#------------------------------------------------------------------------------ #$Date: 2025-02-04 15:56:51 +0200 (Tue, 04 Feb 2025) $ #$Revision: 297586 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/38/1573845.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573845 loop_ _publ_author_name 'Costa, Ant\'onio G.' 'Lopes, Gon\,calo' 'Rodrigues, Jo\~ao F. G.' 'Santos, Isabel C.' 'Sim\~ao, Dulce' 'Lopes, Elsa B.' 'Pereira, Laura C. J.' 'Le Breton, Nolwenn' 'Choua, Sylvie' 'Baudron, St\'ephane A.' 'Almeida, Manuel' 'Raba\,ca, Sandra' _publ_section_title ; Cobalt and Iron Cyano Benzene Bis(Dithiolene) Complexes ; _journal_issue 5 _journal_name_full Crystals _journal_page_first 469 _journal_paper_doi 10.3390/cryst14050469 _journal_volume 14 _journal_year 2024 _chemical_formula_sum 'C62 H46 Co N2 P2 S4' _chemical_formula_weight 1068.12 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 88.930(2) _cell_angle_beta 78.425(2) _cell_angle_gamma 87.578(2) _cell_formula_units_Z 6 _cell_length_a 14.0437(7) _cell_length_b 22.4513(13) _cell_length_c 26.2961(15) _cell_measurement_reflns_used 2982 _cell_measurement_temperature 294(2) _cell_measurement_theta_max 24.10 _cell_measurement_theta_min 2.37 _cell_volume 8114.8(8) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 294(2) _diffrn_measured_fraction_theta_full 0.971 _diffrn_measured_fraction_theta_max 0.970 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.2535 _diffrn_reflns_av_unetI/netI 0.3548 _diffrn_reflns_Laue_measured_fraction_full 0.971 _diffrn_reflns_Laue_measured_fraction_max 0.970 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 64280 _diffrn_reflns_point_group_measured_fraction_full 0.971 _diffrn_reflns_point_group_measured_fraction_max 0.970 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.682 _diffrn_reflns_theta_min 2.910 _exptl_absorpt_coefficient_mu 0.572 _exptl_absorpt_correction_T_max 0.989 _exptl_absorpt_correction_T_min 0.803 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.311 _exptl_crystal_description needle _exptl_crystal_F_000 3318 _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.020 _exptl_crystal_size_min 0.020 _refine_diff_density_max 0.520 _refine_diff_density_min -0.384 _refine_diff_density_rms 0.064 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.825 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1897 _refine_ls_number_reflns 29898 _refine_ls_number_restraints 127 _refine_ls_restrained_S_all 0.824 _refine_ls_R_factor_all 0.3416 _refine_ls_R_factor_gt 0.0945 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0443P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1375 _refine_ls_wR_factor_ref 0.1850 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 7502 _reflns_number_total 29898 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file TPP2Co3-cbdt2-2.cif _cod_data_source_block Co2(3-cbdt)2 _cod_database_code 1573845 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.803 _shelx_estimated_absorpt_t_max 0.989 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL 345_a.res in P-1 CELL 0.71073 14.0437 22.4513 26.2961 88.930 78.425 87.578 ZERR 6.00 0.0007 0.0013 0.0015 0.002 0.002 0.002 LATT 1 SFAC C H CO N P S UNIT 372 276 6 12 12 24 MERG 2 OMIT 0.00 180.00 shel 7 0.82 DFIX 1.450 0.020 C35 C34 isor 0.001 C7f C8f C9f C10f C11f C12f isor 0.001 C29 C30 C31 C32 C33 C34 C35 N5 isor 0.001 C22 C23 C24 C25 C26 C27 C28 FMAP 2 PLAN 20 SIZE 0.020 0.020 0.400 ACTA BOND LIST 4 L.S. 10 TEMP 21.00 WGHT 0.044300 FVAR 0.19364 CO1 3 0.000000 1.000000 0.000000 10.50000 0.06507 0.04260 = 0.05650 0.00470 -0.02108 0.00113 CO2 3 0.500000 0.500000 0.000000 10.50000 0.06248 0.05145 = 0.08343 -0.01304 0.00337 0.00353 CO3 3 0.371339 0.977982 0.361129 11.00000 0.04777 0.07327 = 0.07554 -0.00620 -0.01653 -0.00713 CO4 3 0.170723 0.541605 0.642606 11.00000 0.04926 0.06661 = 0.09221 -0.01542 -0.01369 0.00420 P1 5 0.177739 0.663366 -0.065888 11.00000 0.05143 0.05673 = 0.06829 -0.00355 -0.00560 0.00613 P2 5 0.632184 0.830142 0.062647 11.00000 0.04422 0.05460 = 0.05587 -0.00439 -0.01033 0.01221 P3 5 0.339130 0.610248 0.274719 11.00000 0.06117 0.05598 = 0.06866 0.00459 -0.02760 0.00937 P4 5 0.648508 0.673858 0.580404 11.00000 0.05331 0.05663 = 0.09906 -0.00176 -0.02747 0.00474 P5 5 0.147854 0.141249 0.658219 11.00000 0.04076 0.05126 = 0.05845 0.00071 -0.01246 -0.00102 P6 5 0.048794 0.883855 0.710956 11.00000 0.04645 0.06384 = 0.09220 0.00003 -0.02137 -0.00038 S1 6 0.065097 0.936140 0.047411 11.00000 0.07987 0.07035 = 0.05297 0.01214 -0.01628 0.01885 S2 6 0.136140 1.001032 -0.057304 11.00000 0.07730 0.06873 = 0.08254 0.03333 -0.00889 0.00151 S3 6 0.602379 0.561509 -0.042871 11.00000 0.07432 0.07547 = 0.08158 -0.00889 0.00151 -0.00264 S4 6 0.575976 0.500390 0.064992 11.00000 0.08979 0.06325 = 0.09345 -0.00693 -0.01103 0.00415 S5 6 0.465039 0.911352 0.314844 11.00000 0.07680 0.07564 = 0.06228 0.00312 -0.01858 0.00036 S6 6 0.350827 0.919060 0.429166 11.00000 0.06121 0.10551 = 0.06903 -0.00736 -0.00914 -0.01528 S7 6 0.404976 1.039450 0.295954 11.00000 0.06726 0.06412 = 0.08044 -0.00398 -0.01902 -0.00051 S8 6 0.259624 1.040461 0.401608 11.00000 0.05882 0.09923 = 0.09562 -0.01550 -0.00377 0.00380 S9 6 0.202807 0.615177 0.588500 11.00000 0.08649 0.06988 = 0.12112 -0.00134 -0.01671 -0.00958 S10 6 0.241998 0.584998 0.698073 11.00000 0.10790 0.09755 = 0.13573 -0.01901 -0.04289 -0.01883 S11 6 0.109042 0.497983 0.584315 11.00000 0.08489 0.07078 = 0.08055 0.00402 -0.02887 -0.00057 S12 6 0.123255 0.471629 0.699225 11.00000 0.06108 0.08004 = 0.07572 -0.01153 -0.02263 0.00541 N1 4 0.177264 0.821418 0.114968 11.00000 0.15744 0.18624 = 0.09057 0.06265 0.01778 0.08479 N2 4 0.779440 0.668160 -0.107612 11.00000 0.15432 0.12027 = 0.14666 0.01730 0.02184 -0.06399 N3 4 0.608597 0.785656 0.244063 11.00000 0.16578 0.16849 = 0.11644 -0.03700 -0.04784 0.07676 N4 4 0.448282 1.150972 0.192472 11.00000 0.13206 0.10991 = 0.11354 0.03424 -0.04693 -0.00671 N5 4 0.222669 0.749500 0.514910 11.00000 0.14636 0.14429 = 0.14663 -0.00135 -0.02817 -0.00593 N6 4 0.026887 0.345769 0.786791 11.00000 0.12588 0.16382 = 0.05689 0.01647 -0.01927 -0.00017 C1 1 0.181366 0.919871 0.013299 11.00000 0.03706 0.07728 = 0.07043 -0.00495 -0.02306 0.00314 C2 1 0.214460 0.948088 -0.034324 11.00000 0.05982 0.05024 = 0.08233 0.00812 -0.00582 0.00376 C3 1 0.304585 0.932914 -0.063853 11.00000 0.05633 0.13335 = 0.08664 0.03553 -0.01112 -0.01520 AFIX 43 H3 2 0.325317 0.951659 -0.095757 11.00000 -1.20000 AFIX 0 C4 1 0.365055 0.889596 -0.046241 11.00000 0.03466 0.16025 = 0.11058 0.03160 -0.02081 0.02298 AFIX 43 H4 2 0.426430 0.880396 -0.066004 11.00000 -1.20000 AFIX 0 C5 1 0.334135 0.860689 0.000031 11.00000 0.06746 0.13216 = 0.09404 0.03466 -0.02199 0.02534 AFIX 43 H5 2 0.373182 0.831232 0.011857 11.00000 -1.20000 AFIX 0 C6 1 0.243889 0.876408 0.028471 11.00000 0.06383 0.07099 = 0.07049 0.00725 -0.02064 0.01634 C7 1 0.206522 0.844544 0.076380 11.00000 0.07447 0.11078 = 0.08569 0.02414 -0.01844 0.04491 C8 1 0.683386 0.574701 -0.002612 11.00000 0.05935 0.05255 = 0.09846 -0.01281 -0.00268 0.00919 C9 1 0.674295 0.547383 0.043752 11.00000 0.06175 0.04338 = 0.10313 -0.00864 -0.00038 0.00443 C10 1 0.739010 0.556754 0.077438 11.00000 0.08126 0.08429 = 0.12980 -0.01857 -0.02612 0.01055 AFIX 43 H10 2 0.730996 0.537055 0.109350 11.00000 -1.20000 AFIX 0 C11 1 0.813388 0.594841 0.062989 11.00000 0.10954 0.10749 = 0.12881 -0.02902 -0.03030 0.02860 AFIX 43 H11 2 0.857281 0.600976 0.084389 11.00000 -1.20000 AFIX 0 C12 1 0.821346 0.623923 0.015648 11.00000 0.05353 0.07419 = 0.19509 -0.03966 -0.00422 0.00272 AFIX 43 H12 2 0.870383 0.650864 0.005814 11.00000 -1.20000 AFIX 0 C13 1 0.760008 0.614504 -0.017002 11.00000 0.06786 0.07601 = 0.09178 -0.02989 0.01139 0.01668 C14 1 0.769381 0.644810 -0.068466 11.00000 0.07469 0.09186 = 0.13581 -0.02602 0.04849 -0.02778 C15 1 0.464277 0.849325 0.356403 11.00000 0.04800 0.05943 = 0.06809 0.01011 -0.03686 -0.01117 C16 1 0.411490 0.852747 0.407192 11.00000 0.05102 0.08742 = 0.06718 0.02001 -0.01703 -0.02429 C17 1 0.408672 0.800918 0.439338 11.00000 0.08328 0.09915 = 0.08348 0.02256 -0.00658 -0.00080 AFIX 43 H17 2 0.373586 0.801841 0.473321 11.00000 -1.20000 AFIX 0 C18 1 0.457832 0.749744 0.419994 11.00000 0.09110 0.08409 = 0.12564 0.02991 -0.02787 -0.01711 AFIX 43 H18 2 0.454971 0.716574 0.441887 11.00000 -1.20000 AFIX 0 C19 1 0.510734 0.744140 0.370758 11.00000 0.07531 0.07337 = 0.11907 0.01321 -0.03016 -0.00815 AFIX 43 H19 2 0.543554 0.708617 0.359013 11.00000 -1.20000 AFIX 0 C20 1 0.512903 0.795138 0.338684 11.00000 0.06274 0.07540 = 0.07441 -0.00547 -0.02151 -0.01014 C21 1 0.569155 0.792113 0.284053 11.00000 0.09593 0.06135 = 0.12925 -0.02142 -0.05581 0.01382 AFIX 66 C22 1 0.325730 1.101354 0.311807 11.00000 0.07310 0.07345 = 0.07379 -0.00155 -0.01542 -0.00325 C23 1 0.259609 1.101207 0.358857 11.00000 0.08090 0.08079 = 0.08149 -0.00115 -0.01665 -0.00289 C24 1 0.194353 1.149377 0.372010 11.00000 0.10078 0.10119 = 0.10143 -0.00193 -0.02013 -0.00363 AFIX 43 H24 2 0.150114 1.149278 0.403490 11.00000 -1.20000 AFIX 65 C25 1 0.195217 1.197694 0.338113 11.00000 0.09906 0.09955 = 0.10015 -0.00220 -0.02062 -0.00357 AFIX 43 H25 2 0.151556 1.229923 0.346914 11.00000 -1.20000 AFIX 65 C26 1 0.261337 1.197842 0.291063 11.00000 0.10293 0.10292 = 0.10340 -0.00086 -0.02157 -0.00409 AFIX 43 H26 2 0.261915 1.230170 0.268384 11.00000 -1.20000 AFIX 65 C27 1 0.326594 1.149673 0.277909 11.00000 0.07848 0.07874 = 0.07927 -0.00108 -0.01599 -0.00282 AFIX 0 C28 1 0.390714 1.151409 0.231475 11.00000 0.09070 0.09044 = 0.09067 -0.00071 -0.01874 -0.00354 AFIX 66 C29 1 0.256438 0.666958 0.622615 11.00000 0.07263 0.07300 = 0.07467 -0.00079 -0.01360 -0.00279 C30 1 0.273065 0.654254 0.672107 11.00000 0.09859 0.09888 = 0.09938 -0.00220 -0.01923 -0.00372 C31 1 0.313836 0.696464 0.698375 11.00000 0.13092 0.13124 = 0.13205 -0.00171 -0.02611 -0.00512 AFIX 43 H31 2 0.324960 0.687964 0.731488 11.00000 -1.20000 AFIX 65 C32 1 0.337980 0.751379 0.675151 11.00000 0.11721 0.11764 = 0.11851 -0.00201 -0.02316 -0.00432 AFIX 43 H32 2 0.365258 0.779620 0.692726 11.00000 -1.20000 AFIX 65 C33 1 0.321353 0.764083 0.625659 11.00000 0.09591 0.09613 = 0.09758 -0.00159 -0.01860 -0.00339 AFIX 43 H33 2 0.337508 0.800825 0.610121 11.00000 -1.20000 AFIX 65 C34 1 0.280583 0.721873 0.599391 11.00000 0.09752 0.09817 = 0.09870 -0.00128 -0.01975 -0.00300 AFIX 0 C35 1 0.258231 0.739551 0.554230 11.00000 0.10658 0.10621 = 0.10646 -0.00144 -0.02080 -0.00433 C36 1 0.063930 0.423029 0.666731 11.00000 0.02578 0.05602 = 0.06676 -0.01637 -0.01935 0.00871 C37 1 0.056134 0.434581 0.615186 11.00000 0.03205 0.06806 = 0.07180 -0.01448 -0.00922 0.00405 C38 1 0.009971 0.395883 0.588923 11.00000 0.08520 0.08029 = 0.08372 0.00602 -0.03705 0.02107 AFIX 43 H38 2 0.004151 0.404683 0.554955 11.00000 -1.20000 AFIX 0 C39 1 -0.027644 0.344256 0.612558 11.00000 0.07713 0.09022 = 0.08119 -0.01114 -0.03896 0.00890 AFIX 43 H39 2 -0.056321 0.317650 0.594077 11.00000 -1.20000 AFIX 0 C40 1 -0.022741 0.332040 0.663701 11.00000 0.05985 0.05012 = 0.10107 -0.01451 -0.01435 0.01314 AFIX 43 H40 2 -0.049493 0.297790 0.680071 11.00000 -1.20000 AFIX 0 C41 1 0.022924 0.371764 0.690630 11.00000 0.04250 0.06675 = 0.07136 -0.01330 -0.00118 0.00138 C42 1 0.026100 0.357038 0.744704 11.00000 0.06948 0.08408 = 0.05937 -0.00635 -0.00843 0.00867 C1A 1 0.130842 0.601874 -0.094926 11.00000 0.07062 0.05464 = 0.05547 -0.00646 -0.01463 0.00440 C2A 1 0.057122 0.569570 -0.067402 11.00000 0.08476 0.07914 = 0.08225 -0.01600 0.00090 -0.01891 AFIX 43 H2A 2 0.034353 0.577559 -0.032397 11.00000 -1.20000 AFIX 0 C3A 1 0.015586 0.525212 -0.090477 11.00000 0.12366 0.07490 = 0.12606 0.00757 -0.06892 -0.04685 AFIX 43 H3A 2 -0.035057 0.503807 -0.071412 11.00000 -1.20000 AFIX 0 C4A 1 0.049599 0.513671 -0.140712 11.00000 0.13598 0.08579 = 0.15664 -0.02300 -0.09473 -0.01038 AFIX 43 H4A 2 0.020976 0.484952 -0.157102 11.00000 -1.20000 AFIX 0 C5A 1 0.125081 0.543435 -0.167663 11.00000 0.16678 0.08063 = 0.09265 -0.01733 -0.01898 -0.00901 AFIX 43 H5A 2 0.151082 0.532033 -0.201595 11.00000 -1.20000 AFIX 0 C6A 1 0.165599 0.590083 -0.147220 11.00000 0.12708 0.08958 = 0.07568 -0.00708 -0.01575 -0.01404 AFIX 43 H6A 2 0.213677 0.612479 -0.167382 11.00000 -1.20000 AFIX 0 C7A 1 0.102123 0.728814 -0.070986 11.00000 0.03659 0.06020 = 0.06063 0.01047 -0.00640 -0.00172 C8A 1 0.010981 0.723598 -0.081122 11.00000 0.04778 0.07365 = 0.09902 0.00242 -0.02503 -0.01123 AFIX 43 H8A 2 -0.011866 0.685921 -0.084649 11.00000 -1.20000 AFIX 0 C9A 1 -0.048529 0.774308 -0.086272 11.00000 0.06300 0.08858 = 0.10284 0.01235 -0.03558 -0.02924 AFIX 43 H9A 2 -0.109952 0.770500 -0.093745 11.00000 -1.20000 AFIX 0 C10A 1 -0.015256 0.828355 -0.080226 11.00000 0.05533 0.10108 = 0.10253 0.00141 -0.03580 0.01880 AFIX 43 H10A 2 -0.054282 0.862084 -0.083730 11.00000 -1.20000 AFIX 0 C11A 1 0.071962 0.834828 -0.069370 11.00000 0.09783 0.04204 = 0.11233 -0.01456 -0.03225 0.00124 AFIX 43 H11A 2 0.091936 0.872899 -0.064455 11.00000 -1.20000 AFIX 0 C12A 1 0.134623 0.785578 -0.065149 11.00000 0.05588 0.04741 = 0.14618 0.00021 -0.03665 -0.00619 AFIX 43 H12A 2 0.196428 0.790648 -0.058608 11.00000 -1.20000 AFIX 0 C13A 1 0.298726 0.680855 -0.096485 11.00000 0.05379 0.05031 = 0.09076 0.00753 -0.00186 0.00467 C14A 1 0.313716 0.713133 -0.143462 11.00000 0.05457 0.11813 = 0.14636 0.04172 -0.00558 -0.00182 AFIX 43 H14A 2 0.261358 0.723412 -0.159045 11.00000 -1.20000 AFIX 0 C15A 1 0.405821 0.729574 -0.166469 11.00000 0.07693 0.12441 = 0.22342 0.07135 0.01493 -0.00561 AFIX 43 H15A 2 0.414853 0.753042 -0.196441 11.00000 -1.20000 AFIX 0 C16A 1 0.480590 0.712496 -0.146564 11.00000 0.08898 0.08523 = 0.18329 0.04516 0.01569 -0.00689 AFIX 43 H16A 2 0.542586 0.722302 -0.163720 11.00000 -1.20000 AFIX 0 C17A 1 0.470200 0.680730 -0.101386 11.00000 0.06341 0.10781 = 0.21572 0.05065 -0.01931 0.01108 AFIX 43 H17A 2 0.524496 0.669112 -0.087847 11.00000 -1.20000 AFIX 0 C18A 1 0.377811 0.665761 -0.075600 11.00000 0.06058 0.08675 = 0.14892 0.04088 -0.00979 -0.00197 AFIX 43 H18A 2 0.369954 0.645387 -0.044007 11.00000 -1.20000 AFIX 0 C19A 1 0.174665 0.643692 0.000237 11.00000 0.05110 0.05558 = 0.04847 -0.00452 0.00338 0.00645 C20A 1 0.137145 0.681604 0.040322 11.00000 0.08669 0.08709 = 0.08140 0.00420 -0.02954 0.03613 AFIX 43 H20A 2 0.114748 0.719807 0.033168 11.00000 -1.20000 AFIX 0 C21A 1 0.132456 0.663390 0.091144 11.00000 0.13713 0.11119 = 0.08675 -0.01008 -0.01254 0.09586 AFIX 43 H21A 2 0.104837 0.689092 0.117891 11.00000 -1.20000 AFIX 0 C22A 1 0.167688 0.608244 0.102863 11.00000 0.07517 0.11266 = 0.05400 -0.01544 -0.00930 0.02903 AFIX 43 H22A 2 0.163480 0.596323 0.137277 11.00000 -1.20000 AFIX 0 C23A 1 0.207970 0.571884 0.064614 11.00000 0.06839 0.06023 = 0.07908 0.01759 -0.01918 0.00675 AFIX 43 H23A 2 0.233577 0.534783 0.072541 11.00000 -1.20000 AFIX 0 C24A 1 0.212573 0.587932 0.013669 11.00000 0.09462 0.04683 = 0.08018 -0.00635 -0.00137 0.01814 AFIX 43 H24A 2 0.241157 0.561589 -0.012381 11.00000 -1.20000 AFIX 0 C1B 1 0.664069 0.850947 -0.003959 11.00000 0.03908 0.06553 = 0.04871 0.00936 -0.00989 0.00616 C2B 1 0.643003 0.816687 -0.043474 11.00000 0.07330 0.08961 = 0.05206 -0.00779 -0.01789 0.00040 AFIX 43 H2B 2 0.608552 0.782104 -0.035692 11.00000 -1.20000 AFIX 0 C3B 1 0.673616 0.834486 -0.094058 11.00000 0.13037 0.12425 = 0.05594 0.00121 -0.01220 -0.01701 AFIX 43 H3B 2 0.659563 0.811715 -0.120609 11.00000 -1.20000 AFIX 0 C4B 1 0.724581 0.885272 -0.106150 11.00000 0.09165 0.11212 = 0.05282 0.02984 -0.00039 0.02283 AFIX 43 H5B 2 0.744904 0.896710 -0.140669 11.00000 -1.20000 AFIX 0 C5B 1 0.745266 0.918695 -0.067894 11.00000 0.07606 0.08693 = 0.08870 0.00718 -0.02350 0.01137 AFIX 43 H4X 2 0.779953 0.953120 -0.076153 11.00000 -1.20000 AFIX 0 C6B 1 0.715519 0.902197 -0.017202 11.00000 0.06801 0.07208 = 0.05852 0.00925 -0.01794 0.02195 AFIX 43 H6B 2 0.729943 0.925643 0.008832 11.00000 -1.20000 AFIX 0 C7B 1 0.578052 0.893511 0.097512 11.00000 0.04867 0.03805 = 0.06256 0.00166 -0.00549 0.00609 C8B 1 0.519497 0.932222 0.075359 11.00000 0.08035 0.06002 = 0.07570 -0.02004 -0.01177 0.03760 AFIX 43 H8B 2 0.513090 0.925973 0.041365 11.00000 -1.20000 AFIX 0 C9B 1 0.469822 0.980171 0.102056 11.00000 0.10214 0.07841 = 0.10982 -0.00170 -0.01997 0.01789 AFIX 43 H9B 2 0.429902 1.005510 0.086379 11.00000 -1.20000 AFIX 0 C10B 1 0.479918 0.989844 0.151278 11.00000 0.07391 0.07120 = 0.11558 -0.03097 0.00470 0.03422 AFIX 43 H10B 2 0.447730 1.022500 0.169273 11.00000 -1.20000 AFIX 0 C11B 1 0.536715 0.952239 0.174670 11.00000 0.10253 0.09117 = 0.05720 -0.01341 0.01555 0.00746 AFIX 43 H11B 2 0.542277 0.958822 0.208746 11.00000 -1.20000 AFIX 0 C12B 1 0.586840 0.903613 0.147514 11.00000 0.06679 0.07253 = 0.07364 -0.00405 0.00149 0.02527 AFIX 43 H12B 2 0.626154 0.878143 0.163459 11.00000 -1.20000 AFIX 0 C13B 1 0.738608 0.801642 0.083449 11.00000 0.04692 0.04171 = 0.05179 -0.00331 -0.00634 0.01222 C14B 1 0.831095 0.815116 0.057886 11.00000 0.05218 0.08441 = 0.07737 0.02128 -0.00111 0.00306 AFIX 43 H14B 2 0.840018 0.840998 0.029447 11.00000 -1.20000 AFIX 0 C15B 1 0.910638 0.789444 0.075268 11.00000 0.04354 0.11553 = 0.09926 0.00107 -0.00637 0.01721 AFIX 43 H15B 2 0.973296 0.796663 0.057383 11.00000 -1.20000 AFIX 0 C16B 1 0.897401 0.753902 0.118190 11.00000 0.07482 0.10336 = 0.07056 0.01474 -0.03484 0.02005 AFIX 43 H16B 2 0.951441 0.738275 0.130058 11.00000 -1.20000 AFIX 0 C17B 1 0.806733 0.740579 0.144307 11.00000 0.06993 0.07024 = 0.09196 0.00686 -0.01470 0.00186 AFIX 43 H17B 2 0.799001 0.715204 0.173078 11.00000 -1.20000 AFIX 0 C18B 1 0.727511 0.764840 0.127810 11.00000 0.03974 0.06064 = 0.09222 -0.00329 -0.00931 0.01290 AFIX 43 H18B 2 0.665441 0.756933 0.146135 11.00000 -1.20000 AFIX 0 C19B 1 0.546626 0.772811 0.073652 11.00000 0.03876 0.06534 = 0.04503 0.01213 -0.01231 0.00461 C20B 1 0.573535 0.715273 0.055288 11.00000 0.04142 0.06267 = 0.10485 0.00576 0.00514 0.00799 AFIX 43 H20B 2 0.636460 0.707352 0.036894 11.00000 -1.20000 AFIX 0 C21B 1 0.510184 0.671111 0.063700 11.00000 0.04864 0.06295 = 0.10895 -0.01545 0.00125 -0.00194 AFIX 43 H21B 2 0.530734 0.632786 0.052490 11.00000 -1.20000 AFIX 0 C22B 1 0.414345 0.682139 0.088965 11.00000 0.05765 0.06313 = 0.09590 0.01242 -0.02108 0.00029 AFIX 43 H22B 2 0.369893 0.651983 0.093861 11.00000 -1.20000 AFIX 0 C23B 1 0.387215 0.738606 0.106435 11.00000 0.05773 0.07582 = 0.10587 0.02045 0.00741 -0.00259 AFIX 43 H23B 2 0.323917 0.746657 0.124256 11.00000 -1.20000 AFIX 0 C24B 1 0.451139 0.782843 0.098151 11.00000 0.05364 0.06283 = 0.09525 0.02476 0.00139 0.02969 AFIX 43 H24B 2 0.430042 0.821108 0.109307 11.00000 -1.20000 AFIX 0 C1C 1 0.300058 0.682960 0.257540 11.00000 0.03711 0.05287 = 0.07313 0.01544 -0.01377 0.01272 C2C 1 0.218655 0.690489 0.235063 11.00000 0.06736 0.05599 = 0.06957 0.00689 -0.01643 0.02530 AFIX 43 H2C 2 0.185070 0.657824 0.227959 11.00000 -1.20000 AFIX 0 C3C 1 0.189086 0.747660 0.223596 11.00000 0.08007 0.11571 = 0.05966 0.00590 -0.01904 0.01582 AFIX 43 H3C 2 0.135922 0.753394 0.207665 11.00000 -1.20000 AFIX 0 C4C 1 0.235600 0.795332 0.234990 11.00000 0.11513 0.09295 = 0.07232 0.00108 -0.01077 0.06009 AFIX 43 H4C 2 0.212266 0.833523 0.228502 11.00000 -1.20000 AFIX 0 C5C 1 0.316446 0.788112 0.255915 11.00000 0.12492 0.05317 = 0.16428 0.03403 -0.08637 -0.01362 AFIX 43 H5C 2 0.350058 0.821107 0.262240 11.00000 -1.20000 AFIX 0 C6C 1 0.348118 0.731737 0.267642 11.00000 0.12414 0.07191 = 0.13825 0.04306 -0.08799 -0.01448 AFIX 43 H6C 2 0.402652 0.726706 0.282564 11.00000 -1.20000 AFIX 0 C7C 1 0.470646 0.604063 0.256688 11.00000 0.05476 0.05255 = 0.08792 0.00105 -0.03078 0.01131 C8C 1 0.516550 0.627436 0.209048 11.00000 0.06126 0.08204 = 0.09967 0.02509 -0.01622 0.00450 AFIX 43 H8C 2 0.480300 0.647430 0.187609 11.00000 -1.20000 AFIX 0 C9C 1 0.617124 0.620598 0.193827 11.00000 0.06134 0.11216 = 0.12267 0.01692 -0.00317 -0.00139 AFIX 43 H9C 2 0.649025 0.635819 0.162124 11.00000 -1.20000 AFIX 0 C10C 1 0.667549 0.591445 0.225949 11.00000 0.07490 0.11593 = 0.14376 -0.03284 -0.04237 -0.00566 AFIX 43 H10C 2 0.734724 0.586875 0.215491 11.00000 -1.20000 AFIX 0 C11C 1 0.625251 0.568545 0.272596 11.00000 0.08115 0.08183 = 0.14966 -0.01735 -0.06929 0.02820 AFIX 43 H11C 2 0.662661 0.549009 0.293702 11.00000 -1.20000 AFIX 0 C12C 1 0.523472 0.574877 0.288552 11.00000 0.07110 0.09644 = 0.10340 -0.00217 -0.04785 0.01571 AFIX 43 H12C 2 0.492582 0.559400 0.320362 11.00000 -1.20000 AFIX 0 C13C 1 0.287437 0.555853 0.242747 11.00000 0.04429 0.04511 = 0.07058 0.01031 -0.02192 0.00224 C14C 1 0.337498 0.527707 0.198006 11.00000 0.06832 0.07467 = 0.06993 -0.01082 -0.01807 0.01439 AFIX 43 H14C 2 0.401835 0.536430 0.184449 11.00000 -1.20000 AFIX 0 C15C 1 0.290678 0.486168 0.173425 11.00000 0.10989 0.08783 = 0.04252 -0.00763 -0.02719 0.00427 AFIX 43 H15C 2 0.322886 0.469388 0.142301 11.00000 -1.20000 AFIX 0 C16C 1 0.199910 0.470302 0.194254 11.00000 0.11413 0.06787 = 0.09670 -0.00120 -0.05461 -0.00468 AFIX 43 H16C 2 0.171376 0.440770 0.178736 11.00000 -1.20000 AFIX 0 C17C 1 0.147906 0.498076 0.239329 11.00000 0.07146 0.07713 = 0.13248 -0.00732 -0.02662 0.00220 AFIX 43 H17C 2 0.084293 0.488309 0.253495 11.00000 -1.20000 AFIX 0 C18C 1 0.193062 0.539379 0.261470 11.00000 0.08448 0.06168 = 0.08956 -0.01652 -0.03465 0.00837 AFIX 43 H18C 2 0.158469 0.557950 0.291233 11.00000 -1.20000 AFIX 0 C19C 1 0.302706 0.597671 0.343116 11.00000 0.05539 0.06800 = 0.07362 0.00969 -0.03585 -0.01015 C20C 1 0.292766 0.540054 0.363116 11.00000 0.19837 0.06939 = 0.09223 -0.00139 -0.06577 -0.02197 AFIX 43 H20C 2 0.303407 0.507630 0.340909 11.00000 -1.20000 AFIX 0 C21C 1 0.266636 0.531015 0.416897 11.00000 0.27015 0.14947 = 0.08779 0.04968 -0.08697 -0.06954 AFIX 43 H21C 2 0.263733 0.492758 0.431162 11.00000 -1.20000 AFIX 0 C22C 1 0.245861 0.579275 0.447319 11.00000 0.13108 0.20885 = 0.06486 -0.00080 -0.03684 -0.06694 AFIX 43 H22C 2 0.222655 0.572716 0.482570 11.00000 -1.20000 AFIX 0 C23C 1 0.255549 0.634329 0.431503 11.00000 0.11810 0.13599 = 0.07866 -0.01062 -0.04187 -0.02107 AFIX 43 H23C 2 0.244593 0.665544 0.454981 11.00000 -1.20000 AFIX 0 C24C 1 0.282986 0.645189 0.378036 11.00000 0.06960 0.08679 = 0.08658 0.00048 -0.03142 0.00017 AFIX 43 H24C 2 0.288167 0.684209 0.365595 11.00000 -1.20000 AFIX 0 C1D 1 0.596754 0.748180 0.576159 11.00000 0.03695 0.05386 = 0.10312 -0.00978 -0.02076 0.00451 C2D 1 0.572659 0.783294 0.620343 11.00000 0.05003 0.06270 = 0.11736 -0.01745 -0.02062 0.02471 AFIX 43 H2D 2 0.578122 0.767446 0.652609 11.00000 -1.20000 AFIX 0 C3D 1 0.541050 0.840982 0.615979 11.00000 0.06256 0.05903 = 0.16787 -0.04603 -0.05072 0.01540 AFIX 43 H3D 2 0.523271 0.864384 0.645435 11.00000 -1.20000 AFIX 0 C4D 1 0.535497 0.864318 0.568641 11.00000 0.10586 0.05141 = 0.17524 0.01030 -0.06196 -0.00877 AFIX 43 H4D 2 0.516102 0.904149 0.565742 11.00000 -1.20000 AFIX 0 C5D 1 0.557819 0.830365 0.525643 11.00000 0.14750 0.05704 = 0.12110 0.01160 -0.03918 0.00131 AFIX 43 H5D 2 0.554832 0.847296 0.493425 11.00000 -1.20000 AFIX 0 C6D 1 0.584541 0.771838 0.528975 11.00000 0.10945 0.07105 = 0.08036 0.01189 -0.01901 0.01941 AFIX 43 H6D 2 0.594521 0.747914 0.499741 11.00000 -1.20000 AFIX 0 C7D 1 0.778089 0.678088 0.564539 11.00000 0.04855 0.05653 = 0.09067 -0.01808 -0.02642 0.00702 C8D 1 0.820778 0.727566 0.541050 11.00000 0.05675 0.09147 = 0.10109 0.01982 -0.02504 -0.00560 AFIX 43 H8D 2 0.783470 0.759849 0.532180 11.00000 -1.20000 AFIX 0 C9D 1 0.922961 0.728353 0.530618 11.00000 0.05870 0.13201 = 0.12877 -0.01545 -0.03141 -0.03107 AFIX 43 H9D 2 0.953648 0.761693 0.514669 11.00000 -1.20000 AFIX 0 C10D 1 0.976873 0.681720 0.543332 11.00000 0.05016 0.16271 = 0.14631 -0.07174 -0.04593 0.03301 AFIX 43 H10D 2 1.044209 0.684072 0.536268 11.00000 -1.20000 AFIX 0 C11D 1 0.936896 0.630773 0.566286 11.00000 0.09502 0.08916 = 0.24131 -0.04771 -0.09019 0.03859 AFIX 43 H11D 2 0.974645 0.598372 0.574533 11.00000 -1.20000 AFIX 0 C12D 1 0.836745 0.631067 0.576243 11.00000 0.05710 0.10973 = 0.17869 -0.01503 -0.05949 0.02532 AFIX 43 H12D 2 0.806716 0.597371 0.591873 11.00000 -1.20000 AFIX 0 C13D 1 0.606814 0.628813 0.534039 11.00000 0.04245 0.04432 = 0.10529 0.01314 -0.02843 -0.00288 C14D 1 0.668291 0.590338 0.499374 11.00000 0.05274 0.04601 = 0.10829 0.02589 -0.00354 0.01556 AFIX 43 H14D 2 0.734609 0.586753 0.499094 11.00000 -1.20000 AFIX 0 C15D 1 0.626292 0.557266 0.464957 11.00000 0.13141 0.03629 = 0.09212 -0.00386 -0.05159 -0.01531 AFIX 43 H15D 2 0.664955 0.531161 0.441725 11.00000 -1.20000 AFIX 0 C16D 1 0.528891 0.563660 0.465831 11.00000 0.07177 0.09888 = 0.14045 0.01473 -0.06853 -0.01147 AFIX 43 H16D 2 0.502213 0.543187 0.441973 11.00000 -1.20000 AFIX 0 C17D 1 0.470764 0.599203 0.500753 11.00000 0.04837 0.07339 = 0.14204 0.00509 -0.02879 0.00290 AFIX 43 H17D 2 0.404119 0.600620 0.501806 11.00000 -1.20000 AFIX 0 C18D 1 0.506688 0.633362 0.534799 11.00000 0.05947 0.06400 = 0.12981 -0.02104 -0.04851 0.01174 AFIX 43 H18D 2 0.465786 0.658787 0.557705 11.00000 -1.20000 AFIX 0 C19D 1 0.615484 0.643474 0.643273 11.00000 0.06713 0.05349 = 0.10501 0.00700 -0.02102 -0.00966 C20D 1 0.532503 0.612706 0.658525 11.00000 0.10540 0.07154 = 0.10676 0.00295 -0.02128 0.01675 AFIX 43 H20D 2 0.493202 0.605572 0.634902 11.00000 -1.20000 AFIX 0 C21D 1 0.506008 0.591353 0.711213 11.00000 0.08227 0.07554 = 0.14133 0.01141 0.00711 -0.00806 AFIX 43 H21D 2 0.449856 0.570047 0.721428 11.00000 -1.20000 AFIX 0 C22D 1 0.563535 0.602304 0.746820 11.00000 0.16693 0.12633 = 0.11931 0.02210 -0.04150 0.02080 AFIX 43 H22D 2 0.546390 0.590222 0.781356 11.00000 -1.20000 AFIX 0 C23D 1 0.646448 0.631680 0.728554 11.00000 0.13006 0.13249 = 0.12503 0.02153 -0.05525 -0.00613 AFIX 43 H23D 2 0.687836 0.637124 0.751462 11.00000 -1.20000 AFIX 0 C24D 1 0.673502 0.653556 0.679895 11.00000 0.15422 0.11720 = 0.09193 0.04670 -0.07314 -0.01464 AFIX 43 H24D 2 0.729717 0.675004 0.670674 11.00000 -1.20000 AFIX 0 C1E 1 0.193516 0.212889 0.649374 11.00000 0.03393 0.05845 = 0.04499 0.00449 -0.01410 0.00477 C2E 1 0.222125 0.237415 0.600428 11.00000 0.07916 0.07242 = 0.09048 0.00414 0.00343 -0.01580 AFIX 43 H2E 2 0.223278 0.214054 0.571459 11.00000 -1.20000 AFIX 0 C3E 1 0.248794 0.295336 0.593673 11.00000 0.06748 0.08239 = 0.08031 0.00182 -0.00340 -0.01226 AFIX 43 H3E 2 0.261634 0.311889 0.560434 11.00000 -1.20000 AFIX 0 C4E 1 0.256811 0.329132 0.634997 11.00000 0.03677 0.04990 = 0.12571 -0.00665 0.00781 0.00093 AFIX 43 H4E 2 0.276501 0.368202 0.629956 11.00000 -1.20000 AFIX 0 C5E 1 0.235530 0.304970 0.684252 11.00000 0.07350 0.08407 = 0.07416 -0.02377 0.01362 -0.00610 AFIX 43 H5E 2 0.242382 0.326900 0.712870 11.00000 -1.20000 AFIX 0 C6E 1 0.203476 0.246884 0.690262 11.00000 0.06133 0.04590 = 0.07922 -0.00235 -0.00253 -0.00316 AFIX 43 H6E 2 0.188243 0.230633 0.723557 11.00000 -1.20000 AFIX 0 C7E 1 0.137812 0.119469 0.723362 11.00000 0.06996 0.04247 = 0.05944 0.01501 -0.02051 0.00165 C8E 1 0.063851 0.143713 0.762686 11.00000 0.05645 0.07029 = 0.06797 0.00333 0.00145 0.01014 AFIX 43 H8E 2 0.016392 0.169827 0.753909 11.00000 -1.20000 AFIX 0 C9E 1 0.061313 0.128888 0.814477 11.00000 0.09719 0.10343 = 0.04352 -0.00535 0.01100 -0.05819 AFIX 43 H9E 2 0.012658 0.144725 0.840582 11.00000 -1.20000 AFIX 0 C10E 1 0.130950 0.091099 0.825842 11.00000 0.15295 0.09783 = 0.08924 0.04783 -0.05666 -0.03412 AFIX 43 H10E 2 0.129317 0.081738 0.860600 11.00000 -1.20000 AFIX 0 C11E 1 0.201433 0.066415 0.790981 11.00000 0.07712 0.10337 = 0.11345 0.01606 -0.02426 0.00259 AFIX 43 H11E 2 0.246557 0.039642 0.801184 11.00000 -1.20000 AFIX 0 C12E 1 0.207743 0.080915 0.738323 11.00000 0.08964 0.04686 = 0.06299 0.00743 -0.01597 -0.00931 AFIX 43 H12E 2 0.258469 0.064831 0.713483 11.00000 -1.20000 AFIX 0 C13E 1 0.224042 0.092312 0.614049 11.00000 0.03535 0.05844 = 0.05988 -0.00234 -0.02264 -0.01319 C14E 1 0.324442 0.087912 0.614330 11.00000 0.06507 0.08165 = 0.07696 -0.03021 -0.03019 -0.01571 AFIX 43 H14E 2 0.351056 0.111051 0.636508 11.00000 -1.20000 AFIX 0 C15E 1 0.381842 0.048499 0.580936 11.00000 0.04265 0.08949 = 0.11244 -0.01444 -0.02901 0.01169 AFIX 43 H15E 2 0.446923 0.043030 0.583108 11.00000 -1.20000 AFIX 0 C16E 1 0.348796 0.017483 0.545339 11.00000 0.04661 0.08412 = 0.08948 -0.02009 0.00713 0.01386 AFIX 43 H16E 2 0.390893 -0.006650 0.521797 11.00000 -1.20000 AFIX 0 C71E 1 0.251595 0.022261 0.544553 11.00000 0.08238 0.11732 = 0.08506 -0.05308 -0.00315 0.00170 AFIX 43 H71E 2 0.227177 0.000574 0.520567 11.00000 -1.20000 AFIX 0 C18E 1 0.189164 0.058984 0.579028 11.00000 0.06250 0.09611 = 0.04662 -0.02144 -0.01400 0.00097 AFIX 43 H18E 2 0.123109 0.061087 0.578454 11.00000 -1.20000 AFIX 0 C19E 1 0.027214 0.143828 0.644090 11.00000 0.02834 0.04340 = 0.09566 -0.00705 -0.02261 -0.00108 C20E 1 -0.034533 0.098978 0.664528 11.00000 0.04812 0.07530 = 0.10825 0.00443 -0.01367 0.00300 AFIX 43 H20E 2 -0.013584 0.069788 0.685797 11.00000 -1.20000 AFIX 0 C21E 1 -0.125010 0.096978 0.654006 11.00000 0.07199 0.09408 = 0.13039 0.00736 -0.02906 -0.01905 AFIX 43 H21E 2 -0.166337 0.067385 0.669014 11.00000 -1.20000 AFIX 0 C22E 1 -0.155577 0.138404 0.621366 11.00000 0.07928 0.08384 = 0.19283 -0.01617 -0.07501 -0.00930 AFIX 43 H22E 2 -0.217005 0.136566 0.613438 11.00000 -1.20000 AFIX 0 C23E 1 -0.095901 0.181931 0.600779 11.00000 0.08164 0.07383 = 0.17260 0.01199 -0.07924 -0.00873 AFIX 43 H23E 2 -0.116654 0.210248 0.578692 11.00000 -1.20000 AFIX 0 C24E 1 -0.003484 0.185036 0.612176 11.00000 0.06682 0.07106 = 0.09883 0.02158 -0.03747 -0.01000 AFIX 43 H24E 2 0.036943 0.215364 0.597869 11.00000 -1.20000 AFIX 0 C1F 1 0.054875 0.900366 0.642921 11.00000 0.04902 0.07077 = 0.08218 -0.02057 -0.01045 0.01690 C2F 1 0.119264 0.868119 0.606042 11.00000 0.24102 0.15959 = 0.09338 -0.01196 -0.05742 0.12552 AFIX 43 H2F 2 0.158892 0.838291 0.616904 11.00000 -1.20000 AFIX 0 C3F 1 0.126940 0.878835 0.552682 11.00000 0.26708 0.17171 = 0.08379 -0.01933 -0.04105 0.10082 AFIX 43 H3F 2 0.173524 0.858065 0.528621 11.00000 -1.20000 AFIX 0 C4F 1 0.067689 0.918416 0.537305 11.00000 0.12993 0.14829 = 0.10394 0.00493 -0.02851 0.01767 AFIX 43 H4F 2 0.070421 0.924236 0.501941 11.00000 -1.20000 AFIX 0 C5F 1 0.002513 0.951112 0.571550 11.00000 0.07366 0.14240 = 0.09047 0.04908 -0.01477 0.00835 AFIX 43 H5F 2 -0.038282 0.979818 0.560105 11.00000 -1.20000 AFIX 0 C6F 1 -0.002277 0.940745 0.625027 11.00000 0.06532 0.07047 = 0.10084 0.00798 -0.00961 0.00380 AFIX 43 H6F 2 -0.047252 0.963077 0.648698 11.00000 -1.20000 AFIX 0 C7F 1 0.012538 0.810444 0.728340 11.00000 0.07958 0.08045 = 0.08083 -0.00132 -0.01615 -0.00345 C8F 1 -0.058417 0.797307 0.769687 11.00000 0.10254 0.10133 = 0.10090 -0.00105 -0.02039 -0.00444 AFIX 43 H8F 2 -0.091079 0.828819 0.789157 11.00000 -1.20000 AFIX 0 C9F 1 -0.086040 0.738533 0.785161 11.00000 0.12977 0.12933 = 0.12905 -0.00123 -0.02569 -0.00599 AFIX 43 H9F 2 -0.135139 0.730684 0.813622 11.00000 -1.20000 AFIX 0 C10F 1 -0.035998 0.695368 0.755647 11.00000 0.12908 0.12851 = 0.12919 -0.00043 -0.02585 -0.00477 AFIX 43 H10F 2 -0.043141 0.656516 0.768306 11.00000 -1.20000 AFIX 0 C11F 1 0.023125 0.702832 0.709806 11.00000 0.17415 0.17389 = 0.17489 -0.00170 -0.03451 -0.00636 AFIX 43 H11F 2 0.046136 0.670489 0.688629 11.00000 -1.20000 AFIX 0 C12F 1 0.050824 0.763630 0.693753 11.00000 0.13817 0.13846 = 0.13961 -0.00150 -0.02689 -0.00554 AFIX 43 H12F 2 0.091922 0.771212 0.662106 11.00000 -1.20000 AFIX 0 C13F 1 0.165746 0.890808 0.727015 11.00000 0.05430 0.05532 = 0.09308 -0.00337 -0.02845 -0.00887 C14F 1 0.185945 0.866094 0.772405 11.00000 0.07363 0.10411 = 0.12841 0.03578 -0.04312 -0.00031 AFIX 43 H14F 2 0.139940 0.843321 0.793721 11.00000 -1.20000 AFIX 0 C15F 1 0.272878 0.874880 0.786142 11.00000 0.08793 0.11284 = 0.14267 0.02376 -0.07038 -0.00440 AFIX 43 H15F 2 0.285867 0.857937 0.816692 11.00000 -1.20000 AFIX 0 C16F 1 0.340697 0.908263 0.755445 11.00000 0.06540 0.09042 = 0.15105 -0.00149 -0.02453 -0.00510 AFIX 43 H16F 2 0.399018 0.914687 0.765721 11.00000 -1.20000 AFIX 0 C17F 1 0.324545 0.932450 0.709867 11.00000 0.04777 0.07905 = 0.14977 0.00091 -0.01055 -0.00602 AFIX 43 H17F 2 0.372875 0.953559 0.688514 11.00000 -1.20000 AFIX 0 C18F 1 0.236493 0.925629 0.695386 11.00000 0.04483 0.07360 = 0.12319 0.00676 -0.01016 -0.00094 AFIX 43 H18F 2 0.223841 0.943710 0.665200 11.00000 -1.20000 AFIX 0 C19F 1 -0.036448 0.935244 0.749761 11.00000 0.05053 0.04950 = 0.05475 -0.00802 -0.00831 -0.02999 C20F 1 -0.010261 0.967309 0.788765 11.00000 0.05822 0.08430 = 0.09603 -0.00826 -0.03267 -0.01348 AFIX 43 H20F 2 0.052750 0.963284 0.794768 11.00000 -1.20000 AFIX 0 C21F 1 -0.076474 1.004708 0.818352 11.00000 0.07699 0.11036 = 0.08830 -0.03085 -0.00668 -0.03361 AFIX 43 H21F 2 -0.059085 1.025489 0.845150 11.00000 -1.20000 AFIX 0 C22F 1 -0.168449 1.011982 0.808984 11.00000 0.07971 0.06346 = 0.08114 0.00066 0.01701 -0.00579 AFIX 43 H22F 2 -0.212621 1.038521 0.828934 11.00000 -1.20000 AFIX 0 C23F 1 -0.196646 0.980637 0.770491 11.00000 0.05555 0.12221 = 0.09209 -0.01226 -0.00975 0.00209 AFIX 43 H23F 2 -0.259169 0.985911 0.763991 11.00000 -1.20000 AFIX 0 C24F 1 -0.129954 0.941078 0.741641 11.00000 0.04966 0.08930 = 0.06062 -0.00305 -0.01525 -0.01287 AFIX 43 H24F 2 -0.148637 0.918183 0.716471 11.00000 -1.20000 AFIX 0 HKLF 4 REM 345_a.res in P-1 REM R1 = 0.0945 for 7502 Fo > 4sig(Fo) and 0.3416 for all 29898 data REM 1897 parameters refined using 127 restraints END WGHT 0.0443 0.0000 REM Highest difference peak 0.520, deepest hole -0.384, 1-sigma level 0.064 Q1 1 0.3405 0.7617 0.6489 11.00000 0.05 0.52 Q2 1 0.2439 0.6667 0.5937 11.00000 0.05 0.48 Q3 1 0.2218 1.2036 0.3117 11.00000 0.05 0.43 Q4 1 0.3267 0.7734 0.5929 11.00000 0.05 0.39 Q5 1 0.2638 0.6646 0.6496 11.00000 0.05 0.38 Q6 1 0.0667 0.7625 0.7249 11.00000 0.05 0.38 Q7 1 0.0038 0.7863 0.7641 11.00000 0.05 0.35 Q8 1 0.1032 0.9924 -0.0057 11.00000 0.05 0.35 Q9 1 0.0638 0.7020 0.7510 11.00000 0.05 0.34 Q10 1 0.3379 0.9255 0.3779 11.00000 0.05 0.33 Q11 1 0.1110 1.0001 -0.0179 11.00000 0.05 0.32 Q12 1 0.0468 0.7077 0.7416 11.00000 0.05 0.31 Q13 1 0.4806 0.4563 0.0165 11.00000 0.05 0.31 Q14 1 0.2460 0.7079 0.7733 11.00000 0.05 0.31 Q15 1 0.2406 0.9245 0.4443 11.00000 0.05 0.31 Q16 1 0.0371 0.7695 0.6681 11.00000 0.05 0.30 Q17 1 0.2565 0.7047 0.7584 11.00000 0.05 0.30 Q18 1 0.5046 0.9329 0.0100 11.00000 0.05 0.29 Q19 1 -0.0466 0.7210 0.7826 11.00000 0.05 0.29 Q20 1 0.1676 0.5443 0.6016 11.00000 0.05 0.28 ; _shelx_res_checksum 3035 _shelx_hkl_file ; -2 0 0 369.86 16.40 2 0 0 341.67 15.90 -3 0 0 15.70 11.50 3 0 0 9.30 11.40 -4 0 0 110.09 14.10 4 0 0 113.59 13.60 -5 0 0 833.42 34.60 5 0 0 871.21 34.60 -6 0 0 803.52 34.00 -6 0 0 751.32 29.10 6 0 0 758.92 33.90 -7 0 0 138.89 16.60 -7 0 0 161.48 18.70 7 0 0 131.69 18.90 -8 0 0 41.70 16.10 -8 0 0 54.19 11.80 -8 0 0 97.79 18.10 8 0 0 62.49 18.60 -9 0 0 80.09 12.30 -9 0 0 63.59 18.70 -9 0 0 83.69 20.60 9 0 0 63.79 19.80 -10 0 0 46.90 18.50 -10 0 0 23.90 18.30 -11 0 0 -15.50 18.70 -11 0 0 8.60 19.10 -12 0 0 37.60 23.50 -12 0 0 31.50 20.10 -13 0 0 -17.90 21.30 -13 0 0 -11.30 21.50 -14 0 0 -14.20 21.50 -14 0 0 -8.80 24.10 -15 0 0 3.10 22.30 -15 0 0 -21.10 24.10 -16 0 0 36.50 27.60 -16 0 0 17.30 24.30 -17 0 0 -23.70 27.10 -17 0 0 -25.50 26.80 -17 1 0 -8.10 23.40 -17 1 0 3.90 26.10 -16 1 0 16.40 24.30 -16 1 0 -39.80 24.40 -15 1 0 10.30 26.00 -15 1 0 33.70 23.30 -14 1 0 14.50 24.10 -14 1 0 1.90 22.10 -13 1 0 8.00 22.50 -13 1 0 11.20 20.30 -12 1 0 0.40 19.80 -12 1 0 27.30 21.20 -11 1 0 21.20 18.40 -11 1 0 14.10 19.40 -10 1 0 52.39 19.00 -10 1 0 77.19 14.10 -10 1 0 80.29 21.60 9 -1 0 87.59 18.80 -9 1 0 60.99 13.90 -9 1 0 17.20 16.20 -9 1 0 60.09 17.50 8 -1 0 51.79 17.60 -8 1 0 50.49 15.80 -8 1 0 31.90 13.20 -8 1 0 30.90 17.50 7 -1 0 120.79 19.10 -7 1 0 113.29 18.90 -7 1 0 108.69 16.70 6 -1 0 -13.30 14.60 -6 1 0 -14.80 13.60 -6 1 0 6.10 13.70 5 -1 0 502.75 25.50 -5 1 0 505.95 25.60 -5 1 0 506.85 26.50 4 -1 0 341.87 20.60 -4 1 0 346.17 21.40 -4 1 0 334.87 21.00 3 -1 0 1783.72 55.99 -3 1 0 1790.32 56.59 -3 1 0 1782.32 55.89 2 -1 0 4.50 7.50 2 -1 0 2.90 6.70 -2 1 0 6.40 7.30 -2 1 0 3.80 7.80 -1 1 0 20.40 3.70 -1 1 0 41.30 5.80 -2 -1 0 1475.35 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-15 -2 0 5.30 22.50 -15 -2 0 3.40 21.70 -16 -2 0 -13.50 24.70 -16 -2 0 44.20 26.20 -17 -2 0 -5.50 28.00 -17 -2 0 1.20 26.50 -17 3 0 -3.40 24.80 -17 3 0 -2.70 23.60 -16 3 0 25.90 23.00 -16 3 0 -9.10 22.50 -15 3 0 7.60 22.40 -15 3 0 -29.40 21.00 -14 3 0 -1.00 21.00 -14 3 0 -35.40 20.80 -13 3 0 38.20 20.10 -13 3 0 45.60 16.80 -13 3 0 29.60 23.80 -12 3 0 46.90 19.80 -12 3 0 41.10 17.40 -12 3 0 -1.80 22.30 -11 3 0 84.29 18.60 -11 3 0 66.29 22.40 -11 3 0 107.49 18.70 -10 3 0 72.39 17.80 -10 3 0 109.09 18.10 -10 3 0 99.49 20.60 9 -3 0 25.90 18.20 -9 3 0 17.40 15.30 -9 3 0 -10.80 17.10 8 -3 0 422.26 27.40 -8 3 0 415.26 25.50 -8 3 0 423.36 28.60 7 -3 0 315.07 23.30 -7 3 0 315.67 25.30 -7 3 0 315.27 22.80 6 -3 0 87.29 15.20 -6 3 0 91.19 17.90 -6 3 0 124.09 14.80 5 -3 0 186.08 16.70 -5 3 0 171.68 16.40 -5 3 0 184.18 17.20 4 -3 0 1040.30 35.90 4 -3 0 1036.10 37.40 -4 3 0 1019.40 37.50 -4 3 0 1019.50 35.00 3 -3 0 823.72 30.50 3 -3 0 806.82 28.50 -3 3 0 816.32 27.80 -3 3 0 845.02 30.40 2 -3 0 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21.40 -4 -23 0 -10.60 22.50 -5 -23 0 9.50 23.30 -5 -23 0 28.00 24.80 -6 -23 0 72.29 24.60 -6 -23 0 8.80 24.10 -7 -23 0 2.50 25.10 -7 -23 0 11.10 24.40 -8 -23 0 10.40 25.90 -8 -23 0 -3.60 23.70 -9 -23 0 -56.59 27.00 -9 -23 0 -4.90 22.70 -10 -23 0 5.00 29.60 -10 -23 0 -2.10 24.20 -11 -23 0 2.40 29.70 9 -24 0 -26.80 29.30 -9 24 0 16.90 20.90 8 -24 0 44.90 27.60 -8 24 0 23.40 22.50 7 -24 0 7.30 25.10 -7 24 0 46.60 23.40 6 -24 0 -15.80 25.20 -6 24 0 -5.80 20.30 5 -24 0 -17.50 24.90 -5 24 0 -15.60 20.40 4 -24 0 -1.10 25.80 -4 24 0 16.30 19.90 3 -24 0 41.20 26.60 -3 24 0 -47.30 16.60 2 -24 0 21.70 25.40 1 -24 0 -14.20 24.00 0 -24 0 -8.40 22.80 -1 -24 0 2.50 23.70 -1 -24 0 38.30 19.70 -2 -24 0 13.10 20.50 -2 -24 0 10.20 24.90 -3 -24 0 61.89 21.60 -3 -24 0 -0.80 24.30 -4 -24 0 37.20 23.60 -4 -24 0 12.50 24.20 -5 -24 0 13.70 24.20 -5 -24 0 -24.70 24.70 -6 -24 0 21.90 24.90 -6 -24 0 -5.40 25.10 -7 -24 0 -22.10 25.10 -7 -24 0 0.40 23.40 -8 -24 0 19.10 27.90 -8 -24 0 35.50 25.90 -9 -24 0 63.99 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21.60 -3 -26 0 -11.10 25.50 -4 -26 0 31.60 27.00 -4 -26 0 -5.60 23.50 -5 -26 0 -5.70 24.10 -5 -26 0 -20.50 24.90 -6 -26 0 30.30 26.70 -6 -26 0 35.00 26.40 -7 -26 0 -7.10 25.40 -7 -26 0 26.20 26.80 -8 -26 0 18.60 29.60 5 -27 0 -6.30 27.00 -5 27 0 -2.20 21.20 4 -27 0 23.50 29.40 3 -27 0 26.20 28.20 2 -27 0 36.80 29.20 1 -27 0 2.80 26.80 0 -27 0 10.90 26.50 -1 -27 0 -25.10 24.30 -2 -27 0 -28.20 19.60 -2 -27 0 25.20 27.60 -3 -27 0 42.70 28.60 -3 -27 0 5.60 21.90 -4 -27 0 -0.10 27.10 -4 -27 0 -19.50 21.40 -5 -27 0 4.70 27.10 -5 -27 0 12.50 24.40 -6 -27 0 -16.00 25.00 3 -28 0 -22.90 27.90 2 -28 0 -8.70 27.20 1 -28 0 -68.69 26.60 0 -28 0 41.50 27.50 -1 -28 0 -34.90 25.20 -2 -28 0 10.50 20.80 -2 -28 0 31.40 26.50 -3 -28 0 -31.80 26.10 -3 -28 0 -1.10 21.90 -4 -28 0 15.70 23.40 -4 -28 0 43.00 45.00 -4 -28 1 -6.80 22.70 -4 -28 1 30.30 35.20 -3 -28 1 -14.90 25.30 -3 -28 1 -10.60 21.30 -2 -28 1 -5.30 19.70 -2 -28 1 -13.40 25.90 -1 -28 1 11.90 26.80 0 -28 1 -17.80 26.00 1 -28 1 16.40 31.00 2 -28 1 44.30 29.80 3 -28 1 -30.60 27.00 -6 -27 1 7.20 25.30 -5 -27 1 83.79 25.80 -5 -27 1 41.30 28.30 -4 -27 1 8.40 27.50 -4 -27 1 -19.00 21.20 -3 -27 1 -0.10 21.10 -3 -27 1 24.80 27.50 -2 -27 1 -28.00 25.10 -2 -27 1 -10.60 19.40 -1 -27 1 69.19 29.00 0 -27 1 15.30 27.40 1 -27 1 -0.40 28.30 2 -27 1 63.69 29.10 3 -27 1 -22.60 26.10 4 -27 1 27.40 29.90 -5 27 -1 -20.70 19.60 5 -27 1 -18.10 27.10 -8 -26 1 -16.10 28.30 -7 -26 1 41.20 27.80 -7 -26 1 -0.60 26.20 -6 -26 1 -31.90 23.40 -6 -26 1 -23.60 23.90 -5 -26 1 -5.70 23.40 -5 -26 1 27.20 26.60 -4 -26 1 -2.70 22.50 -4 -26 1 -26.20 25.10 -3 -26 1 -0.30 20.70 -3 -26 1 52.49 27.40 -2 -26 1 -11.50 19.10 -2 -26 1 15.90 25.70 -1 -26 1 62.89 26.60 0 -26 1 -11.70 25.10 1 -26 1 -14.60 26.90 2 -26 1 32.30 28.60 3 -26 1 15.50 27.10 4 -26 1 3.80 28.80 -5 26 -1 -30.50 19.80 5 -26 1 13.90 25.10 -6 26 -1 -16.80 20.50 6 -26 1 -4.70 26.70 -7 26 -1 34.00 24.70 7 -26 1 23.40 29.00 -9 -25 1 -19.30 26.50 -8 -25 1 20.10 26.60 -8 -25 1 -19.00 26.70 -7 -25 1 -12.80 24.80 -7 -25 1 36.60 25.40 -6 -25 1 3.00 25.00 -6 -25 1 9.50 25.20 -5 -25 1 9.70 23.80 -5 -25 1 26.10 23.90 -4 -25 1 53.19 23.40 -4 -25 1 43.50 26.00 -3 -25 1 47.20 26.50 -3 -25 1 36.40 22.40 -2 -25 1 17.70 25.90 -2 -25 1 8.30 20.00 -1 -25 1 97.89 20.10 -1 -25 1 89.09 28.10 0 -25 1 -22.30 23.20 1 -25 1 18.20 26.50 2 -25 1 -18.30 25.10 3 -25 1 9.90 26.90 -4 25 -1 -10.70 17.90 4 -25 1 2.20 27.60 -5 25 -1 -21.20 20.20 5 -25 1 -27.30 24.70 -6 25 -1 -8.90 22.20 6 -25 1 -18.30 26.20 -7 25 -1 65.69 23.80 7 -25 1 -0.20 26.20 -8 25 -1 0.30 21.20 8 -25 1 -27.70 27.30 -10 -24 1 35.40 29.20 -9 -24 1 -41.90 22.60 -9 -24 1 -7.40 27.50 -8 -24 1 -11.40 26.30 -8 -24 1 13.60 25.20 -7 -24 1 -4.50 24.20 -7 -24 1 -12.20 25.60 -6 -24 1 -31.60 23.90 -6 -24 1 72.59 26.00 -5 -24 1 -5.80 23.20 -5 -24 1 1.60 25.20 -4 -24 1 -15.90 23.40 -4 -24 1 -14.50 22.10 -3 -24 1 28.40 25.50 -3 -24 1 -9.30 20.30 -2 -24 1 1.40 24.40 -2 -24 1 3.60 20.10 -1 -24 1 24.10 18.60 -1 -24 1 8.50 24.20 0 -24 1 24.80 23.10 1 -24 1 -13.40 25.10 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48.10 15.50 5 -15 4 16.50 16.50 -6 15 -4 70.99 17.20 6 -15 4 76.79 18.50 -7 15 -4 22.50 17.20 7 -15 4 20.60 17.80 -8 15 -4 9.40 17.00 8 -15 4 -7.20 19.90 -9 15 -4 174.48 22.20 9 -15 4 158.38 22.80 -10 15 -4 -2.50 17.10 10 -15 4 35.40 21.20 -11 15 -4 -17.60 17.30 11 -15 4 21.20 20.70 -12 15 -4 -12.70 17.20 -13 15 -4 -22.10 17.30 -13 15 -4 -27.60 22.20 -14 15 -4 0.20 17.00 -14 15 -4 13.90 25.80 -15 -14 4 16.80 28.90 -14 -14 4 30.80 29.00 -13 -14 4 19.70 27.50 -12 -14 4 25.90 26.70 -11 -14 4 1.00 23.30 -10 -14 4 3.60 23.00 -9 -14 4 -44.20 20.80 -8 -14 4 34.50 22.20 -7 -14 4 8.10 19.80 -6 -14 4 29.50 18.60 -5 -14 4 -32.70 17.30 -4 -14 4 103.89 19.30 -3 -14 4 12.60 14.60 -3 -14 4 -28.80 15.00 -2 -14 4 40.70 16.10 -2 -14 4 49.60 15.10 -1 -14 4 -1.10 12.50 -1 -14 4 10.00 14.20 0 -14 4 101.69 16.70 0 -14 4 113.79 13.30 1 -14 4 83.19 16.30 -2 14 -4 102.79 15.40 2 -14 4 131.09 17.10 -3 14 -4 58.29 15.30 3 -14 4 44.20 16.10 -4 14 -4 49.30 14.80 4 -14 4 19.10 15.50 -5 14 -4 9.60 13.60 5 -14 4 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381.86 21.80 -3 -6 4 413.56 24.90 2 6 -4 34.00 12.60 -2 -6 4 37.20 13.70 1 6 -4 438.16 21.70 -1 -6 4 407.06 20.80 0 6 -4 26.10 9.10 0 -6 4 34.10 9.40 0 -6 4 26.30 9.00 -1 6 -4 461.05 18.40 1 -6 4 530.15 20.30 1 -6 4 456.15 17.70 -2 6 -4 61.29 9.30 -3 6 -4 30.90 9.00 3 -6 4 32.50 10.40 -4 6 -4 115.19 11.50 4 -6 4 117.49 12.50 -5 6 -4 -1.70 9.70 -5 6 -4 -8.30 8.50 5 -6 4 8.50 11.70 -6 6 -4 29.20 11.10 -6 6 -4 24.80 9.60 6 -6 4 20.00 12.80 -7 6 -4 124.09 15.00 -7 6 -4 177.38 15.90 -8 6 -4 196.68 19.20 -8 6 -4 212.88 17.40 -9 6 -4 159.78 19.00 -9 6 -4 139.99 17.80 -9 6 -4 123.79 16.90 -10 6 -4 39.70 18.40 -10 6 -4 78.49 14.10 -10 6 -4 7.80 14.80 -11 6 -4 88.49 16.20 -11 6 -4 7.20 15.90 -11 6 -4 44.70 18.70 -12 6 -4 0.10 17.20 -12 6 -4 69.59 16.60 -12 6 -4 12.70 19.00 -13 6 -4 41.70 20.60 -13 6 -4 92.89 18.00 -13 6 -4 62.19 21.30 -14 6 -4 75.49 19.30 -14 6 -4 -16.70 19.20 -14 6 -4 10.60 19.50 -15 6 -4 29.60 21.00 -15 6 -4 51.59 19.80 -16 6 -4 14.70 22.50 -17 6 -4 16.50 23.60 -16 -5 4 19.50 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4 -15 9.80 13.10 -14 4 -15 2.20 23.20 -15 4 -15 -16.30 22.90 -15 4 -15 27.10 14.40 -16 4 -15 17.40 32.40 -16 4 -15 26.40 14.10 -17 4 -15 16.30 14.20 -14 -3 15 61.49 31.60 -14 -3 15 0.70 29.80 13 3 -15 39.10 34.60 -13 -3 15 -28.20 25.00 -13 -3 15 -33.20 25.10 12 3 -15 -6.70 30.10 -12 -3 15 71.99 26.90 -12 -3 15 -33.10 26.10 11 3 -15 -29.00 27.40 -11 -3 15 4.00 27.70 -11 -3 15 51.49 25.50 10 3 -15 15.50 25.60 -10 -3 15 7.10 25.70 -10 -3 15 -16.40 22.20 9 3 -15 33.00 22.90 -9 -3 15 -7.30 14.20 -9 -3 15 0.50 21.40 -9 -3 15 -5.30 22.70 8 3 -15 -23.30 21.20 -8 -3 15 17.40 22.90 -8 -3 15 -17.10 20.50 7 3 -15 1.40 21.80 -7 -3 15 -25.40 18.10 -7 -3 15 19.40 21.60 6 3 -15 -7.30 18.90 -6 -3 15 -13.80 19.40 -6 -3 15 -1.60 17.70 5 3 -15 -0.10 17.00 -5 -3 15 51.69 20.20 -5 -3 15 24.70 17.60 4 3 -15 42.40 17.20 -4 -3 15 34.20 17.60 -4 -3 15 22.60 16.60 3 3 -15 -7.10 15.10 -3 -3 15 -12.20 15.60 -3 -3 15 8.30 15.30 2 3 -15 13.70 15.50 -2 -3 15 12.50 15.10 -2 -3 15 4.90 15.00 1 3 -15 398.96 27.10 -1 -3 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-3 -4 -32 12.60 29.60 3 4 32 10.50 16.50 -4 -4 -32 -13.20 29.30 4 4 32 26.90 16.20 -5 -4 -32 -9.20 30.10 -6 -4 -32 -8.90 27.30 -7 -4 -32 -3.70 28.20 -1 5 32 27.20 20.00 0 5 32 -16.20 18.40 -1 -5 -32 -41.30 44.40 1 5 32 25.90 21.90 -2 -5 -32 -7.50 30.00 2 5 32 1.50 16.40 -3 -5 -32 -13.70 29.80 3 5 32 32.00 17.00 -4 -5 -32 30.20 30.90 4 5 32 7.90 16.20 -5 -5 -32 2.50 29.30 -6 -5 -32 -2.70 32.10 0 6 32 55.99 20.50 1 6 32 -12.70 16.80 -2 -6 -32 -17.50 42.70 2 6 32 -5.40 16.50 -3 -6 -32 -20.20 36.80 3 6 32 -25.40 15.70 -4 -6 -32 40.90 33.70 4 6 32 -4.10 16.80 -5 -6 -32 -8.70 35.10 -6 -6 -32 -5.00 15.50 0 7 32 -12.10 18.90 1 7 32 15.90 17.60 2 7 32 27.00 17.80 -3 -7 -32 -2.10 20.20 3 7 32 0.90 16.40 -4 -7 -32 -3.30 18.30 4 7 32 -15.30 16.70 -5 -7 -32 -2.90 17.90 -6 -7 -32 4.80 16.70 -7 -7 -32 9.30 15.00 1 8 32 8.20 17.80 -2 -8 -32 7.10 21.20 2 8 32 17.70 18.60 -3 -8 -32 -30.30 19.70 3 8 32 -13.80 17.20 -4 -8 -32 2.50 19.20 4 8 32 -23.70 17.60 -5 -8 -32 33.50 19.90 -6 -8 -32 6.20 17.40 -2 -9 -32 -5.20 22.50 2 9 32 37.00 19.30 -3 -9 -32 15.80 21.80 3 9 32 -5.40 18.00 -4 -9 -32 33.50 21.60 4 9 32 -3.70 18.20 -5 -9 -32 22.90 19.70 -3 5 -33 -35.00 29.80 -2 4 -33 -30.30 31.50 2 -4 33 18.20 38.80 -3 4 -33 4.50 30.20 -4 4 -33 -4.80 31.10 -5 4 -33 30.50 32.50 1 -3 33 26.60 30.80 -2 3 -33 -32.30 30.90 2 -3 33 27.40 34.90 -3 3 -33 -23.50 28.60 -4 3 -33 13.30 32.50 -5 3 -33 -44.90 30.90 -6 3 -33 -6.00 29.20 1 -2 33 11.60 15.30 1 -2 33 22.00 34.50 -2 2 -33 -6.80 34.90 2 -2 33 -0.90 35.90 -3 2 -33 -14.70 28.00 3 -2 33 -22.20 36.50 -4 2 -33 -7.10 30.50 -5 2 -33 -36.10 32.00 -6 2 -33 -4.10 29.90 0 -1 33 21.60 17.10 1 -1 33 37.10 16.70 1 -1 33 -39.10 28.30 -2 1 -33 -11.90 30.70 2 -1 33 11.20 29.30 -3 1 -33 35.00 33.10 3 -1 33 -6.80 36.90 -4 1 -33 -8.40 30.10 -5 1 -33 -9.00 29.90 -6 1 -33 12.70 31.10 0 0 33 23.30 16.90 1 0 33 10.10 16.10 -2 0 -33 19.00 42.10 2 0 33 29.40 32.10 2 0 33 26.50 15.00 -3 0 -33 -22.40 29.40 3 0 33 7.30 38.40 -4 0 -33 33.60 33.40 -5 0 -33 -32.80 27.00 -6 0 -33 -48.80 28.10 -7 0 -33 -36.10 28.60 0 1 33 5.00 18.30 1 1 33 56.49 17.80 2 1 33 15.00 15.10 -3 -1 -33 -73.69 36.60 -4 -1 -33 12.30 29.10 -5 -1 -33 32.70 31.70 -6 -1 -33 10.60 30.80 -7 -1 -33 -27.80 38.70 1 2 33 35.80 17.50 2 2 33 -22.70 14.90 -3 -2 -33 21.00 50.59 -4 -2 -33 -25.70 36.80 -5 -2 -33 -7.10 36.10 -6 -2 -33 -36.60 39.20 1 3 33 27.10 17.70 2 3 33 -13.10 15.40 3 3 33 39.90 16.20 1 4 33 5.80 20.30 2 4 33 16.80 16.10 3 4 33 23.40 16.30 2 5 33 -10.50 16.40 3 5 33 34.80 16.90 4 5 33 -16.80 15.70 3 6 33 1.20 16.30 4 6 33 5.60 16.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 38229 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.0000 1.0000 0.0000 0.0536(5) Uani 1 2 d S . P . . Co2 Co 0.5000 0.5000 0.0000 0.0683(6) Uani 1 2 d S . P . . Co3 Co 0.37134(9) 0.97798(6) 0.36113(5) 0.0647(4) Uani 1 1 d . . . . . Co4 Co 0.17072(9) 0.54160(6) 0.64261(5) 0.0694(4) Uani 1 1 d . . . . . P1 P 0.17774(18) 0.66337(11) -0.06589(9) 0.0599(7) Uani 1 1 d . . . . . P2 P 0.63218(17) 0.83014(10) 0.06265(9) 0.0519(7) Uani 1 1 d . . . . . P3 P 0.33913(18) 0.61025(11) 0.27472(9) 0.0603(7) Uani 1 1 d . . . . . P4 P 0.64851(19) 0.67386(11) 0.58040(11) 0.0681(8) Uani 1 1 d . . . . . P5 P 0.14785(16) 0.14125(10) 0.65822(9) 0.0498(7) Uani 1 1 d . . . . . P6 P 0.04879(18) 0.88385(11) 0.71096(10) 0.0665(8) Uani 1 1 d . . . . . S1 S 0.06510(19) 0.93614(11) 0.04741(8) 0.0681(8) Uani 1 1 d . . . . . S2 S 0.13614(19) 1.00103(11) -0.05730(10) 0.0777(9) Uani 1 1 d . . . . . S3 S 0.6024(2) 0.56151(11) -0.04287(10) 0.0794(9) Uani 1 1 d . . . . . S4 S 0.5760(2) 0.50039(11) 0.06499(10) 0.0833(9) Uani 1 1 d . . . . . S5 S 0.46504(19) 0.91135(11) 0.31484(9) 0.0711(8) Uani 1 1 d . . . . . S6 S 0.35083(19) 0.91906(13) 0.42917(9) 0.0787(8) Uani 1 1 d . . . . . S7 S 0.40498(18) 1.03945(11) 0.29595(9) 0.0700(8) Uani 1 1 d . . . . . S8 S 0.25962(19) 1.04046(12) 0.40161(10) 0.0862(9) Uani 1 1 d . . . . . S9 S 0.2028(2) 0.61518(12) 0.58850(11) 0.0929(10) Uani 1 1 d . . . . . S10 S 0.2420(2) 0.58500(14) 0.69807(13) 0.1105(11) Uani 1 1 d . . . . . S11 S 0.1090(2) 0.49798(11) 0.58431(10) 0.0772(8) Uani 1 1 d . . . . . S12 S 0.12326(18) 0.47163(11) 0.69923(9) 0.0711(8) Uani 1 1 d . . . . . N1 N 0.1773(8) 0.8214(5) 0.1150(4) 0.154(6) Uani 1 1 d . . . . . N2 N 0.7794(10) 0.6682(5) -0.1076(5) 0.146(5) Uani 1 1 d . . . . . N3 N 0.6086(10) 0.7857(6) 0.2441(4) 0.149(6) Uani 1 1 d . . . . . N4 N 0.4483(7) 1.1510(4) 0.1925(4) 0.116(3) Uani 1 1 d . . . . . N5 N 0.2227(8) 0.7495(5) 0.5149(4) 0.146(4) Uani 1 1 d . U . . . N6 N 0.0269(8) 0.3458(5) 0.7868(3) 0.116(4) Uani 1 1 d . . . . . C1 C 0.1814(6) 0.9199(4) 0.0133(4) 0.060(3) Uani 1 1 d . . . . . C2 C 0.2145(7) 0.9481(4) -0.0343(4) 0.066(3) Uani 1 1 d . . . . . C3 C 0.3046(7) 0.9329(5) -0.0639(4) 0.093(4) Uani 1 1 d . . . . . H3 H 0.3253 0.9517 -0.0958 0.111 Uiso 1 1 calc R U . . . C4 C 0.3651(7) 0.8896(5) -0.0462(5) 0.102(4) Uani 1 1 d . . . . . H4 H 0.4264 0.8804 -0.0660 0.123 Uiso 1 1 calc R U . . . C5 C 0.3341(8) 0.8607(5) 0.0000(4) 0.098(4) Uani 1 1 d . . . . . H5 H 0.3732 0.8312 0.0119 0.118 Uiso 1 1 calc R U . . . C6 C 0.2439(7) 0.8764(4) 0.0285(4) 0.068(3) Uani 1 1 d . . . . . C7 C 0.2065(8) 0.8445(5) 0.0764(5) 0.092(4) Uani 1 1 d . . . . . C8 C 0.6834(8) 0.5747(5) -0.0026(5) 0.072(3) Uani 1 1 d . . . . . C9 C 0.6743(8) 0.5474(4) 0.0438(5) 0.072(3) Uani 1 1 d . . . . . C10 C 0.7390(11) 0.5568(6) 0.0774(5) 0.098(4) Uani 1 1 d . . . . . H10 H 0.7310 0.5371 0.1094 0.118 Uiso 1 1 calc R U . . . C11 C 0.8134(12) 0.5948(7) 0.0630(6) 0.115(5) Uani 1 1 d . . . . . H11 H 0.8573 0.6010 0.0844 0.138 Uiso 1 1 calc R U . . . C12 C 0.8213(9) 0.6239(6) 0.0156(8) 0.110(5) Uani 1 1 d . . . . . H12 H 0.8704 0.6509 0.0058 0.132 Uiso 1 1 calc R U . . . C13 C 0.7600(10) 0.6145(6) -0.0170(5) 0.083(4) Uani 1 1 d . . . . . C14 C 0.7694(9) 0.6448(6) -0.0685(7) 0.109(5) Uani 1 1 d . . . . . C15 C 0.4643(6) 0.8493(4) 0.3564(4) 0.055(2) Uani 1 1 d . . . . . C16 C 0.4115(7) 0.8527(4) 0.4072(4) 0.067(3) Uani 1 1 d . . . . . C17 C 0.4087(8) 0.8009(6) 0.4393(4) 0.090(4) Uani 1 1 d . . . . . H17 H 0.3736 0.8018 0.4733 0.109 Uiso 1 1 calc R U . . . C18 C 0.4578(9) 0.7497(5) 0.4200(5) 0.099(4) Uani 1 1 d . . . . . H18 H 0.4550 0.7166 0.4419 0.119 Uiso 1 1 calc R U . . . C19 C 0.5107(8) 0.7441(5) 0.3708(5) 0.088(4) Uani 1 1 d . . . . . H19 H 0.5436 0.7086 0.3590 0.105 Uiso 1 1 calc R U . . . C20 C 0.5129(7) 0.7951(5) 0.3387(4) 0.069(3) Uani 1 1 d . . . . . C21 C 0.5692(10) 0.7921(5) 0.2841(6) 0.091(4) Uani 1 1 d . . . . . C22 C 0.3257(5) 1.1014(2) 0.3118(3) 0.073(3) Uani 1 1 d G U . . . C23 C 0.2596(5) 1.1012(3) 0.3589(2) 0.081(3) Uani 1 1 d G U . . . C24 C 0.1944(5) 1.1494(3) 0.3720(2) 0.101(4) Uani 1 1 d G U . . . H24 H 0.1501 1.1493 0.4035 0.121 Uiso 1 1 calc R U . . . C25 C 0.1952(5) 1.1977(3) 0.3381(3) 0.099(4) Uani 1 1 d G U . . . H25 H 0.1516 1.2299 0.3469 0.119 Uiso 1 1 calc R U . . . C26 C 0.2613(5) 1.1978(3) 0.2911(2) 0.103(4) Uani 1 1 d G U . . . H26 H 0.2619 1.2302 0.2684 0.124 Uiso 1 1 calc R U . . . C27 C 0.3266(5) 1.1497(3) 0.2779(2) 0.079(3) Uani 1 1 d G U . . . C28 C 0.3907(8) 1.1514(5) 0.2315(4) 0.091(4) Uani 1 1 d . U . . . C29 C 0.2564(4) 0.6670(3) 0.6226(3) 0.074(3) Uani 1 1 d G U . . . C30 C 0.2731(5) 0.6543(3) 0.6721(3) 0.099(3) Uani 1 1 d G U . . . C31 C 0.3138(5) 0.6965(4) 0.6984(2) 0.131(4) Uani 1 1 d G U . . . H31 H 0.3250 0.6880 0.7315 0.158 Uiso 1 1 calc R U . . . C32 C 0.3380(4) 0.7514(3) 0.6752(3) 0.118(4) Uani 1 1 d G U . . . H32 H 0.3653 0.7796 0.6927 0.141 Uiso 1 1 calc R U . . . C33 C 0.3214(5) 0.7641(2) 0.6257(3) 0.097(3) Uani 1 1 d G U . . . H33 H 0.3375 0.8008 0.6101 0.116 Uiso 1 1 calc R U . . . C34 C 0.2806(5) 0.7219(3) 0.5994(2) 0.098(3) Uani 1 1 d DG U . . . C35 C 0.2582(8) 0.7396(5) 0.5542(4) 0.106(4) Uani 1 1 d D U . . . C36 C 0.0639(6) 0.4230(4) 0.6667(4) 0.048(2) Uani 1 1 d . . . . . C37 C 0.0561(6) 0.4346(4) 0.6152(4) 0.057(3) Uani 1 1 d . . . . . C38 C 0.0100(8) 0.3959(5) 0.5889(4) 0.081(3) Uani 1 1 d . . . . . H38 H 0.0042 0.4047 0.5550 0.097 Uiso 1 1 calc R U . . . C39 C -0.0276(7) 0.3443(5) 0.6126(4) 0.080(3) Uani 1 1 d . . . . . H39 H -0.0563 0.3176 0.5941 0.096 Uiso 1 1 calc R U . . . C40 C -0.0227(7) 0.3320(4) 0.6637(5) 0.071(3) Uani 1 1 d . . . . . H40 H -0.0495 0.2978 0.6801 0.085 Uiso 1 1 calc R U . . . C41 C 0.0229(7) 0.3718(5) 0.6906(4) 0.062(3) Uani 1 1 d . . . . . C42 C 0.0261(7) 0.3570(4) 0.7447(4) 0.072(3) Uani 1 1 d . . . . . C1A C 0.1308(8) 0.6019(4) -0.0949(4) 0.060(3) Uani 1 1 d . . . . . C2A C 0.0571(8) 0.5696(5) -0.0674(4) 0.084(3) Uani 1 1 d . . . . . H2A H 0.0344 0.5776 -0.0324 0.101 Uiso 1 1 calc R U . . . C3A C 0.0156(9) 0.5252(5) -0.0905(6) 0.101(4) Uani 1 1 d . . . . . H3A H -0.0351 0.5038 -0.0714 0.121 Uiso 1 1 calc R U . . . C4A C 0.0496(11) 0.5137(6) -0.1407(7) 0.117(5) Uani 1 1 d . . . . . H4A H 0.0210 0.4850 -0.1571 0.140 Uiso 1 1 calc R U . . . C5A C 0.1251(12) 0.5434(6) -0.1677(5) 0.114(5) Uani 1 1 d . . . . . H5A H 0.1511 0.5320 -0.2016 0.137 Uiso 1 1 calc R U . . . C6A C 0.1656(9) 0.5901(5) -0.1472(4) 0.098(4) Uani 1 1 d . . . . . H6A H 0.2137 0.6125 -0.1674 0.117 Uiso 1 1 calc R U . . . C7A C 0.1021(6) 0.7288(4) -0.0710(3) 0.053(2) Uani 1 1 d . . . . . C8A C 0.0110(7) 0.7236(5) -0.0811(4) 0.072(3) Uani 1 1 d . . . . . H8A H -0.0119 0.6859 -0.0846 0.086 Uiso 1 1 calc R U . . . C9A C -0.0485(8) 0.7743(5) -0.0863(4) 0.082(3) Uani 1 1 d . . . . . H9A H -0.1100 0.7705 -0.0937 0.098 Uiso 1 1 calc R U . . . C10A C -0.0153(8) 0.8284(6) -0.0802(4) 0.084(4) Uani 1 1 d . . . . . H10A H -0.0543 0.8621 -0.0837 0.101 Uiso 1 1 calc R U . . . C11A C 0.0720(9) 0.8348(4) -0.0694(4) 0.082(3) Uani 1 1 d . . . . . H11A H 0.0919 0.8729 -0.0645 0.099 Uiso 1 1 calc R U . . . C12A C 0.1346(7) 0.7856(4) -0.0651(4) 0.081(3) Uani 1 1 d . . . . . H12A H 0.1964 0.7906 -0.0586 0.097 Uiso 1 1 calc R U . . . C13A C 0.2987(7) 0.6809(4) -0.0965(4) 0.067(3) Uani 1 1 d . . . . . C14A C 0.3137(8) 0.7131(5) -0.1435(5) 0.109(4) Uani 1 1 d . . . . . H14A H 0.2614 0.7234 -0.1590 0.131 Uiso 1 1 calc R U . . . C15A C 0.4058(11) 0.7296(6) -0.1665(6) 0.149(7) Uani 1 1 d . . . . . H15A H 0.4149 0.7530 -0.1964 0.178 Uiso 1 1 calc R U . . . C16A C 0.4806(11) 0.7125(6) -0.1466(6) 0.126(6) Uani 1 1 d . . . . . H16A H 0.5426 0.7223 -0.1637 0.151 Uiso 1 1 calc R U . . . C17A C 0.4702(9) 0.6807(6) -0.1014(6) 0.131(5) Uani 1 1 d . . . . . H17A H 0.5245 0.6691 -0.0878 0.158 Uiso 1 1 calc R U . . . C18A C 0.3778(9) 0.6658(5) -0.0756(5) 0.101(4) Uani 1 1 d . . . . . H18A H 0.3700 0.6454 -0.0440 0.121 Uiso 1 1 calc R U . . . C19A C 0.1747(6) 0.6437(4) 0.0002(3) 0.054(3) Uani 1 1 d . . . . . C20A C 0.1371(7) 0.6816(4) 0.0403(4) 0.084(3) Uani 1 1 d . . . . . H20A H 0.1147 0.7198 0.0332 0.101 Uiso 1 1 calc R U . . . C21A C 0.1325(8) 0.6634(5) 0.0911(4) 0.116(5) Uani 1 1 d . . . . . H21A H 0.1048 0.6891 0.1179 0.139 Uiso 1 1 calc R U . . . C22A C 0.1677(7) 0.6082(5) 0.1029(4) 0.082(4) Uani 1 1 d . . . . . H22A H 0.1635 0.5963 0.1373 0.098 Uiso 1 1 calc R U . . . C23A C 0.2080(7) 0.5719(4) 0.0646(4) 0.069(3) Uani 1 1 d . . . . . H23A H 0.2336 0.5348 0.0725 0.083 Uiso 1 1 calc R U . . . C24A C 0.2126(7) 0.5879(4) 0.0137(4) 0.077(3) Uani 1 1 d . . . . . H24A H 0.2412 0.5616 -0.0124 0.092 Uiso 1 1 calc R U . . . C1B C 0.6641(6) 0.8509(4) -0.0040(3) 0.051(2) Uani 1 1 d . . . . . C2B C 0.6430(7) 0.8167(4) -0.0435(4) 0.071(3) Uani 1 1 d . . . . . H2B H 0.6086 0.7821 -0.0357 0.085 Uiso 1 1 calc R U . . . C3B C 0.6736(9) 0.8345(6) -0.0941(4) 0.104(4) Uani 1 1 d . . . . . H3B H 0.6596 0.8117 -0.1206 0.125 Uiso 1 1 calc R U . . . C4B C 0.7246(9) 0.8853(6) -0.1061(4) 0.089(4) Uani 1 1 d . . . . . H5B H 0.7449 0.8967 -0.1407 0.106 Uiso 1 1 calc R U . . . C5B C 0.7453(8) 0.9187(5) -0.0679(5) 0.083(3) Uani 1 1 d . . . . . H4X H 0.7800 0.9531 -0.0762 0.100 Uiso 1 1 calc R U . . . C6B C 0.7155(7) 0.9022(4) -0.0172(4) 0.066(3) Uani 1 1 d . . . . . H6B H 0.7299 0.9256 0.0088 0.080 Uiso 1 1 calc R U . . . C7B C 0.5781(6) 0.8935(3) 0.0975(3) 0.051(2) Uani 1 1 d . . . . . C8B C 0.5195(7) 0.9322(4) 0.0754(3) 0.073(3) Uani 1 1 d . . . . . H8B H 0.5131 0.9260 0.0414 0.088 Uiso 1 1 calc R U . . . C9B C 0.4698(8) 0.9802(5) 0.1021(5) 0.098(4) Uani 1 1 d . . . . . H9B H 0.4299 1.0055 0.0864 0.117 Uiso 1 1 calc R U . . . C10B C 0.4799(8) 0.9898(5) 0.1513(5) 0.091(4) Uani 1 1 d . . . . . H10B H 0.4477 1.0225 0.1693 0.109 Uiso 1 1 calc R U . . . C11B C 0.5367(8) 0.9522(5) 0.1747(4) 0.088(4) Uani 1 1 d . . . . . H11B H 0.5423 0.9588 0.2087 0.106 Uiso 1 1 calc R U . . . C12B C 0.5868(7) 0.9036(4) 0.1475(4) 0.074(3) Uani 1 1 d . . . . . H12B H 0.6262 0.8781 0.1635 0.089 Uiso 1 1 calc R U . . . C13B C 0.7386(6) 0.8016(4) 0.0834(3) 0.048(2) Uani 1 1 d . . . . . C14B C 0.8311(7) 0.8151(4) 0.0579(4) 0.073(3) Uani 1 1 d . . . . . H14B H 0.8400 0.8410 0.0294 0.088 Uiso 1 1 calc R U . . . C15B C 0.9106(7) 0.7894(5) 0.0753(4) 0.088(4) Uani 1 1 d . . . . . H15B H 0.9733 0.7967 0.0574 0.105 Uiso 1 1 calc R U . . . C16B C 0.8974(8) 0.7539(5) 0.1182(4) 0.081(3) Uani 1 1 d . . . . . H16B H 0.9514 0.7383 0.1301 0.097 Uiso 1 1 calc R U . . . C17B C 0.8067(8) 0.7406(4) 0.1443(4) 0.078(3) Uani 1 1 d . . . . . H17B H 0.7990 0.7152 0.1731 0.093 Uiso 1 1 calc R U . . . C18B C 0.7275(7) 0.7648(4) 0.1278(4) 0.065(3) Uani 1 1 d . . . . . H18B H 0.6654 0.7569 0.1461 0.078 Uiso 1 1 calc R U . . . C19B C 0.5466(6) 0.7728(4) 0.0737(3) 0.050(2) Uani 1 1 d . . . . . C20B C 0.5735(7) 0.7153(4) 0.0553(4) 0.073(3) Uani 1 1 d . . . . . H20B H 0.6365 0.7074 0.0369 0.087 Uiso 1 1 calc R U . . . C21B C 0.5102(7) 0.6711(4) 0.0637(4) 0.076(3) Uani 1 1 d . . . . . H21B H 0.5307 0.6328 0.0525 0.091 Uiso 1 1 calc R U . . . C22B C 0.4143(7) 0.6821(4) 0.0890(4) 0.072(3) Uani 1 1 d . . . . . H22B H 0.3699 0.6520 0.0939 0.086 Uiso 1 1 calc R U . . . C23B C 0.3872(8) 0.7386(5) 0.1064(4) 0.083(4) Uani 1 1 d . . . . . H23B H 0.3239 0.7467 0.1243 0.100 Uiso 1 1 calc R U . . . C24B C 0.4511(7) 0.7828(4) 0.0982(4) 0.074(3) Uani 1 1 d . . . . . H24B H 0.4300 0.8211 0.1093 0.089 Uiso 1 1 calc R U . . . C1C C 0.3001(6) 0.6830(4) 0.2575(3) 0.055(3) Uani 1 1 d . . . . . C2C C 0.2187(7) 0.6905(4) 0.2351(3) 0.065(3) Uani 1 1 d . . . . . H2C H 0.1851 0.6578 0.2280 0.078 Uiso 1 1 calc R U . . . C3C C 0.1891(8) 0.7477(6) 0.2236(4) 0.085(4) Uani 1 1 d . . . . . H3C H 0.1359 0.7534 0.2077 0.102 Uiso 1 1 calc R U . . . C4C C 0.2356(10) 0.7953(6) 0.2350(4) 0.096(5) Uani 1 1 d . . . . . H4C H 0.2123 0.8335 0.2285 0.116 Uiso 1 1 calc R U . . . C5C C 0.3164(9) 0.7881(5) 0.2559(4) 0.106(4) Uani 1 1 d . . . . . H5C H 0.3501 0.8211 0.2622 0.128 Uiso 1 1 calc R U . . . C6C C 0.3481(9) 0.7317(5) 0.2676(4) 0.103(4) Uani 1 1 d . . . . . H6C H 0.4027 0.7267 0.2826 0.124 Uiso 1 1 calc R U . . . C7C C 0.4706(7) 0.6041(4) 0.2567(4) 0.063(3) Uani 1 1 d . . . . . C8C C 0.5165(8) 0.6274(4) 0.2090(4) 0.082(3) Uani 1 1 d . . . . . H8C H 0.4803 0.6474 0.1876 0.098 Uiso 1 1 calc R U . . . C9C C 0.6171(9) 0.6206(5) 0.1938(5) 0.101(4) Uani 1 1 d . . . . . H9C H 0.6490 0.6358 0.1621 0.121 Uiso 1 1 calc R U . . . C10C C 0.6675(10) 0.5914(6) 0.2259(6) 0.108(4) Uani 1 1 d . . . . . H10C H 0.7347 0.5869 0.2155 0.130 Uiso 1 1 calc R U . . . C11C C 0.6253(9) 0.5685(5) 0.2726(6) 0.098(4) Uani 1 1 d . . . . . H11C H 0.6627 0.5490 0.2937 0.118 Uiso 1 1 calc R U . . . C12C C 0.5235(8) 0.5749(4) 0.2886(4) 0.087(3) Uani 1 1 d . . . . . H12C H 0.4926 0.5594 0.3204 0.104 Uiso 1 1 calc R U . . . C13C C 0.2874(7) 0.5559(4) 0.2427(4) 0.052(2) Uani 1 1 d . . . . . C14C C 0.3375(7) 0.5277(4) 0.1980(4) 0.071(3) Uani 1 1 d . . . . . H14C H 0.4018 0.5364 0.1844 0.085 Uiso 1 1 calc R U . . . C15C C 0.2907(10) 0.4862(5) 0.1734(4) 0.079(3) Uani 1 1 d . . . . . H15C H 0.3229 0.4694 0.1423 0.094 Uiso 1 1 calc R U . . . C16C C 0.1999(10) 0.4703(5) 0.1943(5) 0.088(4) Uani 1 1 d . . . . . H16C H 0.1714 0.4408 0.1787 0.106 Uiso 1 1 calc R U . . . C17C C 0.1479(8) 0.4981(5) 0.2393(5) 0.093(4) Uani 1 1 d . . . . . H17C H 0.0843 0.4883 0.2535 0.111 Uiso 1 1 calc R U . . . C18C C 0.1931(9) 0.5394(5) 0.2615(4) 0.076(3) Uani 1 1 d . . . . . H18C H 0.1585 0.5580 0.2912 0.092 Uiso 1 1 calc R U . . . C19C C 0.3027(6) 0.5977(5) 0.3431(4) 0.062(3) Uani 1 1 d . . . . . C20C C 0.2928(10) 0.5401(5) 0.3631(5) 0.114(5) Uani 1 1 d . . . . . H20C H 0.3034 0.5076 0.3409 0.137 Uiso 1 1 calc R U . . . C21C C 0.2666(13) 0.5310(7) 0.4169(6) 0.161(7) Uani 1 1 d . . . . . H21C H 0.2637 0.4928 0.4312 0.193 Uiso 1 1 calc R U . . . C22C C 0.2459(11) 0.5793(9) 0.4473(6) 0.131(6) Uani 1 1 d . . . . . H22C H 0.2227 0.5727 0.4826 0.157 Uiso 1 1 calc R U . . . C23C C 0.2555(10) 0.6343(7) 0.4315(6) 0.107(5) Uani 1 1 d . . . . . H23C H 0.2446 0.6655 0.4550 0.129 Uiso 1 1 calc R U . . . C24C C 0.2830(7) 0.6452(5) 0.3780(5) 0.079(3) Uani 1 1 d . . . . . H24C H 0.2882 0.6842 0.3656 0.095 Uiso 1 1 calc R U . . . C1D C 0.5968(6) 0.7482(4) 0.5762(4) 0.064(3) Uani 1 1 d . . . . . C2D C 0.5727(6) 0.7833(4) 0.6203(4) 0.077(3) Uani 1 1 d . . . . . H2D H 0.5781 0.7674 0.6526 0.092 Uiso 1 1 calc R U . . . C3D C 0.5411(7) 0.8410(5) 0.6160(5) 0.093(4) Uani 1 1 d . . . . . H3D H 0.5233 0.8644 0.6454 0.111 Uiso 1 1 calc R U . . . C4D C 0.5355(9) 0.8643(5) 0.5686(6) 0.106(5) Uani 1 1 d . . . . . H4D H 0.5161 0.9041 0.5657 0.127 Uiso 1 1 calc R U . . . C5D C 0.5578(9) 0.8304(5) 0.5256(5) 0.107(4) Uani 1 1 d . . . . . H5D H 0.5548 0.8473 0.4934 0.129 Uiso 1 1 calc R U . . . C6D C 0.5845(8) 0.7718(5) 0.5290(4) 0.088(4) Uani 1 1 d . . . . . H6D H 0.5945 0.7479 0.4997 0.105 Uiso 1 1 calc R U . . . C7D C 0.7781(7) 0.6781(4) 0.5645(4) 0.064(3) Uani 1 1 d . . . . . C8D C 0.8208(8) 0.7276(5) 0.5411(4) 0.082(3) Uani 1 1 d . . . . . H8D H 0.7835 0.7598 0.5322 0.098 Uiso 1 1 calc R U . . . C9D C 0.9230(9) 0.7284(6) 0.5306(4) 0.104(4) Uani 1 1 d . . . . . H9D H 0.9536 0.7617 0.5147 0.125 Uiso 1 1 calc R U . . . C10D C 0.9769(9) 0.6817(7) 0.5433(5) 0.116(5) Uani 1 1 d . . . . . H10D H 1.0442 0.6841 0.5363 0.139 Uiso 1 1 calc R U . . . C11D C 0.9369(11) 0.6308(6) 0.5663(6) 0.135(6) Uani 1 1 d . . . . . H11D H 0.9746 0.5984 0.5745 0.161 Uiso 1 1 calc R U . . . C12D C 0.8367(8) 0.6311(5) 0.5762(5) 0.111(4) Uani 1 1 d . . . . . H12D H 0.8067 0.5974 0.5919 0.133 Uiso 1 1 calc R U . . . C13D C 0.6068(7) 0.6288(4) 0.5340(4) 0.062(3) Uani 1 1 d . . . . . C14D C 0.6683(7) 0.5903(4) 0.4994(4) 0.072(3) Uani 1 1 d . . . . . H14D H 0.7346 0.5868 0.4991 0.086 Uiso 1 1 calc R U . . . C15D C 0.6263(10) 0.5573(4) 0.4650(4) 0.082(4) Uani 1 1 d . . . . . H15D H 0.6650 0.5312 0.4417 0.099 Uiso 1 1 calc R U . . . C16D C 0.5289(9) 0.5637(5) 0.4658(5) 0.097(4) Uani 1 1 d . . . . . H16D H 0.5022 0.5432 0.4420 0.116 Uiso 1 1 calc R U . . . C17D C 0.4708(8) 0.5992(5) 0.5008(5) 0.087(4) Uani 1 1 d . . . . . H17D H 0.4041 0.6006 0.5018 0.104 Uiso 1 1 calc R U . . . C18D C 0.5067(8) 0.6334(4) 0.5348(4) 0.080(3) Uani 1 1 d . . . . . H18D H 0.4658 0.6588 0.5577 0.097 Uiso 1 1 calc R U . . . C19D C 0.6155(9) 0.6435(4) 0.6433(4) 0.075(3) Uani 1 1 d . . . . . C20D C 0.5325(10) 0.6127(5) 0.6585(5) 0.095(4) Uani 1 1 d . . . . . H20D H 0.4932 0.6056 0.6349 0.114 Uiso 1 1 calc R U . . . C21D C 0.5060(10) 0.5914(5) 0.7112(7) 0.104(4) Uani 1 1 d . . . . . H21D H 0.4499 0.5700 0.7214 0.125 Uiso 1 1 calc R U . . . C22D C 0.5635(15) 0.6023(7) 0.7468(7) 0.137(6) Uani 1 1 d . . . . . H22D H 0.5464 0.5902 0.7814 0.164 Uiso 1 1 calc R U . . . C23D C 0.6464(12) 0.6317(7) 0.7286(7) 0.125(5) Uani 1 1 d . . . . . H23D H 0.6878 0.6371 0.7515 0.150 Uiso 1 1 calc R U . . . C24D C 0.6735(10) 0.6536(5) 0.6799(5) 0.115(5) Uani 1 1 d . . . . . H24D H 0.7297 0.6750 0.6707 0.138 Uiso 1 1 calc R U . . . C1E C 0.1935(6) 0.2129(4) 0.6494(3) 0.045(2) Uani 1 1 d . . . . . C2E C 0.2221(7) 0.2374(5) 0.6004(4) 0.083(3) Uani 1 1 d . . . . . H2E H 0.2233 0.2141 0.5715 0.100 Uiso 1 1 calc R U . . . C3E C 0.2488(7) 0.2953(5) 0.5937(4) 0.078(3) Uani 1 1 d . . . . . H3E H 0.2616 0.3119 0.5604 0.094 Uiso 1 1 calc R U . . . C4E C 0.2568(6) 0.3291(4) 0.6350(5) 0.074(3) Uani 1 1 d . . . . . H4E H 0.2765 0.3682 0.6300 0.089 Uiso 1 1 calc R U . . . C5E C 0.2355(7) 0.3050(5) 0.6843(4) 0.081(3) Uani 1 1 d . . . . . H5E H 0.2424 0.3269 0.7129 0.097 Uiso 1 1 calc R U . . . C6E C 0.2035(7) 0.2469(4) 0.6903(4) 0.064(3) Uani 1 1 d . . . . . H6E H 0.1882 0.2306 0.7236 0.076 Uiso 1 1 calc R U . . . C7E C 0.1378(7) 0.1195(4) 0.7234(3) 0.057(3) Uani 1 1 d . . . . . C8E C 0.0639(6) 0.1437(4) 0.7627(4) 0.067(3) Uani 1 1 d . . . . . H8E H 0.0164 0.1698 0.7539 0.081 Uiso 1 1 calc R U . . . C9E C 0.0613(9) 0.1289(5) 0.8145(4) 0.083(4) Uani 1 1 d . . . . . H9E H 0.0127 0.1447 0.8406 0.100 Uiso 1 1 calc R U . . . C10E C 0.1310(12) 0.0911(6) 0.8258(5) 0.109(5) Uani 1 1 d . . . . . H10E H 0.1293 0.0817 0.8606 0.130 Uiso 1 1 calc R U . . . C11E C 0.2014(9) 0.0664(5) 0.7910(5) 0.098(4) Uani 1 1 d . . . . . H11E H 0.2466 0.0396 0.8012 0.117 Uiso 1 1 calc R U . . . C12E C 0.2077(7) 0.0809(4) 0.7383(4) 0.066(3) Uani 1 1 d . . . . . H12E H 0.2585 0.0648 0.7135 0.080 Uiso 1 1 calc R U . . . C13E C 0.2240(6) 0.0923(4) 0.6140(3) 0.049(2) Uani 1 1 d . . . . . C14E C 0.3244(7) 0.0879(4) 0.6143(3) 0.072(3) Uani 1 1 d . . . . . H14E H 0.3511 0.1111 0.6365 0.086 Uiso 1 1 calc R U . . . C15E C 0.3818(7) 0.0485(5) 0.5809(4) 0.080(3) Uani 1 1 d . . . . . H15E H 0.4469 0.0430 0.5831 0.096 Uiso 1 1 calc R U . . . C16E C 0.3488(8) 0.0175(5) 0.5453(4) 0.077(3) Uani 1 1 d . . . . . H16E H 0.3909 -0.0066 0.5218 0.092 Uiso 1 1 calc R U . . . C71E C 0.2516(8) 0.0223(5) 0.5446(4) 0.096(4) Uani 1 1 d . . . . . H71E H 0.2272 0.0006 0.5206 0.116 Uiso 1 1 calc R U . . . C18E C 0.1892(7) 0.0590(4) 0.5790(3) 0.068(3) Uani 1 1 d . . . . . H18E H 0.1231 0.0611 0.5785 0.081 Uiso 1 1 calc R U . . . C19E C 0.0272(6) 0.1438(4) 0.6441(4) 0.054(2) Uani 1 1 d . . . . . C20E C -0.0345(8) 0.0990(5) 0.6645(4) 0.078(3) Uani 1 1 d . . . . . H20E H -0.0136 0.0698 0.6858 0.093 Uiso 1 1 calc R U . . . C21E C -0.1250(9) 0.0970(5) 0.6540(5) 0.097(4) Uani 1 1 d . . . . . H21E H -0.1663 0.0674 0.6690 0.117 Uiso 1 1 calc R U . . . C22E C -0.1556(9) 0.1384(6) 0.6214(6) 0.112(4) Uani 1 1 d . . . . . H22E H -0.2170 0.1366 0.6134 0.134 Uiso 1 1 calc R U . . . C23E C -0.0959(9) 0.1819(5) 0.6008(5) 0.102(4) Uani 1 1 d . . . . . H23E H -0.1167 0.2102 0.5787 0.122 Uiso 1 1 calc R U . . . C24E C -0.0035(7) 0.1850(4) 0.6122(4) 0.076(3) Uani 1 1 d . . . . . H24E H 0.0369 0.2154 0.5979 0.091 Uiso 1 1 calc R U . . . C1F C 0.0549(7) 0.9004(4) 0.6429(4) 0.068(3) Uani 1 1 d . . . . . C2F C 0.1193(11) 0.8681(6) 0.6060(5) 0.165(7) Uani 1 1 d . . . . . H2F H 0.1589 0.8383 0.6169 0.198 Uiso 1 1 calc R U . . . C3F C 0.1269(14) 0.8788(7) 0.5527(6) 0.176(8) Uani 1 1 d . . . . . H3F H 0.1735 0.8581 0.5286 0.212 Uiso 1 1 calc R U . . . C4F C 0.0677(11) 0.9184(7) 0.5373(5) 0.127(5) Uani 1 1 d . . . . . H4F H 0.0704 0.9242 0.5019 0.153 Uiso 1 1 calc R U . . . C5F C 0.0025(8) 0.9511(6) 0.5716(5) 0.103(4) Uani 1 1 d . . . . . H5F H -0.0383 0.9798 0.5601 0.124 Uiso 1 1 calc R U . . . C6F C -0.0023(7) 0.9407(4) 0.6250(5) 0.080(3) Uani 1 1 d . . . . . H6F H -0.0473 0.9631 0.6487 0.096 Uiso 1 1 calc R U . . . C7F C 0.0125(7) 0.8104(4) 0.7283(4) 0.080(3) Uani 1 1 d . U . . . C8F C -0.0584(8) 0.7973(5) 0.7697(4) 0.102(4) Uani 1 1 d . U . . . H8F H -0.0911 0.8288 0.7892 0.122 Uiso 1 1 calc R U . . . C9F C -0.0860(10) 0.7385(6) 0.7852(5) 0.129(4) Uani 1 1 d . U . . . H9F H -0.1351 0.7307 0.8136 0.155 Uiso 1 1 calc R U . . . C10F C -0.0360(9) 0.6954(6) 0.7556(5) 0.129(4) Uani 1 1 d . U . . . H10F H -0.0431 0.6565 0.7683 0.155 Uiso 1 1 calc R U . . . C11F C 0.0231(12) 0.7028(7) 0.7098(6) 0.174(6) Uani 1 1 d . U . . . H11F H 0.0461 0.6705 0.6886 0.209 Uiso 1 1 calc R U . . . C12F C 0.0508(10) 0.7636(6) 0.6938(5) 0.139(5) Uani 1 1 d . U . . . H12F H 0.0919 0.7712 0.6621 0.167 Uiso 1 1 calc R U . . . C13F C 0.1657(7) 0.8908(4) 0.7270(4) 0.065(3) Uani 1 1 d . . . . . C14F C 0.1859(9) 0.8661(5) 0.7724(5) 0.099(4) Uani 1 1 d . . . . . H14F H 0.1399 0.8433 0.7937 0.119 Uiso 1 1 calc R U . . . C15F C 0.2729(10) 0.8749(5) 0.7861(5) 0.108(4) Uani 1 1 d . . . . . H15F H 0.2859 0.8579 0.8167 0.130 Uiso 1 1 calc R U . . . C16F C 0.3407(9) 0.9083(6) 0.7554(6) 0.102(4) Uani 1 1 d . . . . . H16F H 0.3990 0.9147 0.7657 0.122 Uiso 1 1 calc R U . . . C17F C 0.3245(8) 0.9324(5) 0.7099(5) 0.093(4) Uani 1 1 d . . . . . H17F H 0.3729 0.9536 0.6885 0.112 Uiso 1 1 calc R U . . . C18F C 0.2365(8) 0.9256(4) 0.6954(4) 0.082(3) Uani 1 1 d . . . . . H18F H 0.2238 0.9437 0.6652 0.098 Uiso 1 1 calc R U . . . C19F C -0.0364(7) 0.9352(4) 0.7498(3) 0.051(2) Uani 1 1 d . . . . . C20F C -0.0103(7) 0.9673(4) 0.7888(4) 0.077(3) Uani 1 1 d . . . . . H20F H 0.0527 0.9633 0.7948 0.092 Uiso 1 1 calc R U . . . C21F C -0.0765(9) 1.0047(5) 0.8184(4) 0.092(4) Uani 1 1 d . . . . . H21F H -0.0591 1.0255 0.8452 0.110 Uiso 1 1 calc R U . . . C22F C -0.1684(9) 1.0120(4) 0.8090(4) 0.079(3) Uani 1 1 d . . . . . H22F H -0.2126 1.0385 0.8289 0.095 Uiso 1 1 calc R U . . . C23F C -0.1966(8) 0.9806(5) 0.7705(4) 0.091(4) Uani 1 1 d . . . . . H23F H -0.2592 0.9859 0.7640 0.109 Uiso 1 1 calc R U . . . C24F C -0.1300(7) 0.9411(4) 0.7416(3) 0.066(3) Uani 1 1 d . . . . . H24F H -0.1486 0.9182 0.7165 0.079 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0651(13) 0.0426(11) 0.0565(11) 0.0047(8) -0.0211(10) 0.0011(9) Co2 0.0625(13) 0.0515(12) 0.0834(14) -0.0130(10) 0.0034(11) 0.0035(10) Co3 0.0478(8) 0.0733(9) 0.0755(9) -0.0062(7) -0.0165(7) -0.0071(7) Co4 0.0493(9) 0.0666(9) 0.0922(10) -0.0154(7) -0.0137(8) 0.0042(7) P1 0.0514(17) 0.0567(17) 0.0683(18) -0.0035(13) -0.0056(14) 0.0061(14) P2 0.0442(15) 0.0546(16) 0.0559(16) -0.0044(12) -0.0103(13) 0.0122(13) P3 0.0612(18) 0.0560(17) 0.0687(18) 0.0046(13) -0.0276(14) 0.0094(14) P4 0.0533(18) 0.0566(18) 0.099(2) -0.0018(15) -0.0275(16) 0.0047(14) P5 0.0408(15) 0.0513(16) 0.0585(16) 0.0007(12) -0.0125(12) -0.0010(12) P6 0.0464(17) 0.0638(18) 0.092(2) 0.0000(15) -0.0214(15) -0.0004(14) S1 0.0799(19) 0.0703(18) 0.0530(15) 0.0121(12) -0.0163(14) 0.0189(15) S2 0.077(2) 0.0687(18) 0.0825(19) 0.0333(14) -0.0089(16) 0.0015(15) S3 0.074(2) 0.0755(19) 0.0816(19) -0.0089(15) 0.0015(17) -0.0026(16) S4 0.090(2) 0.0632(18) 0.093(2) -0.0069(15) -0.0110(18) 0.0042(17) S5 0.0768(19) 0.0756(19) 0.0623(17) 0.0031(13) -0.0186(15) 0.0004(15) S6 0.0612(18) 0.106(2) 0.0690(18) -0.0074(15) -0.0091(15) -0.0153(16) S7 0.0673(18) 0.0641(17) 0.0804(18) -0.0040(13) -0.0190(15) -0.0005(14) S8 0.0588(18) 0.099(2) 0.096(2) -0.0155(16) -0.0038(16) 0.0038(16) S9 0.086(2) 0.070(2) 0.121(2) -0.0013(17) -0.0167(19) -0.0096(17) S10 0.108(3) 0.098(2) 0.136(3) -0.019(2) -0.043(2) -0.019(2) S11 0.085(2) 0.0708(19) 0.0805(19) 0.0040(14) -0.0289(16) -0.0006(16) S12 0.0611(18) 0.0800(19) 0.0757(18) -0.0115(14) -0.0226(14) 0.0054(15) N1 0.157(11) 0.186(11) 0.091(8) 0.063(8) 0.018(8) 0.085(9) N2 0.154(12) 0.120(10) 0.147(12) 0.017(8) 0.022(10) -0.064(8) N3 0.166(12) 0.168(11) 0.116(10) -0.037(9) -0.048(9) 0.077(9) N4 0.132(9) 0.110(8) 0.114(8) 0.034(6) -0.047(7) -0.007(7) N5 0.146(4) 0.144(4) 0.147(4) -0.001(2) -0.028(2) -0.006(2) N6 0.126(9) 0.164(10) 0.057(6) 0.016(6) -0.019(7) 0.000(7) C1 0.037(6) 0.077(7) 0.070(7) -0.005(5) -0.023(5) 0.003(5) C2 0.060(7) 0.050(6) 0.082(8) 0.008(5) -0.006(6) 0.004(5) C3 0.056(7) 0.133(10) 0.087(8) 0.036(7) -0.011(7) -0.015(7) C4 0.035(6) 0.160(12) 0.111(10) 0.032(8) -0.021(7) 0.023(7) C5 0.067(8) 0.132(11) 0.094(9) 0.035(8) -0.022(7) 0.025(8) C6 0.064(7) 0.071(7) 0.070(7) 0.007(6) -0.021(6) 0.016(6) C7 0.074(8) 0.111(10) 0.086(9) 0.024(7) -0.018(7) 0.045(7) C8 0.059(8) 0.053(7) 0.098(10) -0.013(6) -0.003(7) 0.009(6) C9 0.062(8) 0.043(7) 0.103(10) -0.009(6) 0.000(8) 0.004(6) C10 0.081(10) 0.084(10) 0.130(12) -0.019(8) -0.026(10) 0.011(8) C11 0.110(14) 0.107(13) 0.129(14) -0.029(10) -0.030(11) 0.029(11) C12 0.054(9) 0.074(10) 0.195(18) -0.040(11) -0.004(11) 0.003(7) C13 0.068(10) 0.076(9) 0.092(10) -0.030(8) 0.011(9) 0.017(8) C14 0.075(9) 0.092(11) 0.136(14) -0.026(9) 0.048(10) -0.028(8) C15 0.048(6) 0.059(7) 0.068(7) 0.010(5) -0.037(5) -0.011(5) C16 0.051(6) 0.087(8) 0.067(7) 0.020(6) -0.017(6) -0.024(6) C17 0.083(9) 0.099(9) 0.083(8) 0.023(8) -0.007(7) -0.001(8) C18 0.091(10) 0.084(10) 0.126(11) 0.030(8) -0.028(9) -0.017(8) C19 0.075(9) 0.073(9) 0.119(10) 0.013(8) -0.030(8) -0.008(7) C20 0.063(7) 0.075(8) 0.074(8) -0.005(7) -0.022(6) -0.010(6) C21 0.096(11) 0.061(8) 0.129(12) -0.021(8) -0.056(10) 0.014(7) C22 0.073(3) 0.073(3) 0.074(3) -0.0015(10) -0.0154(11) -0.0032(10) C23 0.081(3) 0.081(3) 0.081(3) -0.0011(10) -0.0166(11) -0.0029(10) C24 0.101(4) 0.101(4) 0.101(4) -0.0019(10) -0.0201(12) -0.0036(10) C25 0.099(4) 0.100(4) 0.100(4) -0.0022(10) -0.0206(12) -0.0036(10) C26 0.103(4) 0.103(4) 0.103(4) -0.0009(10) -0.0216(12) -0.0041(10) C27 0.078(3) 0.079(3) 0.079(3) -0.0011(10) -0.0160(11) -0.0028(10) C28 0.091(4) 0.090(4) 0.091(4) -0.0007(10) -0.0187(12) -0.0035(10) C29 0.073(3) 0.073(3) 0.075(3) -0.0008(10) -0.0136(11) -0.0028(10) C30 0.099(4) 0.099(4) 0.099(4) -0.0022(10) -0.0192(12) -0.0037(10) C31 0.131(4) 0.131(4) 0.132(4) -0.0017(10) -0.0261(13) -0.0051(10) C32 0.117(4) 0.118(4) 0.119(4) -0.0020(10) -0.0232(13) -0.0043(10) C33 0.096(4) 0.096(4) 0.098(4) -0.0016(10) -0.0186(12) -0.0034(10) C34 0.098(4) 0.098(4) 0.099(4) -0.0013(10) -0.0198(12) -0.0030(10) C35 0.107(4) 0.106(4) 0.106(4) -0.0014(10) -0.0208(12) -0.0043(10) C36 0.026(5) 0.056(6) 0.067(7) -0.016(5) -0.019(5) 0.009(5) C37 0.032(6) 0.068(7) 0.072(8) -0.014(6) -0.009(5) 0.004(5) C38 0.085(9) 0.080(9) 0.084(8) 0.006(7) -0.037(7) 0.021(7) C39 0.077(8) 0.090(10) 0.081(9) -0.011(7) -0.039(7) 0.009(7) C40 0.060(7) 0.050(7) 0.101(9) -0.015(6) -0.014(7) 0.013(6) C41 0.042(6) 0.067(8) 0.071(8) -0.013(6) -0.001(6) 0.001(6) C42 0.069(7) 0.084(8) 0.059(7) -0.006(6) -0.008(7) 0.009(6) C1A 0.071(8) 0.055(7) 0.055(7) -0.006(5) -0.015(6) 0.004(6) C2A 0.085(9) 0.079(8) 0.082(8) -0.016(7) 0.001(7) -0.019(7) C3A 0.124(11) 0.075(9) 0.126(11) 0.008(8) -0.069(10) -0.047(8) C4A 0.136(14) 0.086(11) 0.157(15) -0.023(11) -0.095(12) -0.010(10) C5A 0.167(16) 0.081(10) 0.093(10) -0.017(8) -0.019(10) -0.009(10) C6A 0.127(11) 0.090(10) 0.076(9) -0.007(7) -0.016(8) -0.014(8) C7A 0.037(6) 0.060(7) 0.061(6) 0.010(5) -0.006(5) -0.002(5) C8A 0.048(7) 0.074(8) 0.099(8) 0.002(6) -0.025(6) -0.011(6) C9A 0.063(8) 0.089(9) 0.103(9) 0.012(7) -0.036(6) -0.029(8) C10A 0.055(8) 0.101(11) 0.103(9) 0.001(7) -0.036(7) 0.019(8) C11A 0.098(9) 0.042(7) 0.112(9) -0.015(6) -0.032(8) 0.001(7) C12A 0.056(7) 0.047(7) 0.146(10) 0.000(6) -0.037(7) -0.006(6) C13A 0.054(7) 0.050(7) 0.091(8) 0.008(5) -0.002(6) 0.005(5) C14A 0.055(8) 0.118(10) 0.146(12) 0.042(9) -0.006(8) -0.002(8) C15A 0.077(11) 0.124(12) 0.223(17) 0.071(11) 0.015(12) -0.006(10) C16A 0.089(12) 0.085(10) 0.183(16) 0.045(9) 0.016(11) -0.007(9) C17A 0.063(10) 0.108(11) 0.216(17) 0.051(10) -0.019(10) 0.011(8) C18A 0.061(8) 0.087(9) 0.149(11) 0.041(7) -0.010(9) -0.002(7) C19A 0.051(6) 0.056(6) 0.048(6) -0.005(5) 0.003(5) 0.006(5) C20A 0.087(8) 0.087(8) 0.081(8) 0.004(7) -0.030(7) 0.036(7) C21A 0.137(11) 0.111(10) 0.087(9) -0.010(7) -0.013(8) 0.096(9) C22A 0.075(8) 0.113(9) 0.054(7) -0.015(6) -0.009(6) 0.029(7) C23A 0.068(7) 0.060(7) 0.079(8) 0.018(6) -0.019(6) 0.007(6) C24A 0.095(8) 0.047(7) 0.080(8) -0.006(5) -0.001(7) 0.018(6) C1B 0.039(6) 0.066(7) 0.049(6) 0.009(5) -0.010(5) 0.006(5) C2B 0.073(7) 0.090(8) 0.052(7) -0.008(6) -0.018(6) 0.000(6) C3B 0.130(12) 0.124(11) 0.056(9) 0.001(7) -0.012(8) -0.017(9) C4B 0.092(10) 0.112(11) 0.053(8) 0.030(8) 0.000(7) 0.023(8) C5B 0.076(8) 0.087(9) 0.089(9) 0.007(8) -0.024(8) 0.011(7) C6B 0.068(8) 0.072(8) 0.059(7) 0.009(5) -0.018(6) 0.022(6) C7B 0.049(6) 0.038(6) 0.063(7) 0.002(5) -0.005(5) 0.006(5) C8B 0.080(8) 0.060(7) 0.076(7) -0.020(5) -0.012(6) 0.038(6) C9B 0.102(10) 0.078(9) 0.110(10) -0.002(8) -0.020(9) 0.018(7) C10B 0.074(8) 0.071(8) 0.116(11) -0.031(8) 0.005(8) 0.034(6) C11B 0.103(9) 0.091(9) 0.057(7) -0.013(6) 0.016(7) 0.007(7) C12B 0.067(7) 0.073(7) 0.074(7) -0.004(6) 0.001(6) 0.025(6) C13B 0.047(6) 0.042(6) 0.052(6) -0.003(4) -0.006(5) 0.012(5) C14B 0.052(7) 0.084(8) 0.077(7) 0.021(6) -0.001(6) 0.003(6) C15B 0.044(7) 0.116(10) 0.099(9) 0.001(7) -0.006(7) 0.017(7) C16B 0.075(9) 0.103(9) 0.071(8) 0.015(6) -0.035(7) 0.020(7) C17B 0.070(8) 0.070(8) 0.092(8) 0.007(6) -0.015(7) 0.002(7) C18B 0.040(6) 0.061(7) 0.092(8) -0.003(6) -0.009(6) 0.013(5) C19B 0.039(6) 0.065(7) 0.045(5) 0.012(5) -0.012(5) 0.005(5) C20B 0.041(7) 0.063(7) 0.105(8) 0.006(6) 0.005(6) 0.008(6) C21B 0.049(7) 0.063(7) 0.109(9) -0.015(6) 0.001(6) -0.002(6) C22B 0.058(7) 0.063(7) 0.096(8) 0.012(6) -0.021(6) 0.000(6) C23B 0.058(8) 0.076(8) 0.106(9) 0.020(7) 0.007(6) -0.003(7) C24B 0.054(7) 0.063(7) 0.095(8) 0.025(6) 0.001(6) 0.030(6) C1C 0.037(6) 0.053(6) 0.073(7) 0.015(5) -0.014(5) 0.013(5) C2C 0.067(7) 0.056(7) 0.070(7) 0.007(5) -0.016(6) 0.025(6) C3C 0.080(9) 0.116(11) 0.060(7) 0.006(7) -0.019(6) 0.016(9) C4C 0.115(12) 0.093(10) 0.072(8) 0.001(7) -0.011(8) 0.060(9) C5C 0.125(11) 0.053(8) 0.164(12) 0.034(7) -0.086(9) -0.014(7) C6C 0.124(11) 0.072(9) 0.138(10) 0.043(7) -0.088(9) -0.014(8) C7C 0.055(7) 0.053(6) 0.088(8) 0.001(5) -0.031(6) 0.011(5) C8C 0.061(8) 0.082(8) 0.100(9) 0.025(6) -0.016(7) 0.004(6) C9C 0.061(9) 0.112(10) 0.123(11) 0.017(8) -0.003(8) -0.001(8) C10C 0.075(10) 0.116(12) 0.144(13) -0.033(10) -0.042(10) -0.006(9) C11C 0.081(10) 0.082(9) 0.150(12) -0.017(8) -0.069(9) 0.028(8) C12C 0.071(8) 0.096(9) 0.103(9) -0.002(6) -0.048(7) 0.016(7) C13C 0.044(6) 0.045(6) 0.071(7) 0.010(5) -0.022(5) 0.002(5) C14C 0.068(7) 0.075(8) 0.070(7) -0.011(6) -0.018(6) 0.014(6) C15C 0.110(11) 0.088(9) 0.043(6) -0.008(6) -0.027(7) 0.004(8) C16C 0.114(11) 0.068(8) 0.097(10) -0.001(7) -0.055(8) -0.005(8) C17C 0.071(9) 0.077(9) 0.132(11) -0.007(8) -0.027(8) 0.002(7) C18C 0.084(9) 0.062(7) 0.090(8) -0.017(6) -0.035(7) 0.008(7) C19C 0.055(6) 0.068(7) 0.074(7) 0.010(6) -0.036(6) -0.010(6) C20C 0.198(14) 0.069(9) 0.092(10) -0.001(7) -0.066(10) -0.022(9) C21C 0.27(2) 0.149(16) 0.088(12) 0.050(10) -0.087(13) -0.070(14) C22C 0.131(13) 0.21(2) 0.065(10) -0.001(13) -0.037(9) -0.067(15) C23C 0.118(11) 0.136(13) 0.079(11) -0.011(9) -0.042(9) -0.021(10) C24C 0.070(8) 0.087(9) 0.087(9) 0.000(7) -0.031(7) 0.000(6) C1D 0.037(6) 0.054(7) 0.103(8) -0.010(6) -0.021(6) 0.005(5) C2D 0.050(7) 0.063(7) 0.117(9) -0.017(6) -0.021(6) 0.025(6) C3D 0.063(7) 0.059(8) 0.168(13) -0.046(8) -0.051(8) 0.015(6) C4D 0.106(10) 0.051(9) 0.175(14) 0.010(9) -0.062(11) -0.009(7) C5D 0.148(12) 0.057(9) 0.121(11) 0.012(8) -0.039(9) 0.001(8) C6D 0.109(9) 0.071(8) 0.080(8) 0.012(6) -0.019(7) 0.019(7) C7D 0.049(6) 0.057(7) 0.091(7) -0.018(5) -0.026(6) 0.007(6) C8D 0.057(8) 0.091(9) 0.101(9) 0.020(7) -0.025(7) -0.006(7) C9D 0.059(9) 0.132(12) 0.129(10) -0.015(8) -0.031(8) -0.031(8) C10D 0.050(9) 0.163(15) 0.146(13) -0.072(11) -0.046(8) 0.033(10) C11D 0.095(13) 0.089(11) 0.241(18) -0.048(11) -0.090(12) 0.039(10) C12D 0.057(8) 0.110(10) 0.179(12) -0.015(8) -0.059(8) 0.025(8) C13D 0.042(6) 0.044(6) 0.105(8) 0.013(5) -0.028(6) -0.003(5) C14D 0.053(7) 0.046(6) 0.108(9) 0.026(6) -0.004(7) 0.016(6) C15D 0.131(12) 0.036(6) 0.092(8) -0.004(5) -0.052(8) -0.015(7) C16D 0.072(9) 0.099(10) 0.140(12) 0.015(8) -0.069(9) -0.011(8) C17D 0.048(7) 0.073(9) 0.142(11) 0.005(7) -0.029(8) 0.003(7) C18D 0.059(8) 0.064(7) 0.130(10) -0.021(7) -0.049(7) 0.012(6) C19D 0.067(8) 0.053(7) 0.105(10) 0.007(6) -0.021(8) -0.010(6) C20D 0.105(11) 0.072(8) 0.107(11) 0.003(7) -0.021(9) 0.017(8) C21D 0.082(10) 0.076(9) 0.141(13) 0.011(9) 0.007(10) -0.008(7) C22D 0.167(19) 0.126(14) 0.119(14) 0.022(11) -0.042(14) 0.021(13) C23D 0.130(14) 0.132(13) 0.125(15) 0.022(10) -0.055(11) -0.006(11) C24D 0.154(13) 0.117(10) 0.092(10) 0.047(8) -0.073(10) -0.015(9) C1E 0.034(5) 0.058(6) 0.045(6) 0.004(5) -0.014(5) 0.005(5) C2E 0.079(8) 0.072(8) 0.090(9) 0.004(6) 0.003(7) -0.016(7) C3E 0.067(8) 0.082(9) 0.080(8) 0.002(7) -0.003(6) -0.012(7) C4E 0.037(6) 0.050(7) 0.126(10) -0.007(7) 0.008(7) 0.001(5) C5E 0.074(8) 0.084(9) 0.074(8) -0.024(7) 0.014(6) -0.006(7) C6E 0.061(7) 0.046(7) 0.079(8) -0.002(6) -0.003(6) -0.003(5) C7E 0.070(7) 0.042(6) 0.059(6) 0.015(5) -0.021(6) 0.002(5) C8E 0.056(7) 0.070(7) 0.068(7) 0.003(5) 0.001(6) 0.010(5) C9E 0.097(10) 0.103(10) 0.044(7) -0.005(6) 0.011(7) -0.058(8) C10E 0.153(14) 0.098(11) 0.089(11) 0.048(8) -0.057(11) -0.034(10) C11E 0.077(9) 0.103(10) 0.113(11) 0.016(9) -0.024(8) 0.003(7) C12E 0.090(8) 0.047(6) 0.063(7) 0.007(5) -0.016(6) -0.009(6) C13E 0.035(6) 0.058(6) 0.060(6) -0.002(5) -0.023(5) -0.013(5) C14E 0.065(7) 0.082(8) 0.077(7) -0.030(6) -0.030(6) -0.016(6) C15E 0.043(7) 0.089(9) 0.112(9) -0.014(7) -0.029(7) 0.012(6) C16E 0.047(7) 0.084(8) 0.089(8) -0.020(6) 0.007(6) 0.014(6) C71E 0.082(9) 0.117(10) 0.085(8) -0.053(7) -0.003(7) 0.002(8) C18E 0.062(7) 0.096(8) 0.047(6) -0.021(5) -0.014(5) 0.001(6) C19E 0.028(5) 0.043(6) 0.096(8) -0.007(5) -0.023(5) -0.001(5) C20E 0.048(7) 0.075(8) 0.108(9) 0.004(6) -0.014(7) 0.003(6) C21E 0.072(9) 0.094(10) 0.130(11) 0.007(8) -0.029(8) -0.019(8) C22E 0.079(10) 0.084(10) 0.193(15) -0.016(9) -0.075(10) -0.009(8) C23E 0.082(10) 0.074(9) 0.173(12) 0.012(8) -0.079(9) -0.009(8) C24E 0.067(8) 0.071(8) 0.099(8) 0.022(6) -0.037(7) -0.010(6) C1F 0.049(6) 0.071(7) 0.082(8) -0.021(6) -0.010(6) 0.017(6) C2F 0.241(18) 0.160(13) 0.093(10) -0.012(9) -0.057(11) 0.126(13) C3F 0.27(2) 0.172(16) 0.084(11) -0.019(10) -0.041(12) 0.101(15) C4F 0.130(13) 0.148(14) 0.104(11) 0.005(10) -0.029(10) 0.018(11) C5F 0.074(9) 0.142(12) 0.090(10) 0.049(9) -0.015(8) 0.008(8) C6F 0.065(8) 0.070(8) 0.101(10) 0.008(6) -0.010(7) 0.004(6) C7F 0.080(3) 0.080(3) 0.081(3) -0.0013(10) -0.0162(11) -0.0035(10) C8F 0.103(4) 0.101(4) 0.101(4) -0.0011(10) -0.0204(12) -0.0044(10) C9F 0.130(4) 0.129(4) 0.129(4) -0.0012(10) -0.0257(13) -0.0060(10) C10F 0.129(5) 0.129(5) 0.129(5) -0.0004(10) -0.0258(13) -0.0048(10) C11F 0.174(6) 0.174(6) 0.175(6) -0.0017(10) -0.0345(15) -0.0064(11) C12F 0.138(5) 0.138(5) 0.140(5) -0.0015(10) -0.0269(14) -0.0055(10) C13F 0.054(7) 0.055(7) 0.093(8) -0.003(6) -0.028(6) -0.009(6) C14F 0.074(9) 0.104(10) 0.128(11) 0.036(8) -0.043(8) 0.000(7) C15F 0.088(10) 0.113(11) 0.143(12) 0.024(9) -0.070(10) -0.004(9) C16F 0.065(9) 0.090(10) 0.151(13) -0.001(8) -0.025(10) -0.005(8) C17F 0.048(8) 0.079(9) 0.150(12) 0.001(8) -0.011(8) -0.006(7) C18F 0.045(7) 0.074(8) 0.123(10) 0.007(7) -0.010(7) -0.001(6) C19F 0.051(7) 0.050(6) 0.055(6) -0.008(5) -0.008(5) -0.030(5) C20F 0.058(7) 0.084(8) 0.096(8) -0.008(7) -0.033(7) -0.013(6) C21F 0.077(9) 0.110(10) 0.088(9) -0.031(7) -0.007(8) -0.034(8) C22F 0.080(9) 0.063(7) 0.081(9) 0.001(6) 0.017(7) -0.006(7) C23F 0.056(8) 0.122(10) 0.092(9) -0.012(8) -0.010(7) 0.002(7) C24F 0.050(7) 0.089(8) 0.061(7) -0.003(5) -0.015(6) -0.013(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 S1 Co1 S1 180.00(9) 2_575 . S1 Co1 S2 90.44(9) 2_575 2_575 S1 Co1 S2 89.56(9) . 2_575 S1 Co1 S2 89.56(9) 2_575 . S1 Co1 S2 90.44(9) . . S2 Co1 S2 180.0 2_575 . S3 Co2 S3 180.00(10) 2_665 . S3 Co2 S4 89.73(11) 2_665 . S3 Co2 S4 90.27(11) . . S3 Co2 S4 90.27(11) 2_665 2_665 S3 Co2 S4 89.73(11) . 2_665 S4 Co2 S4 180.0 . 2_665 S7 Co3 S5 88.31(10) . . S7 Co3 S8 90.85(10) . . S5 Co3 S8 171.11(13) . . S7 Co3 S6 174.15(13) . . S5 Co3 S6 91.33(10) . . S8 Co3 S6 90.39(11) . . S9 Co4 S11 87.79(12) . . S9 Co4 S12 174.07(12) . . S11 Co4 S12 91.42(11) . . S9 Co4 S10 90.74(14) . . S11 Co4 S10 176.35(13) . . S12 Co4 S10 90.38(12) . . C19A P1 C13A 109.5(5) . . C19A P1 C7A 110.9(4) . . C13A P1 C7A 106.9(4) . . C19A P1 C1A 107.0(5) . . C13A P1 C1A 113.8(5) . . C7A P1 C1A 108.8(5) . . C7B P2 C1B 107.8(4) . . C7B P2 C19B 107.9(4) . . C1B P2 C19B 112.3(5) . . C7B P2 C13B 113.2(4) . . C1B P2 C13B 108.8(4) . . C19B P2 C13B 107.0(4) . . C13C P3 C1C 110.5(5) . . C13C P3 C19C 108.0(5) . . C1C P3 C19C 110.5(4) . . C13C P3 C7C 110.1(4) . . C1C P3 C7C 108.5(4) . . C19C P3 C7C 109.2(5) . . C19D P4 C7D 108.6(6) . . C19D P4 C13D 110.6(5) . . C7D P4 C13D 110.4(4) . . C19D P4 C1D 111.8(5) . . C7D P4 C1D 107.8(5) . . C13D P4 C1D 107.6(5) . . C1E P5 C7E 109.4(4) . . C1E P5 C13E 108.7(4) . . C7E P5 C13E 113.5(4) . . C1E P5 C19E 108.5(4) . . C7E P5 C19E 107.6(5) . . C13E P5 C19E 109.0(4) . . C7F P6 C13F 106.9(5) . . C7F P6 C19F 108.3(4) . . C13F P6 C19F 108.8(4) . . C7F P6 C1F 112.8(5) . . C13F P6 C1F 110.2(5) . . C19F P6 C1F 109.7(4) . . C1 S1 Co1 106.2(3) . . C2 S2 Co1 105.1(3) . . C8 S3 Co2 105.4(5) . . C9 S4 Co2 104.4(5) . . C15 S5 Co3 104.5(3) . . C16 S6 Co3 104.8(3) . . C22 S7 Co3 105.8(3) . . C23 S8 Co3 104.8(3) . . C29 S9 Co4 104.0(3) . . C30 S10 Co4 106.3(3) . . C37 S11 Co4 105.1(4) . . C36 S12 Co4 104.5(4) . . C6 C1 C2 116.3(8) . . C6 C1 S1 123.9(8) . . C2 C1 S1 119.6(7) . . C3 C2 C1 120.6(8) . . C3 C2 S2 120.7(8) . . C1 C2 S2 118.6(7) . . C2 C3 C4 120.5(9) . . C5 C4 C3 120.1(9) . . C4 C5 C6 118.1(10) . . C5 C6 C1 124.2(9) . . C5 C6 C7 119.6(9) . . C1 C6 C7 116.0(9) . . N1 C7 C6 177.5(14) . . C9 C8 C13 117.7(12) . . C9 C8 S3 120.4(12) . . C13 C8 S3 121.9(12) . . C8 C9 C10 122.0(12) . . C8 C9 S4 119.4(12) . . C10 C9 S4 118.5(12) . . C11 C10 C9 119.9(14) . . C10 C11 C12 118.0(17) . . C13 C12 C11 122.2(16) . . C12 C13 C8 120.2(14) . . C12 C13 C14 122.5(16) . . C8 C13 C14 117.4(14) . . N2 C14 C13 177.9(17) . . C16 C15 C20 119.3(8) . . C16 C15 S5 119.6(7) . . C20 C15 S5 121.1(8) . . C15 C16 C17 118.3(9) . . C15 C16 S6 119.6(7) . . C17 C16 S6 122.1(8) . . C18 C17 C16 119.6(10) . . C19 C18 C17 124.3(11) . . C18 C19 C20 116.2(10) . . C19 C20 C15 122.2(9) . . C19 C20 C21 119.1(10) . . C15 C20 C21 118.7(10) . . N3 C21 C20 174.8(15) . . C23 C22 C27 120.0 . . C23 C22 S7 118.8(4) . . C27 C22 S7 121.2(4) . . C24 C23 C22 120.0 . . C24 C23 S8 120.3(4) . . C22 C23 S8 119.7(4) . . C23 C24 C25 120.0 . . C24 C25 C26 120.0 . . C27 C26 C25 120.0 . . C28 C27 C26 118.4(7) . . C28 C27 C22 121.6(7) . . C26 C27 C22 120.0 . . N4 C28 C27 177.0(12) . . C30 C29 C34 120.0 . . C30 C29 S9 121.4(5) . . C34 C29 S9 118.6(5) . . C29 C30 C31 120.0 . . C29 C30 S10 117.2(5) . . C31 C30 S10 122.8(5) . . C32 C31 C30 120.0 . . C33 C32 C31 120.0 . . C32 C33 C34 120.0 . . C35 C34 C33 116.3(8) . . C35 C34 C29 123.4(8) . . C33 C34 C29 120.0 . . N5 C35 C34 168.2(13) . . C41 C36 C37 118.0(9) . . C41 C36 S12 121.6(8) . . C37 C36 S12 120.4(8) . . C38 C37 C36 120.8(10) . . C38 C37 S11 120.7(9) . . C36 C37 S11 118.5(9) . . C37 C38 C39 120.6(11) . . C38 C39 C40 120.0(11) . . C39 C40 C41 119.3(10) . . C36 C41 C40 121.2(10) . . C36 C41 C42 121.4(10) . . C40 C41 C42 117.4(10) . . N6 C42 C41 178.8(12) . . C2A C1A C6A 119.7(10) . . C2A C1A P1 121.0(8) . . C6A C1A P1 119.2(9) . . C1A C2A C3A 121.4(11) . . C4A C3A C2A 118.8(13) . . C3A C4A C5A 120.3(15) . . C4A C5A C6A 123.0(14) . . C5A C6A C1A 116.6(11) . . C8A C7A C12A 118.7(8) . . C8A C7A P1 120.1(8) . . C12A C7A P1 121.2(8) . . C7A C8A C9A 121.0(10) . . C10A C9A C8A 118.9(11) . . C11A C10A C9A 121.6(11) . . C10A C11A C12A 121.4(10) . . C7A C12A C11A 118.4(10) . . C18A C13A C14A 117.9(10) . . C18A C13A P1 123.0(9) . . C14A C13A P1 119.1(9) . . C15A C14A C13A 120.0(12) . . C16A C15A C14A 120.5(14) . . C15A C16A C17A 121.7(14) . . C16A C17A C18A 119.5(13) . . C13A C18A C17A 120.2(11) . . C20A C19A C24A 116.8(8) . . C20A C19A P1 122.5(7) . . C24A C19A P1 120.7(7) . . C19A C20A C21A 120.4(9) . . C22A C21A C20A 121.2(9) . . C23A C22A C21A 119.3(10) . . C22A C23A C24A 121.3(9) . . C23A C24A C19A 120.9(8) . . C6B C1B C2B 118.6(9) . . C6B C1B P2 118.6(8) . . C2B C1B P2 122.7(9) . . C3B C2B C1B 119.2(10) . . C4B C3B C2B 121.1(12) . . C5B C4B C3B 119.9(11) . . C4B C5B C6B 120.3(12) . . C5B C6B C1B 120.9(10) . . C12B C7B C8B 118.1(8) . . C12B C7B P2 122.4(7) . . C8B C7B P2 119.3(7) . . C7B C8B C9B 121.9(9) . . C10B C9B C8B 119.2(10) . . C9B C10B C11B 120.6(10) . . C10B C11B C12B 120.1(10) . . C7B C12B C11B 120.1(9) . . C14B C13B C18B 119.1(8) . . C14B C13B P2 122.3(7) . . C18B C13B P2 118.6(7) . . C13B C14B C15B 119.0(8) . . C16B C15B C14B 120.3(10) . . C15B C16B C17B 121.5(10) . . C16B C17B C18B 119.3(9) . . C17B C18B C13B 120.7(9) . . C24B C19B C20B 116.9(9) . . C24B C19B P2 122.7(8) . . C20B C19B P2 120.4(7) . . C21B C20B C19B 121.3(8) . . C20B C21B C22B 120.7(9) . . C23B C22B C21B 118.2(10) . . C24B C23B C22B 120.9(9) . . C23B C24B C19B 121.8(9) . . C6C C1C C2C 119.7(9) . . C6C C1C P3 120.3(8) . . C2C C1C P3 120.0(8) . . C3C C2C C1C 118.3(10) . . C4C C3C C2C 121.3(12) . . C3C C4C C5C 120.5(12) . . C4C C5C C6C 119.5(12) . . C1C C6C C5C 120.5(11) . . C12C C7C C8C 120.7(9) . . C12C C7C P3 120.3(8) . . C8C C7C P3 118.9(8) . . C9C C8C C7C 119.4(10) . . C10C C9C C8C 118.8(12) . . C9C C10C C11C 123.3(13) . . C10C C11C C12C 118.7(12) . . C7C C12C C11C 119.2(11) . . C18C C13C C14C 116.9(9) . . C18C C13C P3 120.4(8) . . C14C C13C P3 122.8(8) . . C13C C14C C15C 119.8(10) . . C16C C15C C14C 120.8(11) . . C15C C16C C17C 120.3(12) . . C18C C17C C16C 117.9(11) . . C17C C18C C13C 124.2(10) . . C20C C19C C24C 118.0(10) . . C20C C19C P3 120.5(9) . . C24C C19C P3 121.4(9) . . C19C C20C C21C 119.7(11) . . C22C C21C C20C 118.1(14) . . C23C C22C C21C 125.4(17) . . C22C C23C C24C 118.0(14) . . C23C C24C C19C 120.5(11) . . C6D C1D C2D 119.3(9) . . C6D C1D P4 120.6(8) . . C2D C1D P4 120.0(8) . . C3D C2D C1D 119.6(11) . . C4D C3D C2D 120.0(11) . . C5D C4D C3D 120.8(12) . . C4D C5D C6D 120.7(12) . . C5D C6D C1D 119.4(10) . . C8D C7D C12D 118.7(10) . . C8D C7D P4 121.0(8) . . C12D C7D P4 120.3(9) . . C7D C8D C9D 118.0(10) . . C10D C9D C8D 121.0(12) . . C9D C10D C11D 122.8(14) . . C10D C11D C12D 115.1(13) . . C11D C12D C7D 124.3(13) . . C18D C13D C14D 120.8(10) . . C18D C13D P4 115.7(8) . . C14D C13D P4 123.6(8) . . C13D C14D C15D 118.0(10) . . C16D C15D C14D 119.9(11) . . C17D C16D C15D 121.0(12) . . C16D C17D C18D 122.2(11) . . C17D C18D C13D 118.1(10) . . C20D C19D C24D 118.8(11) . . C20D C19D P4 122.0(11) . . C24D C19D P4 119.2(11) . . C19D C20D C21D 119.9(13) . . C22D C21D C20D 120.5(15) . . C23D C22D C21D 116.4(17) . . C24D C23D C22D 125.3(17) . . C23D C24D C19D 119.1(14) . . C6E C1E C2E 116.8(9) . . C6E C1E P5 121.8(7) . . C2E C1E P5 121.4(8) . . C3E C2E C1E 121.3(10) . . C4E C3E C2E 120.9(11) . . C3E C4E C5E 119.4(10) . . C4E C5E C6E 118.5(10) . . C1E C6E C5E 122.7(9) . . C12E C7E C8E 117.8(8) . . C12E C7E P5 120.5(7) . . C8E C7E P5 121.5(7) . . C9E C8E C7E 120.5(9) . . C10E C9E C8E 118.3(10) . . C11E C10E C9E 124.3(12) . . C10E C11E C12E 119.3(11) . . C7E C12E C11E 119.8(9) . . C18E C13E C14E 118.5(8) . . C18E C13E P5 122.5(7) . . C14E C13E P5 119.0(7) . . C15E C14E C13E 118.2(9) . . C16E C15E C14E 123.4(9) . . C15E C16E C71E 118.4(9) . . C16E C71E C18E 120.8(10) . . C13E C18E C71E 120.5(9) . . C24E C19E C20E 118.7(9) . . C24E C19E P5 123.3(8) . . C20E C19E P5 117.9(8) . . C21E C20E C19E 121.1(10) . . C20E C21E C22E 120.1(12) . . C23E C22E C21E 119.4(12) . . C22E C23E C24E 120.8(11) . . C19E C24E C23E 119.8(10) . . C6F C1F C2F 116.1(10) . . C6F C1F P6 124.2(8) . . C2F C1F P6 119.6(9) . . C1F C2F C3F 122.1(11) . . C4F C3F C2F 119.0(14) . . C3F C4F C5F 121.6(14) . . C4F C5F C6F 118.5(11) . . C1F C6F C5F 122.6(10) . . C8F C7F C12F 117.7(11) . . C8F C7F P6 123.6(8) . . C12F C7F P6 118.3(9) . . C7F C8F C9F 124.2(11) . . C10F C9F C8F 114.8(12) . . C11F C10F C9F 126.1(14) . . C10F C11F C12F 117.9(14) . . C7F C12F C11F 117.5(13) . . C14F C13F C18F 118.8(10) . . C14F C13F P6 120.7(9) . . C18F C13F P6 120.3(9) . . C15F C14F C13F 120.4(12) . . C16F C15F C14F 120.4(13) . . C15F C16F C17F 121.0(13) . . C16F C17F C18F 120.0(12) . . C17F C18F C13F 119.2(11) . . C24F C19F C20F 119.5(9) . . C24F C19F P6 119.4(7) . . C20F C19F P6 121.1(8) . . C21F C20F C19F 120.0(10) . . C20F C21F C22F 120.4(11) . . C21F C22F C23F 120.9(10) . . C22F C23F C24F 118.5(11) . . C19F C24F C23F 120.7(10) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Co1 S1 2.174(2) 2_575 Co1 S1 2.174(2) . Co1 S2 2.185(2) 2_575 Co1 S2 2.185(2) . Co2 S3 2.169(3) 2_665 Co2 S3 2.169(3) . Co2 S4 2.189(3) . Co2 S4 2.189(3) 2_665 Co3 S7 2.170(3) . Co3 S5 2.170(3) . Co3 S8 2.182(3) . Co3 S6 2.184(3) . Co4 S9 2.162(3) . Co4 S11 2.172(3) . Co4 S12 2.175(3) . Co4 S10 2.191(4) . P1 C19A 1.779(8) . P1 C13A 1.785(10) . P1 C7A 1.795(8) . P1 C1A 1.800(10) . P2 C7B 1.766(8) . P2 C1B 1.777(8) . P2 C19B 1.778(9) . P2 C13B 1.782(8) . P3 C13C 1.756(10) . P3 C1C 1.779(8) . P3 C19C 1.789(9) . P3 C7C 1.812(9) . P4 C19D 1.758(11) . P4 C7D 1.790(10) . P4 C13D 1.799(10) . P4 C1D 1.802(9) . P5 C1E 1.751(9) . P5 C7E 1.752(8) . P5 C13E 1.775(8) . P5 C19E 1.804(9) . P6 C7F 1.770(10) . P6 C13F 1.790(10) . P6 C19F 1.801(8) . P6 C1F 1.806(10) . S1 C1 1.726(8) . S2 C2 1.766(9) . S3 C8 1.740(12) . S4 C9 1.767(11) . S5 C15 1.753(8) . S6 C16 1.733(10) . S7 C22 1.746(5) . S8 C23 1.751(5) . S9 C29 1.763(6) . S10 C30 1.724(6) . S11 C37 1.744(10) . S12 C36 1.736(9) . N1 C7 1.140(11) . N2 C14 1.132(15) . N3 C21 1.095(13) . N4 C28 1.172(11) . N5 C35 1.248(13) . N6 C42 1.133(11) . C1 C6 1.391(10) . C1 C2 1.395(11) . C2 C3 1.378(11) . C3 C4 1.397(12) . C4 C5 1.368(12) . C5 C6 1.372(11) . C6 C7 1.452(13) . C8 C9 1.340(12) . C8 C13 1.416(15) . C9 C10 1.415(15) . C10 C11 1.368(16) . C11 C12 1.381(16) . C12 C13 1.358(16) . C13 C14 1.488(17) . C15 C16 1.393(10) . C15 C20 1.410(11) . C16 C17 1.423(11) . C17 C18 1.367(12) . C18 C19 1.362(12) . C19 C20 1.407(12) . C20 C21 1.495(14) . C22 C23 1.3900 . C22 C27 1.3900 . C23 C24 1.3900 . C24 C25 1.3900 . C25 C26 1.3900 . C26 C27 1.3900 . C27 C28 1.365(11) . C29 C30 1.3900 . C29 C34 1.3900 . C30 C31 1.3900 . C31 C32 1.3900 . C32 C33 1.3900 . C33 C34 1.3900 . C34 C35 1.337(11) . C36 C41 1.391(11) . C36 C37 1.400(11) . C37 C38 1.379(13) . C38 C39 1.379(13) . C39 C40 1.382(12) . C40 C41 1.401(13) . C41 C42 1.463(13) . C1A C2A 1.366(12) . C1A C6A 1.390(11) . C2A C3A 1.383(14) . C3A C4A 1.338(14) . C4A C5A 1.347(15) . C5A C6A 1.380(16) . C7A C8A 1.369(12) . C7A C12A 1.393(11) . C8A C9A 1.404(11) . C9A C10A 1.342(13) . C10A C11A 1.327(13) . C11A C12A 1.401(11) . C13A C18A 1.362(13) . C13A C14A 1.404(12) . C14A C15A 1.376(14) . C15A C16A 1.305(17) . C16A C17A 1.360(14) . C17A C18A 1.390(13) . C19A C20A 1.373(10) . C19A C24A 1.406(10) . C20A C21A 1.380(11) . C21A C22A 1.367(11) . C22A C23A 1.327(10) . C23A C24A 1.370(11) . C1B C6B 1.386(12) . C1B C2B 1.390(12) . C2B C3B 1.371(12) . C3B C4B 1.370(14) . C4B C5B 1.350(14) . C5B C6B 1.364(12) . C7B C12B 1.369(11) . C7B C8B 1.373(10) . C8B C9B 1.381(11) . C9B C10B 1.353(13) . C10B C11B 1.359(13) . C11B C12B 1.400(11) . C13B C14B 1.380(11) . C13B C18B 1.403(10) . C14B C15B 1.389(12) . C15B C16B 1.356(11) . C16B C17B 1.362(12) . C17B C18B 1.362(11) . C19B C24B 1.377(10) . C19B C20B 1.398(11) . C20B C21B 1.346(12) . C21B C22B 1.390(11) . C22B C23B 1.369(11) . C23B C24B 1.352(12) . C1C C6C 1.368(13) . C1C C2C 1.391(12) . C2C C3C 1.379(12) . C3C C4C 1.346(15) . C4C C5C 1.360(15) . C5C C6C 1.374(12) . C7C C12C 1.367(11) . C7C C8C 1.393(11) . C8C C9C 1.391(12) . C9C C10C 1.350(14) . C10C C11C 1.353(14) . C11C C12C 1.408(13) . C13C C18C 1.382(12) . C13C C14C 1.391(10) . C14C C15C 1.402(14) . C15C C16C 1.343(13) . C16C C17C 1.403(13) . C17C C18C 1.349(14) . C19C C20C 1.389(12) . C19C C24C 1.403(12) . C20C C21C 1.401(14) . C21C C22C 1.346(17) . C22C C23C 1.301(16) . C23C C24C 1.401(13) . C1D C6D 1.380(11) . C1D C2D 1.393(11) . C2D C3D 1.362(11) . C3D C4D 1.357(13) . C4D C5D 1.352(14) . C5D C6D 1.357(12) . C7D C8D 1.363(12) . C7D C12D 1.380(11) . C8D C9D 1.407(13) . C9D C10D 1.343(14) . C10D C11D 1.371(16) . C11D C12D 1.378(15) . C13D C18D 1.402(12) . C13D C14D 1.405(11) . C14D C15D 1.412(13) . C15D C16D 1.365(13) . C16D C17D 1.348(12) . C17D C18D 1.373(13) . C19D C20D 1.366(14) . C19D C24D 1.408(15) . C20D C21D 1.439(14) . C21D C22D 1.385(18) . C22D C23D 1.360(18) . C23D C24D 1.349(15) . C1E C6E 1.363(11) . C1E C2E 1.381(10) . C2E C3E 1.367(12) . C3E C4E 1.362(13) . C4E C5E 1.376(12) . C5E C6E 1.393(12) . C7E C12E 1.392(11) . C7E C8E 1.409(10) . C8E C9E 1.390(11) . C9E C10E 1.343(14) . C10E C11E 1.317(13) . C11E C12E 1.403(12) . C13E C18E 1.373(11) . C13E C14E 1.411(11) . C14E C15E 1.374(11) . C15E C16E 1.343(13) . C16E C71E 1.369(13) . C71E C18E 1.385(10) . C19E C24E 1.352(10) . C19E C20E 1.386(11) . C20E C21E 1.356(13) . C21E C22E 1.368(13) . C22E C23E 1.348(14) . C23E C24E 1.394(13) . C1F C6F 1.327(11) . C1F C2F 1.379(12) . C2F C3F 1.403(14) . C3F C4F 1.306(14) . C4F C5F 1.351(13) . C5F C6F 1.410(12) . C7F C8F 1.357(11) . C7F C12F 1.419(13) . C8F C9F 1.420(14) . C9F C10F 1.337(13) . C10F C11F 1.332(15) . C11F C12F 1.466(16) . C13F C14F 1.382(12) . C13F C18F 1.414(12) . C14F C15F 1.364(15) . C15F C16F 1.360(14) . C16F C17F 1.363(14) . C17F C18F 1.380(14) . C19F C24F 1.373(11) . C19F C20F 1.381(12) . C20F C21F 1.358(12) . C21F C22F 1.365(14) . C22F C23F 1.374(14) . C23F C24F 1.383(11) .