 2 -30 0 17.90 5.80 -2 -30 0 14.60 5.60 -2 -30 0 12.70 4.80 2 -30 0 22.40 6.20 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95.99 6.80 8 -12 -3 89.19 7.20 -8 -12 3 96.99 9.70 8 -12 -3 90.79 8.60 -8 -12 3 94.49 9.70 -8 12 3 94.89 6.40 8 12 -3 94.09 9.80 8 12 -3 85.49 6.90 -8 12 3 93.69 9.00 7 -12 -3 16.90 3.90 -7 -12 3 8.80 3.00 -7 -12 3 19.10 3.80 7 -12 -3 23.80 4.00 7 -12 -3 16.80 2.90 -7 12 3 12.80 2.60 -7 12 3 13.10 3.50 7 12 -3 11.00 2.60 7 12 -3 17.70 4.10 -6 -12 3 80.89 7.90 6 -12 -3 87.49 6.90 6 -12 -3 83.29 6.80 6 -12 -3 91.99 5.80 -6 -12 3 91.19 7.00 6 12 -3 94.69 7.60 6 12 -3 83.59 6.40 -6 12 3 87.79 5.90 -6 12 3 105.59 7.70 -5 -12 3 194.68 11.00 -5 -12 3 196.18 11.40 5 -12 -3 200.08 11.40 5 -12 -3 203.38 9.50 5 -12 -3 194.68 11.00 -5 12 3 200.48 10.10 5 12 -3 202.08 11.70 5 12 -3 185.18 10.40 4 -12 -3 112.29 5.90 4 -12 -3 111.39 7.90 4 -12 -3 119.99 7.70 -4 -12 3 114.79 7.40 -4 -12 3 110.49 7.80 4 12 -3 118.39 4.70 -4 12 3 120.19 6.90 4 12 -3 115.99 8.10 4 12 -3 102.19 6.90 -4 12 3 118.39 5.20 3 -12 -3 80.69 5.80 3 -12 -3 80.59 6.30 -3 -12 3 76.19 5.90 3 -12 -3 65.49 3.70 -3 -12 3 75.59 5.50 3 12 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1.90 10 13 -3 0.80 2.60 10 13 -3 2.40 2.20 -9 -13 3 42.00 6.70 9 -13 -3 47.60 6.20 9 -13 -3 46.70 5.80 -9 -13 3 49.00 7.00 9 -13 -3 62.19 7.70 9 13 -3 51.09 6.20 9 13 -3 37.60 6.70 -9 13 3 45.20 5.30 -9 13 3 48.80 6.60 8 -13 -3 108.49 8.10 8 -13 -3 98.19 8.00 8 -13 -3 98.69 7.00 -8 -13 3 107.69 10.20 -8 -13 3 99.89 10.10 -8 13 3 112.29 8.50 -8 13 3 103.99 6.90 8 13 -3 94.19 7.40 8 13 -3 89.79 9.80 7 -13 -3 6.00 2.50 7 -13 -3 7.50 2.60 7 -13 -3 5.80 2.00 -7 -13 3 6.50 2.90 -7 -13 3 5.90 2.70 -7 13 3 5.30 2.60 7 13 -3 6.00 2.30 -7 13 3 4.10 1.80 7 13 -3 4.00 2.60 6 -13 -3 204.38 11.80 6 -13 -3 193.48 9.90 -6 -13 3 199.88 11.80 -6 -13 3 209.88 12.20 6 -13 -3 201.08 11.70 6 13 -3 188.38 12.00 6 13 -3 182.68 10.80 -6 13 3 206.18 10.50 5 -13 -3 68.09 4.30 5 -13 -3 54.89 6.10 5 -13 -3 54.79 6.30 -5 -13 3 49.99 6.20 -5 -13 3 64.99 6.60 5 13 -3 63.69 6.20 -5 13 3 66.29 4.90 5 13 -3 62.79 7.00 -4 -13 3 3.00 1.60 -4 -13 3 5.10 2.10 4 -13 -3 4.80 2.20 4 -13 -3 5.00 1.30 4 -13 -3 5.00 2.00 -4 13 3 4.00 0.90 4 13 -3 5.40 1.80 4 13 -3 4.20 2.10 -4 13 3 3.00 1.40 4 13 -3 3.80 1.00 3 -13 -3 3.80 1.80 3 -13 -3 3.50 0.90 3 -13 -3 4.00 2.20 -3 -13 3 2.60 1.60 -3 -13 3 3.40 1.90 -3 13 3 4.30 1.70 3 13 -3 1.30 1.60 3 13 -3 6.10 1.90 -3 13 3 3.50 0.90 3 13 -3 4.20 0.80 2 -13 -3 136.29 9.20 -2 -13 3 142.59 8.90 -2 -13 3 134.19 8.00 -2 -13 3 133.29 8.60 2 -13 -3 137.29 5.80 2 -13 -3 137.59 8.50 -2 13 3 129.49 6.50 2 13 -3 131.19 7.70 2 13 -3 140.69 6.10 2 13 -3 143.09 8.80 -2 13 3 122.79 7.60 1 -13 -3 7.50 2.70 -1 -13 3 8.30 2.00 -1 -13 3 8.20 2.50 -1 -13 3 6.40 2.10 1 -13 -3 5.50 2.00 -1 13 3 5.20 1.30 1 13 -3 7.00 1.20 -1 13 3 8.50 2.00 1 13 -3 3.80 1.50 0 -13 -3 223.48 11.80 0 -13 3 226.08 11.90 0 -13 3 221.88 12.10 0 -13 -3 232.48 12.90 0 -13 -3 209.68 10.90 0 -13 3 222.68 11.00 0 13 -3 218.38 11.00 0 13 3 231.48 10.20 0 13 3 215.88 11.10 0 13 -3 216.98 9.70 -1 -13 -3 17.60 3.50 1 -13 3 16.40 3.20 1 -13 3 13.90 2.50 -1 -13 -3 24.10 3.30 -1 -13 -3 19.90 3.20 1 -13 3 13.00 2.90 1 13 3 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2.40 5 -15 -3 3.30 2.20 -5 -15 3 3.60 1.80 5 -15 -3 6.90 2.60 5 15 -3 4.80 1.90 -5 15 3 2.50 1.60 5 15 -3 5.50 2.60 4 -15 -3 41.90 3.00 -4 -15 3 36.20 5.00 4 -15 -3 43.20 5.90 -4 -15 3 40.90 5.60 4 -15 -3 50.99 6.00 -4 15 3 37.10 2.70 4 15 -3 32.70 4.30 4 15 -3 43.60 5.90 -4 15 3 31.00 4.10 3 -15 -3 113.29 8.00 3 -15 -3 108.89 8.40 3 -15 -3 111.49 5.40 -3 -15 3 118.19 8.50 -3 -15 3 112.39 8.30 -3 -15 3 119.79 8.00 3 15 -3 112.49 7.40 -3 15 3 111.59 7.10 -3 15 3 114.19 5.80 3 15 -3 116.29 8.20 3 15 -3 113.19 5.30 2 -15 -3 1.70 1.60 -2 -15 3 0.80 1.50 -2 -15 3 6.70 2.40 2 -15 -3 1.40 1.90 -2 -15 3 0.60 1.30 2 -15 -3 0.50 0.50 2 15 -3 0.80 0.60 -2 15 3 -0.20 0.90 2 15 -3 1.20 1.50 -2 15 3 1.30 0.80 2 15 -3 1.30 1.30 1 -15 -3 124.49 9.00 -1 -15 3 142.79 8.90 -1 -15 3 163.88 9.90 1 -15 -3 161.08 10.50 -1 -15 3 163.48 9.80 1 15 -3 151.58 7.20 -1 15 3 158.68 7.70 -1 15 3 164.18 8.90 1 15 -3 140.19 8.60 0 -15 -3 28.90 4.40 0 -15 3 33.00 4.60 0 -15 3 26.90 4.20 0 -15 3 26.10 3.70 0 -15 -3 28.00 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26 -3 10.00 3.30 8 -27 -3 0.00 2.80 -8 -27 3 3.20 3.90 8 -27 -3 5.10 3.50 -8 -27 3 5.70 4.50 8 27 -3 3.90 2.70 -8 27 3 2.40 3.50 -8 27 3 1.70 2.20 7 -27 -3 0.40 2.90 -7 -27 3 5.20 3.90 7 -27 -3 -1.50 2.70 -7 -27 3 3.40 4.00 7 27 -3 0.50 2.40 -7 27 3 6.50 3.00 6 -27 -3 54.99 8.60 6 -27 -3 55.19 8.80 -6 -27 3 49.30 9.00 -6 -27 3 67.19 10.90 6 27 -3 41.30 7.50 -6 27 3 44.50 6.50 -5 -27 3 -3.80 2.50 5 -27 -3 0.90 3.30 -5 -27 3 0.40 2.70 5 -27 -3 0.00 2.60 5 27 -3 -0.10 2.70 -5 27 3 3.90 2.40 4 -27 -3 5.10 3.70 -4 -27 3 11.20 5.00 4 -27 -3 7.00 3.70 -4 -27 3 6.00 4.20 4 27 -3 0.30 2.70 -4 27 3 7.30 2.70 3 -27 -3 19.60 5.50 -3 -27 3 25.00 6.20 -3 -27 3 13.50 5.00 3 -27 -3 18.60 5.80 -3 27 3 12.80 3.50 3 27 -3 16.90 4.70 2 -27 -3 1.50 2.30 -2 -27 3 1.40 3.20 -2 -27 3 0.30 2.20 2 -27 -3 0.70 2.70 -2 27 3 0.20 1.70 2 27 -3 0.30 2.40 -1 -27 3 142.39 14.70 -1 -27 3 142.29 11.80 1 -27 -3 144.99 14.30 1 -27 -3 163.88 15.80 1 27 -3 160.78 11.60 -1 27 3 147.69 10.00 -1 27 3 149.29 9.70 0 -27 -3 5.70 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7.60 -9 21 -4 50.79 6.90 10 -22 -4 25.50 6.10 10 -22 -4 13.80 4.60 -10 -22 4 19.10 6.80 -10 -22 4 10.20 4.10 -10 22 4 13.30 3.40 -10 22 4 8.90 3.40 10 22 -4 20.60 5.00 9 -22 -4 0.30 2.70 -9 -22 4 0.40 3.70 -9 -22 4 -3.10 3.00 9 -22 -4 1.60 2.60 9 22 -4 2.90 3.50 -9 22 4 6.20 3.30 -9 22 4 2.10 2.50 8 -22 -4 6.80 3.40 -8 -22 4 8.70 4.40 -8 -22 4 15.10 5.30 8 -22 -4 8.50 3.80 -8 22 4 11.00 3.20 8 22 -4 8.20 3.70 -8 22 4 12.60 4.50 -7 -22 4 1.10 3.20 -7 -22 4 2.50 2.60 7 -22 -4 -1.50 2.10 7 -22 -4 1.90 2.50 7 22 -4 5.10 3.00 7 22 -4 1.90 3.60 -7 22 4 2.30 2.30 -6 -22 4 77.49 9.70 -6 -22 4 49.90 8.00 6 -22 -4 59.39 8.00 6 -22 -4 61.19 8.70 6 22 -4 66.89 8.70 6 22 -4 44.60 6.70 -6 22 4 50.89 6.40 -5 -22 4 39.50 7.00 5 -22 -4 41.70 7.10 5 -22 -4 37.00 6.40 -5 -22 4 24.50 5.50 5 22 -4 34.80 6.50 -5 22 4 45.90 5.90 5 22 -4 32.40 5.70 -4 -22 4 14.20 4.20 4 -22 -4 18.50 4.90 -4 -22 4 21.90 5.30 4 -22 -4 21.40 5.00 -4 -22 4 33.50 6.70 4 22 -4 24.20 4.90 -4 22 4 20.50 3.90 4 22 -4 20.30 5.00 -3 -22 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6.00 9 23 -4 33.00 6.60 -9 23 4 46.70 7.70 -8 -23 4 11.20 4.90 8 -23 -4 6.80 3.60 8 -23 -4 8.30 4.10 -8 -23 4 8.90 4.60 -8 23 4 9.70 3.20 8 23 -4 9.50 3.90 -8 23 4 16.20 5.00 -7 -23 4 24.00 5.70 -7 -23 4 30.10 6.70 7 -23 -4 30.00 6.10 7 -23 -4 24.20 5.80 -7 23 4 28.40 4.90 7 23 -4 28.60 5.70 -6 -23 4 43.90 7.60 6 -23 -4 53.89 7.70 6 -23 -4 62.39 8.70 -6 -23 4 62.09 9.20 6 23 -4 64.89 8.10 -6 23 4 64.79 7.10 5 -23 -4 12.70 4.30 -5 -23 4 14.00 4.70 5 -23 -4 18.70 4.80 -5 -23 4 13.70 4.50 5 23 -4 16.00 4.10 -5 23 4 15.60 3.80 4 -23 -4 178.08 13.40 4 -23 -4 178.88 12.70 -4 -23 4 139.19 14.20 -4 -23 4 180.68 12.90 -4 23 4 174.98 11.00 4 23 -4 183.18 12.20 4 23 -4 146.99 17.50 3 -23 -4 0.50 2.60 3 -23 -4 0.80 2.10 -3 -23 4 0.40 2.10 -3 -23 4 2.20 2.80 -3 23 4 0.30 1.80 3 23 -4 3.20 2.80 -2 -23 4 2.00 2.90 2 -23 -4 2.80 3.20 2 -23 -4 2.40 2.60 -2 -23 4 1.10 2.10 -2 23 4 3.50 2.30 -2 23 4 8.50 2.30 2 23 -4 1.80 2.50 1 -23 -4 52.99 8.40 1 -23 -4 47.20 7.10 -1 -23 4 51.09 7.00 -1 -23 4 43.60 7.00 -1 23 4 52.49 5.60 1 23 -4 58.19 7.20 1 23 -4 57.19 5.00 -1 23 4 69.49 7.20 0 -23 -4 8.80 4.00 0 -23 4 10.30 3.90 0 -23 -4 13.60 4.20 0 -23 4 9.40 3.40 0 -23 4 12.40 3.90 0 23 -4 12.10 3.70 0 23 4 12.40 3.50 0 23 -4 13.90 2.60 0 23 4 8.80 2.60 -1 -23 -4 252.87 16.10 1 -23 4 242.08 15.00 -1 -23 -4 284.37 18.20 1 -23 4 264.67 16.30 1 23 4 262.97 14.40 -1 23 -4 250.17 14.90 1 23 4 270.37 13.80 -1 23 -4 270.37 12.90 -2 -23 -4 26.80 5.60 2 -23 4 28.70 5.90 -2 -23 -4 24.20 6.40 2 -23 4 31.20 5.20 -2 23 -4 27.90 5.00 -2 23 -4 29.70 4.10 2 23 4 25.20 4.60 2 23 4 30.50 4.70 -3 -23 -4 10.70 4.70 3 -23 4 1.90 3.10 -3 -23 -4 10.40 3.70 3 -23 4 4.80 2.80 3 23 4 4.70 2.20 -3 23 -4 6.80 2.10 -3 23 -4 5.20 2.70 3 23 4 4.90 2.60 -4 -23 -4 -1.50 2.40 4 -23 4 -1.10 1.70 -4 -23 -4 -1.30 2.50 4 -23 4 0.20 2.30 -4 -23 -4 1.90 2.00 -4 23 -4 0.20 1.70 4 23 4 0.30 1.80 4 23 4 0.00 1.90 -5 -23 -4 1.60 2.10 5 -23 4 1.70 2.10 5 -23 4 -2.90 1.60 -5 -23 -4 0.40 2.80 -5 -23 -4 -1.80 2.40 5 23 4 -0.20 2.00 -5 23 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2.90 -4 -24 4 -1.60 2.30 4 -24 -4 3.20 2.90 -4 -24 4 4.80 3.30 4 24 -4 2.80 2.40 -4 24 4 4.90 2.30 3 -24 -4 1.80 2.30 -3 -24 4 4.20 3.20 3 -24 -4 1.30 2.80 -3 -24 4 0.80 2.90 -3 24 4 2.30 2.10 3 24 -4 0.70 2.00 2 -24 -4 102.79 11.00 2 -24 -4 84.69 11.00 -2 -24 4 106.39 10.60 -2 -24 4 93.69 10.90 2 24 -4 83.49 9.20 -2 24 4 84.59 6.40 -2 24 4 88.29 8.60 -1 -24 4 209.28 13.40 1 -24 -4 225.38 15.70 -1 -24 4 200.48 14.40 1 -24 -4 211.48 14.30 -1 24 4 215.68 12.60 -1 24 4 196.78 11.20 1 24 -4 202.68 13.20 0 -24 -4 17.50 5.10 0 -24 -4 21.10 4.90 0 -24 4 17.40 4.90 0 24 4 20.80 3.80 0 24 -4 23.30 4.80 0 24 -4 23.30 3.30 0 24 4 18.00 3.90 -1 -24 -4 3.50 3.60 1 -24 4 4.80 3.20 -1 -24 -4 2.80 2.60 -1 24 -4 1.80 1.60 -1 24 -4 -1.40 1.90 1 24 4 2.60 2.20 1 24 4 2.80 2.10 2 -24 4 99.99 11.20 -2 -24 -4 132.19 12.40 -2 -24 -4 75.09 11.00 2 24 4 98.19 9.10 -2 24 -4 90.39 6.70 -2 24 -4 92.89 9.40 2 24 4 109.79 7.80 -3 -24 -4 6.20 3.20 3 -24 4 2.70 3.10 -3 -24 -4 0.80 2.90 -3 24 -4 1.70 1.60 -3 24 -4 3.20 2.20 3 24 4 6.10 2.60 3 24 4 5.30 2.80 4 -24 4 -1.40 2.40 4 -24 4 4.50 4.00 -4 -24 -4 4.70 3.70 -4 -24 -4 1.90 2.70 -4 24 -4 -1.10 1.60 4 24 4 1.00 2.30 4 24 4 2.20 2.20 5 -24 4 15.00 4.00 5 -24 4 16.80 4.50 -5 -24 -4 19.50 5.50 -5 -24 -4 14.40 5.30 5 24 4 13.30 3.90 -5 24 -4 13.90 3.40 6 -24 4 112.29 11.50 6 -24 4 106.79 10.10 -6 -24 -4 117.99 12.50 -6 -24 -4 88.09 13.10 -6 24 -4 114.49 8.40 6 24 4 110.69 9.00 7 -24 4 31.70 6.00 7 -24 4 41.10 6.20 -7 -24 -4 30.10 7.90 7 24 4 27.80 5.50 -7 24 -4 44.90 6.30 -8 -24 -4 -2.20 3.90 8 -24 4 0.30 3.00 8 24 4 0.00 1.80 -8 24 -4 1.70 2.00 -9 -25 4 60.29 9.70 9 -25 -4 60.39 8.80 -9 -25 4 85.09 12.00 9 -25 -4 64.89 9.30 9 25 -4 52.49 8.60 -9 25 4 62.69 8.90 -9 25 4 62.19 7.80 8 -25 -4 2.00 2.70 -8 -25 4 4.20 3.70 -8 -25 4 2.80 4.30 8 -25 -4 2.80 3.20 8 25 -4 3.30 2.80 -8 25 4 0.00 2.20 -8 25 4 4.90 3.80 7 -25 -4 2.20 3.50 -7 -25 4 3.00 4.00 -7 -25 4 4.10 4.00 7 -25 -4 1.30 3.50 7 25 -4 0.10 2.70 -7 25 4 5.40 2.80 -6 -25 4 7.00 4.10 6 -25 -4 9.30 4.10 6 -25 -4 7.40 4.20 -6 -25 4 2.70 3.50 -6 25 4 3.90 2.60 6 25 -4 6.10 3.50 -5 -25 4 4.30 3.50 5 -25 -4 5.80 3.30 5 -25 -4 4.50 3.20 -5 -25 4 0.40 2.70 -5 25 4 4.90 2.60 5 25 -4 4.30 3.10 -4 -25 4 21.30 5.60 4 -25 -4 27.40 6.80 4 -25 -4 19.40 4.90 -4 -25 4 21.90 5.60 4 25 -4 21.80 4.90 -4 25 4 22.80 4.40 3 -25 -4 69.99 9.70 -3 -25 4 50.09 8.20 3 -25 -4 58.79 8.70 -3 -25 4 57.39 8.40 -3 25 4 62.09 7.10 3 25 -4 62.09 8.00 -2 -25 4 52.69 7.60 2 -25 -4 63.89 8.90 -2 -25 4 58.09 8.80 2 -25 -4 68.49 9.70 2 25 -4 56.49 7.60 -2 25 4 67.99 6.40 -2 25 4 43.40 5.90 1 -25 -4 64.89 8.90 1 -25 -4 52.39 8.60 -1 -25 4 49.20 8.20 1 25 -4 44.10 6.80 -1 25 4 51.89 6.40 -1 25 4 51.09 5.90 0 -25 -4 29.00 5.90 0 -25 4 25.90 5.80 0 -25 -4 26.60 6.60 0 25 -4 32.60 4.00 0 25 4 26.60 4.60 0 25 4 16.30 3.50 0 25 -4 31.40 5.60 -1 -25 -4 91.69 10.80 1 -25 4 102.69 11.30 -1 -25 -4 109.99 13.20 -1 25 -4 111.09 7.20 1 25 4 103.59 7.80 -1 25 -4 104.49 10.30 1 25 4 106.79 8.20 -2 -25 -4 1.70 2.50 -2 -25 -4 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4.10 5 -26 -4 -2.90 2.00 -5 -26 4 -0.90 2.90 -5 -26 4 -0.30 2.60 5 -26 -4 -2.30 2.30 5 26 -4 3.20 3.30 -5 26 4 -1.90 1.60 -4 -26 4 10.40 4.10 4 -26 -4 4.50 2.70 -4 -26 4 6.00 4.40 4 -26 -4 8.60 4.30 -4 26 4 6.50 2.90 4 26 -4 13.30 4.40 -3 -26 4 92.59 10.90 3 -26 -4 100.09 11.50 3 -26 -4 114.19 13.10 -3 -26 4 90.59 11.30 3 26 -4 97.69 10.50 -3 26 4 90.29 8.90 2 -26 -4 17.10 4.90 -2 -26 4 10.20 6.10 -2 -26 4 15.20 5.30 2 -26 -4 17.30 5.00 -2 26 4 16.00 3.90 -2 26 4 12.20 3.80 2 26 -4 18.80 4.80 1 -26 -4 3.40 3.20 -1 -26 4 8.20 3.70 1 -26 -4 5.40 3.80 -1 26 4 9.00 2.90 1 26 -4 11.90 4.20 -1 26 4 5.20 2.50 0 -26 -4 3.20 3.50 0 -26 4 8.70 4.00 0 -26 -4 1.10 2.10 0 26 -4 8.50 3.60 0 26 -4 6.30 2.30 0 26 4 8.60 2.70 0 26 4 4.50 2.60 1 -26 4 27.50 6.10 -1 -26 -4 31.80 6.80 -1 -26 -4 26.30 6.80 -1 26 -4 34.20 5.90 1 26 4 35.60 5.10 1 26 4 35.10 5.30 -1 26 -4 34.50 4.40 -2 -26 -4 2.50 3.00 2 -26 4 0.80 3.20 -2 -26 -4 -0.60 2.80 -2 26 -4 -0.70 1.70 2 26 4 3.20 2.30 2 26 4 1.60 2.50 -2 26 -4 1.40 2.20 3 -26 4 3.30 2.80 -3 -26 -4 0.90 3.00 -3 -26 -4 3.20 4.30 -3 26 -4 3.00 2.40 3 26 4 0.10 2.00 3 26 4 2.50 2.40 -4 -26 -4 177.78 15.60 -4 -26 -4 116.99 14.60 4 -26 4 145.99 13.80 4 26 4 138.89 10.30 -4 26 -4 126.89 9.00 5 -26 4 13.70 4.70 -5 -26 -4 10.20 5.40 -5 -26 -4 8.50 4.20 -5 26 -4 11.00 3.00 5 26 4 7.90 3.50 -6 -26 -4 32.70 9.20 6 -26 4 26.70 6.00 -6 -26 -4 25.40 7.00 -6 26 -4 24.90 4.60 6 26 4 37.10 6.20 7 -26 4 21.80 5.50 -7 -26 -4 25.60 7.70 -7 26 -4 29.70 5.40 7 26 4 27.00 5.90 -8 -27 4 2.60 4.10 8 -27 -4 0.10 3.00 -8 -27 4 10.10 5.50 8 -27 -4 2.80 2.90 8 27 -4 2.20 3.20 -8 27 4 6.60 3.40 -8 27 4 3.30 2.70 7 -27 -4 8.20 4.00 -7 -27 4 6.40 3.80 7 -27 -4 18.70 5.60 -7 -27 4 15.70 5.80 -7 27 4 13.40 4.00 7 27 -4 5.50 2.70 6 -27 -4 1.60 3.10 6 -27 -4 6.20 4.60 -6 -27 4 5.40 4.10 -6 -27 4 5.60 4.20 6 27 -4 -0.70 3.00 -6 27 4 6.80 3.10 5 -27 -4 64.89 9.90 -5 -27 4 67.39 10.10 5 -27 -4 73.99 10.10 -5 -27 4 86.59 11.60 5 27 -4 55.89 8.70 -5 27 4 69.89 8.00 4 -27 -4 6.20 3.60 -4 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43.90 6.80 2 -23 -5 30.20 6.60 -2 23 5 30.50 4.10 -2 23 5 32.50 5.20 2 23 -5 26.30 5.20 -1 -23 5 0.00 1.90 1 -23 -5 0.20 2.60 1 -23 -5 1.30 2.50 -1 -23 5 0.10 2.30 -1 23 5 -0.80 1.10 1 23 -5 3.50 2.70 -1 23 5 0.90 1.70 0 -23 5 118.79 12.30 0 -23 5 108.39 11.00 0 -23 -5 147.29 14.60 0 -23 -5 123.69 11.70 0 23 5 121.79 9.20 0 23 -5 125.79 9.90 0 23 5 125.89 8.10 0 23 -5 125.59 7.40 -1 -23 -5 16.80 4.50 1 -23 5 13.50 4.00 1 -23 5 14.80 4.30 -1 -23 -5 15.70 5.10 1 23 5 13.70 3.20 -1 23 -5 10.10 3.50 1 23 5 17.60 3.90 -1 23 -5 14.70 2.90 -2 -23 -5 214.48 14.30 2 -23 5 207.98 13.80 2 -23 5 199.78 14.10 -2 -23 -5 201.08 15.70 -2 -23 -5 242.08 13.60 -2 23 -5 234.68 14.10 -2 23 -5 216.38 11.50 2 23 5 230.58 13.40 2 23 5 218.48 12.30 3 -23 5 1.30 2.50 -3 -23 -5 0.10 1.90 3 -23 5 -0.40 2.00 -3 -23 -5 -2.30 1.70 -3 -23 -5 1.00 3.10 -3 23 -5 0.70 1.80 -3 23 -5 1.30 2.10 3 23 5 -0.20 2.00 3 23 5 0.50 1.80 4 -23 5 4.20 3.20 -4 -23 -5 2.70 3.20 -4 -23 -5 8.30 3.20 -4 -23 -5 3.20 3.00 4 -23 5 4.10 2.60 4 23 5 2.20 2.10 4 23 5 6.10 2.90 -4 23 -5 2.60 1.90 5 -23 5 2.00 2.60 -5 -23 -5 4.40 4.20 5 -23 5 1.10 2.40 -5 -23 -5 1.10 2.30 -5 -23 -5 1.30 3.00 5 23 5 -0.60 2.10 -5 23 -5 2.10 1.90 6 -23 5 1.40 2.50 6 -23 5 3.90 2.70 -6 -23 -5 3.00 3.60 6 23 5 3.90 2.60 -6 23 -5 2.40 2.50 -7 -23 -5 0.50 4.00 7 -23 5 -0.20 2.20 -7 23 -5 1.70 2.50 7 23 5 2.30 2.60 -8 -23 -5 1.40 2.70 8 -23 5 0.50 2.30 -8 23 -5 4.20 2.00 8 23 5 -1.70 2.10 -9 -24 5 21.00 6.30 -9 -24 5 47.30 9.10 9 -24 -5 45.00 7.80 9 -24 -5 28.90 6.40 9 24 -5 30.90 6.50 -9 24 5 31.00 5.40 -9 24 5 29.70 6.50 -8 -24 5 6.90 4.50 8 -24 -5 2.90 3.30 -8 -24 5 2.10 3.70 8 -24 -5 -0.50 2.40 -8 24 5 5.00 3.80 -8 24 5 6.80 3.10 8 24 -5 7.20 3.70 7 -24 -5 95.19 11.50 -7 -24 5 83.49 11.20 -7 -24 5 71.19 10.80 7 -24 -5 84.79 10.50 -7 24 5 83.49 8.60 7 24 -5 111.19 11.80 6 -24 -5 -0.50 2.80 -6 -24 5 0.60 3.10 -6 -24 5 1.90 3.30 6 -24 -5 -0.70 2.50 6 24 -5 2.50 2.90 -6 24 5 -2.10 1.40 -5 -24 5 3.80 3.20 5 -24 -5 15.30 4.70 -5 -24 5 2.80 3.20 5 -24 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5 15.40 4.00 6 25 -5 9.50 4.20 -5 -25 5 24.70 7.20 5 -25 -5 41.70 8.00 5 -25 -5 27.70 6.10 -5 -25 5 43.20 7.60 -5 25 5 30.70 5.00 5 25 -5 18.70 5.50 -4 -25 5 123.19 13.40 -4 -25 5 102.99 12.20 4 -25 -5 95.39 11.20 4 -25 -5 97.59 12.00 4 25 -5 107.09 11.30 -4 25 5 89.29 9.00 3 -25 -5 81.69 10.10 -3 -25 5 78.09 10.60 3 -25 -5 91.69 11.90 -3 25 5 75.19 8.40 3 25 -5 72.79 9.20 2 -25 -5 24.00 6.30 2 -25 -5 20.30 5.10 -2 -25 5 19.20 5.60 -2 25 5 12.00 3.70 -2 25 5 17.80 3.30 2 25 -5 20.30 4.90 1 -25 -5 11.50 5.20 -1 -25 5 17.30 5.20 1 -25 -5 7.40 3.40 -1 25 5 9.80 2.90 1 25 -5 12.60 4.10 -1 25 5 11.80 3.40 0 -25 -5 37.50 8.10 0 -25 -5 64.89 8.70 0 -25 5 40.90 7.30 0 25 5 40.60 6.10 0 25 -5 40.80 6.70 0 25 5 51.49 6.20 -1 -25 -5 -0.40 2.60 1 -25 5 2.90 3.00 -1 -25 -5 -0.90 2.00 1 25 5 1.10 1.80 -1 25 -5 -0.20 2.20 1 25 5 4.00 2.40 -1 25 -5 1.90 1.70 -2 -25 -5 85.29 11.50 -2 -25 -5 61.59 8.50 2 -25 5 62.79 8.90 2 25 5 60.49 7.30 -2 25 -5 80.19 9.30 2 25 5 84.89 8.10 -2 25 -5 66.49 6.50 -3 -25 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7 39.60 3.80 -7 4 7 27.70 4.50 6 -4 -7 2.10 1.30 6 -4 -7 -0.30 1.30 -6 -4 7 2.20 1.20 6 -4 -7 -1.10 0.90 -6 -4 7 0.50 1.50 6 -4 -7 -0.90 1.00 6 4 -7 -1.00 1.40 -6 4 7 0.60 1.00 -6 4 7 1.00 1.50 6 4 -7 0.00 1.80 5 -4 -7 88.19 6.50 5 -4 -7 102.79 6.50 5 -4 -7 98.19 6.70 5 -4 -7 87.49 7.10 -5 -4 7 112.69 6.40 -5 -4 7 93.09 6.80 -5 -4 7 105.19 5.00 5 4 -7 100.19 7.20 -5 4 7 109.69 6.40 -5 4 7 97.89 6.90 5 4 -7 95.19 8.00 5 4 -7 93.59 4.90 4 -4 -7 2.10 1.50 4 -4 -7 1.30 1.10 -4 -4 7 3.40 1.50 4 -4 -7 4.30 1.50 4 -4 -7 2.90 1.40 4 -4 -7 3.70 1.40 -4 -4 7 3.30 1.20 -4 4 7 5.60 1.80 -4 4 7 3.40 1.40 4 4 -7 7.10 2.30 4 4 -7 3.40 1.10 4 4 -7 3.80 2.10 3 -4 -7 18.60 3.00 3 -4 -7 15.30 2.60 3 -4 -7 20.10 3.30 3 -4 -7 17.10 2.90 3 -4 -7 17.00 2.80 -3 -4 7 14.30 2.50 -3 -4 7 19.70 2.30 3 4 -7 17.50 3.30 3 4 -7 24.30 2.80 3 4 -7 18.70 3.90 -2 -4 7 1.00 0.70 2 -4 -7 -0.70 0.80 2 -4 -7 0.10 1.00 2 -4 -7 1.50 1.30 2 -4 -7 -0.40 0.80 -2 -4 7 0.80 1.40 -2 -4 7 0.10 0.70 2 -4 -7 -0.60 0.70 -2 4 7 -1.10 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14 -7 63.39 9.10 -6 -14 7 33.20 5.70 -6 -14 7 27.00 4.50 6 -14 -7 28.90 5.40 6 -14 -7 20.60 4.10 6 14 -7 29.60 6.10 6 14 -7 33.80 5.80 -6 14 7 28.30 4.50 5 -14 -7 31.00 5.00 5 -14 -7 33.20 5.80 -5 -14 7 30.20 5.30 -5 -14 7 41.00 5.10 5 14 -7 24.10 4.70 -5 14 7 39.30 5.30 5 14 -7 36.30 6.80 -4 -14 7 1.10 1.40 -4 -14 7 1.10 2.40 4 -14 -7 1.10 1.80 -4 -14 7 2.10 2.10 4 -14 -7 3.00 2.30 4 14 -7 -1.40 1.50 4 14 -7 3.20 2.60 -4 14 7 2.20 1.90 -4 14 7 3.90 1.40 -3 -14 7 68.19 7.30 3 -14 -7 60.29 7.90 -3 -14 7 63.19 8.30 3 -14 -7 62.19 6.60 3 -14 -7 51.29 5.80 -3 -14 7 59.99 5.70 -3 14 7 55.29 4.10 -3 14 7 60.59 6.50 3 14 -7 54.69 7.10 3 14 -7 56.39 7.90 -2 -14 7 86.69 5.70 2 -14 -7 83.99 9.20 2 -14 -7 81.79 6.40 2 -14 -7 90.99 7.00 -2 -14 7 91.29 7.20 -2 -14 7 84.89 9.90 2 14 -7 101.09 9.60 -2 14 7 79.39 7.70 2 14 -7 88.09 5.20 -2 14 7 74.49 5.30 2 14 -7 96.69 10.50 1 -14 -7 11.00 2.80 -1 -14 7 7.40 3.10 -1 -14 7 13.00 3.30 1 -14 -7 9.00 2.60 1 -14 -7 15.80 4.10 -1 14 7 15.70 2.60 -1 14 7 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20 -7 29.50 6.50 5 20 -7 34.20 6.50 -4 -20 7 4.00 2.70 4 -20 -7 4.50 2.50 4 -20 -7 0.80 2.20 -4 -20 7 1.40 2.60 4 20 -7 1.40 2.50 -4 20 7 6.50 2.70 4 20 -7 6.80 3.20 3 -20 -7 22.90 4.70 3 -20 -7 36.50 7.10 -3 -20 7 26.00 5.90 -3 -20 7 22.30 5.10 -3 20 7 21.60 3.20 3 20 -7 17.00 4.70 -3 20 7 26.10 4.80 -2 -20 7 5.60 3.40 -2 -20 7 4.20 2.90 2 -20 -7 -0.90 1.70 2 -20 -7 2.90 2.50 2 20 -7 3.20 2.70 -2 20 7 3.50 2.10 -2 20 7 1.90 1.50 -1 -20 7 5.10 3.40 1 -20 -7 2.60 2.30 1 -20 -7 7.20 3.30 1 -20 -7 -0.50 1.90 -1 -20 7 3.50 2.60 -1 20 7 4.30 1.80 1 20 -7 5.10 3.00 -1 20 7 7.60 2.90 0 -20 7 0.20 2.30 0 -20 -7 0.40 1.70 0 -20 -7 0.00 1.90 0 -20 7 3.90 2.80 0 -20 -7 5.30 2.90 0 20 7 2.30 1.80 0 20 -7 -0.60 2.00 0 20 7 0.80 1.80 0 20 -7 0.40 1.20 1 -20 7 109.29 11.00 -1 -20 -7 115.19 12.90 -1 -20 -7 120.29 9.20 1 -20 7 118.89 12.10 -1 -20 -7 133.79 9.70 -1 20 -7 129.99 10.20 1 20 7 114.49 8.00 1 20 7 137.19 9.90 -1 20 -7 127.09 7.70 -2 -20 -7 3.10 2.50 -2 -20 -7 -1.00 1.90 2 -20 7 0.90 1.70 2 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2 -21 -7 21.60 4.50 -2 -21 7 10.10 4.10 2 21 -7 20.60 4.90 -2 21 7 26.90 4.90 -2 21 7 19.40 3.40 1 -21 -7 0.10 1.90 -1 -21 7 -2.60 1.90 1 -21 -7 -0.50 2.70 -1 -21 7 -0.50 2.10 -1 21 7 1.30 1.40 1 21 -7 -0.70 2.10 -1 21 7 -0.90 1.50 0 -21 7 80.19 9.20 0 -21 -7 79.49 8.70 0 -21 7 81.29 10.20 0 -21 -7 67.89 9.90 0 -21 -7 70.79 8.30 0 21 -7 69.49 8.60 0 21 -7 70.59 5.40 0 21 7 75.89 6.10 0 21 7 93.89 9.20 -1 -21 -7 80.59 10.60 1 -21 7 92.39 9.70 -1 -21 -7 61.79 7.70 1 -21 7 79.39 9.80 -1 -21 -7 72.49 8.50 1 21 7 66.39 7.90 -1 21 -7 90.89 6.10 -1 21 -7 88.39 10.20 1 21 7 81.19 7.50 -2 -21 -7 4.10 2.60 -2 -21 -7 -0.80 1.60 2 -21 7 -0.70 1.70 -2 -21 -7 -0.30 2.40 2 -21 7 3.00 3.10 -2 21 -7 1.70 1.60 2 21 7 0.70 2.10 2 21 7 1.60 1.70 -2 21 -7 0.80 2.60 -3 -21 -7 -3.20 2.40 -3 -21 -7 4.20 2.70 3 -21 7 4.10 3.00 3 -21 7 -2.00 1.70 3 21 7 1.40 2.40 -3 21 -7 2.50 2.60 3 21 7 1.70 1.90 -3 21 -7 -0.70 1.50 4 -21 7 192.48 13.70 -4 -21 -7 188.18 15.40 4 -21 7 171.98 17.00 -4 -21 -7 189.78 12.80 4 21 7 166.88 11.20 -4 21 -7 189.08 13.00 -4 21 -7 197.38 11.40 4 21 7 189.08 12.80 -5 -21 -7 0.30 3.00 5 -21 7 3.70 2.90 -5 -21 -7 -0.70 2.20 5 21 7 -3.30 1.70 -5 21 -7 0.90 1.80 5 21 7 1.30 2.30 -6 -21 -7 0.70 3.70 6 -21 7 2.80 2.80 -6 -21 -7 -0.40 2.60 6 21 7 0.80 2.40 -6 21 -7 3.80 2.40 -7 -21 -7 -0.60 3.50 7 -21 7 -0.70 1.90 7 21 7 0.80 2.50 -7 21 -7 0.50 2.40 8 -21 7 10.50 3.30 -8 -21 -7 28.30 7.20 -8 21 -7 31.10 5.50 8 21 7 21.60 5.20 -9 -22 7 9.70 4.90 -9 -22 7 15.40 5.40 9 -22 -7 21.00 5.60 9 -22 -7 18.70 5.50 -9 22 7 11.80 4.00 9 22 -7 12.70 6.20 9 22 -7 21.00 5.30 -9 22 7 19.70 5.70 8 -22 -7 24.10 6.10 -8 -22 7 21.20 6.00 -8 -22 7 22.80 7.00 8 -22 -7 22.80 5.30 -8 -22 7 22.50 6.20 -8 22 7 21.70 4.70 8 22 -7 32.80 7.20 8 22 -7 19.80 6.30 -8 22 7 21.10 6.20 -7 -22 7 75.19 13.10 7 -22 -7 79.79 9.80 -7 -22 7 67.79 11.20 7 -22 -7 94.79 11.60 -7 -22 7 75.69 11.20 7 22 -7 76.49 10.10 -7 22 7 62.89 7.80 7 22 -7 82.89 11.70 6 -22 -7 0.00 2.50 -6 -22 7 0.50 3.00 6 -22 -7 3.40 2.90 -6 -22 7 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-23 7 5.50 3.80 8 -23 -7 5.40 2.80 8 -23 -7 1.50 2.80 8 23 -7 9.20 4.80 -8 23 7 7.40 4.00 -8 23 7 5.60 2.90 8 23 -7 7.50 5.10 7 -23 -7 5.30 3.20 7 -23 -7 5.50 3.90 -7 -23 7 12.70 5.60 -7 -23 7 4.30 3.90 -7 23 7 7.20 3.30 7 23 -7 9.80 4.90 7 23 -7 5.80 3.80 6 -23 -7 23.30 5.80 -6 -23 7 21.90 6.50 -6 -23 7 25.40 6.50 6 -23 -7 25.90 6.80 6 23 -7 19.70 6.30 -6 23 7 31.20 5.50 6 23 -7 22.50 5.70 5 -23 -7 16.70 4.60 5 -23 -7 17.00 5.30 -5 -23 7 12.40 4.30 -5 -23 7 20.80 5.90 5 23 -7 30.70 6.40 5 23 -7 20.10 6.20 -5 23 7 23.80 5.00 4 -23 -7 4.80 2.80 -4 -23 7 4.30 3.90 -4 -23 7 5.50 3.70 4 -23 -7 3.60 3.80 4 23 -7 9.20 4.00 -4 23 7 3.80 2.40 -3 -23 7 27.80 6.20 3 -23 -7 27.50 5.60 3 -23 -7 18.00 5.60 -3 -23 7 30.70 6.70 -3 23 7 28.90 5.40 3 23 -7 27.80 5.80 2 -23 -7 7.20 3.50 -2 -23 7 7.70 3.90 -2 -23 7 3.90 3.70 2 -23 -7 6.70 3.90 -2 23 7 2.90 2.20 -2 23 7 11.20 2.80 2 23 -7 20.70 5.20 -1 -23 7 32.50 6.40 1 -23 -7 20.80 5.00 1 -23 -7 33.30 7.30 -1 -23 7 19.20 5.20 -1 23 7 33.60 5.70 1 23 -7 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7 -23 7 3.70 2.50 -7 -23 -7 1.20 3.50 7 23 7 -0.90 2.20 -7 23 -7 0.60 2.30 8 -24 -7 6.70 2.90 -8 -24 7 10.10 4.90 8 -24 -7 7.10 3.60 8 24 -7 6.10 3.20 -8 24 7 9.00 4.40 8 24 -7 6.00 6.40 -8 24 7 1.20 2.00 7 -24 -7 1.30 3.10 -7 -24 7 -0.20 2.60 7 -24 -7 -1.50 3.20 7 24 -7 -4.20 3.50 7 24 -7 0.20 2.80 -7 24 7 0.40 2.40 -6 -24 7 1.80 4.00 -6 -24 7 0.70 3.10 6 -24 -7 -0.90 2.70 6 -24 -7 1.60 3.40 6 24 -7 -1.20 2.20 -6 24 7 0.20 2.40 6 24 -7 2.80 3.90 5 -24 -7 41.80 7.10 -5 -24 7 43.90 8.50 5 -24 -7 57.79 9.20 -5 -24 7 52.29 8.90 5 24 -7 42.70 7.30 5 24 -7 57.29 9.60 -5 24 7 40.20 6.30 4 -24 -7 3.50 3.60 -4 -24 7 6.00 3.90 4 -24 -7 6.70 3.50 -4 -24 7 4.20 4.00 -4 24 7 4.40 2.70 4 24 -7 4.40 3.60 3 -24 -7 147.69 11.40 -3 -24 7 141.29 14.70 3 -24 -7 145.09 15.10 -3 -24 7 145.69 14.40 3 24 -7 127.19 13.00 -3 24 7 132.19 10.20 2 -24 -7 8.70 3.30 -2 -24 7 -0.80 2.50 -2 -24 7 0.20 3.00 2 -24 -7 1.90 2.60 -2 24 7 -0.20 2.00 -2 24 7 -0.20 1.50 2 24 -7 0.60 2.80 -1 -24 7 23.50 5.80 1 -24 -7 43.80 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34.00 4.90 8 -2 9 132.89 9.80 8 -2 9 164.18 11.00 -8 -2 -9 158.28 14.70 -8 2 -9 169.18 12.70 8 2 9 137.69 10.00 8 2 9 157.38 10.10 9 -2 9 -0.90 1.90 -9 -2 -9 2.00 3.30 9 2 9 -1.00 1.90 -9 2 -9 -0.60 2.60 9 2 9 2.50 2.20 -10 -2 -9 159.28 15.40 10 -2 9 128.79 10.50 -10 2 -9 159.98 15.30 10 2 9 113.09 9.60 -12 -3 9 8.00 3.10 12 -3 -9 11.90 4.50 12 -3 -9 18.80 6.30 -12 -3 9 4.60 3.20 12 3 -9 9.60 4.50 -12 3 9 3.80 3.80 -12 3 9 10.20 3.80 11 -3 -9 -2.20 2.00 -11 -3 9 2.80 2.40 -11 -3 9 1.00 2.70 11 -3 -9 2.50 3.80 -11 3 9 0.40 2.40 -11 3 9 -3.00 2.30 11 3 -9 2.10 4.00 -10 -3 9 84.39 9.00 10 -3 -9 97.29 10.50 10 -3 -9 103.49 12.00 -10 -3 9 93.19 10.40 -10 3 9 113.99 11.80 -10 3 9 109.59 10.50 10 3 -9 121.19 13.50 9 -3 -9 3.60 2.90 -9 -3 9 11.30 3.60 -9 -3 9 7.30 2.70 9 -3 -9 5.30 2.70 9 3 -9 1.80 3.00 -9 3 9 4.10 2.80 -9 3 9 8.70 3.80 -8 -3 9 1.20 2.10 -8 -3 9 -0.40 1.40 8 -3 -9 0.20 2.10 8 -3 -9 1.00 1.60 -8 3 9 1.90 2.00 8 3 -9 2.00 2.50 -8 3 9 0.10 1.80 8 3 -9 1.50 2.30 -7 -3 9 3.30 1.90 7 -3 -9 2.50 2.20 7 -3 -9 2.80 2.40 -7 -3 9 -1.00 1.80 7 3 -9 2.00 2.00 -7 3 9 -2.60 1.80 -7 3 9 1.80 1.90 -7 3 9 0.60 1.40 7 3 -9 7.40 3.00 -6 -3 9 -2.40 1.00 6 -3 -9 1.30 1.50 6 -3 -9 0.90 1.70 6 -3 -9 2.60 2.20 6 -3 -9 0.50 1.50 -6 -3 9 1.50 1.30 6 3 -9 -0.20 1.80 6 3 -9 -1.20 2.00 -6 3 9 0.40 1.80 -6 3 9 -0.10 1.50 -6 3 9 0.60 1.30 5 -3 -9 181.08 12.20 -5 -3 9 192.18 9.40 5 -3 -9 193.68 10.60 -5 -3 9 194.18 10.00 -5 -3 9 205.18 11.30 5 -3 -9 180.08 10.60 5 -3 -9 189.58 11.00 5 -3 -9 186.78 10.10 5 3 -9 206.08 13.50 -5 3 9 185.28 11.30 -5 3 9 174.08 10.50 5 3 -9 190.68 11.80 -5 3 9 178.68 10.10 4 -3 -9 427.36 19.50 4 -3 -9 433.76 21.60 4 -3 -9 428.46 20.50 -4 -3 9 439.26 18.70 4 -3 -9 445.96 19.80 4 -3 -9 439.36 19.60 -4 -3 9 420.76 19.60 4 3 -9 434.96 21.30 -4 3 9 454.05 20.40 -4 3 9 439.56 19.80 4 3 -9 447.76 19.00 -4 3 9 436.86 19.80 4 3 -9 444.46 22.70 3 -3 -9 87.19 6.90 3 -3 -9 65.09 5.30 -3 -3 9 92.89 6.10 -3 -3 9 84.59 5.20 3 -3 -9 91.29 6.50 -3 -3 9 88.79 9.60 3 -3 -9 94.69 6.30 3 -3 -9 105.59 7.90 -3 3 9 93.09 6.40 3 3 -9 83.49 9.30 3 3 -9 73.19 7.70 3 3 -9 81.39 5.80 -3 3 9 69.19 7.90 2 -3 -9 39.60 5.40 -2 -3 9 40.20 6.40 -2 -3 9 47.70 4.50 -2 -3 9 39.10 3.00 2 -3 -9 36.00 5.40 2 -3 -9 44.10 5.40 2 -3 -9 42.10 4.70 2 -3 -9 33.30 3.70 -2 3 9 39.50 5.80 2 3 -9 34.30 5.70 -2 3 9 43.00 4.40 2 3 -9 50.19 6.50 2 3 -9 54.39 5.50 -1 -3 9 18.90 2.00 1 -3 -9 15.00 3.30 1 -3 -9 17.50 3.00 -1 -3 9 17.30 4.40 1 -3 -9 15.60 3.50 1 -3 -9 22.20 2.70 -1 -3 9 20.10 2.60 -1 3 9 12.60 3.50 1 3 -9 18.00 3.70 1 3 -9 14.50 1.80 1 3 -9 18.60 3.30 -1 3 9 13.90 3.30 -1 3 9 19.30 2.70 0 -3 -9 174.78 8.00 0 -3 -9 169.48 10.70 0 -3 9 180.28 12.20 0 -3 -9 183.78 10.90 0 -3 -9 178.18 9.70 0 -3 9 175.88 8.30 0 3 -9 184.08 10.40 0 3 9 182.08 8.30 0 3 -9 161.98 11.10 0 3 9 169.98 11.10 0 3 9 178.88 11.20 -1 -3 -9 8.00 2.30 -1 -3 -9 5.00 2.20 -1 -3 -9 6.40 2.30 1 -3 9 9.60 3.40 -1 3 -9 6.50 2.50 1 3 9 9.10 2.80 -1 3 -9 9.20 2.50 1 3 9 4.20 2.20 -2 -3 -9 11.80 3.30 2 -3 9 31.90 5.70 -2 -3 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29.40 4.90 -2 4 9 37.40 5.10 2 4 -9 37.00 4.30 1 -4 -9 49.20 3.60 -1 -4 9 42.50 2.70 1 -4 -9 50.69 5.30 1 -4 -9 40.40 5.10 -1 -4 9 50.69 3.80 -1 -4 9 44.90 6.70 1 -4 -9 43.70 5.60 -1 4 9 37.90 5.50 1 4 -9 36.60 5.50 1 4 -9 44.50 5.00 -1 4 9 57.49 6.70 0 -4 -9 14.30 3.10 0 -4 -9 20.60 2.40 0 -4 -9 34.10 5.00 0 -4 -9 21.90 4.00 0 -4 9 27.20 5.40 0 -4 9 26.30 2.90 0 4 9 25.70 2.80 0 4 -9 22.40 3.80 0 4 9 21.00 4.00 0 4 -9 19.80 3.90 0 4 9 22.10 4.10 -1 -4 -9 142.89 9.40 1 -4 9 131.99 10.40 -1 -4 -9 144.19 8.70 -1 -4 -9 139.09 9.50 -1 4 -9 137.89 9.90 1 4 9 129.49 9.20 1 4 9 147.29 9.70 -1 4 -9 141.39 9.10 -2 -4 -9 8.20 2.50 2 -4 9 7.90 3.20 -2 -4 -9 8.80 2.80 -2 -4 -9 3.50 2.10 -2 4 -9 1.80 1.70 2 4 9 2.90 1.80 -2 4 -9 10.90 3.30 2 4 9 8.30 2.90 -3 -4 -9 80.69 6.40 3 -4 9 51.49 7.40 3 -4 9 57.99 7.20 -3 -4 -9 58.19 7.30 -3 4 -9 68.49 7.30 3 4 9 74.19 7.30 -3 4 -9 71.09 8.00 3 4 9 62.09 7.00 -4 -4 -9 0.70 2.10 4 -4 9 0.60 1.90 4 -4 9 2.80 2.40 -4 -4 -9 -0.80 1.50 -4 4 -9 3.80 2.30 -4 4 -9 5.20 2.30 4 4 9 1.50 1.80 4 4 9 0.30 1.40 5 -4 9 446.86 22.00 -5 -4 -9 440.86 22.70 5 -4 9 432.86 22.30 5 4 9 438.56 21.10 5 4 9 459.35 20.80 -5 4 -9 437.56 22.10 -5 4 -9 418.66 21.30 6 -4 9 0.00 1.90 6 -4 9 6.70 2.80 -6 -4 -9 5.20 3.10 6 4 9 0.60 1.70 -6 4 -9 0.50 2.10 6 4 9 0.90 1.60 -6 4 -9 1.30 2.00 7 -4 9 30.40 5.50 7 -4 9 13.20 3.60 -7 -4 -9 27.30 5.90 7 4 9 19.50 3.90 -7 4 -9 16.60 4.80 7 4 9 23.30 4.30 -8 -4 -9 93.79 11.10 8 -4 9 95.99 9.70 8 4 9 85.59 8.40 8 4 9 86.79 8.40 -8 4 -9 134.59 12.80 9 -4 9 0.60 2.60 -9 -4 -9 1.40 3.40 9 4 9 5.10 2.40 -9 4 -9 8.40 4.00 9 4 9 4.20 2.30 10 -4 9 4.60 3.40 -10 -4 -9 4.00 3.90 10 4 9 12.80 4.00 -10 4 -9 7.90 4.20 -12 -5 9 38.30 6.70 12 -5 -9 24.00 6.50 -12 -5 9 32.60 6.50 12 -5 -9 49.00 7.80 -12 5 9 39.40 6.80 -12 5 9 30.80 7.10 12 5 -9 40.30 8.70 -11 -5 9 1.60 2.20 11 -5 -9 1.00 2.70 -11 -5 9 2.90 2.90 11 -5 -9 -0.80 3.40 -11 5 9 -1.20 2.00 11 5 -9 -4.50 2.40 -11 5 9 -0.10 2.90 -10 -5 9 48.00 6.30 10 -5 -9 53.69 8.80 10 -5 -9 57.49 7.60 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12 143.29 10.60 0 -8 -12 37.10 6.20 0 -8 -12 37.90 6.70 0 -8 12 37.20 7.60 0 8 12 48.30 6.70 0 8 -12 47.50 7.90 0 8 -12 37.50 5.90 1 -8 12 55.79 8.90 -1 -8 -12 45.50 7.00 1 8 12 38.40 6.00 -1 8 -12 29.30 6.10 -1 8 -12 42.60 6.40 2 -8 12 -1.40 2.10 -2 -8 -12 -1.10 1.80 -2 8 -12 -0.90 1.80 -2 8 -12 0.50 2.60 2 8 12 0.00 2.00 3 -8 12 -2.60 2.20 -3 -8 -12 -0.20 2.40 -3 8 -12 -0.20 2.30 3 8 12 -0.20 2.10 -3 8 -12 0.20 2.30 -4 -8 -12 6.90 4.40 4 -8 12 7.00 3.60 4 -8 12 6.50 4.20 -4 8 -12 12.40 4.10 -4 8 -12 7.00 3.80 4 8 12 15.60 4.00 -5 -8 -12 33.10 7.40 5 -8 12 29.80 6.70 5 -8 12 34.00 6.60 -5 8 -12 32.80 6.30 5 8 12 32.60 5.50 -5 8 -12 33.30 6.50 6 -8 12 7.80 4.10 -6 -8 -12 -3.80 3.40 6 -8 12 4.10 3.30 -6 8 -12 9.00 4.10 -6 8 -12 1.70 2.80 6 8 12 2.90 2.70 -7 -8 -12 6.30 4.90 7 -8 12 11.00 4.10 -7 8 -12 12.30 4.40 7 8 12 9.70 3.60 -7 8 -12 20.50 5.10 -10 -9 12 5.40 3.10 10 -9 -12 4.20 3.10 10 9 -12 4.50 4.90 -10 9 12 5.60 3.80 -10 9 12 2.00 3.50 9 -9 -12 58.09 7.80 9 -9 -12 62.39 8.40 -9 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13 -12 57.39 8.90 5 13 12 37.80 6.30 6 -13 12 13.70 4.90 -6 -13 -12 15.10 5.30 6 13 12 19.50 4.30 -6 13 -12 11.40 4.20 -6 13 -12 14.50 5.50 -7 -13 -12 12.00 5.30 9 -14 -12 64.79 9.00 -9 -14 12 79.49 10.70 9 -14 -12 50.69 7.40 -9 -14 12 41.00 10.70 9 14 -12 64.19 11.80 9 14 -12 75.29 11.30 -9 14 12 68.59 9.40 -8 -14 12 5.60 5.40 8 -14 -12 0.50 3.20 -8 -14 12 3.10 3.60 8 -14 -12 4.90 3.40 -8 14 12 1.80 2.50 8 14 -12 0.20 3.80 8 14 -12 6.20 5.00 -8 14 12 2.80 3.40 7 -14 -12 22.50 5.30 -7 -14 12 20.90 5.30 -7 -14 12 26.40 7.40 7 -14 -12 19.90 5.10 -7 14 12 17.90 5.30 7 14 -12 27.10 7.80 7 14 -12 23.40 6.40 -7 14 12 14.80 4.10 6 -14 -12 6.90 3.50 -6 -14 12 4.80 4.00 6 -14 -12 4.10 3.20 -6 -14 12 3.00 2.90 6 14 -12 8.60 4.20 6 14 -12 3.30 4.40 -6 14 12 2.30 2.50 5 -14 -12 59.79 7.70 5 -14 -12 52.19 7.70 -5 -14 12 46.60 7.30 -5 -14 12 55.19 10.00 5 -14 -12 55.49 7.30 5 14 -12 65.99 11.10 -5 14 12 45.80 6.90 5 14 -12 59.89 9.50 -4 -14 12 17.10 6.20 4 -14 -12 23.00 4.90 4 -14 -12 13.60 3.70 4 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42.50 7.10 1 4 14 31.30 6.20 -1 4 -14 29.20 6.60 -1 4 -14 38.50 6.90 2 -4 14 212.48 16.50 -2 -4 -14 226.38 16.20 2 -4 14 225.58 16.30 2 4 14 212.28 15.10 2 4 14 211.18 14.70 -2 4 -14 245.98 16.10 -2 4 -14 218.48 16.00 3 -4 14 15.10 5.20 -3 -4 -14 15.40 5.20 3 -4 14 7.00 4.70 -3 4 -14 4.60 3.90 -3 4 -14 13.70 5.30 3 4 14 7.70 3.30 3 4 14 11.00 4.50 -4 -4 -14 3.60 4.00 4 -4 14 1.10 2.90 4 -4 14 8.40 4.50 4 4 14 -0.90 2.40 -4 4 -14 6.90 3.90 -4 4 -14 3.80 3.40 5 -4 14 0.10 3.10 -5 -4 -14 7.10 4.40 5 -4 14 3.40 3.80 -5 4 -14 -0.10 3.00 5 4 14 2.40 3.20 -5 4 -14 -1.30 2.60 6 -4 14 25.50 6.10 6 -4 14 20.20 5.50 -6 -4 -14 26.90 7.30 6 4 14 29.60 6.00 -6 4 -14 18.40 6.00 -9 -5 14 118.69 12.00 9 -5 -14 88.19 12.40 -9 -5 14 93.39 14.80 -9 5 14 88.89 9.80 9 5 -14 82.19 13.20 -9 5 14 64.19 9.30 -8 -5 14 -4.40 3.00 8 -5 -14 3.40 4.80 8 -5 -14 5.50 3.10 -8 -5 14 4.00 3.10 -8 5 14 2.40 3.10 -8 5 14 2.40 4.00 -8 5 14 3.60 3.00 8 5 -14 0.20 3.40 7 -5 -14 52.79 7.40 -7 -5 14 59.89 8.20 -7 -5 14 61.29 11.40 7 -5 -14 35.80 7.90 7 5 -14 76.89 11.90 -7 5 14 44.60 6.50 7 5 -14 47.50 8.50 -7 5 14 61.79 8.60 -7 5 14 56.59 10.00 -6 -5 14 20.30 6.60 6 -5 -14 18.80 6.00 6 -5 -14 18.10 5.30 -6 -5 14 22.00 5.10 6 5 -14 9.10 5.10 6 5 -14 21.40 5.60 -6 5 14 24.70 6.80 -6 5 14 11.00 4.00 -6 5 14 11.10 5.10 5 -5 -14 11.70 4.10 -5 -5 14 14.70 5.90 5 -5 -14 9.50 4.70 5 5 -14 9.00 4.30 5 5 -14 19.90 5.70 -5 5 14 9.60 3.80 -5 5 14 9.60 4.40 -5 5 14 14.20 3.80 -4 -5 14 26.50 7.20 4 -5 -14 21.60 4.80 4 -5 -14 25.60 5.70 -4 5 14 27.10 5.60 4 5 -14 34.90 7.30 -4 5 14 32.70 5.90 -4 5 14 41.40 7.80 -3 -5 14 84.69 12.10 3 -5 -14 69.89 9.10 3 -5 -14 80.19 9.40 -3 5 14 68.29 9.20 3 5 -14 104.99 12.60 -3 5 14 78.69 10.50 2 -5 -14 47.60 7.30 -2 -5 14 53.59 10.00 2 -5 -14 42.00 7.00 2 5 -14 39.60 10.20 -2 5 14 47.60 7.70 2 5 -14 29.60 6.70 -2 5 14 42.10 7.40 1 -5 -14 1.50 2.10 -1 -5 14 0.10 3.20 1 -5 -14 1.30 2.60 1 5 -14 -1.50 2.60 1 5 -14 1.90 2.50 -1 5 14 -1.80 2.50 -1 5 14 -0.20 2.50 0 -5 14 71.49 11.00 0 -5 -14 72.29 9.00 0 -5 -14 86.19 10.60 0 5 14 87.29 10.60 0 5 -14 69.59 9.70 0 5 14 78.39 9.70 0 5 -14 90.59 10.00 -1 -5 -14 11.00 4.30 1 -5 14 4.60 3.90 1 -5 14 16.90 5.30 -1 -5 -14 10.20 3.70 -1 5 -14 16.90 5.20 -1 5 -14 15.80 4.90 1 5 14 8.60 3.80 -2 -5 -14 54.69 8.70 2 -5 14 66.99 10.10 2 -5 14 59.79 9.70 2 5 14 60.39 8.50 -2 5 -14 60.19 8.90 -2 5 -14 58.79 9.40 -3 -5 -14 6.00 4.10 3 -5 14 17.50 5.70 3 -5 14 11.90 5.10 -3 5 -14 8.60 4.50 -3 5 -14 12.40 4.70 3 5 14 10.50 4.50 -4 -5 -14 6.20 4.50 4 -5 14 9.40 4.40 4 -5 14 7.20 4.10 -4 5 -14 6.50 3.80 -4 5 -14 5.50 3.70 4 5 14 6.10 4.00 -5 -5 -14 21.50 6.30 5 -5 14 29.20 6.50 5 -5 14 19.70 6.00 -5 5 -14 31.80 7.30 -5 5 -14 24.40 6.00 5 5 14 17.30 5.30 -6 -5 -14 -0.40 3.10 6 -5 14 1.20 2.80 6 -5 14 -1.00 2.80 6 5 14 2.30 2.90 -6 5 -14 3.90 3.60 -9 -6 14 42.10 10.20 9 -6 -14 55.79 8.20 -9 -6 14 34.60 6.90 9 6 -14 27.30 7.50 -9 6 14 45.90 7.50 -9 6 14 45.40 8.10 8 -6 -14 2.60 3.10 -8 -6 14 0.30 2.40 -8 -6 14 -1.20 4.10 8 6 -14 -0.70 3.40 -8 6 14 4.90 3.20 -8 6 14 0.70 2.50 -8 6 14 2.00 4.20 -7 -6 14 50.59 10.60 7 -6 -14 33.60 5.60 -7 -6 14 37.10 6.50 7 -6 -14 42.30 6.80 7 6 -14 38.20 7.80 -7 6 14 52.49 7.90 -7 6 14 38.20 6.10 7 6 -14 26.20 7.50 -7 6 14 31.20 7.80 6 -6 -14 38.30 8.60 -6 -6 14 49.10 10.00 -6 -6 14 56.69 7.40 -6 6 14 52.99 9.00 6 6 -14 54.89 9.00 -6 6 14 46.50 6.60 6 6 -14 34.60 8.40 -6 6 14 47.20 7.00 -5 -6 14 14.70 5.90 5 -6 -14 12.70 3.80 5 -6 -14 12.80 4.20 -5 6 14 9.00 3.50 -5 6 14 19.30 5.80 5 6 -14 11.50 4.60 5 6 -14 10.90 5.10 -5 6 14 9.10 3.40 4 -6 -14 7.60 3.50 4 -6 -14 3.40 2.70 -4 -6 14 1.50 3.90 -4 6 14 7.60 3.30 -4 6 14 -0.50 2.60 4 6 -14 9.50 3.90 -4 6 14 6.70 3.40 3 -6 -14 20.70 4.90 -3 -6 14 27.10 7.40 3 -6 -14 20.80 5.30 -3 6 14 17.40 4.80 3 6 -14 24.20 6.30 2 -6 -14 39.30 6.60 2 -6 -14 28.70 5.80 -2 -6 14 35.40 8.20 2 6 -14 28.50 6.60 -2 6 14 44.10 6.80 1 -6 -14 28.20 5.90 1 -6 -14 34.20 6.40 -1 -6 14 23.80 6.90 1 6 -14 20.20 5.70 -1 6 14 28.10 6.10 1 6 -14 16.90 4.50 0 -6 -14 28.60 6.10 0 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12.70 5.40 3 8 14 9.40 3.80 -3 8 -14 12.00 5.20 -3 8 -14 15.90 4.80 -4 -8 -14 188.98 17.90 4 -8 14 191.58 15.60 4 -8 14 184.58 15.10 -4 8 -14 173.18 16.40 4 8 14 201.68 13.70 -4 8 -14 200.38 15.20 5 -8 14 4.70 4.00 5 -8 14 8.70 4.60 -5 -8 -14 7.20 4.00 -5 8 -14 2.40 3.00 5 8 14 3.50 2.50 -5 8 -14 7.60 4.40 -8 -9 14 19.80 5.60 -8 -9 14 16.90 7.00 8 -9 -14 21.30 4.70 8 -9 -14 19.40 5.00 8 9 -14 12.90 5.30 -8 9 14 12.60 4.70 -8 9 14 11.50 4.10 8 9 -14 15.40 6.30 7 -9 -14 19.10 5.20 -7 -9 14 18.90 7.00 7 -9 -14 17.00 4.50 -7 -9 14 21.00 5.30 -7 9 14 25.40 5.90 -7 9 14 17.30 4.40 7 9 -14 10.40 6.10 7 9 -14 20.70 6.10 -6 -9 14 2.20 3.00 6 -9 -14 6.70 3.30 -6 -9 14 7.50 5.70 6 9 -14 2.00 4.20 6 9 -14 2.40 3.50 -6 9 14 7.60 3.30 -6 9 14 7.30 3.10 -6 9 14 1.50 2.60 5 -9 -14 23.80 5.00 -5 -9 14 20.50 7.00 5 -9 -14 33.30 6.10 -5 9 14 34.10 6.10 5 9 -14 28.10 6.90 5 9 -14 37.40 8.70 -5 9 14 15.30 4.50 4 -9 -14 15.80 4.30 -4 -9 14 15.30 5.90 -4 9 14 18.00 4.50 4 9 -14 19.60 6.00 -4 9 14 12.00 3.80 -3 -9 14 24.40 7.10 3 -9 -14 21.50 4.90 -3 9 14 26.90 5.10 -3 9 14 15.10 4.40 3 9 -14 23.20 6.10 2 -9 -14 45.30 7.30 -2 -9 14 51.29 10.00 -2 9 14 35.00 6.20 2 9 -14 55.69 9.20 1 -9 -14 1.00 2.40 -1 -9 14 -4.80 2.80 -1 9 14 2.30 2.40 1 9 -14 3.10 3.60 0 -9 -14 5.80 3.00 0 -9 14 8.30 4.70 0 9 14 5.20 3.00 0 9 -14 6.20 3.60 0 9 -14 9.30 4.60 1 -9 14 3.90 4.30 -1 -9 -14 9.90 4.30 1 9 14 1.40 2.80 -1 9 -14 3.50 4.00 -1 9 -14 -1.00 2.70 -2 -9 -14 -0.60 3.00 2 -9 14 0.80 3.50 -2 9 -14 0.70 2.60 -2 9 -14 1.60 3.40 2 9 14 1.30 2.90 -3 -9 -14 146.59 15.40 3 -9 14 132.89 15.40 3 -9 14 160.28 16.00 -3 9 -14 142.29 14.70 -3 9 -14 143.09 14.20 3 9 14 156.08 11.70 -4 -9 -14 4.70 4.10 4 -9 14 -2.00 3.20 4 -9 14 3.10 4.10 -4 9 -14 0.30 2.90 -4 9 -14 0.80 3.00 4 9 14 4.00 2.90 5 -9 14 104.89 12.60 5 -9 14 115.29 13.40 -5 -9 -14 118.69 14.10 5 9 14 128.49 12.30 -5 9 -14 141.89 14.20 -5 9 -14 148.69 15.00 8 -10 -14 1.80 3.10 -8 -10 14 7.80 5.30 8 -10 -14 5.40 3.30 -8 -10 14 0.10 3.00 -8 10 14 4.10 3.40 8 10 -14 1.10 4.70 -8 10 14 -2.00 2.90 8 10 -14 0.90 4.30 7 -10 -14 -0.50 2.40 7 -10 -14 -0.80 2.60 -7 -10 14 -3.70 2.10 -7 -10 14 -2.20 4.00 -7 10 14 3.00 2.80 7 10 -14 7.40 4.80 -7 10 14 0.70 2.80 7 10 -14 -3.50 2.70 6 -10 -14 25.50 5.30 6 -10 -14 23.20 5.10 -6 -10 14 40.40 6.70 -6 -10 14 19.10 6.90 6 10 -14 45.70 8.50 -6 10 14 44.10 6.80 6 10 -14 38.30 9.00 -6 10 14 26.30 5.50 -6 10 14 35.50 6.10 -5 -10 14 7.50 4.90 5 -10 -14 12.00 4.20 5 -10 -14 10.90 3.70 5 10 -14 13.90 5.50 -5 10 14 11.30 4.10 -5 10 14 7.70 3.10 5 10 -14 18.70 6.90 -4 -10 14 21.90 7.00 4 -10 -14 15.80 4.50 4 -10 -14 20.20 5.50 4 10 -14 33.10 7.40 -4 10 14 21.90 4.70 -4 10 14 18.70 4.90 -3 -10 14 6.50 4.90 3 -10 -14 4.80 3.10 -3 10 14 2.20 2.50 -3 10 14 2.70 2.80 3 10 -14 3.90 4.10 -2 -10 14 10.80 5.80 2 -10 -14 4.20 3.10 2 10 -14 17.30 5.40 -2 10 14 8.20 3.20 1 -10 -14 39.10 7.20 -1 -10 14 29.50 8.20 -1 10 14 30.10 6.00 1 10 -14 43.50 8.40 0 -10 14 21.30 7.00 0 -10 -14 18.40 5.40 0 10 14 20.10 5.10 0 10 -14 27.40 6.80 0 10 -14 19.50 5.10 1 -10 14 125.29 15.50 -1 -10 -14 145.39 14.40 -1 10 -14 134.59 14.40 -1 10 -14 162.98 12.10 1 10 14 131.19 10.80 -2 -10 -14 3.10 2.90 2 -10 14 2.90 3.90 -2 10 -14 4.00 3.20 -2 10 -14 -2.80 2.50 2 10 14 -1.00 2.20 3 -10 14 1.20 3.90 -3 -10 -14 -0.90 3.00 3 -10 14 2.50 3.80 -3 10 -14 3.70 3.40 3 10 14 3.10 3.10 -3 10 -14 1.60 3.80 4 -10 14 10.50 5.30 4 -10 14 14.40 5.50 -4 -10 -14 18.00 6.30 -4 10 -14 22.10 6.20 -4 10 -14 16.80 5.40 4 10 14 13.50 4.40 5 -10 14 6.40 4.30 5 -10 14 1.10 3.20 -5 -10 -14 -2.90 2.70 -5 10 -14 0.20 3.20 5 10 14 1.10 2.60 -5 10 -14 -0.60 3.30 -8 -11 14 10.00 5.70 8 -11 -14 12.70 4.30 8 -11 -14 15.40 4.80 -8 -11 14 9.50 4.50 8 11 -14 13.90 6.80 -8 11 14 22.00 5.80 8 11 -14 7.70 4.90 -8 11 14 13.60 4.70 -7 -11 14 15.90 6.90 7 -11 -14 19.40 5.00 -7 -11 14 29.90 6.20 7 -11 -14 15.40 4.40 7 11 -14 26.50 7.20 -7 11 14 21.20 5.40 -7 11 14 13.10 4.60 7 11 -14 15.60 6.10 -6 -11 14 0.40 2.60 -6 -11 14 6.10 5.00 6 -11 -14 -0.60 2.80 6 11 -14 -1.50 2.80 -6 11 14 2.40 2.90 6 11 -14 1.90 4.00 -6 11 14 0.60 2.20 -6 11 14 -0.40 2.60 5 -11 -14 20.90 5.00 -5 -11 14 29.60 8.60 5 -11 -14 22.80 5.20 5 11 -14 10.00 5.50 5 11 -14 17.10 6.10 -5 11 14 18.60 4.90 -5 11 14 16.20 4.60 4 -11 -14 0.20 2.30 -4 -11 14 4.70 5.10 4 -11 -14 2.10 2.50 -4 11 14 -0.80 2.20 4 11 -14 6.90 4.20 -4 11 14 3.00 2.60 3 -11 -14 72.89 9.20 -3 -11 14 56.29 10.70 -3 11 14 91.39 10.50 -3 11 14 66.09 8.10 3 11 -14 84.09 11.60 2 -11 -14 15.20 4.50 -2 -11 14 10.10 5.60 -2 11 14 14.30 4.10 2 11 -14 21.30 6.90 1 -11 -14 -1.10 2.80 -1 -11 14 1.60 3.70 -1 11 14 1.90 2.40 1 11 -14 -0.20 3.30 0 -11 14 5.30 4.20 0 -11 -14 5.40 4.00 0 11 14 6.30 3.40 0 11 -14 6.40 5.80 0 11 -14 3.60 4.10 -1 -11 -14 234.28 16.90 1 -11 14 228.28 18.40 -1 11 -14 272.37 18.50 -1 11 -14 249.28 16.00 1 11 14 225.88 14.90 2 -11 14 14.40 6.20 -2 -11 -14 16.10 5.40 2 11 14 20.10 4.90 -2 11 -14 19.40 5.10 -2 11 -14 6.90 4.50 3 -11 14 6.50 5.40 -3 -11 -14 13.60 5.60 3 11 14 9.40 4.10 -3 11 -14 11.10 4.50 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7.00 6 5 -15 21.40 6.80 6 5 -15 8.80 4.80 -6 5 15 28.40 8.30 -5 -5 15 43.40 9.50 5 -5 -15 42.60 7.20 -5 5 15 52.29 7.80 5 5 -15 43.30 8.40 5 5 -15 49.30 10.50 -4 -5 15 -1.50 2.90 4 -5 -15 3.30 3.30 4 -5 -15 4.50 3.10 4 5 -15 2.30 3.70 -4 5 15 -3.10 2.30 -4 5 15 2.30 2.70 3 -5 -15 -1.90 2.20 3 -5 -15 -1.80 2.50 -3 -5 15 -2.70 2.80 3 5 -15 -2.40 2.80 -3 5 15 4.50 3.40 -2 -5 15 36.30 8.20 2 -5 -15 37.90 7.00 2 -5 -15 35.20 6.70 -2 5 15 32.40 6.80 2 5 -15 23.70 6.50 1 -5 -15 12.50 4.80 -1 -5 15 16.00 5.80 1 -5 -15 10.00 4.20 -1 5 15 10.30 4.40 1 5 -15 16.70 5.70 1 5 -15 22.20 5.20 0 -5 -15 -1.00 2.60 0 -5 -15 -0.30 3.40 0 -5 15 1.00 4.00 0 5 15 1.60 3.50 0 5 -15 2.70 3.40 0 5 -15 2.10 3.10 1 -5 15 0.20 3.70 -1 -5 -15 6.10 4.10 1 -5 15 5.80 4.10 1 5 15 7.50 4.00 -1 5 -15 5.60 3.70 -1 5 -15 -1.20 3.80 2 -5 15 167.58 16.70 2 -5 15 160.88 16.40 -2 -5 -15 159.18 15.70 -2 5 -15 134.99 14.10 -2 5 -15 198.88 15.00 2 5 15 135.09 13.60 -3 -5 -15 20.20 6.00 3 -5 15 15.10 5.50 3 -5 15 7.30 4.60 -3 5 -15 15.90 5.80 -3 5 -15 23.30 6.60 3 5 15 11.70 4.40 -4 -5 -15 84.79 11.80 4 -5 15 94.79 12.30 4 -5 15 91.69 12.00 -4 5 -15 95.49 11.50 -4 5 -15 87.29 11.30 4 5 15 79.29 9.80 8 -6 -15 5.70 3.80 -8 -6 15 3.50 3.10 -8 -6 15 6.90 5.60 -8 6 15 0.30 3.20 8 6 -15 5.50 4.80 -7 -6 15 64.19 11.90 -7 -6 15 70.79 8.90 7 6 -15 60.09 10.80 7 6 -15 64.59 10.30 -6 -6 15 22.50 7.70 6 6 -15 31.80 8.80 6 6 -15 15.10 5.50 -5 -6 15 3.60 4.70 5 -6 -15 5.60 3.50 -5 6 15 5.60 3.40 5 6 -15 0.70 3.30 -5 6 15 3.70 3.40 5 6 -15 2.70 3.70 4 -6 -15 45.30 7.10 4 -6 -15 30.50 6.10 -4 -6 15 31.60 8.50 -4 6 15 33.30 6.40 -4 6 15 20.70 5.30 4 6 -15 33.50 7.90 -3 -6 15 9.10 5.30 3 -6 -15 8.70 3.70 3 -6 -15 1.00 2.90 -3 6 15 3.30 2.70 3 6 -15 3.90 3.30 2 -6 -15 36.90 6.70 -2 -6 15 38.80 8.70 2 -6 -15 45.60 7.50 -2 6 15 30.50 6.50 2 6 -15 46.10 8.30 1 -6 -15 59.89 8.70 -1 -6 15 90.19 12.80 1 -6 -15 72.29 9.10 1 6 -15 61.59 10.00 1 6 -15 76.49 11.00 -1 6 15 52.89 8.10 0 -6 15 38.50 8.50 0 -6 -15 35.60 7.40 0 6 -15 36.00 6.80 0 6 15 30.80 6.60 0 6 -15 32.70 7.00 1 -6 15 2.10 3.70 -1 -6 -15 -2.00 3.00 1 -6 15 3.20 4.10 -1 6 -15 0.60 3.00 1 6 15 1.20 2.70 -1 6 -15 5.90 4.60 -2 -6 -15 26.40 7.40 2 -6 15 18.90 6.40 2 -6 15 19.90 6.30 -2 6 -15 31.00 7.40 2 6 15 25.60 6.10 -2 6 -15 25.10 6.30 3 -6 15 35.00 8.00 -3 -6 -15 24.80 6.30 3 -6 15 31.30 7.90 -3 6 -15 29.90 7.20 3 6 15 26.60 5.90 -3 6 -15 32.50 7.70 -4 -6 -15 6.00 4.50 4 -6 15 11.90 4.80 4 -6 15 5.50 3.80 -4 6 -15 15.80 5.10 4 6 15 6.80 3.60 -4 6 -15 9.40 3.90 8 -7 -15 -2.20 3.00 -8 -7 15 4.80 3.00 -8 -7 15 7.60 5.60 8 7 -15 8.30 4.90 -8 7 15 0.50 3.20 -7 -7 15 23.10 5.50 -7 -7 15 5.50 4.30 7 7 -15 10.40 5.20 7 7 -15 11.10 5.00 -6 -7 15 63.29 11.80 6 7 -15 64.39 10.30 6 7 -15 43.10 9.40 -5 -7 15 14.00 6.30 -5 7 15 8.60 3.60 5 7 -15 9.80 4.90 5 7 -15 2.30 3.50 -5 7 15 7.70 3.50 4 -7 -15 62.99 8.40 -4 -7 15 64.59 11.70 4 -7 -15 71.99 8.70 4 7 -15 69.99 10.70 -4 7 15 73.89 9.10 -4 7 15 46.80 7.40 3 -7 -15 -0.20 2.60 3 -7 -15 0.60 2.70 -3 -7 15 1.00 3.70 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-4 -8 15 1.20 3.60 4 -8 -15 0.60 2.80 -4 8 15 3.70 3.00 4 8 -15 5.00 3.80 -4 8 15 9.10 3.80 3 -8 -15 -2.40 1.90 -3 -8 15 -1.10 4.20 3 8 -15 -2.00 3.00 -3 8 15 0.40 2.60 -2 -8 15 13.70 6.00 2 -8 -15 16.40 5.10 2 8 -15 16.80 5.90 -2 8 15 14.20 5.00 1 -8 -15 16.40 5.30 -1 -8 15 15.00 6.10 -1 8 15 13.60 4.40 1 8 -15 14.80 5.20 0 -8 15 0.60 4.00 0 -8 -15 0.70 3.20 0 8 -15 -0.60 3.60 0 8 15 3.70 3.10 0 8 -15 11.00 4.30 -1 -8 -15 8.30 4.20 1 -8 15 14.10 6.20 -1 8 -15 13.30 5.50 1 8 15 9.00 3.90 -1 8 -15 11.90 4.60 -2 -8 -15 2.00 3.40 2 -8 15 5.30 4.30 2 -8 15 6.70 4.90 2 8 15 8.50 4.00 -2 8 -15 6.80 4.10 -2 8 -15 10.90 5.40 3 -8 15 17.20 5.90 -3 -8 -15 13.70 4.40 3 -8 15 12.10 5.20 -3 8 -15 12.50 5.60 3 8 15 7.30 3.40 -3 8 -15 14.40 5.60 4 -8 15 8.60 4.00 -4 -8 -15 3.50 4.70 4 -8 15 9.60 3.90 -4 8 -15 1.90 3.00 -4 8 -15 3.10 3.90 4 8 15 9.40 3.60 -7 -9 15 0.80 3.40 -7 -9 15 -0.30 3.20 7 9 -15 2.60 4.20 7 9 -15 -3.50 4.20 -7 9 15 0.40 2.70 -6 -9 15 6.60 5.70 6 9 -15 8.00 5.20 6 9 -15 5.00 4.40 -5 -9 15 45.40 10.20 5 -9 -15 56.89 7.90 -5 9 15 47.90 7.60 5 9 -15 48.80 9.50 4 -9 -15 44.90 7.40 -4 -9 15 83.19 13.20 4 9 -15 67.49 10.40 -4 9 15 50.19 7.80 -4 9 15 59.39 8.00 -3 -9 15 25.70 7.90 3 -9 -15 34.20 7.00 3 9 -15 36.80 8.10 -3 9 15 42.30 7.30 -3 9 15 33.80 6.30 2 -9 -15 31.70 6.60 -2 -9 15 19.00 7.30 -2 9 15 20.40 4.90 2 9 -15 20.70 6.30 -1 -9 15 5.00 4.50 1 -9 -15 -0.20 2.70 1 9 -15 -2.00 3.30 -1 9 15 3.10 2.80 0 -9 15 45.30 9.60 0 -9 -15 53.49 8.40 0 9 15 39.80 7.20 0 9 -15 44.60 9.50 0 9 -15 63.09 10.00 -1 -9 -15 6.10 3.80 1 -9 15 -0.60 3.60 1 9 15 6.50 3.80 -1 9 -15 -2.40 3.20 -1 9 -15 7.20 4.50 2 -9 15 16.00 6.10 -2 -9 -15 18.40 6.10 2 -9 15 7.80 4.60 -2 9 -15 7.80 5.30 2 9 15 8.60 4.00 -2 9 -15 9.90 4.70 -3 -9 -15 48.40 8.50 3 -9 15 28.50 7.50 3 -9 15 40.30 8.50 -3 9 -15 52.89 8.80 -3 9 -15 41.90 8.20 3 9 15 27.40 5.80 -4 -9 -15 215.98 17.10 4 -9 15 285.07 19.30 4 -9 15 215.08 16.90 -4 9 -15 220.18 16.40 4 9 15 189.48 14.20 -4 9 -15 204.48 16.20 -7 -10 15 44.80 9.10 -7 -10 15 33.60 9.10 7 10 -15 31.00 7.60 7 10 -15 56.09 11.20 -7 10 15 40.60 7.10 -6 -10 15 47.70 10.70 6 10 -15 50.89 10.00 -6 10 15 58.39 9.10 6 10 -15 44.30 9.10 -6 10 15 39.10 6.90 5 -10 -15 -1.00 2.80 -5 -10 15 4.20 4.80 5 10 -15 2.10 4.30 -5 10 15 3.10 3.10 4 -10 -15 112.49 11.80 -4 -10 15 136.69 16.80 -4 10 15 118.89 12.50 4 10 -15 126.09 15.10 -4 10 15 109.49 11.10 3 -10 -15 62.29 9.00 -3 -10 15 74.59 12.50 -3 10 15 82.49 9.50 -3 10 15 69.99 9.70 3 10 -15 55.79 9.80 -2 -10 15 72.39 12.00 2 -10 -15 41.90 7.30 2 10 -15 58.89 10.00 -2 10 15 56.79 8.10 -1 -10 15 28.60 7.90 1 -10 -15 30.60 6.60 1 10 -15 13.10 5.40 -1 10 15 17.80 4.80 0 -10 -15 79.69 10.60 0 -10 15 70.59 11.60 0 10 15 73.89 9.40 0 10 -15 76.29 11.30 -1 -10 -15 -0.70 3.50 1 -10 15 1.60 4.10 1 10 15 -1.20 2.80 -1 10 -15 2.10 4.10 -1 10 -15 -0.90 3.40 2 -10 15 51.69 9.80 -2 -10 -15 75.79 10.30 -2 10 -15 65.69 10.20 -2 10 -15 65.09 9.30 2 10 15 61.19 8.50 -3 -10 -15 22.50 7.10 3 -10 15 35.30 7.80 3 -10 15 32.80 7.60 -3 10 -15 14.00 4.70 3 10 15 23.90 5.30 -3 10 -15 13.80 4.90 -7 -11 15 4.30 5.70 -7 -11 15 1.10 4.00 7 -11 -15 -0.20 3.30 -7 11 15 1.10 2.90 7 11 -15 0.30 2.90 7 11 -15 1.70 4.00 -6 -11 15 1.00 3.80 6 11 -15 -0.60 2.50 -6 11 15 3.30 3.00 -6 11 15 3.60 2.80 6 11 -15 7.90 5.20 5 -11 -15 4.50 3.40 -5 -11 15 -1.40 4.00 -5 11 15 3.40 3.30 5 11 -15 7.60 4.90 4 -11 -15 23.50 5.50 -4 -11 15 26.50 8.00 4 11 -15 20.50 6.40 -4 11 15 20.80 5.00 -4 11 15 15.70 5.00 3 -11 -15 97.19 10.90 -3 -11 15 88.49 13.90 3 11 -15 90.79 12.70 -3 11 15 95.59 11.10 -3 11 15 101.79 10.50 2 -11 -15 84.49 10.40 -2 -11 15 74.69 12.50 2 11 -15 74.39 11.20 -2 11 15 77.79 9.20 1 -11 -15 45.00 8.10 -1 -11 15 35.10 8.90 1 11 -15 36.20 8.40 -1 11 15 24.40 5.30 0 -11 -15 7.50 4.40 0 -11 15 6.20 5.00 0 11 -15 1.00 3.90 0 11 15 4.40 3.00 -1 -11 -15 84.99 11.30 1 -11 15 80.79 12.70 -1 11 -15 95.29 12.60 -1 11 -15 99.79 11.50 1 11 15 101.69 10.50 2 -11 15 217.68 17.60 -2 -11 -15 194.88 15.30 -2 11 -15 197.48 14.80 -2 11 -15 210.98 19.60 2 11 15 195.38 13.70 3 -11 15 -1.30 4.10 3 -11 15 0.90 3.30 -3 -11 -15 0.00 3.80 3 11 15 0.10 2.10 -3 11 -15 7.00 3.40 -3 11 -15 6.90 4.00 6 -12 -15 14.50 7.10 -6 -12 15 21.30 7.40 -6 12 15 18.30 5.10 -6 12 15 17.60 4.80 6 12 -15 18.30 6.80 6 12 -15 18.70 5.20 -5 -12 15 9.50 6.10 5 -12 -15 11.00 4.00 -5 12 15 19.90 5.20 5 12 -15 5.30 3.90 -5 12 15 12.00 4.20 4 -12 -15 21.20 5.40 -4 -12 15 11.80 6.20 -4 12 15 15.90 5.20 4 12 -15 21.30 6.30 -3 -12 15 16.20 6.60 3 -12 -15 4.20 3.50 -3 12 15 3.70 3.20 3 12 -15 15.50 6.50 -3 12 15 0.80 2.60 -2 -12 15 13.60 6.70 2 -12 -15 23.30 6.10 2 12 -15 24.40 7.30 -2 12 15 16.60 5.00 -2 12 15 15.10 4.50 1 -12 -15 10.40 4.60 -1 -12 15 8.10 5.10 1 12 -15 0.30 4.30 -1 12 15 7.00 3.90 0 -12 15 6.20 4.80 0 -12 -15 4.20 3.90 0 12 15 1.30 2.70 0 12 -15 5.40 4.40 -1 -12 -15 199.08 15.10 1 -12 15 174.58 19.20 -1 12 -15 178.58 17.50 1 12 15 170.98 12.60 -2 -12 -15 13.70 5.30 2 -12 15 20.20 6.80 2 12 15 16.60 4.60 -2 12 -15 9.00 5.00 -2 12 -15 9.00 4.50 -3 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-14 15 81.09 14.10 5 -14 -15 105.99 11.40 -5 14 15 82.09 10.50 5 14 -15 86.19 12.80 4 -14 -15 75.49 10.00 -4 -14 15 77.29 13.50 4 14 -15 81.49 11.70 -4 14 15 90.89 10.90 3 -14 -15 1.30 3.10 -3 -14 15 1.10 4.70 3 14 -15 9.10 3.80 -3 14 15 1.30 2.40 -3 14 15 0.50 2.80 2 -14 -15 63.69 9.60 -2 -14 15 57.59 11.20 2 14 -15 85.39 12.40 -2 14 15 59.49 9.30 -2 14 15 68.09 8.20 1 -14 -15 13.40 4.60 -1 -14 15 18.00 6.90 1 14 -15 9.70 5.20 -1 14 15 6.20 3.70 -1 14 15 5.90 3.00 0 -14 -15 124.29 13.30 0 -14 15 96.89 14.60 0 14 15 104.09 10.70 0 14 -15 112.79 14.10 1 -14 15 11.40 5.20 -1 -14 -15 7.00 4.30 -1 14 -15 -2.60 2.80 1 14 15 5.50 2.80 2 -14 15 104.29 14.40 -2 -14 -15 100.29 12.70 -2 14 -15 77.09 12.00 -2 14 -15 74.19 10.50 2 14 15 83.99 9.60 5 -15 -15 0.80 3.50 -5 15 15 9.10 3.90 5 15 -15 3.00 3.50 -4 -15 15 32.80 9.20 4 -15 -15 26.90 5.80 -4 15 15 24.50 5.50 4 15 -15 31.60 7.60 3 -15 -15 1.60 3.10 -3 -15 15 2.60 5.30 -3 15 15 1.30 2.60 -3 15 15 1.60 2.40 3 15 -15 4.50 4.70 -2 -15 15 117.99 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2.80 1 10 -16 2.90 3.80 0 -10 16 2.90 3.40 0 -10 -16 6.00 4.00 0 10 -16 6.70 4.10 0 10 16 7.00 3.20 1 -10 16 14.10 5.80 -1 -10 -16 9.00 4.70 1 10 16 20.50 5.20 -1 10 -16 20.20 6.30 4 -11 -16 78.69 10.20 -4 -11 16 83.19 14.10 -4 11 16 79.59 10.50 4 11 -16 80.69 12.20 3 -11 -16 2.10 3.30 -3 -11 16 3.30 4.40 3 11 -16 1.80 3.70 -3 11 16 3.80 3.40 -3 11 16 8.00 3.90 2 -11 -16 20.30 5.50 -2 -11 16 29.90 8.10 -2 11 16 25.20 6.10 2 11 -16 13.00 5.70 -2 11 16 28.60 5.80 -1 -11 16 9.30 5.50 1 -11 -16 9.60 4.10 1 11 -16 20.30 6.60 -1 11 16 7.20 3.90 0 -11 -16 8.60 4.30 0 -11 16 6.60 4.40 0 11 -16 10.20 5.80 0 11 16 16.40 4.70 -1 -11 -16 44.60 8.60 1 11 16 41.70 7.20 4 -12 -16 -0.50 2.30 -4 12 16 4.70 3.20 4 12 -16 0.40 3.60 3 -12 -16 36.20 7.00 -3 -12 16 38.70 9.60 3 12 -16 48.20 9.30 -3 12 16 28.40 6.00 -3 12 16 37.60 7.00 -2 -12 16 50.49 10.40 2 -12 -16 61.09 8.60 2 12 -16 56.09 10.70 -2 12 16 43.50 7.20 -2 12 16 49.90 8.30 1 -12 -16 90.29 11.70 -1 -12 16 104.49 14.90 1 12 -16 96.79 13.80 -1 12 16 107.89 11.10 0 -12 -16 -3.40 2.40 0 -12 16 10.20 5.80 0 12 -16 12.70 5.20 0 12 16 3.20 2.90 -2 -13 16 36.90 8.80 2 -13 -16 55.89 9.20 -2 13 16 43.80 8.00 -2 13 16 45.50 6.90 2 13 -16 41.40 9.30 -4 0 17 6.50 3.80 4 0 -17 2.00 3.30 -4 0 17 -0.40 3.90 -3 0 17 -3.40 3.40 -3 0 17 -1.20 3.00 3 0 -17 2.30 2.70 -2 0 17 -3.20 2.90 2 0 -17 -1.20 2.20 -2 0 17 -0.50 2.90 -1 0 17 44.30 8.70 1 0 -17 59.49 9.60 1 0 -17 54.09 9.50 -1 0 17 57.19 10.50 0 0 17 -5.70 2.90 0 0 17 -0.50 3.80 0 0 -17 -0.20 3.30 0 0 -17 0.10 3.50 -4 -1 17 13.70 5.20 4 -1 -17 18.00 5.50 -4 -1 17 12.40 6.20 -4 1 17 20.00 7.00 4 1 -17 21.40 5.80 -4 1 17 6.90 4.50 -3 -1 17 2.00 3.50 3 -1 -17 -3.30 2.10 -3 -1 17 5.90 4.90 3 1 -17 0.30 3.40 -3 1 17 1.70 4.10 -3 1 17 -4.70 3.10 2 -1 -17 4.50 3.30 -2 -1 17 5.10 4.70 -2 -1 17 0.30 3.50 2 1 -17 7.60 3.90 -2 1 17 4.10 3.20 -2 1 17 2.40 4.20 1 -1 -17 8.00 4.80 -1 -1 17 10.80 5.20 1 -1 -17 3.40 3.50 -1 -1 17 5.30 4.80 -1 1 17 3.90 4.80 -1 1 17 5.90 4.00 1 1 -17 7.70 5.10 1 1 -17 7.50 4.80 0 -1 -17 81.39 11.10 0 -1 17 84.79 11.80 0 -1 -17 100.29 11.90 0 -1 17 70.39 11.10 0 1 -17 110.89 13.00 0 1 17 72.59 10.80 0 1 -17 90.49 12.30 -4 -2 17 3.10 4.40 -4 -2 17 5.80 4.40 4 -2 -17 6.00 4.20 4 2 -17 6.10 4.40 -4 2 17 0.30 3.90 3 -2 -17 15.20 4.40 -3 -2 17 22.20 7.00 -3 -2 17 20.90 6.00 3 2 -17 19.90 5.90 -3 2 17 14.70 4.90 2 -2 -17 6.50 4.40 -2 -2 17 1.10 4.00 -2 -2 17 2.80 3.90 2 -2 -17 5.00 3.40 -2 2 17 9.40 4.60 2 2 -17 1.20 3.80 1 -2 -17 3.40 3.90 1 -2 -17 2.90 3.90 -1 -2 17 3.50 3.70 -1 -2 17 1.20 4.10 1 2 -17 4.70 4.30 -1 2 17 -2.60 3.10 0 -2 -17 2.50 3.80 0 -2 17 -1.90 3.10 0 -2 -17 3.10 3.40 0 -2 17 2.20 4.20 0 2 -17 -2.50 2.40 0 2 -17 1.20 4.00 0 2 17 -4.30 2.70 -4 -3 17 0.50 3.50 4 -3 -17 12.00 4.40 4 3 -17 11.80 5.30 -4 3 17 10.10 4.90 -3 -3 17 0.30 3.10 -3 -3 17 7.30 5.30 3 -3 -17 -2.80 2.20 3 3 -17 3.70 4.00 -3 3 17 5.50 3.90 2 -3 -17 129.29 13.60 2 -3 -17 141.09 14.60 -2 -3 17 142.79 16.60 -2 -3 17 113.49 14.20 -2 3 17 120.99 13.70 2 3 -17 126.09 14.70 -1 -3 17 7.00 4.20 -1 -3 17 3.30 4.10 1 -3 -17 2.40 3.40 1 -3 -17 0.70 3.60 -1 3 17 3.30 3.60 1 3 -17 5.60 4.10 0 -3 17 1.50 3.60 0 -3 -17 1.80 2.80 0 -3 17 0.70 4.30 0 -3 -17 -0.30 3.20 0 3 -17 2.40 3.00 0 3 17 -0.70 3.50 0 3 -17 -0.10 3.90 -4 -4 17 3.20 3.30 4 -4 -17 5.90 3.90 4 4 -17 7.70 4.90 -4 4 17 4.10 3.40 -3 -4 17 67.19 11.80 3 -4 -17 104.19 12.20 3 4 -17 68.29 10.70 -3 4 17 64.09 9.70 2 -4 -17 0.00 4.00 -2 -4 17 2.70 4.20 -2 -4 17 -0.60 3.80 2 -4 -17 -0.70 2.20 -2 4 17 1.20 2.70 2 4 -17 9.10 4.90 1 -4 -17 33.10 7.20 1 -4 -17 41.40 7.70 -1 -4 17 39.40 9.10 -1 -4 17 43.50 9.10 -1 4 17 21.80 5.50 1 4 -17 34.60 8.20 0 -4 17 1.50 3.60 0 -4 -17 -0.70 3.10 0 -4 17 1.30 3.60 0 -4 -17 1.20 3.20 0 4 17 4.60 3.80 0 4 -17 -0.10 4.00 0 4 -17 6.70 4.60 3 -5 -17 0.70 3.00 -3 -5 17 4.10 4.30 3 -5 -17 2.60 4.20 3 5 -17 -5.20 3.00 -3 5 17 1.90 3.50 2 -5 -17 26.10 6.30 2 -5 -17 23.10 5.80 -2 -5 17 15.70 6.50 2 5 -17 8.80 5.70 -2 5 17 15.90 5.30 1 -5 -17 -0.90 2.60 -1 -5 17 3.70 3.90 1 -5 -17 -1.50 3.00 -1 -5 17 1.70 3.50 1 5 -17 -3.20 3.00 -1 5 17 2.70 3.00 -3 -6 17 17.00 6.00 3 -6 -17 10.10 4.80 3 -6 -17 13.00 4.70 3 6 -17 16.20 6.00 -3 6 17 13.60 4.30 -2 -6 17 5.60 4.20 2 -6 -17 5.00 4.00 2 6 -17 1.90 3.10 -2 6 17 -2.40 2.50 -1 -6 17 7.10 4.40 1 -6 -17 1.60 3.40 -1 -6 17 5.90 4.10 1 6 -17 4.20 3.70 -1 6 17 -1.40 2.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 72749 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.83810(3) 0.49930(2) 0.65025(3) 0.01550(7) Uani 1 1 d . . . . . S2 S 0.55076(3) 0.87514(2) 1.09134(3) 0.01511(7) Uani 1 1 d . . . . . O1 O 0.44241(10) 0.68797(4) 0.81359(8) 0.0208(2) Uani 1 1 d . . . . . O2 O 0.51691(10) 0.63613(4) 1.31619(8) 0.0230(2) Uani 1 1 d . . . . . N1 N 0.68926(12) 0.56808(5) 0.50782(9) 0.0168(2) Uani 1 1 d D . . . . H1N H 0.6676(16) 0.5793(7) 0.4420(11) 0.020 Uiso 1 1 d D U . . . N2 N 0.82288(11) 0.50461(5) 0.43493(9) 0.0153(2) Uani 1 1 d D . . . . H2N H 0.8752(15) 0.4758(6) 0.4419(13) 0.018 Uiso 1 1 d D U . . . N3 N 0.76431(11) 0.52308(5) 0.33271(9) 0.0152(2) Uani 1 1 d D . . . . N4 N 0.51884(13) 0.78357(5) 0.96535(9) 0.0186(2) Uani 1 1 d D . . . . H4N H 0.5089(17) 0.7696(7) 0.9019(11) 0.022 Uiso 1 1 d D U . . . N5 N 0.52852(12) 0.86760(5) 0.87740(9) 0.0170(2) Uani 1 1 d D . . . . H5N H 0.5443(17) 0.9031(5) 0.8798(13) 0.020 Uiso 1 1 d D U . . . N6 N 0.51627(11) 0.83910(5) 0.77934(9) 0.0164(2) Uani 1 1 d D . . . . C1 C 0.77930(13) 0.52605(5) 0.52544(10) 0.0135(2) Uani 1 1 d D . . . . C2 C 0.62837(13) 0.59602(5) 0.59147(10) 0.0150(2) Uani 1 1 d D . . . . C3 C 0.49935(14) 0.58048(6) 0.61076(11) 0.0200(3) Uani 1 1 d . . . . . H3 H 0.455292 0.549223 0.573160 0.024 Uiso 1 1 calc R U . . . C4 C 0.43335(14) 0.61023(6) 0.68482(11) 0.0194(3) Uani 1 1 d . . . . . H4 H 0.344031 0.599817 0.696789 0.023 Uiso 1 1 calc R U . . . C5 C 0.49946(13) 0.65525(5) 0.74098(10) 0.0152(2) Uani 1 1 d . . . . . C6 C 0.63167(13) 0.66952(6) 0.72504(11) 0.0174(3) Uani 1 1 d . . . . . H6 H 0.678314 0.699247 0.765933 0.021 Uiso 1 1 calc R U . . . C7 C 0.69517(13) 0.64035(6) 0.64949(11) 0.0177(3) Uani 1 1 d . . . . . H7 H 0.784489 0.650679 0.637386 0.021 Uiso 1 1 calc R U . . . C8 C 0.30540(14) 0.67453(7) 0.82952(13) 0.0257(3) Uani 1 1 d . . . . . H8A H 0.246470 0.673161 0.758325 0.039 Uiso 1 1 calc R U . . . H8B H 0.271560 0.703247 0.875505 0.039 Uiso 1 1 calc R U . . . H8C H 0.304546 0.638018 0.865620 0.039 Uiso 1 1 calc R U . . . C9 C 0.80078(13) 0.49652(5) 0.25124(10) 0.0150(2) Uani 1 1 d . . . . . H9 H 0.865092 0.466907 0.265327 0.018 Uiso 1 1 calc R U . . . C10 C 0.74660(13) 0.51033(5) 0.13727(10) 0.0151(2) Uani 1 1 d . . . . . C11 C 0.79115(15) 0.47862(6) 0.05433(11) 0.0207(3) Uani 1 1 d . . . . . H11 H 0.852927 0.448476 0.072806 0.025 Uiso 1 1 calc R U . . . C12 C 0.74559(17) 0.49090(6) -0.05521(12) 0.0256(3) Uani 1 1 d . . . . . H12 H 0.776470 0.469200 -0.111255 0.031 Uiso 1 1 calc R U . . . C13 C 0.65551(16) 0.53461(7) -0.08269(12) 0.0267(3) Uani 1 1 d . . . . . H13 H 0.625021 0.543171 -0.157533 0.032 Uiso 1 1 calc R U . . . C14 C 0.60969(16) 0.56597(7) -0.00060(12) 0.0266(3) Uani 1 1 d . . . . . H14 H 0.547294 0.595860 -0.019563 0.032 Uiso 1 1 calc R U . . . C15 C 0.65426(14) 0.55401(6) 0.10878(11) 0.0208(3) Uani 1 1 d . . . . . H15 H 0.621993 0.575532 0.164442 0.025 Uiso 1 1 calc R U . . . C16 C 0.53269(12) 0.83930(5) 0.97310(10) 0.0136(2) Uani 1 1 d D . . . . C17 C 0.51696(14) 0.74789(5) 1.05871(10) 0.0158(2) Uani 1 1 d D . . . . C18 C 0.63837(14) 0.72825(6) 1.11792(12) 0.0206(3) Uani 1 1 d . . . . . H18 H 0.723610 0.739853 1.098740 0.025 Uiso 1 1 calc R U . . . C19 C 0.63510(14) 0.69184(6) 1.20470(12) 0.0205(3) Uani 1 1 d . . . . . H19 H 0.718086 0.679069 1.246023 0.025 Uiso 1 1 calc R U . . . C20 C 0.51003(14) 0.67386(5) 1.23157(11) 0.0167(2) Uani 1 1 d . . . . . C21 C 0.38833(14) 0.69380(6) 1.17352(11) 0.0185(3) Uani 1 1 d . . . . . H21 H 0.302985 0.681995 1.192188 0.022 Uiso 1 1 calc R U . . . C22 C 0.39303(14) 0.73128(6) 1.08766(11) 0.0175(3) Uani 1 1 d . . . . . H22 H 0.310289 0.745598 1.048529 0.021 Uiso 1 1 calc R U . . . C23 C 0.3929(2) 0.60856(10) 1.32923(16) 0.0504(6) Uani 1 1 d . . . . . H23A H 0.347503 0.595462 1.257694 0.076 Uiso 1 1 calc R U . . . H23B H 0.332662 0.634710 1.360415 0.076 Uiso 1 1 calc R U . . . H23C H 0.412916 0.576499 1.378570 0.076 Uiso 1 1 calc R U . . . C24 C 0.49796(13) 0.87025(6) 0.69365(10) 0.0162(2) Uani 1 1 d . . . . . H24 H 0.491135 0.909631 0.702092 0.019 Uiso 1 1 calc R U . . . C25 C 0.48734(13) 0.84661(5) 0.58317(10) 0.0152(2) Uani 1 1 d . . . . . C26 C 0.50965(14) 0.78969(6) 0.56453(11) 0.0185(3) Uani 1 1 d . . . . . H26 H 0.530223 0.764732 0.624672 0.022 Uiso 1 1 calc R U . . . C27 C 0.50159(14) 0.76988(6) 0.45795(12) 0.0213(3) Uani 1 1 d . . . . . H27 H 0.516543 0.731294 0.445363 0.026 Uiso 1 1 calc R U . . . C28 C 0.47167(14) 0.80630(6) 0.36920(11) 0.0213(3) Uani 1 1 d . . . . . H28 H 0.468184 0.792694 0.296473 0.026 Uiso 1 1 calc R U . . . C29 C 0.44704(14) 0.86241(6) 0.38745(11) 0.0207(3) Uani 1 1 d . . . . . H29 H 0.425185 0.887177 0.327138 0.025 Uiso 1 1 calc R U . . . C30 C 0.45434(13) 0.88242(6) 0.49398(11) 0.0178(3) Uani 1 1 d . . . . . H30 H 0.436684 0.920831 0.506090 0.021 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.01975(15) 0.01465(15) 0.01222(14) 0.00160(11) 0.00284(11) 0.00164(11) S2 0.02063(15) 0.01315(14) 0.01150(14) -0.00163(11) 0.00219(11) -0.00126(11) O1 0.0179(5) 0.0228(5) 0.0222(5) -0.0104(4) 0.0049(4) -0.0008(4) O2 0.0245(5) 0.0218(5) 0.0214(5) 0.0087(4) -0.0009(4) -0.0065(4) N1 0.0199(5) 0.0191(5) 0.0113(5) 0.0003(4) 0.0020(4) 0.0057(4) N2 0.0185(5) 0.0155(5) 0.0119(5) 0.0009(4) 0.0024(4) 0.0045(4) N3 0.0179(5) 0.0149(5) 0.0123(5) 0.0011(4) 0.0007(4) 0.0008(4) N4 0.0302(6) 0.0142(5) 0.0118(5) -0.0022(4) 0.0041(4) -0.0038(4) N5 0.0265(6) 0.0135(5) 0.0109(5) -0.0012(4) 0.0025(4) -0.0030(4) N6 0.0196(5) 0.0177(5) 0.0120(5) -0.0030(4) 0.0023(4) -0.0028(4) C1 0.0140(5) 0.0130(6) 0.0136(6) -0.0004(4) 0.0025(4) -0.0017(4) C2 0.0166(6) 0.0150(6) 0.0133(6) 0.0001(5) 0.0015(4) 0.0048(5) C3 0.0198(6) 0.0178(6) 0.0224(7) -0.0075(5) 0.0036(5) -0.0026(5) C4 0.0164(6) 0.0201(6) 0.0223(7) -0.0056(5) 0.0050(5) -0.0033(5) C5 0.0172(6) 0.0146(6) 0.0138(6) -0.0013(5) 0.0021(5) 0.0025(5) C6 0.0166(6) 0.0154(6) 0.0195(6) -0.0043(5) 0.0006(5) -0.0020(5) C7 0.0147(6) 0.0182(6) 0.0203(6) -0.0011(5) 0.0029(5) -0.0006(5) C8 0.0172(6) 0.0363(8) 0.0241(7) -0.0124(6) 0.0045(5) 0.0005(6) C9 0.0177(6) 0.0126(6) 0.0148(6) 0.0011(4) 0.0027(5) 0.0004(4) C10 0.0183(6) 0.0133(6) 0.0137(6) 0.0015(4) 0.0019(5) -0.0012(4) C11 0.0281(7) 0.0181(6) 0.0161(6) -0.0002(5) 0.0043(5) 0.0033(5) C12 0.0381(8) 0.0249(7) 0.0140(6) -0.0031(5) 0.0048(6) -0.0017(6) C13 0.0315(8) 0.0307(8) 0.0161(7) 0.0038(6) -0.0032(6) -0.0049(6) C14 0.0266(7) 0.0278(8) 0.0235(7) 0.0058(6) -0.0027(6) 0.0051(6) C15 0.0230(7) 0.0207(7) 0.0185(6) 0.0010(5) 0.0020(5) 0.0044(5) C16 0.0129(5) 0.0139(6) 0.0140(6) -0.0007(4) 0.0018(4) -0.0009(4) C17 0.0238(6) 0.0101(5) 0.0138(6) -0.0008(4) 0.0039(5) -0.0010(5) C18 0.0184(6) 0.0191(6) 0.0253(7) 0.0019(5) 0.0067(5) -0.0017(5) C19 0.0172(6) 0.0186(6) 0.0253(7) 0.0033(5) 0.0015(5) 0.0026(5) C20 0.0222(6) 0.0125(6) 0.0152(6) 0.0002(5) 0.0015(5) -0.0013(5) C21 0.0173(6) 0.0218(7) 0.0164(6) 0.0001(5) 0.0028(5) -0.0040(5) C22 0.0184(6) 0.0180(6) 0.0154(6) -0.0009(5) 0.0001(5) 0.0007(5) C23 0.0383(10) 0.0673(14) 0.0399(10) 0.0329(10) -0.0135(8) -0.0311(10) C24 0.0171(6) 0.0172(6) 0.0143(6) -0.0018(5) 0.0026(5) -0.0011(5) C25 0.0138(6) 0.0178(6) 0.0137(6) -0.0014(5) 0.0014(4) -0.0019(4) C26 0.0204(6) 0.0183(6) 0.0162(6) -0.0001(5) 0.0006(5) 0.0002(5) C27 0.0231(7) 0.0193(6) 0.0211(7) -0.0062(5) 0.0014(5) 0.0005(5) C28 0.0203(6) 0.0278(7) 0.0153(6) -0.0059(5) 0.0008(5) -0.0023(5) C29 0.0229(7) 0.0254(7) 0.0129(6) 0.0010(5) -0.0002(5) -0.0022(5) C30 0.0189(6) 0.0181(6) 0.0160(6) -0.0002(5) 0.0010(5) -0.0002(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C5 O1 C8 116.77(11) . . ? C20 O2 C23 116.32(12) . . ? C1 N1 C2 124.93(12) . . ? C1 N1 H1N 117.3(11) . . ? C2 N1 H1N 117.8(11) . . ? C1 N2 N3 119.35(12) . . ? C1 N2 H2N 118.8(10) . . ? N3 N2 H2N 120.9(10) . . ? C9 N3 N2 115.36(12) . . ? C16 N4 C17 123.10(12) . . ? C16 N4 H4N 117.2(11) . . ? C17 N4 H4N 119.7(11) . . ? C16 N5 N6 120.35(12) . . ? C16 N5 H5N 118.6(11) . . ? N6 N5 H5N 120.6(11) . . ? C24 N6 N5 114.83(13) . . ? N1 C1 N2 115.78(12) . . ? N1 C1 S1 124.26(10) . . ? N2 C1 S1 119.95(11) . . ? C3 C2 C7 119.77(12) . . ? C3 C2 N1 119.68(12) . . ? C7 C2 N1 120.47(12) . . ? C2 C3 C4 120.63(13) . . ? C2 C3 H3 119.7 . . ? C4 C3 H3 119.7 . . ? C5 C4 C3 119.35(13) . . ? C5 C4 H4 120.3 . . ? C3 C4 H4 120.3 . . ? O1 C5 C4 123.92(12) . . ? O1 C5 C6 115.98(12) . . ? C4 C5 C6 120.09(12) . . ? C7 C6 C5 119.99(12) . . ? C7 C6 H6 120.0 . . ? C5 C6 H6 120.0 . . ? C6 C7 C2 120.09(13) . . ? C6 C7 H7 120.0 . . ? C2 C7 H7 120.0 . . ? O1 C8 H8A 109.5 . . ? O1 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? O1 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? N3 C9 C10 122.28(13) . . ? N3 C9 H9 118.9 . . ? C10 C9 H9 118.9 . . ? C11 C10 C15 119.12(13) . . ? C11 C10 C9 118.07(13) . . ? C15 C10 C9 122.81(12) . . ? C12 C11 C10 120.37(14) . . ? C12 C11 H11 119.8 . . ? C10 C11 H11 119.8 . . ? C13 C12 C11 120.14(14) . . ? C13 C12 H12 119.9 . . ? C11 C12 H12 119.9 . . ? C12 C13 C14 119.80(14) . . ? C12 C13 H13 120.1 . . ? C14 C13 H13 120.1 . . ? C15 C14 C13 120.51(15) . . ? C15 C14 H14 119.7 . . ? C13 C14 H14 119.7 . . ? C14 C15 C10 120.06(13) . . ? C14 C15 H15 120.0 . . ? C10 C15 H15 120.0 . . ? N4 C16 N5 116.34(12) . . ? N4 C16 S2 124.43(10) . . ? N5 C16 S2 119.21(11) . . ? C22 C17 C18 119.74(13) . . ? C22 C17 N4 119.63(12) . . ? C18 C17 N4 120.59(12) . . ? C19 C18 C17 120.07(13) . . ? C19 C18 H18 120.0 . . ? C17 C18 H18 120.0 . . ? C18 C19 C20 120.04(13) . . ? C18 C19 H19 120.0 . . ? C20 C19 H19 120.0 . . ? O2 C20 C21 123.92(12) . . ? O2 C20 C19 115.90(12) . . ? C21 C20 C19 120.18(13) . . ? C20 C21 C22 119.21(13) . . ? C20 C21 H21 120.4 . . ? C22 C21 H21 120.4 . . ? C17 C22 C21 120.72(13) . . ? C17 C22 H22 119.6 . . ? C21 C22 H22 119.6 . . ? O2 C23 H23A 109.5 . . ? O2 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? O2 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? N6 C24 C25 121.65(13) . . ? N6 C24 H24 119.2 . . ? C25 C24 H24 119.2 . . ? C30 C25 C26 119.34(13) . . ? C30 C25 C24 118.29(13) . . ? C26 C25 C24 122.37(12) . . ? C27 C26 C25 119.83(13) . . ? C27 C26 H26 120.1 . . ? C25 C26 H26 120.1 . . ? C26 C27 C28 120.41(14) . . ? C26 C27 H27 119.8 . . ? C28 C27 H27 119.8 . . ? C29 C28 C27 119.82(13) . . ? C29 C28 H28 120.1 . . ? C27 C28 H28 120.1 . . ? C28 C29 C30 120.00(13) . . ? C28 C29 H29 120.0 . . ? C30 C29 H29 120.0 . . ? C29 C30 C25 120.56(14) . . ? C29 C30 H30 119.7 . . ? C25 C30 H30 119.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 C1 1.6887(17) . ? S2 C16 1.6778(17) . ? O1 C5 1.3715(17) . ? O1 C8 1.434(2) . ? O2 C20 1.3732(18) . ? O2 C23 1.422(2) . ? N1 C1 1.3381(18) . ? N1 C2 1.4341(18) . ? N1 H1N 0.851(12) . ? N2 C1 1.3554(18) . ? N2 N3 1.3798(17) . ? N2 H2N 0.857(12) . ? N3 C9 1.2845(18) . ? N4 C16 1.340(2) . ? N4 C17 1.4350(19) . ? N4 H4N 0.844(13) . ? N5 C16 1.3557(18) . ? N5 N6 1.3776(17) . ? N5 H5N 0.862(13) . ? N6 C24 1.2834(19) . ? C2 C3 1.383(2) . ? C2 C7 1.389(2) . ? C3 C4 1.394(2) . ? C3 H3 0.9500 . ? C4 C5 1.389(2) . ? C4 H4 0.9500 . ? C5 C6 1.393(2) . ? C6 C7 1.386(2) . ? C6 H6 0.9500 . ? C7 H7 0.9500 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 C10 1.466(2) . ? C9 H9 0.9500 . ? C10 C11 1.396(2) . ? C10 C15 1.397(2) . ? C11 C12 1.391(2) . ? C11 H11 0.9500 . ? C12 C13 1.382(2) . ? C12 H12 0.9500 . ? C13 C14 1.389(2) . ? C13 H13 0.9500 . ? C14 C15 1.386(2) . ? C14 H14 0.9500 . ? C15 H15 0.9500 . ? C17 C22 1.384(2) . ? C17 C18 1.391(2) . ? C18 C19 1.383(2) . ? C18 H18 0.9500 . ? C19 C20 1.395(2) . ? C19 H19 0.9500 . ? C20 C21 1.390(2) . ? C21 C22 1.393(2) . ? C21 H21 0.9500 . ? C22 H22 0.9500 . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 C25 1.464(2) . ? C24 H24 0.9500 . ? C25 C30 1.394(2) . ? C25 C26 1.402(2) . ? C26 C27 1.388(2) . ? C26 H26 0.9500 . ? C27 C28 1.395(2) . ? C27 H27 0.9500 . ? C28 C29 1.387(2) . ? C28 H28 0.9500 . ? C29 C30 1.390(2) . ? C29 H29 0.9500 . ? C30 H30 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 N2 N3 C9 -172.88(12) . . . . ? C16 N5 N6 C24 172.54(12) . . . . ? C2 N1 C1 N2 178.81(12) . . . . ? C2 N1 C1 S1 -0.81(19) . . . . ? N3 N2 C1 N1 -5.89(17) . . . . ? N3 N2 C1 S1 173.76(9) . . . . ? C1 N1 C2 C3 -97.73(17) . . . . ? C1 N1 C2 C7 85.42(18) . . . . ? C7 C2 C3 C4 2.5(2) . . . . ? N1 C2 C3 C4 -174.37(13) . . . . ? C2 C3 C4 C5 -1.2(2) . . . . ? C8 O1 C5 C4 -1.08(19) . . . . ? C8 O1 C5 C6 178.88(12) . . . . ? C3 C4 C5 O1 178.47(13) . . . . ? C3 C4 C5 C6 -1.5(2) . . . . ? O1 C5 C6 C7 -177.13(12) . . . . ? C4 C5 C6 C7 2.8(2) . . . . ? C5 C6 C7 C2 -1.5(2) . . . . ? C3 C2 C7 C6 -1.2(2) . . . . ? N1 C2 C7 C6 175.69(12) . . . . ? N2 N3 C9 C10 179.10(11) . . . . ? N3 C9 C10 C11 -179.22(13) . . . . ? N3 C9 C10 C15 1.6(2) . . . . ? C15 C10 C11 C12 0.9(2) . . . . ? C9 C10 C11 C12 -178.35(13) . . . . ? C10 C11 C12 C13 -0.1(2) . . . . ? C11 C12 C13 C14 -0.5(2) . . . . ? C12 C13 C14 C15 0.4(2) . . . . ? C13 C14 C15 C10 0.4(2) . . . . ? C11 C10 C15 C14 -1.0(2) . . . . ? C9 C10 C15 C14 178.20(13) . . . . ? C17 N4 C16 N5 -178.09(12) . . . . ? C17 N4 C16 S2 0.45(19) . . . . ? N6 N5 C16 N4 -2.57(18) . . . . ? N6 N5 C16 S2 178.81(9) . . . . ? C16 N4 C17 C22 96.42(16) . . . . ? C16 N4 C17 C18 -85.90(17) . . . . ? C22 C17 C18 C19 0.6(2) . . . . ? N4 C17 C18 C19 -177.05(12) . . . . ? C17 C18 C19 C20 1.3(2) . . . . ? C23 O2 C20 C21 12.6(2) . . . . ? C23 O2 C20 C19 -167.05(16) . . . . ? C18 C19 C20 O2 177.61(13) . . . . ? C18 C19 C20 C21 -2.0(2) . . . . ? O2 C20 C21 C22 -178.81(12) . . . . ? C19 C20 C21 C22 0.8(2) . . . . ? C18 C17 C22 C21 -1.9(2) . . . . ? N4 C17 C22 C21 175.83(12) . . . . ? C20 C21 C22 C17 1.2(2) . . . . ? N5 N6 C24 C25 178.04(11) . . . . ? N6 C24 C25 C30 173.89(12) . . . . ? N6 C24 C25 C26 -6.4(2) . . . . ? C30 C25 C26 C27 1.4(2) . . . . ? C24 C25 C26 C27 -178.35(12) . . . . ? C25 C26 C27 C28 0.1(2) . . . . ? C26 C27 C28 C29 -1.3(2) . . . . ? C27 C28 C29 C30 1.0(2) . . . . ? C28 C29 C30 C25 0.5(2) . . . . ? C26 C25 C30 C29 -1.7(2) . . . . ? C24 C25 C30 C29 178.05(12) . . . . ?